#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:39:42 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179801 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/97/7009707.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7009707
loop_
_publ_author_name
'Yang, Shi-Ping'
'Chen, Xiao-Ming'
'Ji, Liang-Nian'
_publ_section_title
;
 Influence of the counter ions and ligands on structures of silver(I)
 helicates with di-Schiff bases containing imidazole groups
;
_journal_issue                   14
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2337
_journal_paper_doi               10.1039/b002837l
_journal_year                    2000
_chemical_formula_sum            'C26 H36 Ag3 N15 O9'
_chemical_formula_weight         1026.31
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.85
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.308(4)
_cell_length_b                   22.628(10)
_cell_length_c                   15.081(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      15
_cell_measurement_theta_min      7
_cell_volume                     3517(2)
_computing_cell_refinement       'SHELXTL-Plus (Sheldrick, 1990)'
_computing_data_collection       'SHELXTL-Plus (Sheldrick, 1990)'
_computing_data_reduction        'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SHELXTL Version 5 (Sheldrick, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.972
_diffrn_measured_fraction_theta_max 0.972
_diffrn_measurement_device_type  'Siemens R3m'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0336
_diffrn_reflns_av_sigmaI/netI    0.064
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            6556
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.17
_diffrn_standards_interval_count 150
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    1.727
_exptl_absorpt_correction_T_max  0.617
_exptl_absorpt_correction_T_min  0.503
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.938
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2040
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.852
_refine_diff_density_min         -1.020
_refine_diff_density_rms         0.126
_refine_ls_extinction_coef       0.00017(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     479
_refine_ls_number_reflns         6194
_refine_ls_number_restraints     18
_refine_ls_restrained_S_all      1.010
_refine_ls_R_factor_all          0.1352
_refine_ls_R_factor_gt           0.0610
_refine_ls_shift/su_max          0.012
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0415P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1045
_refine_ls_wR_factor_ref         0.1244
_reflns_number_gt                3373
_reflns_number_total             6194
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b002837l.txt
_cod_data_source_block           complex_5
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0415P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0415P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7009707
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.17874(6) 0.26743(2) 0.16691(4) 0.04311(17) Uani 1 d . . .
Ag2 Ag 0.26719(6) 0.24315(3) -0.01627(4) 0.04642(18) Uani 1 d . . .
Ag3 Ag 0.35165(6) 0.28574(2) -0.18657(5) 0.05208(19) Uani 1 d . . .
N1 N 0.2700(6) 0.3476(2) 0.1288(4) 0.0393(17) Uani 1 d . . .
N2 N 0.4230(6) 0.4124(2) 0.1056(4) 0.0424(17) Uani 1 d . . .
N3 N 0.4517(5) 0.2566(2) 0.0568(4) 0.0375(16) Uani 1 d . . .
N4 N 0.3684(6) 0.1531(2) 0.1818(4) 0.0404(17) Uani 1 d . . .
N5 N 0.0447(6) 0.0909(2) 0.1788(4) 0.0438(18) Uani 1 d . . .
N6 N 0.0908(5) 0.1857(2) 0.1943(4) 0.0354(16) Uani 1 d . . .
N7 N 0.2380(6) 0.3564(2) -0.1052(4) 0.0398(17) Uani 1 d . . .
N8 N 0.0773(6) 0.4202(3) -0.0948(4) 0.0428(17) Uani 1 d . . .
N9 N 0.0565(5) 0.2652(3) -0.0492(4) 0.0405(16) Uani 1 d . . .
N10 N 0.2179(7) 0.1592(3) -0.1122(6) 0.075(3) Uani 1 d . . .
N11 N 0.4666(6) 0.2031(2) -0.1808(4) 0.0414(17) Uani 1 d . . .
N12 N 0.5354(6) 0.1118(2) -0.1783(4) 0.0428(17) Uani 1 d . . .
C1 C 0.2204(8) 0.4030(3) 0.1436(5) 0.049(2) Uani 1 d . . .
H1A H 0.1334 0.4118 0.1612 0.080 Uiso 1 d R . .
C2 C 0.3124(8) 0.4430(3) 0.1286(5) 0.048(2) Uani 1 d . . .
H2A H 0.3054 0.4851 0.1344 0.080 Uiso 1 d R . .
C3 C 0.5493(7) 0.4382(3) 0.0825(5) 0.061(3) Uani 1 d . . .
H3A H 0.6078 0.4068 0.0677 0.080 Uiso 1 d R . .
H3B H 0.5396 0.4644 0.0329 0.080 Uiso 1 d R . .
H3C H 0.5834 0.4596 0.1326 0.080 Uiso 1 d R . .
C4 C 0.3923(7) 0.3536(3) 0.1069(5) 0.036(2) Uani 1 d . . .
C5 C 0.4867(7) 0.3068(3) 0.0873(4) 0.0358(19) Uani 1 d . . .
H5A H 0.5773 0.3146 0.0971 0.080 Uiso 1 d R . .
C6 C 0.5594(7) 0.2144(3) 0.0420(5) 0.045(2) Uani 1 d . . .
H6A H 0.6324 0.2275 0.0771 0.080 Uiso 1 d R . .
H6B H 0.5835 0.2164 -0.0192 0.080 Uiso 1 d R . .
C7 C 0.5461(11) 0.1599(5) 0.0784(9) 0.171(6) Uani 1 d U . .
H7A H 0.6208 0.1375 0.0611 0.080 Uiso 1 d R . .
H7B H 0.4761 0.1476 0.0399 0.080 Uiso 1 d R . .
C8 C 0.4984(7) 0.1336(3) 0.1541(5) 0.050(2) Uani 1 d . . .
H8A H 0.5022 0.0912 0.1556 0.080 Uiso 1 d R . .
H8B H 0.5617 0.1484 0.1959 0.080 Uiso 1 d R . .
C9 C 0.2758(7) 0.1183(3) 0.1603(4) 0.036(2) Uani 1 d . . .
H9A H 0.2962 0.0825 0.1294 0.080 Uiso 1 d R . .
C10 C 0.1407(7) 0.1318(3) 0.1788(5) 0.037(2) Uani 1 d . . .
C11 C 0.0583(9) 0.0264(3) 0.1643(6) 0.071(3) Uani 1 d . . .
H11A H 0.1478 0.0173 0.1540 0.080 Uiso 1 d R . .
H11B H 0.0303 0.0062 0.2166 0.080 Uiso 1 d R . .
H11C H 0.0065 0.0138 0.1144 0.080 Uiso 1 d R . .
C12 C -0.0696(8) 0.1188(3) 0.1954(5) 0.051(2) Uani 1 d . . .
H12A H -0.1536 0.1007 0.1985 0.080 Uiso 1 d R . .
C13 C -0.0395(7) 0.1767(3) 0.2046(5) 0.039(2) Uani 1 d . . .
H13A H -0.1008 0.2072 0.2178 0.080 Uiso 1 d R . .
C14 C 0.2866(7) 0.4124(3) -0.1143(5) 0.041(2) Uani 1 d . . .
H14A H 0.3763 0.4220 -0.1226 0.080 Uiso 1 d R . .
C15 C 0.1879(7) 0.4522(3) -0.1071(5) 0.051(2) Uani 1 d . . .
H15A H 0.1937 0.4944 -0.1122 0.080 Uiso 1 d R . .
C16 C -0.0538(7) 0.4442(3) -0.0824(6) 0.063(3) Uani 1 d . . .
H16A H -0.0522 0.4865 -0.0869 0.080 Uiso 1 d R . .
H16B H -0.1100 0.4283 -0.1278 0.080 Uiso 1 d R . .
H16C H -0.0852 0.4330 -0.0252 0.080 Uiso 1 d R . .
C17 C 0.1112(7) 0.3620(3) -0.0922(5) 0.035(2) Uani 1 d . . .
C18 C 0.0183(7) 0.3146(3) -0.0785(5) 0.042(2) Uani 1 d . . .
H18A H -0.0720 0.3210 -0.0918 0.080 Uiso 1 d R . .
C19 C -0.0426(7) 0.2184(3) -0.0387(6) 0.054(2) Uani 1 d . . .
H19A H -0.1192 0.2299 -0.0714 0.080 Uiso 1 d R . .
H19B H -0.0650 0.2152 0.0226 0.080 Uiso 1 d R . .
C20 C -0.0007(11) 0.1633(5) -0.0745(10) 0.142(7) Uani 1 d U . .
H20A H -0.0646 0.1561 -0.1202 0.080 Uiso 1 d R . .
H20B H -0.0274 0.1388 -0.0262 0.080 Uiso 1 d R . .
C21 C 0.0879(9) 0.1335(4) -0.0987(9) 0.115(5) Uani 1 d U . .
H21A H 0.1010 0.1013 -0.0582 0.080 Uiso 1 d R . .
H21B H 0.0593 0.1166 -0.1540 0.080 Uiso 1 d R . .
C22 C 0.2984(8) 0.1269(3) -0.1468(5) 0.048(2) Uani 1 d . . .
H22A H 0.2744 0.0867 -0.1591 0.080 Uiso 1 d R . .
C23 C 0.4282(8) 0.1466(3) -0.1691(5) 0.041(2) Uani 1 d . . .
C24 C 0.5375(8) 0.0457(3) -0.1683(6) 0.069(3) Uani 1 d . . .
H24A H 0.4523 0.0310 -0.1561 0.080 Uiso 1 d R . .
H24B H 0.5682 0.0283 -0.2221 0.080 Uiso 1 d R . .
H24C H 0.5954 0.0357 -0.1202 0.080 Uiso 1 d R . .
C25 C 0.6396(8) 0.1461(3) -0.1952(5) 0.051(2) Uani 1 d . . .
H25A H 0.7267 0.1327 -0.2046 0.080 Uiso 1 d R . .
C26 C 0.5955(8) 0.2024(3) -0.1970(5) 0.049(2) Uani 1 d . . .
H26A H 0.6475 0.2367 -0.2081 0.080 Uiso 1 d R . .
N13 N -0.1212(6) 0.3583(3) 0.1397(5) 0.065(2) Uani 1 d . . .
O1 O -0.0640(8) 0.3198(3) 0.1766(6) 0.126(3) Uani 1 d . . .
O2 O -0.1141(7) 0.4088(3) 0.1610(6) 0.115(3) Uani 1 d . . .
O3 O -0.1942(8) 0.3445(5) 0.0790(6) 0.154(4) Uani 1 d . . .
N14 N 0.2611(7) 0.5165(3) 0.4628(5) 0.066(2) Uani 1 d . . .
O4 O 0.3053(8) 0.4729(3) 0.5008(4) 0.097(3) Uani 1 d . . .
O5 O 0.2654(7) 0.5213(3) 0.3806(4) 0.082(2) Uani 1 d . . .
O6 O 0.2171(8) 0.5562(3) 0.5061(5) 0.126(3) Uani 1 d . . .
N15 N 0.6359(6) 0.1334(3) 0.3651(4) 0.0448(18) Uani 1 d . . .
O7 O 0.6261(6) 0.0790(2) 0.3599(5) 0.083(2) Uani 1 d . . .
O8 O 0.7267(5) 0.1598(3) 0.3326(4) 0.071(2) Uani 1 d . . .
O9 O 0.5473(5) 0.1616(2) 0.4007(4) 0.0583(17) Uani 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N6 Ag1 N1 175.4(2) . . yes
N6 Ag1 Ag2 99.15(15) . . yes
N1 Ag1 Ag2 76.31(16) . . yes
N6 Ag1 Ag3 76.16(16) . 4_566 yes
N1 Ag1 Ag3 105.96(16) . 4_566 yes
Ag2 Ag1 Ag3 114.48(3) . 4_566 yes
N3 Ag2 N9 153.1(2) . . yes
N3 Ag2 N10 125.1(2) . . yes
N9 Ag2 N10 81.5(2) . . yes
N3 Ag2 Ag3 97.41(15) . . yes
N9 Ag2 Ag3 91.83(15) . . yes
N10 Ag2 Ag3 78.17(19) . . yes
N3 Ag2 Ag1 77.54(15) . . yes
N9 Ag2 Ag1 81.81(15) . . yes
N10 Ag2 Ag1 129.18(19) . . yes
Ag3 Ag2 Ag1 149.86(3) . . yes
N11 Ag3 N7 145.9(2) . . yes
N11 Ag3 N4 118.0(2) . 4_565 yes
N7 Ag3 N4 94.7(2) . 4_565 yes
N11 Ag3 Ag2 81.46(15) . . yes
N7 Ag3 Ag2 66.55(14) . . yes
N4 Ag3 Ag2 160.51(14) 4_565 . yes
N11 Ag3 Ag1 90.09(15) . 4_565 yes
N7 Ag3 Ag1 110.86(15) . 4_565 yes
N4 Ag3 Ag1 71.46(14) 4_565 4_565 yes
Ag2 Ag3 Ag1 109.29(3) . 4_565 yes
C4 N1 C1 107.8(6) . . ?
C4 N1 Ag1 125.9(5) . . yes
C1 N1 Ag1 124.6(5) . . yes
C4 N2 C2 107.0(6) . . ?
C4 N2 C3 126.5(6) . . ?
C2 N2 C3 126.6(6) . . ?
C5 N3 C6 114.8(6) . . ?
C5 N3 Ag2 122.7(5) . . yes
C6 N3 Ag2 118.5(4) . . yes
C9 N4 C8 115.0(6) . . ?
C9 N4 Ag3 119.9(5) . 4_566 yes
C8 N4 Ag3 118.5(5) . 4_566 yes
C10 N5 C12 108.4(6) . . ?
C10 N5 C11 127.0(7) . . ?
C12 N5 C11 124.6(6) . . ?
C10 N6 C13 105.2(6) . . ?
C10 N6 Ag1 126.6(5) . . yes
C13 N6 Ag1 125.4(5) . . yes
C17 N7 C14 106.7(6) . . ?
C17 N7 Ag3 130.0(5) . . yes
C14 N7 Ag3 113.1(5) . . yes
C17 N8 C15 107.6(6) . . ?
C17 N8 C16 126.1(6) . . ?
C15 N8 C16 126.3(6) . . ?
C18 N9 C19 117.3(6) . . ?
C18 N9 Ag2 124.2(5) . . yes
C19 N9 Ag2 118.5(4) . . yes
C22 N10 C21 116.4(7) . . ?
C22 N10 Ag2 125.5(6) . . yes
C21 N10 Ag2 114.0(6) . . yes
C23 N11 C26 107.7(6) . . ?
C23 N11 Ag3 130.3(5) . . yes
C26 N11 Ag3 121.8(5) . . yes
C25 N12 C23 109.5(6) . . ?
C25 N12 C24 125.4(7) . . ?
C23 N12 C24 125.0(6) . . ?
C2 C1 N1 109.0(7) . . ?
C1 C2 N2 107.2(6) . . ?
N1 C4 N2 109.1(6) . . ?
N1 C4 C5 128.0(6) . . ?
N2 C4 C5 122.9(7) . . ?
N3 C5 C4 121.9(6) . . ?
C7 C6 N3 116.4(7) . . ?
C6 C7 C8 139.7(11) . . ?
C7 C8 N4 116.2(7) . . ?
N4 C9 C10 122.4(6) . . ?
N6 C10 N5 109.8(6) . . ?
N6 C10 C9 126.3(6) . . ?
N5 C10 C9 123.8(6) . . ?
C13 C12 N5 105.7(7) . . ?
C12 C13 N6 110.9(7) . . ?
C15 C14 N7 109.1(6) . . ?
C14 C15 N8 106.6(7) . . ?
N7 C17 N8 109.9(6) . . ?
N7 C17 C18 126.9(6) . . ?
N8 C17 C18 123.2(7) . . ?
N9 C18 C17 120.0(7) . . ?
C20 C19 N9 111.8(7) . . ?
C21 C20 C19 147.6(11) . . ?
C20 C21 N10 121.2(9) . . ?
N10 C22 C23 123.0(7) . . ?
N11 C23 N12 107.0(7) . . ?
N11 C23 C22 126.4(7) . . ?
N12 C23 C22 126.5(6) . . ?
C26 C25 N12 106.0(7) . . ?
C25 C26 N11 109.7(7) . . ?
O1 N13 O2 123.5(9) . . ?
O1 N13 O3 117.6(9) . . ?
O2 N13 O3 118.9(9) . . ?
O6 N14 O4 119.2(9) . . ?
O6 N14 O5 119.6(8) . . ?
O4 N14 O5 121.1(8) . . ?
O8 N15 O7 121.6(7) . . ?
O8 N15 O9 119.6(6) . . ?
O7 N15 O9 118.7(6) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N6 2.103(5) . yes
Ag1 N1 2.126(6) . yes
Ag1 Ag2 2.9732(10) . yes
Ag1 Ag3 3.0643(10) 4_566 yes
Ag2 N3 2.205(6) . yes
Ag2 N9 2.276(6) . yes
Ag2 N10 2.436(7) . yes
Ag2 Ag3 2.8895(11) . yes
Ag3 N11 2.215(6) . yes
Ag3 N7 2.341(6) . yes
Ag3 N4 2.428(6) 4_565 yes
Ag3 Ag1 3.0643(10) 4_565 yes
N1 C4 1.315(9) . ?
N1 C1 1.375(9) . ?
N2 C4 1.368(8) . ?
N2 C2 1.382(9) . ?
N2 C3 1.473(9) . ?
N3 C5 1.275(8) . ?
N3 C6 1.484(9) . ?
N4 C9 1.275(9) . ?
N4 C8 1.477(9) . ?
N4 Ag3 2.428(6) 4_566 yes
N5 C10 1.355(8) . ?
N5 C12 1.364(9) . ?
N5 C11 1.482(9) . ?
N6 C10 1.346(8) . ?
N6 C13 1.369(9) . ?
N7 C17 1.330(9) . ?
N7 C14 1.371(9) . ?
N8 C17 1.361(8) . ?
N8 C15 1.366(9) . ?
N8 C16 1.471(9) . ?
N9 C18 1.263(9) . ?
N9 C19 1.482(9) . ?
N10 C22 1.229(10) . ?
N10 C21 1.478(10) . ?
N11 C23 1.350(9) . ?
N11 C26 1.355(9) . ?
N12 C25 1.353(9) . ?
N12 C23 1.366(9) . ?
N12 C24 1.502(9) . ?
C1 C2 1.331(10) . ?
C4 C5 1.470(10) . ?
C6 C7 1.359(12) . ?
C7 C8 1.384(13) . ?
C9 C10 1.456(10) . ?
C12 C13 1.352(10) . ?
C14 C15 1.363(10) . ?
C17 C18 1.455(10) . ?
C19 C20 1.428(12) . ?
C20 C21 1.196(13) . ?
C22 C23 1.454(11) . ?
C25 C26 1.353(10) . ?
N13 O1 1.186(9) . ?
N13 O2 1.190(9) . ?
N13 O3 1.217(10) . ?
N14 O6 1.204(9) . ?
N14 O4 1.227(9) . ?
N14 O5 1.246(9) . ?
N15 O8 1.220(7) . ?
N15 O7 1.236(7) . ?
N15 O9 1.244(7) . ?
