#------------------------------------------------------------------------------
#$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $
#$Revision: 176729 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/90/1519085.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1519085
loop_
_publ_author_name
'Damsgaard, Anders'
'Hazell, Rita'
'Bols, Mikael'
_publ_section_title
;
 Synthesis of Hydroxypiperidinecarboxylic Acids from
 Pyridinedicarboxylates
;
_journal_name_full               'Acta Chemica Scandinavica'
_journal_page_first              521
_journal_page_last               527
_journal_volume                  53
_journal_year                    1999
_chemical_formula_sum            'C7 H5 N O3'
_chemical_formula_weight         151.13
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      33
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.3942(8)
_cell_length_b                   9.5586(8)
_cell_length_c                   6.3382(5)
_cell_volume                     629.73(9)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.127
_exptl_crystal_density_diffrn    1.59
_refine_ls_number_parameters     120
_refine_ls_number_reflns         549
_refine_ls_R_factor_gt           0.027
_refine_ls_wR_factor_gt          0.046
_cod_data_source_file            Acta-Chem-Scand-1999-53-521-527-2.cif
_cod_data_source_block           9
_cod_depositor_comments
;
No atomic coordinates in the paper.
They ware deposited at CSD.
A dummy atom makes illusion
;
_cod_original_cell_volume        629.73
_cod_database_code               1519085
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,-y,1/2+z
3 1/2-x,1/2+y,1/2+z
4 1/2+x,1/2-y,z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_calc_flag
? ? ? ? ? ? ?
