#------------------------------------------------------------------------------
#$Date: 2016-03-25 15:35:39 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179926 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/21/7022130.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7022130
loop_
_publ_author_name
'Zhang, Xiao-Ping'
'Tian, Han-Rui'
'Yan, Gu-Fan'
'Su, Ying'
'Feng, Yun-Long'
'Cheng, Jian-Wen'
_publ_section_title
;
 Incorporating different secondary building units of {Bi2}, {Bi8} and
 {Bi10} to construct diversity of luminescent bismuth-organic frameworks.
;
_journal_issue                   4
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1088
_journal_page_last               1093
_journal_paper_doi               10.1039/c2dt31821k
_journal_volume                  42
_journal_year                    2013
_chemical_formula_sum            'C28 H24 Bi4 N4 O24'
_chemical_formula_weight         1636.43
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                112.633(2)
_cell_angle_beta                 101.662(2)
_cell_angle_gamma                105.5220(10)
_cell_formula_units_Z            2
_cell_length_a                   10.6283(2)
_cell_length_b                   13.6543(3)
_cell_length_c                   14.4484(5)
_cell_measurement_reflns_used    7074
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.53
_cell_measurement_theta_min      1.63
_cell_volume                     1751.53(9)
_computing_cell_refinement       'SAINT (Bruker, 2006)'
_computing_data_collection       'APEXII (Bruker, 2006)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'DIAMOND (Brandenburg, 1999)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'Bruker APEX-II area-detector diffractometer'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0454
_diffrn_reflns_av_sigmaI/netI    0.0525
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            26923
_diffrn_reflns_theta_full        27.53
_diffrn_reflns_theta_max         27.53
_diffrn_reflns_theta_min         1.63
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    20.142
_exptl_absorpt_correction_T_max  0.4325
_exptl_absorpt_correction_T_min  0.0856
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    3.103
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             1488
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.05
_refine_diff_density_max         4.178
_refine_diff_density_min         -2.042
_refine_diff_density_rms         0.235
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.012
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     541
_refine_ls_number_reflns         7914
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.012
_refine_ls_R_factor_all          0.0532
_refine_ls_R_factor_gt           0.0324
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0322P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0684
_refine_ls_wR_factor_ref         0.0756
_reflns_number_gt                5896
_reflns_number_total             7914
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2dt31821k.txt
_cod_data_source_block           2
_cod_original_cell_volume        1751.53(8)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7022130
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Bi1 Bi 0.20426(3) -0.25187(2) -0.35431(2) 0.01917(8) Uani 1 1 d .
Bi2 Bi 0.34284(3) 0.12042(2) -0.24174(2) 0.01864(8) Uani 1 1 d .
Bi3 Bi 0.50317(3) 0.16401(2) 0.03035(2) 0.01829(8) Uani 1 1 d .
Bi4 Bi 0.62816(3) 0.52851(2) 0.13168(2) 0.01846(7) Uani 1 1 d .
C1 C -0.1024(7) -0.4172(6) -0.3888(6) 0.0236(17) Uani 1 1 d .
C2 C -0.2412(8) -0.4559(7) -0.3991(7) 0.033(2) Uani 1 1 d .
H2A H -0.2852 -0.5265 -0.4024 0.039 Uiso 1 1 calc R
C3 C -0.3121(8) -0.3856(7) -0.4044(7) 0.035(2) Uani 1 1 d .
H3A H -0.4049 -0.4083 -0.4094 0.042 Uiso 1 1 calc R
C4 C -0.2472(8) -0.2821(6) -0.4025(6) 0.0289(18) Uani 1 1 d .
H4A H -0.2951 -0.2354 -0.4073 0.035 Uiso 1 1 calc R
C5 C -0.1086(7) -0.2506(6) -0.3929(6) 0.0236(16) Uani 1 1 d .
C6 C -0.0143(8) -0.4856(6) -0.3867(6) 0.0256(17) Uani 1 1 d .
C7 C -0.0239(8) -0.1381(6) -0.3882(6) 0.0230(16) Uani 1 1 d .
C8 C 0.5728(7) 0.0348(6) -0.3530(6) 0.0214(16) Uani 1 1 d .
C9 C 0.6815(7) 0.0367(6) -0.3914(6) 0.0276(18) Uani 1 1 d .
H9A H 0.7175 -0.0202 -0.4024 0.033 Uiso 1 1 calc R
C10 C 0.7358(8) 0.1274(6) -0.4134(7) 0.033(2) Uani 1 1 d .
H10A H 0.8109 0.1331 -0.4375 0.039 Uiso 1 1 calc R
C11 C 0.6773(8) 0.2077(6) -0.3990(6) 0.0266(18) Uani 1 1 d .
H11A H 0.7080 0.2651 -0.4182 0.032 Uiso 1 1 calc R
C12 C 0.5722(7) 0.2030(6) -0.3558(6) 0.0245(17) Uani 1 1 d .
C13 C 0.5038(7) -0.0607(6) -0.3287(6) 0.0242(17) Uani 1 1 d .
C14 C 0.5095(8) 0.2907(6) -0.3306(6) 0.0277(18) Uani 1 1 d .
C15 C 0.2423(7) 0.0580(6) 0.1037(6) 0.0187(15) Uani 1 1 d .
C16 C 0.1188(7) 0.0397(6) 0.1260(6) 0.0224(17) Uani 1 1 d .
H16A H 0.0783 -0.0245 0.1341 0.027 Uiso 1 1 calc R
C17 C 0.0585(7) 0.1187(6) 0.1358(6) 0.0248(17) Uani 1 1 d .
H17A H -0.0241 0.1081 0.1503 0.030 Uiso 1 1 calc R
C18 C 0.1200(7) 0.2140(6) 0.1240(6) 0.0227(17) Uani 1 1 d .
H18A H 0.0793 0.2674 0.1292 0.027 Uiso 1 1 calc R
C19 C 0.2444(7) 0.2277(6) 0.1042(6) 0.0178(15) Uani 1 1 d .
C20 C 0.3086(7) -0.0280(6) 0.0836(6) 0.0214(16) Uani 1 1 d .
C21 C 0.3220(7) 0.3298(6) 0.0924(6) 0.0204(16) Uani 1 1 d .
C22 C 0.9288(7) 0.5076(6) 0.1326(5) 0.0182(15) Uani 1 1 d .
C23 C 1.0645(7) 0.5337(6) 0.1341(6) 0.0237(17) Uani 1 1 d .
H23A H 1.1096 0.4844 0.1360 0.028 Uiso 1 1 calc R
C24 C 1.1316(7) 0.6348(6) 0.1326(6) 0.0251(17) Uani 1 1 d .
H24A H 1.2216 0.6525 0.1307 0.030 Uiso 1 1 calc R
C25 C 1.0654(7) 0.7093(6) 0.1338(6) 0.0252(17) Uani 1 1 d .
H25A H 1.1098 0.7777 0.1334 0.030 Uiso 1 1 calc R
C26 C 0.9305(7) 0.6791(6) 0.1357(6) 0.0214(16) Uani 1 1 d .
C27 C 0.8465(7) 0.4007(6) 0.1339(6) 0.0194(15) Uani 1 1 d .
C28 C 0.8543(7) 0.7588(6) 0.1499(6) 0.0197(15) Uani 1 1 d .
N1 N -0.0389(6) -0.3162(5) -0.3847(5) 0.0211(13) Uani 1 1 d .
N2 N 0.5201(6) 0.1164(5) -0.3332(5) 0.0187(13) Uani 1 1 d .
N3 N 0.3026(5) 0.1512(4) 0.0935(5) 0.0171(13) Uani 1 1 d .
N4 N 0.8647(6) 0.5791(5) 0.1324(5) 0.0182(13) Uani 1 1 d .
O1 O -0.0698(5) -0.5868(4) -0.4049(5) 0.0343(14) Uani 1 1 d .
OW1 O 0.4193(5) -0.2798(4) -0.2728(5) 0.0325(13) Uani 1 1 d .
O2 O 0.1151(5) -0.4370(4) -0.3712(4) 0.0266(12) Uani 1 1 d .
OW2 O 0.4025(6) -0.4955(5) -0.3283(5) 0.0441(16) Uani 1 1 d .
O3 O 0.1061(5) -0.1170(4) -0.3700(4) 0.0305(13) Uani 1 1 d .
OW3 O 0.1001(7) 0.1213(5) -0.3872(5) 0.0567(18) Uani 1 1 d .
O4 O -0.0839(5) -0.0780(4) -0.4044(5) 0.0337(14) Uani 1 1 d .
OW4 O 0.8454(6) 0.6509(5) 0.3495(5) 0.0420(15) Uani 1 1 d .
O5 O 0.5465(6) -0.1402(5) -0.3458(5) 0.0394(15) Uani 1 1 d .
O6 O 0.4008(5) -0.0555(4) -0.2976(4) 0.0223(11) Uani 1 1 d .
O7 O 0.4230(5) 0.2833(4) -0.2809(4) 0.0272(13) Uani 1 1 d .
O8 O 0.5422(7) 0.3651(5) -0.3605(5) 0.0492(18) Uani 1 1 d .
O9 O 0.2634(6) -0.1134(5) 0.0936(6) 0.057(2) Uani 1 1 d .
O10 O 0.4181(5) -0.0048(4) 0.0555(4) 0.0216(11) Uani 1 1 d .
O11 O 0.4358(5) 0.3317(4) 0.0736(4) 0.0221(11) Uani 1 1 d .
O12 O 0.2763(6) 0.4057(4) 0.1042(5) 0.0380(15) Uani 1 1 d .
O13 O 0.9025(5) 0.3347(4) 0.1425(4) 0.0303(13) Uani 1 1 d .
O14 O 0.7170(5) 0.3838(4) 0.1236(4) 0.0253(12) Uani 1 1 d .
O15 O 0.7263(5) 0.7158(4) 0.1453(4) 0.0210(11) Uani 1 1 d .
O16 O 0.9112(6) 0.8570(4) 0.1676(5) 0.0393(15) Uani 1 1 d .
O17 O 0.2268(5) -0.1753(4) -0.1956(4) 0.0271(12) Uani 1 1 d .
O18 O 0.3259(5) 0.0592(4) -0.1143(4) 0.0185(11) Uani 1 1 d .
O19 O 0.5253(5) 0.2226(4) -0.1062(4) 0.0196(11) Uani 1 1 d .
O20 O 0.5869(5) 0.4518(4) -0.0375(4) 0.0189(11) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O17 Bi1 O2 92.63(18) . .
O17 Bi1 N1 85.2(2) . .
O2 Bi1 N1 68.07(18) . .
O17 Bi1 O3 86.66(19) . .
O2 Bi1 O3 135.08(16) . .
N1 Bi1 O3 67.11(17) . .
O17 Bi1 OW1 79.2(2) . .
O2 Bi1 OW1 76.35(16) . .
N1 Bi1 OW1 140.27(17) . .
O3 Bi1 OW1 146.43(16) . .
O17 Bi1 O6 82.28(16) . .
O2 Bi1 O6 154.91(17) . .
N1 Bi1 O6 135.27(17) . .
O3 Bi1 O6 69.41(15) . .
OW1 Bi1 O6 78.56(15) . .
O19 Bi2 O18 71.11(16) . .
O19 Bi2 O7 82.43(17) . .
O18 Bi2 O7 147.75(16) . .
O19 Bi2 O6 94.38(16) . .
O18 Bi2 O6 73.83(15) . .
O7 Bi2 O6 127.67(15) . .
O19 Bi2 N2 80.91(17) . .
O18 Bi2 N2 126.30(17) . .
O7 Bi2 N2 64.45(16) . .
O6 Bi2 N2 63.49(15) . .
O19 Bi2 O15 80.82(16) . 2_665
O18 Bi2 O15 90.41(15) . 2_665
O7 Bi2 O15 66.89(15) . 2_665
O6 Bi2 O15 164.22(15) . 2_665
N2 Bi2 O15 129.66(15) . 2_665
O19 Bi2 Bi3 38.42(11) . .
O18 Bi2 Bi3 32.76(11) . .
O7 Bi2 Bi3 118.10(13) . .
O6 Bi2 Bi3 83.49(11) . .
N2 Bi2 Bi3 108.52(13) . .
O15 Bi2 Bi3 83.50(11) 2_665 .
O18 Bi3 O19 68.26(15) . .
O18 Bi3 O10 80.80(16) . .
O19 Bi3 O10 142.33(16) . .
O18 Bi3 O11 92.52(16) . .
O19 Bi3 O11 73.82(15) . .
O10 Bi3 O11 130.30(14) . .
O18 Bi3 N3 76.28(17) . .
O19 Bi3 N3 123.15(17) . .
O10 Bi3 N3 65.85(16) . .
O11 Bi3 N3 64.73(15) . .
O18 Bi3 O10 81.44(17) . 2_655
O19 Bi3 O10 90.11(14) . 2_655
O10 Bi3 O10 63.67(17) . 2_655
O11 Bi3 O10 163.92(15) . 2_655
N3 Bi3 O10 127.19(15) . 2_655
O18 Bi3 Bi2 35.61(11) . .
O19 Bi3 Bi2 32.71(11) . .
O10 Bi3 Bi2 114.35(12) . .
O11 Bi3 Bi2 80.01(12) . .
N3 Bi3 Bi2 100.76(14) . .
O10 Bi3 Bi2 86.58(11) 2_655 .
O20 Bi4 O14 84.11(17) . .
O20 Bi4 O15 90.09(16) . .
O14 Bi4 O15 133.44(15) . .
O20 Bi4 N4 80.82(18) . .
O14 Bi4 N4 66.92(16) . .
O15 Bi4 N4 66.55(16) . .
O20 Bi4 O20 69.78(18) . 2_665
O14 Bi4 O20 139.59(16) . 2_665
O15 Bi4 O20 78.47(15) . 2_665
N4 Bi4 O20 133.87(16) . 2_665
O20 Bi4 O11 80.44(16) . .
O14 Bi4 O11 66.87(15) . .
O15 Bi4 O11 156.89(16) . .
N4 Bi4 O11 131.42(16) . .
O20 Bi4 O11 78.47(14) 2_665 .
N1 C1 C2 121.5(7) . .
N1 C1 C6 114.9(6) . .
C2 C1 C6 123.5(6) . .
C1 C2 C3 117.5(7) . .
C4 C3 C2 121.1(7) . .
C5 C4 C3 117.5(7) . .
N1 C5 C4 121.6(6) . .
N1 C5 C7 115.4(6) . .
C4 C5 C7 123.0(7) . .
O1 C6 O2 123.7(7) . .
O1 C6 C1 119.1(6) . .
O2 C6 C1 117.1(6) . .
O4 C7 O3 125.8(7) . .
O4 C7 C5 118.9(7) . .
O3 C7 C5 115.3(6) . .
N2 C8 C9 123.2(6) . .
N2 C8 C13 114.5(6) . .
C9 C8 C13 122.2(7) . .
C8 C9 C10 117.7(7) . .
C11 C10 C9 119.4(7) . .
C10 C11 C12 119.7(6) . .
N2 C12 C11 121.2(7) . .
N2 C12 C14 115.4(6) . .
C11 C12 C14 123.4(6) . .
O5 C13 O6 125.2(6) . .
O5 C13 C8 118.3(6) . .
O6 C13 C8 116.4(6) . .
O8 C14 O7 124.4(7) . .
O8 C14 C12 118.1(6) . .
O7 C14 C12 117.5(6) . .
N3 C15 C16 121.2(6) . .
N3 C15 C20 116.9(6) . .
C16 C15 C20 121.8(6) . .
C17 C16 C15 118.5(6) . .
C16 C17 C18 120.2(6) . .
C17 C18 C19 118.1(7) . .
N3 C19 C18 122.1(6) . .
N3 C19 C21 115.4(6) . .
C18 C19 C21 122.4(6) . .
O9 C20 O10 122.7(7) . .
O9 C20 C15 121.5(6) . .
O10 C20 C15 115.9(5) . .
O12 C21 O11 124.8(6) . .
O12 C21 C19 119.1(6) . .
O11 C21 C19 116.1(6) . .
N4 C22 C23 121.1(6) . .
N4 C22 C27 115.9(6) . .
C23 C22 C27 123.0(6) . .
C22 C23 C24 118.5(7) . .
C25 C24 C23 120.2(7) . .
C24 C25 C26 118.1(6) . .
N4 C26 C25 121.1(7) . .
N4 C26 C28 115.8(6) . .
C25 C26 C28 122.9(6) . .
O13 C27 O14 124.7(6) . .
O13 C27 C22 119.7(6) . .
O14 C27 C22 115.7(6) . .
O16 C28 O15 123.5(7) . .
O16 C28 C26 121.1(6) . .
O15 C28 C26 115.4(6) . .
C5 N1 C1 120.8(6) . .
C5 N1 Bi1 120.5(4) . .
C1 N1 Bi1 118.7(5) . .
C8 N2 C12 118.6(6) . .
C8 N2 Bi2 121.4(4) . .
C12 N2 Bi2 119.8(4) . .
C19 N3 C15 119.9(5) . .
C19 N3 Bi3 120.6(4) . .
C15 N3 Bi3 119.0(4) . .
C22 N4 C26 120.9(6) . .
C22 N4 Bi4 119.2(4) . .
C26 N4 Bi4 119.9(5) . .
C6 O2 Bi1 120.8(4) . .
C7 O3 Bi1 121.6(4) . .
C13 O6 Bi2 122.6(4) . .
C13 O6 Bi1 116.3(4) . .
Bi2 O6 Bi1 118.01(17) . .
C14 O7 Bi2 122.6(4) . .
C20 O10 Bi3 122.2(4) . .
C20 O10 Bi3 118.6(4) . 2_655
Bi3 O10 Bi3 116.33(17) . 2_655
C21 O11 Bi3 121.7(4) . .
C21 O11 Bi4 118.8(4) . .
Bi3 O11 Bi4 117.44(17) . .
C27 O14 Bi4 121.6(4) . .
C28 O15 Bi4 121.9(4) . .
C28 O15 Bi2 108.3(4) . 2_665
Bi4 O15 Bi2 122.96(18) . 2_665
Bi3 O18 Bi2 111.63(17) . .
Bi2 O19 Bi3 108.87(17) . .
Bi4 O20 Bi4 110.22(18) . 2_665
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Bi1 O17 2.051(5) .
Bi1 O2 2.345(5) .
Bi1 N1 2.382(5) .
Bi1 O3 2.405(5) .
Bi1 OW1 2.545(5) .
Bi1 O6 2.616(4) .
Bi2 O19 2.111(5) .
Bi2 O18 2.315(4) .
Bi2 O7 2.478(4) .
Bi2 O6 2.511(5) .
Bi2 N2 2.511(5) .
Bi2 O15 2.526(5) 2_665
Bi2 Bi3 3.6961(4) .
Bi3 O18 2.151(5) .
Bi3 O19 2.427(4) .
Bi3 O10 2.435(4) .
Bi3 O11 2.470(4) .
Bi3 N3 2.473(5) .
Bi3 O10 2.506(5) 2_655
Bi4 O20 2.148(5) .
Bi4 O14 2.382(5) .
Bi4 O15 2.401(4) .
Bi4 N4 2.419(5) .
Bi4 O20 2.550(5) 2_665
Bi4 O11 2.596(4) .
C1 N1 1.335(8) .
C1 C2 1.382(10) .
C1 C6 1.493(10) .
C2 C3 1.385(10) .
C3 C4 1.383(9) .
C4 C5 1.381(10) .
C5 N1 1.329(9) .
C5 C7 1.526(9) .
C6 O1 1.244(8) .
C6 O2 1.286(8) .
C7 O4 1.227(8) .
C7 O3 1.282(8) .
C8 N2 1.339(8) .
C8 C9 1.377(9) .
C8 C13 1.518(9) .
C9 C10 1.401(9) .
C10 C11 1.368(10) .
C11 C12 1.384(9) .
C12 N2 1.354(8) .
C12 C14 1.483(10) .
C13 O5 1.244(8) .
C13 O6 1.274(8) .
C14 O8 1.245(8) .
C14 O7 1.282(8) .
C15 N3 1.342(8) .
C15 C16 1.395(9) .
C15 C20 1.491(9) .
C16 C17 1.373(9) .
C17 C18 1.381(9) .
C18 C19 1.388(9) .
C19 N3 1.325(8) .
C19 C21 1.509(8) .
C20 O9 1.212(7) .
C20 O10 1.308(7) .
C21 O12 1.228(8) .
C21 O11 1.288(8) .
C22 N4 1.333(8) .
C22 C23 1.383(9) .
C22 C27 1.497(9) .
C23 C24 1.385(9) .
C24 C25 1.380(10) .
C25 C26 1.391(9) .
C26 N4 1.335(8) .
C26 C28 1.499(9) .
C27 O13 1.235(8) .
C27 O14 1.300(8) .
C28 O16 1.212(7) .
C28 O15 1.306(8) .
O10 Bi3 2.506(5) 2_655
O15 Bi2 2.526(5) 2_665
O20 Bi4 2.550(5) 2_665
