#------------------------------------------------------------------------------
#$Date: 2016-03-25 14:36:11 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179903 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/99/7019996.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7019996
loop_
_publ_author_name
'Tan, Bin'
'Xie, Zai-Lai'
'Feng, Mei-Ling'
'Hu, Bing'
'Wu, Zhao-Feng'
'Huang, Xiao-Ying'
_publ_section_title
;
 Ionothermal syntheses, crystal structures and properties of
 three-dimensional rare earth metal-organic frameworks with
 1,4-naphthalenedicarboxylic acid.
;
_journal_issue                   35
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              10576
_journal_page_last               10584
_journal_paper_doi               10.1039/c2dt30944k
_journal_volume                  41
_journal_year                    2012
_chemical_formula_moiety         'C36 H18 Cl O12 Dy2, C10 H19 N2'
_chemical_formula_sum            'C46 H37 Cl Dy2 N2 O12'
_chemical_formula_weight         1170.23
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 94.3097(9)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.66597(18)
_cell_length_b                   14.78124(14)
_cell_length_c                   15.84149(16)
_cell_measurement_reflns_used    10636
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      28.9062
_cell_measurement_theta_min      2.2585
_cell_volume                     4124.91(7)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.66
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.66
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.66
;
_computing_molecular_graphics    'DIAMOND. Version 3.0. Crystal Impact'
_computing_publication_material  'Windows Word 2003'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 16.2083
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Xcalibur, Eos'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0179
_diffrn_reflns_av_sigmaI/netI    0.0306
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            17185
_diffrn_reflns_theta_full        26.55
_diffrn_reflns_theta_max         26.55
_diffrn_reflns_theta_min         2.69
_exptl_absorpt_coefficient_mu    3.729
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.80934
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.66 (release 28-04-2010 CrysAlis171 .NET)
(compiled Apr 28 2010,14:27:37)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.884
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2288
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.16
_refine_diff_density_max         1.273
_refine_diff_density_min         -0.904
_refine_diff_density_rms         0.103
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.018
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         8551
_refine_ls_number_restraints     943
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.0354
_refine_ls_R_factor_gt           0.0245
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0350P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0617
_refine_ls_wR_factor_ref         0.0638
_reflns_number_gt                6748
_reflns_number_total             8551
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2dt30944k.txt
_cod_data_source_block           compound-9
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7019996
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.378438(9) 0.024605(10) -0.004156(9) 0.01254(5) Uani 1 1 d . . .
Dy2 Dy 0.117500(9) 0.011639(11) -0.001260(9) 0.01324(5) Uani 1 1 d . . .
Cl1 Cl 0.25226(5) -0.08217(6) 0.02562(6) 0.0283(2) Uani 1 1 d . . .
O1 O 0.45051(16) 0.12171(18) -0.07760(18) 0.0344(7) Uani 1 1 d . . .
O2 O 0.57552(15) 0.10445(18) -0.06563(17) 0.0346(7) Uani 1 1 d . . .
O3 O 0.31561(16) 0.12857(19) 0.07354(18) 0.0371(7) Uani 1 1 d . . .
O5 O 0.46946(16) 0.4280(2) -0.40278(18) 0.0398(8) Uani 1 1 d . . .
O4 O 0.19261(15) 0.13352(17) 0.03156(16) 0.0281(6) Uani 1 1 d . . .
O6 O 0.59467(16) 0.43058(19) -0.38618(17) 0.0364(7) Uani 1 1 d . . .
O7 O 0.29141(15) 0.42965(19) 0.39060(16) 0.0299(7) Uani 1 1 d . . .
O8 O 0.16738(14) 0.45585(17) 0.37016(14) 0.0239(6) Uani 1 1 d . . .
O9 O 0.06125(15) 0.08535(18) 0.11076(16) 0.0281(6) Uani 1 1 d . . .
O10 O -0.06410(15) 0.09984(18) 0.08676(16) 0.0294(7) Uani 1 1 d . . .
O11 O 0.02046(16) 0.40846(18) 0.43551(16) 0.0313(7) Uani 1 1 d . . .
O12 O -0.10127(16) 0.40216(18) 0.39529(17) 0.0329(7) Uani 1 1 d . . .
C1 C 0.5157(2) 0.1416(2) -0.0949(2) 0.0241(9) Uani 1 1 d . . .
C2 C 0.5225(2) 0.2155(2) -0.1598(2) 0.0215(8) Uani 1 1 d . . .
C3 C 0.4715(2) 0.2133(3) -0.2299(3) 0.0296(10) Uani 1 1 d . . .
H3A H 0.4343 0.1687 -0.2347 0.036 Uiso 1 1 calc R . .
C4 C 0.4754(2) 0.2780(3) -0.2942(2) 0.0285(10) Uani 1 1 d . . .
H4A H 0.4409 0.2750 -0.3415 0.034 Uiso 1 1 calc R . .
C5 C 0.5284(2) 0.3451(3) -0.2892(2) 0.0222(8) Uani 1 1 d . . .
C6 C 0.5804(2) 0.3526(2) -0.2160(2) 0.0205(8) Uani 1 1 d . . .
C7 C 0.5777(2) 0.2857(2) -0.1509(2) 0.0214(8) Uani 1 1 d . . .
C8 C 0.6293(2) 0.2936(3) -0.0786(2) 0.0305(10) Uani 1 1 d . . .
H8A H 0.6298 0.2494 -0.0368 0.037 Uiso 1 1 calc R . .
C9 C 0.6784(2) 0.3649(3) -0.0690(3) 0.0366(11) Uani 1 1 d . . .
H9A H 0.7114 0.3690 -0.0206 0.044 Uiso 1 1 calc R . .
C10 C 0.6793(2) 0.4311(3) -0.1310(3) 0.0346(10) Uani 1 1 d . . .
H10A H 0.7125 0.4798 -0.1233 0.041 Uiso 1 1 calc R . .
C11 C 0.6320(2) 0.4258(3) -0.2037(2) 0.0293(9) Uani 1 1 d . . .
H11A H 0.6338 0.4703 -0.2450 0.035 Uiso 1 1 calc R . .
C12 C 0.5311(2) 0.4065(3) -0.3644(2) 0.0254(9) Uani 1 1 d . . .
C13 C 0.2496(2) 0.1605(2) 0.0768(2) 0.0246(9) Uani 1 1 d . . .
C14 C 0.2398(2) 0.2324(2) 0.1418(2) 0.0220(8) Uani 1 1 d . . .
C15 C 0.2832(2) 0.2251(3) 0.2165(3) 0.0339(10) Uani 1 1 d . . .
H15A H 0.3173 0.1773 0.2237 0.041 Uiso 1 1 calc R . .
C16 C 0.2781(2) 0.2863(3) 0.2821(2) 0.0327(10) Uani 1 1 d . . .
H16A H 0.3095 0.2795 0.3315 0.039 Uiso 1 1 calc R . .
C17 C 0.2270(2) 0.3573(2) 0.2751(2) 0.0197(8) Uani 1 1 d . . .
C18 C 0.1799(2) 0.3677(2) 0.1984(2) 0.0171(8) Uani 1 1 d . . .
C19 C 0.1878(2) 0.3061(2) 0.1306(2) 0.0206(8) Uani 1 1 d . . .
C20 C 0.1441(2) 0.3219(3) 0.0529(2) 0.0305(10) Uani 1 1 d . . .
H20A H 0.1490 0.2829 0.0076 0.037 Uiso 1 1 calc R . .
C21 C 0.0954(2) 0.3930(3) 0.0437(2) 0.0342(10) Uani 1 1 d . . .
H21A H 0.0676 0.4023 -0.0078 0.041 Uiso 1 1 calc R . .
C22 C 0.0869(2) 0.4520(3) 0.1108(2) 0.0319(10) Uani 1 1 d . . .
H22A H 0.0530 0.5001 0.1040 0.038 Uiso 1 1 calc R . .
C23 C 0.1271(2) 0.4400(2) 0.1857(2) 0.0251(9) Uani 1 1 d . . .
H23A H 0.1203 0.4798 0.2299 0.030 Uiso 1 1 calc R . .
C24 C 0.2281(2) 0.4199(2) 0.3514(2) 0.0198(8) Uani 1 1 d . . .
C25 C 0.0002(2) 0.1230(2) 0.1204(2) 0.0225(8) Uani 1 1 d . . .
C26 C -0.0003(2) 0.2014(3) 0.1812(2) 0.0223(9) Uani 1 1 d . . .
C27 C 0.0403(2) 0.1931(3) 0.2576(2) 0.0311(10) Uani 1 1 d . . .
H27A H 0.0735 0.1447 0.2670 0.037 Uiso 1 1 calc R . .
C28 C 0.0327(2) 0.2567(3) 0.3223(2) 0.0306(10) Uani 1 1 d . . .
H28A H 0.0611 0.2504 0.3737 0.037 Uiso 1 1 calc R . .
C29 C -0.0166(2) 0.3283(3) 0.3100(2) 0.0232(9) Uani 1 1 d . . .
C30 C -0.0538(2) 0.3447(3) 0.2283(2) 0.0238(9) Uani 1 1 d . . .
C31 C -0.0456(2) 0.2799(2) 0.1637(2) 0.0215(8) Uani 1 1 d . . .
C32 C -0.0807(2) 0.2977(3) 0.0813(3) 0.0338(10) Uani 1 1 d . . .
H32A H -0.0768 0.2559 0.0380 0.041 Uiso 1 1 calc R . .
C33 C -0.1200(3) 0.3764(3) 0.0662(3) 0.0466(13) Uani 1 1 d . . .
H33A H -0.1422 0.3878 0.0121 0.056 Uiso 1 1 calc R . .
C34 C -0.1277(3) 0.4400(3) 0.1300(3) 0.0440(12) Uani 1 1 d . . .
H34A H -0.1541 0.4934 0.1179 0.053 Uiso 1 1 calc R . .
C35 C -0.0969(2) 0.4245(3) 0.2097(3) 0.0347(10) Uani 1 1 d . . .
H35A H -0.1040 0.4661 0.2524 0.042 Uiso 1 1 calc R . .
C36 C -0.0329(2) 0.3843(2) 0.3852(2) 0.0238(9) Uani 1 1 d . . .
N1A N 0.2330(5) -0.2682(5) 0.2703(5) 0.0603(12) Uani 0.592(3) 1 d PDU A 1
N2A N 0.3025(5) -0.1493(5) 0.2706(5) 0.0662(12) Uani 0.592(3) 1 d PDU A 1
C37A C 0.2817(8) -0.2690(12) 0.3411(8) 0.0649(13) Uani 0.592(3) 1 d PDU A 1
H37A H 0.2843 -0.3136 0.3826 0.078 Uiso 0.592(3) 1 calc PR A 1
C38A C 0.3228(6) -0.1991(7) 0.3410(6) 0.0687(12) Uani 0.592(3) 1 d PDU A 1
H38A H 0.3609 -0.1841 0.3823 0.082 Uiso 0.592(3) 1 calc PR A 1
C39A C 0.2498(15) -0.1955(13) 0.2266(11) 0.0647(12) Uani 0.592(3) 1 d PDU A 1
H39A H 0.2280 -0.1797 0.1734 0.078 Uiso 0.592(3) 1 calc PR A 1
C40A C 0.1791(6) -0.3380(6) 0.2470(7) 0.0727(19) Uani 0.592(3) 1 d PDU A 1
H40A H 0.1517 -0.3224 0.1944 0.109 Uiso 0.592(3) 1 calc PR A 1
H40B H 0.1442 -0.3442 0.2902 0.109 Uiso 0.592(3) 1 calc PR A 1
H40C H 0.2054 -0.3942 0.2406 0.109 Uiso 0.592(3) 1 calc PR A 1
C41A C 0.3233(6) -0.0537(6) 0.2472(7) 0.0779(12) Uani 0.592(3) 1 d PDU A 1
H41A H 0.2785 -0.0165 0.2509 0.094 Uiso 0.592(3) 1 calc PR A 1
H41B H 0.3346 -0.0543 0.1882 0.094 Uiso 0.592(3) 1 calc PR A 1
C43A C 0.3474(6) 0.0413(8) 0.3743(7) 0.0924(14) Uani 0.592(3) 1 d PDU A 1
H43A H 0.3100 0.0860 0.3544 0.111 Uiso 0.592(3) 1 calc PR A 1
H43B H 0.3249 -0.0026 0.4104 0.111 Uiso 0.592(3) 1 calc PR A 1
C42A C 0.3903(6) -0.0051(7) 0.2979(6) 0.0802(13) Uani 0.592(3) 1 d PDU A 1
H42A H 0.4135 0.0400 0.2637 0.096 Uiso 0.592(3) 1 calc PR A 1
H42B H 0.4287 -0.0479 0.3195 0.096 Uiso 0.592(3) 1 calc PR A 1
C44A C 0.4240(6) 0.0860(8) 0.4179(6) 0.1001(15) Uani 0.592(3) 1 d PDU A 1
H44A H 0.4657 0.0463 0.4064 0.120 Uiso 0.592(3) 1 calc PR A 1
H44B H 0.4321 0.1424 0.3886 0.120 Uiso 0.592(3) 1 calc PR A 1
C45A C 0.4316(6) 0.1070(9) 0.5150(6) 0.1060(19) Uani 0.592(3) 1 d PDU A 1
H45A H 0.4392 0.0519 0.5478 0.127 Uiso 0.592(3) 1 calc PR A 1
H45B H 0.4736 0.1478 0.5291 0.127 Uiso 0.592(3) 1 calc PR A 1
C46A C 0.3554(7) 0.1518(9) 0.5315(8) 0.134(3) Uani 0.592(3) 1 d PDU A 1
H46A H 0.3565 0.1707 0.5896 0.201 Uiso 0.592(3) 1 calc PR A 1
H46B H 0.3149 0.1092 0.5200 0.201 Uiso 0.592(3) 1 calc PR A 1
H46C H 0.3473 0.2035 0.4953 0.201 Uiso 0.592(3) 1 calc PR A 1
N1B N 0.2071(7) -0.2817(7) 0.2278(7) 0.0603(12) Uani 0.408(3) 1 d PDU A 2
N2B N 0.2901(7) -0.2066(8) 0.2962(7) 0.0662(12) Uani 0.408(3) 1 d PDU A 2
C37B C 0.2183(8) -0.3210(9) 0.3056(7) 0.0649(13) Uani 0.408(3) 1 d PDU A 2
H37B H 0.1934 -0.3714 0.3253 0.078 Uiso 0.408(3) 1 calc PR A 2
C38B C 0.2693(13) -0.2752(15) 0.3454(12) 0.0687(12) Uani 0.408(3) 1 d PDU A 2
H38B H 0.2895 -0.2868 0.4003 0.082 Uiso 0.408(3) 1 calc PR A 2
C39B C 0.248(2) -0.2058(19) 0.2266(16) 0.0647(12) Uani 0.408(3) 1 d PDU A 2
H39B H 0.2468 -0.1620 0.1843 0.078 Uiso 0.408(3) 1 calc PR A 2
C40B C 0.1552(8) -0.3174(9) 0.1611(8) 0.0727(19) Uani 0.408(3) 1 d PDU A 2
H40D H 0.1566 -0.2802 0.1116 0.109 Uiso 0.408(3) 1 calc PR A 2
H40E H 0.1047 -0.3178 0.1795 0.109 Uiso 0.408(3) 1 calc PR A 2
H40F H 0.1699 -0.3780 0.1479 0.109 Uiso 0.408(3) 1 calc PR A 2
C41B C 0.3518(8) -0.1450(9) 0.3256(8) 0.0779(12) Uani 0.408(3) 1 d PDU A 2
H41C H 0.3989 -0.1780 0.3376 0.094 Uiso 0.408(3) 1 calc PR A 2
H41D H 0.3395 -0.1131 0.3763 0.094 Uiso 0.408(3) 1 calc PR A 2
C42B C 0.3583(10) -0.0794(9) 0.2521(8) 0.0802(13) Uani 0.408(3) 1 d PDU A 2
H42C H 0.4093 -0.0735 0.2340 0.096 Uiso 0.408(3) 1 calc PR A 2
H42D H 0.3219 -0.0903 0.2042 0.096 Uiso 0.408(3) 1 calc PR A 2
C43B C 0.3356(9) -0.0043(10) 0.3105(9) 0.0924(14) Uani 0.408(3) 1 d PDU A 2
H43C H 0.2892 -0.0233 0.3345 0.111 Uiso 0.408(3) 1 calc PR A 2
H43D H 0.3229 0.0482 0.2756 0.111 Uiso 0.408(3) 1 calc PR A 2
C44B C 0.3924(9) 0.0279(11) 0.3861(10) 0.1001(15) Uani 0.408(3) 1 d PDU A 2
H44C H 0.4043 -0.0222 0.4244 0.120 Uiso 0.408(3) 1 calc PR A 2
H44D H 0.4393 0.0488 0.3645 0.120 Uiso 0.408(3) 1 calc PR A 2
C45B C 0.3554(9) 0.1061(11) 0.4343(10) 0.1060(19) Uani 0.408(3) 1 d PDU A 2
H45C H 0.3339 0.1500 0.3937 0.127 Uiso 0.408(3) 1 calc PR A 2
H45D H 0.3143 0.0819 0.4649 0.127 Uiso 0.408(3) 1 calc PR A 2
C46B C 0.4120(12) 0.1524(12) 0.4955(12) 0.134(3) Uani 0.408(3) 1 d PDU A 2
H46D H 0.4518 0.1781 0.4651 0.201 Uiso 0.408(3) 1 calc PR A 2
H46E H 0.4333 0.1091 0.5358 0.201 Uiso 0.408(3) 1 calc PR A 2
H46F H 0.3871 0.1995 0.5247 0.201 Uiso 0.408(3) 1 calc PR A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O7 Dy1 O1 79.24(9) 4_565 .
O7 Dy1 O5 144.91(11) 4_565 4_566
O1 Dy1 O5 77.14(11) . 4_566
O7 Dy1 O6 78.09(10) 4_565 2_644
O1 Dy1 O6 80.85(11) . 2_644
O5 Dy1 O6 122.61(10) 4_566 2_644
O7 Dy1 O3 82.40(10) 4_565 .
O1 Dy1 O3 99.30(11) . .
O5 Dy1 O3 76.29(10) 4_566 .
O6 Dy1 O3 160.12(10) 2_644 .
O7 Dy1 O2 141.60(10) 4_565 3_655
O1 Dy1 O2 124.61(10) . 3_655
O5 Dy1 O2 73.48(10) 4_566 3_655
O6 Dy1 O2 77.20(10) 2_644 3_655
O3 Dy1 O2 117.33(11) . 3_655
O7 Dy1 Cl1 77.83(7) 4_565 .
O1 Dy1 Cl1 156.60(7) . .
O5 Dy1 Cl1 125.37(8) 4_566 .
O6 Dy1 Cl1 89.94(8) 2_644 .
O3 Dy1 Cl1 82.21(8) . .
O2 Dy1 Cl1 73.23(7) 3_655 .
O11 Dy2 O4 95.61(10) 4_565 .
O11 Dy2 O10 81.28(10) 4_565 3
O4 Dy2 O10 155.81(10) . 3
O11 Dy2 O8 80.12(9) 4_565 4_565
O4 Dy2 O8 77.52(9) . 4_565
O10 Dy2 O8 78.31(9) 3 4_565
O11 Dy2 O9 75.14(9) 4_565 .
O4 Dy2 O9 74.59(9) . .
O10 Dy2 O9 126.71(9) 3 .
O8 Dy2 O9 140.29(9) 4_565 .
O11 Dy2 O12 123.05(10) 4_565 2_545
O4 Dy2 O12 118.66(10) . 2_545
O10 Dy2 O12 82.01(10) 3 2_545
O8 Dy2 O12 146.72(10) 4_565 2_545
O9 Dy2 O12 72.68(9) . 2_545
O11 Dy2 Cl1 161.85(7) 4_565 .
O4 Dy2 Cl1 83.17(7) . .
O10 Dy2 Cl1 92.41(7) 3 .
O8 Dy2 Cl1 81.95(7) 4_565 .
O9 Dy2 Cl1 121.47(7) . .
O12 Dy2 Cl1 72.30(7) 2_545 .
Dy2 Cl1 Dy1 112.28(3) . .
C1 O1 Dy1 145.2(2) . .
C1 O2 Dy1 142.6(3) . 3_655
C13 O3 Dy1 139.0(2) . .
C12 O5 Dy1 163.4(3) . 4_565
C13 O4 Dy2 144.2(3) . .
C12 O6 Dy1 128.3(2) . 2_654
C24 O7 Dy1 158.1(3) . 4_566
C24 O8 Dy2 133.0(2) . 4_566
C25 O9 Dy2 136.2(2) . .
C25 O10 Dy2 139.5(3) . 3
C36 O11 Dy2 162.2(3) . 4_566
C36 O12 Dy2 113.7(2) . 2
O1 C1 O2 126.1(3) . .
O1 C1 C2 116.4(3) . .
O2 C1 C2 117.4(3) . .
C3 C2 C7 119.9(3) . .
C3 C2 C1 116.8(3) . .
C7 C2 C1 123.3(3) . .
C2 C3 C4 120.4(4) . .
C2 C3 H3A 119.8 . .
C4 C3 H3A 119.8 . .
C5 C4 C3 121.7(3) . .
C5 C4 H4A 119.2 . .
C3 C4 H4A 119.2 . .
C4 C5 C6 120.0(3) . .
C4 C5 C12 117.2(3) . .
C6 C5 C12 122.8(3) . .
C11 C6 C5 122.5(3) . .
C11 C6 C7 118.9(3) . .
C5 C6 C7 118.5(3) . .
C8 C7 C2 122.4(3) . .
C8 C7 C6 118.1(3) . .
C2 C7 C6 119.4(3) . .
C9 C8 C7 121.4(4) . .
C9 C8 H8A 119.3 . .
C7 C8 H8A 119.3 . .
C8 C9 C10 120.4(4) . .
C8 C9 H9A 119.8 . .
C10 C9 H9A 119.8 . .
C11 C10 C9 120.9(4) . .
C11 C10 H10A 119.5 . .
C9 C10 H10A 119.5 . .
C10 C11 C6 120.2(4) . .
C10 C11 H11A 119.9 . .
C6 C11 H11A 119.9 . .
O5 C12 O6 124.2(4) . .
O5 C12 C5 117.5(4) . .
O6 C12 C5 118.2(3) . .
O4 C13 O3 124.1(3) . .
O4 C13 C14 119.2(3) . .
O3 C13 C14 116.6(3) . .
C15 C14 C19 118.9(3) . .
C15 C14 C13 116.9(3) . .
C19 C14 C13 124.2(3) . .
C14 C15 C16 122.3(4) . .
C14 C15 H15A 118.9 . .
C16 C15 H15A 118.9 . .
C17 C16 C15 121.0(4) . .
C17 C16 H16A 119.5 . .
C15 C16 H16A 119.5 . .
C16 C17 C18 119.0(3) . .
C16 C17 C24 115.4(3) . .
C18 C17 C24 125.6(3) . .
C23 C18 C19 118.2(3) . .
C23 C18 C17 122.4(3) . .
C19 C18 C17 119.3(3) . .
C20 C19 C18 118.1(3) . .
C20 C19 C14 122.4(3) . .
C18 C19 C14 119.5(3) . .
C21 C20 C19 121.3(4) . .
C21 C20 H20A 119.4 . .
C19 C20 H20A 119.4 . .
C20 C21 C22 120.4(4) . .
C20 C21 H21A 119.8 . .
C22 C21 H21A 119.8 . .
C23 C22 C21 120.6(4) . .
C23 C22 H22A 119.7 . .
C21 C22 H22A 119.7 . .
C22 C23 C18 121.4(4) . .
C22 C23 H23A 119.3 . .
C18 C23 H23A 119.3 . .
O7 C24 O8 125.8(3) . .
O7 C24 C17 115.1(3) . .
O8 C24 C17 119.1(3) . .
O9 C25 O10 126.2(3) . .
O9 C25 C26 118.3(3) . .
O10 C25 C26 115.4(3) . .
C27 C26 C31 119.7(3) . .
C27 C26 C25 118.0(4) . .
C31 C26 C25 122.1(3) . .
C26 C27 C28 120.9(4) . .
C26 C27 H27A 119.6 . .
C28 C27 H27A 119.6 . .
C29 C28 C27 120.5(4) . .
C29 C28 H28A 119.8 . .
C27 C28 H28A 119.8 . .
C28 C29 C30 120.2(3) . .
C28 C29 C36 118.1(3) . .
C30 C29 C36 121.6(4) . .
C31 C30 C35 119.5(4) . .
C31 C30 C29 118.3(3) . .
C35 C30 C29 122.1(4) . .
C30 C31 C26 119.8(3) . .
C30 C31 C32 118.3(4) . .
C26 C31 C32 121.8(3) . .
C33 C32 C31 119.9(4) . .
C33 C32 H32A 120.1 . .
C31 C32 H32A 120.1 . .
C32 C33 C34 121.4(4) . .
C32 C33 H33A 119.3 . .
C34 C33 H33A 119.3 . .
C35 C34 C33 120.5(4) . .
C35 C34 H34A 119.7 . .
C33 C34 H34A 119.7 . .
C34 C35 C30 120.3(4) . .
C34 C35 H35A 119.9 . .
C30 C35 H35A 119.9 . .
O11 C36 O12 123.3(3) . .
O11 C36 C29 119.2(4) . .
O12 C36 C29 117.5(3) . .
C39A N1A C37A 106.5(10) . .
C39A N1A C40A 128.3(9) . .
C37A N1A C40A 125.0(8) . .
C39A N2A C38A 106.7(8) . .
C39A N2A C41A 122.1(7) . .
C38A N2A C41A 130.7(9) . .
C38A C37A N1A 108.7(11) . .
C38A C37A H37A 125.7 . .
N1A C37A H37A 125.7 . .
C37A C38A N2A 109.1(11) . .
C37A C38A H38A 125.4 . .
N2A C38A H38A 125.4 . .
N2A C39A N1A 108.8(7) . .
N2A C39A H39A 125.6 . .
N1A C39A H39A 125.6 . .
N1A C40A H40A 109.5 . .
N1A C40A H40B 109.5 . .
H40A C40A H40B 109.5 . .
N1A C40A H40C 109.5 . .
H40A C40A H40C 109.5 . .
H40B C40A H40C 109.5 . .
N2A C41A C42A 119.6(8) . .
N2A C41A H41A 107.4 . .
C42A C41A H41A 107.4 . .
N2A C41A H41B 107.4 . .
C42A C41A H41B 107.4 . .
H41A C41A H41B 106.9 . .
C44A C43A C42A 94.0(7) . .
C44A C43A H43A 112.9 . .
C42A C43A H43A 112.9 . .
C44A C43A H43B 112.9 . .
C42A C43A H43B 112.9 . .
H43A C43A H43B 110.3 . .
C41A C42A C43A 101.6(8) . .
C41A C42A H42A 111.5 . .
C43A C42A H42A 111.5 . .
C41A C42A H42B 111.5 . .
C43A C42A H42B 111.5 . .
H42A C42A H42B 109.3 . .
C45A C44A C43A 120.6(9) . .
C45A C44A H44A 107.2 . .
C43A C44A H44A 107.2 . .
C45A C44A H44B 107.2 . .
C43A C44A H44B 107.2 . .
H44A C44A H44B 106.8 . .
C46A C45A C44A 104.0(8) . .
C46A C45A H45A 111.0 . .
C44A C45A H45A 111.0 . .
C46A C45A H45B 111.0 . .
C44A C45A H45B 111.0 . .
H45A C45A H45B 109.0 . .
C45A C46A H46A 109.5 . .
C45A C46A H46B 109.5 . .
H46A C46A H46B 109.5 . .
C45A C46A H46C 109.5 . .
H46A C46A H46C 109.5 . .
H46B C46A H46C 109.5 . .
C39B N1B C37B 109.1(13) . .
C39B N1B C40B 127.7(11) . .
C37B N1B C40B 123.1(9) . .
C39B N2B C38B 109.9(10) . .
C39B N2B C41B 129.4(10) . .
C38B N2B C41B 120.8(10) . .
C38B C37B N1B 105.9(13) . .
C38B C37B H37B 127.1 . .
N1B C37B H37B 127.1 . .
C37B C38B N2B 109.4(13) . .
C37B C38B H38B 125.3 . .
N2B C38B H38B 125.3 . .
N2B C39B N1B 105.0(10) . .
N2B C39B H39B 127.5 . .
N1B C39B H39B 127.5 . .
N1B C40B H40D 109.5 . .
N1B C40B H40E 109.5 . .
H40D C40B H40E 109.5 . .
N1B C40B H40F 109.5 . .
H40D C40B H40F 109.5 . .
H40E C40B H40F 109.5 . .
N2B C41B C42B 104.4(10) . .
N2B C41B H41C 110.9 . .
C42B C41B H41C 110.9 . .
N2B C41B H41D 110.9 . .
C42B C41B H41D 110.9 . .
H41C C41B H41D 108.9 . .
C43B C42B C41B 87.8(11) . .
C43B C42B H42C 114.0 . .
C41B C42B H42C 114.0 . .
C43B C42B H42D 114.0 . .
C41B C42B H42D 114.0 . .
H42C C42B H42D 111.2 . .
C42B C43B C44B 120.1(12) . .
C42B C43B H43C 107.3 . .
C44B C43B H43C 107.3 . .
C42B C43B H43D 107.3 . .
C44B C43B H43D 107.3 . .
H43C C43B H43D 106.9 . .
C45B C44B C43B 109.2(10) . .
C45B C44B H44C 109.8 . .
C43B C44B H44C 109.8 . .
C45B C44B H44D 109.8 . .
C43B C44B H44D 109.8 . .
H44C C44B H44D 108.3 . .
C46B C45B C44B 111.7(10) . .
C46B C45B H45C 109.3 . .
C44B C45B H45C 109.3 . .
C46B C45B H45D 109.3 . .
C44B C45B H45D 109.3 . .
H45C C45B H45D 107.9 . .
C45B C46B H46D 109.5 . .
C45B C46B H46E 109.5 . .
H46D C46B H46E 109.5 . .
C45B C46B H46F 109.5 . .
H46D C46B H46F 109.5 . .
H46E C46B H46F 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O7 2.284(2) 4_565
Dy1 O1 2.293(3) .
Dy1 O5 2.295(3) 4_566
Dy1 O6 2.302(3) 2_644
Dy1 O3 2.305(3) .
Dy1 O2 2.321(2) 3_655
Dy1 Cl1 2.8000(9) .
Dy2 O11 2.254(2) 4_565
Dy2 O4 2.274(2) .
Dy2 O10 2.291(2) 3
Dy2 O8 2.329(2) 4_565
Dy2 O9 2.364(2) .
Dy2 O12 2.365(2) 2_545
Dy2 Cl1 2.7603(9) .
O1 C1 1.238(4) .
O2 C1 1.249(4) .
O2 Dy1 2.321(2) 3_655
O3 C13 1.262(4) .
O5 C12 1.247(4) .
O5 Dy1 2.295(3) 4_565
O4 C13 1.256(4) .
O6 C12 1.251(5) .
O6 Dy1 2.302(3) 2_654
O7 C24 1.246(4) .
O7 Dy1 2.284(2) 4_566
O8 C24 1.253(4) .
O8 Dy2 2.329(2) 4_566
O9 C25 1.234(4) .
O10 C25 1.265(4) .
O10 Dy2 2.291(2) 3
O11 C36 1.240(4) .
O11 Dy2 2.254(2) 4_566
O12 C36 1.258(5) .
O12 Dy2 2.365(2) 2
C1 C2 1.511(5) .
C2 C3 1.378(5) .
C2 C7 1.423(5) .
C3 C4 1.402(5) .
C3 H3A 0.9300 .
C4 C5 1.362(5) .
C4 H4A 0.9300 .
C5 C6 1.429(5) .
C5 C12 1.501(5) .
C6 C11 1.419(5) .
C6 C7 1.432(5) .
C7 C8 1.413(5) .
C8 C9 1.365(5) .
C8 H8A 0.9300 .
C9 C10 1.388(5) .
C9 H9A 0.9300 .
C10 C11 1.374(5) .
C10 H10A 0.9300 .
C11 H11A 0.9300 .
C13 C14 1.499(5) .
C14 C15 1.366(5) .
C14 C19 1.427(5) .
C15 C16 1.385(5) .
C15 H15A 0.9300 .
C16 C17 1.383(5) .
C16 H16A 0.9300 .
C17 C18 1.428(5) .
C17 C24 1.521(5) .
C18 C23 1.422(5) .
C18 C19 1.424(4) .
C19 C20 1.421(5) .
C20 C21 1.360(5) .
C20 H20A 0.9300 .
C21 C22 1.392(5) .
C21 H21A 0.9300 .
C22 C23 1.348(5) .
C22 H22A 0.9300 .
C23 H23A 0.9300 .
C25 C26 1.507(5) .
C26 C27 1.365(5) .
C26 C31 1.425(5) .
C27 C28 1.404(5) .
C27 H27A 0.9300 .
C28 C29 1.374(5) .
C28 H28A 0.9300 .
C29 C30 1.427(5) .
C29 C36 1.497(5) .
C30 C31 1.418(5) .
C30 C35 1.422(5) .
C31 C32 1.427(5) .
C32 C33 1.367(6) .
C32 H32A 0.9300 .
C33 C34 1.395(6) .
C33 H33A 0.9300 .
C34 C35 1.356(6) .
C34 H34A 0.9300 .
C35 H35A 0.9300 .
N1A C39A 1.326(7) .
N1A C37A 1.361(8) .
N1A C40A 1.433(10) .
N2A C39A 1.311(9) .
N2A C38A 1.361(7) .
N2A C41A 1.513(10) .
C37A C38A 1.263(14) .
C37A H37A 0.9300 .
C38A H38A 0.9300 .
C39A H39A 0.9300 .
C40A H40A 0.9600 .
C40A H40B 0.9600 .
C40A H40C 0.9600 .
C41A C42A 1.555(8) .
C41A H41A 0.9700 .
C41A H41B 0.9700 .
C43A C44A 1.613(9) .
C43A C42A 1.627(9) .
C43A H43A 0.9700 .
C43A H43B 0.9700 .
C42A H42A 0.9700 .
C42A H42B 0.9700 .
C44A C45A 1.565(8) .
C44A H44A 0.9700 .
C44A H44B 0.9700 .
C45A C46A 1.540(9) .
C45A H45A 0.9700 .
C45A H45B 0.9700 .
C46A H46A 0.9600 .
C46A H46B 0.9600 .
C46A H46C 0.9600 .
N1B C39B 1.338(8) .
N1B C37B 1.364(9) .
N1B C40B 1.445(12) .
N2B C39B 1.282(10) .
N2B C38B 1.347(9) .
N2B C41B 1.468(11) .
C37B C38B 1.258(17) .
C37B H37B 0.9300 .
C38B H38B 0.9300 .
C39B H39B 0.9300 .
C40B H40D 0.9600 .
C40B H40E 0.9600 .
C40B H40F 0.9600 .
C41B C42B 1.527(10) .
C41B H41C 0.9700 .
C41B H41D 0.9700 .
C42B C43B 1.519(9) .
C42B H42C 0.9700 .
C42B H42D 0.9700 .
C43B C44B 1.578(10) .
C43B H43C 0.9700 .
C43B H43D 0.9700 .
C44B C45B 1.556(10) .
C44B H44C 0.9700 .
C44B H44D 0.9700 .
C45B C46B 1.505(10) .
C45B H45C 0.9700 .
C45B H45D 0.9700 .
C46B H46D 0.9600 .
C46B H46E 0.9600 .
C46B H46F 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
O11 Dy2 Cl1 Dy1 60.5(2) 4_565
O4 Dy2 Cl1 Dy1 -26.67(7) .
O10 Dy2 Cl1 Dy1 129.46(7) 3
O8 Dy2 Cl1 Dy1 51.63(7) 4_565
O9 Dy2 Cl1 Dy1 -93.90(8) .
O12 Dy2 Cl1 Dy1 -149.72(8) 2_545
O7 Dy1 Cl1 Dy2 -38.60(8) 4_565
O1 Dy1 Cl1 Dy2 -50.2(2) .
O5 Dy1 Cl1 Dy2 112.27(9) 4_566
O6 Dy1 Cl1 Dy2 -116.42(8) 2_644
O3 Dy1 Cl1 Dy2 45.25(8) .
O2 Dy1 Cl1 Dy2 166.94(9) 3_655
O7 Dy1 O1 C1 -155.0(5) 4_565
O5 Dy1 O1 C1 51.1(5) 4_566
O6 Dy1 O1 C1 -75.5(5) 2_644
O3 Dy1 O1 C1 124.6(5) .
O2 Dy1 O1 C1 -8.1(5) 3_655
Cl1 Dy1 O1 C1 -143.5(4) .
O7 Dy1 O3 C13 31.6(4) 4_565
O1 Dy1 O3 C13 109.3(4) .
O5 Dy1 O3 C13 -176.5(4) 4_566
O6 Dy1 O3 C13 20.5(6) 2_644
O2 Dy1 O3 C13 -113.6(4) 3_655
Cl1 Dy1 O3 C13 -47.1(4) .
O11 Dy2 O4 C13 163.4(4) 4_565
O10 Dy2 O4 C13 -115.4(4) 3
O8 Dy2 O4 C13 -118.0(4) 4_565
O9 Dy2 O4 C13 90.5(4) .
O12 Dy2 O4 C13 30.7(5) 2_545
Cl1 Dy2 O4 C13 -34.8(4) .
O11 Dy2 O9 C25 17.1(4) 4_565
O4 Dy2 O9 C25 117.4(4) .
O10 Dy2 O9 C25 -49.7(4) 3
O8 Dy2 O9 C25 70.4(4) 4_565
O12 Dy2 O9 C25 -115.3(4) 2_545
Cl1 Dy2 O9 C25 -170.9(3) .
Dy1 O1 C1 O2 -3.6(8) .
Dy1 O1 C1 C2 174.1(3) .
Dy1 O2 C1 O1 16.9(8) 3_655
Dy1 O2 C1 C2 -160.7(3) 3_655
O1 C1 C2 C3 -42.3(5) .
O2 C1 C2 C3 135.5(4) .
O1 C1 C2 C7 137.0(4) .
O2 C1 C2 C7 -45.2(6) .
C7 C2 C3 C4 2.4(6) .
C1 C2 C3 C4 -178.3(4) .
C2 C3 C4 C5 -0.9(6) .
C3 C4 C5 C6 -1.9(6) .
C3 C4 C5 C12 175.6(4) .
C4 C5 C6 C11 -174.0(4) .
C12 C5 C6 C11 8.7(6) .
C4 C5 C6 C7 3.0(6) .
C12 C5 C6 C7 -174.3(4) .
C3 C2 C7 C8 177.2(4) .
C1 C2 C7 C8 -2.1(6) .
C3 C2 C7 C6 -1.2(6) .
C1 C2 C7 C6 179.5(4) .
C11 C6 C7 C8 -2.8(6) .
C5 C6 C7 C8 -179.9(4) .
C11 C6 C7 C2 175.6(4) .
C5 C6 C7 C2 -1.5(6) .
C2 C7 C8 C9 -175.7(4) .
C6 C7 C8 C9 2.7(6) .
C7 C8 C9 C10 -0.8(7) .
C8 C9 C10 C11 -1.0(7) .
C9 C10 C11 C6 0.8(7) .
C5 C6 C11 C10 178.1(4) .
C7 C6 C11 C10 1.1(6) .
Dy1 O5 C12 O6 19.6(13) 4_565
Dy1 O5 C12 C5 -158.2(8) 4_565
Dy1 O6 C12 O5 3.1(6) 2_654
Dy1 O6 C12 C5 -179.2(2) 2_654
C4 C5 C12 O5 37.7(6) .
C6 C5 C12 O5 -144.9(4) .
C4 C5 C12 O6 -140.2(4) .
C6 C5 C12 O6 37.2(6) .
Dy2 O4 C13 O3 60.9(7) .
Dy2 O4 C13 C14 -116.5(4) .
Dy1 O3 C13 O4 4.2(7) .
Dy1 O3 C13 C14 -178.4(3) .
O4 C13 C14 C15 143.0(4) .
O3 C13 C14 C15 -34.5(5) .
O4 C13 C14 C19 -36.0(6) .
O3 C13 C14 C19 146.5(4) .
C19 C14 C15 C16 0.4(7) .
C13 C14 C15 C16 -178.7(4) .
C14 C15 C16 C17 1.4(7) .
C15 C16 C17 C18 -0.9(6) .
C15 C16 C17 C24 -179.3(4) .
C16 C17 C18 C23 -178.7(4) .
C24 C17 C18 C23 -0.4(6) .
C16 C17 C18 C19 -1.3(5) .
C24 C17 C18 C19 177.0(3) .
C23 C18 C19 C20 2.0(5) .
C17 C18 C19 C20 -175.5(3) .
C23 C18 C19 C14 -179.5(3) .
C17 C18 C19 C14 3.0(5) .
C15 C14 C19 C20 175.9(4) .
C13 C14 C19 C20 -5.1(6) .
C15 C14 C19 C18 -2.6(6) .
C13 C14 C19 C18 176.4(3) .
C18 C19 C20 C21 -1.0(6) .
C14 C19 C20 C21 -179.5(4) .
C19 C20 C21 C22 -0.3(7) .
C20 C21 C22 C23 0.5(7) .
C21 C22 C23 C18 0.6(7) .
C19 C18 C23 C22 -1.8(6) .
C17 C18 C23 C22 175.6(4) .
Dy1 O7 C24 O8 7.1(10) 4_566
Dy1 O7 C24 C17 -172.2(5) 4_566
Dy2 O8 C24 O7 -37.0(6) 4_566
Dy2 O8 C24 C17 142.3(3) 4_566
C16 C17 C24 O7 32.6(5) .
C18 C17 C24 O7 -145.7(4) .
C16 C17 C24 O8 -146.7(4) .
C18 C17 C24 O8 35.0(5) .
Dy2 O9 C25 O10 35.7(6) .
Dy2 O9 C25 C26 -147.7(3) .
Dy2 O10 C25 O9 3.3(7) 3
Dy2 O10 C25 C26 -173.4(2) 3
O9 C25 C26 C27 -44.0(5) .
O10 C25 C26 C27 133.0(4) .
O9 C25 C26 C31 140.4(4) .
O10 C25 C26 C31 -42.6(5) .
C31 C26 C27 C28 6.0(6) .
C25 C26 C27 C28 -169.7(4) .
C26 C27 C28 C29 0.6(7) .
C27 C28 C29 C30 -7.3(6) .
C27 C28 C29 C36 169.2(4) .
C28 C29 C30 C31 7.3(6) .
C36 C29 C30 C31 -169.1(3) .
C28 C29 C30 C35 -171.3(4) .
C36 C29 C30 C35 12.3(6) .
C35 C30 C31 C26 177.8(4) .
C29 C30 C31 C26 -0.8(6) .
C35 C30 C31 C32 0.7(6) .
C29 C30 C31 C32 -177.9(4) .
C27 C26 C31 C30 -5.8(6) .
C25 C26 C31 C30 169.7(3) .
C27 C26 C31 C32 171.2(4) .
C25 C26 C31 C32 -13.3(6) .
C30 C31 C32 C33 0.9(6) .
C26 C31 C32 C33 -176.2(4) .
C31 C32 C33 C34 -0.8(7) .
C32 C33 C34 C35 -1.0(8) .
C33 C34 C35 C30 2.6(7) .
C31 C30 C35 C34 -2.4(6) .
C29 C30 C35 C34 176.1(4) .
Dy2 O11 C36 O12 -93.7(9) 4_566
Dy2 O11 C36 C29 88.6(9) 4_566
Dy2 O12 C36 O11 12.6(5) 2
Dy2 O12 C36 C29 -169.6(2) 2
C28 C29 C36 O11 45.3(5) .
C30 C29 C36 O11 -138.2(4) .
C28 C29 C36 O12 -132.6(4) .
C30 C29 C36 O12 44.0(5) .
C39A N1A C37A C38A 2(2) .
C40A N1A C37A C38A 177.8(11) .
N1A C37A C38A N2A 0.4(19) .
C39A N2A C38A C37A -3(2) .
C41A N2A C38A C37A 168.2(13) .
C38A N2A C39A N1A 5(3) .
C41A N2A C39A N1A -167.5(14) .
C37A N1A C39A N2A -5(3) .
C40A N1A C39A N2A -179.7(14) .
C39A N2A C41A C42A -175(2) .
C38A N2A C41A C42A 14.2(16) .
N2A C41A C42A C43A -88.4(11) .
C44A C43A C42A C41A 179.7(9) .
C42A C43A C44A C45A -153.6(11) .
C43A C44A C45A C46A -45.1(15) .
C39B N1B C37B C38B -6(3) .
C40B N1B C37B C38B 176.8(19) .
N1B C37B C38B N2B 1(3) .
C39B N2B C38B C37B 4(4) .
C41B N2B C38B C37B -176.8(17) .
C38B N2B C39B N1B -8(4) .
C41B N2B C39B N1B 173.4(18) .
C37B N1B C39B N2B 8(4) .
C40B N1B C39B N2B -174.5(18) .
C39B N2B C41B C42B -2(3) .
C38B N2B C41B C42B 179.0(19) .
N2B C41B C42B C43B 116.5(12) .
C41B C42B C43B C44B 70.6(18) .
C42B C43B C44B C45B 179.0(15) .
C43B C44B C45B C46B -168.4(16) .
