#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:34:00 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179796 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/92/7009248.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7009248
loop_
_publ_author_name
'De-qiang Ma'
'Shiro Hikichi'
'Munetaka Akita'
'Yoshihiko Moro-oka'
_publ_section_title
;
 An entry to half-sandwich complexes of first row transition metals
 (Ni, Co, Mn) containing the Kläui tripodal ligand, LOMe: synthesis
 and crystal structures of oligomeric, [LOMeM(μ-X)(L)]n
 (n = 2, 4), and monomeric complexes, LOMeM(L2)(X)
;
_journal_issue                   7
_journal_name_full               'J. Chem. Soc., Dalton Trans.'
_journal_page_first              1123
_journal_page_last               1134
_journal_paper_doi               10.1039/a909580b
_journal_year                    2000
_chemical_formula_sum            'C39 H66 Cl2 Co4 O20 P6'
_chemical_formula_weight         1347.36
_chemical_name_common            'compound 5b(Co)'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 113.004(16)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   19.005(7)
_cell_length_b                   14.9328(16)
_cell_length_c                   21.355(3)
_cell_measurement_temperature    213(2)
_cell_volume                     5579(2)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      213(2)
_diffrn_measured_fraction_theta_full 0.826
_diffrn_measured_fraction_theta_max 0.826
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0219
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            10632
_diffrn_reflns_theta_full        27.53
_diffrn_reflns_theta_max         27.53
_diffrn_reflns_theta_min         1.04
_exptl_absorpt_coefficient_mu    1.505
_exptl_crystal_density_diffrn    1.604
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2768
_refine_diff_density_max         0.696
_refine_diff_density_min         -1.679
_refine_diff_density_rms         0.180
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.816
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     796
_refine_ls_number_reflns         10632
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.816
_refine_ls_R_factor_all          0.0780
_refine_ls_R_factor_gt           0.0760
_refine_ls_shift/su_max          1.663
_refine_ls_shift/su_mean         0.109
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2061
_refine_ls_wR_factor_ref         0.2080
_reflns_number_gt                10114
_reflns_number_total             10632
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            a909580b.txt
_cod_data_source_block           5bCo
_cod_database_code               7009248
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x-1/2, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.21988(3) 1.06734(4) 0.13181(3) 0.03775(16) Uani 1 1 d . . .
Co2 Co 0.28477(3) 0.41051(3) 0.36548(3) 0.03369(15) Uani 1 1 d . . .
Co3 Co 0.24897(3) 0.83062(3) 0.21317(2) 0.03358(15) Uani 1 1 d . . .
Co4 Co 0.25776(3) 0.64706(3) 0.28489(2) 0.03342(15) Uani 1 1 d . . .
Cl1 Cl 0.51476(11) 0.28383(12) 0.22643(10) 0.0873(5) Uani 1 1 d . . .
Cl2 Cl 0.54158(9) 0.24598(11) 0.36693(8) 0.0787(4) Uani 1 1 d . . .
P1 P 0.32254(5) 1.02355(6) 0.21492(5) 0.0345(2) Uani 1 1 d . . .
P2 P 0.21277(6) 0.94359(7) 0.07618(5) 0.0411(2) Uani 1 1 d . . .
P3 P 0.14920(6) 1.00982(8) 0.17991(6) 0.0432(3) Uani 1 1 d . . .
P4 P 0.18107(5) 0.45608(6) 0.28395(5) 0.0342(2) Uani 1 1 d . . .
P5 P 0.29767(6) 0.53450(7) 0.42199(5) 0.0370(2) Uani 1 1 d . . .
P6 P 0.35378(6) 0.46472(7) 0.31449(5) 0.0370(2) Uani 1 1 d . . .
O1 O 0.20214(17) 0.70930(18) 0.19605(13) 0.0407(6) Uani 1 1 d . . .
O2 O 0.30470(17) 0.76904(18) 0.30265(14) 0.0431(7) Uani 1 1 d . . .
O11 O 0.33013(16) 0.92862(18) 0.23841(14) 0.0423(6) Uani 1 1 d . . .
O12 O 0.33396(17) 1.08919(19) 0.27739(14) 0.0439(6) Uani 1 1 d . . .
O13 O 0.39892(17) 1.0483(2) 0.20345(16) 0.0446(6) Uani 1 1 d . . .
O21 O 0.22929(19) 0.85611(19) 0.11297(14) 0.0463(7) Uani 1 1 d . . .
O22 O 0.2688(2) 0.9558(2) 0.03696(16) 0.0529(8) Uani 1 1 d . . .
O23 O 0.1330(2) 0.9358(2) 0.01272(17) 0.0647(10) Uani 1 1 d . . .
O31 O 0.16625(17) 0.9183(2) 0.21131(15) 0.0455(7) Uani 1 1 d . . .
O32 O 0.06329(19) 1.0118(3) 0.12379(19) 0.0673(10) Uani 1 1 d . . .
O33 O 0.1417(2) 1.0774(2) 0.2351(2) 0.0681(10) Uani 1 1 d . . .
O41 O 0.17559(15) 0.54963(18) 0.25851(14) 0.0407(6) Uani 1 1 d . . .
O42 O 0.16560(17) 0.3871(2) 0.22256(15) 0.0456(7) Uani 1 1 d . . .
O43 O 0.10596(16) 0.4376(2) 0.29880(16) 0.0444(6) Uani 1 1 d . . .
O51 O 0.27649(17) 0.62116(19) 0.38454(14) 0.0425(6) Uani 1 1 d . . .
O52 O 0.2497(2) 0.5226(2) 0.46850(15) 0.0486(7) Uani 1 1 d . . .
O53 O 0.38166(18) 0.5432(2) 0.47951(15) 0.0513(8) Uani 1 1 d . . .
O61 O 0.33851(17) 0.55712(19) 0.28455(15) 0.0436(6) Uani 1 1 d . . .
O62 O 0.44052(17) 0.4584(2) 0.36762(16) 0.0497(7) Uani 1 1 d . . .
O63 O 0.3562(2) 0.3975(2) 0.25666(17) 0.0527(8) Uani 1 1 d . . .
C12 C 0.3846(2) 1.0632(3) 0.3451(2) 0.0447(9) Uani 1 1 d . . .
H1 H 0.3786 1.0004 0.3514 0.045 Uiso 1 1 calc R . .
H2 H 0.3724 1.0968 0.3779 0.045 Uiso 1 1 calc R . .
H3 H 0.4365 1.0751 0.3511 0.045 Uiso 1 1 calc R . .
C13 C 0.4292(3) 0.9865(4) 0.1685(3) 0.0607(13) Uani 1 1 d . . .
H4 H 0.4173 0.9263 0.1767 0.061 Uiso 1 1 calc R . .
H5 H 0.4837 0.9935 0.1849 0.061 Uiso 1 1 calc R . .
H6 H 0.4069 0.9986 0.1205 0.061 Uiso 1 1 calc R . .
C22 C 0.2795(4) 0.8795(4) 0.0001(3) 0.0751(17) Uani 1 1 d . . .
H7 H 0.2318 0.8643 -0.0359 0.075 Uiso 1 1 calc R . .
H8 H 0.2975 0.8295 0.0306 0.075 Uiso 1 1 calc R . .
H9 H 0.3164 0.8939 -0.0187 0.075 Uiso 1 1 calc R . .
C23 C 0.0785(4) 0.8669(5) 0.0072(4) 0.099(3) Uani 1 1 d . . .
H10 H 0.0913 0.8389 0.0508 0.099 Uiso 1 1 calc R . .
H11 H 0.0794 0.8229 -0.0253 0.099 Uiso 1 1 calc R . .
H12 H 0.0284 0.8926 -0.0075 0.099 Uiso 1 1 calc R . .
C32 C 0.0026(3) 0.9764(5) 0.1409(3) 0.0803(19) Uani 1 1 d . . .
H13 H -0.0032 1.0128 0.1756 0.080 Uiso 1 1 calc R . .
H14 H 0.0149 0.9161 0.1573 0.080 Uiso 1 1 calc R . .
H15 H -0.0442 0.9765 0.1012 0.080 Uiso 1 1 calc R . .
C33 C 0.1714(3) 1.0584(4) 0.3053(3) 0.0613(12) Uani 1 1 d . . .
H16 H 0.1499 1.0033 0.3129 0.061 Uiso 1 1 calc R . .
H17 H 0.1585 1.1061 0.3290 0.061 Uiso 1 1 calc R . .
H18 H 0.2260 1.0528 0.3217 0.061 Uiso 1 1 calc R . .
C42 C 0.1079(3) 0.4081(3) 0.1572(2) 0.0550(11) Uani 1 1 d . . .
H19 H 0.1106 0.4706 0.1478 0.055 Uiso 1 1 calc R . .
H20 H 0.0585 0.3947 0.1570 0.055 Uiso 1 1 calc R . .
H21 H 0.1161 0.3730 0.1229 0.055 Uiso 1 1 calc R . .
C43 C 0.0834(3) 0.5022(4) 0.3375(3) 0.0580(12) Uani 1 1 d . . .
H22 H 0.1086 0.4890 0.3851 0.058 Uiso 1 1 calc R . .
H23 H 0.0291 0.4996 0.3244 0.058 Uiso 1 1 calc R . .
H24 H 0.0977 0.5611 0.3287 0.058 Uiso 1 1 calc R . .
C52 C 0.2435(4) 0.5990(4) 0.5076(3) 0.0719(16) Uani 1 1 d . . .
H25 H 0.2935 0.6155 0.5396 0.072 Uiso 1 1 calc R . .
H26 H 0.2117 0.5839 0.5316 0.072 Uiso 1 1 calc R . .
H27 H 0.2214 0.6483 0.4775 0.072 Uiso 1 1 calc R . .
C53 C 0.4349(3) 0.6109(4) 0.4767(3) 0.0631(13) Uani 1 1 d . . .
H28 H 0.4855 0.5959 0.5082 0.063 Uiso 1 1 calc R . .
H29 H 0.4205 0.6680 0.4885 0.063 Uiso 1 1 calc R . .
H30 H 0.4341 0.6135 0.4315 0.063 Uiso 1 1 calc R . .
C62 C 0.5002(3) 0.4933(4) 0.3489(3) 0.0584(12) Uani 1 1 d . . .
H31 H 0.5488 0.4843 0.3856 0.058 Uiso 1 1 calc R . .
H32 H 0.4921 0.5562 0.3394 0.058 Uiso 1 1 calc R . .
H33 H 0.4994 0.4628 0.3091 0.058 Uiso 1 1 calc R . .
C63 C 0.3252(3) 0.4212(4) 0.1870(3) 0.0616(13) Uani 1 1 d . . .
H34 H 0.3495 0.4747 0.1806 0.062 Uiso 1 1 calc R . .
H35 H 0.2713 0.4315 0.1725 0.062 Uiso 1 1 calc R . .
H36 H 0.3338 0.3735 0.1607 0.062 Uiso 1 1 calc R . .
C71 C 0.1424(3) 1.1687(4) 0.0853(5) 0.100(3) Uani 1 1 d . . .
C72 C 0.1807(6) 1.1419(4) 0.0431(3) 0.098(3) Uani 1 1 d . . .
C73 C 0.2570(4) 1.1583(3) 0.0775(3) 0.0722(17) Uani 1 1 d . . .
C74 C 0.2677(3) 1.1942(3) 0.1385(3) 0.0696(16) Uani 1 1 d . . .
C75 C 0.1987(5) 1.2006(4) 0.1453(3) 0.0797(19) Uani 1 1 d . . .
C81 C 0.3284(3) 0.3370(3) 0.4554(2) 0.0550(12) Uani 1 1 d . . .
C82 C 0.2489(3) 0.3245(3) 0.4242(3) 0.0524(11) Uani 1 1 d . . .
C83 C 0.2324(2) 0.2861(3) 0.3602(2) 0.0457(9) Uani 1 1 d . . .
C84 C 0.3017(3) 0.2755(3) 0.3509(2) 0.0492(10) Uani 1 1 d . . .
C85 C 0.3612(3) 0.3058(3) 0.4101(3) 0.0553(12) Uani 1 1 d . . .
C91 C 0.1573(8) 0.6721(10) 0.1377(8) 0.042(3) Uani 0.60 1 d P . .
C92 C 0.0786(7) 0.6727(7) 0.1239(6) 0.052(2) Uani 0.60 1 d P . .
C93 C 0.0273(9) 0.6368(9) 0.0637(9) 0.074(4) Uani 0.60 1 d P . .
C94 C 0.0490(10) 0.6077(17) 0.0231(9) 0.085(6) Uani 0.60 1 d P . .
C95 C 0.1316(9) 0.5952(7) 0.0322(5) 0.075(3) Uani 0.60 1 d P . .
C96 C 0.1844(7) 0.6328(9) 0.0917(6) 0.049(3) Uani 0.60 1 d P . .
C97 C 0.0533(8) 0.7154(9) 0.1774(9) 0.060(4) Uani 0.60 1 d P . .
C98 C 0.2674(7) 0.6343(8) 0.1072(6) 0.060(3) Uani 0.60 1 d P . .
C101 C 0.3470(13) 0.8082(16) 0.3601(14) 0.044(4) Uani 0.60 1 d P . .
C102 C 0.4264(10) 0.8109(10) 0.3758(8) 0.050(3) Uani 0.60 1 d P . .
C103 C 0.4734(9) 0.8543(15) 0.4362(8) 0.075(5) Uani 0.60 1 d P . .
C104 C 0.4520(17) 0.8908(19) 0.4819(13) 0.087(11) Uani 0.60 1 d P . .
C105 C 0.3687(8) 0.8879(9) 0.4664(7) 0.063(3) Uani 0.60 1 d P . .
C106 C 0.3193(11) 0.8467(13) 0.4036(9) 0.051(4) Uani 0.60 1 d P . .
C107 C 0.4592(13) 0.7718(15) 0.3283(11) 0.063(5) Uani 0.60 1 d P . .
C108 C 0.2371(8) 0.8444(8) 0.3907(8) 0.056(3) Uani 0.60 1 d P . .
C111 C 0.1325(11) 0.6867(14) 0.1435(9) 0.043(4) Uani 0.40 1 d P . .
C112 C 0.0606(12) 0.7046(15) 0.1476(9) 0.056(5) Uani 0.40 1 d P . .
C113 C -0.0050(11) 0.6800(17) 0.0907(11) 0.102(8) Uani 0.40 1 d P . .
C114 C -0.003(2) 0.641(2) 0.0354(16) 0.142(17) Uani 0.40 1 d P . .
C115 C 0.0781(18) 0.603(3) 0.0212(18) 0.098(11) Uani 0.40 1 d P . .
C116 C 0.1402(13) 0.6474(11) 0.0863(7) 0.073(6) Uani 0.40 1 d P . .
C117 C 0.0565(13) 0.7410(14) 0.2103(12) 0.069(5) Uani 0.40 1 d P . .
C118 C 0.2183(18) 0.6327(15) 0.0874(12) 0.076(7) Uani 0.40 1 d P . .
C121 C 0.368(2) 0.799(3) 0.358(2) 0.066(10) Uani 0.40 1 d P . .
C122 C 0.4431(10) 0.7862(19) 0.3519(16) 0.089(14) Uani 0.40 1 d P . .
C123 C 0.5064(17) 0.823(2) 0.417(2) 0.18(2) Uani 0.40 1 d P . .
C124 C 0.489(6) 0.858(2) 0.460(2) 0.26(6) Uani 0.40 1 d P . .
C125 C 0.417(4) 0.880(3) 0.469(2) 0.104(15) Uani 0.40 1 d P . .
C126 C 0.347(3) 0.835(2) 0.415(2) 0.16(2) Uani 0.40 1 d P . .
C127 C 0.4550(18) 0.7502(18) 0.2967(17) 0.091(8) Uani 0.40 1 d P . .
C128 C 0.267(3) 0.836(2) 0.4029(16) 0.20(3) Uani 0.40 1 d P . .
C130 C 0.4816(3) 0.2313(4) 0.2819(3) 0.0642(13) Uani 1 1 d . . .
H37 H 0.0882 1.1680 0.0733 0.119 Uiso 1 1 d . . .
H38 H 0.1585 1.1188 -0.0025 0.115 Uiso 1 1 d . . .
H39 H 0.2973 1.1476 0.0620 0.088 Uiso 1 1 d . . .
H40 H 0.3160 1.2124 0.1731 0.084 Uiso 1 1 d . . .
H41 H 0.1918 1.2249 0.1840 0.098 Uiso 1 1 d . . .
H42 H 0.3560 0.3608 0.4999 0.067 Uiso 1 1 d . . .
H43 H 0.2119 0.3384 0.4431 0.062 Uiso 1 1 d . . .
H44 H 0.1829 0.2699 0.3276 0.056 Uiso 1 1 d . . .
H45 H 0.3076 0.2493 0.3125 0.060 Uiso 1 1 d . . .
H46 H 0.4145 0.3054 0.4193 0.064 Uiso 1 1 d . . .
H47 H 0.4316 0.2543 0.2741 0.073 Uiso 1 1 d . . .
H48 H 0.4763 0.1684 0.2713 0.073 Uiso 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C72 Co1 C75 65.9(3) . . ?
C72 Co1 C71 40.1(3) . . ?
C75 Co1 C71 39.3(3) . . ?
C72 Co1 C73 38.5(3) . . ?
C75 Co1 C73 65.0(2) . . ?
C71 Co1 C73 65.7(3) . . ?
C72 Co1 C74 64.2(2) . . ?
C75 Co1 C74 38.7(3) . . ?
C71 Co1 C74 65.0(2) . . ?
C73 Co1 C74 37.8(2) . . ?
C72 Co1 P3 125.5(3) . . ?
C75 Co1 P3 97.2(2) . . ?
C71 Co1 P3 93.5(2) . . ?
C73 Co1 P3 158.94(18) . . ?
C74 Co1 P3 131.6(2) . . ?
C72 Co1 P1 143.2(3) . . ?
C75 Co1 P1 109.7(2) . . ?
C71 Co1 P1 149.0(3) . . ?
C73 Co1 P1 105.1(2) . . ?
C74 Co1 P1 89.36(15) . . ?
P3 Co1 P1 91.08(5) . . ?
C72 Co1 P2 91.93(19) . . ?
C75 Co1 P2 156.8(2) . . ?
C71 Co1 P2 118.5(3) . . ?
C73 Co1 P2 102.29(18) . . ?
C74 Co1 P2 138.1(2) . . ?
P3 Co1 P2 90.26(5) . . ?
P1 Co1 P2 92.00(4) . . ?
C81 Co2 C82 39.4(2) . . ?
C81 Co2 C84 66.35(19) . . ?
C82 Co2 C84 66.44(18) . . ?
C81 Co2 C83 65.85(18) . . ?
C82 Co2 C83 39.17(19) . . ?
C84 Co2 C83 39.66(18) . . ?
C81 Co2 C85 39.7(2) . . ?
C82 Co2 C85 66.30(19) . . ?
C84 Co2 C85 39.2(2) . . ?
C83 Co2 C85 65.89(17) . . ?
C81 Co2 P6 124.07(16) . . ?
C82 Co2 P6 159.67(14) . . ?
C84 Co2 P6 97.31(13) . . ?
C83 Co2 P6 132.49(14) . . ?
C85 Co2 P6 93.41(15) . . ?
C81 Co2 P4 144.69(16) . . ?
C82 Co2 P4 105.55(15) . . ?
C84 Co2 P4 109.20(14) . . ?
C83 Co2 P4 88.37(12) . . ?
C85 Co2 P4 148.41(15) . . ?
P6 Co2 P4 91.03(5) . . ?
C81 Co2 P5 91.09(14) . . ?
C82 Co2 P5 100.56(15) . . ?
C84 Co2 P5 156.56(14) . . ?
C83 Co2 P5 137.40(14) . . ?
C85 Co2 P5 118.44(16) . . ?
P6 Co2 P5 90.10(4) . . ?
P4 Co2 P5 92.78(4) . . ?
O1 Co3 O2 77.85(11) . . ?
O1 Co3 O31 107.22(13) . . ?
O2 Co3 O31 115.42(13) . . ?
O1 Co3 O11 160.07(12) . . ?
O2 Co3 O11 90.80(11) . . ?
O31 Co3 O11 92.41(12) . . ?
O1 Co3 O21 95.21(11) . . ?
O2 Co3 O21 152.54(13) . . ?
O31 Co3 O21 92.03(12) . . ?
O11 Co3 O21 87.33(12) . . ?
O2 Co4 O1 77.76(11) . . ?
O2 Co4 O61 108.66(13) . . ?
O1 Co4 O61 114.89(12) . . ?
O2 Co4 O41 159.49(12) . . ?
O1 Co4 O41 90.33(11) . . ?
O61 Co4 O41 91.44(12) . . ?
O2 Co4 O51 95.24(11) . . ?
O1 Co4 O51 151.99(13) . . ?
O61 Co4 O51 93.08(12) . . ?
O41 Co4 O51 87.48(12) . . ?
O11 P1 O12 109.74(16) . . ?
O11 P1 O13 107.18(17) . . ?
O12 P1 O13 98.62(17) . . ?
O11 P1 Co1 120.06(12) . . ?
O12 P1 Co1 106.49(11) . . ?
O13 P1 Co1 112.61(12) . . ?
O21 P2 O23 108.52(18) . . ?
O21 P2 O22 109.17(19) . . ?
O23 P2 O22 99.8(2) . . ?
O21 P2 Co1 120.07(13) . . ?
O23 P2 Co1 111.25(15) . . ?
O22 P2 Co1 106.10(12) . . ?
O31 P3 O33 108.12(19) . . ?
O31 P3 O32 109.3(2) . . ?
O33 P3 O32 100.4(2) . . ?
O31 P3 Co1 120.54(13) . . ?
O33 P3 Co1 110.50(16) . . ?
O32 P3 Co1 106.11(14) . . ?
O41 P4 O43 107.05(16) . . ?
O41 P4 O42 109.93(16) . . ?
O43 P4 O42 99.12(17) . . ?
O41 P4 Co2 120.01(12) . . ?
O43 P4 Co2 112.80(12) . . ?
O42 P4 Co2 105.91(12) . . ?
O51 P5 O53 108.74(17) . . ?
O51 P5 O52 109.24(17) . . ?
O53 P5 O52 99.95(18) . . ?
O51 P5 Co2 119.58(12) . . ?
O53 P5 Co2 111.09(13) . . ?
O52 P5 Co2 106.40(12) . . ?
O61 P6 O62 109.34(18) . . ?
O61 P6 O63 107.83(17) . . ?
O62 P6 O63 100.24(18) . . ?
O61 P6 Co2 120.29(12) . . ?
O62 P6 Co2 106.30(12) . . ?
O63 P6 Co2 110.98(13) . . ?
C91 O1 C111 24.1(8) . . ?
C91 O1 Co3 129.2(7) . . ?
C111 O1 Co3 125.5(8) . . ?
C91 O1 Co4 127.1(7) . . ?
C111 O1 Co4 129.1(7) . . ?
Co3 O1 Co4 102.47(12) . . ?
C121 O2 C101 19(2) . . ?
C121 O2 Co4 129.1(13) . . ?
C101 O2 Co4 130.4(11) . . ?
C121 O2 Co3 128.1(13) . . ?
C101 O2 Co3 126.0(10) . . ?
Co4 O2 Co3 101.91(12) . . ?
P1 O11 Co3 128.98(17) . . ?
C12 O12 P1 119.4(3) . . ?
C13 O13 P1 120.0(3) . . ?
P2 O21 Co3 128.62(18) . . ?
C22 O22 P2 117.3(3) . . ?
C23 O23 P2 122.6(4) . . ?
P3 O31 Co3 128.69(18) . . ?
C32 O32 P3 119.1(3) . . ?
C33 O33 P3 122.9(3) . . ?
P4 O41 Co4 129.07(17) . . ?
C42 O42 P4 118.9(3) . . ?
C43 O43 P4 119.1(3) . . ?
P5 O51 Co4 128.35(18) . . ?
C52 O52 P5 117.7(3) . . ?
C53 O53 P5 122.1(3) . . ?
P6 O61 Co4 128.60(17) . . ?
C62 O62 P6 119.2(3) . . ?
C63 O63 P6 121.8(3) . . ?
C75 C71 C72 106.3(6) . . ?
C75 C71 Co1 70.3(3) . . ?
C72 C71 Co1 69.7(3) . . ?
C73 C72 C71 107.9(6) . . ?
C73 C72 Co1 71.2(3) . . ?
C71 C72 Co1 70.2(3) . . ?
C74 C73 C72 108.5(6) . . ?
C74 C73 Co1 71.1(3) . . ?
C72 C73 Co1 70.3(3) . . ?
C73 C74 C75 109.8(6) . . ?
C73 C74 Co1 71.1(3) . . ?
C75 C74 Co1 70.3(3) . . ?
C74 C75 C71 107.4(6) . . ?
C74 C75 Co1 71.0(3) . . ?
C71 C75 Co1 70.4(3) . . ?
C82 C81 C85 108.0(4) . . ?
C82 C81 Co2 70.4(3) . . ?
C85 C81 Co2 70.5(3) . . ?
C83 C82 C81 107.9(4) . . ?
C83 C82 Co2 70.5(2) . . ?
C81 C82 Co2 70.2(3) . . ?
C82 C83 C84 108.5(4) . . ?
C82 C83 Co2 70.3(2) . . ?
C84 C83 Co2 70.0(2) . . ?
C85 C84 C83 107.7(4) . . ?
C85 C84 Co2 70.7(3) . . ?
C83 C84 Co2 70.4(2) . . ?
C84 C85 C81 107.9(4) . . ?
C84 C85 Co2 70.1(2) . . ?
C81 C85 Co2 69.8(2) . . ?
C111 C91 C116 114(4) . . ?
C111 C91 O1 85(3) . . ?
C116 C91 O1 157.7(17) . . ?
C111 C91 C96 150(4) . . ?
C116 C91 C96 36.2(13) . . ?
O1 C91 C96 123.8(11) . . ?
C111 C91 C92 32(3) . . ?
C116 C91 C92 85.2(17) . . ?
O1 C91 C92 115.8(10) . . ?
C96 C91 C92 120.4(13) . . ?
C111 C91 C118 161(4) . . ?
C116 C91 C118 49.1(14) . . ?
O1 C91 C118 110.0(12) . . ?
C96 C91 C118 14.2(10) . . ?
C92 C91 C118 134.2(14) . . ?
C111 C91 C112 10(3) . . ?
C116 C91 C112 105.5(18) . . ?
O1 C91 C112 94.5(8) . . ?
C96 C91 C112 141.5(13) . . ?
C92 C91 C112 21.7(7) . . ?
C118 C91 C112 154.5(14) . . ?
C112 C92 C111 103(2) . . ?
C112 C92 C93 117.7(18) . . ?
C111 C92 C93 136.9(18) . . ?
C112 C92 C91 121.1(16) . . ?
C111 C92 C91 18.2(17) . . ?
C93 C92 C91 119.9(14) . . ?
C112 C92 C113 68.8(19) . . ?
C111 C92 C113 163.0(17) . . ?
C93 C92 C113 48.9(13) . . ?
C91 C92 C113 164.2(15) . . ?
C112 C92 C97 11.5(14) . . ?
C111 C92 C97 100.1(18) . . ?
C93 C92 C97 122.6(15) . . ?
C91 C92 C97 117.5(11) . . ?
C113 C92 C97 74.6(16) . . ?
C112 C92 C116 155.4(16) . . ?
C111 C92 C116 56.2(14) . . ?
C93 C92 C116 80.9(12) . . ?
C91 C92 C116 39.3(9) . . ?
C113 C92 C116 127.1(15) . . ?
C97 C92 C116 156.1(12) . . ?
C112 C92 C114 110(2) . . ?
C111 C92 C114 140(2) . . ?
C93 C92 C114 9.6(15) . . ?
C91 C92 C114 125.1(18) . . ?
C113 C92 C114 42(2) . . ?
C97 C92 C114 116.7(18) . . ?
C116 C92 C114 85.8(16) . . ?
C114 C93 C113 87(6) . . ?
C114 C93 C94 78(5) . . ?
C113 C93 C94 163(2) . . ?
C114 C93 C92 150(5) . . ?
C113 C93 C92 69.4(14) . . ?
C94 C93 C92 120.3(17) . . ?
C114 C93 C115 91(6) . . ?
C113 C93 C115 165(2) . . ?
C94 C93 C115 14.2(17) . . ?
C92 C93 C115 106.1(19) . . ?
C114 C93 C112 131(5) . . ?
C113 C93 C112 46.3(13) . . ?
C94 C93 C112 142.3(16) . . ?
C92 C93 C112 23.1(8) . . ?
C115 C93 C112 128.4(18) . . ?
C114 C93 C116 134(5) . . ?
C113 C93 C116 123.2(14) . . ?
C94 C93 C116 63.9(13) . . ?
C92 C93 C116 56.5(9) . . ?
C115 C93 C116 49.7(16) . . ?
C112 C93 C116 78.7(9) . . ?
C115 C94 C114 161(7) . . ?
C115 C94 C93 136(6) . . ?
C114 C94 C93 31.6(11) . . ?
C115 C94 C95 10(4) . . ?
C114 C94 C95 155(2) . . ?
C93 C94 C95 126.3(17) . . ?
C115 C94 C116 55(5) . . ?
C114 C94 C116 109(2) . . ?
C93 C94 C116 80.8(15) . . ?
C95 C94 C116 46.4(10) . . ?
C115 C95 C96 119(3) . . ?
C115 C95 C116 84(3) . . ?
C96 C95 C116 35.2(10) . . ?
C115 C95 C94 6(2) . . ?
C96 C95 C94 114.2(13) . . ?
C116 C95 C94 79.2(16) . . ?
C115 C95 C118 141(3) . . ?
C96 C95 C118 22.9(7) . . ?
C116 C95 C118 57.1(12) . . ?
C94 C95 C118 136.3(14) . . ?
C118 C96 C116 159(3) . . ?
C118 C96 C95 105(3) . . ?
C116 C96 C95 69.6(15) . . ?
C118 C96 C91 136(3) . . ?
C116 C96 C91 50.2(14) . . ?
C95 C96 C91 118.4(13) . . ?
C118 C96 C98 19(2) . . ?
C116 C96 C98 163.3(19) . . ?
C95 C96 C98 122.4(12) . . ?
C91 C96 C98 119.1(11) . . ?
C118 C96 C111 143(3) . . ?
C116 C96 C111 41.5(13) . . ?
C95 C96 C111 110.2(12) . . ?
C91 C96 C111 8.6(10) . . ?
C98 C96 C111 127.3(11) . . ?
C118 C96 C115 128(3) . . ?
C116 C96 C115 45.5(16) . . ?
C95 C96 C115 24.1(11) . . ?
C91 C96 C115 94.5(13) . . ?
C98 C96 C115 146.1(14) . . ?
C111 C96 C115 86.1(12) . . ?
C112 C97 C117 158(3) . . ?
C112 C97 C92 14(2) . . ?
C117 C97 C92 159(2) . . ?
C112 C97 C113 45(2) . . ?
C117 C97 C113 149(2) . . ?
C92 C97 C113 50.9(13) . . ?
C112 C97 C111 35(2) . . ?
C117 C97 C111 130(2) . . ?
C92 C97 C111 29.1(8) . . ?
C113 C97 C111 79.1(13) . . ?
C118 C98 C96 15.1(16) . . ?
C121 C101 C126 123(10) . . ?
C121 C101 O2 90(10) . . ?
C126 C101 O2 143(3) . . ?
C121 C101 C106 145(10) . . ?
C126 C101 C106 22(2) . . ?
O2 C101 C106 124.6(19) . . ?
C121 C101 C102 27(9) . . ?
C126 C101 C102 99(3) . . ?
O2 C101 C102 116.2(17) . . ?
C106 C101 C102 119(2) . . ?
C121 C101 C122 8(8) . . ?
C126 C101 C122 120(3) . . ?
O2 C101 C122 95.5(17) . . ?
C106 C101 C122 140(2) . . ?
C102 C101 C122 20.8(12) . . ?
C121 C101 C128 162(9) . . ?
C126 C101 C128 42(2) . . ?
O2 C101 C128 102.4(18) . . ?
C106 C101 C128 23.0(16) . . ?
C102 C101 C128 141(2) . . ?
C122 C101 C128 161(2) . . ?
C122 C102 C121 109(4) . . ?
C122 C102 C103 122(3) . . ?
C121 C102 C103 129(3) . . ?
C122 C102 C101 120(3) . . ?
C121 C102 C101 11(4) . . ?
C103 C102 C101 118.0(18) . . ?
C122 C102 C123 82(3) . . ?
C121 C102 C123 166(3) . . ?
C103 C102 C123 41(2) . . ?
C101 C102 C123 158(3) . . ?
C122 C102 C107 4.9(19) . . ?
C121 C102 C107 110(4) . . ?
C103 C102 C107 121(2) . . ?
C101 C102 C107 121(2) . . ?
C123 C102 C107 81(3) . . ?
C122 C102 C126 155(3) . . ?
C121 C102 C126 48(3) . . ?
C103 C102 C126 81.4(16) . . ?
C101 C102 C126 37.1(17) . . ?
C123 C102 C126 121(3) . . ?
C107 C102 C126 157(2) . . ?
C122 C102 C124 122(4) . . ?
C121 C102 C124 128(5) . . ?
C103 C102 C124 5.4(16) . . ?
C101 C102 C124 117(4) . . ?
C123 C102 C124 41(4) . . ?
C107 C102 C124 121(4) . . ?
C126 C102 C124 80(4) . . ?
C124 C103 C123 106(10) . . ?
C124 C103 C104 53(10) . . ?
C123 C103 C104 159(3) . . ?
C124 C103 C102 159(6) . . ?
C123 C103 C102 71(3) . . ?
C104 C103 C102 126.9(16) . . ?
C124 C103 C125 75(10) . . ?
C123 C103 C125 167(4) . . ?
C104 C103 C125 24(2) . . ?
C102 C103 C125 103(2) . . ?
C124 C103 C122 151(10) . . ?
C123 C103 C122 51(2) . . ?
C104 C103 C122 146.8(14) . . ?
C102 C103 C122 20.1(9) . . ?
C125 C103 C122 123(3) . . ?
C124 C104 C125 117(7) . . ?
C124 C104 C103 21(4) . . ?
C125 C104 C103 99(7) . . ?
C124 C104 C105 134(4) . . ?
C125 C104 C105 18(7) . . ?
C103 C104 C105 115.8(14) . . ?
C125 C105 C106 106(4) . . ?
C125 C105 C126 88(5) . . ?
C106 C105 C126 21(2) . . ?
C125 C105 C104 12(5) . . ?
C106 C105 C104 118.0(18) . . ?
C126 C105 C104 100(3) . . ?
C125 C105 C128 132(4) . . ?
C106 C105 C128 27.2(10) . . ?
C126 C105 C128 44(2) . . ?
C104 C105 C128 144.2(18) . . ?
C125 C105 C124 7(4) . . ?
C106 C105 C124 99.2(15) . . ?
C126 C105 C124 81(3) . . ?
C104 C105 C124 19.2(14) . . ?
C128 C105 C124 125.0(15) . . ?
C126 C106 C128 141(7) . . ?
C126 C106 C105 62(7) . . ?
C128 C106 C105 111(2) . . ?
C126 C106 C101 65(7) . . ?
C128 C106 C101 125(3) . . ?
C105 C106 C101 122.1(19) . . ?
C126 C106 C108 153(7) . . ?
C128 C106 C108 12(2) . . ?
C105 C106 C108 116.1(16) . . ?
C101 C106 C108 121.7(18) . . ?
C126 C106 C125 39(6) . . ?
C128 C106 C125 137(3) . . ?
C105 C106 C125 27.1(15) . . ?
C101 C106 C125 95(2) . . ?
C108 C106 C125 143(2) . . ?
C126 C106 C121 57(7) . . ?
C128 C106 C121 132(3) . . ?
C105 C106 C121 113.7(19) . . ?
C101 C106 C121 9(2) . . ?
C108 C106 C121 130(2) . . ?
C125 C106 C121 87(2) . . ?
C127 C107 C122 150(6) . . ?
C127 C107 C102 152(5) . . ?
C122 C107 C102 5(2) . . ?
C127 C107 C121 124(4) . . ?
C122 C107 C121 26(3) . . ?
C102 C107 C121 27.6(18) . . ?
C127 C107 C123 160(4) . . ?
C122 C107 C123 49(3) . . ?
C102 C107 C123 48.2(18) . . ?
C121 C107 C123 75.6(19) . . ?
C128 C108 C106 22(5) . . ?
C91 C111 C92 130(5) . . ?
C91 C111 C116 44(3) . . ?
C92 C111 C116 89.2(19) . . ?
C91 C111 O1 71(3) . . ?
C92 C111 O1 155(2) . . ?
C116 C111 O1 114.1(17) . . ?
C91 C111 C112 166(4) . . ?
C92 C111 C112 35.8(12) . . ?
C116 C111 C112 123.8(18) . . ?
O1 C111 C112 122.1(16) . . ?
C91 C111 C96 22(3) . . ?
C92 C111 C96 110.8(18) . . ?
C116 C111 C96 23.0(10) . . ?
O1 C111 C96 91.5(11) . . ?
C112 C111 C96 146.3(16) . . ?
C91 C111 C97 168(4) . . ?
C92 C111 C97 50.8(13) . . ?
C116 C111 C97 139.9(17) . . ?
O1 C111 C97 105.8(12) . . ?
C112 C111 C97 16.9(9) . . ?
C96 C111 C97 161.2(13) . . ?
C97 C112 C92 155(3) . . ?
C97 C112 C113 114(3) . . ?
C92 C112 C113 77(2) . . ?
C97 C112 C111 128(3) . . ?
C92 C112 C111 41.2(16) . . ?
C113 C112 C111 116(2) . . ?
C97 C112 C117 11.2(16) . . ?
C92 C112 C117 156(3) . . ?
C113 C112 C117 122(3) . . ?
C111 C112 C117 121.1(18) . . ?
C97 C112 C93 146(2) . . ?
C92 C112 C93 39.2(13) . . ?
C113 C112 C93 37.4(15) . . ?
C111 C112 C93 79.6(15) . . ?
C117 C112 C93 156.7(16) . . ?
C97 C112 C91 131(2) . . ?
C92 C112 C91 37.2(12) . . ?
C113 C112 C91 113(2) . . ?
C111 C112 C91 4.1(13) . . ?
C117 C112 C91 124.4(16) . . ?
C93 C112 C91 75.9(13) . . ?
C93 C113 C114 29.7(18) . . ?
C93 C113 C112 96(2) . . ?
C114 C113 C112 124(3) . . ?
C93 C113 C92 61.7(16) . . ?
C114 C113 C92 90(3) . . ?
C112 C113 C92 34.6(11) . . ?
C93 C113 C97 115.2(17) . . ?
C114 C113 C97 144(3) . . ?
C112 C113 C97 21.1(11) . . ?
C92 C113 C97 54.4(8) . . ?
C93 C114 C94 70(5) . . ?
C93 C114 C113 63(4) . . ?
C94 C114 C113 132(2) . . ?
C93 C114 C115 67(5) . . ?
C94 C114 C115 6(2) . . ?
C113 C114 C115 128(3) . . ?
C93 C114 C92 21(3) . . ?
C94 C114 C92 84.3(17) . . ?
C113 C114 C92 48.0(13) . . ?
C115 C114 C92 79.9(18) . . ?
C94 C115 C95 163(7) . . ?
C94 C115 C116 108(6) . . ?
C95 C115 C116 59(2) . . ?
C94 C115 C93 30(4) . . ?
C95 C115 C93 135(4) . . ?
C116 C115 C93 78(2) . . ?
C94 C115 C114 13(5) . . ?
C95 C115 C114 155(4) . . ?
C116 C115 C114 97(2) . . ?
C93 C115 C114 21.7(8) . . ?
C94 C115 C96 129(6) . . ?
C95 C115 C96 36.5(18) . . ?
C116 C115 C96 22.1(10) . . ?
C93 C115 C96 99(2) . . ?
C114 C115 C96 119(2) . . ?
C96 C116 C91 93.7(19) . . ?
C96 C116 C95 75.2(19) . . ?
C91 C116 C95 163(2) . . ?
C96 C116 C111 115.5(18) . . ?
C91 C116 C111 21.9(11) . . ?
C95 C116 C111 163.9(18) . . ?
C96 C116 C118 9.5(15) . . ?
C91 C116 C118 97.6(17) . . ?
C95 C116 C118 73.4(18) . . ?
C111 C116 C118 119.1(16) . . ?
C96 C116 C115 112(2) . . ?
C91 C116 C115 150(2) . . ?
C95 C116 C115 37.2(12) . . ?
C111 C116 C115 130(2) . . ?
C118 C116 C115 110(2) . . ?
C96 C116 C92 147.0(17) . . ?
C91 C116 C92 55.5(12) . . ?
C95 C116 C92 131.0(16) . . ?
C111 C116 C92 34.6(10) . . ?
C118 C116 C92 152.9(14) . . ?
C115 C116 C92 95.3(17) . . ?
C96 C116 C94 129(2) . . ?
C91 C116 C94 133(2) . . ?
C95 C116 C94 54.4(10) . . ?
C111 C116 C94 112.6(18) . . ?
C118 C116 C94 127.8(18) . . ?
C115 C116 C94 17.4(13) . . ?
C92 C116 C94 78.0(12) . . ?
C96 C116 C93 159.5(19) . . ?
C91 C116 C93 98.0(18) . . ?
C95 C116 C93 89.3(12) . . ?
C111 C116 C93 77.3(15) . . ?
C118 C116 C93 162.3(16) . . ?
C115 C116 C93 52.7(14) . . ?
C92 C116 C93 42.7(9) . . ?
C94 C116 C93 35.3(9) . . ?
C97 C117 C112 10.3(14) . . ?
C96 C118 C98 146(4) . . ?
C96 C118 C116 12(2) . . ?
C98 C118 C116 152(2) . . ?
C96 C118 C95 52(2) . . ?
C98 C118 C95 157(2) . . ?
C116 C118 C95 49.4(12) . . ?
C96 C118 C91 30.1(19) . . ?
C98 C118 C91 119(2) . . ?
C116 C118 C91 33.2(8) . . ?
C95 C118 C91 81.8(14) . . ?
C101 C121 C102 141(10) . . ?
C101 C121 O2 71(9) . . ?
C102 C121 O2 145(4) . . ?
C101 C121 C122 169(10) . . ?
C102 C121 C122 30(2) . . ?
O2 C121 C122 116(3) . . ?
C101 C121 C126 43(9) . . ?
C102 C121 C126 103(4) . . ?
O2 C121 C126 112(3) . . ?
C122 C121 C126 132(4) . . ?
C101 C121 C106 27(8) . . ?
C102 C121 C106 116(4) . . ?
O2 C121 C106 97(2) . . ?
C122 C121 C106 147(3) . . ?
C126 C121 C106 16.3(17) . . ?
C101 C121 C107 169(8) . . ?
C102 C121 C107 42(2) . . ?
O2 C121 C107 103(3) . . ?
C122 C121 C107 12.4(15) . . ?
C126 C121 C107 145(3) . . ?
C106 C121 C107 158(3) . . ?
C102 C122 C107 170(4) . . ?
C102 C122 C121 41(3) . . ?
C107 C122 C121 141(4) . . ?
C102 C122 C127 165(3) . . ?
C107 C122 C127 15(3) . . ?
C121 C122 C127 126(3) . . ?
C102 C122 C123 68(4) . . ?
C107 C122 C123 110(4) . . ?
C121 C122 C123 109(4) . . ?
C127 C122 C123 125(3) . . ?
C102 C122 C103 38(2) . . ?
C107 C122 C103 139(3) . . ?
C121 C122 C103 79(3) . . ?
C127 C122 C103 153.7(18) . . ?
C123 C122 C103 30(2) . . ?
C102 C122 C101 39.4(18) . . ?
C107 C122 C101 142(3) . . ?
C121 C122 C101 2(2) . . ?
C127 C122 C101 128(2) . . ?
C123 C122 C101 107(3) . . ?
C103 C122 C101 77(2) . . ?
C103 C123 C124 22(5) . . ?
C103 C123 C102 68(2) . . ?
C124 C123 C102 89(6) . . ?
C103 C123 C122 98(3) . . ?
C124 C123 C122 119(6) . . ?
C102 C123 C122 30.6(14) . . ?
C103 C123 C107 118(2) . . ?
C124 C123 C107 140(6) . . ?
C102 C123 C107 51.0(15) . . ?
C122 C123 C107 20.7(16) . . ?
C103 C124 C104 106(10) . . ?
C103 C124 C125 87(10) . . ?
C104 C124 C125 22(2) . . ?
C103 C124 C123 52(10) . . ?
C104 C124 C123 157(9) . . ?
C125 C124 C123 137(9) . . ?
C103 C124 C102 16(5) . . ?
C104 C124 C102 108(7) . . ?
C125 C124 C102 86(6) . . ?
C123 C124 C102 50(3) . . ?
C103 C124 C105 83(10) . . ?
C104 C124 C105 27(3) . . ?
C125 C124 C105 4(3) . . ?
C123 C124 C105 132(6) . . ?
C102 C124 C105 82(4) . . ?
C105 C125 C104 150(10) . . ?
C105 C125 C124 169(7) . . ?
C104 C125 C124 41(6) . . ?
C105 C125 C126 57(4) . . ?
C104 C125 C126 153(9) . . ?
C124 C125 C126 112(5) . . ?
C105 C125 C106 47(3) . . ?
C104 C125 C106 161(8) . . ?
C124 C125 C106 122(4) . . ?
C126 C125 C106 12(2) . . ?
C105 C125 C103 151(6) . . ?
C104 C125 C103 57(6) . . ?
C124 C125 C103 18.3(19) . . ?
C126 C125 C103 96(4) . . ?
C106 C125 C103 105(3) . . ?
C106 C126 C101 93(7) . . ?
C106 C126 C105 97(8) . . ?
C101 C126 C105 153(4) . . ?
C106 C126 C128 26(5) . . ?
C101 C126 C128 103(3) . . ?
C105 C126 C128 97(4) . . ?
C106 C126 C121 106(7) . . ?
C101 C126 C121 14(2) . . ?
C105 C126 C121 143(4) . . ?
C128 C126 C121 117(3) . . ?
C106 C126 C125 129(8) . . ?
C101 C126 C125 122(4) . . ?
C105 C126 C125 36(2) . . ?
C128 C126 C125 133(5) . . ?
C121 C126 C125 109(4) . . ?
C106 C126 C102 131(8) . . ?
C101 C126 C102 43(2) . . ?
C105 C126 C102 115(3) . . ?
C128 C126 C102 147(3) . . ?
C121 C126 C102 30(2) . . ?
C125 C126 C102 80(3) . . ?
C107 C127 C122 15(3) . . ?
C108 C128 C106 146(7) . . ?
C108 C128 C126 159(7) . . ?
C106 C128 C126 13(2) . . ?
C108 C128 C105 141(5) . . ?
C106 C128 C105 41(2) . . ?
C126 C128 C105 39(2) . . ?
C108 C128 C101 130(5) . . ?
C106 C128 C101 32.4(15) . . ?
C126 C128 C101 35(2) . . ?
C105 C128 C101 73(2) . . ?
Cl1 C130 Cl2 113.0(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 C72 2.068(5) . ?
Co1 C75 2.072(5) . ?
Co1 C71 2.074(5) . ?
Co1 C73 2.081(5) . ?
Co1 C74 2.082(5) . ?
Co1 P3 2.1624(13) . ?
Co1 P1 2.1628(12) . ?
Co1 P2 2.1723(12) . ?
Co2 C81 2.083(4) . ?
Co2 C82 2.087(4) . ?
Co2 C84 2.084(4) . ?
Co2 C83 2.090(4) . ?
Co2 C85 2.093(4) . ?
Co2 P6 2.1628(12) . ?
Co2 P4 2.1671(12) . ?
Co2 P5 2.1710(11) . ?
Co3 O1 1.988(3) . ?
Co3 O2 2.009(3) . ?
Co3 O31 2.035(3) . ?
Co3 O11 2.040(3) . ?
Co3 O21 2.059(3) . ?
Co4 O2 1.998(3) . ?
Co4 O1 2.003(3) . ?
Co4 O61 2.042(3) . ?
Co4 O41 2.046(3) . ?
Co4 O51 2.053(3) . ?
Cl1 C130 1.732(6) . ?
Cl2 C130 1.741(6) . ?
P1 O11 1.492(3) . ?
P1 O12 1.600(3) . ?
P1 O13 1.607(3) . ?
P2 O21 1.493(3) . ?
P2 O23 1.595(3) . ?
P2 O22 1.602(3) . ?
P3 O31 1.501(3) . ?
P3 O33 1.600(4) . ?
P3 O32 1.604(4) . ?
P4 O41 1.488(3) . ?
P4 O43 1.603(3) . ?
P4 O42 1.602(3) . ?
P5 O51 1.491(3) . ?
P5 O53 1.594(3) . ?
P5 O52 1.599(3) . ?
P6 O61 1.501(3) . ?
P6 O62 1.597(3) . ?
P6 O63 1.606(3) . ?
O1 C91 1.325(17) . ?
O1 C111 1.401(19) . ?
O2 C121 1.39(4) . ?
O2 C101 1.31(3) . ?
O12 C12 1.442(5) . ?
O13 C13 1.442(6) . ?
O22 C22 1.443(6) . ?
O23 C23 1.431(7) . ?
O32 C32 1.439(7) . ?
O33 C33 1.408(6) . ?
O42 C42 1.433(5) . ?
O43 C43 1.439(5) . ?
O52 C52 1.445(5) . ?
O53 C53 1.448(6) . ?
O62 C62 1.440(5) . ?
O63 C63 1.414(6) . ?
C71 C75 1.394(11) . ?
C71 C72 1.419(12) . ?
C72 C73 1.368(11) . ?
C73 C74 1.349(9) . ?
C74 C75 1.377(9) . ?
C81 C82 1.406(7) . ?
C81 C85 1.418(8) . ?
C82 C83 1.400(7) . ?
C83 C84 1.416(6) . ?
C84 C85 1.402(7) . ?
C91 C111 0.57(2) . ?
C91 C116 1.08(2) . ?
C91 C96 1.404(16) . ?
C91 C92 1.406(15) . ?
C91 C118 1.95(3) . ?
C91 C112 1.99(3) . ?
C92 C112 0.86(2) . ?
C92 C111 0.97(2) . ?
C92 C93 1.383(18) . ?
C92 C113 1.47(2) . ?
C92 C97 1.541(16) . ?
C92 C116 1.70(3) . ?
C92 C114 1.98(2) . ?
C93 C114 0.66(2) . ?
C93 C113 1.18(3) . ?
C93 C94 1.18(3) . ?
C93 C115 1.64(4) . ?
C93 C112 1.94(3) . ?
C93 C116 2.01(3) . ?
C94 C115 0.57(3) . ?
C94 C114 1.23(5) . ?
C94 C95 1.52(2) . ?
C94 C116 1.83(2) . ?
C95 C115 0.96(3) . ?
C95 C96 1.392(16) . ?
C95 C116 1.350(19) . ?
C95 C118 1.70(3) . ?
C96 C118 0.69(2) . ?
C96 C116 0.83(2) . ?
C96 C98 1.480(15) . ?
C96 C111 1.92(3) . ?
C96 C115 2.04(4) . ?
C97 C112 0.72(2) . ?
C97 C117 0.781(19) . ?
C97 C113 1.83(3) . ?
C97 C111 1.96(2) . ?
C98 C118 0.86(3) . ?
C101 C121 0.45(5) . ?
C101 C126 1.24(6) . ?
C101 C106 1.36(3) . ?
C101 C102 1.41(2) . ?
C101 C122 1.93(4) . ?
C101 C128 2.09(5) . ?
C102 C122 0.79(4) . ?
C102 C121 1.03(4) . ?
C102 C103 1.41(2) . ?
C102 C123 1.44(3) . ?
C102 C107 1.501(18) . ?
C102 C126 2.02(6) . ?
C102 C124 1.87(6) . ?
C103 C124 0.48(5) . ?
C103 C123 0.99(5) . ?
C103 C104 1.31(4) . ?
C103 C125 1.54(6) . ?
C103 C122 1.95(4) . ?
C104 C124 1.10(12) . ?
C104 C125 0.63(6) . ?
C104 C105 1.49(4) . ?
C105 C125 0.90(6) . ?
C105 C106 1.44(2) . ?
C105 C126 1.28(4) . ?
C105 C128 2.03(6) . ?
C105 C124 2.38(12) . ?
C106 C126 0.51(5) . ?
C106 C128 0.99(5) . ?
C106 C108 1.48(3) . ?
C106 C125 1.90(7) . ?
C106 C121 1.75(5) . ?
C107 C127 0.72(3) . ?
C107 C122 0.72(4) . ?
C107 C121 2.09(4) . ?
C107 C123 1.91(5) . ?
C108 C128 0.55(5) . ?
C111 C116 1.41(3) . ?
C111 C112 1.43(3) . ?
C112 C113 1.41(2) . ?
C112 C117 1.47(3) . ?
C113 C114 1.33(5) . ?
C114 C115 1.78(5) . ?
C115 C116 1.57(4) . ?
C116 C118 1.49(3) . ?
C121 C122 1.49(4) . ?
C121 C126 1.53(6) . ?
C122 C127 1.39(4) . ?
C122 C123 1.54(4) . ?
C123 C124 1.22(10) . ?
C124 C125 1.49(14) . ?
C125 C126 1.54(8) . ?
C126 C128 1.43(7) . ?
