#------------------------------------------------------------------------------
#$Date: 2016-03-25 14:36:11 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179903 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/99/7019921.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7019921
loop_
_publ_author_name
'Rankin, Matthew A.'
'Cummins, Christopher C.'
_publ_section_title
;
 Terminal phosphinidene formation via tantalaziridine complexes.
;
_journal_issue                   32
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9615
_journal_page_last               9618
_journal_paper_doi               10.1039/c2dt31082a
_journal_volume                  41
_journal_year                    2012
_chemical_formula_sum            'C78 H124 N6 Ta2'
_chemical_formula_weight         1507.70
_chemical_name_common            (HTa(N(CH2tBu)Ar)3)2
_chemical_name_systematic
;
?
;
_space_group_IT_number           148
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            3
_cell_length_a                   12.9616(9)
_cell_length_b                   12.9616(9)
_cell_length_c                   38.840(3)
_cell_measurement_reflns_used    9689
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      31.30
_cell_measurement_theta_min      2.77
_cell_volume                     5651.0(7)
_computing_cell_refinement       'SAINT 7.46A (Bruker-AXS, 2008)'
_computing_data_collection       'APEX2 3.0 (Bruker-AXS, 2008)'
_computing_data_reduction        'SAINT 7.46A (Bruker-AXS, 2008)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 8.3
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Smart APEX CCD'
_diffrn_measurement_method       'omega and phi scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0375
_diffrn_reflns_av_sigmaI/netI    0.0174
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       54
_diffrn_reflns_limit_l_min       -54
_diffrn_reflns_number            36616
_diffrn_reflns_theta_full        30.03
_diffrn_reflns_theta_max         30.03
_diffrn_reflns_theta_min         1.57
_exptl_absorpt_coefficient_mu    2.946
_exptl_absorpt_correction_T_max  0.7571
_exptl_absorpt_correction_T_min  0.3507
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 2008)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.329
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       hexagonal
_exptl_crystal_F_000             2340
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.277
_refine_diff_density_min         -0.953
_refine_diff_density_rms         0.090
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.105
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     255
_refine_ls_number_reflns         3690
_refine_ls_number_restraints     384
_refine_ls_restrained_S_all      1.073
_refine_ls_R_factor_all          0.0236
_refine_ls_R_factor_gt           0.0215
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0208P)²+24.0347P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0515
_refine_ls_wR_factor_ref         0.0529
_reflns_number_gt                3490
_reflns_number_total             3690
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2dt31082a.txt
_cod_data_source_block           09140hb_e
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      R-3
_cod_database_code               7019921
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ta1 Ta 0.0000 0.0000 0.035987(3) 0.01415(4) Uani 1 3 d SDU . .
N1 N -0.1419(2) 0.0124(2) 0.05154(6) 0.0268(5) Uani 0.812(3) 1 d PDU A 1
C11 C -0.1971(3) -0.0452(3) 0.08350(8) 0.0296(6) Uani 0.812(3) 1 d PDU A 1
C12 C -0.1522(3) 0.0093(3) 0.11476(9) 0.0376(7) Uani 0.812(3) 1 d PDU A 1
H12 H -0.0813 0.0848 0.1155 0.045 Uiso 0.812(3) 1 calc PR A 1
C13 C -0.2105(4) -0.0460(4) 0.14539(10) 0.0544(9) Uani 0.812(3) 1 d PDU A 1
C14 C -0.3155(4) -0.1572(4) 0.14333(11) 0.0596(10) Uani 0.812(3) 1 d PDU A 1
H14 H -0.3561 -0.1953 0.1640 0.072 Uiso 0.812(3) 1 calc PR A 1
C15 C -0.3620(4) -0.2133(3) 0.11192(12) 0.0535(10) Uani 0.812(3) 1 d PDU A 1
C16 C -0.3006(3) -0.1564(3) 0.08238(10) 0.0419(8) Uani 0.812(3) 1 d PDU A 1
H16 H -0.3296 -0.1940 0.0607 0.050 Uiso 0.812(3) 1 calc PR A 1
C131 C -0.1621(7) 0.0193(7) 0.17950(13) 0.093(2) Uani 0.812(3) 1 d PDU A 1
H13A H -0.0915 0.0971 0.1751 0.139 Uiso 0.812(3) 1 calc PR A 1
H13B H -0.1404 -0.0279 0.1944 0.139 Uiso 0.812(3) 1 calc PR A 1
H13C H -0.2233 0.0305 0.1908 0.139 Uiso 0.812(3) 1 calc PR A 1
C151 C -0.4768(6) -0.3300(5) 0.11002(19) 0.090(2) Uani 0.812(3) 1 d PDU A 1
H15A H -0.5198 -0.3323 0.0890 0.136 Uiso 0.812(3) 1 calc PR A 1
H15B H -0.5260 -0.3382 0.1302 0.136 Uiso 0.812(3) 1 calc PR A 1
H15C H -0.4597 -0.3956 0.1097 0.136 Uiso 0.812(3) 1 calc PR A 1
C17 C -0.2217(3) 0.0387(3) 0.02934(8) 0.0338(6) Uani 0.812(3) 1 d PDU A 1
H17A H -0.2956 -0.0376 0.0247 0.041 Uiso 0.812(3) 1 calc PR A 1
H17B H -0.1812 0.0696 0.0070 0.041 Uiso 0.812(3) 1 calc PR A 1
C18 C -0.2571(5) 0.1269(6) 0.04357(12) 0.0334(9) Uani 0.812(3) 1 d PDU A 1
C181 C -0.3495(4) 0.0774(5) 0.07219(11) 0.0561(11) Uani 0.812(3) 1 d PDU A 1
H18A H -0.4195 0.0039 0.0643 0.084 Uiso 0.812(3) 1 calc PR A 1
H18B H -0.3731 0.1361 0.0782 0.084 Uiso 0.812(3) 1 calc PR A 1
H18C H -0.3155 0.0604 0.0925 0.084 Uiso 0.812(3) 1 calc PR A 1
C182 C -0.1479(4) 0.2393(3) 0.05705(10) 0.0486(9) Uani 0.812(3) 1 d PDU A 1
H18D H -0.1719 0.2956 0.0653 0.073 Uiso 0.812(3) 1 calc PR A 1
H18E H -0.0895 0.2761 0.0385 0.073 Uiso 0.812(3) 1 calc PR A 1
H18F H -0.1121 0.2181 0.0760 0.073 Uiso 0.812(3) 1 calc PR A 1
C183 C -0.3089(5) 0.1625(5) 0.01280(15) 0.0516(14) Uani 0.812(3) 1 d PDU A 1
H18G H -0.3722 0.0906 0.0018 0.077 Uiso 0.812(3) 1 calc PR A 1
H18H H -0.2456 0.2079 -0.0040 0.077 Uiso 0.812(3) 1 calc PR A 1
H18I H -0.3417 0.2117 0.0211 0.077 Uiso 0.812(3) 1 calc PR A 1
N2 N -0.0837(9) 0.0868(10) 0.0527(2) 0.0280(18) Uani 0.188(3) 1 d PDU A 2
C21 C -0.0416(9) 0.1527(9) 0.0845(3) 0.0253(18) Uani 0.188(3) 1 d PDU A 2
C22 C 0.0437(9) 0.2725(10) 0.0847(3) 0.032(2) Uani 0.188(3) 1 d PDU A 2
H22 H 0.0754 0.3129 0.0636 0.038 Uiso 0.188(3) 1 calc PR A 2
C23 C 0.0839(10) 0.3349(10) 0.1161(3) 0.036(3) Uani 0.188(3) 1 d PDU A 2
C24 C 0.0350(11) 0.2747(10) 0.1461(3) 0.035(2) Uani 0.188(3) 1 d PDU A 2
H24 H 0.0604 0.3167 0.1673 0.042 Uiso 0.188(3) 1 calc PR A 2
C25 C -0.0508(11) 0.1538(11) 0.1467(3) 0.034(2) Uani 0.188(3) 1 d PDU A 2
C26 C -0.0872(11) 0.0931(11) 0.1155(3) 0.031(2) Uani 0.188(3) 1 d PDU A 2
H26 H -0.1436 0.0103 0.1153 0.037 Uiso 0.188(3) 1 calc PR A 2
C231 C 0.171(2) 0.4684(15) 0.1132(8) 0.090(2) Uani 0.188(3) 1 d PDU A 2
H23A H 0.1870 0.5045 0.1362 0.136 Uiso 0.188(3) 1 calc PR A 2
H23B H 0.1369 0.5051 0.0985 0.136 Uiso 0.188(3) 1 calc PR A 2
H23C H 0.2460 0.4813 0.1030 0.136 Uiso 0.188(3) 1 calc PR A 2
C251 C -0.1085(15) 0.0852(16) 0.1798(3) 0.040(3) Uani 0.188(3) 1 d PDU A 2
H25A H -0.0463 0.0956 0.1961 0.060 Uiso 0.188(3) 1 calc PR A 2
H25B H -0.1591 0.0004 0.1744 0.060 Uiso 0.188(3) 1 calc PR A 2
H25C H -0.1571 0.1157 0.1900 0.060 Uiso 0.188(3) 1 calc PR A 2
C27 C -0.1482(11) 0.1337(11) 0.0313(3) 0.032(2) Uani 0.188(3) 1 d PDU A 2
H27A H -0.1605 0.0982 0.0080 0.038 Uiso 0.188(3) 1 calc PR A 2
H27B H -0.0953 0.2208 0.0287 0.038 Uiso 0.188(3) 1 calc PR A 2
C28 C -0.2685(18) 0.112(2) 0.0445(5) 0.035(3) Uani 0.188(3) 1 d PDU A 2
C281 C -0.2611(14) 0.1940(15) 0.0731(4) 0.048(3) Uani 0.188(3) 1 d PDU A 2
H28A H -0.2148 0.1886 0.0922 0.072 Uiso 0.188(3) 1 calc PR A 2
H28B H -0.3416 0.1707 0.0811 0.072 Uiso 0.188(3) 1 calc PR A 2
H28C H -0.2221 0.2760 0.0645 0.072 Uiso 0.188(3) 1 calc PR A 2
C282 C -0.3498(12) -0.0190(12) 0.0545(4) 0.044(3) Uani 0.188(3) 1 d PDU A 2
H28D H -0.3133 -0.0397 0.0734 0.066 Uiso 0.188(3) 1 calc PR A 2
H28E H -0.3608 -0.0699 0.0346 0.066 Uiso 0.188(3) 1 calc PR A 2
H28F H -0.4272 -0.0309 0.0619 0.066 Uiso 0.188(3) 1 calc PR A 2
C283 C -0.334(3) 0.130(3) 0.0138(6) 0.0516(14) Uani 0.188(3) 1 d PDU A 2
H28G H -0.3998 0.1387 0.0223 0.077 Uiso 0.188(3) 1 calc PR A 2
H28H H -0.3644 0.0604 -0.0015 0.077 Uiso 0.188(3) 1 calc PR A 2
H28I H -0.2777 0.2015 0.0011 0.077 Uiso 0.188(3) 1 calc PR A 2
H1 H 0.0815 0.0955 0.0029 0.062 Uiso 0.33 1 d PRD A -1
H1A H -0.0696 -0.0748 0.0013 0.062 Uiso 0.33 1 d PRD A -1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ta Ta -0.7052 6.5227 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ta1 N1 111.43(7) . 3
N1 Ta1 N1 111.43(7) . 2
N1 Ta1 N1 111.43(7) 3 2
N1 Ta1 N2 131.1(3) . 3
N1 Ta1 N2 25.2(3) 3 3
N1 Ta1 N2 87.7(3) 2 3
N1 Ta1 N2 87.7(3) . 2
N1 Ta1 N2 131.1(3) 3 2
N1 Ta1 N2 25.2(3) 2 2
N2 Ta1 N2 110.2(3) 3 2
N1 Ta1 N2 25.2(3) . .
N1 Ta1 N2 87.7(3) 3 .
N1 Ta1 N2 131.1(3) 2 .
N2 Ta1 N2 110.2(3) 3 .
N2 Ta1 N2 110.2(3) 2 .
N1 Ta1 Ta1 107.43(7) . 10
N1 Ta1 Ta1 107.43(7) 3 10
N1 Ta1 Ta1 107.43(7) 2 10
N2 Ta1 Ta1 108.7(3) 3 10
N2 Ta1 Ta1 108.7(3) 2 10
N2 Ta1 Ta1 108.7(3) . 10
N2 Ta1 H1 75.0 3 .
N2 Ta1 H1 145.9 2 .
N2 Ta1 H1 98.4 . .
Ta1 Ta1 H1 42.0 10 .
N2 Ta1 H1A 135.4 3 .
N2 Ta1 H1A 77.1 2 .
N2 Ta1 H1A 107.6 . .
Ta1 Ta1 H1A 34.8 10 .
C11 N1 C17 113.0(2) . .
C11 N1 Ta1 116.94(18) . .
C17 N1 Ta1 126.96(19) . .
C12 C11 C16 119.9(3) . .
C12 C11 N1 121.3(3) . .
C16 C11 N1 118.7(3) . .
C11 C12 C13 120.3(4) . .
C11 C12 H12 119.9 . .
C13 C12 H12 119.9 . .
C12 C13 C14 118.3(4) . .
C12 C13 C131 119.1(5) . .
C14 C13 C131 122.4(4) . .
C15 C14 C13 122.0(3) . .
C15 C14 H14 119.0 . .
C13 C14 H14 119.0 . .
C16 C15 C14 117.7(4) . .
C16 C15 C151 120.9(5) . .
C14 C15 C151 121.4(4) . .
C15 C16 C11 121.7(4) . .
C15 C16 H16 119.1 . .
C11 C16 H16 119.1 . .
N1 C17 C18 117.2(3) . .
N1 C17 H17A 108.0 . .
C18 C17 H17A 108.0 . .
N1 C17 H17B 108.0 . .
C18 C17 H17B 108.0 . .
H17A C17 H17B 107.2 . .
C181 C18 C182 108.1(4) . .
C181 C18 C17 114.5(4) . .
C182 C18 C17 110.7(3) . .
C181 C18 C183 108.8(4) . .
C182 C18 C183 108.3(4) . .
C17 C18 C183 106.3(4) . .
C21 N2 C27 110.7(9) . .
C21 N2 Ta1 117.1(6) . .
C27 N2 Ta1 127.5(7) . .
C22 C21 C26 119.8(10) . .
C22 C21 N2 121.5(10) . .
C26 C21 N2 118.7(10) . .
C21 C22 C23 120.5(10) . .
C21 C22 H22 119.8 . .
C23 C22 H22 119.8 . .
C24 C23 C22 118.4(10) . .
C24 C23 C231 125.3(14) . .
C22 C23 C231 116.0(14) . .
C23 C24 C25 122.4(11) . .
C23 C24 H24 118.8 . .
C25 C24 H24 118.8 . .
C26 C25 C24 118.3(10) . .
C26 C25 C251 118.3(11) . .
C24 C25 C251 123.4(11) . .
C21 C26 C25 120.6(11) . .
C21 C26 H26 119.7 . .
C25 C26 H26 119.7 . .
C23 C231 H23A 109.5 . .
C23 C231 H23B 109.5 . .
H23A C231 H23B 109.5 . .
C23 C231 H23C 109.5 . .
H23A C231 H23C 109.5 . .
H23B C231 H23C 109.5 . .
C25 C251 H25A 109.5 . .
C25 C251 H25B 109.5 . .
H25A C251 H25B 109.5 . .
C25 C251 H25C 109.5 . .
H25A C251 H25C 109.5 . .
H25B C251 H25C 109.5 . .
N2 C27 C28 117.4(12) . .
N2 C27 H27A 108.0 . .
C28 C27 H27A 108.0 . .
N2 C27 H27B 108.0 . .
C28 C27 H27B 108.0 . .
H27A C27 H27B 107.2 . .
C281 C28 C27 114.7(16) . .
C281 C28 C282 111.2(15) . .
C27 C28 C282 111.5(13) . .
C281 C28 C283 107.9(17) . .
C27 C28 C283 107.2(17) . .
C282 C28 C283 103.7(17) . .
C28 C281 H28A 109.5 . .
C28 C281 H28B 109.5 . .
H28A C281 H28B 109.5 . .
C28 C281 H28C 109.5 . .
H28A C281 H28C 109.5 . .
H28B C281 H28C 109.5 . .
C28 C282 H28D 109.5 . .
C28 C282 H28E 109.5 . .
H28D C282 H28E 109.5 . .
C28 C282 H28F 109.5 . .
H28D C282 H28F 109.5 . .
H28E C282 H28F 109.5 . .
C28 C283 H28G 109.5 . .
C28 C283 H28H 109.5 . .
H28G C283 H28H 109.5 . .
C28 C283 H28I 109.5 . .
H28G C283 H28I 109.5 . .
H28H C283 H28I 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ta1 N1 2.017(2) .
Ta1 N1 2.017(2) 3
Ta1 N1 2.017(2) 2
Ta1 N2 2.020(9) 3
Ta1 N2 2.020(9) 2
Ta1 N2 2.020(9) .
Ta1 Ta1 2.7954(3) 10
Ta1 H1 1.7290 .
Ta1 H1A 1.6417 .
N1 C11 1.441(4) .
N1 C17 1.510(4) .
C11 C12 1.379(5) .
C11 C16 1.394(4) .
C12 C13 1.399(5) .
C12 H12 0.9500 .
C13 C14 1.406(7) .
C13 C131 1.527(7) .
C14 C15 1.393(7) .
C14 H14 0.9500 .
C15 C16 1.381(5) .
C15 C151 1.503(6) .
C16 H16 0.9500 .
C131 H13A 0.9800 .
C131 H13B 0.9800 .
C131 H13C 0.9800 .
C151 H15A 0.9800 .
C151 H15B 0.9800 .
C151 H15C 0.9800 .
C17 C18 1.533(5) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 C181 1.521(6) .
C18 C182 1.529(8) .
C18 C183 1.550(5) .
C181 H18A 0.9800 .
C181 H18B 0.9800 .
C181 H18C 0.9800 .
C182 H18D 0.9800 .
C182 H18E 0.9800 .
C182 H18F 0.9800 .
C183 H18G 0.9800 .
C183 H18H 0.9800 .
C183 H18I 0.9800 .
N2 C21 1.446(12) .
N2 C27 1.507(12) .
C21 C22 1.384(13) .
C21 C26 1.390(13) .
C22 C23 1.410(13) .
C22 H22 0.9500 .
C23 C24 1.370(14) .
C23 C231 1.526(16) .
C24 C25 1.396(14) .
C24 H24 0.9500 .
C25 C26 1.395(13) .
C25 C251 1.527(14) .
C26 H26 0.9500 .
C231 H23A 0.9800 .
C231 H23B 0.9800 .
C231 H23C 0.9800 .
C251 H25A 0.9800 .
C251 H25B 0.9800 .
C251 H25C 0.9800 .
C27 C28 1.527(16) .
C27 H27A 0.9900 .
C27 H27B 0.9900 .
C28 C281 1.509(17) .
C28 C282 1.53(2) .
C28 C283 1.545(16) .
C281 H28A 0.9800 .
C281 H28B 0.9800 .
C281 H28C 0.9800 .
C282 H28D 0.9800 .
C282 H28E 0.9800 .
C282 H28F 0.9800 .
C283 H28G 0.9800 .
C283 H28H 0.9800 .
C283 H28I 0.9800 .
