#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/45/7004578.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7004578
loop_
_publ_author_name
'Armitt, David J.'
'Bruce, Michael I.'
'Gaudio, Maryka'
'Zaitseva, Natasha N.'
'Skelton, Brian W.'
'White, Allan H.'
'Le Guennic, Boris'
'Halet, Jean-François'
'Fox, Mark A.'
'Roberts, Rachel L.'
'Hartl, František'
'Low, Paul J.'
_publ_section_title
;
 Some transition metal complexes derived from mono- and di-ethynyl
 perfluorobenzenes
;
_journal_issue                   47
_journal_name_full               'Dalton Transactions'
_journal_page_first              6763
_journal_page_last               6775
_journal_paper_doi               10.1039/b808798a
_journal_year                    2008
_chemical_formula_moiety         'C41 H22 Co3 F5 O7 P2'
_chemical_formula_sum            'C41 H22 Co3 F5 O7 P2'
_chemical_formula_weight         960.32
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2006-07-14T14:55:43-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                97.855(9)
_cell_angle_beta                 91.445(11)
_cell_angle_gamma                93.438(7)
_cell_formula_units_Z            4
_cell_length_a                   11.6170(10)
_cell_length_b                   17.643(2)
_cell_length_c                   19.108(3)
_cell_measurement_reflns_used    35639
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      34.1063
_cell_measurement_theta_min      2.52
_cell_volume                     3870.4(8)
_computing_cell_refinement
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.30.5 (release 12-06-2006 CrysAlis171 .NET)
(compiled Jun 12 2006,17:01:16)
;
_computing_data_collection
;
CrysAlis CCD, Oxford Diffraction Ltd.,
Version 1.171.30.5 (release 12-06-2006 CrysAlis171 .NET)
(compiled Jun 12 2006,17:01:16)
;
_computing_data_reduction
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.30.5 (release 12-06-2006 CrysAlis171 .NET)
(compiled Jun 12 2006,17:01:16)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 16.0009
_diffrn_measured_fraction_theta_full 0.98
_diffrn_measured_fraction_theta_max 0.95
_diffrn_measurement_device_type
;
Oxford Diffraction Xcalibur diffractometer
;
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      -0.0283055087
_diffrn_orient_matrix_UB_12      0.0098214312
_diffrn_orient_matrix_UB_13      0.0321844559
_diffrn_orient_matrix_UB_21      -0.0422159249
_diffrn_orient_matrix_UB_22      0.0181802051
_diffrn_orient_matrix_UB_23      -0.0181926576
_diffrn_orient_matrix_UB_31      -0.0343438482
_diffrn_orient_matrix_UB_32      -0.0351391959
_diffrn_orient_matrix_UB_33      -0.0064131153
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0244
_diffrn_reflns_av_unetI/netI     0.0536
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            76417
_diffrn_reflns_theta_full        34.14
_diffrn_reflns_theta_max         34.14
_diffrn_reflns_theta_min         2.52
_exptl_absorpt_coefficient_mu    1.428
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_correction_T_min  0.91814
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.30.5 (release 12-06-2006 CrysAlis171 .NET)
(compiled Jun 12 2006,17:01:16)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.648
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1920
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.24
_refine_diff_density_max         0.694
_refine_diff_density_min         -0.418
_refine_diff_density_rms         0.083
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.987
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1045
_refine_ls_number_reflns         29976
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.987
_refine_ls_R_factor_all          0.0531
_refine_ls_R_factor_gt           0.0318
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0436P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0744
_refine_ls_wR_factor_ref         0.0829
_reflns_number_gt                20530
_reflns_number_total             29976
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b808798a.txt
_cod_data_source_block           br1282_compound_6
_cod_original_sg_symbol_Hall     -P_1
_cod_database_code               7004578
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.370384(16) 0.598379(10) 0.278160(10) 0.01176(4) Uani 1 1 d . . .
Co2 Co 0.421385(16) 0.547656(11) 0.156259(10) 0.01224(4) Uani 1 1 d . . .
Co3 Co 0.555361(16) 0.642526(11) 0.230260(11) 0.01306(4) Uani 1 1 d . . .
C11 C 0.27107(13) 0.66022(8) 0.24499(8) 0.0168(3) Uani 1 1 d . . .
O11 O 0.20985(10) 0.69980(7) 0.22174(6) 0.0252(3) Uani 1 1 d . . .
C12 C 0.39450(13) 0.64001(9) 0.36797(8) 0.0190(3) Uani 1 1 d . . .
O12 O 0.40627(11) 0.66758(7) 0.42566(7) 0.0319(3) Uani 1 1 d . . .
C21 C 0.35538(13) 0.60736(8) 0.09827(8) 0.0169(3) Uani 1 1 d . . .
O21 O 0.31642(10) 0.64585(7) 0.06157(6) 0.0251(3) Uani 1 1 d . . .
C22 C 0.52423(13) 0.50248(9) 0.09883(8) 0.0189(3) Uani 1 1 d . . .
O22 O 0.59158(10) 0.47396(7) 0.06321(7) 0.0287(3) Uani 1 1 d . . .
C31 C 0.49777(13) 0.72353(8) 0.19614(8) 0.0172(3) Uani 1 1 d . . .
O31 O 0.45792(10) 0.77313(6) 0.17352(7) 0.0252(3) Uani 1 1 d . . .
C32 C 0.68019(13) 0.62250(9) 0.17987(9) 0.0193(3) Uani 1 1 d . . .
O32 O 0.75976(10) 0.60975(7) 0.14693(7) 0.0295(3) Uani 1 1 d . . .
C33 C 0.62685(13) 0.68799(9) 0.31125(9) 0.0208(3) Uani 1 1 d . . .
O33 O 0.67457(12) 0.71942(8) 0.36077(7) 0.0334(3) Uani 1 1 d . . .
C1 C 0.49604(12) 0.54069(8) 0.24539(8) 0.0131(3) Uani 1 1 d . . .
C2 C 0.55870(12) 0.48275(8) 0.26861(8) 0.0140(3) Uani 1 1 d . . .
C3 C 0.61152(13) 0.43215(8) 0.28887(9) 0.0184(3) Uani 1 1 d . . .
C131 C 0.67918(12) 0.37684(8) 0.31562(8) 0.0157(3) Uani 1 1 d . . .
C132 C 0.71809(14) 0.38545(9) 0.38576(9) 0.0222(3) Uani 1 1 d . . .
C133 C 0.78844(16) 0.33402(11) 0.41120(9) 0.0272(4) Uani 1 1 d . . .
C134 C 0.82115(15) 0.27155(10) 0.36592(10) 0.0257(4) Uani 1 1 d . . .
C135 C 0.78295(14) 0.26018(9) 0.29653(9) 0.0225(3) Uani 1 1 d . . .
C136 C 0.71351(13) 0.31248(9) 0.27199(8) 0.0185(3) Uani 1 1 d . . .
F132 F 0.68845(10) 0.44575(6) 0.43055(6) 0.0344(3) Uani 1 1 d . . .
F133 F 0.82619(11) 0.34493(7) 0.47926(6) 0.0453(3) Uani 1 1 d . . .
F134 F 0.88961(10) 0.22163(6) 0.39072(6) 0.0398(3) Uani 1 1 d . . .
F135 F 0.81257(9) 0.19875(6) 0.25295(6) 0.0317(2) Uani 1 1 d . . .
F136 F 0.68074(9) 0.30171(6) 0.20336(5) 0.0272(2) Uani 1 1 d . . .
P1 P 0.25269(3) 0.50270(2) 0.30032(2) 0.01284(7) Uani 1 1 d . . .
C111 C 0.27031(14) 0.46199(8) 0.38234(8) 0.0178(3) Uani 1 1 d . . .
C112 C 0.38110(15) 0.45606(10) 0.41011(8) 0.0229(3) Uani 1 1 d . . .
H112 H 0.4456 0.4794 0.3898 0.027 Uiso 1 1 calc R . .
C113 C 0.39801(18) 0.41637(10) 0.46723(9) 0.0301(4) Uani 1 1 d . . .
H113 H 0.4739 0.4119 0.4852 0.036 Uiso 1 1 calc R . .
C114 C 0.3049(2) 0.38349(11) 0.49772(10) 0.0367(5) Uani 1 1 d . . .
H114 H 0.3167 0.356 0.5365 0.044 Uiso 1 1 calc R . .
C115 C 0.1943(2) 0.39034(12) 0.47213(10) 0.0400(5) Uani 1 1 d . . .
H115 H 0.1303 0.3684 0.4939 0.048 Uiso 1 1 calc R . .
C116 C 0.17625(16) 0.42933(10) 0.41439(9) 0.0292(4) Uani 1 1 d . . .
H116 H 0.1 0.4337 0.3969 0.035 Uiso 1 1 calc R . .
C121 C 0.09995(12) 0.52136(8) 0.29889(8) 0.0151(3) Uani 1 1 d . . .
C122 C 0.01383(13) 0.46947(9) 0.26448(8) 0.0184(3) Uani 1 1 d . . .
H122 H 0.0339 0.422 0.2396 0.022 Uiso 1 1 calc R . .
C123 C -0.10142(13) 0.48757(9) 0.26676(9) 0.0208(3) Uani 1 1 d . . .
H123 H -0.1593 0.453 0.2422 0.025 Uiso 1 1 calc R . .
C124 C -0.13201(14) 0.55543(10) 0.30451(9) 0.0244(3) Uani 1 1 d . . .
H124 H -0.2108 0.567 0.3064 0.029 Uiso 1 1 calc R . .
C125 C -0.04722(15) 0.60701(10) 0.33976(10) 0.0273(4) Uani 1 1 d . . .
H125 H -0.0682 0.6535 0.3661 0.033 Uiso 1 1 calc R . .
C126 C 0.06818(14) 0.59034(9) 0.33624(9) 0.0210(3) Uani 1 1 d . . .
H126 H 0.1259 0.6261 0.3594 0.025 Uiso 1 1 calc R . .
C10 C 0.27365(12) 0.41824(8) 0.23559(7) 0.0140(3) Uani 1 1 d . . .
H10A H 0.2048 0.382 0.2332 0.017 Uiso 1 1 calc R . .
H10B H 0.3411 0.3919 0.2505 0.017 Uiso 1 1 calc R . .
P2 P 0.29714(3) 0.44718(2) 0.14793(2) 0.01221(7) Uani 1 1 d . . .
C211 C 0.35118(12) 0.36344(8) 0.09536(8) 0.0142(3) Uani 1 1 d . . .
C212 C 0.43053(13) 0.31900(8) 0.12462(8) 0.0178(3) Uani 1 1 d . . .
H212 H 0.4488 0.3279 0.1739 0.021 Uiso 1 1 calc R . .
C213 C 0.48294(14) 0.26154(9) 0.08143(8) 0.0199(3) Uani 1 1 d . . .
H213 H 0.5367 0.2314 0.1014 0.024 Uiso 1 1 calc R . .
C214 C 0.45669(14) 0.24855(9) 0.00964(9) 0.0213(3) Uani 1 1 d . . .
H214 H 0.4931 0.2098 -0.0197 0.026 Uiso 1 1 calc R . .
C215 C 0.37749(14) 0.29186(9) -0.01955(8) 0.0215(3) Uani 1 1 d . . .
H215 H 0.3584 0.282 -0.0687 0.026 Uiso 1 1 calc R . .
C216 C 0.32591(13) 0.34952(9) 0.02272(8) 0.0188(3) Uani 1 1 d . . .
H216 H 0.273 0.3798 0.0022 0.023 Uiso 1 1 calc R . .
C221 C 0.14931(12) 0.44818(9) 0.11311(8) 0.0161(3) Uani 1 1 d . . .
C222 C 0.08209(14) 0.37853(10) 0.09781(9) 0.0228(3) Uani 1 1 d . . .
H222 H 0.1163 0.3314 0.1007 0.027 Uiso 1 1 calc R . .
C223 C -0.03365(15) 0.37842(11) 0.07861(10) 0.0300(4) Uani 1 1 d . . .
H223 H -0.0785 0.3312 0.0684 0.036 Uiso 1 1 calc R . .
C224 C -0.08461(15) 0.44687(12) 0.07425(10) 0.0310(4) Uani 1 1 d . . .
H224 H -0.1642 0.4465 0.0613 0.037 Uiso 1 1 calc R . .
C225 C -0.01910(15) 0.51579(11) 0.08889(9) 0.0271(4) Uani 1 1 d . . .
H225 H -0.0538 0.5627 0.0856 0.033 Uiso 1 1 calc R . .
C226 C 0.09741(13) 0.51661(9) 0.10833(8) 0.0197(3) Uani 1 1 d . . .
H226 H 0.1417 0.5641 0.1184 0.024 Uiso 1 1 calc R . .
Co4 Co 0.122581(17) 0.056662(11) 0.271561(11) 0.01381(4) Uani 1 1 d . . .
Co5 Co 0.306767(17) 0.089012(11) 0.214829(11) 0.01339(4) Uani 1 1 d . . .
Co6 Co 0.234320(17) 0.179168(11) 0.313258(11) 0.01503(4) Uani 1 1 d . . .
C41 C 0.01526(14) 0.07984(9) 0.20915(9) 0.0237(3) Uani 1 1 d . . .
O41 O -0.05168(13) 0.09556(8) 0.16975(8) 0.0412(4) Uani 1 1 d . . .
C42 C 0.04203(14) 0.05935(9) 0.35050(9) 0.0216(3) Uani 1 1 d . . .
O42 O -0.00623(12) 0.06296(7) 0.40193(7) 0.0346(3) Uani 1 1 d . . .
C51 C 0.24150(14) 0.13268(9) 0.14525(9) 0.0215(3) Uani 1 1 d . . .
O51 O 0.19740(12) 0.16357(8) 0.10397(7) 0.0352(3) Uani 1 1 d . . .
C52 C 0.45575(14) 0.12358(9) 0.21572(8) 0.0185(3) Uani 1 1 d . . .
O52 O 0.55042(10) 0.14463(7) 0.21621(7) 0.0280(3) Uani 1 1 d . . .
C61 C 0.12520(14) 0.23064(9) 0.27391(9) 0.0227(3) Uani 1 1 d . . .
O61 O 0.05684(11) 0.26444(7) 0.25026(8) 0.0344(3) Uani 1 1 d . . .
C62 C 0.35911(14) 0.24414(9) 0.31265(8) 0.0191(3) Uani 1 1 d . . .
O62 O 0.43691(10) 0.28679(6) 0.31160(7) 0.0254(3) Uani 1 1 d . . .
C63 C 0.20973(14) 0.19230(9) 0.40681(9) 0.0215(3) Uani 1 1 d . . .
O63 O 0.19765(11) 0.19893(8) 0.46609(7) 0.0326(3) Uani 1 1 d . . .
C4 C 0.27754(12) 0.07417(8) 0.30916(8) 0.0141(3) Uani 1 1 d . . .
C5 C 0.32340(12) 0.03681(8) 0.36289(8) 0.0162(3) Uani 1 1 d . . .
C6 C 0.35314(13) -0.00012(9) 0.40820(8) 0.0194(3) Uani 1 1 d . . .
C231 C 0.37395(13) -0.04649(9) 0.46245(8) 0.0189(3) Uani 1 1 d . . .
C232 C 0.31405(15) -0.03810(9) 0.52534(9) 0.0232(3) Uani 1 1 d . . .
C233 C 0.33125(16) -0.08429(10) 0.57718(9) 0.0273(4) Uani 1 1 d . . .
C234 C 0.41063(16) -0.13985(10) 0.56719(10) 0.0292(4) Uani 1 1 d . . .
C235 C 0.47200(15) -0.14960(9) 0.50645(10) 0.0265(4) Uani 1 1 d . . .
C236 C 0.45285(14) -0.10354(9) 0.45476(9) 0.0226(3) Uani 1 1 d . . .
F232 F 0.23825(9) 0.01621(6) 0.53621(6) 0.0331(2) Uani 1 1 d . . .
F233 F 0.27243(11) -0.07509(7) 0.63675(6) 0.0428(3) Uani 1 1 d . . .
F234 F 0.42889(11) -0.18341(7) 0.61821(6) 0.0440(3) Uani 1 1 d . . .
F235 F 0.55077(10) -0.20237(6) 0.49834(7) 0.0391(3) Uani 1 1 d . . .
F236 F 0.51352(9) -0.11423(6) 0.39569(6) 0.0326(2) Uani 1 1 d . . .
P4 P 0.12738(3) -0.06897(2) 0.24684(2) 0.01248(7) Uani 1 1 d . . .
C411 C 0.08951(13) -0.12258(8) 0.31889(8) 0.0157(3) Uani 1 1 d . . .
C412 C -0.02344(13) -0.12139(9) 0.34226(9) 0.0208(3) Uani 1 1 d . . .
H412 H -0.0788 -0.0957 0.3185 0.025 Uiso 1 1 calc R . .
C413 C -0.05587(15) -0.15725(10) 0.39962(9) 0.0251(3) Uani 1 1 d . . .
H413 H -0.1333 -0.1567 0.4145 0.03 Uiso 1 1 calc R . .
C414 C 0.02581(15) -0.19439(9) 0.43570(9) 0.0245(3) Uani 1 1 d . . .
H414 H 0.0045 -0.2181 0.4757 0.029 Uiso 1 1 calc R . .
C415 C 0.13744(15) -0.19622(9) 0.41258(9) 0.0222(3) Uani 1 1 d . . .
H415 H 0.1928 -0.2218 0.4365 0.027 Uiso 1 1 calc R . .
C416 C 0.16968(13) -0.16090(8) 0.35460(8) 0.0175(3) Uani 1 1 d . . .
H416 H 0.2467 -0.1628 0.3391 0.021 Uiso 1 1 calc R . .
C421 C 0.04288(12) -0.12018(8) 0.17085(8) 0.0139(3) Uani 1 1 d . . .
C422 C 0.00402(13) -0.19750(9) 0.16820(9) 0.0187(3) Uani 1 1 d . . .
H422 H 0.0173 -0.2235 0.2078 0.022 Uiso 1 1 calc R . .
C423 C -0.05355(14) -0.23599(9) 0.10814(9) 0.0239(3) Uani 1 1 d . . .
H423 H -0.0797 -0.2882 0.1068 0.029 Uiso 1 1 calc R . .
C424 C -0.07340(14) -0.19876(9) 0.04962(9) 0.0228(3) Uani 1 1 d . . .
H424 H -0.1131 -0.2253 0.0086 0.027 Uiso 1 1 calc R . .
C425 C -0.03449(13) -0.12226(9) 0.05181(8) 0.0201(3) Uani 1 1 d . . .
H425 H -0.0472 -0.0967 0.0119 0.024 Uiso 1 1 calc R . .
C426 C 0.02239(12) -0.08343(8) 0.11150(8) 0.0161(3) Uani 1 1 d . . .
H426 H 0.048 -0.0311 0.1125 0.019 Uiso 1 1 calc R . .
C20 C 0.27473(12) -0.09549(8) 0.22744(8) 0.0137(3) Uani 1 1 d . . .
H20A H 0.2729 -0.1488 0.203 0.016 Uiso 1 1 calc R . .
H20B H 0.321 -0.0926 0.2721 0.016 Uiso 1 1 calc R . .
P5 P 0.34111(3) -0.02976(2) 0.17106(2) 0.01321(7) Uani 1 1 d . . .
C511 C 0.49287(12) -0.05303(8) 0.17568(8) 0.0149(3) Uani 1 1 d . . .
C512 C 0.54763(13) -0.05051(9) 0.24220(9) 0.0221(3) Uani 1 1 d . . .
H512 H 0.5082 -0.033 0.2837 0.026 Uiso 1 1 calc R . .
C513 C 0.65922(14) -0.07349(10) 0.24756(10) 0.0275(4) Uani 1 1 d . . .
H513 H 0.6955 -0.0728 0.2928 0.033 Uiso 1 1 calc R . .
C514 C 0.71860(14) -0.09772(10) 0.18643(10) 0.0270(4) Uani 1 1 d . . .
H514 H 0.7945 -0.1144 0.1901 0.032 Uiso 1 1 calc R . .
C515 C 0.66636(14) -0.09728(9) 0.12122(10) 0.0240(3) Uani 1 1 d . . .
H515 H 0.7072 -0.1127 0.0797 0.029 Uiso 1 1 calc R . .
C516 C 0.55409(13) -0.07447(8) 0.11521(8) 0.0182(3) Uani 1 1 d . . .
H516 H 0.5193 -0.0736 0.0698 0.022 Uiso 1 1 calc R . .
C521 C 0.29588(12) -0.07307(8) 0.08117(8) 0.0151(3) Uani 1 1 d . . .
C522 C 0.28264(13) -0.15261(9) 0.06377(8) 0.0185(3) Uani 1 1 d . . .
H522 H 0.2944 -0.1843 0.0994 0.022 Uiso 1 1 calc R . .
C523 C 0.25257(13) -0.18619(9) -0.00481(8) 0.0196(3) Uani 1 1 d . . .
H523 H 0.2446 -0.2404 -0.0158 0.023 Uiso 1 1 calc R . .
C524 C 0.23411(15) -0.14058(10) -0.05721(9) 0.0237(3) Uani 1 1 d . . .
H524 H 0.213 -0.1634 -0.1041 0.028 Uiso 1 1 calc R . .
C525 C 0.24678(16) -0.06116(10) -0.04050(9) 0.0276(4) Uani 1 1 d . . .
H525 H 0.2336 -0.0297 -0.0761 0.033 Uiso 1 1 calc R . .
C526 C 0.27845(15) -0.02744(9) 0.02772(9) 0.0225(3) Uani 1 1 d . . .
H526 H 0.2884 0.0268 0.0383 0.027 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C12 Co1 C11 102.92(7) . . ?
C12 Co1 C1 111.10(7) . . ?
C11 Co1 C1 138.44(7) . . ?
C12 Co1 P1 95.83(5) . . ?
C11 Co1 P1 101.36(5) . . ?
C1 Co1 P1 98.27(4) . . ?
C12 Co1 Co2 157.14(5) . . ?
C11 Co1 Co2 90.94(5) . . ?
C1 Co1 Co2 49.73(4) . . ?
P1 Co1 Co2 99.192(16) . . ?
C12 Co1 Co3 98.88(5) . . ?
C11 Co1 Co3 101.97(5) . . ?
C1 Co1 Co3 50.67(4) . . ?
P1 Co1 Co3 148.762(14) . . ?
Co2 Co1 Co3 60.026(12) . . ?
C22 Co2 C21 100.68(7) . . ?
C22 Co2 C1 99.14(7) . . ?
C21 Co2 C1 148.02(6) . . ?
C22 Co2 P2 95.77(5) . . ?
C21 Co2 P2 102.46(5) . . ?
C1 Co2 P2 100.22(4) . . ?
C22 Co2 Co1 148.10(5) . . ?
C21 Co2 Co1 106.48(5) . . ?
C1 Co2 Co1 49.23(4) . . ?
P2 Co2 Co1 94.426(16) . . ?
C22 Co2 Co3 98.63(5) . . ?
C21 Co2 Co3 101.49(5) . . ?
C1 Co2 Co3 50.61(4) . . ?
P2 Co2 Co3 149.131(15) . . ?
Co1 Co2 Co3 60.045(12) . . ?
C32 Co3 C33 98.53(7) . . ?
C32 Co3 C31 104.74(7) . . ?
C33 Co3 C31 101.49(7) . . ?
C32 Co3 C1 102.47(6) . . ?
C33 Co3 C1 107.84(7) . . ?
C31 Co3 C1 136.04(6) . . ?
C32 Co3 Co2 96.04(5) . . ?
C33 Co3 Co2 155.51(5) . . ?
C31 Co3 Co2 93.65(5) . . ?
C1 Co3 Co2 49.44(4) . . ?
C32 Co3 Co1 150.11(5) . . ?
C33 Co3 Co1 99.29(5) . . ?
C31 Co3 Co1 94.96(5) . . ?
C1 Co3 Co1 49.01(4) . . ?
Co2 Co3 Co1 59.929(12) . . ?
O11 C11 Co1 177.61(14) . . ?
O12 C12 Co1 177.68(15) . . ?
O21 C21 Co2 178.31(14) . . ?
O22 C22 Co2 178.62(15) . . ?
O31 C31 Co3 177.51(14) . . ?
O32 C32 Co3 179.34(15) . . ?
O33 C33 Co3 176.65(14) . . ?
C2 C1 Co1 136.34(11) . . ?
C2 C1 Co2 131.39(11) . . ?
Co1 C1 Co2 81.05(6) . . ?
C2 C1 Co3 127.20(10) . . ?
Co1 C1 Co3 80.32(5) . . ?
Co2 C1 Co3 79.95(5) . . ?
C3 C2 C1 179.14(16) . . ?
C2 C3 C131 175.82(16) . . ?
C132 C131 C136 116.31(14) . . ?
C132 C131 C3 121.86(14) . . ?
C136 C131 C3 121.78(14) . . ?
F132 C132 C133 118.32(15) . . ?
F132 C132 C131 119.53(14) . . ?
C133 C132 C131 122.14(15) . . ?
F133 C133 C134 119.96(15) . . ?
F133 C133 C132 120.51(16) . . ?
C134 C133 C132 119.53(16) . . ?
F134 C134 C135 120.35(16) . . ?
F134 C134 C133 119.46(16) . . ?
C135 C134 C133 120.19(15) . . ?
F135 C135 C134 120.26(15) . . ?
F135 C135 C136 120.32(15) . . ?
C134 C135 C136 119.42(15) . . ?
F136 C136 C135 118.37(14) . . ?
F136 C136 C131 119.22(13) . . ?
C135 C136 C131 122.39(15) . . ?
C111 P1 C121 102.61(7) . . ?
C111 P1 C10 100.25(7) . . ?
C121 P1 C10 108.42(7) . . ?
C111 P1 Co1 120.11(5) . . ?
C121 P1 Co1 115.02(5) . . ?
C10 P1 Co1 109.03(5) . . ?
C112 C111 C116 118.75(15) . . ?
C112 C111 P1 119.38(12) . . ?
C116 C111 P1 121.55(13) . . ?
C113 C112 C111 120.63(16) . . ?
C113 C112 H112 119.7 . . ?
C111 C112 H112 119.7 . . ?
C114 C113 C112 120.09(18) . . ?
C114 C113 H113 120 . . ?
C112 C113 H113 120 . . ?
C113 C114 C115 120.15(16) . . ?
C113 C114 H114 119.9 . . ?
C115 C114 H114 119.9 . . ?
C114 C115 C116 120.33(18) . . ?
C114 C115 H115 119.8 . . ?
C116 C115 H115 119.8 . . ?
C115 C116 C111 120.02(18) . . ?
C115 C116 H116 120 . . ?
C111 C116 H116 120 . . ?
C126 C121 C122 119.02(14) . . ?
C126 C121 P1 117.47(11) . . ?
C122 C121 P1 123.48(11) . . ?
C123 C122 C121 119.98(14) . . ?
C123 C122 H122 120 . . ?
C121 C122 H122 120 . . ?
C124 C123 C122 120.52(15) . . ?
C124 C123 H123 119.7 . . ?
C122 C123 H123 119.7 . . ?
C123 C124 C125 119.98(15) . . ?
C123 C124 H124 120 . . ?
C125 C124 H124 120 . . ?
C126 C125 C124 119.89(16) . . ?
C126 C125 H125 120.1 . . ?
C124 C125 H125 120.1 . . ?
C125 C126 C121 120.59(15) . . ?
C125 C126 H126 119.7 . . ?
C121 C126 H126 119.7 . . ?
P1 C10 P2 110.09(7) . . ?
P1 C10 H10A 109.6 . . ?
P2 C10 H10A 109.6 . . ?
P1 C10 H10B 109.6 . . ?
P2 C10 H10B 109.6 . . ?
H10A C10 H10B 108.2 . . ?
C211 P2 C221 103.07(7) . . ?
C211 P2 C10 105.04(7) . . ?
C221 P2 C10 101.84(7) . . ?
C211 P2 Co2 111.96(5) . . ?
C221 P2 Co2 122.78(5) . . ?
C10 P2 Co2 110.42(5) . . ?
C216 C211 C212 119.02(14) . . ?
C216 C211 P2 119.57(11) . . ?
C212 C211 P2 120.81(11) . . ?
C213 C212 C211 120.07(14) . . ?
C213 C212 H212 120 . . ?
C211 C212 H212 120 . . ?
C214 C213 C212 120.07(15) . . ?
C214 C213 H213 120 . . ?
C212 C213 H213 120 . . ?
C213 C214 C215 120.16(15) . . ?
C213 C214 H214 119.9 . . ?
C215 C214 H214 119.9 . . ?
C214 C215 C216 120.21(15) . . ?
C214 C215 H215 119.9 . . ?
C216 C215 H215 119.9 . . ?
C215 C216 C211 120.46(15) . . ?
C215 C216 H216 119.8 . . ?
C211 C216 H216 119.8 . . ?
C226 C221 C222 118.87(14) . . ?
C226 C221 P2 121.67(12) . . ?
C222 C221 P2 119.11(12) . . ?
C223 C222 C221 120.25(16) . . ?
C223 C222 H222 119.9 . . ?
C221 C222 H222 119.9 . . ?
C222 C223 C224 120.44(17) . . ?
C222 C223 H223 119.8 . . ?
C224 C223 H223 119.8 . . ?
C225 C224 C223 119.80(16) . . ?
C225 C224 H224 120.1 . . ?
C223 C224 H224 120.1 . . ?
C224 C225 C226 120.26(17) . . ?
C224 C225 H225 119.9 . . ?
C226 C225 H225 119.9 . . ?
C225 C226 C221 120.38(15) . . ?
C225 C226 H226 119.8 . . ?
C221 C226 H226 119.8 . . ?
C42 Co4 C41 101.47(8) . . ?
C42 Co4 C4 101.68(7) . . ?
C41 Co4 C4 147.33(7) . . ?
C42 Co4 P4 97.96(5) . . ?
C41 Co4 P4 103.46(5) . . ?
C4 Co4 P4 95.81(4) . . ?
C42 Co4 Co6 93.54(5) . . ?
C41 Co4 Co6 105.33(5) . . ?
C4 Co4 Co6 50.49(4) . . ?
P4 Co4 Co6 146.079(14) . . ?
C42 Co4 Co5 148.32(5) . . ?
C41 Co4 Co5 102.40(6) . . ?
C4 Co4 Co5 48.71(4) . . ?
P4 Co4 Co5 96.426(15) . . ?
Co6 Co4 Co5 60.122(11) . . ?
C51 Co5 C52 103.40(7) . . ?
C51 Co5 C4 138.54(7) . . ?
C52 Co5 C4 105.42(7) . . ?
C51 Co5 P5 107.78(5) . . ?
C52 Co5 P5 94.15(5) . . ?
C4 Co5 P5 99.21(5) . . ?
C51 Co5 Co6 95.47(5) . . ?
C52 Co5 Co6 100.69(5) . . ?
C4 Co5 Co6 50.33(4) . . ?
P5 Co5 Co6 148.676(15) . . ?
C51 Co5 Co4 95.82(5) . . ?
C52 Co5 Co4 153.95(5) . . ?
C4 Co5 Co4 49.41(4) . . ?
P5 Co5 Co4 96.565(15) . . ?
Co6 Co5 Co4 59.591(12) . . ?
C62 Co6 C63 99.16(7) . . ?
C62 Co6 C61 101.25(7) . . ?
C63 Co6 C61 105.73(8) . . ?
C62 Co6 C4 111.14(7) . . ?
C63 Co6 C4 95.24(7) . . ?
C61 Co6 C4 137.83(7) . . ?
C62 Co6 Co4 151.97(5) . . ?
C63 Co6 Co4 102.51(5) . . ?
C61 Co6 Co4 89.81(5) . . ?
C4 Co6 Co4 49.53(4) . . ?
C62 Co6 Co5 91.79(5) . . ?
C63 Co6 Co5 143.60(5) . . ?
C61 Co6 Co5 105.96(6) . . ?
C4 Co6 Co5 48.66(4) . . ?
Co4 Co6 Co5 60.287(11) . . ?
O41 C41 Co4 178.96(16) . . ?
O42 C42 Co4 177.50(15) . . ?
O51 C51 Co5 175.94(16) . . ?
O52 C52 Co5 179.23(14) . . ?
O61 C61 Co6 178.48(16) . . ?
O62 C62 Co6 178.30(15) . . ?
O63 C63 Co6 177.42(16) . . ?
C5 C4 Co5 139.50(11) . . ?
C5 C4 Co4 124.45(10) . . ?
Co5 C4 Co4 81.88(6) . . ?
C5 C4 Co6 129.37(11) . . ?
Co5 C4 Co6 81.01(6) . . ?
Co4 C4 Co6 79.98(6) . . ?
C6 C5 C4 173.54(15) . . ?
C5 C6 C231 173.10(16) . . ?
C236 C231 C232 116.63(14) . . ?
C236 C231 C6 121.88(15) . . ?
C232 C231 C6 121.47(15) . . ?
F232 C232 C233 118.75(16) . . ?
F232 C232 C231 119.45(14) . . ?
C233 C232 C231 121.80(16) . . ?
F233 C233 C234 120.11(16) . . ?
F233 C233 C232 120.48(17) . . ?
C234 C233 C232 119.41(17) . . ?
F234 C234 C235 120.07(17) . . ?
F234 C234 C233 119.24(18) . . ?
C235 C234 C233 120.68(15) . . ?
F235 C235 C234 119.96(16) . . ?
F235 C235 C236 120.82(17) . . ?
C234 C235 C236 119.21(17) . . ?
F236 C236 C235 118.22(16) . . ?
F236 C236 C231 119.51(14) . . ?
C235 C236 C231 122.26(17) . . ?
C411 P4 C421 103.74(7) . . ?
C411 P4 C20 103.13(7) . . ?
C421 P4 C20 102.71(7) . . ?
C411 P4 Co4 115.25(5) . . ?
C421 P4 Co4 119.65(5) . . ?
C20 P4 Co4 110.45(5) . . ?
C412 C411 C416 118.55(14) . . ?
C412 C411 P4 118.19(12) . . ?
C416 C411 P4 123.15(11) . . ?
C413 C412 C411 120.96(15) . . ?
C413 C412 H412 119.5 . . ?
C411 C412 H412 119.5 . . ?
C412 C413 C414 119.94(16) . . ?
C412 C413 H413 120 . . ?
C414 C413 H413 120 . . ?
C415 C414 C413 119.38(15) . . ?
C415 C414 H414 120.3 . . ?
C413 C414 H414 120.3 . . ?
C414 C415 C416 120.66(15) . . ?
C414 C415 H415 119.7 . . ?
C416 C415 H415 119.7 . . ?
C415 C416 C411 120.49(15) . . ?
C415 C416 H416 119.8 . . ?
C411 C416 H416 119.8 . . ?
C426 C421 C422 118.54(13) . . ?
C426 C421 P4 119.68(11) . . ?
C422 C421 P4 121.65(11) . . ?
C423 C422 C421 120.26(15) . . ?
C423 C422 H422 119.9 . . ?
C421 C422 H422 119.9 . . ?
C422 C423 C424 120.59(15) . . ?
C422 C423 H423 119.7 . . ?
C424 C423 H423 119.7 . . ?
C425 C424 C423 119.39(15) . . ?
C425 C424 H424 120.3 . . ?
C423 C424 H424 120.3 . . ?
C426 C425 C424 120.40(15) . . ?
C426 C425 H425 119.8 . . ?
C424 C425 H425 119.8 . . ?
C425 C426 C421 120.83(14) . . ?
C425 C426 H426 119.6 . . ?
C421 C426 H426 119.6 . . ?
P4 C20 P5 109.46(7) . . ?
P4 C20 H20A 109.8 . . ?
P5 C20 H20A 109.8 . . ?
P4 C20 H20B 109.8 . . ?
P5 C20 H20B 109.8 . . ?
H20A C20 H20B 108.2 . . ?
C521 P5 C511 102.11(7) . . ?
C521 P5 C20 103.91(7) . . ?
C511 P5 C20 101.22(7) . . ?
C521 P5 Co5 123.02(5) . . ?
C511 P5 Co5 115.31(5) . . ?
C20 P5 Co5 108.68(5) . . ?
C516 C511 C512 119.21(14) . . ?
C516 C511 P5 121.98(12) . . ?
C512 C511 P5 118.79(12) . . ?
C513 C512 C511 120.14(15) . . ?
C513 C512 H512 119.9 . . ?
C511 C512 H512 119.9 . . ?
C512 C513 C514 120.15(17) . . ?
C512 C513 H513 119.9 . . ?
C514 C513 H513 119.9 . . ?
C515 C514 C513 119.58(16) . . ?
C515 C514 H514 120.2 . . ?
C513 C514 H514 120.2 . . ?
C514 C515 C516 120.74(16) . . ?
C514 C515 H515 119.6 . . ?
C516 C515 H515 119.6 . . ?
C511 C516 C515 120.06(15) . . ?
C511 C516 H516 120 . . ?
C515 C516 H516 120 . . ?
C522 C521 C526 118.49(14) . . ?
C522 C521 P5 120.50(11) . . ?
C526 C521 P5 120.96(11) . . ?
C523 C522 C521 121.04(14) . . ?
C523 C522 H522 119.5 . . ?
C521 C522 H522 119.5 . . ?
C524 C523 C522 120.09(14) . . ?
C524 C523 H523 120 . . ?
C522 C523 H523 120 . . ?
C523 C524 C525 119.43(15) . . ?
C523 C524 H524 120.3 . . ?
C525 C524 H524 120.3 . . ?
C526 C525 C524 120.63(15) . . ?
C526 C525 H525 119.7 . . ?
C524 C525 H525 119.7 . . ?
C525 C526 C521 120.30(15) . . ?
C525 C526 H526 119.8 . . ?
C521 C526 H526 119.8 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 C12 1.7803(16) . ?
Co1 C11 1.7962(16) . ?
Co1 C1 1.8998(14) . ?
Co1 P1 2.2014(5) . ?
Co1 Co2 2.4781(5) . ?
Co1 Co3 2.4810(4) . ?
Co2 C22 1.7912(16) . ?
Co2 C21 1.8162(16) . ?
Co2 C1 1.9140(15) . ?
Co2 P2 2.2035(4) . ?
Co2 Co3 2.4805(4) . ?
Co3 C32 1.7871(16) . ?
Co3 C33 1.8012(17) . ?
Co3 C31 1.8063(15) . ?
Co3 C1 1.9468(14) . ?
C11 O11 1.1486(18) . ?
C12 O12 1.1437(19) . ?
C21 O21 1.1440(18) . ?
C22 O22 1.1441(19) . ?
C31 O31 1.1440(18) . ?
C32 O32 1.1475(19) . ?
C33 O33 1.142(2) . ?
C1 C2 1.403(2) . ?
C2 C3 1.213(2) . ?
C3 C131 1.428(2) . ?
C131 C132 1.389(2) . ?
C131 C136 1.399(2) . ?
C132 F132 1.3389(19) . ?
C132 C133 1.385(2) . ?
C133 F133 1.347(2) . ?
C133 C134 1.383(3) . ?
C134 F134 1.3461(18) . ?
C134 C135 1.372(2) . ?
C135 F135 1.3413(19) . ?
C135 C136 1.382(2) . ?
C136 F136 1.3413(18) . ?
P1 C111 1.8229(15) . ?
P1 C121 1.8242(15) . ?
P1 C10 1.8343(15) . ?
C111 C112 1.395(2) . ?
C111 C116 1.398(2) . ?
C112 C113 1.391(2) . ?
C112 H112 0.95 . ?
C113 C114 1.377(3) . ?
C113 H113 0.95 . ?
C114 C115 1.380(3) . ?
C114 H114 0.95 . ?
C115 C116 1.396(2) . ?
C115 H115 0.95 . ?
C116 H116 0.95 . ?
C121 C126 1.399(2) . ?
C121 C122 1.401(2) . ?
C122 C123 1.395(2) . ?
C122 H122 0.95 . ?
C123 C124 1.381(2) . ?
C123 H123 0.95 . ?
C124 C125 1.394(2) . ?
C124 H124 0.95 . ?
C125 C126 1.391(2) . ?
C125 H125 0.95 . ?
C126 H126 0.95 . ?
C10 P2 1.8387(14) . ?
C10 H10A 0.99 . ?
C10 H10B 0.99 . ?
P2 C211 1.8230(15) . ?
P2 C221 1.8279(15) . ?
C211 C216 1.397(2) . ?
C211 C212 1.399(2) . ?
C212 C213 1.396(2) . ?
C212 H212 0.95 . ?
C213 C214 1.383(2) . ?
C213 H213 0.95 . ?
C214 C215 1.384(2) . ?
C214 H214 0.95 . ?
C215 C216 1.385(2) . ?
C215 H215 0.95 . ?
C216 H216 0.95 . ?
C221 C226 1.394(2) . ?
C221 C222 1.407(2) . ?
C222 C223 1.385(2) . ?
C222 H222 0.95 . ?
C223 C224 1.388(3) . ?
C223 H223 0.95 . ?
C224 C225 1.386(3) . ?
C224 H224 0.95 . ?
C225 C226 1.393(2) . ?
C225 H225 0.95 . ?
C226 H226 0.95 . ?
Co4 C42 1.7916(17) . ?
Co4 C41 1.8064(17) . ?
Co4 C4 1.9130(14) . ?
Co4 P4 2.2067(5) . ?
Co4 Co6 2.4763(4) . ?
Co4 Co5 2.4938(4) . ?
Co5 C51 1.7986(17) . ?
Co5 C52 1.7990(16) . ?
Co5 C4 1.8926(15) . ?
Co5 P5 2.2108(5) . ?
Co5 Co6 2.4897(4) . ?
Co6 C62 1.7947(16) . ?
Co6 C63 1.8031(17) . ?
Co6 C61 1.8092(17) . ?
Co6 C4 1.9401(14) . ?
C41 O41 1.141(2) . ?
C42 O42 1.140(2) . ?
C51 O51 1.1456(19) . ?
C52 O52 1.1389(19) . ?
C61 O61 1.141(2) . ?
C62 O62 1.1432(18) . ?
C63 O63 1.136(2) . ?
C4 C5 1.404(2) . ?
C5 C6 1.208(2) . ?
C6 C231 1.430(2) . ?
C231 C236 1.397(2) . ?
C231 C232 1.399(2) . ?
C232 F232 1.339(2) . ?
C232 C233 1.384(2) . ?
C233 F233 1.338(2) . ?
C233 C234 1.383(3) . ?
C234 F234 1.3416(19) . ?
C234 C235 1.374(3) . ?
C235 F235 1.341(2) . ?
C235 C236 1.384(2) . ?
C236 F236 1.343(2) . ?
P4 C411 1.8221(15) . ?
P4 C421 1.8306(15) . ?
P4 C20 1.8350(14) . ?
C411 C412 1.397(2) . ?
C411 C416 1.400(2) . ?
C412 C413 1.387(2) . ?
C412 H412 0.95 . ?
C413 C414 1.404(2) . ?
C413 H413 0.95 . ?
C414 C415 1.381(2) . ?
C414 H414 0.95 . ?
C415 C416 1.392(2) . ?
C415 H415 0.95 . ?
C416 H416 0.95 . ?
C421 C426 1.403(2) . ?
C421 C422 1.405(2) . ?
C422 C423 1.385(2) . ?
C422 H422 0.95 . ?
C423 C424 1.393(2) . ?
C423 H423 0.95 . ?
C424 C425 1.392(2) . ?
C424 H424 0.95 . ?
C425 C426 1.379(2) . ?
C425 H425 0.95 . ?
C426 H426 0.95 . ?
C20 P5 1.8375(14) . ?
C20 H20A 0.99 . ?
C20 H20B 0.99 . ?
P5 C521 1.8324(15) . ?
P5 C511 1.8366(15) . ?
C511 C516 1.392(2) . ?
C511 C512 1.401(2) . ?
C512 C513 1.387(2) . ?
C512 H512 0.95 . ?
C513 C514 1.401(3) . ?
C513 H513 0.95 . ?
C514 C515 1.373(3) . ?
C514 H514 0.95 . ?
C515 C516 1.394(2) . ?
C515 H515 0.95 . ?
C516 H516 0.95 . ?
C521 C522 1.395(2) . ?
C521 C526 1.402(2) . ?
C522 C523 1.389(2) . ?
C522 H522 0.95 . ?
C523 C524 1.388(2) . ?
C523 H523 0.95 . ?
C524 C525 1.392(2) . ?
C524 H524 0.95 . ?
C525 C526 1.388(2) . ?
C525 H525 0.95 . ?
C526 H526 0.95 . ?
