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Information card for entry 7248495
Preview
| Coordinates | 7248495.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H32 Fe Si3 |
|---|---|
| Calculated formula | C30 H32 Fe Si3 |
| Title of publication | Solvent-free copper-catalyzed trisilylation of alkynes: a practical and atom-economical approach for accessing 1,1,1-trisilylalkanes |
| Authors of publication | Li, Jia; Ge, Shaozhong |
| Journal of publication | Green Chemistry |
| Year of publication | 2024 |
| a | 10.438 ± 0.0003 Å |
| b | 10.4738 ± 0.0003 Å |
| c | 13.8516 ± 0.0004 Å |
| α | 105.82 ± 0.001° |
| β | 109.039 ± 0.001° |
| γ | 96.807 ± 0.001° |
| Cell volume | 1340.97 ± 0.07 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.042 |
| Residual factor for significantly intense reflections | 0.0306 |
| Weighted residual factors for significantly intense reflections | 0.0704 |
| Weighted residual factors for all reflections included in the refinement | 0.0744 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 291302 (current) | 2024-04-20 | cif/ Adding structures of 7248495 via cif-deposit CGI script. |
7248495.cif |
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Users of the data should acknowledge the original authors of the
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