#------------------------------------------------------------------------------
#$Date: 2016-03-25 13:13:36 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179832 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/28/7012824.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7012824
loop_
_publ_author_name
'Reger, Daniel L.'
'Gardinier, James R.'
'Semeniuc, Radu F.'
'Smith, Mark D.'
_publ_section_title
;
 Silver complexes of 1,1',3,3'-tetrakis(pyrazol-1-yl)propane: the
 “quadruple pyrazolyl embrace” as a supramolecular
 synthonElectronic supplementary information (ESI) available: two
 possible representations of the coordination sphere about Ag(2a) in
 2·CH3CN. See http://www.rsc.org/suppdata/dt/b3/b301635h/
;
_journal_issue                   9
_journal_name_full               'Dalton Transactions'
_journal_page_first              1712
_journal_paper_doi               10.1039/b301635h
_journal_year                    2003
_chemical_formula_sum            'C32 H32 Ag2 F6 N16 O6 S2'
_chemical_formula_weight         1130.60
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                96.8090(10)
_cell_angle_beta                 111.2290(10)
_cell_angle_gamma                107.9600(10)
_cell_formula_units_Z            2
_cell_length_a                   9.8259(5)
_cell_length_b                   10.4688(5)
_cell_length_c                   12.3726(6)
_cell_measurement_reflns_used    7613
_cell_measurement_temperature    220.0(2)
_cell_measurement_theta_max      26.386
_cell_measurement_theta_min      2.404
_cell_volume                     1089.84(9)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      220.0(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0228
_diffrn_reflns_av_sigmaI/netI    0.0375
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            9992
_diffrn_reflns_theta_full        26.39
_diffrn_reflns_theta_max         26.39
_diffrn_reflns_theta_min         1.83
_diffrn_standards_decay_%        <1
_exptl_absorpt_coefficient_mu    1.082
_exptl_absorpt_correction_T_max  0.7728
_exptl_absorpt_correction_T_min  0.6166
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.723
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             564
_exptl_crystal_size_max          0.36
_exptl_crystal_size_mid          0.32
_exptl_crystal_size_min          0.26
_refine_diff_density_max         0.447
_refine_diff_density_min         -0.419
_refine_diff_density_rms         0.062
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     363
_refine_ls_number_reflns         4444
_refine_ls_number_restraints     7
_refine_ls_restrained_S_all      1.017
_refine_ls_R_factor_all          0.0393
_refine_ls_R_factor_gt           0.0327
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0292P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0683
_refine_ls_wR_factor_ref         0.0696
_reflns_number_gt                3544
_reflns_number_total             4444
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b301635h.txt
_cod_data_source_block           jg123iis
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7012824
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag Ag 0.33379(3) 0.10331(2) 0.46222(2) 0.05739(10) Uani 1 1 d . . .
C1 C 0.6579(3) 0.3378(3) 0.7087(2) 0.0421(6) Uani 1 1 d . . .
H1 H 0.7482 0.4141 0.7751 0.038(6) Uiso 1 1 calc R . .
C2 C 0.6952(3) 0.2063(3) 0.7126(2) 0.0389(6) Uani 1 1 d . . .
H2A H 0.6902 0.1763 0.7836 0.049(7) Uiso 1 1 calc R . .
H2B H 0.6161 0.1315 0.6412 0.041(7) Uiso 1 1 calc R . .
C3 C 0.8591(3) 0.2332(3) 0.7169(2) 0.0392(6) Uani 1 1 d . . .
H3 H 0.9277 0.3290 0.7674 0.027(6) Uiso 1 1 calc R . .
C11 C 0.5045(4) 0.4129(3) 0.8090(3) 0.0547(7) Uani 1 1 d . . .
H11 H 0.5842 0.4964 0.8628 0.067(9) Uiso 1 1 calc R . .
C12 C 0.3533(4) 0.3595(3) 0.7964(3) 0.0608(8) Uani 1 1 d . . .
H12 H 0.3073 0.3978 0.8394 0.074(9) Uiso 1 1 calc R . .
C13 C 0.2818(3) 0.2373(3) 0.7071(3) 0.0538(7) Uani 1 1 d . . .
H13 H 0.1756 0.1777 0.6792 0.054(8) Uiso 1 1 calc R . .
C21 C 0.7194(3) 0.5046(3) 0.5868(3) 0.0596(8) Uani 1 1 d . . .
H21 H 0.7941 0.5830 0.6499 0.058(9) Uiso 1 1 calc R . .
C22 C 0.6691(4) 0.4964(4) 0.4672(4) 0.0698(10) Uani 1 1 d . . .
H22 H 0.7017 0.5669 0.4311 0.073(9) Uiso 1 1 calc R . .
C23 C 0.5604(4) 0.3627(4) 0.4106(3) 0.0631(9) Uani 1 1 d . . .
H23 H 0.5055 0.3275 0.3268 0.069(10) Uiso 1 1 calc R . .
C31 C 0.9522(3) 0.3255(3) 0.5665(3) 0.0500(7) Uani 1 1 d . . .
H31 H 1.0295 0.4124 0.6158 0.045(7) Uiso 1 1 calc R . .
C32 C 0.9110(4) 0.2739(3) 0.4477(3) 0.0619(8) Uani 1 1 d . . .
H32 H 0.9530 0.3179 0.3986 0.048(7) Uiso 1 1 calc R . .
C33 C 0.7958(4) 0.1447(3) 0.4152(3) 0.0602(8) Uani 1 1 d . . .
H33 H 0.7460 0.0846 0.3376 0.071(10) Uiso 1 1 calc R . .
C41 C 1.0538(3) 0.1769(3) 0.8794(2) 0.0550(7) Uani 1 1 d . . .
H41 H 1.1136 0.2671 0.9303 0.052(8) Uiso 1 1 calc R . .
C42 C 1.0786(4) 0.0603(4) 0.8993(3) 0.0680(9) Uani 1 1 d . . .
H42 H 1.1588 0.0531 0.9657 0.079(10) Uiso 1 1 calc R . .
C43 C 0.9622(4) -0.0455(4) 0.8025(3) 0.0676(9) Uani 1 1 d . . .
H43 H 0.9498 -0.1395 0.7927 0.085(11) Uiso 1 1 calc R . .
N11 N 0.3813(2) 0.2138(2) 0.6653(2) 0.0487(5) Uani 1 1 d . . .
N12 N 0.5190(2) 0.3240(2) 0.73026(19) 0.0428(5) Uani 1 1 d . . .
N21 N 0.5419(3) 0.2888(2) 0.4890(2) 0.0504(6) Uani 1 1 d . . .
N22 N 0.6421(2) 0.3792(2) 0.5980(2) 0.0445(5) Uani 1 1 d . . .
N31 N 0.7626(3) 0.1141(2) 0.5060(2) 0.0519(6) Uani 1 1 d . . .
N32 N 0.8608(2) 0.2279(2) 0.59941(18) 0.0411(5) Uani 1 1 d . . .
N41 N 0.8691(3) 0.0017(2) 0.7242(2) 0.0592(6) Uani 1 1 d . . .
N42 N 0.9286(2) 0.1406(2) 0.77367(18) 0.0433(5) Uani 1 1 d . . .
S1A S 0.14182(8) 0.63571(7) 0.91731(6) 0.0496(3) Uani 0.598(3) 1 d PD A 1
O1A O 0.1881(5) 0.5249(5) 0.9476(6) 0.0848(14) Uani 0.598(3) 1 d P A 1
O2A O 0.1261(6) 0.7138(6) 1.0059(5) 0.115(2) Uani 0.598(3) 1 d P A 1
O3A O 0.0276(5) 0.6050(5) 0.8010(4) 0.0924(16) Uani 0.598(3) 1 d P A 1
C51A C 0.3181(11) 0.7545(8) 0.9103(9) 0.072(2) Uani 0.598(3) 1 d PD A 1
F1A F 0.2957(14) 0.8635(10) 0.8778(9) 0.094(3) Uani 0.598(3) 1 d PD A 1
F2A F 0.3593(8) 0.6977(5) 0.8344(6) 0.141(2) Uani 0.598(3) 1 d PD A 1
F3A F 0.4396(11) 0.8040(9) 1.0223(8) 0.102(3) Uani 0.598(3) 1 d P A 1
S1B S 0.14182(8) 0.63571(7) 0.91731(6) 0.0496(3) Uani 0.40 1 d PD A 2
O1B O 0.0108(9) 0.6819(8) 0.8824(8) 0.094(2) Uani 0.402(3) 1 d P A 2
O2B O 0.1224(10) 0.5382(8) 0.8239(10) 0.124(4) Uani 0.402(3) 1 d P A 2
O3B O 0.1703(8) 0.5995(10) 1.0270(7) 0.103(3) Uani 0.402(3) 1 d P A 2
C51B C 0.3224(17) 0.7809(13) 0.9446(15) 0.072(2) Uani 0.40 1 d PD A 2
F1B F 0.296(3) 0.8339(19) 0.8526(14) 0.140(7) Uani 0.402(3) 1 d PD A 2
F2B F 0.3312(12) 0.8844(7) 1.0281(6) 0.162(4) Uani 0.402(3) 1 d PD A 2
F3B F 0.4339(18) 0.7466(19) 0.9637(14) 0.151(7) Uani 0.402(3) 1 d P A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N21 Ag N41 120.27(8) . 2_656 ?
N21 Ag N31 148.32(8) . 2_656 ?
N41 Ag N31 82.57(8) 2_656 2_656 ?
N21 Ag N11 84.91(8) . . ?
N41 Ag N11 139.92(8) 2_656 . ?
N31 Ag N11 90.04(8) 2_656 . ?
N12 C1 N22 110.5(2) . . ?
N12 C1 C2 111.6(2) . . ?
N22 C1 C2 113.2(2) . . ?
C3 C2 C1 110.7(2) . . ?
N32 C3 N42 110.62(19) . . ?
N32 C3 C2 112.67(19) . . ?
N42 C3 C2 112.4(2) . . ?
N12 C11 C12 107.2(3) . . ?
C11 C12 C13 105.2(3) . . ?
N11 C13 C12 111.8(3) . . ?
N22 C21 C22 107.3(3) . . ?
C21 C22 C23 105.2(3) . . ?
N21 C23 C22 112.0(3) . . ?
N32 C31 C32 106.8(3) . . ?
C31 C32 C33 105.5(3) . . ?
N31 C33 C32 112.1(3) . . ?
N42 C41 C42 107.6(3) . . ?
C41 C42 C43 105.6(3) . . ?
N41 C43 C42 111.4(3) . . ?
C13 N11 N12 104.2(2) . . ?
C13 N11 Ag 130.2(2) . . ?
N12 N11 Ag 117.16(15) . . ?
C11 N12 N11 111.5(2) . . ?
C11 N12 C1 127.6(2) . . ?
N11 N12 C1 120.9(2) . . ?
C23 N21 N22 104.1(2) . . ?
C23 N21 Ag 128.2(2) . . ?
N22 N21 Ag 122.97(16) . . ?
C21 N22 N21 111.3(2) . . ?
C21 N22 C1 127.3(3) . . ?
N21 N22 C1 121.3(2) . . ?
C33 N31 N32 104.3(2) . . ?
C33 N31 Ag 128.3(2) . 2_656 ?
N32 N31 Ag 121.20(15) . 2_656 ?
C31 N32 N31 111.3(2) . . ?
C31 N32 C3 128.1(2) . . ?
N31 N32 C3 120.6(2) . . ?
C43 N41 N42 104.5(2) . . ?
C43 N41 Ag 132.5(2) . 2_656 ?
N42 N41 Ag 122.78(16) . 2_656 ?
C41 N42 N41 110.9(2) . . ?
C41 N42 C3 126.5(2) . . ?
N41 N42 C3 122.6(2) . . ?
O2A S1A O3A 116.6(4) . . ?
O2A S1A O1A 115.1(4) . . ?
O3A S1A O1A 114.9(3) . . ?
O2A S1A C51A 103.1(3) . . ?
O3A S1A C51A 102.2(4) . . ?
O1A S1A C51A 101.8(5) . . ?
F2A C51A F1A 106.8(8) . . ?
F2A C51A F3A 110.2(10) . . ?
F1A C51A F3A 106.0(8) . . ?
F2A C51A S1A 113.2(5) . . ?
F1A C51A S1A 111.1(9) . . ?
F3A C51A S1A 109.3(7) . . ?
F3B C51B F1B 110.8(15) . . ?
F3B C51B F2B 119.4(15) . . ?
F1B C51B F2B 100.2(14) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag N21 2.230(2) . ?
Ag N41 2.285(2) 2_656 ?
Ag N31 2.320(2) 2_656 ?
Ag N11 2.449(2) . ?
C1 N12 1.451(3) . ?
C1 N22 1.454(3) . ?
C1 C2 1.531(3) . ?
C2 C3 1.526(3) . ?
C3 N32 1.454(3) . ?
C3 N42 1.457(3) . ?
C11 N12 1.343(3) . ?
C11 C12 1.358(4) . ?
C12 C13 1.379(4) . ?
C13 N11 1.330(3) . ?
C21 N22 1.350(3) . ?
C21 C22 1.362(5) . ?
C22 C23 1.376(5) . ?
C23 N21 1.339(3) . ?
C31 N32 1.347(3) . ?
C31 C32 1.364(4) . ?
C32 C33 1.367(4) . ?
C33 N31 1.326(3) . ?
C41 N42 1.341(3) . ?
C41 C42 1.350(4) . ?
C42 C43 1.372(5) . ?
C43 N41 1.331(4) . ?
N11 N12 1.356(3) . ?
N21 N22 1.358(3) . ?
N31 N32 1.357(3) . ?
N31 Ag 2.320(2) 2_656 ?
N41 N42 1.355(3) . ?
N41 Ag 2.285(2) 2_656 ?
S1A O2A 1.371(4) . ?
S1A O3A 1.390(4) . ?
S1A O1A 1.414(4) . ?
S1A C51A 1.833(6) . ?
C51A F2A 1.300(9) . ?
C51A F1A 1.308(12) . ?
C51A F3A 1.365(14) . ?
C51B F3B 1.21(3) . ?
C51B F1B 1.302(17) . ?
C51B F2B 1.364(12) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N12 C1 C2 C3 -167.7(2) . . . . ?
N22 C1 C2 C3 66.8(3) . . . . ?
C1 C2 C3 N32 -80.3(3) . . . . ?
C1 C2 C3 N42 153.9(2) . . . . ?
N12 C11 C12 C13 -0.3(3) . . . . ?
C11 C12 C13 N11 0.1(3) . . . . ?
N22 C21 C22 C23 0.2(3) . . . . ?
C21 C22 C23 N21 -0.2(3) . . . . ?
N32 C31 C32 C33 -0.7(3) . . . . ?
C31 C32 C33 N31 0.6(4) . . . . ?
N42 C41 C42 C43 -0.8(3) . . . . ?
C41 C42 C43 N41 0.7(4) . . . . ?
C12 C13 N11 N12 0.2(3) . . . . ?
C12 C13 N11 Ag -145.8(2) . . . . ?
N21 Ag N11 C13 131.1(2) . . . . ?
N41 Ag N11 C13 -1.8(3) 2_656 . . . ?
N31 Ag N11 C13 -80.2(2) 2_656 . . . ?
N21 Ag N11 N12 -11.37(17) . . . . ?
N41 Ag N11 N12 -144.23(16) 2_656 . . . ?
N31 Ag N11 N12 137.31(18) 2_656 . . . ?
C12 C11 N12 N11 0.4(3) . . . . ?
C12 C11 N12 C1 178.6(2) . . . . ?
C13 N11 N12 C11 -0.4(3) . . . . ?
Ag N11 N12 C11 150.91(18) . . . . ?
C13 N11 N12 C1 -178.7(2) . . . . ?
Ag N11 N12 C1 -27.4(3) . . . . ?
N22 C1 N12 C11 -103.7(3) . . . . ?
C2 C1 N12 C11 129.5(3) . . . . ?
N22 C1 N12 N11 74.3(3) . . . . ?
C2 C1 N12 N11 -52.6(3) . . . . ?
C22 C23 N21 N22 0.1(3) . . . . ?
C22 C23 N21 Ag 155.8(2) . . . . ?
N41 Ag N21 C23 8.7(3) 2_656 . . . ?
N31 Ag N21 C23 140.1(2) 2_656 . . . ?
N11 Ag N21 C23 -138.2(2) . . . . ?
N41 Ag N21 N22 160.29(17) 2_656 . . . ?
N31 Ag N21 N22 -68.4(2) 2_656 . . . ?
N11 Ag N21 N22 13.41(18) . . . . ?
C22 C21 N22 N21 -0.2(3) . . . . ?
C22 C21 N22 C1 179.5(2) . . . . ?
C23 N21 N22 C21 0.0(3) . . . . ?
Ag N21 N22 C21 -157.25(17) . . . . ?
C23 N21 N22 C1 -179.6(2) . . . . ?
Ag N21 N22 C1 23.1(3) . . . . ?
N12 C1 N22 C21 107.8(3) . . . . ?
C2 C1 N22 C21 -126.2(3) . . . . ?
N12 C1 N22 N21 -72.6(3) . . . . ?
C2 C1 N22 N21 53.4(3) . . . . ?
C32 C33 N31 N32 -0.2(3) . . . . ?
C32 C33 N31 Ag -152.2(2) . . . 2_656 ?
C32 C31 N32 N31 0.6(3) . . . . ?
C32 C31 N32 C3 -179.8(2) . . . . ?
C33 N31 N32 C31 -0.2(3) . . . . ?
Ag N31 N32 C31 154.28(17) 2_656 . . . ?
C33 N31 N32 C3 -179.9(2) . . . . ?
Ag N31 N32 C3 -25.4(3) 2_656 . . . ?
N42 C3 N32 C31 -107.8(3) . . . . ?
C2 C3 N32 C31 125.5(3) . . . . ?
N42 C3 N32 N31 71.7(3) . . . . ?
C2 C3 N32 N31 -55.0(3) . . . . ?
C42 C43 N41 N42 -0.2(4) . . . . ?
C42 C43 N41 Ag 174.2(2) . . . 2_656 ?
C42 C41 N42 N41 0.8(3) . . . . ?
C42 C41 N42 C3 179.5(2) . . . . ?
C43 N41 N42 C41 -0.4(3) . . . . ?
Ag N41 N42 C41 -175.45(18) 2_656 . . . ?
C43 N41 N42 C3 -179.2(2) . . . . ?
Ag N41 N42 C3 5.7(3) 2_656 . . . ?
N32 C3 N42 C41 121.2(3) . . . . ?
C2 C3 N42 C41 -111.9(3) . . . . ?
N32 C3 N42 N41 -60.2(3) . . . . ?
C2 C3 N42 N41 66.7(3) . . . . ?
O2A S1A C51A F2A 176.8(9) . . . . ?
O3A S1A C51A F2A -61.9(10) . . . . ?
O1A S1A C51A F2A 57.2(10) . . . . ?
O2A S1A C51A F1A -63.1(8) . . . . ?
O3A S1A C51A F1A 58.3(7) . . . . ?
O1A S1A C51A F1A 177.3(7) . . . . ?
O2A S1A C51A F3A 53.6(9) . . . . ?
O3A S1A C51A F3A 174.9(8) . . . . ?
O1A S1A C51A F3A -66.1(8) . . . . ?
