#------------------------------------------------------------------------------
#$Date: 2016-03-26 03:42:01 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180192 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/88/7108813.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7108813
loop_
_publ_author_name
'Evgueni G. Mednikov'
'Lawrence F. Dahl'
_publ_section_title
;
 How innocent is thallium(I)? Corrected formulations of
 [Tl2Pd14(CO)9(PMe3)11][PF6]2 and [TlPd9(CO)9(PPh3)6][PF6] clusters
 previously reported as corresponding Au2Pd14 and AuPd9 clusters
;
_journal_issue                   11
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              1085
_journal_page_last               1087
_journal_paper_doi               10.1039/c2cc37959g
_journal_volume                  49
_journal_year                    2013
_chemical_formula_sum            'C124.26 H104.52 Cl1.32 F6 O10.65 P7 Pd9 Tl'
_chemical_formula_weight         3307.67
_chemical_name_common
;
palladium-thallium carbonylphosphine hexafluorophosphate
;
_chemical_name_systematic
;
tris(μ₃-carbonyl)-hexakis(μ₂-carbonyl)-hexakis
(triphenylphosphine)-thallium-nona-palladium
hexafluorophosphate tetrahydrofuran-methylenchloride
solvate
;
_space_group_IT_number           148
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            6
_cell_length_a                   22.5771(8)
_cell_length_b                   22.5771(8)
_cell_length_c                   39.3024(15)
_cell_measurement_reflns_used    9816
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.1781
_cell_measurement_theta_min      2.3816
_cell_volume                     17349.5(11)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker Apex2 diffractometer'
_diffrn_measurement_method       'w scans'
_diffrn_radiation_monochromator  'mirror optics'
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0585
_diffrn_reflns_av_sigmaI/netI    0.0286
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       52
_diffrn_reflns_limit_l_min       -52
_diffrn_reflns_number            105353
_diffrn_reflns_theta_full        28.34
_diffrn_reflns_theta_max         28.34
_diffrn_reflns_theta_min         2.32
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.948
_exptl_absorpt_correction_T_max  0.9434
_exptl_absorpt_correction_T_min  0.7814
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour
;
black; greenish-grey in transmitted light
;
_exptl_crystal_density_diffrn    1.899
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'plate crystal'
_exptl_crystal_F_000             9670
_exptl_crystal_size_max          0.09
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.02
_refine_diff_density_max         3.070
_refine_diff_density_min         -2.326
_refine_diff_density_rms         0.182
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     433
_refine_ls_number_reflns         9600
_refine_ls_number_restraints     54
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0739
_refine_ls_R_factor_gt           0.0526
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0608P)²+599.5322P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1311
_refine_ls_wR_factor_ref         0.1495
_reflns_number_gt                7675
_reflns_number_total             9600
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2cc37959g.txt
_cod_data_source_block           dahl403
_cod_original_cell_volume        17349.5(9)
_cod_original_sg_symbol_H-M      'R -3'
_cod_database_code               7108813
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Tl1 Tl 0.3333 0.6667 0.401655(11) 0.02691(11) Uani 1 3 d S . .
Pd1 Pd 0.40206(3) 0.64880(3) 0.457500(13) 0.02517(12) Uani 1 1 d . . .
Pd2 Pd 0.31704(2) 0.58775(2) 0.512104(12) 0.02410(12) Uani 1 1 d . . .
Pd3 Pd 0.47290(3) 0.77983(3) 0.432818(14) 0.03081(13) Uani 1 1 d . . .
P1 P 0.56126(10) 0.82512(10) 0.39281(5) 0.0332(4) Uani 1 1 d . . .
P2 P 0.30330(9) 0.49712(9) 0.54623(4) 0.0259(3) Uani 1 1 d . . .
O51 O 0.8034(7) 0.8096(9) 0.4619(5) 0.097(3) Uiso 0.55 1 d PD A -1
C51 C 0.8233(9) 0.8627(10) 0.4880(4) 0.097(3) Uiso 0.55 1 d PD A -1
H51A H 0.8088 0.8414 0.5108 0.116 Uiso 0.55 1 calc PR A -1
H51B H 0.8012 0.8902 0.4836 0.116 Uiso 0.55 1 calc PR A -1
C52 C 0.9009(10) 0.9082(11) 0.4869(6) 0.097(3) Uiso 0.55 1 d PD A -1
H52A H 0.9228 0.9011 0.5071 0.116 Uiso 0.55 1 calc PR A -1
H52B H 0.9146 0.9571 0.4852 0.116 Uiso 0.55 1 calc PR A -1
C53 C 0.9184(8) 0.8829(10) 0.4544(6) 0.097(3) Uiso 0.55 1 d PD A -1
H53A H 0.9656 0.8905 0.4553 0.116 Uiso 0.55 1 calc PR A -1
H53B H 0.9135 0.9058 0.4340 0.116 Uiso 0.55 1 calc PR A -1
C54 C 0.8654(10) 0.8064(10) 0.4546(7) 0.097(3) Uiso 0.55 1 d PD A -1
H54A H 0.8626 0.7849 0.4323 0.116 Uiso 0.55 1 calc PR A -1
H54B H 0.8749 0.7816 0.4726 0.116 Uiso 0.55 1 calc PR A -1
C71 C 0.864(2) 0.8568(19) 0.4463(11) 0.073(2) Uiso 0.22 1 d PD B 2
H71A H 0.8463 0.8616 0.4242 0.088 Uiso 0.22 1 calc PR B 2
H71B H 0.9071 0.9001 0.4512 0.088 Uiso 0.22 1 calc PR B 2
Cl1 Cl 0.8039(8) 0.8397(8) 0.4788(4) 0.073(2) Uiso 0.22 1 d PD B 2
Cl2 Cl 0.8811(7) 0.7899(8) 0.4444(4) 0.073(2) Uiso 0.22 1 d PD B 2
P3 P 0.3333 0.6667 0.2907(5) 0.040(8) Uani 0.44 3 d SPD . 3
F1 F 0.2835(12) 0.6590(17) 0.3213(5) 0.033(5) Uiso 0.15 1 d PD . 3
F2 F 0.3845(12) 0.6694(17) 0.2611(5) 0.033(5) Uiso 0.15 1 d PD . 3
F3 F 0.3508(14) 0.6149(17) 0.3109(9) 0.050(5) Uiso 0.15 1 d PD . 3
F4 F 0.3964(11) 0.7280(15) 0.3093(9) 0.050(5) Uiso 0.15 1 d PD . 3
F5 F 0.3182(15) 0.7174(18) 0.2715(10) 0.050(5) Uiso 0.15 1 d PD . 3
F6 F 0.2728(12) 0.6036(17) 0.2719(10) 0.050(5) Uiso 0.15 1 d PD . 3
P3A P 0.3378(12) 0.6652(13) 0.2834(4) 0.039(7) Uani 0.19 1 d PD . 4
F1A F 0.3182(11) 0.6598(17) 0.3231(4) 0.047(5) Uiso 0.19 1 d PD . 4
F2A F 0.3574(10) 0.6700(14) 0.2449(4) 0.047(5) Uiso 0.19 1 d PD . 4
F3A F 0.3629(14) 0.6118(12) 0.2903(6) 0.053(4) Uiso 0.19 1 d PD . 4
F4A F 0.4123(10) 0.7268(12) 0.2922(6) 0.053(4) Uiso 0.19 1 d PD . 4
F5A F 0.3107(16) 0.7172(15) 0.2786(7) 0.053(4) Uiso 0.19 1 d PD . 4
F6A F 0.2635(10) 0.6042(14) 0.2749(7) 0.053(4) Uiso 0.19 1 d PD . 4
O1 O 0.4356(3) 0.8911(3) 0.42334(17) 0.0512(15) Uani 1 1 d . . .
O2 O 0.5534(3) 0.7142(4) 0.45669(18) 0.0567(18) Uani 1 1 d . . .
O3 O 0.1674(3) 0.5335(3) 0.52831(14) 0.0352(11) Uani 1 1 d . . .
C1 C 0.4314(4) 0.8394(4) 0.42986(19) 0.0355(16) Uani 1 1 d . . .
C2 C 0.5060(4) 0.7183(4) 0.4501(2) 0.0430(19) Uani 1 1 d . . .
C3 C 0.2194(4) 0.5754(3) 0.51812(17) 0.0283(13) Uani 1 1 d . . .
C10 C 0.64639(19) 0.8762(2) 0.41028(12) 0.0394(17) Uani 1 1 d G . .
C11 C 0.6536(2) 0.8854(3) 0.44531(12) 0.047(2) Uani 1 1 d G . .
H11 H 0.6142 0.8677 0.4594 0.056 Uiso 1 1 calc R . .
C12 C 0.7184(3) 0.9206(3) 0.45973(10) 0.054(2) Uani 1 1 d G . .
H12 H 0.7233 0.9269 0.4837 0.064 Uiso 1 1 calc R . .
C13 C 0.7761(2) 0.9465(3) 0.43910(14) 0.059(3) Uani 1 1 d G . .
H13 H 0.8204 0.9705 0.4490 0.071 Uiso 1 1 calc R . .
C14 C 0.7689(2) 0.9372(3) 0.40407(13) 0.0452(19) Uani 1 1 d G . .
H14 H 0.8083 0.9549 0.3900 0.054 Uiso 1 1 calc R . .
C15 C 0.7040(2) 0.9021(3) 0.38966(10) 0.0381(16) Uani 1 1 d G . .
H15 H 0.6991 0.8957 0.3657 0.046 Uiso 1 1 calc R . .
C16 C 0.5597(3) 0.8811(2) 0.35982(12) 0.0387(17) Uani 1 1 d G . .
C17 C 0.5709(3) 0.9445(3) 0.37055(13) 0.047(2) Uani 1 1 d G . .
H17 H 0.5802 0.9571 0.3938 0.057 Uiso 1 1 calc R . .
C18 C 0.5683(3) 0.9894(2) 0.34723(19) 0.064(3) Uani 1 1 d G . .
H18 H 0.5759 1.0328 0.3546 0.077 Uiso 1 1 calc R . .
C19 C 0.5545(3) 0.9709(3) 0.31318(17) 0.068(3) Uani 1 1 d G . .
H19 H 0.5528 1.0016 0.2972 0.082 Uiso 1 1 calc R . .
C20 C 0.5434(3) 0.9075(3) 0.30245(11) 0.067(3) Uani 1 1 d G . .
H20 H 0.5340 0.8948 0.2792 0.080 Uiso 1 1 calc R . .
C21 C 0.5460(3) 0.8626(2) 0.32577(13) 0.048(2) Uani 1 1 d G . .
H21 H 0.5384 0.8192 0.3184 0.057 Uiso 1 1 calc R . .
C22 C 0.5575(3) 0.7513(2) 0.37124(13) 0.0353(16) Uani 1 1 d G . .
C23 C 0.6092(2) 0.7352(2) 0.37432(14) 0.0438(19) Uani 1 1 d G . .
H23 H 0.6506 0.7658 0.3857 0.053 Uiso 1 1 calc R . .
C24 C 0.6004(3) 0.6745(3) 0.36083(18) 0.055(2) Uani 1 1 d G . .
H24 H 0.6358 0.6635 0.3629 0.066 Uiso 1 1 calc R . .
C25 C 0.5399(3) 0.6297(2) 0.34425(17) 0.058(3) Uani 1 1 d G . .
H25 H 0.5339 0.5881 0.3350 0.069 Uiso 1 1 calc R . .
C26 C 0.4882(2) 0.6457(2) 0.34116(14) 0.049(2) Uani 1 1 d G . .
H26 H 0.4468 0.6151 0.3298 0.058 Uiso 1 1 calc R . .
C27 C 0.4970(2) 0.7065(3) 0.35466(14) 0.0394(17) Uani 1 1 d G . .
H27 H 0.4616 0.7175 0.3526 0.047 Uiso 1 1 calc R . .
C30 C 0.3488(3) 0.5250(2) 0.58690(10) 0.0303(14) Uani 1 1 d G . .
C31 C 0.3657(3) 0.5898(2) 0.59854(11) 0.0349(15) Uani 1 1 d G . .
H31 H 0.3546 0.6181 0.5853 0.042 Uiso 1 1 calc R . .
C32 C 0.3989(3) 0.6131(2) 0.62957(12) 0.0399(17) Uani 1 1 d G . .
H32 H 0.4105 0.6574 0.6375 0.048 Uiso 1 1 calc R . .
C33 C 0.4152(3) 0.5717(3) 0.64896(11) 0.048(2) Uani 1 1 d G . .
H33 H 0.4379 0.5877 0.6702 0.057 Uiso 1 1 calc R . .
C34 C 0.3983(3) 0.5070(3) 0.63733(13) 0.056(3) Uani 1 1 d G . .
H34 H 0.4094 0.4787 0.6506 0.068 Uiso 1 1 calc R . .
C35 C 0.3650(3) 0.4837(2) 0.60630(14) 0.047(2) Uani 1 1 d G . .
H35 H 0.3535 0.4394 0.5983 0.057 Uiso 1 1 calc R . .
C36 C 0.21667(18) 0.4349(2) 0.55991(12) 0.0259(13) Uani 1 1 d G . .
C37 C 0.1918(2) 0.4436(2) 0.59077(12) 0.0452(19) Uani 1 1 d G . .
H37 H 0.2209 0.4801 0.6054 0.054 Uiso 1 1 calc R . .
C38 C 0.1245(3) 0.3987(3) 0.60015(12) 0.051(2) Uani 1 1 d G . .
H38 H 0.1076 0.4046 0.6212 0.062 Uiso 1 1 calc R . .
C39 C 0.0820(2) 0.3452(3) 0.57867(15) 0.046(2) Uani 1 1 d G . .
H39 H 0.0360 0.3146 0.5851 0.055 Uiso 1 1 calc R . .
C40 C 0.1069(2) 0.3366(3) 0.54781(14) 0.061(3) Uani 1 1 d G . .
H40 H 0.0778 0.3001 0.5331 0.073 Uiso 1 1 calc R . .
C41 C 0.1742(2) 0.3815(3) 0.53843(11) 0.048(2) Uani 1 1 d G . .
H41 H 0.1912 0.3756 0.5173 0.058 Uiso 1 1 calc R . .
C42 C 0.3357(3) 0.4437(2) 0.52747(13) 0.0329(15) Uani 1 1 d G . .
C43 C 0.3160(3) 0.3786(3) 0.53949(13) 0.048(2) Uani 1 1 d G . .
H43 H 0.2823 0.3587 0.5568 0.057 Uiso 1 1 calc R . .
C44 C 0.3456(3) 0.3424(2) 0.52615(17) 0.057(3) Uani 1 1 d G . .
H44 H 0.3321 0.2979 0.5344 0.069 Uiso 1 1 calc R . .
C45 C 0.3949(3) 0.3715(3) 0.50080(16) 0.057(2) Uani 1 1 d G . .
H45 H 0.4151 0.3468 0.4917 0.069 Uiso 1 1 calc R . .
C46 C 0.4146(3) 0.4367(3) 0.48879(13) 0.050(2) Uani 1 1 d G . .
H46 H 0.4483 0.4565 0.4715 0.059 Uiso 1 1 calc R . .
C47 C 0.3850(3) 0.4728(2) 0.50212(14) 0.0408(17) Uani 1 1 d G . .
H47 H 0.3984 0.5174 0.4939 0.049 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Tl Tl -2.8358 9.6688 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Pd1 Tl1 Pd1 66.316(18) 2_665 3_565
Pd1 Tl1 Pd1 66.316(18) 2_665 .
Pd1 Tl1 Pd1 66.314(18) 3_565 .
Pd1 Tl1 Pd3 54.287(15) 2_665 2_665
Pd1 Tl1 Pd3 53.025(15) 3_565 2_665
Pd1 Tl1 Pd3 106.255(19) . 2_665
Pd1 Tl1 Pd3 53.027(15) 2_665 .
Pd1 Tl1 Pd3 106.258(19) 3_565 .
Pd1 Tl1 Pd3 54.290(15) . .
Pd3 Tl1 Pd3 105.832(14) 2_665 .
Pd1 Tl1 Pd3 106.256(19) 2_665 3_565
Pd1 Tl1 Pd3 54.287(15) 3_565 3_565
Pd1 Tl1 Pd3 53.024(15) . 3_565
Pd3 Tl1 Pd3 105.830(14) 2_665 3_565
Pd3 Tl1 Pd3 105.831(13) . 3_565
C2 Pd1 C1 92.4(3) . 3_565
C2 Pd1 C3 89.3(3) . 2_665
C1 Pd1 C3 110.4(3) 3_565 2_665
C2 Pd1 Pd3 137.9(2) . 3_565
C1 Pd1 Pd3 47.0(2) 3_565 3_565
C3 Pd1 Pd3 112.61(16) 2_665 3_565
C2 Pd1 Pd3 46.4(2) . .
C1 Pd1 Pd3 118.4(2) 3_565 .
C3 Pd1 Pd3 111.66(16) 2_665 .
Pd3 Pd1 Pd3 135.50(3) 3_565 .
C2 Pd1 Pd2 85.4(2) . 2_665
C1 Pd1 Pd2 157.3(2) 3_565 2_665
C3 Pd1 Pd2 47.03(17) 2_665 2_665
Pd3 Pd1 Pd2 135.99(2) 3_565 2_665
Pd3 Pd1 Pd2 75.63(2) . 2_665
C2 Pd1 Pd2 136.5(2) . .
C1 Pd1 Pd2 107.0(2) 3_565 .
C3 Pd1 Pd2 47.68(15) 2_665 .
Pd3 Pd1 Pd2 76.58(2) 3_565 .
Pd3 Pd1 Pd2 134.59(2) . .
Pd2 Pd1 Pd2 61.82(2) 2_665 .
C2 Pd1 Tl1 105.9(2) . .
C1 Pd1 Tl1 89.9(2) 3_565 .
C3 Pd1 Tl1 154.29(16) 2_665 .
Pd3 Pd1 Tl1 69.547(17) 3_565 .
Pd3 Pd1 Tl1 68.750(16) . .
Pd2 Pd1 Tl1 112.46(2) 2_665 .
Pd2 Pd1 Tl1 112.46(2) . .
C2 Pd1 Pd1 156.4(2) . 3_565
C1 Pd1 Pd1 102.8(2) 3_565 3_565
C3 Pd1 Pd1 101.86(16) 2_665 3_565
Pd3 Pd1 Pd1 56.09(2) 3_565 3_565
Pd3 Pd1 Pd1 109.97(2) . 3_565
Pd2 Pd1 Pd1 87.136(14) 2_665 3_565
Pd2 Pd1 Pd1 55.685(17) . 3_565
Tl1 Pd1 Pd1 56.841(9) . 3_565
C2 Pd1 Pd1 97.6(3) . 2_665
C1 Pd1 Pd1 146.7(2) 3_565 2_665
C3 Pd1 Pd1 101.39(17) 2_665 2_665
Pd3 Pd1 Pd1 111.59(2) 3_565 2_665
Pd3 Pd1 Pd1 54.32(2) . 2_665
Pd2 Pd1 Pd1 55.690(16) 2_665 2_665
Pd2 Pd1 Pd1 87.133(14) . 2_665
Tl1 Pd1 Pd1 56.840(9) . 2_665
Pd1 Pd1 Pd1 60.000(1) 3_565 2_665
C3 Pd2 C3 152.0(3) . 2_665
C3 Pd2 P2 98.5(2) . .
C3 Pd2 P2 94.13(19) 2_665 .
C3 Pd2 Pd1 59.02(19) . 3_565
C3 Pd2 Pd1 125.06(18) 2_665 3_565
P2 Pd2 Pd1 133.90(5) . 3_565
C3 Pd2 Pd1 125.50(19) . .
C3 Pd2 Pd1 58.80(18) 2_665 .
P2 Pd2 Pd1 129.95(5) . .
Pd1 Pd2 Pd1 68.63(2) 3_565 .
C3 Pd2 Pd2 107.85(18) . 2_665
C3 Pd2 Pd2 47.50(19) 2_665 2_665
P2 Pd2 Pd2 133.23(5) . 2_665
Pd1 Pd2 Pd2 92.868(15) 3_565 2_665
Pd1 Pd2 Pd2 59.085(18) . 2_665
C3 Pd2 Pd2 48.30(18) . 3_565
C3 Pd2 Pd2 107.06(19) 2_665 3_565
P2 Pd2 Pd2 136.92(5) . 3_565
Pd1 Pd2 Pd2 59.094(17) 3_565 3_565
Pd1 Pd2 Pd2 92.865(15) . 3_565
Pd2 Pd2 Pd2 59.998(2) 2_665 3_565
C1 Pd3 C2 163.0(3) . .
C1 Pd3 P1 104.6(2) . .
C2 Pd3 P1 89.9(2) . .
C1 Pd3 Pd1 52.9(2) . 2_665
C2 Pd3 Pd1 114.8(2) . 2_665
P1 Pd3 Pd1 153.62(6) . 2_665
C1 Pd3 Pd1 122.1(2) . .
C2 Pd3 Pd1 49.3(2) . .
P1 Pd3 Pd1 128.32(6) . .
Pd1 Pd3 Pd1 69.59(2) 2_665 .
C1 Pd3 Tl1 84.7(2) . .
C2 Pd3 Tl1 98.0(2) . .
P1 Pd3 Tl1 112.50(5) . .
Pd1 Pd3 Tl1 57.427(16) 2_665 .
Pd1 Pd3 Tl1 56.960(16) . .
C10 P1 C16 102.2(3) . .
C10 P1 C22 107.8(2) . .
C16 P1 C22 107.0(3) . .
C10 P1 Pd3 115.20(18) . .
C16 P1 Pd3 118.3(2) . .
C22 P1 Pd3 105.78(18) . .
C36 P2 C30 102.0(2) . .
C36 P2 C42 103.7(2) . .
C30 P2 C42 103.7(2) . .
C36 P2 Pd2 117.68(18) . .
C30 P2 Pd2 113.17(17) . .
C42 P2 Pd2 114.85(17) . .
C54 O51 C51 105.5(8) . .
O51 C51 C52 108.1(7) . .
O51 C51 H51A 110.1 . .
C52 C51 H51A 110.1 . .
O51 C51 H51B 110.1 . .
C52 C51 H51B 110.1 . .
H51A C51 H51B 108.4 . .
C51 C52 C53 101.4(8) . .
C51 C52 H52A 111.5 . .
C53 C52 H52A 111.5 . .
C51 C52 H52B 111.5 . .
C53 C52 H52B 111.5 . .
H52A C52 H52B 109.3 . .
C52 C53 C54 102.4(10) . .
C52 C53 H53A 111.3 . .
C54 C53 H53A 111.3 . .
C52 C53 H53B 111.3 . .
C54 C53 H53B 111.3 . .
H53A C53 H53B 109.2 . .
O51 C54 C53 99.9(9) . .
O51 C54 H54A 111.8 . .
C53 C54 H54A 111.8 . .
O51 C54 H54B 111.8 . .
C53 C54 H54B 111.8 . .
H54A C54 H54B 109.5 . .
Cl2 C71 Cl1 108.8(15) . .
Cl2 C71 H71A 109.9 . .
Cl1 C71 H71A 109.9 . .
Cl2 C71 H71B 109.9 . .
Cl1 C71 H71B 109.9 . .
H71A C71 H71B 108.3 . .
F5 P3 F5 98(2) . 2_665
F5 P3 F5 98(2) . 3_565
F5 P3 F5 98(2) 2_665 3_565
F5 P3 F6 9.5(15) . 3_565
F5 P3 F6 106.0(17) 2_665 3_565
F5 P3 F6 91.5(13) 3_565 3_565
F5 P3 F6 91.6(13) . .
F5 P3 F6 9.5(15) 2_665 .
F5 P3 F6 106.0(17) 3_565 .
F6 P3 F6 100(2) 3_565 .
F5 P3 F6 106.0(17) . 2_665
F5 P3 F6 91.5(13) 2_665 2_665
F5 P3 F6 9.5(15) 3_565 2_665
F6 P3 F6 100(2) 3_565 2_665
F6 P3 F6 100(2) . 2_665
F5 P3 F4 71.8(14) . 2_665
F5 P3 F4 90.7(13) 2_665 2_665
F5 P3 F4 167.5(13) 3_565 2_665
F6 P3 F4 78(2) 3_565 2_665
F6 P3 F4 82.2(19) . 2_665
F6 P3 F4 177.0(14) 2_665 2_665
F5 P3 F4 90.7(13) . .
F5 P3 F4 167.5(13) 2_665 .
F5 P3 F4 71.8(14) 3_565 .
F6 P3 F4 82.2(19) 3_565 .
F6 P3 F4 177.0(15) . .
F6 P3 F4 78(2) 2_665 .
F4 P3 F4 100.3(19) 2_665 .
F5 P3 F4 167.5(13) . 3_565
F5 P3 F4 71.8(14) 2_665 3_565
F5 P3 F4 90.7(13) 3_565 3_565
F6 P3 F4 177.0(15) 3_565 3_565
F6 P3 F4 78(2) . 3_565
F6 P3 F4 82.2(19) 2_665 3_565
F4 P3 F4 100.3(19) 2_665 3_565
F4 P3 F4 100.3(19) . 3_565
F5 P3 F1 92.4(12) . .
F5 P3 F1 97(2) 2_665 .
F5 P3 F1 160.0(19) 3_565 .
F6 P3 F1 97(2) 3_565 .
F6 P3 F1 90.5(11) . .
F6 P3 F1 158.5(18) 2_665 .
F4 P3 F1 22.6(14) 2_665 .
F4 P3 F1 91.4(13) . .
F4 P3 F1 82(2) 3_565 .
F5 P3 F1 97(2) . 3_565
F5 P3 F1 160.0(19) 2_665 3_565
F5 P3 F1 92.4(12) 3_565 3_565
F6 P3 F1 90.5(11) 3_565 3_565
F6 P3 F1 158.5(18) . 3_565
F6 P3 F1 97(2) 2_665 3_565
F4 P3 F1 82(2) 2_665 3_565
F4 P3 F1 22.6(14) . 3_565
F4 P3 F1 91.4(13) 3_565 3_565
F1 P3 F1 69.5(14) . 3_565
F5 P3 F1 160.0(19) . 2_665
F5 P3 F1 92.4(12) 2_665 2_665
F5 P3 F1 97(2) 3_565 2_665
F6 P3 F1 158.5(18) 3_565 2_665
F6 P3 F1 97(2) . 2_665
F6 P3 F1 90.5(11) 2_665 2_665
F4 P3 F1 91.4(13) 2_665 2_665
F4 P3 F1 82(2) . 2_665
F4 P3 F1 22.6(14) 3_565 2_665
F1 P3 F1 69.5(14) . 2_665
F1 P3 F1 69.5(14) 3_565 2_665
F5 P3 F3 83(2) . 3_565
F5 P3 F3 81(2) 2_665 3_565
F5 P3 F3 178.8(15) 3_565 3_565
F6 P3 F3 89.5(13) 3_565 3_565
F6 P3 F3 73.4(13) . 3_565
F6 P3 F3 169.4(13) 2_665 3_565
F4 P3 F3 13.6(13) 2_665 3_565
F4 P3 F3 108.8(15) . 3_565
F4 P3 F3 88.2(12) 3_565 3_565
F1 P3 F3 19.9(15) . 3_565
F1 P3 F3 88.0(12) 3_565 3_565
F1 P3 F3 82(3) 2_665 3_565
F5 P3 F3 81(2) . 2_665
F5 P3 F3 178.8(15) 2_665 2_665
F5 P3 F3 83(2) 3_565 2_665
F6 P3 F3 73.4(13) 3_565 2_665
F6 P3 F3 169.4(13) . 2_665
F6 P3 F3 89.5(13) 2_665 2_665
F4 P3 F3 88.2(12) 2_665 2_665
F4 P3 F3 13.6(13) . 2_665
F4 P3 F3 108.8(15) 3_565 2_665
F1 P3 F3 82(3) . 2_665
F1 P3 F3 19.9(15) 3_565 2_665
F1 P3 F3 88.0(12) 2_665 2_665
F3 P3 F3 98(2) 3_565 2_665
F5 P3 F3 178.8(16) . .
F5 P3 F3 83(2) 2_665 .
F5 P3 F3 81(2) 3_565 .
F6 P3 F3 169.4(14) 3_565 .
F6 P3 F3 89.5(13) . .
F6 P3 F3 73.4(13) 2_665 .
F4 P3 F3 108.8(15) 2_665 .
F4 P3 F3 88.2(12) . .
F4 P3 F3 13.6(13) 3_565 .
F1 P3 F3 88.0(12) . .
F1 P3 F3 82(3) 3_565 .
F1 P3 F3 19.9(15) 2_665 .
F3 P3 F3 98(2) 3_565 .
F3 P3 F3 98(2) 2_665 .
F5 P3 F2 18.5(16) . 2_665
F5 P3 F2 92.3(13) 2_665 2_665
F5 P3 F2 82(2) 3_565 2_665
F6 P3 F2 18.1(17) 3_565 2_665
F6 P3 F2 88(3) . 2_665
F6 P3 F2 88.7(12) 2_665 2_665
F4 P3 F2 89.2(10) 2_665 2_665
F4 P3 F2 94(2) . 2_665
F4 P3 F2 161.3(18) 3_565 2_665
F1 P3 F2 110.6(13) . 2_665
F1 P3 F2 106.0(14) 3_565 2_665
F1 P3 F2 175.3(14) 2_665 2_665
F3 P3 F2 99(2) 3_565 2_665
F3 P3 F2 87.3(11) 2_665 2_665
F3 P3 F2 161.2(16) . 2_665
F5 P3 F2 82(2) . 3_565
F5 P3 F2 18.5(16) 2_665 3_565
F5 P3 F2 92.3(13) 3_565 3_565
F6 P3 F2 88.7(13) 3_565 3_565
F6 P3 F2 18.1(17) . 3_565
F6 P3 F2 88(3) 2_665 3_565
F4 P3 F2 94(2) 2_665 3_565
F4 P3 F2 161.3(18) . 3_565
F4 P3 F2 89.2(11) 3_565 3_565
F1 P3 F2 106.0(14) . 3_565
F1 P3 F2 175.3(13) 3_565 3_565
F1 P3 F2 110.6(13) 2_665 3_565
F3 P3 F2 87.3(11) 3_565 3_565
F3 P3 F2 161.2(16) 2_665 3_565
F3 P3 F2 99(2) . 3_565
F2 P3 F2 74.0(16) 2_665 3_565
F5 P3 F2 92.3(13) . .
F5 P3 F2 82(2) 2_665 .
F5 P3 F2 18.5(16) 3_565 .
F6 P3 F2 88(3) 3_565 .
F6 P3 F2 88.7(12) . .
F6 P3 F2 18.1(17) 2_665 .
F4 P3 F2 161.3(18) 2_665 .
F4 P3 F2 89.2(11) . .
F4 P3 F2 94(2) 3_565 .
F1 P3 F2 175.3(13) . .
F1 P3 F2 110.6(13) 3_565 .
F1 P3 F2 106.0(14) 2_665 .
F3 P3 F2 161.3(16) 3_565 .
F3 P3 F2 99(2) 2_665 .
F3 P3 F2 87.3(11) . .
F2 P3 F2 74.0(16) 2_665 .
F2 P3 F2 74.0(16) 3_565 .
F3 F1 F4 37(3) 3_565 2_665
F3 F1 P3 82(3) 3_565 .
F4 F1 P3 78(2) 2_665 .
F6 F2 F5 30(4) 2_665 3_565
F6 F2 P3 77(3) 2_665 .
F5 F2 P3 73(3) 3_565 .
F4 F3 F1 81(7) 3_565 2_665
F4 F3 P3 78(4) 3_565 .
F1 F3 P3 78(3) 2_665 .
F3 F4 F1 62(7) 2_665 3_565
F3 F4 P3 88(4) 2_665 .
F1 F4 P3 80(3) 3_565 .
F6 F5 F2 73(10) 3_565 2_665
F6 F5 P3 93(7) 3_565 .
F2 F5 P3 89(4) 2_665 .
F5 F6 F2 77(10) 2_665 3_565
F5 F6 P3 78(6) 2_665 .
F2 F6 P3 85(3) 3_565 .
P3A P3A P3A 60.0(2) 3_565 2_665
P3A P3A F5A 171(7) 3_565 3_565
P3A P3A F5A 116(10) 2_665 3_565
P3A P3A F6A 155(10) 3_565 2_665
P3A P3A F6A 139(10) 2_665 2_665
F5A P3A F6A 25.2(12) 3_565 2_665
P3A P3A F5A 57(10) 3_565 2_665
P3A P3A F5A 116(10) 2_665 2_665
F5A P3A F5A 125.4(18) 3_565 2_665
F6A P3A F5A 100(2) 2_665 2_665
P3A P3A F2A 104.8(11) 3_565 .
P3A P3A F2A 98(3) 2_665 .
F5A P3A F2A 67.3(15) 3_565 .
F6A P3A F2A 62.4(14) 2_665 .
F5A P3A F2A 90.3(17) 2_665 .
P3A P3A F1A 93(2) 3_565 2_665
P3A P3A F1A 96.8(13) 2_665 2_665
F5A P3A F1A 95(2) 3_565 2_665
F6A P3A F1A 98.5(17) 2_665 2_665
F5A P3A F1A 94.2(18) 2_665 2_665
F2A P3A F1A 161(2) . 2_665
P3A P3A F5A 57(10) 3_565 .
P3A P3A F5A 8(5) 2_665 .
F5A P3A F5A 117.8(17) 3_565 .
F6A P3A F5A 139.2(19) 2_665 .
F5A P3A F5A 111.8(15) 2_665 .
F2A P3A F5A 91.9(13) . .
F1A P3A F5A 103.7(18) 2_665 .
P3A P3A F6A 36(10) 3_565 .
P3A P3A F6A 94(10) 2_665 .
F5A P3A F6A 144(2) 3_565 .
F6A P3A F6A 119.6(18) 2_665 .
F5A P3A F6A 22.7(12) 2_665 .
F2A P3A F6A 89.8(13) . .
F1A P3A F6A 101(2) 2_665 .
F5A P3A F6A 89.1(13) . .
P3A P3A F3A 121(10) 3_565 .
P3A P3A F3A 170(3) 2_665 .
F5A P3A F3A 64.3(17) 3_565 .
F6A P3A F3A 43.6(14) 2_665 .
F5A P3A F3A 67.4(15) 2_665 .
F2A P3A F3A 91.3(13) . .
F1A P3A F3A 73.4(17) 2_665 .
F5A P3A F3A 176.7(16) . .
F6A P3A F3A 90.1(14) . .
P3A P3A F4A 87(10) 3_565 3_565
P3A P3A F4A 145(10) 2_665 3_565
F5A P3A F4A 99(2) 3_565 3_565
F6A P3A F4A 76(2) 2_665 3_565
F5A P3A F4A 35.9(11) 2_665 3_565
F2A P3A F4A 102.3(18) . 3_565
F1A P3A F4A 71.7(17) 2_665 3_565
F5A P3A F4A 143.3(18) . 3_565
F6A P3A F4A 57.7(14) . 3_565
F3A P3A F4A 34.7(12) . 3_565
P3A P3A F4A 144(10) 3_565 .
P3A P3A F4A 86(10) 2_665 .
F5A P3A F4A 36.5(14) 3_565 .
F6A P3A F4A 60.9(16) 2_665 .
F5A P3A F4A 157.6(19) 2_665 .
F2A P3A F4A 90.6(13) . .
F1A P3A F4A 78(2) 2_665 .
F5A P3A F4A 90.6(14) . .
F6A P3A F4A 179.5(19) . .
F3A P3A F4A 90.2(13) . .
F4A P3A F4A 122.5(15) 3_565 .
P3A P3A F1A 90(3) 3_565 3_565
P3A P3A F1A 79(2) 2_665 3_565
F5A P3A F1A 97.2(17) 3_565 3_565
F6A P3A F1A 108(2) 2_665 3_565
F5A P3A F1A 107.5(19) 2_665 3_565
F2A P3A F1A 162(2) . 3_565
F1A P3A F1A 18.6(14) 2_665 3_565
F5A P3A F1A 86(2) . 3_565
F6A P3A F1A 108.6(17) . 3_565
F3A P3A F1A 91(2) . 3_565
F4A P3A F1A 89.8(14) 3_565 3_565
F4A P3A F1A 71.0(16) . 3_565
P3A P3A F2A 75(3) 3_565 3_565
P3A P3A F2A 93(3) 2_665 3_565
F5A P3A F2A 98.4(15) 3_565 3_565
F6A P3A F2A 86.9(19) 2_665 3_565
F5A P3A F2A 63.9(15) 2_665 3_565
F2A P3A F2A 32.4(12) . 3_565
F1A P3A F2A 158(2) 2_665 3_565
F5A P3A F2A 85.1(18) . 3_565
F6A P3A F2A 58.1(14) . 3_565
F3A P3A F2A 97.2(18) . 3_565
F4A P3A F2A 89.1(16) 3_565 3_565
F4A P3A F2A 122.2(16) . 3_565
F1A P3A F2A 164(2) 3_565 3_565
P3A P3A F1A 75.8(10) 3_565 .
P3A P3A F1A 83(3) 2_665 .
F5A P3A F1A 112.2(17) 3_565 .
F6A P3A F1A 116.9(18) 2_665 .
F5A P3A F1A 89.6(19) 2_665 .
F2A P3A F1A 179.3(18) . .
F1A P3A F1A 18.5(14) 2_665 .
F5A P3A F1A 88.8(13) . .
F6A P3A F1A 90.4(13) . .
F3A P3A F1A 88.0(13) . .
F4A P3A F1A 77.3(17) 3_565 .
F4A P3A F1A 89.2(12) . .
F1A P3A F1A 18.4(14) 3_565 .
F2A P3A F1A 147.9(18) 3_565 .
P3A P3A F6A 79(10) 3_565 3_565
P3A P3A F6A 22(10) 2_665 3_565
F5A P3A F6A 95.8(19) 3_565 3_565
F6A P3A F6A 117.8(16) 2_665 3_565
F5A P3A F6A 131(2) 2_665 3_565
F2A P3A F6A 82.1(16) . 3_565
F1A P3A F6A 108.5(19) 2_665 3_565
F5A P3A F6A 22.0(12) . 3_565
F6A P3A F6A 108.6(15) . 3_565
F3A P3A F6A 160.0(18) . 3_565
F4A P3A F6A 165(2) 3_565 3_565
F4A P3A F6A 71.1(15) . 3_565
F1A P3A F6A 89.8(17) 3_565 3_565
F2A P3A F6A 87.3(14) 3_565 3_565
F1A P3A F6A 98.5(19) . 3_565
P3A P3A F2A 80(3) 3_565 2_665
P3A P3A F2A 68.0(11) 2_665 2_665
F5A P3A F2A 91(2) 3_565 2_665
F6A P3A F2A 93.3(14) 2_665 2_665
F5A P3A F2A 93.2(15) 2_665 2_665
F2A P3A F2A 32.1(12) . 2_665
F1A P3A F2A 165(2) 2_665 2_665
F5A P3A F2A 61.2(14) . 2_665
F6A P3A F2A 80.9(18) . 2_665
F3A P3A F2A 121.8(16) . 2_665
F4A P3A F2A 120.8(17) 3_565 2_665
F4A P3A F2A 99.3(18) . 2_665
F1A P3A F2A 147(2) 3_565 2_665
F2A P3A F2A 31.7(12) 3_565 2_665
F1A P3A F2A 148.6(18) . 2_665
F6A P3A F2A 57.1(14) 3_565 2_665
P3A P3A F3A 112(10) 3_565 2_665
P3A P3A F3A 53(10) 2_665 2_665
F5A P3A F3A 66.1(19) 3_565 2_665
F6A P3A F3A 91.3(19) 2_665 2_665
F5A P3A F3A 168(2) 2_665 2_665
F2A P3A F3A 94.1(17) . 2_665
F1A P3A F3A 85.2(15) 2_665 2_665
F5A P3A F3A 57.5(13) . 2_665
F6A P3A F3A 146.4(17) . 2_665
F3A P3A F3A 123.1(15) . 2_665
F4A P3A F3A 151.5(18) 3_565 2_665
F4A P3A F3A 33.2(11) . 2_665
F1A P3A F3A 69.6(15) 3_565 2_665
F2A P3A F3A 116.1(17) 3_565 2_665
F1A P3A F3A 86.2(17) . 2_665
F6A P3A F3A 39.5(11) 3_565 2_665
F2A P3A F3A 84.9(15) 2_665 2_665
P3A P3A F4A 31(10) 3_565 2_665
P3A P3A F4A 32(10) 2_665 2_665
F5A P3A F4A 147(2) 3_565 2_665
F6A P3A F4A 171(2) 2_665 2_665
F5A P3A F4A 87.6(17) 2_665 2_665
F2A P3A F4A 114.3(15) . 2_665
F1A P3A F4A 84.5(13) 2_665 2_665
F5A P3A F4A 32.5(12) . 2_665
F6A P3A F4A 67.3(14) . 2_665
F3A P3A F4A 144.7(17) . 2_665
F4A P3A F4A 112.3(13) 3_565 2_665
F4A P3A F4A 112.2(15) . 2_665
F1A P3A F4A 72.7(19) 3_565 2_665
F2A P3A F4A 93.3(17) 3_565 2_665
F1A P3A F4A 66.4(13) . 2_665
F6A P3A F4A 53.7(16) 3_565 2_665
F2A P3A F4A 82.5(14) 2_665 2_665
F3A P3A F4A 80.9(14) 2_665 2_665
P3A P3A F3A 9(3) 3_565 3_565
P3A P3A F3A 62(10) 2_665 3_565
F5A P3A F3A 178(2) 3_565 3_565
F6A P3A F3A 157(2) 2_665 3_565
F5A P3A F3A 56.9(17) 2_665 3_565
F2A P3A F3A 113.5(15) . 3_565
F1A P3A F3A 84.3(18) 2_665 3_565
F5A P3A F3A 60.2(14) . 3_565
F6A P3A F3A 38.3(12) . 3_565
F3A P3A F3A 117.7(15) . 3_565
F4A P3A F3A 83.2(14) 3_565 3_565
F4A P3A F3A 141.2(16) . 3_565
F1A P3A F3A 81.6(14) 3_565 3_565
F2A P3A F3A 82.7(14) 3_565 3_565
F1A P3A F3A 67.1(13) . 3_565
F6A P3A F3A 82.2(16) 3_565 3_565
F2A P3A F3A 88.6(17) 2_665 3_565
F3A P3A F3A 111.6(13) 2_665 3_565
F4A P3A F3A 30.9(9) 2_665 3_565
F1A F1A F1A 60.01(4) 2_665 3_565
F1A F1A P3A 83.5(13) 2_665 3_565
F1A F1A P3A 85.0(12) 3_565 3_565
F1A F1A P3A 82.2(13) 2_665 2_665
F1A F1A P3A 77.9(13) 3_565 2_665
P3A F1A P3A 7.6(15) 3_565 2_665
F1A F1A P3A 76.5(10) 2_665 .
F1A F1A P3A 79.4(12) 3_565 .
P3A F1A P3A 7.5(15) 3_565 .
P3A F1A P3A 7.5(15) 2_665 .
F2A F2A F2A 60.005(11) 2_665 3_565
F2A F2A F6A 129.7(13) 2_665 2_665
F2A F2A F6A 115(3) 3_565 2_665
F2A F2A P3A 78.1(10) 2_665 .
F2A F2A P3A 76.5(10) 3_565 .
F6A F2A P3A 54.2(13) 2_665 .
F2A F2A P3A 71.2(10) 2_665 2_665
F2A F2A P3A 75.6(10) 3_565 2_665
F6A F2A P3A 60.2(10) 2_665 2_665
P3A F2A P3A 7.5(14) . 2_665
F2A F2A P3A 72.7(10) 2_665 3_565
F2A F2A P3A 69.8(10) 3_565 3_565
F6A F2A P3A 60.9(14) 2_665 3_565
P3A F2A P3A 7.2(14) . 3_565
P3A F2A P3A 7.4(14) 2_665 3_565
F2A F2A F5A 114(2) 2_665 3_565
F2A F2A F5A 124.9(14) 3_565 3_565
F6A F2A F5A 21.9(11) 2_665 3_565
P3A F2A F5A 50.8(13) . 3_565
P3A F2A F5A 54.2(14) 2_665 3_565
P3A F2A F5A 58.0(9) 3_565 3_565
F4A F3A F6A 127(2) 3_565 2_665
F4A F3A F5A 124(2) 3_565 3_565
F6A F3A F5A 17.3(15) 2_665 3_565
F4A F3A P3A 73(2) 3_565 .
F6A F3A P3A 60.2(16) 2_665 .
F5A F3A P3A 51.3(13) 3_565 .
F4A F3A F5A 26.5(14) 3_565 2_665
F6A F3A F5A 101.5(18) 2_665 2_665
F5A F3A F5A 101(2) 3_565 2_665
P3A F3A F5A 53.2(13) . 2_665
F4A F3A P3A 66.7(19) 3_565 3_565
F6A F3A P3A 65.6(12) 2_665 3_565
F5A F3A P3A 57.3(11) 3_565 3_565
P3A F3A P3A 6.1(14) . 3_565
F5A F3A P3A 47.5(15) 2_665 3_565
F4A F3A P3A 72.9(14) 3_565 2_665
F6A F3A P3A 60.6(15) 2_665 2_665
F5A F3A P3A 51.3(17) 3_565 2_665
P3A F3A P3A 1.2(4) . 2_665
F5A F3A P3A 53.7(9) 2_665 2_665
P3A F3A P3A 6.3(13) 3_565 2_665
F3A F4A F5A 127(3) 2_665 3_565
F3A F4A F6A 128(3) 2_665 2_665
F5A F4A F6A 9.1(17) 3_565 2_665
F3A F4A P3A 72.5(19) 2_665 2_665
F5A F4A P3A 65.5(14) 3_565 2_665
F6A F4A P3A 60.9(12) 2_665 2_665
F3A F4A P3A 80(2) 2_665 .
F5A F4A P3A 59.1(19) 3_565 .
F6A F4A P3A 53.9(13) 2_665 .
P3A F4A P3A 7.6(15) 2_665 .
F3A F4A P3A 76.2(14) 2_665 3_565
F5A F4A P3A 63.0(17) 3_565 3_565
F6A F4A P3A 58.0(17) 2_665 3_565
P3A F4A P3A 4.0(13) 2_665 3_565
P3A F4A P3A 4.1(14) . 3_565
F6A F5A F4A 157(4) 3_565 2_665
F6A F5A P3A 82(3) 3_565 2_665
F4A F5A P3A 84(2) 2_665 2_665
F6A F5A P3A 89(3) 3_565 3_565
F4A F5A P3A 78.5(16) 2_665 3_565
P3A F5A P3A 7.4(18) 2_665 3_565
F6A F5A P3A 82(3) 3_565 .
F4A F5A P3A 85(2) 2_665 .
P3A F5A P3A 1.2(9) 2_665 .
P3A F5A P3A 6.9(15) 3_565 .
F6A F5A F3A 33(3) 3_565 2_665
F4A F5A F3A 123(3) 2_665 2_665
P3A F5A F3A 64.4(13) 2_665 2_665
P3A F5A F3A 71.7(19) 3_565 2_665
P3A F5A F3A 65.2(14) . 2_665
F6A F5A F2A 71(3) 3_565 2_665
F4A F5A F2A 118(3) 2_665 2_665
P3A F5A F2A 61.9(13) 2_665 2_665
P3A F5A F2A 61.9(13) 3_565 2_665
P3A F5A F2A 60.8(11) . 2_665
F3A F5A F2A 88.8(15) 2_665 2_665
F6A F5A F3A 148(4) 3_565 3_565
F4A F5A F3A 26.4(15) 2_665 3_565
P3A F5A F3A 66(2) 2_665 3_565
P3A F5A F3A 59.4(12) 3_565 3_565
P3A F5A F3A 66.2(13) . 3_565
F3A F5A F3A 124(2) 2_665 3_565
F2A F5A F3A 92(2) 2_665 3_565
F5A F6A F3A 129(4) 2_665 3_565
F5A F6A P3A 73(2) 2_665 3_565
F3A F6A P3A 76.3(18) 3_565 3_565
F5A F6A F4A 14(3) 2_665 3_565
F3A F6A F4A 115(2) 3_565 3_565
P3A F6A F4A 65.2(13) 3_565 3_565
F5A F6A F2A 87(3) 2_665 3_565
F3A F6A F2A 114(2) 3_565 3_565
P3A F6A F2A 63.4(13) 3_565 3_565
F4A F6A F2A 93.4(16) 3_565 3_565
F5A F6A P3A 69(3) 2_665 .
F3A F6A P3A 81.1(18) 3_565 .
P3A F6A P3A 5.0(16) 3_565 .
F4A F6A P3A 61.4(13) 3_565 .
F2A F6A P3A 61.6(11) 3_565 .
F5A F6A P3A 76(3) 2_665 2_665
F3A F6A P3A 74.8(13) 3_565 2_665
P3A F6A P3A 3.2(14) 3_565 2_665
F4A F6A P3A 68.3(17) 3_565 2_665
F2A F6A P3A 62.0(13) 3_565 2_665
P3A F6A P3A 7.5(14) . 2_665
O1 C1 Pd3 150.4(7) . .
O1 C1 Pd1 128.9(6) . 2_665
Pd3 C1 Pd1 80.1(3) . 2_665
O2 C2 Pd3 145.1(7) . .
O2 C2 Pd1 130.5(7) . .
Pd3 C2 Pd1 84.3(3) . .
O3 C3 Pd2 136.4(6) . .
O3 C3 Pd2 136.9(5) . 3_565
Pd2 C3 Pd2 84.2(3) . 3_565
O3 C3 Pd1 123.8(5) . 3_565
Pd2 C3 Pd1 74.0(2) . 3_565
Pd2 C3 Pd1 73.5(2) 3_565 3_565
C11 C10 C15 120.0 . .
C11 C10 P1 118.6(3) . .
C15 C10 P1 121.3(3) . .
C10 C11 C12 120.0 . .
C10 C11 H11 120.0 . .
C12 C11 H11 120.0 . .
C13 C12 C11 120.0 . .
C13 C12 H12 120.0 . .
C11 C12 H12 120.0 . .
C12 C13 C14 120.0 . .
C12 C13 H13 120.0 . .
C14 C13 H13 120.0 . .
C15 C14 C13 120.0 . .
C15 C14 H14 120.0 . .
C13 C14 H14 120.0 . .
C14 C15 C10 120.0 . .
C14 C15 H15 120.0 . .
C10 C15 H15 120.0 . .
C17 C16 C21 120.0 . .
C17 C16 P1 116.2(3) . .
C21 C16 P1 123.8(3) . .
C18 C17 C16 120.0 . .
C18 C17 H17 120.0 . .
C16 C17 H17 120.0 . .
C17 C18 C19 120.0 . .
C17 C18 H18 120.0 . .
C19 C18 H18 120.0 . .
C20 C19 C18 120.0 . .
C20 C19 H19 120.0 . .
C18 C19 H19 120.0 . .
C21 C20 C19 120.0 . .
C21 C20 H20 120.0 . .
C19 C20 H20 120.0 . .
C20 C21 C16 120.0 . .
C20 C21 H21 120.0 . .
C16 C21 H21 120.0 . .
C23 C22 C27 120.0 . .
C23 C22 P1 122.2(3) . .
C27 C22 P1 117.4(3) . .
C24 C23 C22 120.0 . .
C24 C23 H23 120.0 . .
C22 C23 H23 120.0 . .
C23 C24 C25 120.0 . .
C23 C24 H24 120.0 . .
C25 C24 H24 120.0 . .
C26 C25 C24 120.0 . .
C26 C25 H25 120.0 . .
C24 C25 H25 120.0 . .
C25 C26 C27 120.0 . .
C25 C26 H26 120.0 . .
C27 C26 H26 120.0 . .
C26 C27 C22 120.0 . .
C26 C27 H27 120.0 . .
C22 C27 H27 120.0 . .
C31 C30 C35 120.0 . .
C31 C30 P2 117.5(3) . .
C35 C30 P2 122.5(3) . .
C30 C31 C32 120.0 . .
C30 C31 H31 120.0 . .
C32 C31 H31 120.0 . .
C31 C32 C33 120.0 . .
C31 C32 H32 120.0 . .
C33 C32 H32 120.0 . .
C34 C33 C32 120.0 . .
C34 C33 H33 120.0 . .
C32 C33 H33 120.0 . .
C33 C34 C35 120.0 . .
C33 C34 H34 120.0 . .
C35 C34 H34 120.0 . .
C34 C35 C30 120.0 . .
C34 C35 H35 120.0 . .
C30 C35 H35 120.0 . .
C37 C36 C41 120.0 . .
C37 C36 P2 120.1(3) . .
C41 C36 P2 119.8(3) . .
C38 C37 C36 120.0 . .
C38 C37 H37 120.0 . .
C36 C37 H37 120.0 . .
C37 C38 C39 120.0 . .
C37 C38 H38 120.0 . .
C39 C38 H38 120.0 . .
C40 C39 C38 120.0 . .
C40 C39 H39 120.0 . .
C38 C39 H39 120.0 . .
C41 C40 C39 120.0 . .
C41 C40 H40 120.0 . .
C39 C40 H40 120.0 . .
C40 C41 C36 120.0 . .
C40 C41 H41 120.0 . .
C36 C41 H41 120.0 . .
C43 C42 C47 120.0 . .
C43 C42 P2 122.3(3) . .
C47 C42 P2 117.6(3) . .
C44 C43 C42 120.0 . .
C44 C43 H43 120.0 . .
C42 C43 H43 120.0 . .
C43 C44 C45 120.0 . .
C43 C44 H44 120.0 . .
C45 C44 H44 120.0 . .
C46 C45 C44 120.0 . .
C46 C45 H45 120.0 . .
C44 C45 H45 120.0 . .
C47 C46 C45 120.0 . .
C47 C46 H46 120.0 . .
C45 C46 H46 120.0 . .
C46 C47 C42 120.0 . .
C46 C47 H47 120.0 . .
C42 C47 H47 120.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Tl1 Pd1 2.8307(6) 2_665
Tl1 Pd1 2.8307(6) 3_565
Tl1 Pd1 2.8308(6) .
Tl1 Pd3 3.1474(6) 2_665
Tl1 Pd3 3.1473(6) .
Tl1 Pd3 3.1474(6) 3_565
Pd1 C2 2.090(8) .
Pd1 C1 2.172(8) 3_565
Pd1 C3 2.450(7) 2_665
Pd1 Pd3 2.6836(8) 3_565
Pd1 Pd3 2.7420(7) .
Pd1 Pd2 2.7465(7) 2_665
Pd1 Pd2 2.7467(7) .
Pd1 Pd1 3.0965(9) 3_565
Pd1 Pd1 3.0966(8) 2_665
Pd2 C3 2.091(7) .
Pd2 C3 2.118(7) 2_665
Pd2 P2 2.3339(17) .
Pd2 Pd1 2.7465(7) 3_565
Pd2 Pd2 2.8219(9) 2_665
Pd2 Pd2 2.8220(8) 3_565
Pd3 C1 1.991(7) .
Pd3 C2 1.996(9) .
Pd3 P1 2.336(2) .
Pd3 Pd1 2.6836(8) 2_665
P1 C10 1.811(4) .
P1 C16 1.822(4) .
P1 C22 1.834(4) .
P2 C36 1.827(4) .
P2 C30 1.833(4) .
P2 C42 1.846(4) .
O51 C54 1.467(10) .
O51 C51 1.467(10) .
C51 C52 1.525(12) .
C51 H51A 0.9900 .
C51 H51B 0.9900 .
C52 C53 1.529(13) .
C52 H52A 0.9900 .
C52 H52B 0.9900 .
C53 C54 1.533(13) .
C53 H53A 0.9900 .
C53 H53B 0.9900 .
C54 H54A 0.9900 .
C54 H54B 0.9900 .
C71 Cl2 1.731(19) .
C71 Cl1 1.77(2) .
C71 H71A 0.9900 .
C71 H71B 0.9900 .
P3 F5 1.547(19) .
P3 F5 1.547(19) 2_665
P3 F5 1.547(19) 3_565
P3 F6 1.580(19) 3_565
P3 F6 1.580(19) .
P3 F6 1.580(19) 2_665
P3 F4 1.583(18) 2_665
P3 F4 1.583(19) .
P3 F4 1.583(18) 3_565
P3 F1 1.594(18) .
P3 F1 1.594(18) 3_565
P3 F1 1.594(18) 2_665
P3 F3 1.615(19) 3_565
P3 F3 1.615(19) 2_665
P3 F3 1.615(19) .
P3 F2 1.619(18) 2_665
P3 F2 1.619(18) 3_565
P3 F2 1.619(18) .
F1 F3 0.56(4) 3_565
F1 F4 0.62(4) 2_665
F2 F6 0.50(5) 2_665
F2 F5 0.51(4) 3_565
F3 F4 0.38(4) 3_565
F3 F1 0.56(4) 2_665
F4 F3 0.38(4) 2_665
F4 F1 0.62(4) 3_565
F5 F6 0.26(4) 3_565
F5 F2 0.51(4) 2_665
F6 F5 0.26(4) 2_665
F6 F2 0.50(5) 3_565
P3A P3A 0.21(4) 3_565
P3A P3A 0.21(4) 2_665
P3A F5A 1.37(3) 3_565
P3A F6A 1.42(3) 2_665
P3A F5A 1.48(4) 2_665
P3A F2A 1.565(18) .
P3A F1A 1.572(17) 2_665
P3A F5A 1.58(2) .
P3A F6A 1.59(2) .
P3A F3A 1.59(2) .
P3A F4A 1.59(3) 3_565
P3A F4A 1.59(2) .
P3A F1A 1.597(18) 3_565
P3A F2A 1.61(2) 3_565
P3A F1A 1.610(17) .
P3A F6A 1.61(4) 3_565
P3A F2A 1.63(2) 2_665
P3A F3A 1.71(4) 2_665
P3A F4A 1.77(3) 2_665
P3A F3A 1.80(3) 3_565
F1A F1A 0.51(4) 2_665
F1A F1A 0.51(4) 3_565
F1A P3A 1.572(17) 3_565
F1A P3A 1.597(18) 2_665
F2A F2A 0.88(3) 2_665
F2A F2A 0.88(3) 3_565
F2A F6A 1.55(3) 2_665
F2A P3A 1.61(2) 2_665
F2A P3A 1.63(2) 3_565
F2A F5A 1.64(3) 3_565
F3A F4A 0.95(3) 3_565
F3A F6A 1.13(3) 2_665
F3A F5A 1.59(3) 3_565
F3A F5A 1.71(3) 2_665
F3A P3A 1.71(4) 3_565
F3A P3A 1.80(3) 2_665
F4A F3A 0.95(3) 2_665
F4A F5A 0.95(3) 3_565
F4A F6A 1.53(3) 2_665
F4A P3A 1.59(3) 2_665
F4A P3A 1.77(3) 3_565
F5A F6A 0.61(3) 3_565
F5A F4A 0.95(3) 2_665
F5A P3A 1.37(3) 2_665
F5A P3A 1.48(4) 3_565
F5A F3A 1.59(3) 2_665
F5A F2A 1.64(3) 2_665
F5A F3A 1.71(3) 3_565
F6A F5A 0.61(3) 2_665
F6A F3A 1.13(3) 3_565
F6A P3A 1.42(3) 3_565
F6A F4A 1.53(3) 3_565
F6A F2A 1.55(3) 3_565
F6A P3A 1.61(4) 2_665
O1 C1 1.152(9) .
O2 C2 1.151(10) .
O3 C3 1.150(9) .
C1 Pd1 2.172(8) 2_665
C3 Pd2 2.118(7) 3_565
C3 Pd1 2.450(7) 3_565
C10 C11 1.3900 .
C10 C15 1.3900 .
C11 C12 1.3900 .
C11 H11 0.9500 .
C12 C13 1.3900 .
C12 H12 0.9500 .
C13 C14 1.3900 .
C13 H13 0.9500 .
C14 C15 1.3900 .
C14 H14 0.9500 .
C15 H15 0.9500 .
C16 C17 1.3900 .
C16 C21 1.3900 .
C17 C18 1.3900 .
C17 H17 0.9500 .
C18 C19 1.3900 .
C18 H18 0.9500 .
C19 C20 1.3900 .
C19 H19 0.9500 .
C20 C21 1.3900 .
C20 H20 0.9500 .
C21 H21 0.9500 .
C22 C23 1.3900 .
C22 C27 1.3900 .
C23 C24 1.3900 .
C23 H23 0.9500 .
C24 C25 1.3900 .
C24 H24 0.9500 .
C25 C26 1.3900 .
C25 H25 0.9500 .
C26 C27 1.3900 .
C26 H26 0.9500 .
C27 H27 0.9500 .
C30 C31 1.3900 .
C30 C35 1.3900 .
C31 C32 1.3900 .
C31 H31 0.9500 .
C32 C33 1.3900 .
C32 H32 0.9500 .
C33 C34 1.3900 .
C33 H33 0.9500 .
C34 C35 1.3900 .
C34 H34 0.9500 .
C35 H35 0.9500 .
C36 C37 1.3900 .
C36 C41 1.3900 .
C37 C38 1.3900 .
C37 H37 0.9500 .
C38 C39 1.3900 .
C38 H38 0.9500 .
C39 C40 1.3900 .
C39 H39 0.9500 .
C40 C41 1.3900 .
C40 H40 0.9500 .
C41 H41 0.9500 .
C42 C43 1.3900 .
C42 C47 1.3900 .
C43 C44 1.3900 .
C43 H43 0.9500 .
C44 C45 1.3900 .
C44 H44 0.9500 .
C45 C46 1.3900 .
C45 H45 0.9500 .
C46 C47 1.3900 .
C46 H46 0.9500 .
C47 H47 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Pd1 Tl1 Pd1 C2 -88.7(3) 2_665 .
Pd1 Tl1 Pd1 C2 -162.1(3) 3_565 .
Pd3 Tl1 Pd1 C2 -126.4(3) 2_665 .
Pd3 Tl1 Pd1 C2 -28.3(3) . .
Pd3 Tl1 Pd1 C2 135.8(3) 3_565 .
Pd1 Tl1 Pd1 C1 178.8(2) 2_665 3_565
Pd1 Tl1 Pd1 C1 105.4(2) 3_565 3_565
Pd3 Tl1 Pd1 C1 141.1(2) 2_665 3_565
Pd3 Tl1 Pd1 C1 -120.8(2) . 3_565
Pd3 Tl1 Pd1 C1 43.3(2) 3_565 3_565
Pd1 Tl1 Pd1 C3 35.6(4) 2_665 2_665
Pd1 Tl1 Pd1 C3 -37.7(4) 3_565 2_665
Pd3 Tl1 Pd1 C3 -2.0(4) 2_665 2_665
Pd3 Tl1 Pd1 C3 96.0(4) . 2_665
Pd3 Tl1 Pd1 C3 -99.8(4) 3_565 2_665
Pd1 Tl1 Pd1 Pd3 135.469(19) 2_665 3_565
Pd1 Tl1 Pd1 Pd3 62.12(2) 3_565 3_565
Pd3 Tl1 Pd1 Pd3 97.826(11) 2_665 3_565
Pd3 Tl1 Pd1 Pd3 -164.10(2) . 3_565
Pd1 Tl1 Pd1 Pd3 -60.43(2) 2_665 .
Pd1 Tl1 Pd1 Pd3 -133.78(2) 3_565 .
Pd3 Tl1 Pd1 Pd3 -98.070(11) 2_665 .
Pd3 Tl1 Pd1 Pd3 164.10(2) 3_565 .
Pd1 Tl1 Pd1 Pd2 2.902(17) 2_665 2_665
Pd1 Tl1 Pd1 Pd2 -70.446(12) 3_565 2_665
Pd3 Tl1 Pd1 Pd2 -34.74(2) 2_665 2_665
Pd3 Tl1 Pd1 Pd2 63.33(2) . 2_665
Pd3 Tl1 Pd1 Pd2 -132.57(3) 3_565 2_665
Pd1 Tl1 Pd1 Pd2 70.444(12) 2_665 .
Pd1 Tl1 Pd1 Pd2 -2.903(17) 3_565 .
Pd3 Tl1 Pd1 Pd2 32.80(2) 2_665 .
Pd3 Tl1 Pd1 Pd2 130.87(3) . .
Pd3 Tl1 Pd1 Pd2 -65.02(2) 3_565 .
Pd1 Tl1 Pd1 Pd1 73.348(9) 2_665 3_565
Pd3 Tl1 Pd1 Pd1 35.70(2) 2_665 3_565
Pd3 Tl1 Pd1 Pd1 133.78(2) . 3_565
Pd3 Tl1 Pd1 Pd1 -62.12(2) 3_565 3_565
Pd1 Tl1 Pd1 Pd1 -73.348(9) 3_565 2_665
Pd3 Tl1 Pd1 Pd1 -37.64(2) 2_665 2_665
Pd3 Tl1 Pd1 Pd1 60.43(2) . 2_665
Pd3 Tl1 Pd1 Pd1 -135.469(19) 3_565 2_665
C2 Pd1 Pd2 C3 136.6(4) . .
C1 Pd1 Pd2 C3 -110.8(3) 3_565 .
C3 Pd1 Pd2 C3 146.8(3) 2_665 .
Pd3 Pd1 Pd2 C3 -74.5(2) 3_565 .
Pd3 Pd1 Pd2 C3 68.1(2) . .
Pd2 Pd1 Pd2 C3 90.7(2) 2_665 .
Tl1 Pd1 Pd2 C3 -13.7(2) . .
Pd1 Pd1 Pd2 C3 -16.6(2) 3_565 .
Pd1 Pd1 Pd2 C3 38.5(2) 2_665 .
C2 Pd1 Pd2 C3 -10.2(4) . 2_665
C1 Pd1 Pd2 C3 102.5(3) 3_565 2_665
Pd3 Pd1 Pd2 C3 138.7(2) 3_565 2_665
Pd3 Pd1 Pd2 C3 -78.7(2) . 2_665
Pd2 Pd1 Pd2 C3 -56.1(2) 2_665 2_665
Tl1 Pd1 Pd2 C3 -160.4(2) . 2_665
Pd1 Pd1 Pd2 C3 -163.4(2) 3_565 2_665
Pd1 Pd1 Pd2 C3 -108.3(2) 2_665 2_665
C2 Pd1 Pd2 P2 -76.8(4) . .
C1 Pd1 Pd2 P2 35.9(2) 3_565 .
C3 Pd1 Pd2 P2 -66.6(2) 2_665 .
Pd3 Pd1 Pd2 P2 72.16(7) 3_565 .
Pd3 Pd1 Pd2 P2 -145.24(7) . .
Pd2 Pd1 Pd2 P2 -122.67(7) 2_665 .
Tl1 Pd1 Pd2 P2 132.99(6) . .
Pd1 Pd1 Pd2 P2 130.05(7) 3_565 .
Pd1 Pd1 Pd2 P2 -174.83(6) 2_665 .
C2 Pd1 Pd2 Pd1 153.2(4) . 3_565
C1 Pd1 Pd2 Pd1 -94.2(2) 3_565 3_565
C3 Pd1 Pd2 Pd1 163.4(2) 2_665 3_565
Pd3 Pd1 Pd2 Pd1 -57.89(2) 3_565 3_565
Pd3 Pd1 Pd2 Pd1 84.71(3) . 3_565
Pd2 Pd1 Pd2 Pd1 107.28(2) 2_665 3_565
Tl1 Pd1 Pd2 Pd1 2.943(17) . 3_565
Pd1 Pd1 Pd2 Pd1 55.114(8) 2_665 3_565
C2 Pd1 Pd2 Pd2 45.9(4) . 2_665
C1 Pd1 Pd2 Pd2 158.6(2) 3_565 2_665
C3 Pd1 Pd2 Pd2 56.1(2) 2_665 2_665
Pd3 Pd1 Pd2 Pd2 -165.17(2) 3_565 2_665
Pd3 Pd1 Pd2 Pd2 -22.57(3) . 2_665
Tl1 Pd1 Pd2 Pd2 -104.33(2) . 2_665
Pd1 Pd1 Pd2 Pd2 -107.28(2) 3_565 2_665
Pd1 Pd1 Pd2 Pd2 -52.163(19) 2_665 2_665
C2 Pd1 Pd2 Pd2 98.0(4) . 3_565
C1 Pd1 Pd2 Pd2 -149.3(2) 3_565 3_565
C3 Pd1 Pd2 Pd2 108.2(2) 2_665 3_565
Pd3 Pd1 Pd2 Pd2 -113.01(2) 3_565 3_565
Pd3 Pd1 Pd2 Pd2 29.59(4) . 3_565
Pd2 Pd1 Pd2 Pd2 52.156(8) 2_665 3_565
Tl1 Pd1 Pd2 Pd2 -52.18(2) . 3_565
Pd1 Pd1 Pd2 Pd2 -55.12(2) 3_565 3_565
Pd1 Pd1 Pd2 Pd2 -0.007(19) 2_665 3_565
C2 Pd1 Pd3 C1 -161.7(4) . .
C1 Pd1 Pd3 C1 135.0(4) 3_565 .
C3 Pd1 Pd3 C1 -95.0(3) 2_665 .
Pd3 Pd1 Pd3 C1 78.8(3) 3_565 .
Pd2 Pd1 Pd3 C1 -64.2(3) 2_665 .
Pd2 Pd1 Pd3 C1 -43.7(3) . .
Tl1 Pd1 Pd3 C1 57.4(3) . .
Pd1 Pd1 Pd3 C1 17.3(3) 3_565 .
Pd1 Pd1 Pd3 C1 -6.3(3) 2_665 .
C1 Pd1 Pd3 C2 -63.3(4) 3_565 .
C3 Pd1 Pd3 C2 66.7(4) 2_665 .
Pd3 Pd1 Pd3 C2 -119.5(3) 3_565 .
Pd2 Pd1 Pd3 C2 97.5(3) 2_665 .
Pd2 Pd1 Pd3 C2 117.9(3) . .
Tl1 Pd1 Pd3 C2 -141.0(3) . .
Pd1 Pd1 Pd3 C2 179.0(3) 3_565 .
Pd1 Pd1 Pd3 C2 155.3(3) 2_665 .
C2 Pd1 Pd3 P1 47.1(3) . .
C1 Pd1 Pd3 P1 -16.2(2) 3_565 .
C3 Pd1 Pd3 P1 113.78(19) 2_665 .
Pd3 Pd1 Pd3 P1 -72.41(7) 3_565 .
Pd2 Pd1 Pd3 P1 144.60(7) 2_665 .
Pd2 Pd1 Pd3 P1 165.04(7) . .
Tl1 Pd1 Pd3 P1 -93.88(7) . .
Pd1 Pd1 Pd3 P1 -133.91(7) 3_565 .
Pd1 Pd1 Pd3 P1 -157.57(7) 2_665 .
C2 Pd1 Pd3 Pd1 -155.3(3) . 2_665
C1 Pd1 Pd3 Pd1 141.4(2) 3_565 2_665
C3 Pd1 Pd3 Pd1 -88.65(18) 2_665 2_665
Pd3 Pd1 Pd3 Pd1 85.16(3) 3_565 2_665
Pd2 Pd1 Pd3 Pd1 -57.831(18) 2_665 2_665
Pd2 Pd1 Pd3 Pd1 -37.39(4) . 2_665
Tl1 Pd1 Pd3 Pd1 63.688(15) . 2_665
Pd1 Pd1 Pd3 Pd1 23.660(16) 3_565 2_665
C2 Pd1 Pd3 Tl1 141.0(3) . .
C1 Pd1 Pd3 Tl1 77.7(2) 3_565 .
C3 Pd1 Pd3 Tl1 -152.34(18) 2_665 .
Pd3 Pd1 Pd3 Tl1 21.48(3) 3_565 .
Pd2 Pd1 Pd3 Tl1 -121.519(19) 2_665 .
Pd2 Pd1 Pd3 Tl1 -101.08(3) . .
Pd1 Pd1 Pd3 Tl1 -40.027(13) 3_565 .
Pd1 Pd1 Pd3 Tl1 -63.688(15) 2_665 .
Pd1 Tl1 Pd3 C1 -48.7(2) 2_665 .
Pd1 Tl1 Pd3 C1 -90.7(2) 3_565 .
Pd1 Tl1 Pd3 C1 -134.3(2) . .
Pd3 Tl1 Pd3 C1 -35.4(2) 2_665 .
Pd3 Tl1 Pd3 C1 -147.4(2) 3_565 .
Pd1 Tl1 Pd3 C2 114.4(2) 2_665 .
Pd1 Tl1 Pd3 C2 72.4(2) 3_565 .
Pd1 Tl1 Pd3 C2 28.8(2) . .
Pd3 Tl1 Pd3 C2 127.7(2) 2_665 .
Pd3 Tl1 Pd3 C2 15.7(2) 3_565 .
Pd1 Tl1 Pd3 P1 -152.39(6) 2_665 .
Pd1 Tl1 Pd3 P1 165.62(6) 3_565 .
Pd1 Tl1 Pd3 P1 122.09(6) . .
Pd3 Tl1 Pd3 P1 -139.02(6) 2_665 .
Pd3 Tl1 Pd3 P1 108.94(6) 3_565 .
Pd1 Tl1 Pd3 Pd1 -41.99(2) 3_565 2_665
Pd1 Tl1 Pd3 Pd1 -85.52(3) . 2_665
Pd3 Tl1 Pd3 Pd1 13.36(2) 2_665 2_665
Pd3 Tl1 Pd3 Pd1 -98.669(18) 3_565 2_665
Pd1 Tl1 Pd3 Pd1 85.52(3) 2_665 .
Pd1 Tl1 Pd3 Pd1 43.53(2) 3_565 .
Pd3 Tl1 Pd3 Pd1 98.886(18) 2_665 .
Pd3 Tl1 Pd3 Pd1 -13.15(2) 3_565 .
C1 Pd3 P1 C10 102.7(3) . .
C2 Pd3 P1 C10 -68.4(3) . .
Pd1 Pd3 P1 C10 131.4(2) 2_665 .
Pd1 Pd3 P1 C10 -102.2(2) . .
Tl1 Pd3 P1 C10 -167.0(2) . .
C1 Pd3 P1 C16 -18.4(3) . .
C2 Pd3 P1 C16 170.4(3) . .
Pd1 Pd3 P1 C16 10.3(3) 2_665 .
Pd1 Pd3 P1 C16 136.7(2) . .
Tl1 Pd3 P1 C16 71.8(2) . .
C1 Pd3 P1 C22 -138.3(3) . .
C2 Pd3 P1 C22 50.6(3) . .
Pd1 Pd3 P1 C22 -109.6(2) 2_665 .
Pd1 Pd3 P1 C22 16.8(2) . .
Tl1 Pd3 P1 C22 -48.03(19) . .
C3 Pd2 P2 C36 12.0(3) . .
C3 Pd2 P2 C36 167.0(3) 2_665 .
Pd1 Pd2 P2 C36 -42.7(2) 3_565 .
Pd1 Pd2 P2 C36 -141.07(18) . .
Pd2 Pd2 P2 C36 136.54(18) 2_665 .
Pd2 Pd2 P2 C36 46.5(2) 3_565 .
C3 Pd2 P2 C30 -106.6(3) . .
C3 Pd2 P2 C30 48.3(3) 2_665 .
Pd1 Pd2 P2 C30 -161.34(19) 3_565 .
Pd1 Pd2 P2 C30 100.3(2) . .
Pd2 Pd2 P2 C30 17.9(2) 2_665 .
Pd2 Pd2 P2 C30 -72.2(2) 3_565 .
C3 Pd2 P2 C42 134.6(3) . .
C3 Pd2 P2 C42 -70.4(3) 2_665 .
Pd1 Pd2 P2 C42 79.9(2) 3_565 .
Pd1 Pd2 P2 C42 -18.5(2) . .
Pd2 Pd2 P2 C42 -100.9(2) 2_665 .
Pd2 Pd2 P2 C42 169.0(2) 3_565 .
C54 O51 C51 C52 20(2) . .
O51 C51 C52 C53 10(2) . .
C51 C52 C53 C54 -35(2) . .
C51 O51 C54 C53 -41.4(19) . .
C52 C53 C54 O51 47.3(19) . .
F5 P3 F1 F3 61(5) . 3_565
F5 P3 F1 F3 -38(7) 2_665 3_565
F5 P3 F1 F3 -177(4) 3_565 3_565
F6 P3 F1 F3 69(6) 3_565 3_565
F6 P3 F1 F3 -31(5) . 3_565
F6 P3 F1 F3 -150(4) 2_665 3_565
F4 P3 F1 F3 38(3) 2_665 3_565
F4 P3 F1 F3 152(5) . 3_565
F4 P3 F1 F3 -108(6) 3_565 3_565
F1 P3 F1 F3 157(7) 3_565 3_565
F1 P3 F1 F3 -128(7) 2_665 3_565
F3 P3 F1 F3 142(6) 2_665 3_565
F3 P3 F1 F3 -120(5) . 3_565
F2 P3 F1 F3 57(7) 2_665 3_565
F2 P3 F1 F3 -21(7) 3_565 3_565
F2 P3 F1 F3 -111(16) . 3_565
F5 P3 F1 F4 23(5) . 2_665
F5 P3 F1 F4 -75(6) 2_665 2_665
F5 P3 F1 F4 146(4) 3_565 2_665
F6 P3 F1 F4 32(6) 3_565 2_665
F6 P3 F1 F4 -68(5) . 2_665
F6 P3 F1 F4 172(4) 2_665 2_665
F4 P3 F1 F4 114(4) . 2_665
F4 P3 F1 F4 -146(6) 3_565 2_665
F1 P3 F1 F4 120(7) 3_565 2_665
F1 P3 F1 F4 -165(7) 2_665 2_665
F3 P3 F1 F4 -38(3) 3_565 2_665
F3 P3 F1 F4 104(6) 2_665 2_665
F3 P3 F1 F4 -158(4) . 2_665
F2 P3 F1 F4 20(6) 2_665 2_665
F2 P3 F1 F4 -59(6) 3_565 2_665
F2 P3 F1 F4 -148(15) . 2_665
F5 P3 F2 F6 140(6) . 2_665
F5 P3 F2 F6 -122(7) 2_665 2_665
F5 P3 F2 F6 30(4) 3_565 2_665
F6 P3 F2 F6 132(6) 3_565 2_665
F6 P3 F2 F6 -128(5) . 2_665
F4 P3 F2 F6 171(5) 2_665 2_665
F4 P3 F2 F6 49(6) . 2_665
F4 P3 F2 F6 -51(7) 3_565 2_665
F1 P3 F2 F6 -48(18) . 2_665
F1 P3 F2 F6 42(7) 3_565 2_665
F1 P3 F2 F6 -32(7) 2_665 2_665
F3 P3 F2 F6 -146(4) 3_565 2_665
F3 P3 F2 F6 59(7) 2_665 2_665
F3 P3 F2 F6 -39(6) . 2_665
F2 P3 F2 F6 143(8) 2_665 2_665
F2 P3 F2 F6 -139(7) 3_565 2_665
F5 P3 F2 F5 110(6) . 3_565
F5 P3 F2 F5 -152(8) 2_665 3_565
F6 P3 F2 F5 101(7) 3_565 3_565
F6 P3 F2 F5 -159(6) . 3_565
F6 P3 F2 F5 -30(4) 2_665 3_565
F4 P3 F2 F5 140(4) 2_665 3_565
F4 P3 F2 F5 19(6) . 3_565
F4 P3 F2 F5 -81(7) 3_565 3_565
F1 P3 F2 F5 -79(18) . 3_565
F1 P3 F2 F5 11(8) 3_565 3_565
F1 P3 F2 F5 -62(8) 2_665 3_565
F3 P3 F2 F5 -176(5) 3_565 3_565
F3 P3 F2 F5 28(8) 2_665 3_565
F3 P3 F2 F5 -69(6) . 3_565
F2 P3 F2 F5 113(8) 2_665 3_565
F2 P3 F2 F5 -170(8) 3_565 3_565
F5 P3 F3 F4 173(100) . 3_565
F5 P3 F3 F4 -35(10) 2_665 3_565
F5 P3 F3 F4 -135(12) 3_565 3_565
F4 P3 F3 F4 53(10) 2_665 3_565
F4 P3 F3 F4 153(12) . 3_565
F1 P3 F3 F4 62(12) . 3_565
F1 P3 F3 F4 131(12) 3_565 3_565
F1 P3 F3 F4 83(7) 2_665 3_565
F3 P3 F3 F4 45(12) 3_565 3_565
F3 P3 F3 F4 144(10) 2_665 3_565
F2 P3 F3 F4 -111(7) 2_665 3_565
F2 P3 F3 F4 -44(12) 3_565 3_565
F2 P3 F3 F4 -117(12) . 3_565
F5 P3 F3 F1 90(81) . 2_665
F5 P3 F3 F1 -118(5) 2_665 2_665
F5 P3 F3 F1 142(7) 3_565 2_665
F6 P3 F3 F1 96(12) 3_565 2_665
F6 P3 F3 F1 -112(7) . 2_665
F6 P3 F3 F1 148(6) 2_665 2_665
F4 P3 F3 F1 -30(5) 2_665 2_665
F4 P3 F3 F1 70(7) . 2_665
F4 P3 F3 F1 -83(7) 3_565 2_665
F1 P3 F3 F1 -21(7) . 2_665
F1 P3 F3 F1 49(7) 3_565 2_665
F3 P3 F3 F1 -38(7) 3_565 2_665
F3 P3 F3 F1 61(5) 2_665 2_665
F2 P3 F3 F1 166(4) 2_665 2_665
F2 P3 F3 F1 -127(7) 3_565 2_665
F2 P3 F3 F1 160(6) . 2_665
F6 P3 F4 F3 49(10) 3_565 2_665
F6 P3 F4 F3 -176(100) . 2_665
F6 P3 F4 F3 151(12) 2_665 2_665
F4 P3 F4 F3 -27(12) 2_665 2_665
F4 P3 F4 F3 -130(10) 3_565 2_665
F1 P3 F4 F3 -48(12) . 2_665
F1 P3 F4 F3 -62(7) 3_565 2_665
F1 P3 F4 F3 -117(12) 2_665 2_665
F3 P3 F4 F3 -38(10) 3_565 2_665
F3 P3 F4 F3 -136(12) . 2_665
F2 P3 F4 F3 63(12) 2_665 2_665
F2 P3 F4 F3 110(8) 3_565 2_665
F2 P3 F4 F3 137(12) . 2_665
F5 P3 F4 F1 106(6) . 3_565
F5 P3 F4 F1 -118(10) 2_665 3_565
F5 P3 F4 F1 -155(5) 3_565 3_565
F6 P3 F4 F1 111(5) 3_565 3_565
F6 P3 F4 F1 -114(31) . 3_565
F6 P3 F4 F1 -148(6) 2_665 3_565
F4 P3 F4 F1 35(6) 2_665 3_565
F4 P3 F4 F1 -68(4) 3_565 3_565
F1 P3 F4 F1 14(6) . 3_565
F1 P3 F4 F1 -55(6) 2_665 3_565
F3 P3 F4 F1 24(5) 3_565 3_565
F3 P3 F4 F1 62(7) 2_665 3_565
F3 P3 F4 F1 -74(6) . 3_565
F2 P3 F4 F1 125(6) 2_665 3_565
F2 P3 F4 F1 172(4) 3_565 3_565
F2 P3 F4 F1 -161(6) . 3_565
F5 P3 F5 F6 -145(16) 2_665 3_565
F5 P3 F5 F6 -45(19) 3_565 3_565
F6 P3 F5 F6 -152(19) . 3_565
F6 P3 F5 F6 -51(17) 2_665 3_565
F1 P3 F5 F6 118(18) . 3_565
F1 P3 F5 F6 48(18) 3_565 3_565
F1 P3 F5 F6 93(14) 2_665 3_565
F3 P3 F5 F6 135(19) 3_565 3_565
F3 P3 F5 F6 36(17) 2_665 3_565
F3 P3 F5 F6 6(88) . 3_565
F2 P3 F5 F6 -73(13) 2_665 3_565
F2 P3 F5 F6 -136(19) 3_565 3_565
F2 P3 F5 F6 -63(19) . 3_565
F5 P3 F5 F2 -72(6) 2_665 2_665
F5 P3 F5 F2 28(8) 3_565 2_665
F6 P3 F5 F2 73(13) 3_565 2_665
F6 P3 F5 F2 -79(8) . 2_665
F6 P3 F5 F2 22(6) 2_665 2_665
F4 P3 F5 F2 -160(7) 2_665 2_665
F4 P3 F5 F2 99(8) . 2_665
F4 P3 F5 F2 -108(10) 3_565 2_665
F1 P3 F5 F2 -169(7) . 2_665
F1 P3 F5 F2 121(8) 3_565 2_665
F1 P3 F5 F2 166(4) 2_665 2_665
F3 P3 F5 F2 -152(8) 3_565 2_665
F3 P3 F5 F2 109(6) 2_665 2_665
F3 P3 F5 F2 79(82) . 2_665
F2 P3 F5 F2 -64(8) 3_565 2_665
F2 P3 F5 F2 10(8) . 2_665
F5 P3 F6 F5 135(19) . 2_665
F5 P3 F6 F5 36(17) 3_565 2_665
F6 P3 F6 F5 131(16) 3_565 2_665
F6 P3 F6 F5 29(19) 2_665 2_665
F4 P3 F6 F5 -153(19) 2_665 2_665
F4 P3 F6 F5 -4(40) . 2_665
F4 P3 F6 F5 -51(17) 3_565 2_665
F1 P3 F6 F5 -132(19) . 2_665
F1 P3 F6 F5 -112(14) 3_565 2_665
F1 P3 F6 F5 -63(19) 2_665 2_665
F2 P3 F6 F5 117(18) 2_665 2_665
F2 P3 F6 F5 78(13) 3_565 2_665
F2 P3 F6 F5 43(19) . 2_665
F5 P3 F6 F2 57(7) . 3_565
F5 P3 F6 F2 -78(13) 2_665 3_565
F5 P3 F6 F2 -42(6) 3_565 3_565
F6 P3 F6 F2 53(5) 3_565 3_565
F6 P3 F6 F2 -49(7) 2_665 3_565
F4 P3 F6 F2 128(7) 2_665 3_565
F4 P3 F6 F2 -82(33) . 3_565
F4 P3 F6 F2 -129(6) 3_565 3_565
F1 P3 F6 F2 150(7) . 3_565
F1 P3 F6 F2 170(4) 3_565 3_565
F1 P3 F6 F2 -141(7) 2_665 3_565
F3 P3 F6 F2 139(6) 3_565 3_565
F3 P3 F6 F2 103(12) 2_665 3_565
F3 P3 F6 F2 -122(7) . 3_565
F2 P3 F6 F2 39(7) 2_665 3_565
F2 P3 F6 F2 -35(7) . 3_565
P3A P3A F1A F1A 160(15) 3_565 2_665
P3A P3A F1A F1A -139(15) 2_665 2_665
F5A P3A F1A F1A -24(7) 3_565 2_665
F6A P3A F1A F1A 3(7) 2_665 2_665
F5A P3A F1A F1A 104(7) 2_665 2_665
F2A P3A F1A F1A 22(100) . 2_665
F5A P3A F1A F1A -144(7) . 2_665
F6A P3A F1A F1A 127(7) . 2_665
F3A P3A F1A F1A 37(7) . 2_665
F4A P3A F1A F1A 70(7) 3_565 2_665
F4A P3A F1A F1A -53(7) . 2_665
F1A P3A F1A F1A -61.4(3) 3_565 2_665
F2A P3A F1A F1A 137(7) 3_565 2_665
F6A P3A F1A F1A -124(7) 3_565 2_665
F2A P3A F1A F1A -160(7) 2_665 2_665
F3A P3A F1A F1A -86(7) 2_665 2_665
F4A P3A F1A F1A -168(7) 2_665 2_665
F3A P3A F1A F1A 158(7) 3_565 2_665
P3A P3A F1A F1A -138(15) 3_565 3_565
P3A P3A F1A F1A -78(15) 2_665 3_565
F5A P3A F1A F1A 37(7) 3_565 3_565
F6A P3A F1A F1A 65(7) 2_665 3_565
F5A P3A F1A F1A 166(7) 2_665 3_565
F2A P3A F1A F1A 83(100) . 3_565
F1A P3A F1A F1A 61.4(3) 2_665 3_565
F5A P3A F1A F1A -82(7) . 3_565
F6A P3A F1A F1A -172(7) . 3_565
F3A P3A F1A F1A 98(7) . 3_565
F4A P3A F1A F1A 132(7) 3_565 3_565
F4A P3A F1A F1A 8(7) . 3_565
F2A P3A F1A F1A -161(7) 3_565 3_565
F6A P3A F1A F1A -63(7) 3_565 3_565
F2A P3A F1A F1A -99(7) 2_665 3_565
F3A P3A F1A F1A -25(6) 2_665 3_565
F4A P3A F1A F1A -107(7) 2_665 3_565
F3A P3A F1A F1A -140(7) 3_565 3_565
P3A P3A F1A P3A 60.8(5) 2_665 3_565
F5A P3A F1A P3A 176(13) 3_565 3_565
F6A P3A F1A P3A -157(13) 2_665 3_565
F5A P3A F1A P3A -56(12) 2_665 3_565
F2A P3A F1A P3A -139(100) . 3_565
F1A P3A F1A P3A -160(15) 2_665 3_565
F5A P3A F1A P3A 56(11) . 3_565
F6A P3A F1A P3A -33(12) . 3_565
F3A P3A F1A P3A -123(12) . 3_565
F4A P3A F1A P3A -90(12) 3_565 3_565
F4A P3A F1A P3A 147(12) . 3_565
F1A P3A F1A P3A 138(15) 3_565 3_565
C2 Pd3 C1 O1 123.2(14) . .
P1 Pd3 C1 O1 -25.0(14) . .
Pd1 Pd3 C1 O1 170.5(15) 2_665 .
Pd1 Pd3 C1 O1 177.9(12) . .
Tl1 Pd3 C1 O1 -136.9(14) . .
C2 Pd3 C1 Pd1 -47.2(11) . 2_665
P1 Pd3 C1 Pd1 164.48(12) . 2_665
Pd1 Pd3 C1 Pd1 7.4(3) . 2_665
Tl1 Pd3 C1 Pd1 52.59(15) . 2_665
C1 Pd3 C2 O2 -109.5(14) . .
P1 Pd3 C2 O2 39.9(13) . .
Pd1 Pd3 C2 O2 -149.7(12) 2_665 .
Pd1 Pd3 C2 O2 -175.2(15) . .
Tl1 Pd3 C2 O2 152.6(13) . .
C1 Pd3 C2 Pd1 65.7(11) . .
P1 Pd3 C2 Pd1 -144.9(2) . .
Pd1 Pd3 C2 Pd1 25.5(3) 2_665 .
Tl1 Pd3 C2 Pd1 -32.2(2) . .
C1 Pd1 C2 O2 -55.5(10) 3_565 .
C3 Pd1 C2 O2 55.0(10) 2_665 .
Pd3 Pd1 C2 O2 -69.1(10) 3_565 .
Pd3 Pd1 C2 O2 176.4(11) . .
Pd2 Pd1 C2 O2 101.9(9) 2_665 .
Pd2 Pd1 C2 O2 62.5(11) . .
Tl1 Pd1 C2 O2 -146.0(9) . .
Pd1 Pd1 C2 O2 174.0(6) 3_565 .
Pd1 Pd1 C2 O2 156.4(9) 2_665 .
C1 Pd1 C2 Pd3 128.2(3) 3_565 .
C3 Pd1 C2 Pd3 -121.4(3) 2_665 .
Pd3 Pd1 C2 Pd3 114.5(3) 3_565 .
Pd2 Pd1 C2 Pd3 -74.5(2) 2_665 .
Pd2 Pd1 C2 Pd3 -113.9(2) . .
Tl1 Pd1 C2 Pd3 37.6(3) . .
Pd1 Pd1 C2 Pd3 -2.3(8) 3_565 .
Pd1 Pd1 C2 Pd3 -20.0(2) 2_665 .
C3 Pd2 C3 O3 -130.1(6) 2_665 .
P2 Pd2 C3 O3 -14.2(8) . .
Pd1 Pd2 C3 O3 122.5(8) 3_565 .
Pd1 Pd2 C3 O3 140.6(7) . .
Pd2 Pd2 C3 O3 -155.1(7) 2_665 .
Pd2 Pd2 C3 O3 -163.0(9) 3_565 .
C3 Pd2 C3 Pd2 32.8(8) 2_665 3_565
P2 Pd2 C3 Pd2 148.82(15) . 3_565
Pd1 Pd2 C3 Pd2 -74.49(18) 3_565 3_565
Pd1 Pd2 C3 Pd2 -56.4(3) . 3_565
Pd2 Pd2 C3 Pd2 7.9(2) 2_665 3_565
C3 Pd2 C3 Pd1 107.3(7) 2_665 3_565
P2 Pd2 C3 Pd1 -136.69(10) . 3_565
Pd1 Pd2 C3 Pd1 18.1(2) . 3_565
Pd2 Pd2 C3 Pd1 82.41(12) 2_665 3_565
Pd2 Pd2 C3 Pd1 74.49(18) 3_565 3_565
C16 P1 C10 C11 129.1(3) . .
C22 P1 C10 C11 -118.4(3) . .
Pd3 P1 C10 C11 -0.5(3) . .
C16 P1 C10 C15 -55.1(4) . .
C22 P1 C10 C15 57.4(4) . .
Pd3 P1 C10 C15 175.2(2) . .
C15 C10 C11 C12 0.0 . .
P1 C10 C11 C12 175.8(4) . .
C10 C11 C12 C13 0.0 . .
C11 C12 C13 C14 0.0 . .
C12 C13 C14 C15 0.0 . .
C13 C14 C15 C10 0.0 . .
C11 C10 C15 C14 0.0 . .
P1 C10 C15 C14 -175.7(4) . .
C10 P1 C16 C17 -59.0(4) . .
C22 P1 C16 C17 -172.2(3) . .
Pd3 P1 C16 C17 68.6(3) . .
C10 P1 C16 C21 123.2(4) . .
C22 P1 C16 C21 10.1(4) . .
Pd3 P1 C16 C21 -109.1(3) . .
C21 C16 C17 C18 0.0 . .
P1 C16 C17 C18 -177.8(4) . .
C16 C17 C18 C19 0.0 . .
C17 C18 C19 C20 0.0 . .
C18 C19 C20 C21 0.0 . .
C19 C20 C21 C16 0.0 . .
C17 C16 C21 C20 0.0 . .
P1 C16 C21 C20 177.7(4) . .
C10 P1 C22 C23 10.1(4) . .
C16 P1 C22 C23 119.3(3) . .
Pd3 P1 C22 C23 -113.7(3) . .
C10 P1 C22 C27 -177.4(3) . .
C16 P1 C22 C27 -68.1(3) . .
Pd3 P1 C22 C27 58.9(3) . .
C27 C22 C23 C24 0.0 . .
P1 C22 C23 C24 172.4(4) . .
C22 C23 C24 C25 0.0 . .
C23 C24 C25 C26 0.0 . .
C24 C25 C26 C27 0.0 . .
C25 C26 C27 C22 0.0 . .
C23 C22 C27 C26 0.0 . .
P1 C22 C27 C26 -172.8(4) . .
C36 P2 C30 C31 -106.1(3) . .
C42 P2 C30 C31 146.3(3) . .
Pd2 P2 C30 C31 21.3(4) . .
C36 P2 C30 C35 72.5(4) . .
C42 P2 C30 C35 -35.1(4) . .
Pd2 P2 C30 C35 -160.1(3) . .
C35 C30 C31 C32 0.0 . .
P2 C30 C31 C32 178.6(4) . .
C30 C31 C32 C33 0.0 . .
C31 C32 C33 C34 0.0 . .
C32 C33 C34 C35 0.0 . .
C33 C34 C35 C30 0.0 . .
C31 C30 C35 C34 0.0 . .
P2 C30 C35 C34 -178.6(4) . .
C30 P2 C36 C37 32.0(4) . .
C42 P2 C36 C37 139.5(3) . .
Pd2 P2 C36 C37 -92.4(3) . .
C30 P2 C36 C41 -152.0(3) . .
C42 P2 C36 C41 -44.6(4) . .
Pd2 P2 C36 C41 83.5(3) . .
C41 C36 C37 C38 0.0 . .
P2 C36 C37 C38 175.9(4) . .
C36 C37 C38 C39 0.0 . .
C37 C38 C39 C40 0.0 . .
C38 C39 C40 C41 0.0 . .
C39 C40 C41 C36 0.0 . .
C37 C36 C41 C40 0.0 . .
P2 C36 C41 C40 -175.9(4) . .
C36 P2 C42 C43 -32.5(4) . .
C30 P2 C42 C43 73.7(4) . .
Pd2 P2 C42 C43 -162.3(3) . .
C36 P2 C42 C47 152.1(3) . .
C30 P2 C42 C47 -101.7(3) . .
Pd2 P2 C42 C47 22.3(4) . .
C47 C42 C43 C44 0.0 . .
P2 C42 C43 C44 -175.3(4) . .
C42 C43 C44 C45 0.0 . .
C43 C44 C45 C46 0.0 . .
C44 C45 C46 C47 0.0 . .
C45 C46 C47 C42 0.0 . .
C43 C42 C47 C46 0.0 . .
P2 C42 C47 C46 175.5(4) . .
