#------------------------------------------------------------------------------
#$Date: 2016-03-25 08:53:21 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179710 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/13/7001341.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7001341
loop_
_publ_author_name
'Wang, Kefeng'
'Shen, Miao'
'Sun, Wen-Hua'
_publ_section_title
;
 Synthesis, characterization and ethylene oligomerization of nickel
 complexes bearing
 N-(2-(1H-benzo[d]imidazol-2-yl)quinolin-8-yl)benzamide derivatives
;
_journal_issue                   21
_journal_name_full               'Dalton Transactions'
_journal_page_first              4085
_journal_page_last               4095
_journal_paper_doi               10.1039/b822441b
_journal_year                    2009
_chemical_formula_sum            'C48 H60 Cl4 N12 Ni2 O4'
_chemical_formula_weight         1128.30
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.40(8)
_cell_angle_beta                 101.03(6)
_cell_angle_gamma                116.31(4)
_cell_formula_units_Z            1
_cell_length_a                   10.186(7)
_cell_length_b                   11.301(10)
_cell_length_c                   13.024(10)
_cell_measurement_reflns_used    3787
_cell_measurement_temperature    83(2)
_cell_measurement_theta_max      27.45
_cell_measurement_theta_min      3.28
_cell_volume                     1279.6(19)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      83(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.978
_diffrn_measured_fraction_theta_max 0.978
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       Multi-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0981
_diffrn_reflns_av_sigmaI/netI    0.1596
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            8480
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.20
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.001
_exptl_absorpt_correction_T_max  0.9360
_exptl_absorpt_correction_T_min  0.8563
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.464
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             588
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.09
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.632
_refine_diff_density_min         -1.187
_refine_diff_density_rms         0.197
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.083
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     316
_refine_ls_number_reflns         4412
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.083
_refine_ls_R_factor_all          0.1874
_refine_ls_R_factor_gt           0.1167
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1500P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2696
_refine_ls_wR_factor_ref         0.3251
_reflns_number_gt                2358
_reflns_number_total             4412
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b822441b.txt
_cod_data_source_block           14a
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1279.7(18)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7001341
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni1 Ni 0.82794(14) 0.83346(12) 0.44253(11) 0.0363(5) Uani 1 1 d . . .
Cl1 Cl 0.9143(3) 1.0543(2) 0.4104(2) 0.0378(7) Uani 1 1 d . . .
Cl2 Cl 0.6063(3) 0.7239(2) 0.2924(2) 0.0389(7) Uani 1 1 d . . .
N1 N 0.7874(9) 0.6580(8) 0.4862(7) 0.035(2) Uani 1 1 d . . .
N2 N 0.9503(9) 0.7658(8) 0.3496(7) 0.038(2) Uani 1 1 d . . .
H2 H 1.0513 0.8169 0.3912 0.046 Uiso 1 1 calc R . .
N3 N 0.7093(9) 0.8339(8) 0.5582(7) 0.037(2) Uani 1 1 d . . .
N4 N 0.6086(10) 0.7347(9) 0.6816(7) 0.043(2) Uani 1 1 d . . .
C1 C 0.8311(11) 0.5752(10) 0.4313(10) 0.042(3) Uani 1 1 d . . .
C2 C 0.9125(11) 0.6259(11) 0.3571(8) 0.035(2) Uani 1 1 d . . .
C3 C 0.9508(12) 0.5440(11) 0.2983(9) 0.043(3) Uani 1 1 d . . .
H3 H 1.0057 0.5767 0.2477 0.052 Uiso 1 1 calc R . .
C4 C 0.9095(12) 0.4083(11) 0.3115(10) 0.049(3) Uani 1 1 d . . .
H4 H 0.9337 0.3509 0.2680 0.059 Uiso 1 1 calc R . .
C5 C 0.8349(11) 0.3622(10) 0.3871(9) 0.040(3) Uani 1 1 d . . .
H5 H 0.8135 0.2750 0.3988 0.048 Uiso 1 1 calc R . .
C6 C 0.7898(12) 0.4431(10) 0.4476(9) 0.041(3) Uani 1 1 d . . .
C7 C 0.7122(12) 0.4074(11) 0.5268(9) 0.045(3) Uani 1 1 d . . .
H7 H 0.6870 0.3217 0.5431 0.054 Uiso 1 1 calc R . .
C8 C 0.6721(12) 0.4922(10) 0.5809(9) 0.039(3) Uani 1 1 d . . .
H8 H 0.6160 0.4636 0.6316 0.046 Uiso 1 1 calc R . .
C9 C 0.7142(11) 0.6227(10) 0.5612(9) 0.036(2) Uani 1 1 d . . .
C10 C 0.6770(10) 0.7300(9) 0.6040(9) 0.034(2) Uani 1 1 d . . .
C11 C 0.5886(11) 0.8490(9) 0.6863(8) 0.033(2) Uani 1 1 d . . .
C12 C 0.5205(12) 0.9026(11) 0.7493(10) 0.047(3) Uani 1 1 d . . .
H12 H 0.4755 0.8595 0.8009 0.056 Uiso 1 1 calc R . .
C13 C 0.5226(11) 1.0205(11) 0.7319(9) 0.042(3) Uani 1 1 d . . .
H13 H 0.4782 1.0598 0.7733 0.051 Uiso 1 1 calc R . .
C14 C 0.5871(12) 1.0853(11) 0.6562(10) 0.047(3) Uani 1 1 d . . .
H14 H 0.5843 1.1662 0.6469 0.056 Uiso 1 1 calc R . .
C15 C 0.6556(11) 1.0332(10) 0.5939(9) 0.040(3) Uani 1 1 d . . .
H15 H 0.6982 1.0769 0.5417 0.047 Uiso 1 1 calc R . .
C16 C 0.6599(11) 0.9134(10) 0.6107(9) 0.039(3) Uani 1 1 d . . .
C17 C 0.5550(12) 0.6356(10) 0.7502(8) 0.043(3) Uani 1 1 d . . .
H17A H 0.5809 0.5631 0.7324 0.064 Uiso 1 1 calc R . .
H17B H 0.4443 0.5960 0.7367 0.064 Uiso 1 1 calc R . .
H17C H 0.6051 0.6830 0.8265 0.064 Uiso 1 1 calc R . .
C18 C 0.9572(13) 0.7926(11) 0.2430(9) 0.049(3) Uani 1 1 d . . .
H18A H 1.0175 0.7562 0.2142 0.074 Uiso 1 1 calc R . .
H18B H 1.0050 0.8910 0.2494 0.074 Uiso 1 1 calc R . .
H18C H 0.8537 0.7486 0.1942 0.074 Uiso 1 1 calc R . .
O1 O 0.9278(10) 0.7540(9) 0.8502(8) 0.071(3) Uani 1 1 d . . .
O2 O 0.3594(12) 0.7253(14) -0.0828(10) 0.127(5) Uani 1 1 d . . .
N5 N 1.1441(11) 0.9545(10) 0.9361(8) 0.053(3) Uani 1 1 d . . .
N6 N 0.2623(13) 0.5917(14) 0.0247(9) 0.079(4) Uani 1 1 d . . .
C19 C 1.0403(14) 0.8597(12) 0.8495(10) 0.053(3) Uani 1 1 d . . .
H19 H 1.0535 0.8743 0.7811 0.063 Uiso 1 1 calc R . .
C20 C 1.2742(15) 1.0728(15) 0.9269(13) 0.085(5) Uani 1 1 d . . .
H20A H 1.2714 1.0674 0.8507 0.127 Uiso 1 1 calc R . .
H20B H 1.3684 1.0761 0.9664 0.127 Uiso 1 1 calc R . .
H20C H 1.2712 1.1552 0.9574 0.127 Uiso 1 1 calc R . .
C21 C 1.1272(14) 0.9402(13) 1.0413(10) 0.062(4) Uani 1 1 d . . .
H21A H 1.0358 0.8546 1.0347 0.092 Uiso 1 1 calc R . .
H21B H 1.1174 1.0166 1.0767 0.092 Uiso 1 1 calc R . .
H21C H 1.2170 0.9397 1.0843 0.092 Uiso 1 1 calc R . .
C22 C 0.2773(18) 0.6994(17) -0.0225(13) 0.081(5) Uani 1 1 d . . .
H22 H 0.2263 0.7500 -0.0085 0.097 Uiso 1 1 calc R . .
C23 C 0.3564(19) 0.5323(18) 0.0058(13) 0.110(7) Uani 1 1 d . . .
H23A H 0.3946 0.5585 -0.0557 0.164 Uiso 1 1 calc R . .
H23B H 0.2964 0.4330 -0.0098 0.164 Uiso 1 1 calc R . .
H23C H 0.4426 0.5648 0.0701 0.164 Uiso 1 1 calc R . .
C24 C 0.1886(17) 0.5738(16) 0.1070(12) 0.088(5) Uani 1 1 d . . .
H24A H 0.1294 0.6226 0.1035 0.132 Uiso 1 1 calc R . .
H24B H 0.2650 0.6097 0.1773 0.132 Uiso 1 1 calc R . .
H24C H 0.1201 0.4767 0.0976 0.132 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Ni1 N3 77.5(3) . . ?
N1 Ni1 N2 79.8(3) . . ?
N3 Ni1 N2 156.9(3) . . ?
N1 Ni1 Cl1 171.0(2) . . ?
N3 Ni1 Cl1 103.6(2) . . ?
N2 Ni1 Cl1 98.1(2) . . ?
N1 Ni1 Cl2 93.0(3) . . ?
N3 Ni1 Cl2 95.1(3) . . ?
N2 Ni1 Cl2 90.3(2) . . ?
Cl1 Ni1 Cl2 95.79(13) . . ?
N1 Ni1 Cl1 86.8(2) . 2_776 ?
N3 Ni1 Cl1 91.8(2) . 2_776 ?
N2 Ni1 Cl1 82.8(2) . 2_776 ?
Cl1 Ni1 Cl1 84.22(12) . 2_776 ?
Cl2 Ni1 Cl1 172.94(10) . 2_776 ?
Ni1 Cl1 Ni1 95.78(12) . 2_776 ?
C9 N1 C1 122.5(9) . . ?
C9 N1 Ni1 120.4(7) . . ?
C1 N1 Ni1 117.1(7) . . ?
C18 N2 C2 115.5(9) . . ?
C18 N2 Ni1 120.9(7) . . ?
C2 N2 Ni1 108.1(6) . . ?
C18 N2 H2 103.3 . . ?
C2 N2 H2 103.3 . . ?
Ni1 N2 H2 103.2 . . ?
C10 N3 C16 105.1(8) . . ?
C10 N3 Ni1 113.7(7) . . ?
C16 N3 Ni1 140.9(7) . . ?
C10 N4 C11 107.4(8) . . ?
C10 N4 C17 128.6(9) . . ?
C11 N4 C17 124.0(9) . . ?
N1 C1 C2 117.2(9) . . ?
N1 C1 C6 120.5(10) . . ?
C2 C1 C6 122.3(10) . . ?
C3 C2 C1 118.5(10) . . ?
C3 C2 N2 124.8(9) . . ?
C1 C2 N2 116.7(9) . . ?
C2 C3 C4 121.0(10) . . ?
C2 C3 H3 119.5 . . ?
C4 C3 H3 119.5 . . ?
C5 C4 C3 119.8(10) . . ?
C5 C4 H4 120.1 . . ?
C3 C4 H4 120.1 . . ?
C4 C5 C6 120.7(10) . . ?
C4 C5 H5 119.7 . . ?
C6 C5 H5 119.7 . . ?
C7 C6 C5 126.2(10) . . ?
C7 C6 C1 116.1(10) . . ?
C5 C6 C1 117.6(10) . . ?
C8 C7 C6 122.1(10) . . ?
C8 C7 H7 119.0 . . ?
C6 C7 H7 119.0 . . ?
C7 C8 C9 119.9(10) . . ?
C7 C8 H8 120.1 . . ?
C9 C8 H8 120.1 . . ?
N1 C9 C8 118.8(9) . . ?
N1 C9 C10 110.6(9) . . ?
C8 C9 C10 130.3(9) . . ?
N3 C10 N4 113.4(9) . . ?
N3 C10 C9 117.6(9) . . ?
N4 C10 C9 129.0(9) . . ?
N4 C11 C12 132.6(9) . . ?
N4 C11 C16 104.4(8) . . ?
C12 C11 C16 122.9(9) . . ?
C13 C12 C11 116.2(10) . . ?
C13 C12 H12 121.9 . . ?
C11 C12 H12 121.9 . . ?
C12 C13 C14 123.0(11) . . ?
C12 C13 H13 118.5 . . ?
C14 C13 H13 118.5 . . ?
C13 C14 C15 121.2(10) . . ?
C13 C14 H14 119.4 . . ?
C15 C14 H14 119.4 . . ?
C14 C15 C16 118.1(10) . . ?
C14 C15 H15 121.0 . . ?
C16 C15 H15 121.0 . . ?
N3 C16 C15 131.6(10) . . ?
N3 C16 C11 109.4(9) . . ?
C15 C16 C11 118.6(10) . . ?
N4 C17 H17A 109.5 . . ?
N4 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
N4 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
N2 C18 H18A 109.5 . . ?
N2 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
N2 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C19 N5 C21 119.7(10) . . ?
C19 N5 C20 121.5(11) . . ?
C21 N5 C20 118.9(11) . . ?
C22 N6 C24 117.4(15) . . ?
C22 N6 C23 116.3(14) . . ?
C24 N6 C23 124.1(14) . . ?
O1 C19 N5 125.6(12) . . ?
O1 C19 H19 117.2 . . ?
N5 C19 H19 117.2 . . ?
N5 C20 H20A 109.5 . . ?
N5 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
N5 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
N5 C21 H21A 109.5 . . ?
N5 C21 H21B 109.5 . . ?
H21A C21 H21B 109.5 . . ?
N5 C21 H21C 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
O2 C22 N6 116.6(17) . . ?
O2 C22 H22 121.7 . . ?
N6 C22 H22 121.7 . . ?
N6 C23 H23A 109.5 . . ?
N6 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
N6 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
N6 C24 H24A 109.5 . . ?
N6 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
N6 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ni1 N1 2.019(8) . ?
Ni1 N3 2.105(8) . ?
Ni1 N2 2.188(9) . ?
Ni1 Cl1 2.375(3) . ?
Ni1 Cl2 2.379(4) . ?
Ni1 Cl1 2.582(4) 2_776 ?
Cl1 Ni1 2.582(4) 2_776 ?
N1 C9 1.337(12) . ?
N1 C1 1.380(12) . ?
N2 C18 1.466(13) . ?
N2 C2 1.474(12) . ?
N2 H2 0.9300 . ?
N3 C10 1.326(12) . ?
N3 C16 1.379(13) . ?
N4 C10 1.341(12) . ?
N4 C11 1.389(13) . ?
N4 C17 1.502(12) . ?
C1 C2 1.406(14) . ?
C1 C6 1.418(14) . ?
C2 C3 1.359(14) . ?
C3 C4 1.444(15) . ?
C3 H3 0.9500 . ?
C4 C5 1.372(15) . ?
C4 H4 0.9500 . ?
C5 C6 1.412(14) . ?
C5 H5 0.9500 . ?
C6 C7 1.410(15) . ?
C7 C8 1.365(14) . ?
C7 H7 0.9500 . ?
C8 C9 1.415(13) . ?
C8 H8 0.9500 . ?
C9 C10 1.496(13) . ?
C11 C12 1.408(14) . ?
C11 C16 1.421(14) . ?
C12 C13 1.372(15) . ?
C12 H12 0.9500 . ?
C13 C14 1.395(14) . ?
C13 H13 0.9500 . ?
C14 C15 1.397(14) . ?
C14 H14 0.9500 . ?
C15 C16 1.417(13) . ?
C15 H15 0.9500 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
O1 C19 1.239(14) . ?
O2 C22 1.223(17) . ?
N5 C19 1.329(14) . ?
N5 C21 1.433(15) . ?
N5 C20 1.446(15) . ?
N6 C22 1.395(18) . ?
N6 C24 1.409(16) . ?
N6 C23 1.431(18) . ?
C19 H19 0.9500 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 H21A 0.9800 . ?
C21 H21B 0.9800 . ?
C21 H21C 0.9800 . ?
C22 H22 0.9500 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1 Ni1 Cl1 Ni1 -5.9(16) . . . 2_776 ?
N3 Ni1 Cl1 Ni1 90.4(3) . . . 2_776 ?
N2 Ni1 Cl1 Ni1 -81.8(2) . . . 2_776 ?
Cl2 Ni1 Cl1 Ni1 -172.91(10) . . . 2_776 ?
Cl1 Ni1 Cl1 Ni1 0.0 2_776 . . 2_776 ?
N3 Ni1 N1 C9 -0.9(8) . . . . ?
N2 Ni1 N1 C9 174.9(8) . . . . ?
Cl1 Ni1 N1 C9 97.6(16) . . . . ?
Cl2 Ni1 N1 C9 -95.4(8) . . . . ?
Cl1 Ni1 N1 C9 91.6(8) 2_776 . . . ?
N3 Ni1 N1 C1 175.7(8) . . . . ?
N2 Ni1 N1 C1 -8.5(7) . . . . ?
Cl1 Ni1 N1 C1 -85.8(18) . . . . ?
Cl2 Ni1 N1 C1 81.2(7) . . . . ?
Cl1 Ni1 N1 C1 -91.7(7) 2_776 . . . ?
N1 Ni1 N2 C18 145.8(8) . . . . ?
N3 Ni1 N2 C18 156.3(8) . . . . ?
Cl1 Ni1 N2 C18 -43.1(7) . . . . ?
Cl2 Ni1 N2 C18 52.8(7) . . . . ?
Cl1 Ni1 N2 C18 -126.2(7) 2_776 . . . ?
N1 Ni1 N2 C2 9.3(6) . . . . ?
N3 Ni1 N2 C2 19.9(11) . . . . ?
Cl1 Ni1 N2 C2 -179.6(6) . . . . ?
Cl2 Ni1 N2 C2 -83.7(6) . . . . ?
Cl1 Ni1 N2 C2 97.3(6) 2_776 . . . ?
N1 Ni1 N3 C10 3.6(7) . . . . ?
N2 Ni1 N3 C10 -7.1(13) . . . . ?
Cl1 Ni1 N3 C10 -167.2(7) . . . . ?
Cl2 Ni1 N3 C10 95.6(7) . . . . ?
Cl1 Ni1 N3 C10 -82.7(7) 2_776 . . . ?
N1 Ni1 N3 C16 177.3(12) . . . . ?
N2 Ni1 N3 C16 166.7(10) . . . . ?
Cl1 Ni1 N3 C16 6.5(12) . . . . ?
Cl2 Ni1 N3 C16 -90.7(11) . . . . ?
Cl1 Ni1 N3 C16 91.0(11) 2_776 . . . ?
C9 N1 C1 C2 -177.7(9) . . . . ?
Ni1 N1 C1 C2 5.7(13) . . . . ?
C9 N1 C1 C6 4.5(16) . . . . ?
Ni1 N1 C1 C6 -172.1(8) . . . . ?
N1 C1 C2 C3 -177.0(9) . . . . ?
C6 C1 C2 C3 0.8(17) . . . . ?
N1 C1 C2 N2 3.2(14) . . . . ?
C6 C1 C2 N2 -179.0(9) . . . . ?
C18 N2 C2 C3 31.7(14) . . . . ?
Ni1 N2 C2 C3 170.8(9) . . . . ?
C18 N2 C2 C1 -148.5(10) . . . . ?
Ni1 N2 C2 C1 -9.4(11) . . . . ?
C1 C2 C3 C4 -0.1(16) . . . . ?
N2 C2 C3 C4 179.7(9) . . . . ?
C2 C3 C4 C5 -2.3(17) . . . . ?
C3 C4 C5 C6 3.9(17) . . . . ?
C4 C5 C6 C7 179.6(11) . . . . ?
C4 C5 C6 C1 -3.1(16) . . . . ?
N1 C1 C6 C7 -4.0(16) . . . . ?
C2 C1 C6 C7 178.3(10) . . . . ?
N1 C1 C6 C5 178.5(10) . . . . ?
C2 C1 C6 C5 0.7(16) . . . . ?
C5 C6 C7 C8 -179.5(11) . . . . ?
C1 C6 C7 C8 3.2(16) . . . . ?
C6 C7 C8 C9 -2.7(17) . . . . ?
C1 N1 C9 C8 -3.7(15) . . . . ?
Ni1 N1 C9 C8 172.7(7) . . . . ?
C1 N1 C9 C10 -178.1(9) . . . . ?
Ni1 N1 C9 C10 -1.6(12) . . . . ?
C7 C8 C9 N1 2.8(16) . . . . ?
C7 C8 C9 C10 175.9(11) . . . . ?
C16 N3 C10 N4 0.8(12) . . . . ?
Ni1 N3 C10 N4 176.7(7) . . . . ?
C16 N3 C10 C9 178.4(9) . . . . ?
Ni1 N3 C10 C9 -5.7(12) . . . . ?
C11 N4 C10 N3 2.0(12) . . . . ?
C17 N4 C10 N3 179.7(9) . . . . ?
C11 N4 C10 C9 -175.3(10) . . . . ?
C17 N4 C10 C9 2.4(18) . . . . ?
N1 C9 C10 N3 4.9(14) . . . . ?
C8 C9 C10 N3 -168.6(10) . . . . ?
N1 C9 C10 N4 -177.9(10) . . . . ?
C8 C9 C10 N4 8.6(19) . . . . ?
C10 N4 C11 C12 178.0(11) . . . . ?
C17 N4 C11 C12 0.2(19) . . . . ?
C10 N4 C11 C16 -3.8(12) . . . . ?
C17 N4 C11 C16 178.4(9) . . . . ?
N4 C11 C12 C13 179.6(11) . . . . ?
C16 C11 C12 C13 1.7(16) . . . . ?
C11 C12 C13 C14 0.4(17) . . . . ?
C12 C13 C14 C15 -0.8(18) . . . . ?
C13 C14 C15 C16 -0.9(16) . . . . ?
C10 N3 C16 C15 -176.0(11) . . . . ?
Ni1 N3 C16 C15 10(2) . . . . ?
C10 N3 C16 C11 -3.2(11) . . . . ?
Ni1 N3 C16 C11 -177.3(8) . . . . ?
C14 C15 C16 N3 175.1(11) . . . . ?
C14 C15 C16 C11 2.8(16) . . . . ?
N4 C11 C16 N3 4.4(12) . . . . ?
C12 C11 C16 N3 -177.2(10) . . . . ?
N4 C11 C16 C15 178.3(9) . . . . ?
C12 C11 C16 C15 -3.3(16) . . . . ?
C21 N5 C19 O1 -2(2) . . . . ?
C20 N5 C19 O1 178.2(13) . . . . ?
C24 N6 C22 O2 170.1(13) . . . . ?
C23 N6 C22 O2 6(2) . . . . ?
