#------------------------------------------------------------------------------
#$Date: 2016-03-25 10:21:20 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179748 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/44/7004461.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7004461
loop_
_publ_author_name
'Sarju, Julien'
'Arbour, Jannine'
'Sayer, James'
'Rohrmoser, Benjamin'
'Scherer, Wolfgang'
'Wagner, Gabriele'
_publ_section_title
;
 Synthesis and characterisation of mixed ligand Pt(ii) and Pt(iv)
 oxadiazoline complexes
;
_journal_issue                   39
_journal_name_full               'Dalton Transactions'
_journal_page_first              5302
_journal_page_last               5312
_journal_paper_doi               10.1039/b807410k
_journal_year                    2008
_chemical_compound_source        'see text'
_chemical_formula_moiety         'C20 H19 Cl2 N3 O Pt'
_chemical_formula_sum            'C20 H19 Cl2 N3 O Pt'
_chemical_formula_weight         583.36
_chemical_name_systematic        ?
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                90
_cell_angle_beta                 113.062(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.4796(10)
_cell_length_b                   8.9290(6)
_cell_length_c                   15.4594(10)
_cell_measurement_reflns_used    23750
_cell_measurement_temperature    295
_cell_measurement_theta_max      30.71
_cell_measurement_theta_min      2.28
_cell_volume                     2093.0(2)
_computing_cell_refinement       'X-Area, (STOE&Cie, 2006)'
_computing_data_collection       'X-Area, (STOE&Cie, 2006)'
_computing_data_reduction        'SORTAV, (Blessing 1995)'
_computing_molecular_graphics    'PLATON (Spek, 2003)'
_computing_publication_material  'PLATON (Spek, 2003)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR92 (Altomare (1993)'
_diffrn_ambient_temperature      295
_diffrn_detector_area_resol_mean 6.67
_diffrn_measured_fraction_theta_full 0.98
_diffrn_measured_fraction_theta_max 0.98
_diffrn_measurement_device_type  'STOE IPDS II'
_diffrn_measurement_method       'rotation method'
_diffrn_radiation_monochromator  'plane graphite'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'sealed X-ray tube,12x0.4mmlong-finefocus'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0415
_diffrn_reflns_av_sigmaI/netI    0.0393
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            13473
_diffrn_reflns_reduction_process
;
;
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         2.64
_exptl_absorpt_coefficient_mu    6.974
_exptl_absorpt_correction_T_max  0.45
_exptl_absorpt_correction_T_min  0.27
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
A multi-scan absorption correction was performed using 'Sortav'
R. H. Blessing Acta Crystallogr. 1995, A51, 33-37.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.851
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_description       fragment
_exptl_crystal_F_000             1120
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.415
_refine_diff_density_min         -0.947
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.082
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     244
_refine_ls_number_reflns         4222
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.082
_refine_ls_R_factor_all          0.0486
_refine_ls_R_factor_gt           0.0356
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
'w=1/sigma2(Fo)2 + (0.042*P)^2 where P=(Max(Fo^2,0) + 2*Fc^2)/3'
;
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0747
_refine_ls_wR_factor_ref         0.0788
_reflns_number_gt                3504
_reflns_number_total             4222
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            b807410k.txt
_cod_data_source_block           ptcl2
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7004461
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,1/2+y,1/2-z
3 -x,-y,-z
4 x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_thermal_displace_type
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt Uani 0.17010(1) 0.22220(3) 0.18745(1) 1.000 0.0449(1) . .
Cl1 Cl Uani 0.09561(10) 0.09872(19) 0.26555(12) 1.000 0.0618(5) . .
Cl2 Cl Uani 0.24478(12) 0.3418(2) 0.10944(13) 1.000 0.0741(6) . .
O1 O Uani 0.4191(3) 0.1226(5) 0.3939(3) 1.000 0.0546(14) . .
N1 N Uani 0.2849(3) 0.1910(5) 0.2981(3) 1.000 0.0440(14) . .
N2 N Uani 0.3971(3) 0.2553(6) 0.4391(4) 1.000 0.0528(17) . .
N3 N Uani 0.0551(3) 0.2605(5) 0.0795(3) 1.000 0.0494(14) . .
C1 C Uani 0.4248(5) 0.2158(11) 0.5383(5) 1.000 0.086(3) . .
C2 C Uani 0.3532(4) 0.1123(6) 0.3088(4) 1.000 0.0458(17) . .
C3 C Uani 0.3005(4) 0.2689(7) 0.3889(4) 1.000 0.0475(17) . .
C4 C Uani 0.3700(4) 0.0132(6) 0.2424(4) 1.000 0.0488(17) . .
C5 C Uani 0.4569(4) -0.0147(8) 0.2538(5) 1.000 0.061(2) . .
C6 C Uani 0.4749(5) -0.1087(9) 0.1931(6) 1.000 0.077(3) . .
C7 C Uani 0.4081(6) -0.1717(10) 0.1201(6) 1.000 0.079(3) . .
C8 C Uani 0.3216(6) -0.1446(9) 0.1059(5) 1.000 0.076(3) . .
C9 C Uani 0.3023(5) -0.0539(8) 0.1683(5) 1.000 0.065(2) . .
C10 C Uani 0.2723(4) 0.4303(7) 0.3759(4) 1.000 0.0523(19) . .
C11 C Uani 0.1874(5) 0.4666(9) 0.3662(5) 1.000 0.071(3) . .
C12 C Uani 0.1580(6) 0.6140(13) 0.3478(6) 1.000 0.097(4) . .
C13 C Uani 0.2137(9) 0.7222(12) 0.3427(7) 1.000 0.104(4) . .
C14 C Uani 0.2981(7) 0.6890(10) 0.3542(7) 1.000 0.091(4) . .
C15 C Uani 0.3271(6) 0.5433(9) 0.3707(6) 1.000 0.074(3) . .
C16 C Uani -0.0057(4) 0.3505(7) 0.0896(4) 1.000 0.0517(19) . .
C17 C Uani -0.0836(4) 0.3851(8) 0.0172(5) 1.000 0.063(2) . .
C18 C Uani -0.1027(5) 0.3237(9) -0.0707(5) 1.000 0.072(3) . .
C19 C Uani -0.0417(6) 0.2299(10) -0.0824(5) 1.000 0.085(3) . .
C20 C Uani 0.0369(5) 0.1990(8) -0.0062(5) 1.000 0.069(2) . .
H1A H Uiso 0.48790 0.20870 0.56670 1.000 0.1290 calc R
H1B H Uiso 0.39950 0.12110 0.54350 1.000 0.1290 calc R
H1C H Uiso 0.40520 0.29150 0.56980 1.000 0.1290 calc R
H3 H Uiso 0.27050 0.21540 0.42320 1.000 0.0570 calc R
H5 H Uiso 0.50300 0.03050 0.30290 1.000 0.0730 calc R
H6 H Uiso 0.53300 -0.12900 0.20220 1.000 0.0920 calc R
H7 H Uiso 0.42090 -0.23420 0.07900 1.000 0.0950 calc R
H8 H Uiso 0.27620 -0.18680 0.05460 1.000 0.0920 calc R
H9 H Uiso 0.24400 -0.03850 0.16040 1.000 0.0770 calc R
H11 H Uiso 0.15000 0.39270 0.37190 1.000 0.0860 calc R
H12 H Uiso 0.10040 0.63820 0.33900 1.000 0.1160 calc R
H13 H Uiso 0.19400 0.82060 0.33130 1.000 0.1250 calc R
H14 H Uiso 0.33580 0.76440 0.35090 1.000 0.1090 calc R
H15 H Uiso 0.38470 0.52070 0.37840 1.000 0.0890 calc R
H16 H Uiso 0.00560 0.39120 0.14850 1.000 0.0630 calc R
H17 H Uiso -0.12350 0.44950 0.02710 1.000 0.0750 calc R
H18 H Uiso -0.15550 0.34550 -0.12070 1.000 0.0870 calc R
H19 H Uiso -0.05280 0.18710 -0.14080 1.000 0.1020 calc R
H20 H Uiso 0.07780 0.13480 -0.01440 1.000 0.0830 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
? ? ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Pt1 Cl2 179.22(6) . . . yes
Cl1 Pt1 N1 90.27(15) . . . yes
Cl1 Pt1 N3 89.65(15) . . . yes
Cl2 Pt1 N1 89.54(15) . . . yes
Cl2 Pt1 N3 90.56(15) . . . yes
N1 Pt1 N3 177.83(18) . . . yes
N2 O1 C2 105.2(5) . . . yes
Pt1 N1 C2 132.2(4) . . . yes
Pt1 N1 C3 119.5(4) . . . yes
C2 N1 C3 108.3(5) . . . yes
O1 N2 C1 105.5(5) . . . yes
O1 N2 C3 103.2(5) . . . yes
C1 N2 C3 113.6(6) . . . yes
Pt1 N3 C16 120.8(4) . . . yes
Pt1 N3 C20 121.3(5) . . . yes
C16 N3 C20 117.9(5) . . . yes
O1 C2 N1 114.9(5) . . . yes
O1 C2 C4 115.3(6) . . . yes
N1 C2 C4 129.8(5) . . . yes
N1 C3 N2 102.0(5) . . . yes
N1 C3 C10 112.9(5) . . . yes
N2 C3 C10 111.2(5) . . . yes
C2 C4 C5 119.1(6) . . . no
C2 C4 C9 122.0(7) . . . no
C5 C4 C9 118.8(6) . . . no
C4 C5 C6 120.5(7) . . . no
C5 C6 C7 120.1(8) . . . no
C6 C7 C8 120.9(8) . . . no
C7 C8 C9 119.8(8) . . . no
C4 C9 C8 119.9(8) . . . no
C3 C10 C11 119.0(6) . . . no
C3 C10 C15 122.3(7) . . . no
C11 C10 C15 118.7(7) . . . no
C10 C11 C12 119.9(8) . . . no
C11 C12 C13 119.7(10) . . . no
C12 C13 C14 121.1(10) . . . no
C13 C14 C15 119.5(10) . . . no
C10 C15 C14 121.1(9) . . . no
N3 C16 C17 123.0(6) . . . yes
C16 C17 C18 119.6(7) . . . no
C17 C18 C19 118.3(7) . . . no
C18 C19 C20 119.7(7) . . . no
N3 C20 C19 121.5(7) . . . yes
N2 C1 H1A 109.00 . . . no
N2 C1 H1B 109.00 . . . no
N2 C1 H1C 109.00 . . . no
H1A C1 H1B 109.00 . . . no
H1A C1 H1C 110.00 . . . no
H1B C1 H1C 110.00 . . . no
N1 C3 H3 110.00 . . . no
N2 C3 H3 110.00 . . . no
C10 C3 H3 110.00 . . . no
C4 C5 H5 120.00 . . . no
C6 C5 H5 120.00 . . . no
C5 C6 H6 120.00 . . . no
C7 C6 H6 120.00 . . . no
C6 C7 H7 119.00 . . . no
C8 C7 H7 120.00 . . . no
C7 C8 H8 120.00 . . . no
C9 C8 H8 120.00 . . . no
C4 C9 H9 120.00 . . . no
C8 C9 H9 120.00 . . . no
C10 C11 H11 120.00 . . . no
C12 C11 H11 120.00 . . . no
C11 C12 H12 120.00 . . . no
C13 C12 H12 120.00 . . . no
C12 C13 H13 119.00 . . . no
C14 C13 H13 120.00 . . . no
C13 C14 H14 120.00 . . . no
C15 C14 H14 120.00 . . . no
C10 C15 H15 120.00 . . . no
C14 C15 H15 119.00 . . . no
N3 C16 H16 118.00 . . . no
C17 C16 H16 119.00 . . . no
C16 C17 H17 120.00 . . . no
C18 C17 H17 120.00 . . . no
C17 C18 H18 121.00 . . . no
C19 C18 H18 121.00 . . . no
C18 C19 H19 120.00 . . . no
C20 C19 H19 120.00 . . . no
N3 C20 H20 119.00 . . . no
C19 C20 H20 119.00 . . . no
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Cl1 2.3111(18) . . yes
Pt1 Cl2 2.296(2) . . yes
Pt1 N1 2.012(5) . . yes
Pt1 N3 2.004(5) . . yes
O1 N2 1.491(7) . . yes
O1 C2 1.341(7) . . yes
N1 C2 1.282(8) . . yes
N1 C3 1.496(7) . . yes
N2 C1 1.462(9) . . yes
N2 C3 1.478(9) . . yes
N3 C16 1.340(8) . . yes
N3 C20 1.355(8) . . yes
C2 C4 1.462(8) . . no
C3 C10 1.503(9) . . no
C4 C5 1.395(10) . . no
C4 C9 1.384(10) . . no
C5 C6 1.375(11) . . no
C6 C7 1.352(13) . . no
C7 C8 1.376(15) . . no
C8 C9 1.389(11) . . no
C10 C11 1.386(11) . . no
C10 C15 1.377(11) . . no
C11 C12 1.393(14) . . no
C12 C13 1.356(17) . . no
C13 C14 1.364(19) . . no
C14 C15 1.375(12) . . no
C16 C17 1.368(10) . . no
C17 C18 1.382(10) . . no
C18 C19 1.374(13) . . no
C19 C20 1.395(11) . . no
C1 H1A 0.9600 . . no
C1 H1B 0.9600 . . no
C1 H1C 0.9600 . . no
C3 H3 0.9800 . . no
C5 H5 0.9300 . . no
C6 H6 0.9300 . . no
C7 H7 0.9300 . . no
C8 H8 0.9300 . . no
C9 H9 0.9300 . . no
C11 H11 0.9300 . . no
C12 H12 0.9300 . . no
C13 H13 0.9300 . . no
C14 H14 0.9300 . . no
C15 H15 0.9300 . . no
C16 H16 0.9300 . . no
C17 H17 0.9300 . . no
C18 H18 0.9300 . . no
C19 H19 0.9300 . . no
C20 H20 0.9300 . . no
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_1
_geom_contact_site_symmetry_2
_geom_contact_publ_flag
Pt1 C9 3.379(8) . . no
Pt1 C11 3.444(8) . . no
Pt1 C15 4.147(9) . . no
Pt1 H9 2.7300 . . no
Pt1 H11 3.3600 . . no
Cl1 N1 3.071(5) . . no
Cl1 N3 3.050(5) . . no
Cl1 C3 3.507(7) . . no
Cl1 C16 3.418(6) . . no
Cl2 N3 3.063(6) . . no
Cl2 C2 3.546(6) . . no
Cl2 C20 3.429(8) . . no
Cl2 C17 3.572(7) . 3_565 no
Cl2 C1 3.582(9) . 4_554 no
Cl2 N1 3.041(5) . . no
Cl1 H16 3.1200 . 2_545 no
Cl1 H3 3.1400 . . no
Cl1 H11 3.0400 . . no
Cl1 H13 2.9200 . 1_545 no
Cl1 H12 3.0100 . 2_545 no
Cl1 H19 3.1100 . 3_555 no
Cl2 H17 2.9400 . 3_565 no
Cl2 H1B 3.1100 . 4_554 no
Cl2 H3 3.1100 . 4_554 no
O1 N1 2.212(7) . . no
O1 H5 2.4700 . . no
O1 H7 2.8100 . 2_655 no
N1 Cl1 3.071(5) . . no
N1 Cl2 3.041(5) . . no
N1 N2 2.311(7) . . no
N2 N1 2.311(7) . . no
N3 Cl1 3.050(5) . . no
N3 Cl2 3.063(6) . . no
N1 H9 2.8400 . . no
N2 H15 2.5300 . . no
C1 C5 3.528(11) . 3_656 no
C1 Cl2 3.582(9) . 4_555 no
C5 C1 3.528(11) . 3_656 no
C9 Pt1 3.379(8) . . no
C11 Pt1 3.444(8) . . no
C15 Pt1 4.147(9) . . no
C16 C17 3.517(10) . 3_565 no
C16 C18 3.485(11) . 3_565 no
C17 Cl2 3.572(7) . 3_565 no
C17 C16 3.517(10) . 3_565 no
C18 C16 3.485(11) . 3_565 no
C2 H6 3.0200 . 2_655 no
C4 H14 2.9700 . 1_545 no
C5 H1A 3.0900 . 3_656 no
C7 H5 3.0400 . 2_645 no
C12 H8 3.0900 . 4_555 no
C13 H8 3.0400 . 4_555 no
C16 H12 2.9300 . 2_545 no
H1A C5 3.0900 . 3_656 no
H1B H3 2.3600 . . no
H1B Cl2 3.1100 . 4_555 no
H1C H3 2.5700 . . no
H3 Cl1 3.1400 . . no
H3 H1B 2.3600 . . no
H3 H1C 2.5700 . . no
H3 H11 2.4200 . . no
H3 Cl2 3.1100 . 4_555 no
H5 O1 2.4700 . . no
H5 C7 3.0400 . 2_655 no
H6 C2 3.0200 . 2_645 no
H6 H15 2.5500 . 2_645 no
H7 O1 2.8100 . 2_645 no
H8 C12 3.0900 . 4_554 no
H8 C13 3.0400 . 4_554 no
H9 Pt1 2.7300 . . no
H9 N1 2.8400 . . no
H11 Pt1 3.3600 . . no
H11 Cl1 3.0400 . . no
H11 H3 2.4200 . . no
H11 H20 2.4900 . 4_555 no
H12 Cl1 3.0100 . 2_555 no
H12 C16 2.9300 . 2_555 no
H13 Cl1 2.9200 . 1_565 no
H14 C4 2.9700 . 1_565 no
H15 N2 2.5300 . . no
H15 H6 2.5500 . 2_655 no
H16 Cl1 3.1200 . 2_555 no
H17 Cl2 2.9400 . 3_565 no
H19 Cl1 3.1100 . 3_555 no
H20 H11 2.4900 . 4_554 no
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
_geom_hbond_publ_flag
C15 H15 N2 0.9300 2.5300 2.847(10) 100.00 . yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Cl1 Pt1 N1 C2 112.8(5) . . . . no
Cl1 Pt1 N1 C3 -67.0(4) . . . . no
Cl2 Pt1 N1 C2 -66.4(5) . . . . no
Cl2 Pt1 N1 C3 113.7(4) . . . . no
Cl1 Pt1 N3 C16 66.3(5) . . . . no
Cl1 Pt1 N3 C20 -115.0(5) . . . . no
Cl2 Pt1 N3 C16 -114.5(5) . . . . no
Cl2 Pt1 N3 C20 64.2(5) . . . . no
C2 O1 N2 C1 143.0(6) . . . . no
C2 O1 N2 C3 23.5(6) . . . . no
N2 O1 C2 N1 -14.1(7) . . . . no
N2 O1 C2 C4 165.9(5) . . . . no
Pt1 N1 C2 O1 178.5(4) . . . . no
Pt1 N1 C2 C4 -1.6(10) . . . . no
C3 N1 C2 O1 -1.7(7) . . . . no
C3 N1 C2 C4 178.3(6) . . . . no
Pt1 N1 C3 N2 -163.5(4) . . . . no
Pt1 N1 C3 C10 -44.0(7) . . . . no
C2 N1 C3 N2 16.7(6) . . . . no
C2 N1 C3 C10 136.1(6) . . . . no
O1 N2 C3 N1 -23.5(5) . . . . no
O1 N2 C3 C10 -144.2(5) . . . . no
C1 N2 C3 N1 -137.2(6) . . . . no
C1 N2 C3 C10 102.2(7) . . . . no
Pt1 N3 C16 C17 177.2(5) . . . . no
C20 N3 C16 C17 -1.5(9) . . . . no
Pt1 N3 C20 C19 -177.6(6) . . . . no
C16 N3 C20 C19 1.2(10) . . . . no
O1 C2 C4 C5 -24.9(8) . . . . no
O1 C2 C4 C9 155.2(6) . . . . no
N1 C2 C4 C5 155.1(7) . . . . no
N1 C2 C4 C9 -24.8(10) . . . . no
N1 C3 C10 C11 91.7(7) . . . . no
N1 C3 C10 C15 -86.5(8) . . . . no
N2 C3 C10 C11 -154.3(6) . . . . no
N2 C3 C10 C15 27.5(8) . . . . no
C2 C4 C5 C6 179.3(6) . . . . no
C9 C4 C5 C6 -0.8(10) . . . . no
C2 C4 C9 C8 178.6(6) . . . . no
C5 C4 C9 C8 -1.3(10) . . . . no
C4 C5 C6 C7 1.8(12) . . . . no
C5 C6 C7 C8 -0.8(13) . . . . no
C6 C7 C8 C9 -1.4(13) . . . . no
C7 C8 C9 C4 2.4(11) . . . . no
C3 C10 C11 C12 -175.7(6) . . . . no
C15 C10 C11 C12 2.6(10) . . . . no
C3 C10 C15 C14 176.8(7) . . . . no
C11 C10 C15 C14 -1.4(11) . . . . no
C10 C11 C12 C13 -2.3(12) . . . . no
C11 C12 C13 C14 0.8(14) . . . . no
C12 C13 C14 C15 0.4(15) . . . . no
C13 C14 C15 C10 -0.1(14) . . . . no
N3 C16 C17 C18 1.2(11) . . . . no
C16 C17 C18 C19 -0.5(12) . . . . no
C17 C18 C19 C20 0.2(13) . . . . no
C18 C19 C20 N3 -0.6(13) . . . . no
