#------------------------------------------------------------------------------
#$Date: 2016-03-26 00:39:48 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180090 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/36/7053658.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7053658
loop_
_publ_author_name
'Zhang, Lijuan'
'Xu, Donghua'
'Zhou, Yunshan'
'Jiang, Fei'
_publ_section_title
;
 Design of 3-D europium(iii)--organic frameworks based on pyridine
 carboxylate N-oxide and acyclic binary carboxylate: syntheses,
 structures, and luminescence properties
;
_journal_issue                   11
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              2470
_journal_paper_doi               10.1039/c0nj00373e
_journal_volume                  34
_journal_year                    2010
_chemical_formula_sum            'C20 H21.98 Eu2 N2 O16.99'
_chemical_formula_weight         866.12
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                95.79(2)
_cell_angle_beta                 112.084(14)
_cell_angle_gamma                110.002(15)
_cell_formula_units_Z            1
_cell_length_a                   7.970(2)
_cell_length_b                   9.419(3)
_cell_length_c                   10.391(3)
_cell_measurement_reflns_used    2326
_cell_measurement_temperature    93(2)
_cell_measurement_theta_max      27.52
_cell_measurement_theta_min      3.03
_cell_volume                     655.2(4)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      93(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  AFC10/Saturn724+
_diffrn_measurement_method       Multi-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rotating Anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0345
_diffrn_reflns_av_sigmaI/netI    0.0554
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            6551
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_diffrn_reflns_theta_min         3.03
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    4.828
_exptl_absorpt_correction_T_max  0.7943
_exptl_absorpt_correction_T_min  0.4451
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    2.195
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Platelet
_exptl_crystal_F_000             418
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.195
_refine_diff_density_min         -1.442
_refine_diff_density_rms         0.181
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     201
_refine_ls_number_reflns         2972
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.007
_refine_ls_R_factor_all          0.0310
_refine_ls_R_factor_gt           0.0260
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0260P)²+0.1600P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0598
_refine_ls_wR_factor_ref         0.0615
_reflns_number_gt                2692
_reflns_number_total             2972
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c0nj00373e.txt
_cod_data_source_block           bo428
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Empirical'
changed to 'empirical' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        655.2(3)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7053658
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Eu1 Eu 0.28165(3) 0.05090(2) 0.011014(19) 0.00632(7) Uani 1 1 d . . .
O1 O 0.9273(4) -0.0172(3) 0.8624(3) 0.0092(6) Uani 1 1 d . . .
O2 O 0.4972(4) 0.0433(3) 0.2420(3) 0.0116(6) Uani 1 1 d . . .
O3 O 0.7569(4) 0.0071(4) 0.2307(3) 0.0123(6) Uani 1 1 d . . .
O4 O 0.3916(4) 0.3134(3) 0.1690(3) 0.0128(6) Uani 1 1 d . . .
O5 O 0.2564(4) 0.2811(3) -0.0658(3) 0.0112(6) Uani 1 1 d . . .
O6 O 0.1046(4) 0.7621(3) -0.0276(3) 0.0151(6) Uani 1 1 d . . .
O7 O 0.3988(4) 0.8325(3) -0.0232(3) 0.0085(6) Uani 1 1 d . . .
N1 N 0.8595(5) -0.0070(4) 0.7250(3) 0.0070(7) Uani 1 1 d . . .
C1 C 0.8083(6) -0.1318(5) 0.6206(4) 0.0111(8) Uani 1 1 d . . .
H1 H 0.8158 -0.2252 0.6435 0.013 Uiso 1 1 calc R . .
C2 C 0.7446(6) -0.1227(5) 0.4795(4) 0.0132(9) Uani 1 1 d . . .
H2 H 0.7143 -0.2082 0.4054 0.016 Uiso 1 1 calc R . .
C3 C 0.7249(6) 0.0108(5) 0.4462(4) 0.0085(8) Uani 1 1 d . . .
C4 C 0.7730(6) 0.1358(5) 0.5579(4) 0.0112(8) Uani 1 1 d . . .
H4 H 0.7562 0.2274 0.5372 0.013 Uiso 1 1 calc R . .
C5 C 0.8443(6) 0.1251(5) 0.6971(4) 0.0101(8) Uani 1 1 d . . .
H5 H 0.8829 0.2113 0.7739 0.012 Uiso 1 1 calc R . .
C6 C 0.6530(6) 0.0217(5) 0.2924(4) 0.0092(8) Uani 1 1 d . . .
C7 C 0.3241(6) 0.3635(5) 0.0604(4) 0.0107(8) Uani 1 1 d . . .
C8 C 0.3277(6) 0.5267(5) 0.0838(4) 0.0105(8) Uani 1 1 d . . .
H8A H 0.4673 0.6055 0.1306 0.013 Uiso 1 1 calc R . .
H8B H 0.2665 0.5378 0.1492 0.013 Uiso 1 1 calc R . .
C9 C 0.2159(6) 0.5585(5) -0.0576(4) 0.0103(8) Uani 1 1 d . . .
H9A H 0.2671 0.5360 -0.1269 0.012 Uiso 1 1 calc R . .
H9B H 0.0731 0.4876 -0.0990 0.012 Uiso 1 1 calc R . .
C10 C 0.2390(6) 0.7250(5) -0.0358(4) 0.0082(8) Uani 1 1 d . . .
O8 O 1.0041(13) 0.5740(10) 0.5893(9) 0.051(3) Uani 0.494(12) 1 d P . .
O9 O 0.611(9) 0.4844(18) 0.4496(17) 0.062(9) Uani 0.66(12) 1 d P A 1
O9' O 0.689(9) 0.501(4) 0.433(4) 0.042(9) Uani 0.34(12) 1 d P A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O7 Eu1 O3 73.53(9) 2_665 2_655
O7 Eu1 O2 75.89(9) 2_665 .
O3 Eu1 O2 136.97(9) 2_655 .
O7 Eu1 O5 82.06(9) 2_665 .
O3 Eu1 O5 77.13(10) 2_655 .
O2 Eu1 O5 127.33(10) . .
O7 Eu1 O1 147.45(9) 2_665 2_656
O3 Eu1 O1 138.66(9) 2_655 2_656
O2 Eu1 O1 78.11(9) . 2_656
O5 Eu1 O1 98.75(9) . 2_656
O7 Eu1 O1 144.04(9) 2_665 1_454
O3 Eu1 O1 76.16(9) 2_655 1_454
O2 Eu1 O1 140.00(9) . 1_454
O5 Eu1 O1 72.66(9) . 1_454
O1 Eu1 O1 63.66(10) 2_656 1_454
O7 Eu1 O4 81.69(9) 2_665 .
O3 Eu1 O4 127.02(10) 2_655 .
O2 Eu1 O4 76.41(10) . .
O5 Eu1 O4 53.22(9) . .
O1 Eu1 O4 73.39(9) 2_656 .
O1 Eu1 O4 101.99(9) 1_454 .
O7 Eu1 O6 122.93(9) 2_665 1_545
O3 Eu1 O6 87.25(10) 2_655 1_545
O2 Eu1 O6 84.65(10) . 1_545
O5 Eu1 O6 145.52(10) . 1_545
O1 Eu1 O6 73.14(9) 2_656 1_545
O1 Eu1 O6 73.83(10) 1_454 1_545
O4 Eu1 O6 144.20(9) . 1_545
O7 Eu1 O7 71.97(10) 2_665 1_545
O3 Eu1 O7 71.20(9) 2_655 1_545
O2 Eu1 O7 70.99(9) . 1_545
O5 Eu1 O7 143.45(9) . 1_545
O1 Eu1 O7 117.02(9) 2_656 1_545
O1 Eu1 O7 115.48(9) 1_454 1_545
O4 Eu1 O7 142.00(9) . 1_545
O6 Eu1 O7 50.96(9) 1_545 1_545
O7 Eu1 C7 82.46(10) 2_665 .
O3 Eu1 C7 102.64(11) 2_655 .
O2 Eu1 C7 102.55(11) . .
O5 Eu1 C7 26.52(10) . .
O1 Eu1 C7 84.42(10) 2_656 .
O1 Eu1 C7 85.74(10) 1_454 .
O4 Eu1 C7 26.79(10) . .
O6 Eu1 C7 154.59(10) 1_545 .
O7 Eu1 C7 154.42(10) 1_545 .
O7 Eu1 C10 97.68(10) 2_665 1_545
O3 Eu1 C10 78.22(10) 2_655 1_545
O2 Eu1 C10 76.66(10) . 1_545
O5 Eu1 C10 154.35(9) . 1_545
O1 Eu1 C10 95.03(10) 2_656 1_545
O1 Eu1 C10 94.62(10) 1_454 1_545
O4 Eu1 C10 152.36(10) . 1_545
O6 Eu1 C10 25.25(10) 1_545 1_545
O7 Eu1 C10 25.71(9) 1_545 1_545
C7 Eu1 C10 179.13(10) . 1_545
O7 Eu1 Eu1 37.91(7) 2_665 2_655
O3 Eu1 Eu1 67.96(7) 2_655 2_655
O2 Eu1 Eu1 69.27(6) . 2_655
O5 Eu1 Eu1 115.95(6) . 2_655
O1 Eu1 Eu1 142.19(7) 2_656 2_655
O1 Eu1 Eu1 139.00(6) 1_454 2_655
O4 Eu1 Eu1 115.09(7) . 2_655
O6 Eu1 Eu1 85.02(7) 1_545 2_655
O7 Eu1 Eu1 34.06(6) 1_545 2_655
C7 Eu1 Eu1 120.36(8) . 2_655
C10 Eu1 Eu1 59.77(8) 1_545 2_655
N1 O1 Eu1 121.0(2) . 2_656
N1 O1 Eu1 121.5(2) . 1_656
Eu1 O1 Eu1 116.34(10) 2_656 1_656
C6 O2 Eu1 135.9(2) . .
C6 O3 Eu1 137.3(2) . 2_655
C7 O4 Eu1 91.1(2) . .
C7 O5 Eu1 94.1(3) . .
C10 O6 Eu1 96.9(2) . 1_565
C10 O7 Eu1 158.9(3) . 2_665
C10 O7 Eu1 93.1(2) . 1_565
Eu1 O7 Eu1 108.03(10) 2_665 1_565
C5 N1 C1 122.4(3) . .
C5 N1 O1 119.5(3) . .
C1 N1 O1 118.1(3) . .
N1 C1 C2 119.3(4) . .
N1 C1 H1 120.4 . .
C2 C1 H1 120.4 . .
C3 C2 C1 120.0(4) . .
C3 C2 H2 120.0 . .
C1 C2 H2 120.0 . .
C2 C3 C4 118.8(4) . .
C2 C3 C6 120.6(3) . .
C4 C3 C6 120.7(4) . .
C5 C4 C3 119.5(4) . .
C5 C4 H4 120.2 . .
C3 C4 H4 120.2 . .
N1 C5 C4 119.9(4) . .
N1 C5 H5 120.0 . .
C4 C5 H5 120.0 . .
O2 C6 O3 128.0(4) . .
O2 C6 C3 116.2(3) . .
O3 C6 C3 115.8(3) . .
O5 C7 O4 121.2(4) . .
O5 C7 C8 119.7(4) . .
O4 C7 C8 119.1(3) . .
O5 C7 Eu1 59.4(2) . .
O4 C7 Eu1 62.1(2) . .
C8 C7 Eu1 174.9(3) . .
C7 C8 C9 111.8(3) . .
C7 C8 H8A 109.3 . .
C9 C8 H8A 109.3 . .
C7 C8 H8B 109.3 . .
C9 C8 H8B 109.3 . .
H8A C8 H8B 107.9 . .
C10 C9 C8 111.4(3) . .
C10 C9 H9A 109.3 . .
C8 C9 H9A 109.3 . .
C10 C9 H9B 109.3 . .
C8 C9 H9B 109.3 . .
H9A C9 H9B 108.0 . .
O6 C10 O7 119.0(4) . .
O6 C10 C9 121.4(4) . .
O7 C10 C9 119.5(3) . .
O6 C10 Eu1 57.8(2) . 1_565
O7 C10 Eu1 61.2(2) . 1_565
C9 C10 Eu1 178.9(3) . 1_565
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 O7 2.351(3) 2_665
Eu1 O3 2.394(3) 2_655
Eu1 O2 2.395(3) .
Eu1 O5 2.430(3) .
Eu1 O1 2.444(3) 2_656
Eu1 O1 2.461(3) 1_454
Eu1 O4 2.489(3) .
Eu1 O6 2.506(3) 1_545
Eu1 O7 2.578(3) 1_545
Eu1 C7 2.816(4) .
Eu1 C10 2.938(4) 1_545
Eu1 Eu1 3.9904(10) 2_655
O1 N1 1.350(4) .
O1 Eu1 2.444(3) 2_656
O1 Eu1 2.461(3) 1_656
O2 C6 1.251(5) .
O3 C6 1.255(5) .
O3 Eu1 2.394(3) 2_655
O4 C7 1.269(5) .
O5 C7 1.260(5) .
O6 C10 1.262(5) .
O6 Eu1 2.506(3) 1_565
O7 C10 1.276(5) .
O7 Eu1 2.351(3) 2_665
O7 Eu1 2.578(3) 1_565
N1 C5 1.340(5) .
N1 C1 1.344(5) .
C1 C2 1.383(5) .
C1 H1 0.9500 .
C2 C3 1.381(6) .
C2 H2 0.9500 .
C3 C4 1.400(5) .
C3 C6 1.509(5) .
C4 C5 1.370(5) .
C4 H4 0.9500 .
C5 H5 0.9500 .
C7 C8 1.521(6) .
C8 C9 1.526(6) .
C8 H8A 0.9900 .
C8 H8B 0.9900 .
C9 C10 1.499(6) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
C10 Eu1 2.938(4) 1_565
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O7 Eu1 O2 C6 -37.0(4) 2_665 .
O3 Eu1 O2 C6 8.8(4) 2_655 .
O5 Eu1 O2 C6 -105.2(4) . .
O1 Eu1 O2 C6 162.8(4) 2_656 .
O1 Eu1 O2 C6 145.8(3) 1_454 .
O4 Eu1 O2 C6 -121.7(4) . .
O6 Eu1 O2 C6 88.9(4) 1_545 .
O7 Eu1 O2 C6 38.5(4) 1_545 .
C7 Eu1 O2 C6 -115.8(4) . .
C10 Eu1 O2 C6 64.6(4) 1_545 .
Eu1 Eu1 O2 C6 2.2(4) 2_655 .
O7 Eu1 O4 C7 89.7(2) 2_665 .
O3 Eu1 O4 C7 27.7(3) 2_655 .
O2 Eu1 O4 C7 167.1(2) . .
O5 Eu1 O4 C7 3.5(2) . .
O1 Eu1 O4 C7 -111.5(2) 2_656 .
O1 Eu1 O4 C7 -53.9(2) 1_454 .
O6 Eu1 O4 C7 -132.8(2) 1_545 .
O7 Eu1 O4 C7 135.7(2) 1_545 .
C10 Eu1 O4 C7 -179.6(2) 1_545 .
Eu1 Eu1 O4 C7 108.1(2) 2_655 .
O7 Eu1 O5 C7 -89.0(2) 2_665 .
O3 Eu1 O5 C7 -163.9(2) 2_655 .
O2 Eu1 O5 C7 -23.6(3) . .
O1 Eu1 O5 C7 58.1(2) 2_656 .
O1 Eu1 O5 C7 116.9(2) 1_454 .
O4 Eu1 O5 C7 -3.5(2) . .
O6 Eu1 O5 C7 131.0(2) 1_545 .
O7 Eu1 O5 C7 -133.5(2) 1_545 .
C10 Eu1 O5 C7 179.8(2) 1_545 .
Eu1 Eu1 O5 C7 -106.5(2) 2_655 .
Eu1 O1 N1 C5 74.4(4) 2_656 .
Eu1 O1 N1 C5 -92.7(3) 1_656 .
Eu1 O1 N1 C1 -105.1(3) 2_656 .
Eu1 O1 N1 C1 87.7(4) 1_656 .
C5 N1 C1 C2 2.5(6) . .
O1 N1 C1 C2 -177.9(3) . .
N1 C1 C2 C3 -3.1(6) . .
C1 C2 C3 C4 0.8(6) . .
C1 C2 C3 C6 -179.2(4) . .
C2 C3 C4 C5 2.2(6) . .
C6 C3 C4 C5 -177.8(4) . .
C1 N1 C5 C4 0.5(6) . .
O1 N1 C5 C4 -179.0(3) . .
C3 C4 C5 N1 -2.9(6) . .
Eu1 O2 C6 O3 6.0(7) . .
Eu1 O2 C6 C3 -173.7(2) . .
Eu1 O3 C6 O2 -17.8(7) 2_655 .
Eu1 O3 C6 C3 161.8(3) 2_655 .
C2 C3 C6 O2 120.2(4) . .
C4 C3 C6 O2 -59.8(5) . .
C2 C3 C6 O3 -59.5(5) . .
C4 C3 C6 O3 120.5(4) . .
Eu1 O5 C7 O4 6.4(4) . .
Eu1 O5 C7 C8 -174.2(3) . .
Eu1 O4 C7 O5 -6.2(4) . .
Eu1 O4 C7 C8 174.4(3) . .
O7 Eu1 C7 O5 87.3(2) 2_665 .
O3 Eu1 C7 O5 16.1(2) 2_655 .
O2 Eu1 C7 O5 161.0(2) . .
O1 Eu1 C7 O5 -122.6(2) 2_656 .
O1 Eu1 C7 O5 -58.6(2) 1_454 .
O4 Eu1 C7 O5 173.8(4) . .
O6 Eu1 C7 O5 -94.8(3) 1_545 .
O7 Eu1 C7 O5 88.9(3) 1_545 .
C10 Eu1 C7 O5 -173(7) 1_545 .
Eu1 Eu1 C7 O5 87.8(2) 2_655 .
O7 Eu1 C7 O4 -86.5(2) 2_665 .
O3 Eu1 C7 O4 -157.7(2) 2_655 .
O2 Eu1 C7 O4 -12.8(2) . .
O5 Eu1 C7 O4 -173.8(4) . .
O1 Eu1 C7 O4 63.6(2) 2_656 .
O1 Eu1 C7 O4 127.6(2) 1_454 .
O6 Eu1 C7 O4 91.4(3) 1_545 .
O7 Eu1 C7 O4 -84.9(3) 1_545 .
C10 Eu1 C7 O4 13(7) 1_545 .
Eu1 Eu1 C7 O4 -86.0(2) 2_655 .
O7 Eu1 C7 C8 169(3) 2_665 .
O3 Eu1 C7 C8 98(3) 2_655 .
O2 Eu1 C7 C8 -117(3) . .
O5 Eu1 C7 C8 82(3) . .
O1 Eu1 C7 C8 -41(3) 2_656 .
O1 Eu1 C7 C8 23(3) 1_454 .
O4 Eu1 C7 C8 -105(3) . .
O6 Eu1 C7 C8 -13(3) 1_545 .
O7 Eu1 C7 C8 171(3) 1_545 .
C10 Eu1 C7 C8 -92(8) 1_545 .
Eu1 Eu1 C7 C8 169(3) 2_655 .
O5 C7 C8 C9 8.4(5) . .
O4 C7 C8 C9 -172.2(3) . .
Eu1 C7 C8 C9 -70(3) . .
C7 C8 C9 C10 -173.7(3) . .
Eu1 O6 C10 O7 0.1(4) 1_565 .
Eu1 O6 C10 C9 179.1(3) 1_565 .
Eu1 O7 C10 O6 179.0(5) 2_665 .
Eu1 O7 C10 O6 -0.1(4) 1_565 .
Eu1 O7 C10 C9 0.0(9) 2_665 .
Eu1 O7 C10 C9 -179.1(3) 1_565 .
Eu1 O7 C10 Eu1 179.1(7) 2_665 1_565
C8 C9 C10 O6 -100.1(4) . .
C8 C9 C10 O7 78.9(4) . .
C8 C9 C10 Eu1 -53(15) . 1_565
