#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/43/7024315.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7024315
loop_
_publ_author_name
'Kaiba, A.'
'Shepherd, H. J.'
'Fedaoui, D.'
'Rosa, P.'
'Goeta, A. E.'
'Rebbani, N.'
'Létard, J F'
'Guionneau, P.'
_publ_section_title
;
 Crystallographic elucidation of purely structural, thermal and
 light-induced spin transitions in an iron(II) binuclear complex.
;
_journal_issue                   11
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2910
_journal_page_last               2918
_journal_paper_doi               10.1039/b914841h
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety         'C36 H26 Fe2 N16 S4, 2(C H4 O)'
_chemical_formula_sum            'C38 H34 Fe2 N16 O2 S4'
_chemical_formula_weight         986.75
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                72.0480(10)
_cell_angle_beta                 90.0010(10)
_cell_angle_gamma                62.7980(10)
_cell_formula_units_Z            4
_cell_length_a                   15.8910(7)
_cell_length_b                   17.3839(7)
_cell_length_c                   18.3423(8)
_cell_measurement_reflns_used    9753
_cell_measurement_temperature    30(2)
_cell_measurement_theta_max      55.655
_cell_measurement_theta_min      4.795
_cell_volume                     4227.3(3)
_computing_cell_refinement       'SAINT v6.45A (Bruker, 2003)'
_computing_data_collection       'SMART (Bruker, 2001)'
_computing_data_reduction        'SAINT v6.45A (Bruker, 2003)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      30(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.914
_diffrn_measurement_device_type  'Bruker SMART 1K CCD area detector'
_diffrn_measurement_method       ω-scans
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0374
_diffrn_reflns_av_sigmaI/netI    0.0350
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            72991
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         28.29
_diffrn_reflns_theta_min         2.30
_exptl_absorpt_coefficient_mu    0.941
_exptl_absorpt_correction_T_max  0.79
_exptl_absorpt_correction_T_min  0.72
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   Sadabs_G.M.Sheldrick
_exptl_crystal_colour            dark_red
_exptl_crystal_density_diffrn    1.550
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             2024
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.545
_refine_diff_density_min         -0.576
_refine_diff_density_rms         0.080
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.081
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1125
_refine_ls_number_reflns         19179
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.081
_refine_ls_R_factor_all          0.0473
_refine_ls_R_factor_gt           0.0404
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
calc w=1/[σ²(Fo²)+(0.0298P)²+5.3165P] where P=(Fo²+2Fc²)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0894
_refine_ls_wR_factor_ref         0.0922
_reflns_number_gt                17330
_reflns_number_total             19179
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b914841h.txt
_cod_data_source_block           2404_P-1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'multi_scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        ' C38 H34 Fe2 N16 O2 S4'
_cod_database_code               7024315
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Fe1 Fe -0.16104(5) 0.93310(4) 0.31234(5) 0.01266(14) Uani 1 1 d .
Fe2 Fe -0.33909(6) 1.06959(4) -0.32613(5) 0.01332(14) Uani 1 1 d .
S1A S -0.17886(9) 1.22350(7) 0.30403(6) 0.0165(2) Uani 1 1 d .
S1B S -0.41771(9) 1.38479(7) -0.41123(6) 0.0157(2) Uani 1 1 d .
S2A S -0.08308(9) 0.61063(7) 0.41923(6) 0.0156(2) Uani 1 1 d .
S2B S -0.34058(9) 0.78837(7) -0.29828(6) 0.0173(2) Uani 1 1 d .
N1A N -0.1062(3) 0.8782(2) 0.4347(2) 0.0122(7) Uani 1 1 d .
N1B N -0.3918(3) 1.1222(2) -0.43845(19) 0.0103(7) Uani 1 1 d .
N2A N -0.0023(3) 0.8635(2) 0.32279(18) 0.0129(7) Uani 1 1 d .
N2B N -0.2190(3) 1.0429(2) -0.37385(18) 0.0131(7) Uani 1 1 d .
N3A N -0.2873(3) 0.9663(2) 0.37091(18) 0.0112(7) Uani 1 1 d .
N3B N -0.4829(3) 1.1215(2) -0.32458(19) 0.0151(7) Uani 1 1 d .
N4A N -0.2054(2) 0.9677(2) 0.1887(2) 0.0174(7) Uani 1 1 d .
N4B N -0.2932(2) 1.0308(2) -0.2124(2) 0.0179(7) Uani 1 1 d .
N5A N -0.1712(3) 1.0629(2) 0.2941(2) 0.0196(7) Uani 1 1 d .
N5B N -0.3587(3) 1.1961(2) -0.34000(19) 0.0134(7) Uani 1 1 d .
N6A N -0.1464(3) 0.7980(2) 0.33401(19) 0.0119(7) Uani 1 1 d .
N6B N -0.3246(3) 0.9471(3) -0.3135(2) 0.0228(8) Uani 1 1 d .
N7A N 0.0646(3) 0.8392(2) 0.27691(18) 0.0127(7) Uani 1 1 d .
H7AN H 0.0521 0.8583 0.2259 0.015 Uiso 1 1 calc R
N7B N -0.1244(3) 1.0033(2) -0.3495(2) 0.0172(8) Uani 1 1 d .
H7BN H -0.0964 0.9752 -0.3005 0.021 Uiso 1 1 calc R
N8A N -0.3827(3) 1.0061(2) 0.35175(19) 0.0124(7) Uani 1 1 d .
H8AN H -0.4143 1.0339 0.3038 0.015 Uiso 1 1 calc R
N8B N -0.5430(3) 1.1333(2) -0.27191(19) 0.0169(7) Uani 1 1 d .
H8BN H -0.5245 1.1113 -0.2212 0.020 Uiso 1 1 calc R
C1A C -0.0343(3) 0.8022(3) 0.5913(2) 0.0122(8) Uani 1 1 d .
H1A H -0.0099 0.7781 0.6453 0.018 Uiso 1 1 calc R
C1B C -0.4674(3) 1.2104(3) -0.5935(2) 0.0148(8) Uani 1 1 d .
H1B H -0.4930 1.2395 -0.6474 0.022 Uiso 1 1 calc R
C2A C 0.0280(3) 0.7933(3) 0.5374(2) 0.0127(8) Uani 1 1 d .
H2A H 0.0954 0.7620 0.5545 0.019 Uiso 1 1 calc R
C2B C -0.3686(4) 1.1679(3) -0.5689(2) 0.0184(9) Uani 1 1 d .
H2B H -0.3267 1.1687 -0.6057 0.028 Uiso 1 1 calc R
C3A C -0.1332(3) 0.8471(3) 0.5653(2) 0.0138(8) Uani 1 1 d .
H3A H -0.1768 0.8522 0.6012 0.021 Uiso 1 1 calc R
C3B C -0.5288(3) 1.2103(3) -0.5391(2) 0.0159(9) Uani 1 1 d .
H3B H -0.5961 1.2397 -0.5553 0.024 Uiso 1 1 calc R
C4A C -0.0088(3) 0.8304(3) 0.4587(2) 0.0109(8) Uani 1 1 d .
C4B C -0.3325(3) 1.1243(3) -0.4897(2) 0.0107(8) Uani 1 1 d .
C5A C -0.1667(3) 0.8844(3) 0.4852(2) 0.0100(7) Uani 1 1 d .
C5B C -0.4893(3) 1.1664(3) -0.4606(2) 0.0123(8) Uani 1 1 d .
C6A C 0.0453(3) 0.8211(3) 0.3953(2) 0.0091(7) Uani 1 1 d .
C6B C -0.2321(3) 1.0778(3) -0.4519(2) 0.0122(8) Uani 1 1 d .
C7A C -0.2689(3) 0.9332(2) 0.4487(2) 0.0110(8) Uani 1 1 d .
C8A C 0.1454(3) 0.7667(2) 0.3970(2) 0.0117(8) Uani 1 1 d .
H8A H 0.1949 0.7292 0.4410 0.018 Uiso 1 1 calc R
C8B C -0.1467(4) 1.0614(3) -0.4790(3) 0.0203(9) Uani 1 1 d .
H8B H -0.1368 1.0788 -0.5313 0.030 Uiso 1 1 calc R
C9A C -0.3508(3) 0.9510(3) 0.4809(2) 0.0135(8) Uani 1 1 d .
H9A H -0.3564 0.9354 0.5344 0.020 Uiso 1 1 calc R
C9B C -0.6375(3) 1.2062(3) -0.3873(3) 0.0186(9) Uani 1 1 d .
H9B H -0.6917 1.2405 -0.4276 0.028 Uiso 1 1 calc R
C10A C 0.1532(3) 0.7815(3) 0.3196(2) 0.0150(8) Uani 1 1 d .
H10A H 0.2110 0.7556 0.2997 0.023 Uiso 1 1 calc R
C10B C -0.0778(3) 1.0128(3) -0.4108(3) 0.0189(9) Uani 1 1 d .
H10B H -0.0106 0.9905 -0.4082 0.028 Uiso 1 1 calc R
C11A C -0.4238(3) 0.9976(3) 0.4165(2) 0.0132(8) Uani 1 1 d .
H11A H -0.4904 1.0193 0.4178 0.020 Uiso 1 1 calc R
C11B C -0.6357(3) 1.1838(3) -0.3080(2) 0.0200(9) Uani 1 1 d .
H11B H -0.6903 1.2011 -0.2829 0.030 Uiso 1 1 calc R
C12A C -0.2022(3) 1.0374(3) 0.1323(2) 0.0192(8) Uani 1 1 d .
H12A H -0.1887 1.0789 0.1472 0.029 Uiso 1 1 calc R
C12B C -0.2424(3) 1.0644(3) -0.1867(2) 0.0212(8) Uani 1 1 d .
H12B H -0.2186 1.0977 -0.2239 0.032 Uiso 1 1 calc R
C13A C -0.2282(3) 0.9127(3) 0.1644(2) 0.0200(8) Uani 1 1 d .
H13A H -0.2316 0.8634 0.2027 0.030 Uiso 1 1 calc R
C13B C -0.3198(3) 0.9775(3) -0.1574(2) 0.0172(8) Uani 1 1 d .
H13B H -0.3511 0.9486 -0.1733 0.026 Uiso 1 1 calc R
C14A C -0.2177(3) 1.0512(3) 0.0540(2) 0.0189(8) Uani 1 1 d .
H14A H -0.2131 1.1004 0.0166 0.028 Uiso 1 1 calc R
C14B C -0.2229(3) 1.0535(3) -0.1103(2) 0.0204(8) Uani 1 1 d .
H14B H -0.1875 1.0797 -0.0959 0.031 Uiso 1 1 calc R
C15A C -0.2468(3) 0.9235(3) 0.0876(2) 0.0238(9) Uani 1 1 d .
H15A H -0.2642 0.8835 0.0741 0.036 Uiso 1 1 calc R
C15B C -0.3034(3) 0.9633(3) -0.0783(2) 0.0172(8) Uani 1 1 d .
H15B H -0.3245 0.9265 -0.0419 0.026 Uiso 1 1 calc R
C16A C -0.2400(3) 0.9936(2) 0.0297(2) 0.0155(8) Uani 1 1 d .
C16B C -0.2562(3) 1.0031(3) -0.0531(2) 0.0164(8) Uani 1 1 d .
C17A C -0.1741(3) 1.1294(3) 0.2989(2) 0.0154(8) Uani 1 1 d .
C17B C -0.3841(3) 1.2739(3) -0.3708(2) 0.0119(8) Uani 1 1 d .
C18A C -0.1197(3) 0.7209(3) 0.3710(2) 0.0133(8) Uani 1 1 d .
C18B C -0.3299(3) 0.8806(3) -0.3058(2) 0.0188(9) Uani 1 1 d .
Fe3 Fe 0.27456(4) 0.56999(4) -0.82947(4) 0.01190(13) Uani 1 1 d .
Fe4 Fe 0.23294(4) 0.43556(4) -0.19141(4) 0.01123(13) Uani 1 1 d .
S1C S 0.54336(9) 0.27645(9) -0.80023(6) 0.0227(3) Uani 1 1 d .
S1D S 0.46305(8) 0.10975(7) -0.08238(6) 0.0148(2) Uani 1 1 d .
S2C S 0.02728(8) 0.88190(7) -0.91267(6) 0.0145(2) Uani 1 1 d .
S2D S -0.05497(9) 0.71369(8) -0.20010(6) 0.0195(2) Uani 1 1 d .
N1C N 0.2723(3) 0.6242(2) -0.94176(19) 0.0113(7) Uani 1 1 d .
N1D N 0.2311(3) 0.3806(2) -0.06927(18) 0.0116(7) Uani 1 1 d .
N2C N 0.1830(3) 0.5390(2) -0.8770(2) 0.0187(8) Uani 1 1 d .
N2D N 0.1345(3) 0.3768(2) -0.18311(18) 0.0123(7) Uani 1 1 d .
N3C N 0.3601(3) 0.6290(2) -0.82884(18) 0.0124(7) Uani 1 1 d .
N3D N 0.3314(3) 0.4629(2) -0.13195(19) 0.0135(7) Uani 1 1 d .
N4C N 0.2722(2) 0.5258(2) -0.7139(2) 0.0179(7) Uani 1 1 d .
N4D N 0.2455(2) 0.4673(2) -0.31462(17) 0.0152(7) Uani 1 1 d .
N5C N 0.3850(3) 0.4491(2) -0.81784(18) 0.0168(7) Uani 1 1 d .
N5D N 0.3447(3) 0.2973(3) -0.1688(2) 0.0186(8) Uani 1 1 d .
N6C N 0.1646(3) 0.6947(2) -0.84373(19) 0.0141(7) Uani 1 1 d .
N6D N 0.1167(2) 0.5673(2) -0.21040(18) 0.0142(7) Uani 1 1 d .
N7C N 0.1281(3) 0.4975(3) -0.8546(2) 0.0250(9) Uani 1 1 d .
H7CN H 0.1268 0.4697 -0.8059 0.030 Uiso 1 1 calc R
N7D N 0.0874(3) 0.3562(2) -0.2283(2) 0.0164(7) Uani 1 1 d .
H7DN H 0.0808 0.3755 -0.2794 0.020 Uiso 1 1 calc R
N8C N 0.4016(3) 0.6488(3) -0.7784(2) 0.0187(8) Uani 1 1 d .
H8CN H 0.4065 0.6267 -0.7276 0.022 Uiso 1 1 calc R
N8D N 0.3915(3) 0.4999(2) -0.1476(2) 0.0131(7) Uani 1 1 d .
H8DN H 0.3961 0.5286 -0.1949 0.016 Uiso 1 1 calc R
C1C C 0.2667(3) 0.7023(3) -1.0987(2) 0.0162(9) Uani 1 1 d .
H1C H 0.2674 0.7268 -1.1526 0.019 Uiso 1 1 calc R
C1D C 0.2453(3) 0.2941(3) 0.0873(2) 0.0153(9) Uani 1 1 d .
H1D H 0.2488 0.2653 0.1413 0.023 Uiso 1 1 calc R
C2C C 0.2114(3) 0.6587(3) -1.0741(2) 0.0122(8) Uani 1 1 d .
H2C H 0.1713 0.6561 -1.1106 0.018 Uiso 1 1 calc R
C2D C 0.1846(3) 0.2931(3) 0.0337(2) 0.0130(8) Uani 1 1 d .
H2D H 0.1466 0.2637 0.0500 0.020 Uiso 1 1 calc R
C3C C 0.3209(3) 0.7100(3) -1.0443(2) 0.0123(8) Uani 1 1 d .
H3C H 0.3570 0.7415 -1.0602 0.018 Uiso 1 1 calc R
C3D C 0.3011(3) 0.3367(3) 0.0629(2) 0.0116(8) Uani 1 1 d .
H3D H 0.3445 0.3359 0.0992 0.017 Uiso 1 1 calc R
C4C C 0.2166(3) 0.6195(3) -0.9953(2) 0.0106(8) Uani 1 1 d .
C4D C 0.1813(3) 0.3366(3) -0.0446(2) 0.0118(8) Uani 1 1 d .
C5C C 0.3205(3) 0.6702(3) -0.9658(2) 0.0116(8) Uani 1 1 d .
C5D C 0.2910(3) 0.3803(3) -0.0162(2) 0.0138(8) Uani 1 1 d .
C6C C 0.1645(3) 0.5723(3) -0.9558(2) 0.0135(8) Uani 1 1 d .
C6D C 0.1264(3) 0.3341(3) -0.1092(2) 0.0152(9) Uani 1 1 d .
C7C C 0.3689(3) 0.6763(3) -0.9003(2) 0.0149(8) Uani 1 1 d .
C7D C 0.3459(3) 0.4263(3) -0.0529(2) 0.0135(8) Uani 1 1 d .
C8C C 0.0947(3) 0.5518(3) -0.9814(3) 0.0198(9) Uani 1 1 d .
H8C H 0.0671 0.5679 -1.0334 0.030 Uiso 1 1 calc R
C8D C 0.0740(3) 0.2894(3) -0.1103(2) 0.0171(8) Uani 1 1 d .
H8D H 0.0570 0.2561 -0.0669 0.026 Uiso 1 1 calc R
C9C C 0.4171(3) 0.7236(3) -0.8933(3) 0.0210(9) Uani 1 1 d .
H9C H 0.4344 0.7601 -0.9341 0.031 Uiso 1 1 calc R
C9D C 0.4173(3) 0.4407(3) -0.0212(2) 0.0104(8) Uani 1 1 d .
H9D H 0.4421 0.4213 0.0322 0.016 Uiso 1 1 calc R
C10C C 0.0767(4) 0.5041(3) -0.9150(3) 0.0278(11) Uani 1 1 d .
H10C H 0.0340 0.4793 -0.9125 0.042 Uiso 1 1 calc R
C10D C 0.0515(3) 0.3029(3) -0.1869(2) 0.0192(9) Uani 1 1 d .
H10D H 0.0172 0.2791 -0.2070 0.029 Uiso 1 1 calc R
C11C C 0.4346(3) 0.7065(3) -0.8154(3) 0.0220(10) Uani 1 1 d .
H11C H 0.4648 0.7311 -0.7917 0.033 Uiso 1 1 calc R
C11D C 0.4427(3) 0.4882(3) -0.0836(2) 0.0148(8) Uani 1 1 d .
H11D H 0.4882 0.5090 -0.0817 0.022 Uiso 1 1 calc R
C12C C 0.1877(3) 0.5562(3) -0.6885(2) 0.0191(8) Uani 1 1 d .
H12C H 0.1305 0.5883 -0.7256 0.029 Uiso 1 1 calc R
C12D C 0.1735(3) 0.5352(2) -0.3722(2) 0.0140(7) Uani 1 1 d .
H12D H 0.1174 0.5766 -0.3583 0.021 Uiso 1 1 calc R
C13C C 0.3525(3) 0.4768(2) -0.6597(2) 0.0181(8) Uani 1 1 d .
H13C H 0.4130 0.4526 -0.6762 0.027 Uiso 1 1 calc R
C13D C 0.3244(3) 0.4098(2) -0.3370(2) 0.0184(8) Uani 1 1 d .
H13D H 0.3768 0.3615 -0.2979 0.028 Uiso 1 1 calc R
C14C C 0.1795(2) 0.5433(2) -0.6111(2) 0.0155(7) Uani 1 1 d .
H14C H 0.1180 0.5660 -0.5960 0.023 Uiso 1 1 calc R
C14D C 0.1763(3) 0.5483(2) -0.4504(2) 0.0137(7) Uani 1 1 d .
H14D H 0.1237 0.5980 -0.4886 0.021 Uiso 1 1 calc R
C15C C 0.3506(3) 0.4605(2) -0.5818(2) 0.0154(8) Uani 1 1 d .
H15C H 0.4088 0.4250 -0.5457 0.023 Uiso 1 1 calc R
C15D C 0.3322(3) 0.4182(2) -0.4137(2) 0.0164(7) Uani 1 1 d .
H15D H 0.3890 0.3760 -0.4261 0.025 Uiso 1 1 calc R
C16C C 0.2622(3) 0.4965(3) -0.5553(2) 0.0150(8) Uani 1 1 d .
C16D C 0.2573(3) 0.4879(2) -0.4726(2) 0.0129(7) Uani 1 1 d .
C17C C 0.4498(4) 0.3780(3) -0.8101(2) 0.0193(9) Uani 1 1 d .
C17D C 0.3934(3) 0.2195(3) -0.1326(2) 0.0111(8) Uani 1 1 d .
C18C C 0.1084(3) 0.7724(3) -0.8725(2) 0.0135(8) Uani 1 1 d .
C18D C 0.0464(3) 0.6291(3) -0.2064(2) 0.0143(8) Uani 1 1 d .
O1M O 0.5036(2) 0.09626(17) -0.79761(14) 0.0207(6) Uani 1 1 d .
H1O H 0.4785 0.1481 -0.7924 0.031 Uiso 1 1 calc R
C1M C 0.5267(3) 0.1054(3) -0.8741(2) 0.0250(9) Uani 1 1 d .
H13M H 0.5710 0.1309 -0.8823 0.038 Uiso 1 1 calc R
H11M H 0.4678 0.1469 -0.9125 0.038 Uiso 1 1 calc R
H12M H 0.5569 0.0447 -0.8799 0.038 Uiso 1 1 calc R
O2M O -0.0393(3) 0.8940(2) -0.19921(17) 0.0460(11) Uani 1 1 d .
H2O H -0.0113 0.8423 -0.2046 0.069 Uiso 1 1 calc R
C2M C 0.0028(4) 0.8893(3) -0.1321(3) 0.0518(17) Uani 1 1 d .
H22M H -0.0268 0.8687 -0.0888 0.078 Uiso 1 1 calc R
H23M H -0.0061 0.9504 -0.1369 0.078 Uiso 1 1 calc R
H21M H 0.0715 0.8455 -0.1223 0.078 Uiso 1 1 calc R
O3M O 0.3999(2) 0.60256(19) -0.29974(15) 0.0224(6) Uani 1 1 d .
H3O H 0.3553 0.6070 -0.2739 0.034 Uiso 1 1 calc R
C3M C 0.3730(3) 0.6047(3) -0.3742(2) 0.0187(8) Uani 1 1 d .
H33M H 0.3832 0.6507 -0.4142 0.028 Uiso 1 1 calc R
H31M H 0.3051 0.6209 -0.3816 0.028 Uiso 1 1 calc R
H32M H 0.4122 0.5438 -0.3784 0.028 Uiso 1 1 calc R
O4M O -0.1579(2) 0.60496(17) -0.30017(15) 0.0218(6) Uani 1 1 d .
H4O H -0.1979 0.6588 -0.3034 0.033 Uiso 1 1 calc R
C4M C -0.0982(3) 0.6087(2) -0.3574(2) 0.0193(8) Uani 1 1 d .
H43M H -0.0563 0.6313 -0.3438 0.029 Uiso 1 1 calc R
H41M H -0.1382 0.6504 -0.4082 0.029 Uiso 1 1 calc R
H42M H -0.0589 0.5468 -0.3596 0.029 Uiso 1 1 calc R
C7B C -0.5381(3) 1.1651(2) -0.3942(2) 0.0101(8) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N5A Fe1 N1A 95.25(13)
N5A Fe1 N6A 178.03(15)
N1A Fe1 N6A 83.10(12)
N5A Fe1 N4A 92.27(13)
N1A Fe1 N4A 171.51(13)
N6A Fe1 N4A 89.30(12)
N5A Fe1 N3A 91.95(13)
N1A Fe1 N3A 74.05(13)
N6A Fe1 N3A 88.63(13)
N4A Fe1 N3A 109.68(13)
N5A Fe1 N2A 93.09(13)
N1A Fe1 N2A 74.11(13)
N6A Fe1 N2A 85.43(13)
N4A Fe1 N2A 101.60(12)
N3A Fe1 N2A 148.08(12)
N6B Fe2 N1B 94.27(14)
N6B Fe2 N4B 91.61(14)
N1B Fe2 N4B 173.57(14)
N6B Fe2 N5B 178.01(17)
N1B Fe2 N5B 84.83(14)
N4B Fe2 N5B 89.22(14)
N6B Fe2 N2B 92.02(15)
N1B Fe2 N2B 78.37(14)
N4B Fe2 N2B 104.06(14)
N5B Fe2 N2B 89.54(14)
N6B Fe2 N3B 91.08(15)
N1B Fe2 N3B 78.37(14)
N4B Fe2 N3B 98.93(13)
N5B Fe2 N3B 87.01(14)
N2B Fe2 N3B 156.70(14)
C5A N1A C4A 121.5(3)
C5A N1A Fe1 119.4(3)
C4A N1A Fe1 118.8(3)
C4B N1B C5B 122.1(3)
C4B N1B Fe2 118.8(3)
C5B N1B Fe2 118.5(3)
C6A N2A N7A 105.8(3)
C6A N2A Fe1 114.9(3)
N7A N2A Fe1 138.4(3)
N7B N2B C6B 106.1(4)
N7B N2B Fe2 137.7(3)
C6B N2B Fe2 116.0(3)
N8A N3A C7A 105.7(3)
N8A N3A Fe1 138.2(2)
C7A N3A Fe1 115.8(3)
C7B N3B N8B 106.4(4)
C7B N3B Fe2 115.1(3)
N8B N3B Fe2 138.1(3)
C12A N4A C13A 116.1(3)
C12A N4A Fe1 123.4(3)
C13A N4A Fe1 120.2(3)
C12B N4B C13B 116.4(3)
C12B N4B Fe2 121.3(3)
C13B N4B Fe2 121.9(3)
C17A N5A Fe1 167.4(3)
C17B N5B Fe2 158.2(3)
C18A N6A Fe1 154.3(3)
C18B N6B Fe2 170.3(4)
N2A N7A C10A 111.2(3)
N2A N7A H7AN 124.4
C10A N7A H7AN 124.4
N2B N7B C10B 110.6(3)
N2B N7B H7BN 124.7
C10B N7B H7BN 124.7
N3A N8A C11A 110.5(3)
N3A N8A H8AN 124.7
C11A N8A H8AN 124.7
N3B N8B C11B 110.6(3)
N3B N8B H8BN 124.7
C11B N8B H8BN 124.7
C2A C1A C3A 119.4(4)
C2A C1A H1A 120.3
C3A C1A H1A 120.3
C3B C1B C2B 120.2(4)
C3B C1B H1B 119.9
C2B C1B H1B 119.9
C4A C2A C1A 119.6(4)
C4A C2A H2A 120.2
C1A C2A H2A 120.2
C4B C2B C1B 119.0(4)
C4B C2B H2B 120.5
C1B C2B H2B 120.5
C1A C3A C5A 118.7(4)
C1A C3A H3A 120.7
C5A C3A H3A 120.7
C5B C3B C1B 118.6(4)
C5B C3B H3B 120.7
C1B C3B H3B 120.7
N1A C4A C2A 119.7(4)
N1A C4A C6A 113.4(3)
C2A C4A C6A 126.9(4)
N1B C4B C2B 120.1(4)
N1B C4B C6B 112.3(3)
C2B C4B C6B 127.6(4)
N1A C5A C3A 120.9(4)
N1A C5A C7A 114.0(3)
C3A C5A C7A 125.1(4)
N1B C5B C3B 119.8(4)
N1B C5B C7B 111.5(3)
C3B C5B C7B 128.5(4)
N2A C6A C8A 111.1(3)
N2A C6A C4A 118.6(4)
C8A C6A C4A 130.1(4)
N2B C6B C8B 111.9(4)
N2B C6B C4B 114.2(4)
C8B C6B C4B 133.9(4)
N3A C7A C9A 112.3(4)
N3A C7A C5A 116.5(4)
C9A C7A C5A 131.1(3)
C10A C8A C6A 103.6(3)
C10A C8A H8A 128.2
C6A C8A H8A 128.2
C6B C8B C10B 103.7(4)
C6B C8B H8B 128.2
C10B C8B H8B 128.2
C7A C9A C11A 103.7(3)
C7A C9A H9A 128.2
C11A C9A H9A 128.2
C11B C9B C7B 103.3(4)
C11B C9B H9B 128.3
C7B C9B H9B 128.3
N7A C10A C8A 108.3(3)
N7A C10A H10A 125.9
C8A C10A H10A 125.9
N7B C10B C8B 107.8(4)
N7B C10B H10B 126.1
C8B C10B H10B 126.1
N8A C11A C9A 107.7(4)
N8A C11A H11A 126.1
C9A C11A H11A 126.1
N8B C11B C9B 108.7(4)
N8B C11B H11B 125.6
C9B C11B H11B 125.6
N4A C12A C14A 123.1(4)
N4A C12A H12A 118.5
C14A C12A H12A 118.5
N4B C12B C14B 124.3(4)
N4B C12B H12B 117.9
C14B C12B H12B 117.9
N4A C13A C15A 124.1(3)
N4A C13A H13A 118.0
C15A C13A H13A 118.0
N4B C13B C15B 122.9(4)
N4B C13B H13B 118.6
C15B C13B H13B 118.6
C12A C14A C16A 120.4(4)
C12A C14A H14A 119.8
C16A C14A H14A 119.8
C12B C14B C16B 119.4(4)
C12B C14B H14B 120.3
C16B C14B H14B 120.3
C13A C15A C16A 119.6(4)
C13A C15A H15A 120.2
C16A C15A H15A 120.2
C16B C15B C13B 119.9(4)
C16B C15B H15B 120.0
C13B C15B H15B 120.0
C14A C16A C15A 116.8(4)
C14A C16A C16B 123.6(4)
C15A C16A C16B 119.7(4)
C15B C16B C14B 116.8(3)
C15B C16B C16A 122.4(4)
C14B C16B C16A 120.7(4)
N5A C17A S1A 179.0(4)
N5B C17B S1B 177.5(4)
N6A C18A S2A 177.0(4)
N6B C18B S2B 177.7(4)
N5C Fe3 N1C 94.35(13)
N5C Fe3 N6C 178.08(15)
N1C Fe3 N6C 84.14(14)
N5C Fe3 N4C 90.04(13)
N1C Fe3 N4C 174.94(13)
N6C Fe3 N4C 91.42(13)
N5C Fe3 N2C 91.57(14)
N1C Fe3 N2C 78.36(15)
N6C Fe3 N2C 89.29(14)
N4C Fe3 N2C 104.07(14)
N5C Fe3 N3C 92.72(14)
N1C Fe3 N3C 78.39(14)
N6C Fe3 N3C 85.83(14)
N4C Fe3 N3C 98.91(13)
N2C Fe3 N3C 156.61(14)
N6D Fe4 N5D 175.86(14)
N6D Fe4 N1D 95.76(12)
N5D Fe4 N1D 81.94(13)
N6D Fe4 N4D 92.86(12)
N5D Fe4 N4D 89.19(13)
N1D Fe4 N4D 170.34(12)
N6D Fe4 N3D 92.80(13)
N5D Fe4 N3D 89.91(13)
N1D Fe4 N3D 74.60(13)
N4D Fe4 N3D 109.37(13)
N6D Fe4 N2D 90.76(13)
N5D Fe4 N2D 85.30(14)
N1D Fe4 N2D 74.03(13)
N4D Fe4 N2D 101.56(12)
N3D Fe4 N2D 148.63(12)
C5C N1C C4C 119.4(3)
C5C N1C Fe3 120.1(3)
C4C N1C Fe3 120.4(3)
C4D N1D C5D 118.9(3)
C4D N1D Fe4 120.8(3)
C5D N1D Fe4 119.7(3)
C6C N2C N7C 105.5(4)
C6C N2C Fe3 114.5(3)
N7C N2C Fe3 139.9(3)
N7D N2D C6D 104.1(3)
N7D N2D Fe4 139.6(3)
C6D N2D Fe4 115.4(3)
N8C N3C C7C 104.9(4)
N8C N3C Fe3 139.0(3)
C7C N3C Fe3 115.1(3)
C7D N3D N8D 104.7(4)
C7D N3D Fe4 114.2(3)
N8D N3D Fe4 140.9(3)
C12C N4C C13C 117.2(3)
C12C N4C Fe3 119.2(3)
C13C N4C Fe3 122.9(3)
C12D N4D C13D 116.1(3)
C12D N4D Fe4 123.5(3)
C13D N4D Fe4 119.8(2)
C17C N5C Fe3 179.2(3)
C17D N5D Fe4 156.3(3)
C18C N6C Fe3 160.6(3)
C18D N6D Fe4 164.3(3)
C10C N7C N2C 111.6(4)
C10C N7C H7CN 124.2
N2C N7C H7CN 124.2
N2D N7D C10D 112.5(3)
N2D N7D H7DN 123.7
C10D N7D H7DN 123.7
C11C N8C N3C 111.5(3)
C11C N8C H8CN 124.2
N3C N8C H8CN 124.2
C11D N8D N3D 113.0(3)
C11D N8D H8DN 123.5
N3D N8D H8DN 123.5
C3C C1C C2C 120.0(4)
C3C C1C H1C 120.0
C2C C1C H1C 120.0
C2D C1D C3D 120.7(4)
C2D C1D H1D 119.6
C3D C1D H1D 119.6
C4C C2C C1C 118.2(4)
C4C C2C H2C 120.9
C1C C2C H2C 120.9
C1D C2D C4D 117.6(4)
C1D C2D H2D 121.2
C4D C2D H2D 121.2
C5C C3C C1C 118.0(4)
C5C C3C H3C 121.0
C1C C3C H3C 121.0
C5D C3D C1D 117.4(4)
C5D C3D H3D 121.3
C1D C3D H3D 121.3
N1C C4C C2C 121.8(4)
N1C C4C C6C 109.9(3)
C2C C4C C6C 128.2(4)
N1D C4D C2D 122.9(4)
N1D C4D C6D 113.2(3)
C2D C4D C6D 123.8(4)
N1C C5C C3C 122.3(4)
N1C C5C C7C 112.1(3)
C3C C5C C7C 125.5(4)
N1D C5D C3D 122.4(4)
N1D C5D C7D 112.3(3)
C3D C5D C7D 125.2(4)
N2C C6C C8C 108.9(4)
N2C C6C C4C 116.7(4)
C8C C6C C4C 134.4(4)
N2D C6D C8D 110.6(4)
N2D C6D C4D 116.4(4)
C8D C6D C4D 132.7(4)
N3C C7C C9C 110.4(4)
N3C C7C C5C 114.1(4)
C9C C7C C5C 135.4(4)
N3D C7D C9D 109.2(4)
N3D C7D C5D 118.8(4)
C9D C7D C5D 132.0(4)
C10C C8C C6C 104.8(4)
C10C C8C H8C 127.6
C6C C8C H8C 127.6
C10D C8D C6D 105.9(4)
C10D C8D H8D 127.0
C6D C8D H8D 127.0
C11C C9C C7C 105.4(4)
C11C C9C H9C 127.3
C7C C9C H9C 127.3
C11D C9D C7D 105.8(4)
C11D C9D H9D 127.1
C7D C9D H9D 127.1
N7C C10C C8C 109.2(5)
N7C C10C H10C 125.4
C8C C10C H10C 125.4
N7D C10D C8D 106.7(4)
N7D C10D H10D 126.6
C8D C10D H10D 126.6
N8C C11C C9C 107.8(4)
N8C C11C H11C 126.1
C9C C11C H11C 126.1
N8D C11D C9D 107.3(4)
N8D C11D H11D 126.3
C9D C11D H11D 126.3
N4C C12C C14C 123.4(4)
N4C C12C H12C 118.3
C14C C12C H12C 118.3
N4D C12D C14D 123.9(3)
N4D C12D H12D 118.1
C14D C12D H12D 118.1
N4C C13C C15C 122.9(3)
N4C C13C H13C 118.5
C15C C13C H13C 118.5
N4D C13D C15D 123.3(3)
N4D C13D H13D 118.4
C15D C13D H13D 118.4
C12C C14C C16C 119.5(3)
C12C C14C H14C 120.2
C16C C14C H14C 120.2
C12D C14D C16D 119.4(3)
C12D C14D H14D 120.3
C16D C14D H14D 120.3
C13C C15C C16C 120.0(4)
C13C C15C H15C 120.0
C16C C15C H15C 120.0
C13D C15D C16D 120.2(3)
C13D C15D H15D 119.9
C16D C15D H15D 119.9
C14C C16C C15C 116.8(3)
C14C C16C C16D 121.5(3)
C15C C16C C16D 121.7(4)
C15D C16D C14D 117.1(3)
C15D C16D C16C 121.4(3)
C14D C16D C16C 121.5(3)
N5C C17C S1C 179.1(4)
N5D C17D S1D 179.2(4)
N6C C18C S2C 179.0(4)
N6D C18D S2D 177.6(4)
C1M O1M H1O 109.5
O1M C1M H13M 109.5
O1M C1M H11M 109.5
H13M C1M H11M 109.5
O1M C1M H12M 109.5
H13M C1M H12M 109.5
H11M C1M H12M 109.5
C2M O2M H2O 109.5
O2M C2M H22M 109.5
O2M C2M H23M 109.5
H22M C2M H23M 109.5
O2M C2M H21M 109.5
H22M C2M H21M 109.5
H23M C2M H21M 109.5
C3M O3M H3O 109.5
O3M C3M H33M 109.5
O3M C3M H31M 109.5
H33M C3M H31M 109.5
O3M C3M H32M 109.5
H33M C3M H32M 109.5
H31M C3M H32M 109.5
C4M O4M H4O 109.5
O4M C4M H43M 109.5
O4M C4M H41M 109.5
H43M C4M H41M 109.5
O4M C4M H42M 109.5
H43M C4M H42M 109.5
H41M C4M H42M 109.5
N3B C7B C9B 111.0(4)
N3B C7B C5B 116.5(4)
C9B C7B C5B 132.4(4)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Fe1 N5A 2.105(4)
Fe1 N1A 2.151(3)
Fe1 N6A 2.157(3)
Fe1 N4A 2.185(3)
Fe1 N3A 2.199(4)
Fe1 N2A 2.220(4)
Fe2 N6B 1.972(4)
Fe2 N1B 1.980(3)
Fe2 N4B 2.005(3)
Fe2 N5B 2.006(3)
Fe2 N2B 2.015(4)
Fe2 N3B 2.042(4)
S1A C17A 1.635(5)
S1B C17B 1.651(4)
S2A C18A 1.652(4)
S2B C18B 1.651(5)
N1A C5A 1.328(5)
N1A C4A 1.370(6)
N1B C4B 1.335(5)
N1B C5B 1.369(6)
N2A C6A 1.331(5)
N2A N7A 1.351(5)
N2B N7B 1.342(5)
N2B C6B 1.346(5)
N3A N8A 1.339(5)
N3A C7A 1.339(5)
N3B C7B 1.330(5)
N3B N8B 1.353(5)
N4A C12A 1.350(5)
N4A C13A 1.351(5)
N4B C12B 1.347(5)
N4B C13B 1.356(5)
N5A C17A 1.166(6)
N5B C17B 1.159(5)
N6A C18A 1.165(5)
N6B C18B 1.163(6)
N7A C10A 1.352(5)
N7A H7AN 0.8800
N7B C10B 1.356(6)
N7B H7BN 0.8800
N8A C11A 1.356(5)
N8A H8AN 0.8800
N8B C11B 1.355(6)
N8B H8BN 0.8800
C1A C2A 1.391(6)
C1A C3A 1.399(6)
C1A H1A 0.9500
C1B C3B 1.395(6)
C1B C2B 1.395(7)
C1B H1B 0.9500
C2A C4A 1.388(5)
C2A H2A 0.9500
C2B C4B 1.392(5)
C2B H2B 0.9500
C3A C5A 1.399(5)
C3A H3A 0.9500
C3B C5B 1.390(5)
C3B H3B 0.9500
C4A C6A 1.450(5)
C4B C6B 1.468(6)
C5A C7A 1.480(6)
C5B C7B 1.445(6)
C6A C8A 1.426(6)
C6B C8B 1.379(7)
C7A C9A 1.372(6)
C8A C10A 1.380(5)
C8A H8A 0.9500
C8B C10B 1.407(6)
C8B H8B 0.9500
C9A C11A 1.397(6)
C9A H9A 0.9500
C9B C11B 1.382(6)
C9B C7B 1.429(6)
C9B H9B 0.9500
C10A H10A 0.9500
C10B H10B 0.9500
C11A H11A 0.9500
C11B H11B 0.9500
C12A C14A 1.385(6)
C12A H12A 0.9500
C12B C14B 1.371(6)
C12B H12B 0.9500
C13A C15A 1.376(5)
C13A H13A 0.9500
C13B C15B 1.397(5)
C13B H13B 0.9500
C14A C16A 1.388(5)
C14A H14A 0.9500
C14B C16B 1.416(5)
C14B H14B 0.9500
C15A C16A 1.396(5)
C15A H15A 0.9500
C15B C16B 1.388(5)
C15B H15B 0.9500
C16A C16B 1.486(5)
Fe3 N5C 1.973(4)
Fe3 N1C 1.976(3)
Fe3 N6C 2.003(4)
Fe3 N4C 2.027(3)
Fe3 N2C 2.043(4)
Fe3 N3C 2.045(4)
Fe4 N6D 2.102(3)
Fe4 N5D 2.141(4)
Fe4 N1D 2.154(3)
Fe4 N4D 2.187(3)
Fe4 N3D 2.205(4)
Fe4 N2D 2.209(4)
S1C C17C 1.662(5)
S1D C17D 1.643(4)
S2C C18C 1.649(4)
S2D C18D 1.646(4)
N1C C5C 1.329(6)
N1C C4C 1.367(5)
N1D C4D 1.325(6)
N1D C5D 1.359(5)
N2C C6C 1.357(5)
N2C N7C 1.359(6)
N2D N7D 1.342(5)
N2D C6D 1.368(5)
N3C N8C 1.347(5)
N3C C7C 1.361(5)
N3D C7D 1.363(5)
N3D N8D 1.363(5)
N4C C12C 1.344(5)
N4C C13C 1.352(5)
N4D C12D 1.347(5)
N4D C13D 1.359(5)
N5C C17C 1.156(6)
N5D C17D 1.166(5)
N6C C18C 1.165(5)
N6D C18D 1.166(5)
N7C C10C 1.320(7)
N7C H7CN 0.8800
N7D C10D 1.347(5)
N7D H7DN 0.8800
N8C C11C 1.343(6)
N8C H8CN 0.8800
N8D C11D 1.334(5)
N8D H8DN 0.8800
C1C C3C 1.394(6)
C1C C2C 1.396(6)
C1C H1C 0.9500
C1D C2D 1.387(6)
C1D C3D 1.390(6)
C1D H1D 0.9500
C2C C4C 1.378(5)
C2C H2C 0.9500
C2D C4D 1.390(5)
C2D H2D 0.9500
C3C C5C 1.392(5)
C3C H3C 0.9500
C3D C5D 1.385(5)
C3D H3D 0.9500
C4C C6C 1.462(6)
C4D C6D 1.496(6)
C5C C7C 1.484(6)
C5D C7D 1.469(6)
C6C C8C 1.429(6)
C6D C8D 1.377(6)
C7C C9C 1.386(7)
C7D C9D 1.427(6)
C8C C10C 1.359(7)
C8C H8C 0.9500
C8D C10D 1.371(6)
C8D H8D 0.9500
C9C C11C 1.368(6)
C9C H9C 0.9500
C9D C11D 1.370(6)
C9D H9D 0.9500
C10C H10C 0.9500
C10D H10D 0.9500
C11C H11C 0.9500
C11D H11D 0.9500
C12C C14C 1.383(5)
C12C H12C 0.9500
C12D C14D 1.386(5)
C12D H12D 0.9500
C13C C15C 1.371(5)
C13C H13C 0.9500
C13D C15D 1.380(5)
C13D H13D 0.9500
C14C C16C 1.395(5)
C14C H14C 0.9500
C14D C16D 1.397(5)
C14D H14D 0.9500
C15C C16C 1.408(5)
C15C H15C 0.9500
C15D C16D 1.388(5)
C15D H15D 0.9500
C16C C16D 1.484(4)
O1M C1M 1.429(4)
O1M H1O 0.8400
C1M H13M 0.9800
C1M H11M 0.9800
C1M H12M 0.9800
O2M C2M 1.363(6)
O2M H2O 0.8400
C2M H22M 0.9800
C2M H23M 0.9800
C2M H21M 0.9800
O3M C3M 1.416(4)
O3M H3O 0.8400
C3M H33M 0.9800
C3M H31M 0.9800
C3M H32M 0.9800
O4M C4M 1.422(4)
O4M H4O 0.8400
C4M H43M 0.9800
C4M H41M 0.9800
C4M H42M 0.9800
