#------------------------------------------------------------------------------
#$Date: 2016-03-25 17:07:58 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180004 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/98/7029817.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7029817
loop_
_publ_author_name
'Zhang, Lei'
'Kuang, Xiaofei'
'Wu, Xiaoyuan'
'Yang, Wenbin'
'Lu, Canzhong'
_publ_section_title
;
 Supramolecular interactions induced hinge-like motion of a metal-organic
 framework accompanied by anisotropic thermal expansion.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7146
_journal_page_last               7152
_journal_paper_doi               10.1039/c3dt53580k
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C72 H48 Ag4 Mo8 N24 O26'
_chemical_formula_weight         2864.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.029(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9302(11)
_cell_length_b                   16.7795(8)
_cell_length_c                   25.4880(18)
_cell_measurement_reflns_used    6451
_cell_measurement_temperature    500.00(10)
_cell_measurement_theta_max      27.4820
_cell_measurement_theta_min      3.1770
_cell_volume                     8498.3(10)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      500.00(10)
_diffrn_detector_area_resol_mean 10.3503
_diffrn_measured_fraction_theta_full 0.957
_diffrn_measured_fraction_theta_max 0.957
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0364
_diffrn_reflns_av_sigmaI/netI    0.0448
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            18392
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    2.128
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.44401
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.239
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block-like
_exptl_crystal_F_000             5520
_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.09
_exptl_crystal_size_min          0.06
_refine_diff_density_max         2.243
_refine_diff_density_min         -0.912
_refine_diff_density_rms         0.159
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         7171
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.072
_refine_ls_R_factor_all          0.0793
_refine_ls_R_factor_gt           0.0578
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0989P)²+60.6199P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1657
_refine_ls_wR_factor_ref         0.1879
_reflns_number_gt                5268
_reflns_number_total             7171
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt53580k2.cif
_cod_data_source_block           B_500K
_cod_depositor_comments
;Adding full bibliography for
 ./tmp-cod-update-bibliographies-12899/cifs/7029817.cif.
;
_cod_original_cell_volume        8498.3(8)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7029817
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.34423(4) 0.45588(6) -0.63369(3) 0.0677(3) Uani 1 1 d .
Ag2 Ag 0.32111(5) 0.75773(6) -0.13403(4) 0.0774(3) Uani 1 1 d .
C6 C 0.5976(4) 0.9718(5) -0.0014(4) 0.0377(18) Uani 1 1 d .
C10 C 0.0324(5) 0.8091(6) -0.5918(4) 0.056(3) Uani 1 1 d .
H10B H 0.0537 0.7878 -0.6133 0.067 Uiso 1 1 calc R
C12 C 0.7762(5) 1.1387(5) 0.0070(4) 0.050(2) Uani 1 1 d .
H12B H 0.7969 1.1347 0.0472 0.060 Uiso 1 1 calc R
C14 C 0.0597(4) 0.7995(5) -0.5329(4) 0.041(2) Uani 1 1 d .
C15 C 0.2973(4) 0.5833(5) -0.4971(4) 0.042(2) Uani 1 1 d .
H15A H 0.3194 0.5873 -0.4570 0.050 Uiso 1 1 calc R
C18 C 0.1228(4) 0.7556(5) -0.5007(4) 0.042(2) Uani 1 1 d .
C19 C 0.5035(4) 0.8857(6) -0.0061(4) 0.048(2) Uani 1 1 d .
H19A H 0.5232 0.8841 0.0341 0.058 Uiso 1 1 calc R
C24 C 0.5326(4) 0.9279(5) -0.0356(4) 0.0388(18) Uani 1 1 d .
C25 C 0.6815(4) 1.0524(5) 0.0044(4) 0.043(2) Uani 1 1 d .
C26 C 0.2093(4) 0.7251(5) -0.4149(4) 0.0405(19) Uani 1 1 d .
C27 C 0.7137(4) 1.1017(5) -0.0250(4) 0.041(2) Uani 1 1 d .
C28 C 0.7196(4) 1.1525(5) -0.1102(4) 0.046(2) Uani 1 1 d .
H28A H 0.7003 1.1564 -0.1503 0.055 Uiso 1 1 calc R
C29 C 0.4435(5) 0.8450(6) -0.0380(4) 0.050(2) Uani 1 1 d .
H29A H 0.4241 0.8161 -0.0178 0.060 Uiso 1 1 calc R
C31 C 0.7117(4) 0.9917(6) 0.1500(4) 0.046(2) Uani 1 1 d .
C32 C 0.2348(4) 0.6208(5) -0.5280(4) 0.043(2) Uani 1 1 d .
C35 C 0.2357(5) 0.5645(6) -0.6133(4) 0.054(2) Uani 1 1 d .
H35A H 0.2147 0.5586 -0.6533 0.064 Uiso 1 1 calc R
C36 C 0.2426(5) 0.7363(6) -0.3512(4) 0.047(2) Uani 1 1 d .
C37 C 0.6787(5) 0.9554(7) 0.1792(5) 0.065(3) Uani 1 1 d .
H37A H 0.6349 0.9371 0.1589 0.078 Uiso 1 1 calc R
C38 C 0.0249(5) 0.8342(6) -0.5034(4) 0.052(2) Uani 1 1 d .
H38A H 0.0419 0.8308 -0.4633 0.063 Uiso 1 1 calc R
C39 C 0.8063(5) 1.1812(6) -0.0224(5) 0.057(3) Uani 1 1 d .
H39A H 0.8472 1.2063 -0.0011 0.068 Uiso 1 1 calc R
C40 C 0.6794(4) 1.0025(5) 0.0848(4) 0.043(2) Uani 1 1 d .
C41 C 0.2041(5) 0.6093(6) -0.5867(4) 0.053(2) Uani 1 1 d .
H41A H 0.1620 0.6315 -0.6086 0.064 Uiso 1 1 calc R
C42 C 0.2047(4) 0.6712(5) -0.4980(4) 0.0387(19) Uani 1 1 d .
C43 C 0.6855(4) 1.1105(5) -0.0838(4) 0.046(2) Uani 1 1 d .
H43A H 0.6436 1.0884 -0.1061 0.056 Uiso 1 1 calc R
C44 C 0.3249(5) 0.5409(6) -0.5275(4) 0.051(2) Uani 1 1 d .
H44A H 0.3672 0.5187 -0.5071 0.062 Uiso 1 1 calc R
C46 C 0.5011(5) 0.9286(6) -0.0955(4) 0.053(2) Uani 1 1 d .
H46A H 0.5189 0.9579 -0.1167 0.063 Uiso 1 1 calc R
C48 C -0.0275(5) 0.8510(7) -0.6191(4) 0.055(2) Uani 1 1 d .
H48A H -0.0451 0.8583 -0.6590 0.066 Uiso 1 1 calc R
C49 C 0.8059(6) 1.0046(8) 0.2403(5) 0.070(3) Uani 1 1 d .
H49A H 0.8495 1.0231 0.2614 0.084 Uiso 1 1 calc R
C50 C 0.2135(5) 0.7860(7) -0.3244(5) 0.064(3) Uani 1 1 d .
H50A H 0.1738 0.8131 -0.3459 0.077 Uiso 1 1 calc R
C51 C -0.0332(5) 0.8723(7) -0.5340(5) 0.062(3) Uani 1 1 d .
H51A H -0.0557 0.8945 -0.5137 0.074 Uiso 1 1 calc R
C52 C 0.7107(5) 0.9463(8) 0.2379(4) 0.075(4) Uani 1 1 d .
H52A H 0.6873 0.9229 0.2569 0.089 Uiso 1 1 calc R
C53 C 0.2452(7) 0.7937(8) -0.2654(5) 0.074(3) Uani 1 1 d .
H53A H 0.2266 0.8284 -0.2478 0.089 Uiso 1 1 calc R
C55 C 0.4431(5) 0.8854(7) -0.1230(4) 0.063(3) Uani 1 1 d .
H55A H 0.4238 0.8838 -0.1633 0.075 Uiso 1 1 calc R
C56 C 0.7774(5) 1.0152(7) 0.1808(5) 0.063(3) Uani 1 1 d .
H56A H 0.8020 1.0374 0.1623 0.076 Uiso 1 1 calc R
C58 C 0.3020(5) 0.6998(7) -0.3180(4) 0.062(3) Uani 1 1 d .
H58A H 0.3245 0.6688 -0.3346 0.074 Uiso 1 1 calc R
C59 C 0.3278(6) 0.7108(8) -0.2582(5) 0.078(4) Uani 1 1 d .
H59A H 0.3676 0.6845 -0.2353 0.093 Uiso 1 1 calc R
N1 N 0.2951(4) 0.5295(5) -0.5842(3) 0.0510(19) Uani 1 1 d .
N2 N -0.0606(4) 0.8807(5) -0.5906(3) 0.0515(19) Uani 1 1 d .
N3 N 0.3004(5) 0.7551(6) -0.2320(4) 0.069(3) Uani 1 1 d .
N4 N 0.2368(4) 0.6773(5) -0.4400(3) 0.0459(18) Uani 1 1 d .
N5 N 0.1476(4) 0.7095(4) -0.5303(3) 0.0442(17) Uani 1 1 d .
N6 N 0.1523(4) 0.7655(5) -0.4434(3) 0.0468(18) Uani 1 1 d .
N7 N 0.7792(4) 1.1876(5) -0.0799(3) 0.0497(19) Uani 1 1 d .
N8 N 0.4127(4) 0.8453(5) -0.0952(3) 0.0507(19) Uani 1 1 d .
N9 N 0.7751(4) 0.9698(6) 0.2695(4) 0.066(2) Uani 1 1 d .
N10 N 0.6249(3) 1.0135(4) -0.0295(3) 0.0431(17) Uani 1 1 d .
N11 N 0.7107(4) 1.0490(5) 0.0625(3) 0.0475(18) Uani 1 1 d .
N12 N 0.6223(4) 0.9623(4) 0.0561(3) 0.0454(17) Uani 1 1 d .
Mo1 Mo 0.5000 0.46806(9) -0.7500 0.0671(4) Uani 1 2 d S
Mo2 Mo 0.49857(4) 0.59027(5) -0.63878(3) 0.0446(2) Uani 1 1 d .
Mo3 Mo 0.49269(4) 0.78953(5) -0.64193(3) 0.0469(2) Uani 1 1 d .
Mo4 Mo 0.5000 0.90685(9) -0.7500 0.0656(4) Uani 1 2 d S
Mo5 Mo 0.40751(4) 0.69202(5) -0.78956(3) 0.0440(2) Uani 1 1 d .
O1 O 0.5638(9) 0.4059(10) -0.7100(9) 0.220(9) Uani 1 1 d .
O2 O 0.4668(5) 0.5153(5) -0.7050(4) 0.093(3) Uani 1 1 d .
O3 O 0.5538(5) 0.5341(8) -0.5842(4) 0.128(5) Uani 1 1 d .
O4 O 0.4287(4) 0.5794(7) -0.6298(4) 0.099(3) Uani 1 1 d .
O5 O 0.5331(5) 0.6885(5) -0.6057(4) 0.084(2) Uani 1 1 d .
O6 O 0.4472(5) 0.6865(5) -0.7147(4) 0.094(3) Uani 1 1 d .
O7 O 0.4244(5) 0.6038(6) -0.8228(4) 0.098(3) Uani 1 1 d .
O8 O 0.3234(4) 0.6952(5) -0.8177(4) 0.087(3) Uani 1 1 d .
O9 O 0.4227(5) 0.7884(7) -0.6293(5) 0.109(3) Uani 1 1 d .
O10 O 0.5465(5) 0.8457(8) -0.5896(4) 0.129(5) Uani 1 1 d .
O11 O 0.4550(5) 0.8574(6) -0.7102(4) 0.103(3) Uani 1 1 d .
O12 O 0.4334(5) 0.7783(5) -0.8173(4) 0.087(3) Uani 1 1 d .
O13 O 0.5594(7) 0.9652(8) -0.7044(6) 0.148(5) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N9 128.8(3) 3_545 3_444
N2 Ag1 N1 124.8(3) 3_545 .
N9 Ag1 N1 106.3(3) 3_444 .
N7 Ag2 N8 124.1(3) 3_445 .
N7 Ag2 N3 133.6(3) 3_445 .
N8 Ag2 N3 102.0(3) . .
N10 C6 N12 126.3(7) . .
N10 C6 C24 118.8(7) . .
N12 C6 C24 114.9(7) . .
C14 C10 C48 119.5(8) . .
C39 C12 C27 118.8(9) . .
C10 C14 C38 116.9(8) . .
C10 C14 C18 122.9(8) . .
C38 C14 C18 120.3(8) . .
C44 C15 C32 118.4(8) . .
N6 C18 N5 124.2(8) . .
N6 C18 C14 117.0(7) . .
N5 C18 C14 118.8(8) . .
C24 C19 C29 118.4(8) . .
C19 C24 C46 118.5(8) . .
C19 C24 C6 118.7(7) . .
C46 C24 C6 122.8(7) . .
N11 C25 N10 124.6(8) . .
N11 C25 C27 118.4(8) . .
N10 C25 C27 117.0(8) . .
N4 C26 N6 124.1(8) . .
N4 C26 C36 119.6(7) . .
N6 C26 C36 116.4(7) . .
C43 C27 C12 117.8(8) . .
C43 C27 C25 121.6(8) . .
C12 C27 C25 120.5(8) . .
N7 C28 C43 122.4(8) . .
N8 C29 C19 123.7(8) . .
C56 C31 C37 118.7(9) . .
C56 C31 C40 118.8(8) . .
C37 C31 C40 122.3(8) . .
C41 C32 C15 117.3(8) . .
C41 C32 C42 121.9(8) . .
C15 C32 C42 120.8(8) . .
N1 C35 C41 123.0(9) . .
C58 C36 C50 118.8(9) . .
C58 C36 C26 121.3(8) . .
C50 C36 C26 119.8(8) . .
C52 C37 C31 119.8(10) . .
C51 C38 C14 119.0(9) . .
N7 C39 C12 122.9(9) . .
N11 C40 N12 127.0(8) . .
N11 C40 C31 117.2(8) . .
N12 C40 C31 115.8(7) . .
C32 C41 C35 119.8(9) . .
N5 C42 N4 124.0(7) . .
N5 C42 C32 117.7(8) . .
N4 C42 C32 118.2(7) . .
C27 C43 C28 120.0(8) . .
N1 C44 C15 124.2(9) . .
C55 C46 C24 118.9(9) . .
N2 C48 C10 122.5(9) . .
N9 C49 C56 124.6(10) . .
C53 C50 C36 118.0(10) . .
N2 C51 C38 124.6(8) . .
N9 C52 C37 122.8(10) . .
N3 C53 C50 124.3(10) . .
N8 C55 C46 123.6(9) . .
C31 C56 C49 117.8(10) . .
C36 C58 C59 117.2(9) . .
N3 C59 C58 124.9(10) . .
C44 N1 C35 117.2(8) . .
C44 N1 Ag1 122.7(6) . .
C35 N1 Ag1 120.0(6) . .
C51 N2 C48 117.4(8) . .
C51 N2 Ag1 119.2(6) . 3_455
C48 N2 Ag1 123.1(6) . 3_455
C59 N3 C53 116.5(9) . .
C59 N3 Ag2 129.2(8) . .
C53 N3 Ag2 113.0(7) . .
C26 N4 C42 116.3(7) . .
C42 N5 C18 115.2(7) . .
C26 N6 C18 116.2(7) . .
C39 N7 C28 118.1(8) . .
C39 N7 Ag2 126.9(6) . 3
C28 N7 Ag2 115.0(6) . 3
C29 N8 C55 116.7(8) . .
C29 N8 Ag2 114.2(6) . .
C55 N8 Ag2 128.3(6) . .
C49 N9 C52 116.2(9) . .
C49 N9 Ag1 112.6(7) . 3_556
C52 N9 Ag1 131.1(7) . 3_556
C6 N10 C25 114.8(7) . .
C40 N11 C25 114.2(7) . .
C40 N12 C6 113.1(7) . .
O1 Mo1 O1 104.1(15) 2_653 .
O1 Mo1 O2 110.1(8) 2_653 2_653
O1 Mo1 O2 101.7(7) . 2_653
O1 Mo1 O2 101.7(7) 2_653 .
O1 Mo1 O2 110.1(8) . .
O2 Mo1 O2 127.3(6) 2_653 .
O4 Mo2 O3 102.0(5) . .
O4 Mo2 O5 105.0(5) . .
O3 Mo2 O5 96.2(5) . .
O4 Mo2 O2 92.0(4) . .
O3 Mo2 O2 102.6(6) . .
O5 Mo2 O2 151.4(4) . .
O4 Mo2 O7 164.5(4) . 2_653
O3 Mo2 O7 90.3(4) . 2_653
O5 Mo2 O7 82.8(4) . 2_653
O2 Mo2 O7 75.9(4) . 2_653
O4 Mo2 O6 92.3(5) . .
O3 Mo2 O6 164.7(5) . .
O5 Mo2 O6 74.4(4) . .
O2 Mo2 O6 82.3(3) . .
O7 Mo2 O6 76.6(3) 2_653 .
O10 Mo3 O9 104.4(5) . .
O10 Mo3 O11 106.0(6) . .
O9 Mo3 O11 95.8(5) . .
O10 Mo3 O5 95.0(6) . .
O9 Mo3 O5 99.6(5) . .
O11 Mo3 O5 150.0(4) . .
O10 Mo3 O12 90.7(4) . 2_653
O9 Mo3 O12 164.4(5) . 2_653
O11 Mo3 O12 75.9(4) . 2_653
O5 Mo3 O12 82.8(3) . 2_653
O10 Mo3 O6 161.5(5) . .
O9 Mo3 O6 91.4(5) . .
O11 Mo3 O6 81.5(4) . .
O5 Mo3 O6 72.6(3) . .
O12 Mo3 O6 74.5(3) 2_653 .
O13 Mo4 O13 107.3(9) . 2_653
O13 Mo4 O11 108.6(6) . .
O13 Mo4 O11 101.8(6) 2_653 .
O13 Mo4 O11 101.8(6) . 2_653
O13 Mo4 O11 108.6(6) 2_653 2_653
O11 Mo4 O11 127.6(6) . 2_653
O8 Mo5 O6 115.0(5) . .
O8 Mo5 O12 106.2(4) . .
O6 Mo5 O12 112.3(4) . .
O8 Mo5 O7 103.4(5) . .
O6 Mo5 O7 111.3(5) . .
O12 Mo5 O7 108.1(4) . .
Mo1 O2 Mo2 137.5(6) . .
Mo2 O5 Mo3 122.5(5) . .
Mo5 O6 Mo2 140.2(5) . .
Mo5 O6 Mo3 131.2(4) . .
Mo2 O6 Mo3 87.9(3) . .
Mo5 O7 Mo2 127.6(4) . 2_653
Mo4 O11 Mo3 128.2(5) . .
Mo5 O12 Mo3 130.5(5) . 2_653
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.283(7) 3_545
Ag1 N9 2.297(8) 3_444
Ag1 N1 2.329(7) .
Ag2 N7 2.283(7) 3_445
Ag2 N8 2.343(7) .
Ag2 N3 2.342(8) .
C6 N10 1.312(10) .
C6 N12 1.340(11) .
C6 C24 1.510(11) .
C10 C14 1.369(13) .
C10 C48 1.389(14) .
C12 C39 1.388(12) .
C12 C27 1.408(12) .
C14 C38 1.403(12) .
C14 C18 1.473(12) .
C15 C44 1.365(12) .
C15 C32 1.409(12) .
C18 N6 1.334(11) .
C18 N5 1.346(11) .
C19 C24 1.372(12) .
C19 C29 1.397(13) .
C24 C46 1.383(12) .
C25 N11 1.341(11) .
C25 N10 1.345(11) .
C25 C27 1.481(12) .
C26 N4 1.319(11) .
C26 N6 1.335(11) .
C26 C36 1.484(12) .
C27 C43 1.365(12) .
C28 N7 1.341(12) .
C28 C43 1.390(12) .
C29 N8 1.322(12) .
C31 C56 1.374(13) .
C31 C37 1.379(13) .
C31 C40 1.517(12) .
C32 C41 1.372(13) .
C32 C42 1.470(12) .
C35 N1 1.332(12) .
C35 C41 1.378(13) .
C36 C58 1.362(13) .
C36 C50 1.391(13) .
C37 C52 1.366(14) .
C38 C51 1.342(13) .
C39 N7 1.330(13) .
C40 N11 1.316(11) .
C40 N12 1.335(11) .
C42 N5 1.336(11) .
C42 N4 1.346(11) .
C44 N1 1.324(12) .
C46 C55 1.370(13) .
C48 N2 1.322(11) .
C49 N9 1.332(14) .
C49 C56 1.387(15) .
C50 C53 1.370(15) .
C51 N2 1.315(12) .
C52 N9 1.355(14) .
C53 N3 1.316(15) .
C55 N8 1.344(12) .
C58 C59 1.396(15) .
C59 N3 1.305(14) .
N2 Ag1 2.283(7) 3_455
N7 Ag2 2.283(7) 3
N9 Ag1 2.297(8) 3_556
Mo1 O1 1.697(14) 2_653
Mo1 O1 1.697(14) .
Mo1 O2 1.784(9) 2_653
Mo1 O2 1.784(9) .
Mo2 O4 1.653(8) .
Mo2 O3 1.693(9) .
Mo2 O5 1.861(9) .
Mo2 O2 1.980(9) .
Mo2 O7 2.295(9) 2_653
Mo2 O6 2.403(9) .
Mo3 O10 1.651(9) .
Mo3 O9 1.696(9) .
Mo3 O11 1.947(10) .
Mo3 O5 1.954(9) .
Mo3 O12 2.273(8) 2_653
Mo3 O6 2.420(9) .
Mo4 O13 1.651(12) .
Mo4 O13 1.651(12) 2_653
Mo4 O11 1.881(9) .
Mo4 O11 1.881(9) 2_653
Mo5 O8 1.674(7) .
Mo5 O6 1.733(9) .
Mo5 O12 1.805(9) .
Mo5 O7 1.820(10) .
O7 Mo2 2.295(9) 2_653
O12 Mo3 2.273(8) 2_653
