#------------------------------------------------------------------------------
#$Date: 2016-03-26 00:21:35 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180074 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/20/7052077.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7052077
loop_
_publ_author_name
'Bourlier, Julien'
'Hosseini, Mir Wais'
'Planeix, Jean-Marc'
'Kyritsakas, Nathalie'
_publ_section_title
;
 Molecular tectonics: generation of 1-D interdigitated and 2-D
 interwoven helical silver coordination networks by oligoethylene
 glycol based tectons bearing two benzonitrile moieties
;
_journal_issue                   1
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              25
_journal_paper_doi               10.1039/b611415f
_journal_volume                  31
_journal_year                    2007
_chemical_formula_moiety         'C22 H24 N2 O5, As F6'
_chemical_formula_sum            'C22 H24 Ag As F6 N2 O5'
_chemical_formula_weight         693.22
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 96.9200(9)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.7680(2)
_cell_length_b                   25.7570(6)
_cell_length_c                   8.5870(4)
_cell_measurement_reflns_used    5101
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      30.034
_cell_measurement_theta_min      0.998
_cell_volume                     2583.83(14)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0660
_diffrn_reflns_av_sigmaI/netI    0.1700
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            11916
_diffrn_reflns_theta_full        30.04
_diffrn_reflns_theta_max         30.04
_diffrn_reflns_theta_min         2.35
_exptl_absorpt_coefficient_mu    2.130
_exptl_absorpt_correction_T_max  0.7406
_exptl_absorpt_correction_T_min  0.6753
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.782
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1376
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.672
_refine_diff_density_min         -0.979
_refine_diff_density_rms         0.122
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.975
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     370
_refine_ls_number_reflns         7520
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.975
_refine_ls_R_factor_all          0.1806
_refine_ls_R_factor_gt           0.0508
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0001P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0709
_refine_ls_wR_factor_ref         0.0920
_reflns_number_gt                3136
_reflns_number_total             7520
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b611415f.txt
_cod_data_source_block           4-AgAsF6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7052077
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 1.25827(3) -0.164900(12) 1.15658(4) 0.04232(12) Uani 1 1 d . . .
C1 C 1.0286(3) 0.08005(15) 0.7953(5) 0.0297(10) Uani 1 1 d . . .
C2 C 0.9877(4) 0.03715(15) 0.7065(4) 0.0340(11) Uani 1 1 d . . .
H2 H 0.9329 0.0420 0.6170 0.041 Uiso 1 1 calc R . .
C3 C 1.0255(4) -0.01208(15) 0.7467(5) 0.0345(11) Uani 1 1 d . . .
H3 H 0.9969 -0.0411 0.6859 0.041 Uiso 1 1 calc R . .
C4 C 1.1058(4) -0.01890(15) 0.8768(5) 0.0305(10) Uani 1 1 d . . .
C5 C 1.1462(3) 0.02379(15) 0.9661(4) 0.0323(10) Uani 1 1 d . . .
H5 H 1.2010 0.0191 1.0557 0.039 Uiso 1 1 calc R . .
C6 C 1.1071(3) 0.07273(14) 0.9250(5) 0.0306(10) Uani 1 1 d . . .
H6 H 1.1346 0.1017 0.9868 0.037 Uiso 1 1 calc R . .
C7 C 1.1488(4) -0.06976(17) 0.9243(5) 0.0362(11) Uani 1 1 d . . .
N2 N 1.1848(3) -0.10919(13) 0.9672(4) 0.0423(10) Uani 1 1 d . . .
O1 O 0.9852(2) 0.12696(10) 0.7460(3) 0.0329(7) Uani 1 1 d . . .
C8 C 1.0460(4) 0.17239(14) 0.8077(5) 0.0369(11) Uani 1 1 d . . .
H8A H 1.1278 0.1698 0.7920 0.044 Uiso 1 1 calc R . .
H8B H 1.0409 0.1755 0.9216 0.044 Uiso 1 1 calc R . .
C9 C 0.9932(3) 0.21844(14) 0.7235(5) 0.0384(11) Uani 1 1 d . . .
H9A H 1.0471 0.2481 0.7355 0.046 Uiso 1 1 calc R . .
H9B H 0.9758 0.2106 0.6103 0.046 Uiso 1 1 calc R . .
O2 O 0.8899(2) 0.23165(9) 0.7873(3) 0.0351(7) Uani 1 1 d . . .
C10 C 0.8395(3) 0.27755(14) 0.7168(4) 0.0340(11) Uani 1 1 d . . .
H10A H 0.8079 0.2704 0.6068 0.041 Uiso 1 1 calc R . .
H10B H 0.8983 0.3050 0.7164 0.041 Uiso 1 1 calc R . .
C11 C 0.7460(3) 0.29544(14) 0.8076(5) 0.0345(11) Uani 1 1 d . . .
H11A H 0.7777 0.3037 0.9169 0.041 Uiso 1 1 calc R . .
H11B H 0.7096 0.3271 0.7593 0.041 Uiso 1 1 calc R . .
O3 O 0.6632(2) 0.25459(9) 0.8063(3) 0.0355(7) Uani 1 1 d . . .
C12 C 0.5711(4) 0.26881(15) 0.8920(5) 0.0427(12) Uani 1 1 d . . .
H12A H 0.5301 0.2993 0.8428 0.051 Uiso 1 1 calc R . .
H12B H 0.6010 0.2779 1.0013 0.051 Uiso 1 1 calc R . .
C13 C 0.4915(4) 0.22339(16) 0.8904(5) 0.0521(13) Uani 1 1 d . . .
H13A H 0.4247 0.2324 0.9450 0.062 Uiso 1 1 calc R . .
H13B H 0.4635 0.2136 0.7810 0.062 Uiso 1 1 calc R . .
O4 O 0.5532(3) 0.18148(10) 0.9683(3) 0.0459(8) Uani 1 1 d . . .
C14 C 0.4851(4) 0.14369(17) 1.0365(5) 0.0545(14) Uani 1 1 d . . .
H14A H 0.4292 0.1620 1.0942 0.065 Uiso 1 1 calc R . .
H14B H 0.5356 0.1230 1.1136 0.065 Uiso 1 1 calc R . .
C15 C 0.4226(4) 0.10805(17) 0.9231(5) 0.0511(13) Uani 1 1 d . . .
H15A H 0.3600 0.0909 0.9711 0.061 Uiso 1 1 calc R . .
H15B H 0.3885 0.1276 0.8296 0.061 Uiso 1 1 calc R . .
O5 O 0.5018(2) 0.06951(10) 0.8779(3) 0.0419(8) Uani 1 1 d . . .
C16 C 0.4577(4) 0.03189(15) 0.7763(5) 0.0325(10) Uani 1 1 d . . .
C17 C 0.5328(4) -0.00862(15) 0.7512(5) 0.0410(11) Uani 1 1 d . . .
H17 H 0.6087 -0.0087 0.8034 0.049 Uiso 1 1 calc R . .
C18 C 0.4956(4) -0.04828(15) 0.6504(5) 0.0381(11) Uani 1 1 d . . .
H18 H 0.5461 -0.0759 0.6334 0.046 Uiso 1 1 calc R . .
C19 C 0.3862(4) -0.04823(16) 0.5741(5) 0.0352(11) Uani 1 1 d . . .
C20 C 0.3119(4) -0.00794(16) 0.5996(5) 0.0405(12) Uani 1 1 d . . .
H20 H 0.2363 -0.0079 0.5466 0.049 Uiso 1 1 calc R . .
C21 C 0.3470(4) 0.03169(15) 0.7006(5) 0.0385(11) Uani 1 1 d . . .
H21 H 0.2956 0.0589 0.7185 0.046 Uiso 1 1 calc R . .
C22 C 0.3488(4) -0.08865(17) 0.4655(5) 0.0416(12) Uani 1 1 d . . .
N3 N 0.3190(4) -0.12035(14) 0.3757(4) 0.0544(12) Uani 1 1 d . . .
As1 As 0.21223(4) 0.147994(18) 0.37182(5) 0.04278(15) Uani 1 1 d . . .
F1 F 0.1905(12) 0.1200(6) 0.5483(14) 0.100(5) Uani 0.50 1 d P . .
F2 F 0.2625(17) 0.0921(8) 0.264(3) 0.090(5) Uani 0.50 1 d P . .
F3 F 0.3479(2) 0.14996(10) 0.4654(4) 0.0910(11) Uani 1 1 d . . .
F4 F 0.2323(14) 0.1727(5) 0.1982(13) 0.098(4) Uani 0.50 1 d P . .
F5 F 0.168(2) 0.1982(10) 0.469(3) 0.083(6) Uani 0.50 1 d P . .
F6 F 0.0789(3) 0.14498(11) 0.2725(4) 0.1152(13) Uani 1 1 d . . .
F7 F 0.2322(15) 0.0916(6) 0.302(2) 0.070(4) Uani 0.50 1 d P . .
F8 F 0.1595(13) 0.1054(6) 0.4864(14) 0.090(4) Uani 0.50 1 d P . .
F9 F 0.186(2) 0.2075(10) 0.448(3) 0.091(7) Uani 0.50 1 d P . .
F10 F 0.2691(12) 0.1918(4) 0.2519(13) 0.080(3) Uani 0.50 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N3 Ag1 N2 109.49(13) 1_656 . ?
N3 Ag1 O3 106.89(11) 1_656 3_757 ?
N2 Ag1 O3 141.58(10) . 3_757 ?
N3 Ag1 O2 110.09(11) 1_656 3_757 ?
N2 Ag1 O2 110.80(11) . 3_757 ?
O3 Ag1 O2 66.44(9) 3_757 3_757 ?
O1 C1 C6 124.5(4) . . ?
O1 C1 C2 116.2(4) . . ?
C6 C1 C2 119.3(4) . . ?
C3 C2 C1 120.9(4) . . ?
C3 C2 H2 119.5 . . ?
C1 C2 H2 119.5 . . ?
C2 C3 C4 119.2(4) . . ?
C2 C3 H3 120.4 . . ?
C4 C3 H3 120.4 . . ?
C3 C4 C5 120.0(4) . . ?
C3 C4 C7 121.6(4) . . ?
C5 C4 C7 118.4(4) . . ?
C6 C5 C4 120.1(4) . . ?
C6 C5 H5 119.9 . . ?
C4 C5 H5 119.9 . . ?
C1 C6 C5 120.5(4) . . ?
C1 C6 H6 119.8 . . ?
C5 C6 H6 119.8 . . ?
N2 C7 C4 177.4(5) . . ?
C7 N2 Ag1 152.8(3) . . ?
C1 O1 C8 117.2(3) . . ?
O1 C8 C9 108.0(3) . . ?
O1 C8 H8A 110.1 . . ?
C9 C8 H8A 110.1 . . ?
O1 C8 H8B 110.1 . . ?
C9 C8 H8B 110.1 . . ?
H8A C8 H8B 108.4 . . ?
O2 C9 C8 109.1(3) . . ?
O2 C9 H9A 109.9 . . ?
C8 C9 H9A 109.9 . . ?
O2 C9 H9B 109.9 . . ?
C8 C9 H9B 109.9 . . ?
H9A C9 H9B 108.3 . . ?
C10 O2 C9 111.3(3) . . ?
C10 O2 Ag1 112.5(2) . 3_757 ?
C9 O2 Ag1 123.1(2) . 3_757 ?
O2 C10 C11 109.2(3) . . ?
O2 C10 H10A 109.8 . . ?
C11 C10 H10A 109.8 . . ?
O2 C10 H10B 109.8 . . ?
C11 C10 H10B 109.8 . . ?
H10A C10 H10B 108.3 . . ?
O3 C11 C10 108.2(3) . . ?
O3 C11 H11A 110.1 . . ?
C10 C11 H11A 110.1 . . ?
O3 C11 H11B 110.1 . . ?
C10 C11 H11B 110.1 . . ?
H11A C11 H11B 108.4 . . ?
C12 O3 C11 111.4(3) . . ?
C12 O3 Ag1 117.6(2) . 3_757 ?
C11 O3 Ag1 116.0(2) . 3_757 ?
O3 C12 C13 107.9(3) . . ?
O3 C12 H12A 110.1 . . ?
C13 C12 H12A 110.1 . . ?
O3 C12 H12B 110.1 . . ?
C13 C12 H12B 110.1 . . ?
H12A C12 H12B 108.4 . . ?
O4 C13 C12 107.7(4) . . ?
O4 C13 H13A 110.2 . . ?
C12 C13 H13A 110.2 . . ?
O4 C13 H13B 110.2 . . ?
C12 C13 H13B 110.2 . . ?
H13A C13 H13B 108.5 . . ?
C13 O4 C14 115.4(3) . . ?
O4 C14 C15 114.5(4) . . ?
O4 C14 H14A 108.6 . . ?
C15 C14 H14A 108.6 . . ?
O4 C14 H14B 108.6 . . ?
C15 C14 H14B 108.6 . . ?
H14A C14 H14B 107.6 . . ?
O5 C15 C14 108.6(4) . . ?
O5 C15 H15A 110.0 . . ?
C14 C15 H15A 110.0 . . ?
O5 C15 H15B 110.0 . . ?
C14 C15 H15B 110.0 . . ?
H15A C15 H15B 108.4 . . ?
C16 O5 C15 116.8(3) . . ?
O5 C16 C21 124.6(4) . . ?
O5 C16 C17 115.4(4) . . ?
C21 C16 C17 120.0(4) . . ?
C18 C17 C16 119.4(4) . . ?
C18 C17 H17 120.3 . . ?
C16 C17 H17 120.3 . . ?
C19 C18 C17 120.6(4) . . ?
C19 C18 H18 119.7 . . ?
C17 C18 H18 119.7 . . ?
C18 C19 C20 119.8(4) . . ?
C18 C19 C22 120.5(4) . . ?
C20 C19 C22 119.7(4) . . ?
C21 C20 C19 120.6(4) . . ?
C21 C20 H20 119.7 . . ?
C19 C20 H20 119.7 . . ?
C20 C21 C16 119.7(4) . . ?
C20 C21 H21 120.2 . . ?
C16 C21 H21 120.2 . . ?
N3 C22 C19 178.5(5) . . ?
C22 N3 Ag1 165.1(4) . 1_454 ?
F7 As1 F8 72.6(9) . . ?
F7 As1 F5 165.4(12) . . ?
F8 As1 F5 93.3(11) . . ?
F7 As1 F4 88.2(9) . . ?
F8 As1 F4 153.6(5) . . ?
F5 As1 F4 103.9(10) . . ?
F7 As1 F6 86.5(7) . . ?
F8 As1 F6 82.9(5) . . ?
F5 As1 F6 87.9(10) . . ?
F4 As1 F6 77.8(5) . . ?
F7 As1 F3 91.8(7) . . ?
F8 As1 F3 97.9(5) . . ?
F5 As1 F3 94.0(10) . . ?
F4 As1 F3 100.7(5) . . ?
F6 As1 F3 177.81(16) . . ?
F7 As1 F9 177.9(11) . . ?
F8 As1 F9 105.7(11) . . ?
F4 As1 F9 93.0(10) . . ?
F6 As1 F9 92.0(9) . . ?
F3 As1 F9 89.7(9) . . ?
F7 As1 F10 106.6(8) . . ?
F8 As1 F10 179.0(8) . . ?
F5 As1 F10 87.5(11) . . ?
F6 As1 F10 97.6(5) . . ?
F3 As1 F10 81.5(5) . . ?
F9 As1 F10 75.1(10) . . ?
F7 As1 F1 89.6(9) . . ?
F5 As1 F1 78.2(11) . . ?
F4 As1 F1 177.7(6) . . ?
F6 As1 F1 101.3(5) . . ?
F3 As1 F1 80.0(5) . . ?
F9 As1 F1 89.2(10) . . ?
F10 As1 F1 155.7(5) . . ?
F8 As1 F2 86.9(9) . . ?
F5 As1 F2 179.5(13) . . ?
F4 As1 F2 76.1(9) . . ?
F6 As1 F2 92.6(7) . . ?
F3 As1 F2 85.5(7) . . ?
F9 As1 F2 167.0(12) . . ?
F10 As1 F2 92.3(8) . . ?
F1 As1 F2 101.8(9) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N3 2.246(4) 1_656 ?
Ag1 N2 2.261(3) . ?
Ag1 O3 2.494(2) 3_757 ?
Ag1 O2 2.536(3) 3_757 ?
C1 O1 1.359(4) . ?
C1 C6 1.372(5) . ?
C1 C2 1.395(5) . ?
C2 C3 1.374(5) . ?
C2 H2 0.9500 . ?
C3 C4 1.385(5) . ?
C3 H3 0.9500 . ?
C4 C5 1.391(5) . ?
C4 C7 1.445(5) . ?
C5 C6 1.373(5) . ?
C5 H5 0.9500 . ?
C6 H6 0.9500 . ?
C7 N2 1.144(5) . ?
O1 C8 1.439(4) . ?
C8 C9 1.486(5) . ?
C8 H8A 0.9900 . ?
C8 H8B 0.9900 . ?
C9 O2 1.433(4) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
O2 C10 1.425(4) . ?
O2 Ag1 2.536(3) 3_757 ?
C10 C11 1.496(5) . ?
C10 H10A 0.9900 . ?
C10 H10B 0.9900 . ?
C11 O3 1.433(4) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
O3 C12 1.430(4) . ?
O3 Ag1 2.494(2) 3_757 ?
C12 C13 1.498(5) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C13 O4 1.423(4) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
O4 C14 1.430(4) . ?
C14 C15 1.470(5) . ?
C14 H14A 0.9900 . ?
C14 H14B 0.9900 . ?
C15 O5 1.447(5) . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
O5 C16 1.364(4) . ?
C16 C21 1.384(5) . ?
C16 C17 1.401(5) . ?
C17 C18 1.376(5) . ?
C17 H17 0.9500 . ?
C18 C19 1.373(5) . ?
C18 H18 0.9500 . ?
C19 C20 1.391(5) . ?
C19 C22 1.431(6) . ?
C20 C21 1.370(5) . ?
C20 H20 0.9500 . ?
C21 H21 0.9500 . ?
C22 N3 1.148(5) . ?
N3 Ag1 2.246(4) 1_454 ?
As1 F7 1.598(13) . ?
As1 F8 1.645(14) . ?
As1 F5 1.654(16) . ?
As1 F4 1.664(13) . ?
As1 F6 1.695(3) . ?
As1 F3 1.700(3) . ?
As1 F9 1.71(2) . ?
As1 F10 1.716(12) . ?
As1 F1 1.725(14) . ?
As1 F2 1.847(15) . ?
F1 F8 0.715(18) . ?
F2 F7 0.51(3) . ?
F4 F10 0.770(13) . ?
