#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029813.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029813
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.203(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9867(10)
_cell_length_b                   16.5916(5)
_cell_length_c                   25.5520(12)
_cell_measurement_reflns_used    11514
_cell_measurement_temperature    380.00(10)
_cell_measurement_theta_max      28.8720
_cell_measurement_theta_min      3.2200
_cell_volume                     8433.9(7)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      380.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.958
_diffrn_measured_fraction_theta_max 0.958
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0319
_diffrn_reflns_av_sigmaI/netI    0.0399
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            18212
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.144
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.48192
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.256
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.882
_refine_diff_density_min         -0.953
_refine_diff_density_rms         0.151
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.069
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7123
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.069
_refine_ls_R_factor_all          0.0605
_refine_ls_R_factor_gt           0.0472
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0741P)²+65.3017P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1329
_refine_ls_wR_factor_ref         0.1458
_reflns_number_gt                5688
_reflns_number_total             7123
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           B_380K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029813.cif.
;
_cod_original_cell_volume        8433.9(6)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029813
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag -0.15573(3) 0.45709(4) -0.63275(3) 0.0501(2) Uani 1 1 d .
Ag2 Ag -0.17779(4) 0.75508(5) -0.13326(3) 0.0567(2) Uani 1 1 d .
C13 C 0.0978(3) 0.9705(4) -0.0006(3) 0.0286(15) Uani 1 1 d .
C16 C -0.3763(3) 0.7559(4) -0.4988(3) 0.0276(15) Uani 1 1 d .
C18 C 0.2772(4) 1.1384(5) 0.0084(3) 0.0395(18) Uani 1 1 d .
H18A H 0.2979 1.1350 0.0485 0.047 Uiso 1 1 calc R
C19 C -0.4404(3) 0.8014(4) -0.5316(3) 0.0290(15) Uani 1 1 d .
C20 C 0.1818(3) 1.0525(4) 0.0055(3) 0.0297(15) Uani 1 1 d .
C21 C 0.0038(3) 0.8847(5) -0.0049(3) 0.0353(16) Uani 1 1 d .
H21A H 0.0237 0.8831 0.0353 0.042 Uiso 1 1 calc R
C22 C -0.2026(3) 0.5836(4) -0.4961(3) 0.0333(16) Uani 1 1 d .
H22A H -0.1806 0.5875 -0.4560 0.040 Uiso 1 1 calc R
C24 C -0.4671(4) 0.8110(5) -0.5899(3) 0.0417(19) Uani 1 1 d .
H24A H -0.4455 0.7898 -0.6112 0.050 Uiso 1 1 calc R
C26 C -0.2900(4) 0.7262(4) -0.4136(3) 0.0323(16) Uani 1 1 d .
C28 C -0.0559(4) 0.8442(4) -0.0364(3) 0.0370(17) Uani 1 1 d .
H28A H -0.0759 0.8162 -0.0163 0.044 Uiso 1 1 calc R
C29 C 0.2201(4) 1.1530(4) -0.1088(3) 0.0356(16) Uani 1 1 d .
H29A H 0.2004 1.1581 -0.1489 0.043 Uiso 1 1 calc R
C30 C 0.1801(3) 1.0023(4) 0.0867(3) 0.0325(16) Uani 1 1 d .
C32 C 0.1789(4) 0.9559(6) 0.1798(4) 0.051(2) Uani 1 1 d .
H32A H 0.1349 0.9381 0.1596 0.061 Uiso 1 1 calc R
C33 C -0.2569(4) 0.7364(4) -0.3498(3) 0.0333(16) Uani 1 1 d .
C34 C 0.0333(3) 0.9275(4) -0.0345(3) 0.0307(15) Uani 1 1 d .
C35 C -0.2644(4) 0.5648(5) -0.6122(3) 0.0390(17) Uani 1 1 d .
H35A H -0.2857 0.5585 -0.6522 0.047 Uiso 1 1 calc R
C36 C -0.2645(3) 0.6209(4) -0.5267(3) 0.0315(15) Uani 1 1 d .
C37 C -0.4744(4) 0.8351(5) -0.5020(3) 0.0410(19) Uani 1 1 d .
H37A H -0.4571 0.8308 -0.4619 0.049 Uiso 1 1 calc R
C39 C 0.2147(3) 1.1013(4) -0.0234(3) 0.0295(15) Uani 1 1 d .
C42 C -0.2961(4) 0.6095(4) -0.5860(3) 0.0363(17) Uani 1 1 d .
H42A H -0.3382 0.6318 -0.6077 0.044 Uiso 1 1 calc R
C43 C 0.2123(4) 0.9918(5) 0.1510(3) 0.0366(17) Uani 1 1 d .
C44 C 0.1860(3) 1.1103(4) -0.0828(3) 0.0328(16) Uani 1 1 d .
H44A H 0.1442 1.0878 -0.1053 0.039 Uiso 1 1 calc R
C45 C -0.2950(3) 0.6723(4) -0.4964(3) 0.0291(15) Uani 1 1 d .
C46 C -0.5267(4) 0.8528(5) -0.6172(3) 0.0407(18) Uani 1 1 d .
H46A H -0.5441 0.8603 -0.6570 0.049 Uiso 1 1 calc R
C47 C -0.5330(4) 0.8744(5) -0.5321(3) 0.045(2) Uani 1 1 d .
H47A H -0.5552 0.8968 -0.5116 0.054 Uiso 1 1 calc R
C48 C -0.1747(4) 0.5410(5) -0.5266(3) 0.0369(17) Uani 1 1 d .
H48A H -0.1324 0.5184 -0.5061 0.044 Uiso 1 1 calc R
C49 C 0.3074(4) 1.1807(5) -0.0217(4) 0.045(2) Uani 1 1 d .
H49A H 0.3487 1.2054 -0.0007 0.054 Uiso 1 1 calc R
C51 C 0.0020(4) 0.9280(5) -0.0943(3) 0.0406(18) Uani 1 1 d .
H51A H 0.0197 0.9577 -0.1154 0.049 Uiso 1 1 calc R
C52 C 0.3068(4) 1.0050(6) 0.2416(4) 0.053(2) Uani 1 1 d .
H52A H 0.3511 1.0216 0.2626 0.063 Uiso 1 1 calc R
C54 C -0.2855(4) 0.7880(5) -0.3233(3) 0.045(2) Uani 1 1 d .
H54A H -0.3242 0.8172 -0.3450 0.054 Uiso 1 1 calc R
C55 C -0.0559(4) 0.8837(5) -0.1219(3) 0.046(2) Uani 1 1 d .
H55A H -0.0752 0.8817 -0.1621 0.055 Uiso 1 1 calc R
C56 C 0.2114(4) 0.9466(6) 0.2390(3) 0.054(2) Uani 1 1 d .
H56A H 0.1885 0.9222 0.2581 0.065 Uiso 1 1 calc R
C57 C 0.2778(4) 1.0168(5) 0.1825(4) 0.046(2) Uani 1 1 d .
H57A H 0.3018 1.0409 0.1643 0.055 Uiso 1 1 calc R
C58 C -0.2545(5) 0.7942(6) -0.2640(4) 0.053(2) Uani 1 1 d .
H58A H -0.2735 0.8287 -0.2464 0.063 Uiso 1 1 calc R
C59 C -0.1719(5) 0.7085(6) -0.2568(4) 0.059(3) Uani 1 1 d .
H59A H -0.1327 0.6808 -0.2341 0.070 Uiso 1 1 calc R
C60 C -0.1979(4) 0.6991(5) -0.3160(4) 0.050(2) Uani 1 1 d .
H60A H -0.1756 0.6678 -0.3325 0.060 Uiso 1 1 calc R
N1 N -0.2046(3) 0.5302(4) -0.5835(3) 0.0360(14) Uani 1 1 d .
N2 N -0.5606(3) 0.8827(4) -0.5890(3) 0.0388(15) Uani 1 1 d .
N3 N -0.1995(4) 0.7549(5) -0.2303(3) 0.0517(18) Uani 1 1 d .
N4 N -0.2624(3) 0.6773(4) -0.4385(3) 0.0350(14) Uani 1 1 d .
N5 N -0.3521(3) 0.7101(4) -0.5287(3) 0.0340(14) Uani 1 1 d .
N6 N -0.3473(3) 0.7669(4) -0.4418(3) 0.0346(14) Uani 1 1 d .
N7 N -0.0863(3) 0.8433(4) -0.0942(3) 0.0388(15) Uani 1 1 d .
N8 N 0.2751(3) 0.9714(5) 0.2703(3) 0.0499(18) Uani 1 1 d .
N9 N 0.2798(3) 1.1870(4) -0.0788(3) 0.0367(14) Uani 1 1 d .
N10 N 0.1256(3) 1.0127(3) -0.0282(2) 0.0312(13) Uani 1 1 d .
N11 N 0.1227(3) 0.9633(4) 0.0573(3) 0.0339(14) Uani 1 1 d .
N12 N 0.2111(3) 1.0499(4) 0.0635(3) 0.0364(14) Uani 1 1 d .
Mo1 Mo 0.0000 0.46487(7) -0.7500 0.0543(3) Uani 1 2 d S
Mo2 Mo -0.00129(3) 0.58983(4) -0.63920(3) 0.03291(18) Uani 1 1 d .
Mo3 Mo -0.00866(3) 0.79067(4) -0.64284(3) 0.03486(18) Uani 1 1 d .
Mo4 Mo 0.0000 0.90716(7) -0.7500 0.0516(3) Uani 1 2 d S
Mo5 Mo -0.09195(3) 0.69280(4) -0.79034(3) 0.03278(18) Uani 1 1 d .
O1 O 0.0624(6) 0.4024(7) -0.7074(6) 0.160(6) Uani 1 1 d .
O2 O -0.0340(3) 0.5144(4) -0.7058(3) 0.0618(17) Uani 1 1 d .
O3 O 0.0526(4) 0.5281(5) -0.5861(3) 0.078(2) Uani 1 1 d .
O4 O -0.0724(3) 0.5815(4) -0.6303(3) 0.0680(18) Uani 1 1 d .
O5 O 0.0329(3) 0.6898(4) -0.6062(3) 0.0619(17) Uani 1 1 d .
O6 O -0.0512(4) 0.6860(4) -0.7140(3) 0.0652(18) Uani 1 1 d .
O7 O -0.0758(4) 0.6043(4) -0.8232(3) 0.0696(19) Uani 1 1 d .
O8 O -0.1762(3) 0.6971(4) -0.8168(3) 0.0669(19) Uani 1 1 d .
O9 O -0.0779(4) 0.7875(5) -0.6295(3) 0.076(2) Uani 1 1 d .
O10 O 0.0428(4) 0.8522(5) -0.5918(3) 0.082(2) Uani 1 1 d .
O11 O -0.0471(3) 0.8584(4) -0.7115(3) 0.0668(18) Uani 1 1 d .
O12 O -0.0657(3) 0.7810(4) -0.8165(3) 0.0626(17) Uani 1 1 d .
O13 O 0.0580(5) 0.9663(5) -0.7016(4) 0.097(3) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N8 129.3(2) 3_545 3_444
N2 Ag1 N1 124.1(2) 3_545 .
N8 Ag1 N1 106.5(2) 3_444 .
N9 Ag2 N3 134.5(3) 3_445 .
N9 Ag2 N7 123.4(2) 3_445 .
N3 Ag2 N7 101.9(2) . .
N10 C13 N11 124.9(6) . .
N10 C13 C34 119.3(6) . .
N11 C13 C34 115.9(6) . .
N6 C16 N5 125.5(6) . .
N6 C16 C19 116.3(6) . .
N5 C16 C19 118.2(6) . .
C49 C18 C39 118.6(7) . .
C24 C19 C37 118.0(6) . .
C24 C19 C16 122.5(6) . .
C37 C19 C16 119.5(6) . .
N10 C20 N12 124.7(6) . .
N10 C20 C39 117.6(6) . .
N12 C20 C39 117.6(6) . .
C34 C21 C28 118.6(7) . .
C48 C22 C36 118.5(7) . .
C19 C24 C46 119.1(7) . .
N4 C26 N6 124.7(6) . .
N4 C26 C33 119.1(6) . .
N6 C26 C33 116.3(6) . .
N7 C28 C21 123.5(6) . .
N9 C29 C44 122.8(7) . .
N11 C30 N12 125.3(6) . .
N11 C30 C43 117.0(6) . .
N12 C30 C43 117.6(6) . .
C56 C32 C43 119.4(8) . .
C60 C33 C54 118.3(7) . .
C60 C33 C26 122.2(7) . .
C54 C33 C26 119.5(6) . .
C51 C34 C21 118.6(7) . .
C51 C34 C13 122.7(6) . .
C21 C34 C13 118.7(6) . .
N1 C35 C42 123.4(7) . .
C42 C36 C22 117.9(6) . .
C42 C36 C45 121.3(6) . .
C22 C36 C45 120.8(6) . .
C47 C37 C19 119.2(7) . .
C44 C39 C18 117.6(6) . .
C44 C39 C20 121.1(6) . .
C18 C39 C20 121.2(6) . .
C35 C42 C36 119.1(7) . .
C57 C43 C32 118.7(7) . .
C57 C43 C30 119.5(7) . .
C32 C43 C30 121.8(7) . .
C39 C44 C29 119.6(6) . .
N5 C45 N4 125.0(6) . .
N5 C45 C36 117.6(6) . .
N4 C45 C36 117.4(6) . .
N2 C46 C24 123.0(7) . .
N2 C47 C37 123.7(7) . .
N1 C48 C22 123.9(7) . .
N9 C49 C18 122.8(7) . .
C55 C51 C34 118.6(7) . .
N8 C52 C57 123.8(7) . .
C58 C54 C33 117.8(7) . .
N7 C55 C51 123.8(7) . .
N8 C56 C32 122.6(7) . .
C43 C57 C52 118.4(7) . .
N3 C58 C54 124.7(8) . .
N3 C59 C60 123.9(8) . .
C33 C60 C59 118.8(7) . .
C48 N1 C35 117.2(6) . .
C48 N1 Ag1 122.6(5) . .
C35 N1 Ag1 120.2(5) . .
C47 N2 C46 117.0(6) . .
C47 N2 Ag1 119.6(5) . 3_455
C46 N2 Ag1 123.1(5) . 3_455
C58 N3 C59 116.3(7) . .
C58 N3 Ag2 114.3(5) . .
C59 N3 Ag2 128.0(6) . .
C26 N4 C45 115.2(6) . .
C45 N5 C16 114.4(6) . .
C16 N6 C26 115.1(6) . .
C28 N7 C55 116.8(6) . .
C28 N7 Ag2 114.4(5) . .
C55 N7 Ag2 128.2(5) . .
C52 N8 C56 117.2(7) . .
C52 N8 Ag1 112.0(5) . 3_556
C56 N8 Ag1 130.6(5) . 3_556
C29 N9 C49 118.6(6) . .
C29 N9 Ag2 114.7(5) . 3
C49 N9 Ag2 126.6(5) . 3
C13 N10 C20 115.5(6) . .
C30 N11 C13 114.9(6) . .
C30 N12 C20 114.5(6) . .
O1 Mo1 O1 104.5(10) 2_553 .
O1 Mo1 O2 108.4(5) 2_553 2_553
O1 Mo1 O2 104.1(4) . 2_553
O1 Mo1 O2 104.1(4) 2_553 .
O1 Mo1 O2 108.4(5) . .
O2 Mo1 O2 125.6(4) 2_553 .
O4 Mo2 O3 102.3(4) . .
O4 Mo2 O5 103.4(3) . .
O3 Mo2 O5 99.4(3) . .
O4 Mo2 O2 92.6(3) . .
O3 Mo2 O2 100.3(3) . .
O5 Mo2 O2 151.2(3) . .
O4 Mo2 O7 164.6(3) . 2_553
O3 Mo2 O7 90.5(3) . 2_553
O5 Mo2 O7 82.4(3) . 2_553
O2 Mo2 O7 76.7(3) . 2_553
O4 Mo2 O6 91.5(3) . .
O3 Mo2 O6 165.8(3) . .
O5 Mo2 O6 74.0(3) . .
O2 Mo2 O6 81.9(2) . .
O7 Mo2 O6 76.3(2) 2_553 .
O10 Mo3 O9 103.4(4) . .
O10 Mo3 O5 97.3(4) . .
O9 Mo3 O5 98.9(3) . .
O10 Mo3 O11 104.0(4) . .
O9 Mo3 O11 96.7(3) . .
O5 Mo3 O11 149.8(3) . .
O10 Mo3 O12 91.1(3) . 2_553
O9 Mo3 O12 165.0(3) . 2_553
O5 Mo3 O12 83.0(3) . 2_553
O11 Mo3 O12 75.6(3) . 2_553
O10 Mo3 O6 162.6(3) . .
O9 Mo3 O6 92.1(3) . .
O5 Mo3 O6 72.1(2) . .
O11 Mo3 O6 81.6(3) . .
O12 Mo3 O6 74.2(2) 2_553 .
O13 Mo4 O13 107.8(6) 2_553 .
O13 Mo4 O11 106.4(4) 2_553 2_553
O13 Mo4 O11 102.8(4) . 2_553
O13 Mo4 O11 102.8(4) 2_553 .
O13 Mo4 O11 106.4(4) . .
O11 Mo4 O11 129.2(4) 2_553 .
O8 Mo5 O6 113.6(4) . .
O8 Mo5 O7 104.5(3) . .
O6 Mo5 O7 110.8(3) . .
O8 Mo5 O12 106.7(3) . .
O6 Mo5 O12 111.6(3) . .
O7 Mo5 O12 109.3(3) . .
Mo1 O2 Mo2 137.0(4) . .
Mo2 O5 Mo3 122.1(3) . .
Mo5 O6 Mo2 140.8(3) . .
Mo5 O6 Mo3 129.9(3) . .
Mo2 O6 Mo3 88.8(2) . .
Mo5 O7 Mo2 127.5(3) . 2_553
Mo4 O11 Mo3 126.4(4) . .
Mo5 O12 Mo3 129.0(3) . 2_553
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.270(6) 3_545
Ag1 N8 2.301(7) 3_444
Ag1 N1 2.315(6) .
Ag2 N9 2.277(6) 3_445
Ag2 N3 2.317(7) .
Ag2 N7 2.340(6) .
C13 N10 1.314(9) .
C13 N11 1.348(9) .
C13 C34 1.491(10) .
C16 N6 1.329(9) .
C16 N5 1.339(9) .
C16 C19 1.500(9) .
C18 C49 1.400(10) .
C18 C39 1.405(10) .
C19 C24 1.358(10) .
C19 C37 1.388(9) .
C20 N10 1.341(9) .
C20 N12 1.342(9) .
C20 C39 1.475(9) .
C21 C34 1.382(10) .
C21 C28 1.387(10) .
C22 C48 1.374(10) .
C22 C36 1.393(10) .
C24 C46 1.381(11) .
C26 N4 1.326(9) .
C26 N6 1.337(9) .
C26 C33 1.486(10) .
C28 N7 1.336(10) .
C29 N9 1.330(9) .
C29 C44 1.389(10) .
C30 N11 1.329(9) .
C30 N12 1.336(9) .
C30 C43 1.497(10) .
C32 C56 1.378(11) .
C32 C43 1.377(11) .
C33 C60 1.363(11) .
C33 C54 1.396(10) .
C34 C51 1.384(10) .
C35 N1 1.333(10) .
C35 C42 1.373(10) .
C36 C42 1.386(10) .
C36 C45 1.488(9) .
C37 C47 1.355(10) .
C39 C44 1.383(10) .
C43 C57 1.380(10) .
C45 N5 1.330(9) .
C45 N4 1.346(9) .
C46 N2 1.334(9) .
C47 N2 1.322(10) .
C48 N1 1.329(9) .
C49 N9 1.326(10) .
C51 C55 1.376(11) .
C52 N8 1.330(11) .
C52 C57 1.382(12) .
C54 C58 1.373(11) .
C55 N7 1.342(10) .
C56 N8 1.348(11) .
C58 N3 1.320(11) .
C59 N3 1.329(11) .
C59 C60 1.378(12) .
N2 Ag1 2.270(6) 3_455
N8 Ag1 2.301(7) 3_556
N9 Ag2 2.277(6) 3
Mo1 O1 1.694(10) 2_553
Mo1 O1 1.694(10) .
Mo1 O2 1.797(6) 2_553
Mo1 O2 1.797(6) .
Mo2 O4 1.679(6) .
Mo2 O3 1.710(7) .
Mo2 O5 1.867(7) .
Mo2 O2 1.985(6) .
Mo2 O7 2.289(6) 2_553
Mo2 O6 2.371(6) .
Mo3 O10 1.663(7) .
Mo3 O9 1.696(7) .
Mo3 O5 1.945(7) .
Mo3 O11 1.948(7) .
Mo3 O12 2.286(6) 2_553
Mo3 O6 2.398(6) .
Mo4 O13 1.665(8) 2_553
Mo4 O13 1.665(8) .
Mo4 O11 1.887(7) 2_553
Mo4 O11 1.887(7) .
Mo5 O8 1.680(6) .
Mo5 O6 1.769(6) .
Mo5 O7 1.801(7) .
Mo5 O12 1.802(7) .
O7 Mo2 2.289(6) 2_553
O12 Mo3 2.286(6) 2_553
