#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:04:14 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179774 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/70/7007021.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7007021
loop_
_publ_author_name
'Liu, Fenghui'
'Chen, Wanzhi'
'Wang, Daqi'
_publ_section_title
;
 Synthesis and characterization of amidate bridged dimeric and
 oligomeric platinum complexes having short platinum-platinum
 interactions.
;
_journal_issue                   28
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3445
_journal_page_last               3453
_journal_paper_doi               10.1039/b516410a
_journal_year                    2006
_chemical_formula_sum            'C26 H60 N12 O16 Pd Pt2'
_chemical_formula_weight         1293.44
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                113.877(5)
_cell_angle_beta                 104.490(6)
_cell_angle_gamma                103.086(6)
_cell_formula_units_Z            1
_cell_length_a                   10.644(5)
_cell_length_b                   11.104(5)
_cell_length_c                   11.577(5)
_cell_measurement_temperature    293(2)
_cell_volume                     1125.4(9)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.856
_diffrn_measured_fraction_theta_max 0.856
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0260
_diffrn_reflns_av_sigmaI/netI    0.0521
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            3323
_diffrn_reflns_theta_full        22.98
_diffrn_reflns_theta_max         22.98
_diffrn_reflns_theta_min         4.82
_exptl_absorpt_coefficient_mu    6.669
_exptl_absorpt_correction_T_max  0.6904
_exptl_absorpt_correction_T_min  0.2760
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.908
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             630
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.06
_refine_diff_density_max         2.513
_refine_diff_density_min         -1.935
_refine_diff_density_rms         0.220
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     253
_refine_ls_number_reflns         2679
_refine_ls_number_restraints     1393
_refine_ls_restrained_S_all      0.931
_refine_ls_R_factor_all          0.0617
_refine_ls_R_factor_gt           0.0564
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1034P)²+10.1755P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1558
_refine_ls_wR_factor_ref         0.1615
_reflns_number_gt                2398
_reflns_number_total             2679
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b516410a.txt
_cod_data_source_block           pr
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7007021
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd1 Pd 0.5000 1.0000 0.5000 0.0325(3) Uani 1 2 d S . .
Pt1 Pt 0.61443(5) 0.95307(5) 0.70219(4) 0.0393(2) Uani 1 1 d . . .
N1 N 0.6042(14) 0.7775(15) 0.5438(14) 0.0672(18) Uani 1 1 d U . .
H1 H 0.6391 0.7232 0.5654 0.081 Uiso 1 1 calc R . .
N2 N 0.4136(14) 0.8654(14) 0.6699(13) 0.0632(17) Uani 1 1 d U . .
H2 H 0.3979 0.8301 0.7210 0.076 Uiso 1 1 calc R . .
N3 N 0.6419(14) 1.1409(15) 0.8638(14) 0.0691(19) Uani 1 1 d U . .
H3D H 0.5980 1.1878 0.8314 0.083 Uiso 1 1 calc R . .
H3E H 0.6022 1.1220 0.9176 0.083 Uiso 1 1 calc R . .
N4 N 0.8216(15) 1.0556(15) 0.7462(15) 0.0743(19) Uani 1 1 d U . .
H4D H 0.8749 1.0164 0.7805 0.089 Uiso 1 1 calc R . .
H4E H 0.8335 1.0492 0.6699 0.089 Uiso 1 1 calc R . .
N5 N 0.5923(13) 0.8587(15) 0.9721(13) 0.073(2) Uani 1 1 d DU . .
N6 N 0.8584(15) 0.7419(14) 0.7753(14) 0.082(2) Uani 1 1 d DU . .
O1 O 0.4958(11) 0.8110(11) 0.3701(10) 0.0618(12) Uani 1 1 d U . .
O2 O 0.3144(11) 0.9029(11) 0.4947(10) 0.0618(12) Uani 1 1 d U . .
O3 O 0.4646(10) 0.8292(13) 0.9164(11) 0.076(2) Uani 1 1 d DU . .
O4 O 0.6731(12) 0.8839(14) 0.9169(12) 0.087(2) Uani 1 1 d DU . .
O5 O 0.6393(13) 0.8637(15) 1.0833(11) 0.096(3) Uani 1 1 d DU . .
O6 O 0.9355(14) 0.8702(12) 0.8371(13) 0.108(3) Uani 1 1 d DU . .
O7 O 0.9017(16) 0.6732(14) 0.8354(14) 0.120(4) Uani 1 1 d DU . .
O8 O 0.8004(15) 0.6761(14) 0.6545(12) 0.114(3) Uani 1 1 d DU . .
C1 C 0.5523(18) 0.7358(18) 0.4145(17) 0.0671(19) Uani 1 1 d U . .
C2 C 0.5529(18) 0.6043(18) 0.3055(17) 0.069(2) Uani 1 1 d U . .
C3 C 0.596(2) 0.507(2) 0.353(2) 0.092(3) Uani 1 1 d U . .
H3A H 0.6698 0.5617 0.4416 0.138 Uiso 1 1 calc R . .
H3B H 0.6270 0.4469 0.2893 0.138 Uiso 1 1 calc R . .
H3C H 0.5170 0.4490 0.3576 0.138 Uiso 1 1 calc R . .
C4 C 0.670(2) 0.659(2) 0.255(2) 0.095(4) Uani 1 1 d U . .
H4A H 0.6348 0.6978 0.1992 0.143 Uiso 1 1 calc R . .
H4B H 0.6923 0.5805 0.2020 0.143 Uiso 1 1 calc R . .
H4C H 0.7521 0.7301 0.3326 0.143 Uiso 1 1 calc R . .
C5 C 0.418(2) 0.526(2) 0.185(2) 0.101(4) Uani 1 1 d U . .
H5A H 0.3542 0.4619 0.1993 0.152 Uiso 1 1 calc R . .
H5B H 0.4331 0.4733 0.1043 0.152 Uiso 1 1 calc R . .
H5C H 0.3782 0.5922 0.1740 0.152 Uiso 1 1 calc R . .
C6 C 0.3043(17) 0.8561(17) 0.5803(16) 0.0635(19) Uani 1 1 d U . .
C7 C 0.1555(16) 0.7851(17) 0.5634(16) 0.062(2) Uani 1 1 d U . .
C8 C 0.0791(19) 0.6545(19) 0.4179(18) 0.080(3) Uani 1 1 d U . .
H8A H 0.0871 0.6834 0.3514 0.120 Uiso 1 1 calc R . .
H8B H -0.0177 0.6144 0.4013 0.120 Uiso 1 1 calc R . .
H8C H 0.1208 0.5850 0.4108 0.120 Uiso 1 1 calc R . .
C9 C 0.0829(17) 0.8936(18) 0.5805(18) 0.070(3) Uani 1 1 d U . .
H9A H 0.1316 0.9743 0.6706 0.105 Uiso 1 1 calc R . .
H9B H -0.0120 0.8503 0.5680 0.105 Uiso 1 1 calc R . .
H9C H 0.0839 0.9236 0.5136 0.105 Uiso 1 1 calc R . .
C10 C 0.1521(18) 0.7387(18) 0.6722(17) 0.070(3) Uani 1 1 d U . .
H10A H 0.1927 0.6678 0.6602 0.104 Uiso 1 1 calc R . .
H10B H 0.0572 0.7003 0.6619 0.104 Uiso 1 1 calc R . .
H10C H 0.2045 0.8192 0.7619 0.104 Uiso 1 1 calc R . .
C11 C 0.7864(18) 1.230(2) 0.9445(18) 0.080(2) Uani 1 1 d DU . .
H11 H 0.8187 1.1845 0.9964 0.096 Uiso 1 1 calc R . .
C12 C 0.8613(19) 1.207(2) 0.8487(18) 0.083(2) Uani 1 1 d DU . .
H12A H 0.8434 1.2587 0.8003 0.100 Uiso 1 1 calc R . .
H12B H 0.9609 1.2460 0.9021 0.100 Uiso 1 1 calc R . .
C13 C 0.815(2) 1.371(2) 1.050(2) 0.105(4) Uani 1 1 d U . .
H13A H 0.9040 1.4044 1.1219 0.157 Uiso 1 1 calc R . .
H13B H 0.7435 1.3697 1.0858 0.157 Uiso 1 1 calc R . .
H13C H 0.8183 1.4339 1.0117 0.157 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Pd1 O2 180.0 2_676 . ?
O2 Pd1 O1 90.6(4) 2_676 . ?
O2 Pd1 O1 89.4(4) . . ?
O2 Pd1 O1 89.4(4) 2_676 2_676 ?
O2 Pd1 O1 90.6(4) . 2_676 ?
O1 Pd1 O1 180.0 . 2_676 ?
O2 Pd1 Pt1 92.8(3) 2_676 . ?
O2 Pd1 Pt1 87.2(3) . . ?
O1 Pd1 Pt1 87.4(3) . . ?
O1 Pd1 Pt1 92.6(3) 2_676 . ?
O2 Pd1 Pt1 87.2(3) 2_676 2_676 ?
O2 Pd1 Pt1 92.8(3) . 2_676 ?
O1 Pd1 Pt1 92.6(3) . 2_676 ?
O1 Pd1 Pt1 87.4(3) 2_676 2_676 ?
Pt1 Pd1 Pt1 180.0 . 2_676 ?
N2 Pt1 N1 92.3(6) . . ?
N2 Pt1 N3 92.8(5) . . ?
N1 Pt1 N3 174.8(5) . . ?
N2 Pt1 N4 176.1(5) . . ?
N1 Pt1 N4 91.6(6) . . ?
N3 Pt1 N4 83.3(6) . . ?
N2 Pt1 Pd1 82.0(3) . . ?
N1 Pt1 Pd1 81.4(4) . . ?
N3 Pt1 Pd1 98.2(4) . . ?
N4 Pt1 Pd1 98.5(4) . . ?
C1 N1 Pt1 128.7(11) . . ?
C1 N1 H1 115.7 . . ?
Pt1 N1 H1 115.7 . . ?
C6 N2 Pt1 127.3(10) . . ?
C6 N2 H2 116.4 . . ?
Pt1 N2 H2 116.4 . . ?
C11 N3 Pt1 112.9(10) . . ?
C11 N3 H3D 109.0 . . ?
Pt1 N3 H3D 109.0 . . ?
C11 N3 H3E 109.0 . . ?
Pt1 N3 H3E 109.0 . . ?
H3D N3 H3E 107.8 . . ?
C12 N4 Pt1 107.0(10) . . ?
C12 N4 H4D 110.3 . . ?
Pt1 N4 H4D 110.3 . . ?
C12 N4 H4E 110.3 . . ?
Pt1 N4 H4E 110.3 . . ?
H4D N4 H4E 108.6 . . ?
O5 N5 O4 119.3(12) . . ?
O5 N5 O3 120.1(11) . . ?
O4 N5 O3 120.6(11) . . ?
O8 N6 O6 122.4(13) . . ?
O8 N6 O7 116.4(13) . . ?
O6 N6 O7 112.5(12) . . ?
C1 O1 Pd1 121.6(10) . . ?
C6 O2 Pd1 121.4(10) . . ?
N1 C1 O1 120.7(15) . . ?
N1 C1 C2 124.1(14) . . ?
O1 C1 C2 115.2(13) . . ?
C5 C2 C1 111.7(15) . . ?
C5 C2 C3 111.0(16) . . ?
C1 C2 C3 115.2(14) . . ?
C5 C2 C4 107.1(16) . . ?
C1 C2 C4 105.3(14) . . ?
C3 C2 C4 106.0(15) . . ?
C2 C3 H3A 109.5 . . ?
C2 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C2 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C2 C4 H4A 109.5 . . ?
C2 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C2 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C2 C5 H5A 109.5 . . ?
C2 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C2 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
N2 C6 O2 122.2(15) . . ?
N2 C6 C7 122.8(12) . . ?
O2 C6 C7 115.0(13) . . ?
C6 C7 C10 112.0(12) . . ?
C6 C7 C9 108.0(12) . . ?
C10 C7 C9 108.3(13) . . ?
C6 C7 C8 108.1(13) . . ?
C10 C7 C8 110.1(13) . . ?
C9 C7 C8 110.3(13) . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C7 C9 H9A 109.5 . . ?
C7 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C7 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C7 C10 H10A 109.5 . . ?
C7 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C7 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
N3 C11 C13 116.7(15) . . ?
N3 C11 C12 107.0(15) . . ?
C13 C11 C12 120.8(17) . . ?
N3 C11 H11 103.3 . . ?
C13 C11 H11 103.3 . . ?
C12 C11 H11 103.3 . . ?
N4 C12 C11 114.9(15) . . ?
N4 C12 H12A 108.5 . . ?
C11 C12 H12A 108.5 . . ?
N4 C12 H12B 108.5 . . ?
C11 C12 H12B 108.5 . . ?
H12A C12 H12B 107.5 . . ?
C11 C13 H13A 109.5 . . ?
C11 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C11 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pd1 O2 1.998(10) 2_676 ?
Pd1 O2 1.998(10) . ?
Pd1 O1 2.009(11) . ?
Pd1 O1 2.009(11) 2_676 ?
Pd1 Pt1 2.6613(10) . ?
Pd1 Pt1 2.6613(10) 2_676 ?
Pt1 N2 2.005(13) . ?
Pt1 N1 2.021(14) . ?
Pt1 N3 2.056(14) . ?
Pt1 N4 2.062(14) . ?
N1 C1 1.29(2) . ?
N1 H1 0.8600 . ?
N2 C6 1.302(19) . ?
N2 H2 0.8600 . ?
N3 C11 1.44(2) . ?
N3 H3D 0.9000 . ?
N3 H3E 0.9000 . ?
N4 C12 1.49(2) . ?
N4 H4D 0.9000 . ?
N4 H4E 0.9000 . ?
N5 O5 1.232(11) . ?
N5 O4 1.240(12) . ?
N5 O3 1.249(11) . ?
N6 O8 1.186(12) . ?
N6 O6 1.252(12) . ?
N6 O7 1.307(12) . ?
O1 C1 1.321(17) . ?
O2 C6 1.306(16) . ?
C1 C2 1.50(2) . ?
C2 C5 1.49(2) . ?
C2 C3 1.50(2) . ?
C2 C4 1.60(2) . ?
C3 H3A 0.9600 . ?
C3 H3B 0.9600 . ?
C3 H3C 0.9600 . ?
C4 H4A 0.9600 . ?
C4 H4B 0.9600 . ?
C4 H4C 0.9600 . ?
C5 H5A 0.9600 . ?
C5 H5B 0.9600 . ?
C5 H5C 0.9600 . ?
C6 C7 1.52(2) . ?
C7 C10 1.546(19) . ?
C7 C9 1.55(2) . ?
C7 C8 1.55(2) . ?
C8 H8A 0.9600 . ?
C8 H8B 0.9600 . ?
C8 H8C 0.9600 . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
C11 C13 1.44(3) . ?
C11 C12 1.495(15) . ?
C11 H11 0.9800 . ?
C12 H12A 0.9700 . ?
C12 H12B 0.9700 . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O2 Pd1 Pt1 N2 179.3(5) 2_676 . . . ?
O2 Pd1 Pt1 N2 -0.7(5) . . . . ?
O1 Pd1 Pt1 N2 -90.3(5) . . . . ?
O1 Pd1 Pt1 N2 89.7(5) 2_676 . . . ?
O2 Pd1 Pt1 N1 -87.2(5) 2_676 . . . ?
O2 Pd1 Pt1 N1 92.8(5) . . . . ?
O1 Pd1 Pt1 N1 3.3(5) . . . . ?
O1 Pd1 Pt1 N1 -176.7(5) 2_676 . . . ?
O2 Pd1 Pt1 N3 87.6(5) 2_676 . . . ?
O2 Pd1 Pt1 N3 -92.4(5) . . . . ?
O1 Pd1 Pt1 N3 178.1(4) . . . . ?
O1 Pd1 Pt1 N3 -1.9(4) 2_676 . . . ?
O2 Pd1 Pt1 N4 3.2(5) 2_676 . . . ?
O2 Pd1 Pt1 N4 -176.8(5) . . . . ?
O1 Pd1 Pt1 N4 93.7(5) . . . . ?
O1 Pd1 Pt1 N4 -86.3(5) 2_676 . . . ?
N2 Pt1 N1 C1 78.7(15) . . . . ?
N4 Pt1 N1 C1 -101.2(15) . . . . ?
Pd1 Pt1 N1 C1 -2.9(14) . . . . ?
N1 Pt1 N2 C6 -81.2(14) . . . . ?
N3 Pt1 N2 C6 97.8(14) . . . . ?
Pd1 Pt1 N2 C6 -0.2(13) . . . . ?
N2 Pt1 N3 C11 165.7(11) . . . . ?
N4 Pt1 N3 C11 -14.4(11) . . . . ?
Pd1 Pt1 N3 C11 -112.1(10) . . . . ?
N1 Pt1 N4 C12 169.8(11) . . . . ?
N3 Pt1 N4 C12 -9.1(10) . . . . ?
Pd1 Pt1 N4 C12 88.2(10) . . . . ?
O2 Pd1 O1 C1 87.6(11) 2_676 . . . ?
O2 Pd1 O1 C1 -92.4(11) . . . . ?
Pt1 Pd1 O1 C1 -5.1(11) . . . . ?
Pt1 Pd1 O1 C1 174.9(11) 2_676 . . . ?
O1 Pd1 O2 C6 89.2(11) . . . . ?
O1 Pd1 O2 C6 -90.8(11) 2_676 . . . ?
Pt1 Pd1 O2 C6 1.9(11) . . . . ?
Pt1 Pd1 O2 C6 -178.1(11) 2_676 . . . ?
Pt1 N1 C1 O1 0(2) . . . . ?
Pt1 N1 C1 C2 178.7(12) . . . . ?
Pd1 O1 C1 N1 5(2) . . . . ?
Pd1 O1 C1 C2 -174.4(10) . . . . ?
N1 C1 C2 C5 138.3(18) . . . . ?
O1 C1 C2 C5 -43(2) . . . . ?
N1 C1 C2 C3 11(2) . . . . ?
O1 C1 C2 C3 -170.5(15) . . . . ?
N1 C1 C2 C4 -105.9(18) . . . . ?
O1 C1 C2 C4 73.0(18) . . . . ?
Pt1 N2 C6 O2 2(2) . . . . ?
Pt1 N2 C6 C7 179.2(11) . . . . ?
Pd1 O2 C6 N2 -3(2) . . . . ?
Pd1 O2 C6 C7 179.7(9) . . . . ?
N2 C6 C7 C10 5(2) . . . . ?
O2 C6 C7 C10 -177.4(14) . . . . ?
N2 C6 C7 C9 124.1(16) . . . . ?
O2 C6 C7 C9 -58.2(17) . . . . ?
N2 C6 C7 C8 -116.6(17) . . . . ?
O2 C6 C7 C8 61.1(17) . . . . ?
Pt1 N3 C11 C13 172.6(14) . . . . ?
Pt1 N3 C11 C12 33.7(16) . . . . ?
Pt1 N4 C12 C11 31.7(18) . . . . ?
N3 C11 C12 N4 -44(2) . . . . ?
C13 C11 C12 N4 179.4(16) . . . . ?
