#------------------------------------------------------------------------------
#$Date: 2016-03-21 09:30:05 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178624 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/35/4073533.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4073533
loop_
_publ_author_name
'Beckmann, Jens'
'Heek, Timm'
'Takahashi, Masashi'
_publ_section_title
;
 The First Mixed-Valent Antimony(III/V) Oxo Clusters
 (2,6-Mes2C6H3Sb)2(ClSb)4O8and (2,6-Mes2C6H3Sb)4(ClSb)4(HOSb)2O14†
;
_journal_issue                   15
_journal_name_full               Organometallics
_journal_page_first              3633
_journal_paper_doi               10.1021/om700434m
_journal_volume                  26
_journal_year                    2007
_chemical_formula_sum            'C48 H50 Cl4 O8 Sb6'
_chemical_formula_weight         1627.18
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 100.473(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   8.7910(7)
_cell_length_b                   21.8251(12)
_cell_length_c                   14.2469(11)
_cell_measurement_temperature    200
_cell_volume                     2687.9(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      200
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans with .3 deg in omega'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0612
_diffrn_reflns_av_sigmaI/netI    0.0515
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            11917
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         2.91
_exptl_absorpt_coefficient_mu    3.220
_exptl_absorpt_correction_T_max  1.0
_exptl_absorpt_correction_T_min  0.75
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.010
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1552
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.531
_refine_diff_density_min         -0.883
_refine_diff_density_rms         0.096
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.005
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     368
_refine_ls_number_reflns         4712
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.005
_refine_ls_R_factor_all          0.0532
_refine_ls_R_factor_gt           0.0365
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0470P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0798
_refine_ls_wR_factor_ref         0.0852
_reflns_number_gt                3751
_reflns_number_total             4712
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om700434m-file002.cif
_cod_data_source_block           publication_text
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P21/n
_cod_database_code               4073533
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb 0.89992(3) 0.960555(14) 0.872195(19) 0.02996(10) Uani 1 1 d . . .
C10 C 0.8054(5) 0.9197(2) 0.7387(3) 0.0371(11) Uani 1 1 d . A .
C31 C 1.0526(7) 1.0130(3) 0.6518(3) 0.0492(13) Uani 1 1 d . . .
C15 C 0.8131(6) 0.9525(3) 0.6552(3) 0.0461(12) Uani 1 1 d . . .
C11 C 0.7373(6) 0.8619(2) 0.7385(3) 0.0395(11) Uani 1 1 d . . .
C35 C 0.8141(7) 1.0669(3) 0.6571(5) 0.0640(17) Uani 1 1 d . . .
C30 C 0.8933(6) 1.0122(3) 0.6544(3) 0.0426(12) Uani 1 1 d . A .
C32 C 1.1268(7) 1.0687(3) 0.6568(4) 0.0541(14) Uani 1 1 d . A .
H32 H 1.2321 1.0693 0.6554 0.065 Uiso 1 1 calc R . .
C33 C 1.0535(7) 1.1235(3) 0.6636(4) 0.0578(16) Uani 1 1 d . . .
C14 C 0.7478(9) 0.9244(3) 0.5692(4) 0.075(2) Uani 1 1 d . A .
H14 H 0.7481 0.9450 0.5121 0.090 Uiso 1 1 calc R . .
C20 C 0.7286(6) 0.8271(2) 0.8277(3) 0.0388(11) Uani 1 1 d . A .
C22 C 0.5915(9) 0.8008(4) 0.9520(5) 0.074(2) Uani 1 1 d . A .
H22 H 0.5040 0.8046 0.9797 0.089 Uiso 1 1 calc R . .
C21 C 0.5970(6) 0.8330(3) 0.8679(4) 0.0508(13) Uani 1 1 d . . .
C13 C 0.6837(10) 0.8674(4) 0.5670(4) 0.085(2) Uani 1 1 d . . .
H13 H 0.6428 0.8498 0.5084 0.101 Uiso 1 1 calc R A .
C23 C 0.7093(11) 0.7640(3) 0.9951(5) 0.077(2) Uani 1 1 d . . .
C12 C 0.6784(8) 0.8355(3) 0.6496(4) 0.0637(17) Uani 1 1 d . A .
H12 H 0.6356 0.7965 0.6465 0.076 Uiso 1 1 calc R . .
C24 C 0.8333(11) 0.7585(3) 0.9520(5) 0.083(2) Uani 1 1 d . A .
H24 H 0.9134 0.7328 0.9797 0.099 Uiso 1 1 calc R . .
C26 C 0.4629(8) 0.8715(5) 0.8226(5) 0.095(3) Uani 1 1 d . A .
H26A H 0.3832 0.8698 0.8605 0.142 Uiso 1 1 calc R . .
H26B H 0.4233 0.8563 0.7597 0.142 Uiso 1 1 calc R . .
H26C H 0.4962 0.9132 0.8186 0.142 Uiso 1 1 calc R . .
O1A O 1.0254(7) 0.8894(3) 0.9234(4) 0.0365(14) Uiso 0.50 1 d P A 1
Cl2 Cl 0.58835(15) 0.94437(8) 1.13185(10) 0.0558(4) Uani 1 1 d . . .
C25 C 0.8479(8) 0.7890(3) 0.8693(4) 0.0653(17) Uani 1 1 d . . .
C36 C 1.1401(9) 0.9542(4) 0.6445(6) 0.081(2) Uani 1 1 d . . .
H36A H 1.0705 0.9201 0.6417 0.122 Uiso 1 1 calc R . .
H36B H 1.2209 0.9501 0.6993 0.122 Uiso 1 1 calc R . .
H36C H 1.1845 0.9550 0.5877 0.122 Uiso 1 1 calc R . .
C34 C 0.8968(8) 1.1217(3) 0.6615(6) 0.076(2) Uani 1 1 d . A .
H34 H 0.8437 1.1584 0.6631 0.091 Uiso 1 1 calc R . .
C27 C 0.6966(16) 0.7274(5) 1.0838(6) 0.136(5) Uani 1 1 d . A .
H27A H 0.6006 0.7370 1.1036 0.204 Uiso 1 1 calc R . .
H27B H 0.7812 0.7378 1.1340 0.204 Uiso 1 1 calc R . .
H27C H 0.6999 0.6845 1.0700 0.204 Uiso 1 1 calc R . .
C38 C 0.6428(8) 1.0684(4) 0.6565(10) 0.132(5) Uani 1 1 d . A .
H38A H 0.6093 1.1101 0.6586 0.198 Uiso 1 1 calc R . .
H38B H 0.6209 1.0468 0.7112 0.198 Uiso 1 1 calc R . .
H38C H 0.5891 1.0492 0.5994 0.198 Uiso 1 1 calc R . .
Cl1 Cl 1.24253(18) 0.82081(7) 1.09396(13) 0.0692(4) Uani 1 1 d . . .
C37 C 1.1411(11) 1.1827(4) 0.6720(6) 0.095(3) Uani 1 1 d . A .
H37A H 1.0713 1.2160 0.6760 0.142 Uiso 1 1 calc R . .
H37B H 1.1886 1.1881 0.6170 0.142 Uiso 1 1 calc R . .
H37C H 1.2196 1.1820 0.7285 0.142 Uiso 1 1 calc R . .
C28 C 0.9901(11) 0.7795(5) 0.8237(7) 0.128(4) Uani 1 1 d . A .
H28A H 0.9806 0.8037 0.7667 0.192 Uiso 1 1 calc R . .
H28B H 0.9984 0.7370 0.8080 0.192 Uiso 1 1 calc R . .
H28C H 1.0810 0.7918 0.8678 0.192 Uiso 1 1 calc R . .
O1B O 1.0268(7) 0.9165(3) 0.9818(4) 0.0355(14) Uiso 0.50 1 d P A -1
O2B O 0.7992(8) 0.9561(3) 0.9773(4) 0.0359(14) Uiso 0.50 1 d P A -1
O2A O 0.7334(8) 0.9459(3) 0.9501(5) 0.0361(15) Uiso 0.50 1 d P A 1
Sb2A Sb 1.22988(14) 0.91347(6) 0.99442(10) 0.0301(3) Uani 0.30 1 d P . 1
Sb2B Sb 1.25148(14) 0.92499(6) 1.03725(10) 0.0290(3) Uani 0.30 1 d P . -1
Sb2D Sb 1.0274(2) 0.89355(8) 1.10930(14) 0.0325(4) Uani 0.20 1 d P . -1
Sb2C Sb 1.0055(2) 0.87905(8) 1.05922(15) 0.0344(4) Uani 0.20 1 d P A 1
Sb3A Sb 0.8251(4) 0.91619(19) 1.0840(2) 0.0298(5) Uani 0.30 1 d P A 1
Sb3B Sb 0.8549(4) 0.92517(18) 1.1073(2) 0.0291(5) Uani 0.30 1 d P . -1
Sb3D Sb 0.7225(14) 1.0201(6) 1.0485(7) 0.0405(16) Uani 0.20 1 d P A -1
Sb3C Sb 0.7009(14) 1.0157(5) 1.0281(7) 0.0344(12) Uani 0.20 1 d P . 1
O3B O 1.1948(8) 0.9599(3) 1.1534(5) 0.0347(14) Uani 0.50 1 d P . -1
O3A O 1.1343(8) 0.9522(3) 1.0933(5) 0.0333(14) Uani 0.50 1 d P . 1
O4B O 0.9039(13) 1.0100(5) 1.1517(6) 0.035(2) Uani 0.50 1 d P . -1
O4A O 0.9003(13) 0.9988(5) 1.1128(6) 0.035(2) Uani 0.50 1 d P . 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2B Sb1 O4B 136.5(3) . 3_777
O2B Sb1 O3B 87.0(3) . 3_777
O4B Sb1 O3B 92.1(4) 3_777 3_777
O2B Sb1 O4A 118.9(3) . 3_777
O4B Sb1 O4A 17.9(2) 3_777 3_777
O3B Sb1 O4A 87.8(4) 3_777 3_777
O2B Sb1 O1A 88.7(3) . .
O4B Sb1 O1A 82.5(4) 3_777 .
O3B Sb1 O1A 166.7(3) 3_777 .
O4A Sb1 O1A 83.4(4) 3_777 .
O2B Sb1 O1B 68.1(3) . .
O4B Sb1 O1B 84.7(4) 3_777 .
O3B Sb1 O1B 137.9(3) 3_777 .
O4A Sb1 O1B 76.6(4) 3_777 .
O1A Sb1 O1B 29.8(2) . .
O2B Sb1 O3A 74.9(3) . 3_777
O4B Sb1 O3A 84.6(4) 3_777 3_777
O3B Sb1 O3A 27.5(2) 3_777 3_777
O4A Sb1 O3A 73.3(4) 3_777 3_777
O1A Sb1 O3A 139.3(3) . 3_777
O1B Sb1 O3A 110.7(3) . 3_777
O2B Sb1 O2A 19.5(2) . .
O4B Sb1 O2A 155.8(3) 3_777 .
O3B Sb1 O2A 85.1(3) 3_777 .
O4A Sb1 O2A 138.0(3) 3_777 .
O1A Sb1 O2A 94.9(3) . .
O1B Sb1 O2A 81.5(3) . .
O3A Sb1 O2A 81.9(3) 3_777 .
O2B Sb1 C10 121.8(3) . .
O4B Sb1 C10 101.4(3) 3_777 .
O3B Sb1 C10 97.1(2) 3_777 .
O4A Sb1 C10 119.2(3) 3_777 .
O1A Sb1 C10 95.9(2) . .
O1B Sb1 C10 124.7(2) . .
O3A Sb1 C10 124.5(2) 3_777 .
O2A Sb1 C10 102.8(2) . .
O2B Sb1 Sb2C 54.1(2) . .
O4B Sb1 Sb2C 101.5(3) 3_777 .
O3B Sb1 Sb2C 135.0(2) 3_777 .
O4A Sb1 Sb2C 92.4(3) 3_777 .
O1A Sb1 Sb2C 36.23(19) . .
O1B Sb1 Sb2C 16.82(19) . .
O3A Sb1 Sb2C 110.98(19) 3_777 .
O2A Sb1 Sb2C 65.36(19) . .
C10 Sb1 Sb2C 121.25(14) . .
O2B Sb1 Sb2B 55.2(2) . 3_777
O4B Sb1 Sb2B 105.2(3) 3_777 3_777
O3B Sb1 Sb2B 34.9(2) 3_777 3_777
O4A Sb1 Sb2B 91.9(3) 3_777 3_777
O1A Sb1 Sb2B 135.31(18) . 3_777
O1B Sb1 Sb2B 105.94(19) . 3_777
O3A Sb1 Sb2B 21.50(18) 3_777 3_777
O2A Sb1 Sb2B 60.43(19) . 3_777
C10 Sb1 Sb2B 124.21(13) . 3_777
Sb2C Sb1 Sb2B 100.18(4) . 3_777
O2B Sb1 Sb2D 95.8(2) . 3_777
O4B Sb1 Sb2D 61.3(4) 3_777 3_777
O3B Sb1 Sb2D 37.4(2) 3_777 3_777
O4A Sb1 Sb2D 52.0(3) 3_777 3_777
O1A Sb1 Sb2D 130.92(19) . 3_777
O1B Sb1 Sb2D 109.60(19) . 3_777
O3A Sb1 Sb2D 23.72(19) 3_777 3_777
O2A Sb1 Sb2D 105.2(2) . 3_777
C10 Sb1 Sb2D 121.48(14) . 3_777
Sb2C Sb1 Sb2D 117.04(3) . 3_777
Sb2B Sb1 Sb2D 45.12(4) 3_777 3_777
C11 C10 C15 123.2(4) . .
C11 C10 Sb1 118.6(3) . .
C15 C10 Sb1 118.3(4) . .
C32 C31 C30 118.2(6) . .
C32 C31 C36 120.9(6) . .
C30 C31 C36 120.9(6) . .
C14 C15 C10 116.3(5) . .
C14 C15 C30 120.0(5) . .
C10 C15 C30 123.5(4) . .
C10 C11 C12 117.4(5) . .
C10 C11 C20 123.0(4) . .
C12 C11 C20 119.6(5) . .
C30 C35 C34 118.6(6) . .
C30 C35 C38 121.7(6) . .
C34 C35 C38 119.6(7) . .
C35 C30 C31 119.8(5) . .
C35 C30 C15 120.9(5) . .
C31 C30 C15 119.2(5) . .
C33 C32 C31 123.4(5) . .
C32 C33 C34 117.2(6) . .
C32 C33 C37 121.1(7) . .
C34 C33 C37 121.7(7) . .
C13 C14 C15 121.6(6) . .
C25 C20 C21 120.2(5) . .
C25 C20 C11 121.1(5) . .
C21 C20 C11 118.7(5) . .
C23 C22 C21 122.7(7) . .
C20 C21 C22 117.9(6) . .
C20 C21 C26 121.7(5) . .
C22 C21 C26 120.4(6) . .
C14 C13 C12 121.3(5) . .
C24 C23 C22 117.2(6) . .
C24 C23 C27 121.4(9) . .
C22 C23 C27 121.3(10) . .
C13 C12 C11 120.1(6) . .
C23 C24 C25 123.6(7) . .
O1B O1A Sb2A 63.3(5) . .
O1B O1A Sb1 76.5(5) . .
Sb2A O1A Sb1 112.2(3) . .
O1B O1A Sb2C 42.4(4) . .
Sb2A O1A Sb2C 76.3(2) . .
Sb1 O1A Sb2C 107.9(3) . .
O1B O1A Sb2B 52.3(4) . .
Sb2A O1A Sb2B 11.53(7) . .
Sb1 O1A Sb2B 109.1(3) . .
Sb2C O1A Sb2B 66.20(18) . .
Sb3A Cl2 Sb3D 61.0(3) . .
Sb3A Cl2 Sb3B 10.00(9) . .
Sb3D Cl2 Sb3B 59.6(3) . .
Sb3A Cl2 Sb3C 61.8(3) . .
Sb3D Cl2 Sb3C 7.7(4) . .
Sb3B Cl2 Sb3C 61.9(3) . .
C24 C25 C20 118.3(7) . .
C24 C25 C28 120.6(7) . .
C20 C25 C28 121.1(6) . .
C33 C34 C35 122.5(7) . .
Sb2C Cl1 Sb2B 61.05(6) . .
Sb2C Cl1 Sb2A 60.15(6) . .
Sb2B Cl1 Sb2A 15.40(3) . .
Sb2C Cl1 Sb2D 17.91(4) . .
Sb2B Cl1 Sb2D 60.34(6) . .
Sb2A Cl1 Sb2D 64.81(6) . .
O1A O1B Sb2C 108.5(6) . .
O1A O1B Sb2A 85.6(5) . .
Sb2C O1B Sb2A 100.0(3) . .
O1A O1B Sb2D 129.0(6) . .
Sb2C O1B Sb2D 21.62(13) . .
Sb2A O1B Sb2D 93.8(3) . .
O1A O1B Sb1 73.7(5) . .
Sb2C O1B Sb1 139.1(4) . .
Sb2A O1B Sb1 120.7(3) . .
Sb2D O1B Sb1 141.9(4) . .
O1A O1B Sb2B 103.9(6) . .
Sb2C O1B Sb2B 90.4(3) . .
Sb2A O1B Sb2B 18.75(7) . .
Sb2D O1B Sb2B 79.3(2) . .
Sb1 O1B Sb2B 129.6(3) . .
O1A O1B Sb3A 124.8(6) . .
Sb2C O1B Sb3A 48.1(2) . .
Sb2A O1B Sb3A 139.1(3) . .
Sb2D O1B Sb3A 46.57(17) . .
Sb1 O1B Sb3A 95.9(3) . .
Sb2B O1B Sb3A 121.7(3) . .
O1A O1B Sb3B 134.0(6) . .
Sb2C O1B Sb3B 46.8(2) . .
Sb2A O1B Sb3B 130.5(3) . .
Sb2D O1B Sb3B 40.64(16) . .
Sb1 O1B Sb3B 101.2(3) . .
Sb2B O1B Sb3B 112.6(3) . .
Sb3A O1B Sb3B 9.71(9) . .
O2A O2B Sb3A 107.6(10) . .
O2A O2B Sb3C 92.5(10) . .
Sb3A O2B Sb3C 90.3(5) . .
O2A O2B Sb1 92.2(9) . .
Sb3A O2B Sb1 136.2(4) . .
Sb3C O2B Sb1 128.3(6) . .
O2A O2B Sb3D 101.3(10) . .
Sb3A O2B Sb3D 84.5(5) . .
Sb3C O2B Sb3D 9.4(5) . .
Sb1 O2B Sb3D 130.3(6) . .
O2A O2B Sb3B 118.3(10) . .
Sb3A O2B Sb3B 11.61(18) . .
Sb3C O2B Sb3B 85.6(4) . .
Sb1 O2B Sb3B 134.7(4) . .
Sb3D O2B Sb3B 78.5(4) . .
O2B O2A Sb3C 67.2(9) . .
O2B O2A Sb1 68.3(8) . .
Sb3C O2A Sb1 112.9(5) . .
O2B O2A Sb3A 54.1(8) . .
Sb3C O2A Sb3A 77.7(4) . .
Sb1 O2A Sb3A 111.3(4) . .
O2B O2A Sb3D 60.9(9) . .
Sb3C O2A Sb3D 7.0(5) . .
Sb1 O2A Sb3D 111.2(5) . .
Sb3A O2A Sb3D 71.8(4) . .
O2B O2A Sb3B 47.0(8) . .
Sb3C O2A Sb3B 72.1(4) . .
Sb1 O2A Sb3B 107.9(3) . .
Sb3A O2A Sb3B 7.95(18) . .
Sb3D O2A Sb3B 65.8(4) . .
Sb2B Sb2A Sb3C 77.0(4) . 3_777
Sb2B Sb2A O1B 101.4(3) . .
Sb3C Sb2A O1B 109.5(4) 3_777 .
Sb2B Sb2A O3A 41.8(3) . .
Sb3C Sb2A O3A 87.6(4) 3_777 .
O1B Sb2A O3A 59.9(3) . .
Sb2B Sb2A O1A 131.6(3) . .
Sb3C Sb2A O1A 117.9(4) 3_777 .
O1B Sb2A O1A 31.1(3) . .
O3A Sb2A O1A 90.8(3) . .
Sb2B Sb2A Sb2C 83.3(2) . .
Sb3C Sb2A Sb2C 133.4(4) 3_777 .
O1B Sb2A Sb2C 34.7(2) . .
O3A Sb2A Sb2C 51.7(2) . .
O1A Sb2A Sb2C 52.19(19) . .
Sb2B Sb2A Cl1 78.7(2) . .
Sb3C Sb2A Cl1 150.4(3) 3_777 .
O1B Sb2A Cl1 91.6(2) . .
O3A Sb2A Cl1 85.45(19) . .
O1A Sb2A Cl1 91.0(2) . .
Sb2C Sb2A Cl1 58.98(6) . .
Sb2B Sb2A O3B 23.4(2) . .
Sb3C Sb2A O3B 85.0(4) 3_777 .
O1B Sb2A O3B 78.0(3) . .
O3A Sb2A O3B 18.7(2) . .
O1A Sb2A O3B 108.4(3) . .
Sb2C Sb2A O3B 63.29(16) . .
Cl1 Sb2A O3B 79.33(15) . .
Sb2B Sb2A Sb2D 66.63(19) . .
Sb3C Sb2A Sb2D 124.2(4) 3_777 .
O1B Sb2A Sb2D 44.9(2) . .
O3A Sb2A Sb2D 37.49(19) . .
O1A Sb2A Sb2D 67.79(19) . .
Sb2C Sb2A Sb2D 16.68(4) . .
Cl1 Sb2A Sb2D 58.47(6) . .
O3B Sb2A Sb2D 46.93(16) . .
Sb2B Sb2A Sb1 117.1(2) . .
Sb3C Sb2A Sb1 85.8(3) 3_777 .
O1B Sb2A Sb1 31.7(2) . .
O3A Sb2A Sb1 78.0(2) . .
O1A Sb2A Sb1 33.90(19) . .
Sb2C Sb2A Sb1 66.32(5) . .
Cl1 Sb2A Sb1 120.57(6) . .
O3B Sb2A Sb1 96.29(15) . .
Sb2D Sb2A Sb1 75.58(5) . .
Sb2A Sb2B O3A 121.7(3) . .
Sb2A Sb2B O3B 149.0(3) . .
O3A Sb2B O3B 27.7(3) . .
Sb2A Sb2B O1B 59.8(3) . .
O3A Sb2B O1B 62.1(3) . .
O3B Sb2B O1B 89.2(3) . .
Sb2A Sb2B Cl1 85.9(2) . .
O3A Sb2B Cl1 97.2(2) . .
O3B Sb2B Cl1 93.13(19) . .
O1B Sb2B Cl1 87.4(2) . .
Sb2A Sb2B O1A 36.8(2) . .
O3A Sb2B O1A 85.8(3) . .
O3B Sb2B O1A 112.4(3) . .
O1B Sb2B O1A 23.8(2) . .
Cl1 Sb2B O1A 81.45(17) . .
Sb2A Sb2B Sb2C 81.3(2) . .
O3A Sb2B Sb2C 53.2(2) . .
O3B Sb2B Sb2C 71.8(2) . .
O1B Sb2B Sb2C 35.14(18) . .
Cl1 Sb2B Sb2C 59.38(6) . .
O1A Sb2B Sb2C 47.77(16) . .
Sb2A Sb2B Sb2D 99.3(2) . .
O3A Sb2B Sb2D 39.8(2) . .
O3B Sb2B Sb2D 54.3(2) . .
O1B Sb2B Sb2D 48.33(18) . .
Cl1 Sb2B Sb2D 61.63(6) . .
O1A Sb2B Sb2D 64.93(16) . .
Sb2C Sb2B Sb2D 18.01(4) . .
Sb2A Sb2B Sb1 127.0(2) . 3_777
O3A Sb2B Sb1 28.6(2) . 3_777
O3B Sb2B Sb1 34.21(18) . 3_777
O1B Sb2B Sb1 77.23(19) . 3_777
Cl1 Sb2B Sb1 123.80(7) . 3_777
O1A Sb2B Sb1 99.62(16) . 3_777
Sb2C Sb2B Sb1 80.06(6) . 3_777
Sb2D Sb2B Sb1 68.28(6) . 3_777
Sb2C Sb2D O3A 104.3(3) . .
Sb2C Sb2D Sb3B 94.6(2) . .
O3A Sb2D Sb3B 102.7(3) . .
Sb2C Sb2D Sb3A 81.8(2) . .
O3A Sb2D Sb3A 109.1(3) . .
Sb3B Sb2D Sb3A 13.27(16) . .
Sb2C Sb2D O1B 42.4(3) . .
O3A Sb2D O1B 63.7(3) . .
Sb3B Sb2D O1B 91.8(2) . .
Sb3A Sb2D O1B 84.6(2) . .
Sb2C Sb2D O3B 127.5(3) . .
O3A Sb2D O3B 25.8(2) . .
Sb3B Sb2D O3B 108.0(2) . .
Sb3A Sb2D O3B 119.0(2) . .
O1B Sb2D O3B 89.1(3) . .
Sb2C Sb2D Sb2B 79.3(2) . .
O3A Sb2D Sb2B 37.0(2) . .
Sb3B Sb2D Sb2B 132.06(17) . .
Sb3A Sb2D Sb2B 131.73(16) . .
O1B Sb2D Sb2B 52.40(19) . .
O3B Sb2D Sb2B 50.18(19) . .
Sb2C Sb2D Cl1 74.1(2) . .
O3A Sb2D Cl1 91.3(2) . .
Sb3B Sb2D Cl1 164.01(16) . .
Sb3A Sb2D Cl1 151.72(15) . .
O1B Sb2D Cl1 87.4(2) . .
O3B Sb2D Cl1 87.90(19) . .
Sb2B Sb2D Cl1 58.03(6) . .
Sb2C Sb2D O4A 110.4(3) . .
O3A Sb2D O4A 64.0(3) . .
Sb3B Sb2D O4A 39.4(3) . .
Sb3A Sb2D O4A 49.1(3) . .
O1B Sb2D O4A 81.7(3) . .
O3B Sb2D O4A 69.9(3) . .
Sb2B Sb2D O4A 98.2(3) . .
Cl1 Sb2D O4A 155.3(3) . .
Sb2C Sb2D Sb2A 65.27(19) . .
O3A Sb2D Sb2A 47.0(2) . .
Sb3B Sb2D Sb2A 129.17(17) . .
Sb3A Sb2D Sb2A 124.96(15) . .
O1B Sb2D Sb2A 41.32(19) . .
O3B Sb2D Sb2A 63.66(19) . .
Sb2B Sb2D Sb2A 14.05(3) . .
Cl1 Sb2D Sb2A 56.72(6) . .
O4A Sb2D Sb2A 102.0(3) . .
Sb2C Sb2D Sb1 119.3(2) . 3_777
O3A Sb2D Sb1 29.6(2) . 3_777
Sb3B Sb2D Sb1 76.11(14) . 3_777
Sb3A Sb2D Sb1 85.45(13) . 3_777
O1B Sb2D Sb1 77.5(2) . 3_777
O3B Sb2D Sb1 34.39(18) . 3_777
Sb2B Sb2D Sb1 66.59(5) . 3_777
Cl1 Sb2D Sb1 119.13(7) . 3_777
O4A Sb2D Sb1 36.7(3) . 3_777
Sb2A Sb2D Sb1 75.30(5) . 3_777
Sb2D Sb2C O1B 116.0(3) . .
Sb2D Sb2C Sb3A 74.1(2) . .
O1B Sb2C Sb3A 97.7(3) . .
Sb2D Sb2C Sb3B 61.3(2) . .
O1B Sb2C Sb3B 100.2(3) . .
Sb3A Sb2C Sb3B 13.15(11) . .
Sb2D Sb2C O3A 53.4(3) . .
O1B Sb2C O3A 64.6(3) . .
Sb3A Sb2C O3A 94.1(2) . .
Sb3B Sb2C O3A 83.6(2) . .
Sb2D Sb2C O1A 143.3(3) . .
O1B Sb2C O1A 29.1(3) . .
Sb3A Sb2C O1A 111.3(2) . .
Sb3B Sb2C O1A 119.0(2) . .
O3A Sb2C O1A 90.0(3) . .
Sb2D Sb2C Cl1 88.0(2) . .
O1B Sb2C Cl1 103.4(3) . .
Sb3A Sb2C Cl1 156.79(16) . .
Sb3B Sb2C Cl1 147.38(15) . .
O3A Sb2C Cl1 86.6(2) . .
O1A Sb2C Cl1 91.9(2) . .
Sb2D Sb2C Sb2A 98.0(2) . .
O1B Sb2C Sb2A 45.3(3) . .
Sb3A Sb2C Sb2A 135.11(16) . .
Sb3B Sb2C Sb2A 129.85(15) . .
O3A Sb2C Sb2A 51.3(2) . .
O1A Sb2C Sb2A 51.46(19) . .
Cl1 Sb2C Sb2A 60.87(6) . .
Sb2D Sb2C Sb2B 82.7(2) . .
O1B Sb2C Sb2B 54.5(2) . .
Sb3A Sb2C Sb2B 130.07(15) . .
Sb3B Sb2C Sb2B 121.37(14) . .
O3A Sb2C Sb2B 38.6(2) . .
O1A Sb2C Sb2B 66.03(19) . .
Cl1 Sb2C Sb2B 59.57(6) . .
Sb2A Sb2C Sb2B 15.37(3) . .
Sb2D Sb2C Sb1 121.9(2) . .
O1B Sb2C Sb1 24.1(2) . .
Sb3A Sb2C Sb1 77.82(13) . .
Sb3B Sb2C Sb1 83.66(13) . .
O3A Sb2C Sb1 79.7(2) . .
O1A Sb2C Sb1 35.83(19) . .
Cl1 Sb2C Sb1 124.93(8) . .
Sb2A Sb2C Sb1 69.27(5) . .
Sb2B Sb2C Sb1 78.20(5) . .
O2B Sb3A Sb2D 106.1(3) . .
O2B Sb3A Sb2C 91.8(3) . .
Sb2D Sb3A Sb2C 24.12(8) . .
O2B Sb3A O4A 72.7(4) . .
Sb2D Sb3A O4A 85.8(4) . .
Sb2C Sb3A O4A 100.1(4) . .
O2B Sb3A O2A 18.3(3) . .
Sb2D Sb3A O2A 118.6(3) . .
Sb2C Sb3A O2A 99.5(3) . .
O4A Sb3A O2A 87.9(4) . .
O2B Sb3A O4B 84.4(4) . .
Sb2D Sb3A O4B 87.1(3) . .
Sb2C Sb3A O4B 105.2(3) . .
O4A Sb3A O4B 12.7(4) . .
O2A Sb3A O4B 98.4(4) . .
O2B Sb3A Cl2 98.0(3) . .
Sb2D Sb3A Cl2 152.46(19) . .
Sb2C Sb3A Cl2 168.3(2) . .
O4A Sb3A Cl2 88.9(4) . .
O2A Sb3A Cl2 88.2(2) . .
O4B Sb3A Cl2 82.1(3) . .
O2B Sb3A Sb3D 51.0(4) . .
Sb2D Sb3A Sb3D 126.9(4) . .
Sb2C Sb3A Sb3D 130.7(4) . .
O4A Sb3A Sb3D 44.3(4) . .
O2A Sb3A Sb3D 56.3(3) . .
O4B Sb3A Sb3D 48.8(4) . .
Cl2 Sb3A Sb3D 61.0(4) . .
O2B Sb3A O1B 58.6(3) . .
Sb2D Sb3A O1B 48.84(18) . .
Sb2C Sb3A O1B 34.19(17) . .
O4A Sb3A O1B 82.5(4) . .
O2A Sb3A O1B 69.7(3) . .
O4B Sb3A O1B 92.9(3) . .
Cl2 Sb3A O1B 156.5(2) . .
Sb3D Sb3A O1B 98.7(4) . .
O2B Sb3A Sb3C 45.7(4) . .
Sb2D Sb3A Sb3C 131.0(4) . .
Sb2C Sb3A Sb3C 130.8(4) . .
O4A Sb3A Sb3C 51.0(4) . .
O2A Sb3A Sb3C 49.3(3) . .
O4B Sb3A Sb3C 56.2(3) . .
Cl2 Sb3A Sb3C 60.9(3) . .
Sb3D Sb3A Sb3C 7.6(4) . .
O1B Sb3A Sb3C 97.3(4) . .
O4A Sb3B Sb2D 101.0(4) . .
O4A Sb3B Sb2C 110.8(4) . .
Sb2D Sb3B Sb2C 24.06(9) . .
O4A Sb3B O2B 74.0(4) . .
Sb2D Sb3B O2B 103.3(3) . .
Sb2C Sb3B O2B 84.9(3) . .
O4A Sb3B O4B 16.1(4) . .
Sb2D Sb3B O4B 103.8(4) . .
Sb2C Sb3B O4B 119.3(4) . .
O2B Sb3B O4B 89.0(4) . .
O4A Sb3B O2A 85.5(4) . .
Sb2D Sb3B O2A 110.6(3) . .
Sb2C Sb3B O2A 89.1(2) . .
O2B Sb3B O2A 14.6(2) . .
O4B Sb3B O2A 99.2(4) . .
O4A Sb3B Sb3D 44.8(5) . .
Sb2D Sb3B Sb3D 137.1(4) . .
Sb2C Sb3B Sb3D 130.4(4) . .
O2B Sb3B Sb3D 50.2(3) . .
O4B Sb3B Sb3D 51.7(4) . .
O2A Sb3B Sb3D 53.4(3) . .
O4A Sb3B Cl2 93.2(4) . .
Sb2D Sb3B Cl2 162.9(2) . .
Sb2C Sb3B Cl2 152.70(16) . .
O2B Sb3B Cl2 89.7(2) . .
O4B Sb3B Cl2 87.3(4) . .
O2A Sb3B Cl2 79.8(2) . .
Sb3D Sb3B Cl2 60.0(4) . .
O4A Sb3B Sb3C 51.0(4) . .
Sb2D Sb3B Sb3C 137.8(4) . .
Sb2C Sb3B Sb3C 127.3(3) . .
O2B Sb3B Sb3C 44.5(3) . .
O4B Sb3B Sb3C 58.8(4) . .
O2A Sb3B Sb3C 46.5(3) . .
Sb3D Sb3B Sb3C 7.3(4) . .
Cl2 Sb3B Sb3C 59.2(3) . .
O4A Sb3B O1B 86.3(4) . .
Sb2D Sb3B O1B 47.59(18) . .
Sb2C Sb3B O1B 33.05(17) . .
O2B Sb3B O1B 55.7(3) . .
O4B Sb3B O1B 99.9(4) . .
O2A Sb3B O1B 64.5(2) . .
Sb3D Sb3B O1B 97.4(4) . .
Cl2 Sb3B O1B 144.22(19) . .
Sb3C Sb3B O1B 94.7(3) . .
O4A Sb3B O3A 63.5(4) . .
Sb2D Sb3B O3A 38.21(17) . .
Sb2C Sb3B O3A 49.53(18) . .
O2B Sb3B O3A 85.7(3) . .
O4B Sb3B O3A 69.8(4) . .
O2A Sb3B O3A 99.0(3) . .
Sb3D Sb3B O3A 100.4(4) . .
Cl2 Sb3B O3A 156.7(2) . .
Sb3C Sb3B O3A 103.1(4) . .
O1B Sb3B O3A 42.7(2) . .
O4A Sb3B Sb1 26.7(4) . 3_777
Sb2D Sb3B Sb1 74.38(14) . 3_777
Sb2C Sb3B Sb1 86.83(14) . 3_777
O2B Sb3B Sb1 82.4(3) . 3_777
O4B Sb3B Sb1 32.6(3) . 3_777
O2A Sb3B Sb1 96.7(2) . 3_777
Sb3D Sb3B Sb1 69.5(3) . 3_777
Cl2 Sb3B Sb1 119.00(15) . 3_777
Sb3C Sb3B Sb1 74.7(3) . 3_777
O1B Sb3B Sb1 69.79(17) . 3_777
O3A Sb3B Sb1 37.69(15) . 3_777
O4A Sb3D O2B 73.3(6) . .
O4A Sb3D O4B 17.1(4) . .
O2B Sb3D O4B 89.9(6) . .
O4A Sb3D O2A 90.0(6) . .
O2B Sb3D O2A 17.8(2) . .
O4B Sb3D O2A 106.0(7) . .
O4A Sb3D Sb3B 42.5(5) . .
O2B Sb3D Sb3B 51.3(4) . .
O4B Sb3D Sb3B 51.8(4) . .
O2A Sb3D Sb3B 60.8(4) . .
O4A Sb3D Cl2 91.8(6) . .
O2B Sb3D Cl2 90.7(6) . .
O4B Sb3D Cl2 87.6(5) . .
O2A Sb3D Cl2 83.8(5) . .
Sb3B Sb3D Cl2 60.4(3) . .
O4A Sb3D Sb3A 51.7(5) . .
O2B Sb3D Sb3A 44.5(3) . .
O4B Sb3D Sb3A 61.8(5) . .
O2A Sb3D Sb3A 51.9(3) . .
Sb3B Sb3D Sb3A 10.07(10) . .
Cl2 Sb3D Sb3A 58.0(3) . .
Sb2A Sb3C O2B 111.5(8) 3_777 .
Sb2A Sb3C O2A 120.5(7) 3_777 .
O2B Sb3C O2A 20.3(3) . .
Sb2A Sb3C O4A 88.6(6) 3_777 .
O2B Sb3C O4A 70.8(5) . .
O2A Sb3C O4A 89.8(6) . .
Sb2A Sb3C O4B 86.5(5) 3_777 .
O2B Sb3C O4B 84.6(5) . .
O2A Sb3C O4B 103.0(6) . .
O4A Sb3C O4B 14.2(4) . .
Sb2A Sb3C Cl2 150.9(6) 3_777 .
O2B Sb3C Cl2 93.4(5) . .
O2A Sb3C Cl2 88.0(5) . .
O4A Sb3C Cl2 85.7(5) . .
O4B Sb3C Cl2 81.1(4) . .
Sb2A Sb3C Sb3A 134.1(6) 3_777 .
O2B Sb3C Sb3A 43.9(3) . .
O2A Sb3C Sb3A 53.0(3) . .
O4A Sb3C Sb3A 49.8(4) . .
O4B Sb3C Sb3A 57.9(4) . .
Cl2 Sb3C Sb3A 57.4(3) . .
Sb2A Sb3C Sb3B 127.3(6) 3_777 .
O2B Sb3C Sb3B 49.9(3) . .
O2A Sb3C Sb3B 61.4(4) . .
O4A Sb3C Sb3B 40.7(4) . .
O4B Sb3C Sb3B 48.2(4) . .
Cl2 Sb3C Sb3B 58.9(3) . .
Sb3A Sb3C Sb3B 9.76(9) . .
Sb2A Sb3C O3A 50.2(4) 3_777 3_777
O2B Sb3C O3A 63.1(5) . 3_777
O2A Sb3C O3A 70.4(4) . 3_777
O4A Sb3C O3A 85.1(6) . 3_777
O4B Sb3C O3A 94.5(5) . 3_777
Cl2 Sb3C O3A 156.5(5) . 3_777
Sb3A Sb3C O3A 100.7(5) . 3_777
Sb3B Sb3C O3A 101.1(4) . 3_777
Sb2A Sb3C Sb1 87.3(5) 3_777 .
O2B Sb3C Sb1 26.5(3) . .
O2A Sb3C Sb1 34.3(3) . .
O4A Sb3C Sb1 79.8(5) . .
O4B Sb3C Sb1 93.7(4) . .
Cl2 Sb3C Sb1 119.5(4) . .
Sb3A Sb3C Sb1 69.1(3) . .
Sb3B Sb3C Sb1 73.2(3) . .
O3A Sb3C Sb1 37.4(2) 3_777 .
O3A O3B Sb1 80.5(5) . 3_777
O3A O3B Sb2B 49.5(5) . .
Sb1 O3B Sb2B 110.9(3) 3_777 .
O3A O3B Sb2D 49.2(5) . .
Sb1 O3B Sb2D 108.2(3) 3_777 .
Sb2B O3B Sb2D 75.5(2) . .
O3A O3B Sb2A 42.1(5) . .
Sb1 O3B Sb2A 107.9(3) 3_777 .
Sb2B O3B Sb2A 7.60(7) . .
Sb2D O3B Sb2A 69.4(2) . .
O3B O3A Sb2B 102.8(6) . .
O3B O3A Sb2D 105.0(6) . .
Sb2B O3A Sb2D 103.2(4) . .
O3B O3A Sb2A 119.2(6) . .
Sb2B O3A Sb2A 16.55(10) . .
Sb2D O3A Sb2A 95.5(3) . .
O3B O3A Sb2C 125.2(6) . .
Sb2B O3A Sb2C 88.2(3) . .
Sb2D O3A Sb2C 22.37(11) . .
Sb2A O3A Sb2C 77.0(2) . .
O3B O3A Sb1 72.0(5) . 3_777
Sb2B O3A Sb1 129.9(4) . 3_777
Sb2D O3A Sb1 126.6(4) . 3_777
Sb2A O3A Sb1 133.7(3) . 3_777
Sb2C O3A Sb1 136.6(4) . 3_777
O3B O3A Sb3C 105.8(6) . 3_777
Sb2B O3A Sb3C 40.0(3) . 3_777
Sb2D O3A Sb3C 136.5(4) . 3_777
Sb2A O3A Sb3C 42.2(3) . 3_777
Sb2C O3A Sb3C 115.4(4) . 3_777
Sb1 O3A Sb3C 92.0(3) 3_777 3_777
O3B O3A Sb3B 111.2(6) . .
Sb2B O3A Sb3B 133.9(4) . .
Sb2D O3A Sb3B 39.13(19) . .
Sb2A O3A Sb3B 119.9(3) . .
Sb2C O3A Sb3B 46.91(17) . .
Sb1 O3A Sb3B 90.6(3) 3_777 .
Sb3C O3A Sb3B 141.8(4) 3_777 .
O4A O4B Sb1 82.5(19) . 3_777
O4A O4B Sb3D 57.2(19) . .
Sb1 O4B Sb3D 117.3(6) 3_777 .
O4A O4B Sb3B 49.7(19) . .
Sb1 O4B Sb3B 113.9(6) 3_777 .
Sb3D O4B Sb3B 76.5(5) . .
O4A O4B Sb3C 53.5(19) . .
Sb1 O4B Sb3C 116.5(5) 3_777 .
Sb3D O4B Sb3C 4.0(6) . .
Sb3B O4B Sb3C 73.0(4) . .
O4A O4B Sb3A 45.2(19) . .
Sb1 O4B Sb3A 115.5(5) 3_777 .
Sb3D O4B Sb3A 69.4(5) . .
Sb3B O4B Sb3A 7.20(18) . .
Sb3C O4B Sb3A 65.9(4) . .
O4B O4A Sb3B 114(2) . .
O4B O4A Sb3D 106(2) . .
Sb3B O4A Sb3D 92.8(7) . .
O4B O4A Sb3A 122(2) . .
Sb3B O4A Sb3A 10.4(2) . .
Sb3D O4A Sb3A 84.1(6) . .
O4B O4A Sb1 79.6(19) . 3_777
Sb3B O4A Sb1 130.8(7) . 3_777
Sb3D O4A Sb1 130.5(8) . 3_777
Sb3A O4A Sb1 135.6(6) . 3_777
O4B O4A Sb3C 112(2) . .
Sb3B O4A Sb3C 88.4(6) . .
Sb3D O4A Sb3C 6.8(7) . .
Sb3A O4A Sb3C 79.2(5) . .
Sb1 O4A Sb3C 131.8(7) 3_777 .
O4B O4A Sb2D 116(2) . .
Sb3B O4A Sb2D 39.6(3) . .
Sb3D O4A Sb2D 126.0(6) . .
Sb3A O4A Sb2D 45.1(3) . .
Sb1 O4A Sb2D 91.3(4) 3_777 .
Sb3C O4A Sb2D 119.8(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sb1 O2B 1.875(6) .
Sb1 O4B 1.928(11) 3_777
Sb1 O3B 1.931(6) 3_777
Sb1 O4A 1.944(11) 3_777
Sb1 O1A 1.968(6) .
Sb1 O1B 1.993(6) .
Sb1 O3A 2.002(6) 3_777
Sb1 O2A 2.016(7) .
Sb1 C10 2.128(4) .
Sb1 Sb2C 3.1978(18) .
Sb1 Sb2B 3.2093(14) 3_777
Sb1 Sb2D 3.2489(19) 3_777
C10 C11 1.397(7) .
C10 C15 1.401(7) .
C31 C32 1.376(9) .
C31 C30 1.408(8) .
C31 C36 1.509(9) .
C15 C14 1.397(7) .
C15 C30 1.482(7) .
C11 C12 1.401(7) .
C11 C20 1.494(7) .
C35 C30 1.386(9) .
C35 C34 1.395(9) .
C35 C38 1.505(10) .
C32 C33 1.369(9) .
C33 C34 1.373(9) .
C33 C37 1.498(9) .
C14 C13 1.362(9) .
C20 C25 1.384(8) .
C20 C21 1.387(8) .
C22 C23 1.365(11) .
C22 C21 1.397(9) .
C21 C26 1.495(9) .
C13 C12 1.376(9) .
C23 C24 1.350(12) .
C23 C27 1.515(10) .
C24 C25 1.380(10) .
O1A O1B 1.018(8) .
O1A Sb2A 1.967(6) .
O1A Sb2C 1.987(6) .
O1A Sb2B 2.452(6) .
Cl2 Sb3A 2.385(5) .
Cl2 Sb3D 2.458(15) .
Cl2 Sb3B 2.467(5) .
Cl2 Sb3C 2.473(14) .
C25 C28 1.524(10) .
Cl1 Sb2C 2.414(2) .
Cl1 Sb2B 2.419(2) .
Cl1 Sb2A 2.461(2) .
Cl1 Sb2D 2.509(2) .
O1B Sb2C 1.413(6) .
O1B Sb2A 1.763(6) .
O1B Sb2D 1.884(6) .
O1B Sb2B 1.998(6) .
O1B Sb3A 2.491(8) .
O1B Sb3B 2.550(8) .
O2B O2A 0.673(7) .
O2B Sb3A 1.731(7) .
O2B Sb3C 1.786(13) .
O2B Sb3D 1.920(14) .
O2B Sb3B 1.949(7) .
O2A Sb3C 1.936(12) .
O2A Sb3A 2.038(7) .
O2A Sb3D 2.155(13) .
O2A Sb3B 2.344(7) .
Sb2A Sb2B 0.6554(10) .
Sb2A Sb3C 1.714(13) 3_777
Sb2A O3A 1.958(7) .
Sb2A Sb2C 2.444(2) .
Sb2A O3B 2.550(7) .
Sb2A Sb2D 2.664(2) .
Sb2B O3A 1.533(7) .
Sb2B O3B 1.966(7) .
Sb2B Sb2C 2.455(2) .
Sb2B Sb2D 2.478(2) .
Sb2B Sb1 3.2093(14) 3_777
Sb2D Sb2C 0.7723(18) .
Sb2D O3A 1.629(6) .
Sb2D Sb3B 1.662(5) .
Sb2D Sb3A 1.818(4) .
Sb2D O3B 2.079(7) .
Sb2D O4A 2.559(11) .
Sb2D Sb1 3.2489(19) 3_777
Sb2C Sb3A 1.871(5) .
Sb2C Sb3B 1.888(5) .
Sb2C O3A 1.967(7) .
Sb3A O4A 1.939(12) .
Sb3A O4B 2.316(11) .
Sb3A Sb3D 2.459(14) .
Sb3A Sb3C 2.495(12) .
Sb3B O4A 1.655(12) .
Sb3B O4B 1.979(12) .
Sb3B Sb3D 2.448(13) .
Sb3B Sb3C 2.540(11) .
Sb3B O3A 2.569(7) .
Sb3B Sb1 3.275(3) 3_777
Sb3D O4A 1.726(15) .
Sb3D O4B 1.975(14) .
Sb3C Sb2A 1.714(13) 3_777
Sb3C O4A 1.973(14) .
Sb3C O4B 2.271(13) .
Sb3C O3A 2.548(15) 3_777
O3B O3A 0.937(7) .
O3B Sb1 1.931(6) 3_777
O3A Sb1 2.002(6) 3_777
O3A Sb3C 2.548(15) 3_777
O4B O4A 0.602(8) .
O4B Sb1 1.928(11) 3_777
O4A Sb1 1.944(11) 3_777
