#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:51:56 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179993 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/87/7028782.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7028782
loop_
_publ_author_name
'Funes, Alejandro V.'
'Carrella, Luca'
'Rentschler, Eva'
'Alborés, Pablo'
_publ_section_title
;
 {Co(III)2Dy(III)2} single molecule magnet with two resolved thermal
 activated magnetization relaxation pathways at zero field.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2361
_journal_page_last               2364
_journal_paper_doi               10.1039/c3dt52765d
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C44 H86 Co2 Dy2 N2 O20'
_chemical_formula_weight         1406.01
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                104.787(3)
_cell_angle_beta                 90.745(3)
_cell_angle_gamma                94.220(3)
_cell_formula_units_Z            1
_cell_length_a                   10.9410(4)
_cell_length_b                   11.2485(4)
_cell_length_c                   12.2043(5)
_cell_measurement_reflns_used    5475
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      28.7987
_cell_measurement_theta_min      3.7042
_cell_volume                     1447.51(10)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      298(2)
_diffrn_detector_area_resol_mean 16.1158
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Xcalibur, Eos, Gemini'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0550
_diffrn_reflns_av_sigmaI/netI    0.0594
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            18734
_diffrn_reflns_theta_full        27.00
_diffrn_reflns_theta_max         27.00
_diffrn_reflns_theta_min         3.71
_exptl_absorpt_coefficient_mu    3.183
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.54401
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.20 (release 27-06-2012 CrysAlis171 .NET)
(compiled Jul 11 2012,15:38:31)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.613
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             710
_exptl_crystal_size_max          0.51
_exptl_crystal_size_mid          0.4
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.399
_refine_diff_density_min         -1.029
_refine_diff_density_rms         0.135
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     314
_refine_ls_number_reflns         6252
_refine_ls_number_restraints     30
_refine_ls_restrained_S_all      1.092
_refine_ls_R_factor_all          0.0557
_refine_ls_R_factor_gt           0.0384
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0423P)²+1.4130P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0878
_refine_ls_wR_factor_ref         0.1011
_reflns_number_gt                5086
_reflns_number_total             6252
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt52765d.txt
_cod_data_source_block           exp_3
_cod_original_cell_volume        1447.50(9)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7028782
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C11 C 0.6029(5) 0.6566(5) 0.3508(4) 0.0325(12) Uani 1 1 d . A .
C12 C 0.7139(5) 1.1529(5) 0.7785(4) 0.0339(12) Uani 1 1 d . . .
C13 C 0.8235(5) 0.7953(5) 0.6299(4) 0.0337(12) Uani 1 1 d . A .
C14 C 0.6106(8) 1.0050(7) 0.1378(6) 0.068(2) Uani 1 1 d . . .
H14A H 0.6855 1.0433 0.1159 0.081 Uiso 1 1 calc R . .
H14B H 0.5534 0.9861 0.0731 0.081 Uiso 1 1 calc R . .
C15 C 0.3636(5) 0.7940(5) 0.4486(5) 0.0357(12) Uani 1 1 d . A .
H15A H 0.3312 0.8164 0.5232 0.054 Uiso 1 1 calc R . .
H15B H 0.4026 0.7184 0.4386 0.054 Uiso 1 1 calc R . .
H15C H 0.2981 0.7830 0.3930 0.054 Uiso 1 1 calc R . .
C21 C 0.6304(7) 0.5219(6) 0.3040(5) 0.0514(17) Uani 1 1 d . . .
C22 C 0.8126(5) 1.2332(6) 0.8596(5) 0.0499(16) Uani 1 1 d D . .
C23 C 0.9243(5) 0.7279(5) 0.6647(5) 0.0369(13) Uani 1 1 d . . .
C24 C 0.5616(11) 1.0890(8) 0.2256(8) 0.117(5) Uani 1 1 d . . .
H24A H 0.6269 1.1500 0.2617 0.141 Uiso 1 1 calc R . .
H24B H 0.5022 1.1315 0.1934 0.141 Uiso 1 1 calc R . .
C31 C 0.7604(11) 0.5305(10) 0.2546(11) 0.145(5) Uani 1 1 d . . .
H31A H 0.8186 0.5705 0.3146 0.218 Uiso 1 1 calc R . .
H31B H 0.7592 0.5773 0.1989 0.218 Uiso 1 1 calc R . .
H31C H 0.7834 0.4490 0.2197 0.218 Uiso 1 1 calc R . .
C41 C 0.5519(15) 0.4597(9) 0.2077(12) 0.200(9) Uani 1 1 d . . .
H41A H 0.5501 0.5099 0.1549 0.300 Uiso 1 1 calc R . .
H41B H 0.4704 0.4456 0.2325 0.300 Uiso 1 1 calc R . .
H41C H 0.5828 0.3821 0.1715 0.300 Uiso 1 1 calc R . .
C51 C 0.6460(12) 0.4584(8) 0.3942(8) 0.122(5) Uani 1 1 d . . .
H51A H 0.7002 0.5089 0.4530 0.182 Uiso 1 1 calc R . .
H51B H 0.6802 0.3811 0.3633 0.182 Uiso 1 1 calc R . .
H51C H 0.5677 0.4437 0.4250 0.182 Uiso 1 1 calc R . .
C32 C 0.7792(14) 1.3694(11) 0.8822(14) 0.101(3) Uani 0.516(8) 1 d PD A 1
H32A H 0.8397 1.4223 0.9332 0.152 Uiso 0.516(8) 1 calc PR A 1
H32B H 0.7002 1.3769 0.9155 0.152 Uiso 0.516(8) 1 calc PR A 1
H32C H 0.7771 1.3929 0.8120 0.152 Uiso 0.516(8) 1 calc PR A 1
C42 C 0.9369(10) 1.2244(16) 0.8068(12) 0.101(3) Uani 0.516(8) 1 d PD A 1
H42A H 0.9973 1.2759 0.8589 0.152 Uiso 0.516(8) 1 calc PR A 1
H42B H 0.9343 1.2511 0.7382 0.152 Uiso 0.516(8) 1 calc PR A 1
H42C H 0.9580 1.1404 0.7898 0.152 Uiso 0.516(8) 1 calc PR A 1
C52 C 0.8110(14) 1.1979(16) 0.9707(10) 0.101(3) Uani 0.516(8) 1 d PD A 1
H52A H 0.8726 1.2487 1.0219 0.152 Uiso 0.516(8) 1 calc PR A 1
H52B H 0.8274 1.1128 0.9579 0.152 Uiso 0.516(8) 1 calc PR A 1
H52C H 0.7318 1.2096 1.0029 0.152 Uiso 0.516(8) 1 calc PR A 1
C32' C 0.7648(14) 1.3156(15) 0.9657(11) 0.101(3) Uani 0.484(8) 1 d PD A 2
H32D H 0.8323 1.3630 1.0115 0.152 Uiso 0.484(8) 1 calc PR A 2
H32E H 0.7210 1.2658 1.0078 0.152 Uiso 0.484(8) 1 calc PR A 2
H32F H 0.7106 1.3703 0.9451 0.152 Uiso 0.484(8) 1 calc PR A 2
C42' C 0.8919(14) 1.3063(16) 0.7944(12) 0.101(3) Uani 0.484(8) 1 d PD A 2
H42D H 0.9539 1.3577 0.8447 0.152 Uiso 0.484(8) 1 calc PR A 2
H42E H 0.8418 1.3569 0.7632 0.152 Uiso 0.484(8) 1 calc PR A 2
H42F H 0.9302 1.2504 0.7341 0.152 Uiso 0.484(8) 1 calc PR A 2
C52' C 0.8939(14) 1.1412(13) 0.8959(15) 0.101(3) Uani 0.484(8) 1 d PD A 2
H52D H 0.9582 1.1863 0.9475 0.152 Uiso 0.484(8) 1 calc PR A 2
H52E H 0.9291 1.0909 0.8301 0.152 Uiso 0.484(8) 1 calc PR A 2
H52F H 0.8445 1.0896 0.9325 0.152 Uiso 0.484(8) 1 calc PR A 2
C33 C 0.8762(8) 0.6077(8) 0.6876(8) 0.087(3) Uani 1 1 d . . .
H33A H 0.9431 0.5675 0.7099 0.131 Uiso 1 1 calc R . .
H33B H 0.8361 0.5555 0.6201 0.131 Uiso 1 1 calc R . .
H33C H 0.8187 0.6237 0.7473 0.131 Uiso 1 1 calc R . .
C34 C 0.7669(6) 0.8885(8) 0.2034(5) 0.062(2) Uani 1 1 d . . .
H34A H 0.7913 0.8048 0.1809 0.074 Uiso 1 1 calc R . .
H34B H 0.8194 0.9380 0.1658 0.074 Uiso 1 1 calc R . .
C43 C 1.0190(7) 0.7005(9) 0.5687(7) 0.084(3) Uani 1 1 d . . .
H43A H 1.0837 0.6575 0.5910 0.125 Uiso 1 1 calc R . .
H43B H 1.0528 0.7768 0.5557 0.125 Uiso 1 1 calc R . .
H43C H 0.9788 0.6505 0.5003 0.125 Uiso 1 1 calc R . .
C44 C 0.7867(6) 0.9346(9) 0.3228(5) 0.074(3) Uani 1 1 d . A .
H44A H 0.8454 0.8859 0.3482 0.089 Uiso 1 1 calc R . .
H44B H 0.8229 1.0188 0.3386 0.089 Uiso 1 1 calc R . .
C53 C 0.9895(8) 0.8091(9) 0.7691(7) 0.084(3) Uani 1 1 d . . .
H53A H 1.0542 0.7666 0.7922 0.126 Uiso 1 1 calc R . .
H53B H 0.9325 0.8290 0.8289 0.126 Uiso 1 1 calc R . .
H53C H 1.0236 0.8837 0.7529 0.126 Uiso 1 1 calc R . .
C54 C 0.6102(7) 0.7825(7) 0.0626(5) 0.0582(19) Uani 1 1 d . . .
H54A H 0.5276 0.7877 0.0353 0.070 Uiso 1 1 calc R . .
H54B H 0.6098 0.7074 0.0878 0.070 Uiso 1 1 calc R . .
C64 C 0.6938(7) 0.7694(7) -0.0367(5) 0.0573(19) Uani 1 1 d . . .
H64A H 0.7769 0.7639 -0.0110 0.069 Uiso 1 1 calc R . .
H64B H 0.6689 0.6932 -0.0930 0.069 Uiso 1 1 calc R . .
N1 N 0.6386(4) 0.8885(4) 0.1631(3) 0.0318(10) Uani 1 1 d . . .
O11 O 0.5698(3) 0.7105(3) 0.2755(3) 0.0323(8) Uani 1 1 d . . .
O12 O 0.7465(3) 1.0676(4) 0.7015(3) 0.0387(9) Uani 1 1 d . . .
O13 O 0.7250(4) 0.8001(4) 0.6833(3) 0.0396(9) Uani 1 1 d . . .
O14 O 0.5064(3) 1.0447(3) 0.3068(3) 0.0277(8) Uani 1 1 d . . .
O15 O 0.4523(3) 0.8907(3) 0.4353(3) 0.0257(7) Uani 1 1 d . . .
O21 O 0.6133(4) 0.7046(3) 0.4542(3) 0.0374(9) Uani 1 1 d . . .
O22 O 0.3946(3) 0.8162(3) 0.2010(3) 0.0337(8) Uani 1 1 d . . .
O23 O 0.8383(4) 0.8476(4) 0.5514(3) 0.0406(9) Uani 1 1 d . . .
O24 O 0.6829(3) 0.9328(3) 0.3845(3) 0.0285(8) Uani 1 1 d . . .
O34 O 0.6923(8) 0.8635(7) -0.0851(5) 0.128(3) Uani 1 1 d . . .
H34 H 0.7390 0.8527 -0.1382 0.191 Uiso 1 1 calc R . .
Co2 Co 0.53788(6) 0.87899(6) 0.29568(5) 0.02390(15) Uani 1 1 d . . .
Dy1 Dy 0.63551(2) 0.91418(2) 0.559438(19) 0.02729(9) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O21 C11 O11 125.5(5) . .
O21 C11 C21 119.7(5) . .
O11 C11 C21 114.8(5) . .
O12 C12 O22 127.4(5) . 2_676
O12 C12 C22 118.2(5) . .
O22 C12 C22 114.4(5) 2_676 .
O23 C13 O13 121.3(5) . .
O23 C13 C23 120.4(5) . .
O13 C13 C23 118.4(5) . .
O23 C13 Dy1 59.1(3) . .
O13 C13 Dy1 62.2(3) . .
C23 C13 Dy1 178.2(4) . .
C24 C14 N1 115.1(5) . .
C41 C21 C51 117.5(9) . .
C41 C21 C11 112.2(6) . .
C51 C21 C11 112.4(6) . .
C41 C21 C31 104.6(10) . .
C51 C21 C31 104.5(8) . .
C11 C21 C31 103.9(6) . .
C52 C22 C42 112.6(6) . .
C52 C22 C32' 58.1(7) . .
C42 C22 C32' 133.7(10) . .
C52 C22 C42' 140.9(9) . .
C42 C22 C42' 43.3(7) . .
C32' C22 C42' 111.8(6) . .
C52 C22 C12 109.4(7) . .
C42 C22 C12 110.9(7) . .
C32' C22 C12 114.8(7) . .
C42' C22 C12 108.7(7) . .
C52 C22 C52' 53.1(7) . .
C42 C22 C52' 65.4(7) . .
C32' C22 C52' 108.0(6) . .
C42' C22 C52' 107.7(6) . .
C12 C22 C52' 105.3(7) . .
C52 C22 C32 108.2(6) . .
C42 C22 C32 108.2(6) . .
C32' C22 C32 50.8(7) . .
C42' C22 C32 67.9(7) . .
C12 C22 C32 107.5(7) . .
C52' C22 C32 146.4(9) . .
C13 C23 C53 108.8(6) . .
C13 C23 C33 111.9(5) . .
C53 C23 C33 109.8(6) . .
C13 C23 C43 109.5(5) . .
C53 C23 C43 107.9(6) . .
C33 C23 C43 108.8(6) . .
O14 C24 C14 117.2(7) . .
C44 C34 N1 114.5(5) . .
O24 C44 C34 114.5(5) . .
N1 C54 C64 117.8(6) . .
O34 C64 C54 112.9(7) . .
C14 N1 C34 113.6(6) . .
C14 N1 C54 110.7(5) . .
C34 N1 C54 109.7(5) . .
C14 N1 Co2 104.8(3) . .
C34 N1 Co2 104.7(3) . .
C54 N1 Co2 113.2(4) . .
C11 O11 Co2 128.3(3) . .
C12 O12 Dy1 132.4(4) . .
C13 O13 Dy1 90.7(3) . .
C24 O14 Co2 112.2(4) . .
C24 O14 Dy1 142.6(4) . 2_676
Co2 O14 Dy1 104.41(14) . 2_676
C15 O15 Co2 121.7(3) . .
C15 O15 Dy1 113.9(3) . 2_676
Co2 O15 Dy1 96.35(13) . 2_676
C15 O15 Dy1 112.9(3) . .
Co2 O15 Dy1 96.60(14) . .
Dy1 O15 Dy1 113.44(13) 2_676 .
C11 O21 Dy1 131.5(3) . .
C12 O22 Co2 126.3(3) 2_676 .
C13 O23 Dy1 94.1(3) . .
C44 O24 Co2 114.1(3) . .
C44 O24 Dy1 137.0(4) . .
Co2 O24 Dy1 105.03(16) . .
O24 Co2 O14 90.11(15) . .
O24 Co2 O11 91.48(15) . .
O14 Co2 O11 176.80(14) . .
O24 Co2 O22 176.81(16) . .
O14 Co2 O22 92.62(15) . .
O11 Co2 O22 85.72(16) . .
O24 Co2 O15 87.73(15) . .
O14 Co2 O15 88.05(14) . .
O11 Co2 O15 94.79(15) . .
O22 Co2 O15 94.01(15) . .
O24 Co2 N1 86.39(17) . .
O14 Co2 N1 86.83(16) . .
O11 Co2 N1 90.50(17) . .
O22 Co2 N1 92.11(17) . .
O15 Co2 N1 172.19(17) . .
O24 Co2 Dy1 97.44(11) . 2_676
O14 Co2 Dy1 41.66(10) . 2_676
O11 Co2 Dy1 140.71(11) . 2_676
O22 Co2 Dy1 85.70(11) . 2_676
O15 Co2 Dy1 47.79(10) . 2_676
N1 Co2 Dy1 128.08(13) . 2_676
O24 Co2 Dy1 41.51(10) . .
O14 Co2 Dy1 97.94(10) . .
O11 Co2 Dy1 85.08(10) . .
O22 Co2 Dy1 139.45(11) . .
O15 Co2 Dy1 47.73(10) . .
N1 Co2 Dy1 127.35(13) . .
Dy1 Co2 Dy1 77.05(3) 2_676 .
O14 Dy1 O24 143.14(12) 2_676 .
O14 Dy1 O12 79.33(13) 2_676 .
O24 Dy1 O12 111.16(13) . .
O14 Dy1 O21 111.47(13) 2_676 .
O24 Dy1 O21 79.23(13) . .
O12 Dy1 O21 147.38(13) . .
O14 Dy1 O23 135.51(12) 2_676 .
O24 Dy1 O23 80.87(12) . .
O12 Dy1 O23 76.23(13) . .
O21 Dy1 O23 75.13(14) . .
O14 Dy1 O15 68.78(11) 2_676 2_676
O24 Dy1 O15 80.42(11) . 2_676
O12 Dy1 O15 73.06(12) . 2_676
O21 Dy1 O15 139.43(12) . 2_676
O23 Dy1 O15 134.94(13) . 2_676
O14 Dy1 O15 81.08(12) 2_676 .
O24 Dy1 O15 68.06(12) . .
O12 Dy1 O15 139.22(12) . .
O21 Dy1 O15 73.34(12) . .
O23 Dy1 O15 138.99(12) . .
O15 Dy1 O15 66.56(13) 2_676 .
O14 Dy1 O13 84.41(12) 2_676 .
O24 Dy1 O13 132.05(12) . .
O12 Dy1 O13 75.60(14) . .
O21 Dy1 O13 75.06(13) . .
O23 Dy1 O13 53.81(13) . .
O15 Dy1 O13 141.74(12) 2_676 .
O15 Dy1 O13 137.19(12) . .
O14 Dy1 C13 110.62(14) 2_676 .
O24 Dy1 C13 106.24(14) . .
O12 Dy1 C13 75.04(15) . .
O21 Dy1 C13 72.36(15) . .
O23 Dy1 C13 26.75(14) . .
O15 Dy1 C13 147.59(14) 2_676 .
O15 Dy1 C13 145.68(14) . .
O13 Dy1 C13 27.08(14) . .
O14 Dy1 Co2 33.93(8) 2_676 2_676
O24 Dy1 Co2 115.73(9) . 2_676
O12 Dy1 Co2 67.07(9) . 2_676
O21 Dy1 Co2 137.93(10) . 2_676
O23 Dy1 Co2 143.05(10) . 2_676
O15 Dy1 Co2 35.85(8) 2_676 2_676
O15 Dy1 Co2 76.78(8) . 2_676
O13 Dy1 Co2 110.49(9) . 2_676
C13 Dy1 Co2 130.89(11) . 2_676
O14 Dy1 Co2 116.25(9) 2_676 .
O24 Dy1 Co2 33.45(9) . .
O12 Dy1 Co2 137.38(10) . .
O21 Dy1 Co2 67.11(9) . .
O23 Dy1 Co2 106.88(9) . .
O15 Dy1 Co2 76.63(8) 2_676 .
O15 Dy1 Co2 35.68(7) . .
O13 Dy1 Co2 141.33(9) . .
C13 Dy1 Co2 126.16(11) . .
Co2 Dy1 Co2 102.95(3) 2_676 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C11 O21 1.240(6) .
C11 O11 1.285(6) .
C11 C21 1.531(8) .
C12 O12 1.236(6) .
C12 O22 1.272(6) 2_676
C12 C22 1.528(8) .
C13 O23 1.253(6) .
C13 O13 1.263(6) .
C13 C23 1.499(7) .
C13 Dy1 2.775(5) .
C14 C24 1.379(10) .
C14 N1 1.473(8) .
C15 O15 1.446(6) .
C21 C41 1.440(12) .
C21 C51 1.470(10) .
C21 C31 1.558(12) .
C22 C52 1.507(9) .
C22 C42 1.511(9) .
C22 C32' 1.512(9) .
C22 C42' 1.519(9) .
C22 C52' 1.555(9) .
C22 C32 1.557(9) .
C23 C53 1.501(10) .
C23 C33 1.508(10) .
C23 C43 1.561(9) .
C24 O14 1.348(7) .
C34 C44 1.424(9) .
C34 N1 1.481(7) .
C44 O24 1.372(7) .
C54 N1 1.487(7) .
C54 C64 1.512(8) .
C64 O34 1.338(9) .
N1 Co2 1.990(4) .
O11 Co2 1.907(4) .
O12 Dy1 2.360(4) .
O13 Dy1 2.455(4) .
O14 Co2 1.891(3) .
O14 Dy1 2.253(3) 2_676
O15 Co2 1.934(3) .
O15 Dy1 2.446(3) 2_676
O15 Dy1 2.454(3) .
O21 Dy1 2.372(4) .
O22 C12 1.272(6) 2_676
O22 Co2 1.914(4) .
O23 Dy1 2.388(4) .
O24 Co2 1.881(3) .
O24 Dy1 2.261(3) .
Co2 Dy1 3.2824(11) 2_676
Co2 Dy1 3.2949(14) .
Dy1 O14 2.253(3) 2_676
Dy1 O15 2.446(3) 2_676
Dy1 Co2 3.2824(11) 2_676
