#------------------------------------------------------------------------------
#$Date: 2019-05-15 03:48:35 +0300 (Wed, 15 May 2019) $
#$Revision: 215154 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/12/34/7123457.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7123457
loop_
_publ_author_name
'Nan, Zi-Ang'
'Xiao, Ying'
'Liu, Xiyan'
'Wang, Tan'
'Cheng, Xiaoling'
'Yang, Yang'
'Lei, Zhen'
'Wang, Quan-Ming'
_publ_section_title
;
 Monitoring the Growth of Ag-S Clusters through Crystallization of
 Intermediate Clusters
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/C9CC03533H
_journal_year                    2019
_chemical_formula_moiety
'C92 H165 Ag31 F24 N4 O16 S20, C2 N, C O, O, C'
_chemical_formula_sum            'C92 H0.5 Ag31 F24 N4 O16 S20'
_chemical_formula_weight         5858.63
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_date             2015-02-05
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2019-03-31 deposited with the CCDC.    2019-05-14 downloaded from the CCDC.
;
_cell_angle_alpha                97.942(2)
_cell_angle_beta                 95.315(2)
_cell_angle_gamma                110.522(2)
_cell_formula_units_Z            2
_cell_length_a                   14.9808(4)
_cell_length_b                   19.2453(5)
_cell_length_c                   32.5658(8)
_cell_measurement_temperature    293(2)
_cell_volume                     8607.5(4)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.847
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0397
_diffrn_reflns_av_unetI/netI     0.0673
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.847
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            77681
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.847
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         29.115
_diffrn_reflns_theta_min         2.988
_exptl_absorpt_coefficient_mu    3.743
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.260
_exptl_crystal_description       block
_exptl_crystal_F_000             5403
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.15
_refine_diff_density_max         2.446
_refine_diff_density_min         -1.378
_refine_diff_density_rms         0.206
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.151
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1767
_refine_ls_number_reflns         39238
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.151
_refine_ls_R_factor_all          0.0947
_refine_ls_R_factor_gt           0.0682
_refine_ls_shift/su_max          0.093
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[σ²(Fo²)+(0.0279P)²+130.8195P]
 where P=(Fo²+2Fc²)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1411
_refine_ls_wR_factor_ref         0.1513
_reflns_Friedel_coverage         0.000
_reflns_number_gt                29544
_reflns_number_total             39238
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c9cc03533h2.cif
_cod_data_source_block           p_CCDC1
_cod_original_formula_sum        'C92 H0.50 Ag31 F24 N4 O16 S20'
_cod_database_code               7123457
_shelxl_version_number           2013-2
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.5 times of:
  All C(H,H,H) groups
2.a Idealised Me refined as rotating group:
 C12(H12A,H12B,H12C), C10(H10A,H10B,H10C), C19(H19A,H19B,H19C), C27(H27A,H27B,
 H27C), C30(H30A,H30B,H30C), C25(H25A,H25B,H25C), C16(H16A,H16B,H16C), C31(H31A,
 H31B,H31C), C21(H21A,H21B,H21C), C22(H22A,H22B,H22C), C26(H26A,H26B,H26C),
 C24(H24A,H24B,H24C), C18(H18A,H18B,H18C), C43(H43A,H43B,H43C), C36(H36A,H36B,
 H36C), C39(H39A,H39B,H39C), C35(H35A,H35B,H35C), C40(H40A,H40B,H40C), C37(H37A,
 H37B,H37C), C41(H41A,H41B,H41C), C34(H34A,H34B,H34C), C32(H32A,H32B,H32C),
 C45(H45A,H45B,H45C), C53(H53A,H53B,H53C), C52(H52A,H52B,H52C), C58(H58A,H58B,
 H58C), C50(H50A,H50B,H50C), C51(H51A,H51B,H51C), C56(H56A,H56B,H56C), C47(H47A,
 H47B,H47C), C54(H54A,H54B,H54C), C46(H46A,H46B,H46C), C57(H57A,H57B,H57C),
 C59(H59A,H59B,H59C), C67(H67A,H67B,H67C), C61(H61A,H61B,H61C), C64(H64A,H64B,
 H64C), C63(H63A,H63B,H63C), C69(H69A,H69B,H69C), C204(H20A,H20B,H20C),
 C203(H20D,H20E,H20F), C65(H65A,H65B,H65C), C70(H70A,H70B,H70C), C206(H20G,H20H,
 H20I), C74(H74A,H74B,H74C), C72(H72A,H72B,H72C), C71(H71A,H71B,H71C), C76(H76A,
 H76B,H76C), C75(H75A,H75B,H75C), C208(H20J,H20K,H20L), C80(H80A,H80B,H80C),
 C81(H81A,H81B,H81C), C79(H79A,H79B,H79C), C77(H77A,H77B,H77C), C82(H82A,H82B,
 H82C)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
Ag1 Ag 0.52050(6) 0.15120(4) 0.77955(2) 0.02636(16) Uani 1 1 d .
Ag3 Ag 0.59297(6) 0.30585(4) 0.76260(2) 0.02669(17) Uani 1 1 d .
Ag2 Ag 0.45392(6) 0.18483(4) 0.70228(2) 0.02847(17) Uani 1 1 d .
Ag11 Ag 0.60405(7) 0.26467(5) 0.94952(3) 0.03379(19) Uani 1 1 d .
Ag9 Ag 0.47447(6) 0.40663(5) 0.74351(3) 0.03365(19) Uani 1 1 d .
Ag14 Ag 0.33401(6) 0.36795(5) 0.60312(3) 0.03461(19) Uani 1 1 d .
Ag5 Ag 0.48998(6) 0.18974(4) 0.86478(3) 0.03154(18) Uani 1 1 d .
Ag10 Ag 0.65218(6) 0.41699(5) 0.93149(3) 0.03437(19) Uani 1 1 d .
Ag4 Ag 0.54859(7) 0.36492(5) 0.84308(3) 0.0351(2) Uani 1 1 d .
Ag18 Ag 0.35234(6) -0.11367(5) 0.68931(3) 0.03333(19) Uani 1 1 d .
Ag8 Ag 0.31883(7) 0.25344(5) 0.66338(3) 0.0361(2) Uani 1 1 d .
Ag13 Ag 0.14231(7) -0.11041(5) 0.65693(3) 0.0362(2) Uani 1 1 d .
Ag20 Ag 0.49650(7) 0.24337(5) 0.60807(3) 0.0380(2) Uani 1 1 d .
Ag6 Ag 0.31554(7) 0.02517(5) 0.78348(3) 0.03483(19) Uani 1 1 d .
Ag30 Ag 0.66331(6) 0.25740(6) 0.67965(3) 0.0391(2) Uani 1 1 d .
Ag17 Ag 0.42038(8) -0.06876(5) 0.82615(3) 0.0424(2) Uani 1 1 d .
Ag23 Ag 0.76581(7) 0.52428(5) 0.83031(3) 0.0386(2) Uani 1 1 d .
Ag24 Ag 0.83272(7) 0.38870(5) 0.87310(3) 0.0391(2) Uani 1 1 d .
Ag7 Ag 0.22817(7) 0.05541(5) 0.69379(3) 0.0366(2) Uani 1 1 d .
Ag25 Ag 0.77273(7) 0.22754(5) 0.88802(3) 0.0383(2) Uani 1 1 d .
Ag26 Ag 0.52663(7) -0.01053(5) 0.75622(3) 0.0380(2) Uani 1 1 d .
Ag16 Ag 0.57147(7) 0.04676(5) 0.88721(3) 0.0391(2) Uani 1 1 d .
Ag15 Ag 0.47208(6) 0.49298(5) 0.67006(3) 0.0361(2) Uani 1 1 d .
Ag21 Ag 0.61454(7) 0.45876(5) 0.61117(3) 0.0414(2) Uani 1 1 d .
Ag19 Ag 0.38524(7) 0.04228(5) 0.62415(3) 0.0430(2) Uani 1 1 d .
Ag29 Ag 0.58959(6) 0.09533(5) 0.69475(3) 0.0395(2) Uani 1 1 d .
Ag22 Ag 0.66174(8) 0.54515(5) 0.75481(3) 0.0457(2) Uani 1 1 d .
Ag12 Ag 0.19130(7) -0.16348(6) 0.74328(3) 0.0445(2) Uani 1 1 d .
Ag31 Ag 0.80570(8) 0.33198(5) 0.77541(4) 0.0524(3) Uani 1 1 d .
Ag27 Ag 0.70620(7) 0.42178(6) 0.70273(3) 0.0505(3) Uani 1 1 d .
Ag28 Ag 0.71647(8) 0.15175(7) 0.79214(4) 0.0573(3) Uani 1 1 d .
S5 S 0.39922(19) 0.05345(13) 0.85642(8) 0.0241(5) Uani 1 1 d .
S3 S 0.53678(18) 0.31912(14) 0.69239(8) 0.0242(5) Uani 1 1 d .
S20 S 0.75530(18) 0.20394(15) 0.72820(8) 0.0256(5) Uani 1 1 d .
S1 S 0.63066(17) 0.26423(13) 0.82725(7) 0.0211(5) Uani 1 1 d .
S2 S 0.42141(17) 0.05489(13) 0.72091(8) 0.0217(5) Uani 1 1 d .
S9 S 0.57448(19) 0.47925(14) 0.81088(8) 0.0255(5) Uani 1 1 d .
S6 S 0.15858(18) -0.04524(14) 0.73341(8) 0.0268(5) Uani 1 1 d .
S19 S 0.54029(19) 0.13662(14) 0.61715(8) 0.0265(5) Uani 1 1 d .
S8 S 0.33822(18) 0.38416(14) 0.68537(8) 0.0252(5) Uani 1 1 d .
S16 S 0.81922(19) 0.46009(14) 0.76972(9) 0.0296(6) Uani 1 1 d .
S4 S 0.4929(2) 0.31296(14) 0.91053(8) 0.0278(5) Uani 1 1 d .
S15 S 0.6458(2) 0.54729(14) 0.67955(8) 0.0278(5) Uani 1 1 d .
S13 S 0.2896(2) -0.08936(14) 0.62494(8) 0.0274(5) Uani 1 1 d .
S14 S 0.4748(2) 0.34468(15) 0.57932(8) 0.0301(6) Uani 1 1 d .
S11 S 0.6720(2) 0.16875(14) 0.93512(8) 0.0281(5) Uani 1 1 d .
S10 S 0.7865(2) 0.48927(15) 0.90134(8) 0.0310(6) Uani 1 1 d .
S7 S 0.2656(2) 0.12084(15) 0.63535(10) 0.0338(6) Uani 1 1 d .
S12 S 0.3642(2) -0.15090(14) 0.75719(8) 0.0287(6) Uani 1 1 d .
S18 S 0.6480(2) 0.03750(15) 0.82046(9) 0.0297(6) Uani 1 1 d .
O10 O 0.6812(7) 0.4503(5) 1.0057(3) 0.051(2) Uani 1 1 d .
O13 O 0.7813(7) 0.3165(5) 0.6394(3) 0.055(3) Uani 1 1 d .
O9 O 0.6366(7) -0.0028(5) 0.6665(3) 0.050(2) Uani 1 1 d .
O3 O 0.7582(8) 0.6706(6) 0.7918(3) 0.062(3) Uani 1 1 d .
O2 O 0.3124(8) 0.4761(5) 0.5818(3) 0.055(3) Uani 1 1 d .
O8 O 0.5459(7) -0.0917(5) 0.6982(3) 0.043(2) Uani 1 1 d .
O12 O 0.7813(8) 0.4341(5) 0.6411(3) 0.055(3) Uani 1 1 d .
O6 O 0.4399(9) -0.1429(5) 0.8732(3) 0.067(3) Uani 1 1 d .
O7 O 0.5508(7) -0.0541(5) 0.9223(3) 0.053(2) Uani 1 1 d .
C9 C 0.5184(8) 0.5420(6) 0.8387(4) 0.033(2) Uani 1 1 d .
C11 C 0.3173(8) 0.0327(6) 0.8972(3) 0.030(2) Uani 1 1 d .
C13 C 0.5796(8) 0.1062(6) 0.5672(3) 0.029(2) Uani 1 1 d .
C4 C 0.6793(9) 0.6462(6) 0.6708(4) 0.033(3) Uani 1 1 d .
O1 O 0.3905(7) 0.5617(5) 0.6399(3) 0.052(2) Uani 1 1 d .
C3 C 0.9428(8) 0.5213(7) 0.7628(4) 0.036(3) Uani 1 1 d .
C8 C 0.2333(7) 0.4072(6) 0.7019(4) 0.030(2) Uani 1 1 d .
O4 O 0.8425(9) 0.6547(5) 0.8469(3) 0.073(3) Uani 1 1 d .
C5 C 0.4631(8) 0.3301(6) 0.5210(3) 0.033(2) Uani 1 1 d .
C7 C 0.5989(8) -0.0672(6) 0.6733(4) 0.031(2) Uani 1 1 d .
C12 C 0.2542(9) -0.0503(7) 0.8864(4) 0.043(3) Uani 1 1 d .
H12A H 0.2199 -0.0615 0.8584 0.064 Uiso 1 1 calc GR
H12B H 0.2089 -0.0620 0.9058 0.064 Uiso 1 1 calc GR
H12C H 0.2938 -0.0800 0.8880 0.064 Uiso 1 1 calc GR
C2 C 0.8614(7) 0.1893(6) 0.7071(3) 0.028(2) Uani 1 1 d .
O11 O 0.6774(9) 0.3362(6) 1.0159(3) 0.070(3) Uani 1 1 d .
C10 C 0.5784(12) 0.5767(8) 0.8822(4) 0.057(4) Uani 1 1 d .
H10A H 0.5810 0.5372 0.8968 0.086 Uiso 1 1 calc GR
H10B H 0.5492 0.6067 0.8979 0.086 Uiso 1 1 calc GR
H10C H 0.6426 0.6080 0.8794 0.086 Uiso 1 1 calc GR
C1 C 0.3800(9) -0.2436(6) 0.7520(4) 0.036(3) Uani 1 1 d .
C6 C 0.7451(10) 0.1593(7) 0.9818(4) 0.041(3) Uani 1 1 d .
C19 C 0.2159(9) -0.2407(6) 0.5888(4) 0.045(3) Uani 1 1 d .
H19A H 0.2490 -0.2508 0.6126 0.067 Uiso 1 1 calc GR
H19B H 0.2067 -0.2791 0.5648 0.067 Uiso 1 1 calc GR
H19C H 0.1543 -0.2407 0.5947 0.067 Uiso 1 1 calc GR
C27 C 0.6354(9) 0.6464(6) 0.6270(4) 0.038(3) Uani 1 1 d .
H27A H 0.6621 0.6214 0.6068 0.057 Uiso 1 1 calc GR
H27B H 0.6495 0.6975 0.6231 0.057 Uiso 1 1 calc GR
H27C H 0.5668 0.6202 0.6234 0.057 Uiso 1 1 calc GR
C30 C 0.1552(8) 0.3851(8) 0.6631(4) 0.045(3) Uani 1 1 d .
H30A H 0.1792 0.4161 0.6429 0.068 Uiso 1 1 calc GR
H30B H 0.0988 0.3925 0.6714 0.068 Uiso 1 1 calc GR
H30C H 0.1389 0.3330 0.6510 0.068 Uiso 1 1 calc GR
C15 C 0.0366(8) -0.0537(6) 0.7460(4) 0.037(3) Uani 1 1 d .
C14 C 0.3395(10) 0.5379(7) 0.6060(4) 0.040(3) Uani 1 1 d .
C23 C 0.4080(8) 0.3340(6) 0.9460(4) 0.036(3) Uani 1 1 d .
C25 C 0.2546(9) 0.0791(7) 0.8945(4) 0.043(3) Uani 1 1 d .
H25A H 0.2941 0.1318 0.9020 0.064 Uiso 1 1 calc GR
H25B H 0.2083 0.0664 0.9134 0.064 Uiso 1 1 calc GR
H25C H 0.2215 0.0686 0.8664 0.064 Uiso 1 1 calc GR
C16 C -0.0289(9) -0.1373(7) 0.7350(5) 0.050(3) Uani 1 1 d .
H16A H -0.0347 -0.1549 0.7054 0.075 Uiso 1 1 calc GR
H16B H -0.0915 -0.1433 0.7423 0.075 Uiso 1 1 calc GR
H16C H -0.0015 -0.1660 0.7503 0.075 Uiso 1 1 calc GR
C17 C 0.2754(8) -0.1643(6) 0.5796(3) 0.030(2) Uani 1 1 d .
C29 C 0.1561(9) 0.0964(7) 0.5957(4) 0.041(3) Uani 1 1 d .
C31 C 0.2709(10) 0.4902(7) 0.7196(4) 0.047(3) Uani 1 1 d .
H31A H 0.3176 0.5010 0.7442 0.071 Uiso 1 1 calc GR
H31B H 0.2184 0.5047 0.7270 0.071 Uiso 1 1 calc GR
H31C H 0.3005 0.5181 0.6991 0.071 Uiso 1 1 calc GR
C21 C 0.4975(10) 0.0879(7) 0.5316(4) 0.044(3) Uani 1 1 d .
H21A H 0.4420 0.0479 0.5366 0.067 Uiso 1 1 calc GR
H21B H 0.5166 0.0724 0.5056 0.067 Uiso 1 1 calc GR
H21C H 0.4819 0.1319 0.5301 0.067 Uiso 1 1 calc GR
C22 C 0.6078(10) 0.0408(7) 0.5713(4) 0.046(3) Uani 1 1 d .
H22A H 0.6594 0.0548 0.5943 0.069 Uiso 1 1 calc GR
H22B H 0.6286 0.0251 0.5459 0.069 Uiso 1 1 calc GR
H22C H 0.5534 -0.0001 0.5765 0.069 Uiso 1 1 calc GR
C26 C 0.3792(9) 0.0509(7) 0.9389(3) 0.041(3) Uani 1 1 d .
H26A H 0.4207 0.0226 0.9380 0.061 Uiso 1 1 calc GR
H26B H 0.3391 0.0378 0.9601 0.061 Uiso 1 1 calc GR
H26C H 0.4175 0.1038 0.9452 0.061 Uiso 1 1 calc GR
C28 C 0.7997(9) 0.3785(7) 0.6281(4) 0.040(3) Uani 1 1 d .
C24 C 0.4449(10) 0.4175(7) 0.9621(5) 0.052(4) Uani 1 1 d .
H24A H 0.5089 0.4335 0.9773 0.078 Uiso 1 1 calc GR
H24B H 0.4033 0.4289 0.9804 0.078 Uiso 1 1 calc GR
H24C H 0.4462 0.4435 0.9389 0.078 Uiso 1 1 calc GR
C20 C 0.8822(9) 0.5612(7) 0.9416(4) 0.043(3) Uani 1 1 d .
C18 C 0.2215(10) -0.1459(8) 0.5430(3) 0.045(3) Uani 1 1 d .
H18A H 0.1627 -0.1422 0.5507 0.067 Uiso 1 1 calc GR
H18B H 0.2066 -0.1852 0.5189 0.067 Uiso 1 1 calc GR
H18C H 0.2611 -0.0988 0.5364 0.067 Uiso 1 1 calc GR
O101 O 0.3882(7) 0.2981(6) 0.7878(3) 0.061(3) Uani 1 1 d .
O100 O 0.3141(8) 0.1942(6) 0.7408(4) 0.079(4) Uani 1 1 d .
C43 C 0.7405(9) -0.0487(8) 0.7790(4) 0.044(3) Uani 1 1 d .
H43A H 0.6771 -0.0823 0.7657 0.066 Uiso 1 1 calc GR
H43B H 0.7819 -0.0768 0.7815 0.066 Uiso 1 1 calc GR
H43C H 0.7659 -0.0110 0.7623 0.066 Uiso 1 1 calc GR
C201 C 0.7652(10) 0.5374(7) 0.5423(4) 0.043(3) Uani 1 1 d .
C44 C 0.8140(10) 0.6912(7) 0.8248(4) 0.040(3) Uani 1 1 d .
N1 N 0.7137(10) 0.5165(7) 0.5645(4) 0.060(3) Uani 1 1 d .
C36 C 0.1979(9) 0.3593(8) 0.7350(4) 0.045(3) Uani 1 1 d .
H36A H 0.1727 0.3069 0.7223 0.067 Uiso 1 1 calc GR
H36B H 0.1480 0.3722 0.7467 0.067 Uiso 1 1 calc GR
H36C H 0.2505 0.3687 0.7568 0.067 Uiso 1 1 calc GR
C42 C 0.7348(8) -0.0101(7) 0.8231(4) 0.036(3) Uani 1 1 d .
C39 C 0.3164(11) -0.2904(7) 0.7793(5) 0.059(4) Uani 1 1 d .
H39A H 0.3326 -0.2634 0.8077 0.088 Uiso 1 1 calc GR
H39B H 0.3261 -0.3373 0.7783 0.088 Uiso 1 1 calc GR
H39C H 0.2500 -0.3004 0.7692 0.088 Uiso 1 1 calc GR
C35 C 0.4048(11) 0.2903(8) 0.9809(4) 0.056(4) Uani 1 1 d .
H35A H 0.3811 0.2373 0.9694 0.084 Uiso 1 1 calc GR
H35B H 0.3628 0.3003 0.9994 0.084 Uiso 1 1 calc GR
H35C H 0.4685 0.3052 0.9962 0.084 Uiso 1 1 calc GR
C40 C 0.6400(14) 0.6879(8) 0.7033(4) 0.068(5) Uani 1 1 d .
H40A H 0.5710 0.6643 0.6996 0.101 Uiso 1 1 calc GR
H40B H 0.6577 0.7395 0.6999 0.101 Uiso 1 1 calc GR
H40C H 0.6666 0.6861 0.7310 0.101 Uiso 1 1 calc GR
C37 C 0.8252(10) 0.2339(8) 1.0000(4) 0.049(3) Uani 1 1 d .
H37A H 0.8733 0.2443 0.9818 0.073 Uiso 1 1 calc GR
H37B H 0.8538 0.2316 1.0272 0.073 Uiso 1 1 calc GR
H37C H 0.7996 0.2733 1.0026 0.073 Uiso 1 1 calc GR
C41 C 0.5202(11) 0.6027(8) 0.8136(4) 0.053(4) Uani 1 1 d .
H41A H 0.5858 0.6331 0.8122 0.079 Uiso 1 1 calc GR
H41B H 0.4894 0.6340 0.8268 0.079 Uiso 1 1 calc GR
H41C H 0.4866 0.5798 0.7857 0.079 Uiso 1 1 calc GR
C34 C 0.3748(10) -0.1603(8) 0.5715(5) 0.055(4) Uani 1 1 d .
H34A H 0.4098 -0.1119 0.5650 0.082 Uiso 1 1 calc GR
H34B H 0.3688 -0.1992 0.5482 0.082 Uiso 1 1 calc GR
H34C H 0.4088 -0.1675 0.5960 0.082 Uiso 1 1 calc GR
C38 C 0.5019(11) -0.1199(7) 0.9047(4) 0.045(3) Uani 1 1 d .
C33 C 0.6930(9) 0.4046(7) 1.0263(4) 0.039(3) Uani 1 1 d .
C32 C 0.5523(10) 0.3200(8) 0.5082(4) 0.050(3) Uani 1 1 d .
H32A H 0.6082 0.3626 0.5220 0.074 Uiso 1 1 calc GR
H32B H 0.5495 0.3162 0.4784 0.074 Uiso 1 1 calc GR
H32C H 0.5563 0.2748 0.5161 0.074 Uiso 1 1 calc GR
F4 F 0.6219(8) -0.1188(5) 0.6059(3) 0.076(3) Uani 1 1 d .
F5 F 0.5641(8) -0.1976(5) 0.6443(3) 0.080(3) Uani 1 1 d .
F3 F 0.2257(8) 0.2783(6) 0.8162(3) 0.083(3) Uani 1 1 d .
N2 N 0.1791(8) 0.3059(6) 0.5646(3) 0.046(3) Uani 1 1 d .
F1 F 0.1516(6) 0.1847(6) 0.7671(3) 0.084(3) Uani 1 1 d .
F2 F 0.2341(8) 0.1719(6) 0.8208(3) 0.088(3) Uani 1 1 d .
F6 F 0.7116(7) -0.1234(6) 0.6597(3) 0.090(3) Uani 1 1 d .
C49 C 0.2304(9) 0.2173(7) 0.7943(4) 0.038(3) Uani 1 1 d .
C45 C -0.0023(11) -0.0089(10) 0.7204(5) 0.068(5) Uani 1 1 d .
H45A H 0.0393 0.0433 0.7275 0.101 Uiso 1 1 calc GR
H45B H -0.0658 -0.0142 0.7262 0.101 Uiso 1 1 calc GR
H45C H -0.0053 -0.0271 0.6912 0.101 Uiso 1 1 calc GR
C48 C 0.3231(9) 0.2366(7) 0.7736(4) 0.043(3) Uani 1 1 d .
C53 C 0.7015(11) -0.0690(8) 0.8513(5) 0.058(4) Uani 1 1 d .
H53A H 0.7050 -0.0439 0.8793 0.087 Uiso 1 1 calc GR
H53B H 0.7424 -0.0978 0.8514 0.087 Uiso 1 1 calc GR
H53C H 0.6361 -0.1021 0.8408 0.087 Uiso 1 1 calc GR
C202 C 0.1035(10) 0.2822(7) 0.5467(4) 0.044(3) Uani 1 1 d .
C52 C 0.4859(9) -0.2284(7) 0.7675(5) 0.049(3) Uani 1 1 d .
H52A H 0.5264 -0.1921 0.7532 0.073 Uiso 1 1 calc GR
H52B H 0.4975 -0.2746 0.7619 0.073 Uiso 1 1 calc GR
H52C H 0.5002 -0.2092 0.7971 0.073 Uiso 1 1 calc GR
C55 C 0.6253(11) -0.1266(8) 0.6449(5) 0.051(4) Uani 1 1 d .
C58 C 0.6658(10) 0.1733(9) 0.5603(4) 0.058(4) Uani 1 1 d .
H58A H 0.6437 0.2112 0.5520 0.088 Uiso 1 1 calc GR
H58B H 0.6971 0.1566 0.5387 0.088 Uiso 1 1 calc GR
H58C H 0.7107 0.1942 0.5859 0.088 Uiso 1 1 calc GR
C50 C 0.9355(11) 0.5898(8) 0.7469(6) 0.064(5) Uani 1 1 d .
H50A H 0.8999 0.5745 0.7191 0.096 Uiso 1 1 calc GR
H50B H 0.9991 0.6252 0.7465 0.096 Uiso 1 1 calc GR
H50C H 0.9030 0.6130 0.7651 0.096 Uiso 1 1 calc GR
C51 C 0.3521(13) -0.2808(7) 0.7061(4) 0.060(4) Uani 1 1 d .
H51A H 0.2905 -0.2802 0.6955 0.090 Uiso 1 1 calc GR
H51B H 0.3485 -0.3321 0.7032 0.090 Uiso 1 1 calc GR
H51C H 0.3997 -0.2538 0.6904 0.090 Uiso 1 1 calc GR
C56 C 0.8390(12) 0.6173(8) 0.9594(5) 0.064(4) Uani 1 1 d .
H56A H 0.8276 0.6445 0.9381 0.096 Uiso 1 1 calc GR
H56B H 0.8829 0.6521 0.9828 0.096 Uiso 1 1 calc GR
H56C H 0.7791 0.5908 0.9684 0.096 Uiso 1 1 calc GR
C47 C 0.0894(9) 0.1326(7) 0.6144(5) 0.051(4) Uani 1 1 d .
H47A H 0.0778 0.1184 0.6411 0.077 Uiso 1 1 calc GR
H47B H 0.0293 0.1156 0.5958 0.077 Uiso 1 1 calc GR
H47C H 0.1193 0.1865 0.6180 0.077 Uiso 1 1 calc GR
C54 C 0.8339(8) 0.0474(7) 0.8428(4) 0.047(3) Uani 1 1 d .
H54A H 0.8536 0.0860 0.8261 0.071 Uiso 1 1 calc GR
H54B H 0.8796 0.0228 0.8440 0.071 Uiso 1 1 calc GR
H54C H 0.8311 0.0698 0.8706 0.071 Uiso 1 1 calc GR
C46 C 0.0464(10) -0.0233(9) 0.7930(4) 0.062(4) Uani 1 1 d .
H46A H 0.0643 -0.0560 0.8090 0.093 Uiso 1 1 calc GR
H46B H -0.0140 -0.0213 0.7994 0.093 Uiso 1 1 calc GR
H46C H 0.0952 0.0265 0.8000 0.093 Uiso 1 1 calc GR
C57 C 0.9401(10) 0.2667(9) 0.7124(7) 0.087(6) Uani 1 1 d .
H57A H 0.9203 0.2959 0.6944 0.130 Uiso 1 1 calc GR
H57B H 0.9983 0.2614 0.7050 0.130 Uiso 1 1 calc GR
H57C H 0.9517 0.2918 0.7410 0.130 Uiso 1 1 calc GR
C59 C 0.3735(10) 0.2572(8) 0.5035(4) 0.052(3) Uani 1 1 d .
H59A H 0.3865 0.2142 0.5100 0.077 Uiso 1 1 calc GR
H59B H 0.3596 0.2521 0.4736 0.077 Uiso 1 1 calc GR
H59C H 0.3191 0.2602 0.5159 0.077 Uiso 1 1 calc GR
F7 F 0.7371(7) 0.5047(5) 1.0859(3) 0.079(3) Uani 1 1 d .
F10 F 0.2247(7) 0.5972(6) 0.6128(4) 0.092(4) Uani 1 1 d .
F11 F 0.2651(9) 0.5829(5) 0.5520(3) 0.098(4) Uani 1 1 d .
F12 F 0.3629(8) 0.6651(5) 0.6002(3) 0.089(3) Uani 1 1 d .
F16 F 0.8953(12) 0.4522(6) 0.5841(5) 0.142(6) Uani 1 1 d .
F14 F 0.5433(12) -0.1641(7) 0.9653(3) 0.133(6) Uani 1 1 d .
F8 F 0.6959(11) 0.3950(6) 1.0981(3) 0.118(5) Uani 1 1 d .
F9 F 0.8297(9) 0.4442(9) 1.0773(4) 0.141(6) Uani 1 1 d .
N3 N 0.0932(9) -0.2689(7) 0.6927(4) 0.059(3) Uani 1 1 d .
C60 C 0.7368(10) 0.4353(8) 1.0725(4) 0.051(3) Uani 1 1 d .
C68 C 0.8638(12) 0.3888(8) 0.5939(5) 0.054(4) Uani 1 1 d .
C205 C 0.0548(11) -0.3178(8) 0.6662(5) 0.050(3) Uani 1 1 d .
C67 C 0.4483(13) 0.3966(9) 0.5073(5) 0.067(5) Uani 1 1 d .
H67A H 0.3958 0.4046 0.5193 0.100 Uiso 1 1 calc GR
H67B H 0.4337 0.3875 0.4773 0.100 Uiso 1 1 calc GR
H67C H 0.5060 0.4406 0.5166 0.100 Uiso 1 1 calc GR
F13 F 0.4509(12) -0.2441(6) 0.9183(5) 0.152(7) Uani 1 1 d .
C61 C 0.9101(11) 0.5249(9) 0.9758(4) 0.063(4) Uani 1 1 d .
H61A H 0.8562 0.5051 0.9902 0.095 Uiso 1 1 calc GR
H61B H 0.9631 0.5617 0.9952 0.095 Uiso 1 1 calc GR
H61C H 0.9289 0.4845 0.9639 0.095 Uiso 1 1 calc GR
C64 C 0.3109(9) 0.3087(8) 0.9182(5) 0.054(4) Uani 1 1 d .
H64A H 0.3151 0.3405 0.8977 0.081 Uiso 1 1 calc GR
H64B H 0.2629 0.3120 0.9351 0.081 Uiso 1 1 calc GR
H64C H 0.2936 0.2574 0.9043 0.081 Uiso 1 1 calc GR
C63 C 0.4171(10) 0.4912(9) 0.8416(5) 0.057(4) Uani 1 1 d .
H63A H 0.3808 0.4714 0.8139 0.085 Uiso 1 1 calc GR
H63B H 0.3867 0.5195 0.8577 0.085 Uiso 1 1 calc GR
H63C H 0.4193 0.4502 0.8550 0.085 Uiso 1 1 calc GR
C62 C 0.2942(12) 0.5941(8) 0.5922(4) 0.053(4) Uani 1 1 d .
C69 C 0.1049(11) 0.0095(7) 0.5870(5) 0.062(4) Uani 1 1 d .
H69A H 0.1480 -0.0134 0.5767 0.093 Uiso 1 1 calc GR
H69B H 0.0485 -0.0049 0.5664 0.093 Uiso 1 1 calc GR
H69C H 0.0866 -0.0072 0.6125 0.093 Uiso 1 1 calc GR
C204 C 0.0060(10) 0.2520(9) 0.5232(5) 0.061(4) Uani 1 1 d .
H20A H 0.0088 0.2403 0.4938 0.092 Uiso 1 1 calc GR
H20B H -0.0234 0.2889 0.5278 0.092 Uiso 1 1 calc GR
H20C H -0.0316 0.2071 0.5325 0.092 Uiso 1 1 calc GR
F15 F 0.5856(14) -0.2003(10) 0.9090(6) 0.181(9) Uani 1 1 d .
C203 C 0.8369(12) 0.5696(9) 0.5152(5) 0.065(4) Uani 1 1 d .
H20D H 0.8061 0.5822 0.4917 0.097 Uiso 1 1 calc GR
H20E H 0.8641 0.5333 0.5053 0.097 Uiso 1 1 calc GR
H20F H 0.8871 0.6143 0.5310 0.097 Uiso 1 1 calc GR
C65 C 0.7877(10) 0.6797(8) 0.6765(6) 0.066(5) Uani 1 1 d .
H65A H 0.8134 0.6837 0.7052 0.099 Uiso 1 1 calc GR
H65B H 0.8081 0.7289 0.6691 0.099 Uiso 1 1 calc GR
H65C H 0.8109 0.6478 0.6587 0.099 Uiso 1 1 calc GR
C70 C 0.9778(11) 0.4773(9) 0.7303(5) 0.068(5) Uani 1 1 d .
H70A H 0.9814 0.4334 0.7401 0.103 Uiso 1 1 calc GR
H70B H 1.0405 0.5084 0.7257 0.103 Uiso 1 1 calc GR
H70C H 0.9337 0.4621 0.7045 0.103 Uiso 1 1 calc GR
C66 C 0.5246(14) -0.1793(9) 0.9258(5) 0.065(4) Uani 1 1 d .
F20 F 0.8417(11) 0.8180(6) 0.8158(4) 0.116(5) Uani 1 1 d .
N4 N 0.1304(10) -0.2155(7) 0.8031(4) 0.060(3) Uani 1 1 d .
F19 F 0.8085(12) 0.7902(6) 0.8728(4) 0.131(6) Uani 1 1 d .
C206 C 0.0065(12) -0.3826(8) 0.6328(5) 0.064(4) Uani 1 1 d .
H20G H 0.0026 -0.3658 0.6065 0.097 Uiso 1 1 calc GR
H20H H -0.0573 -0.4094 0.6382 0.097 Uiso 1 1 calc GR
H20I H 0.0423 -0.4154 0.6317 0.097 Uiso 1 1 calc GR
C207 C 0.1386(14) -0.2349(8) 0.8336(5) 0.077(6) Uani 1 1 d .
C74 C 0.8319(10) 0.1571(10) 0.6616(5) 0.069(5) Uani 1 1 d .
H74A H 0.7760 0.1115 0.6576 0.103 Uiso 1 1 calc GR
H74B H 0.8837 0.1461 0.6505 0.103 Uiso 1 1 calc GR
H74C H 0.8170 0.1929 0.6472 0.103 Uiso 1 1 calc GR
C72 C 0.9672(10) 0.5969(9) 0.9200(5) 0.068(5) Uani 1 1 d .
H72A H 0.9937 0.5600 0.9103 0.103 Uiso 1 1 calc GR
H72B H 1.0154 0.6379 0.9393 0.103 Uiso 1 1 calc GR
H72C H 0.9464 0.6156 0.8965 0.103 Uiso 1 1 calc GR
C71 C 0.1899(13) 0.1257(9) 0.5573(5) 0.072(5) Uani 1 1 d .
H71A H 0.2374 0.1758 0.5654 0.108 Uiso 1 1 calc GR
H71B H 0.1362 0.1265 0.5391 0.108 Uiso 1 1 calc GR
H71C H 0.2178 0.0934 0.5428 0.108 Uiso 1 1 calc GR
F22 F 0.9461(11) 0.8033(7) 0.8564(7) 0.175(8) Uani 1 1 d .
C76 C 1.0047(10) 0.5452(9) 0.8043(5) 0.068(5) Uani 1 1 d .
H76A H 0.9650 0.5405 0.8261 0.102 Uiso 1 1 calc GR
H76B H 1.0474 0.5968 0.8073 0.102 Uiso 1 1 calc GR
H76C H 1.0419 0.5138 0.8065 0.102 Uiso 1 1 calc GR
C73 C 0.8544(14) 0.7773(8) 0.8417(6) 0.067(5) Uani 1 1 d .
F17 F 0.8232(14) 0.3482(10) 0.5593(5) 0.204(11) Uani 1 1 d .
C75 C 0.8934(14) 0.1419(13) 0.7319(6) 0.104(8) Uani 1 1 d .
H75A H 0.9209 0.1697 0.7598 0.155 Uiso 1 1 calc GR
H75B H 0.9410 0.1276 0.7190 0.155 Uiso 1 1 calc GR
H75C H 0.8393 0.0975 0.7332 0.155 Uiso 1 1 calc GR
F18 F 0.9350(15) 0.3735(17) 0.6018(7) 0.259(15) Uani 1 1 d .
C208 C 0.151(2) -0.2583(12) 0.8739(6) 0.169(16) Uani 1 1 d .
H20J H 0.1636 -0.3041 0.8696 0.253 Uiso 1 1 calc GR
H20K H 0.0933 -0.2667 0.8863 0.253 Uiso 1 1 calc GR
H20L H 0.2042 -0.2195 0.8922 0.253 Uiso 1 1 calc GR
S17 S 0.88576(19) 0.28978(16) 0.84498(9) 0.0316(6) Uani 1 1 d .
O20 O -0.0130(6) -0.1522(5) 0.6268(3) 0.055(2) Uani 1 1 d .
O21 O -0.0167(7) -0.2562(6) 0.5842(3) 0.067(3) Uani 1 1 d .
C78 C 1.0131(8) 0.3122(7) 0.8697(4) 0.035(3) Uani 1 1 d .
C80 C 1.0789(9) 0.3638(7) 0.8449(4) 0.046(3) Uani 1 1 d .
H80A H 1.0647 0.3403 0.8158 0.068 Uiso 1 1 calc GR
H80B H 1.1449 0.3730 0.8554 0.068 Uiso 1 1 calc GR
H80C H 1.0690 0.4108 0.8477 0.068 Uiso 1 1 calc GR
C209 C -0.0476(9) -0.2058(8) 0.5972(4) 0.041(3) Uani 1 1 d .
C81 C 1.0279(9) 0.2380(8) 0.8673(5) 0.058(4) Uani 1 1 d .
H81A H 0.9865 0.2073 0.8839 0.088 Uiso 1 1 calc GR
H81B H 1.0939 0.2474 0.8778 0.088 Uiso 1 1 calc GR
H81C H 1.0128 0.2121 0.8387 0.088 Uiso 1 1 calc GR
C79 C 1.0288(10) 0.3528(9) 0.9148(4) 0.055(4) Uani 1 1 d .
H79A H 0.9984 0.3892 0.9162 0.082 Uiso 1 1 calc GR
H79B H 1.0967 0.3779 0.9246 0.082 Uiso 1 1 calc GR
H79C H 1.0014 0.3167 0.9322 0.082 Uiso 1 1 calc GR
C77 C 0.6741(13) 0.1395(11) 1.0141(5) 0.081(6) Uani 1 1 d .
H77A H 0.6383 0.1723 1.0152 0.121 Uiso 1 1 calc GR
H77B H 0.7097 0.1460 1.0413 0.121 Uiso 1 1 calc GR
H77C H 0.6303 0.0881 1.0057 0.121 Uiso 1 1 calc GR
C82 C 0.7792(16) 0.0961(11) 0.9688(6) 0.097(7) Uani 1 1 d .
H82A H 0.7252 0.0520 0.9551 0.146 Uiso 1 1 calc GR
H82B H 0.8094 0.0852 0.9931 0.146 Uiso 1 1 calc GR
H82C H 0.8249 0.1107 0.9498 0.146 Uiso 1 1 calc GR
F26 F -0.1993(6) -0.1904(5) 0.5953(3) 0.062(2) Uani 1 1 d .
F27 F -0.1301(7) -0.1778(6) 0.5417(3) 0.069(2) Uani 1 1 d .
F28 F -0.2010(6) -0.2880(5) 0.5574(3) 0.081(3) Uani 1 1 d .
C100 C -0.1445(9) -0.2147(7) 0.5733(4) 0.041(3) Uani 1 1 d .
C501 C -0.1540(17) 0.0276(14) 0.5493(7) 0.098(6) Uiso 1 1 d .
N5 N -0.1229(18) 0.0692(14) 0.5287(8) 0.145(8) Uiso 1 1 d .
C502 C -0.182(2) -0.0305(15) 0.5756(8) 0.123(8) Uiso 1 1 d .
O5 O 0.047(4) -0.034(3) 0.9538(16) 0.39(3) Uiso 1 1 d .
O58 O 0.156(5) 0.103(4) 1.0238(19) 0.48(3) Uiso 1 1 d .
C503 C 0.099(7) 0.166(5) 0.990(3) 0.47(5) Uiso 1 1 d .
C89 C -0.051(7) -0.021(5) 0.933(3) 0.43(5) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
Ag3 Ag1 Ag6 137.14(3) .
Ag3 Ag1 Ag26 144.44(4) .
Ag3 Ag1 Ag29 89.02(3) .
Ag2 Ag1 Ag3 59.14(3) .
Ag2 Ag1 Ag5 131.90(4) .
Ag2 Ag1 Ag6 93.37(3) .
Ag2 Ag1 Ag26 105.29(3) .
Ag2 Ag1 Ag29 60.93(3) .
Ag2 Ag1 Ag28 118.00(4) .
Ag5 Ag1 Ag3 96.85(3) .
Ag5 Ag1 Ag6 77.02(3) .
Ag5 Ag1 Ag26 114.54(3) .
Ag5 Ag1 Ag29 167.02(4) .
Ag5 Ag1 Ag28 101.89(4) .
Ag6 Ag1 Ag29 106.37(3) .
Ag26 Ag1 Ag6 69.73(3) .
Ag26 Ag1 Ag29 56.95(3) .
Ag28 Ag1 Ag3 90.89(3) .
Ag28 Ag1 Ag6 131.96(4) .
Ag28 Ag1 Ag26 67.48(3) .
Ag28 Ag1 Ag29 66.32(3) .
S1 Ag1 Ag3 52.98(6) .
S1 Ag1 Ag2 112.02(6) .
S1 Ag1 Ag5 57.99(6) .
S1 Ag1 Ag6 134.73(7) .
S1 Ag1 Ag26 131.54(6) .
S1 Ag1 Ag29 118.60(7) .
S1 Ag1 Ag28 68.17(6) .
S2 Ag1 Ag3 115.48(6) .
S2 Ag1 Ag2 56.90(6) .
S2 Ag1 Ag5 132.20(7) .
S2 Ag1 Ag6 55.24(6) .
S2 Ag1 Ag26 54.37(6) .
S2 Ag1 Ag29 53.24(6) .
S2 Ag1 Ag28 111.25(7) .
S2 Ag1 S1 167.87(9) .
Ag1 Ag3 Ag9 128.00(4) .
Ag1 Ag3 Ag30 92.99(3) .
Ag1 Ag3 Ag31 97.74(3) .
Ag1 Ag3 Ag27 147.94(4) .
Ag2 Ag3 Ag1 59.06(3) .
Ag2 Ag3 Ag9 88.39(3) .
Ag2 Ag3 Ag4 123.04(4) .
Ag2 Ag3 Ag30 63.41(3) .
Ag2 Ag3 Ag31 123.08(4) .
Ag2 Ag3 Ag27 102.10(3) .
Ag9 Ag3 Ag27 71.62(3) .
Ag4 Ag3 Ag1 91.24(3) .
Ag4 Ag3 Ag9 72.95(3) .
Ag4 Ag3 Ag30 173.53(4) .
Ag4 Ag3 Ag31 107.02(4) .
Ag4 Ag3 Ag27 120.41(3) .
Ag30 Ag3 Ag9 108.01(3) .
Ag30 Ag3 Ag27 55.03(3) .
Ag31 Ag3 Ag9 134.15(4) .
Ag31 Ag3 Ag30 67.55(3) .
Ag31 Ag3 Ag27 69.78(3) .
S3 Ag3 Ag1 115.03(7) .
S3 Ag3 Ag2 56.19(7) .
S3 Ag3 Ag9 55.35(6) .
S3 Ag3 Ag4 128.02(7) .
S3 Ag3 Ag30 53.96(6) .
S3 Ag3 Ag31 112.23(7) .
S3 Ag3 Ag27 50.68(7) .
S1 Ag3 Ag1 52.90(6) .
S1 Ag3 Ag2 111.86(6) .
S1 Ag3 Ag9 130.79(6) .
S1 Ag3 Ag4 58.26(6) .
S1 Ag3 Ag30 121.20(6) .
S1 Ag3 Ag31 71.63(6) .
S1 Ag3 Ag27 138.30(7) .
S1 Ag3 S3 167.90(9) .
Ag1 Ag2 Ag3 61.80(3) .
Ag1 Ag2 Ag8 142.95(4) .
Ag1 Ag2 Ag30 93.94(3) .
Ag1 Ag2 Ag19 113.50(3) .
Ag1 Ag2 Ag29 65.21(3) .
Ag3 Ag2 Ag8 105.13(3) .
Ag3 Ag2 Ag30 62.41(3) .
Ag3 Ag2 Ag19 154.58(4) .
Ag3 Ag2 Ag29 92.83(3) .
Ag8 Ag2 Ag30 110.82(3) .
Ag8 Ag2 Ag19 92.31(3) .
Ag8 Ag2 Ag29 151.55(4) .
Ag30 Ag2 Ag19 94.35(3) .
Ag29 Ag2 Ag30 58.35(3) .
Ag29 Ag2 Ag19 64.53(3) .
S3 Ag2 Ag1 115.00(6) .
S3 Ag2 Ag3 53.42(6) .
S3 Ag2 Ag8 65.76(6) .
S3 Ag2 Ag30 53.06(6) .
S3 Ag2 Ag19 122.03(6) .
S3 Ag2 Ag29 111.31(6) .
S3 Ag2 S2 162.93(9) .
S3 Ag2 O100 102.1(2) .
S2 Ag2 Ag1 52.78(6) .
S2 Ag2 Ag3 114.03(6) .
S2 Ag2 Ag8 131.31(6) .
S2 Ag2 Ag30 112.37(6) .
S2 Ag2 Ag19 63.25(6) .
S2 Ag2 Ag29 54.37(6) .
S2 Ag2 O100 89.0(3) .
O100 Ag2 Ag1 83.5(3) .
O100 Ag2 Ag3 91.7(3) .
O100 Ag2 Ag8 61.4(3) .
O100 Ag2 Ag30 151.1(2) .
O100 Ag2 Ag19 113.1(2) .
O100 Ag2 Ag29 141.3(3) .
Ag10 Ag11 Ag5 94.12(3) .
S4 Ag11 Ag5 55.82(6) .
S4 Ag11 Ag10 53.69(7) .
S11 Ag11 Ag5 81.92(7) .
S11 Ag11 Ag10 133.49(8) .
S11 Ag11 S4 137.27(9) .
O11 Ag11 Ag5 170.2(3) .
O11 Ag11 Ag10 79.6(3) .
O11 Ag11 S4 114.5(3) .
O11 Ag11 S11 107.9(3) .
Ag15 Ag9 Ag3 129.77(4) .
Ag22 Ag9 Ag3 90.39(3) .
Ag22 Ag9 Ag15 69.89(3) .
S3 Ag9 Ag3 48.93(6) .
S3 Ag9 Ag15 85.75(6) .
S3 Ag9 Ag22 94.21(7) .
S9 Ag9 Ag3 78.96(6) .
S9 Ag9 Ag15 117.54(7) .
S9 Ag9 Ag22 53.87(7) .
S9 Ag9 S3 120.22(9) .
S9 Ag9 S8 150.36(9) .
S8 Ag9 Ag3 130.28(7) .
S8 Ag9 Ag15 51.24(6) .
S8 Ag9 Ag22 120.77(7) .
S8 Ag9 S3 88.12(8) .
Ag15 Ag14 Ag8 90.14(3) .
S8 Ag14 Ag8 48.98(6) .
S8 Ag14 Ag15 51.71(6) .
S14 Ag14 Ag8 89.51(7) .
S14 Ag14 Ag15 88.02(7) .
S14 Ag14 S8 113.62(9) .
O2 Ag14 Ag8 153.7(2) .
O2 Ag14 Ag15 78.9(2) .
O2 Ag14 S8 107.4(2) .
O2 Ag14 S14 113.6(3) .
N2 Ag14 Ag8 96.7(3) .
N2 Ag14 Ag15 150.0(3) .
N2 Ag14 S8 114.0(3) .
N2 Ag14 S14 121.1(3) .
N2 Ag14 O2 82.3(4) .
Ag1 Ag5 Ag11 139.60(4) .
Ag1 Ag5 Ag4 83.95(3) .
Ag11 Ag5 Ag4 86.06(3) .
S5 Ag5 Ag1 83.74(6) .
S5 Ag5 Ag11 115.46(7) .
S5 Ag5 Ag4 157.22(7) .
S5 Ag5 S1 130.38(8) .
S5 Ag5 S4 137.22(9) .
S1 Ag5 Ag1 52.25(6) .
S1 Ag5 Ag11 92.04(6) .
S1 Ag5 Ag4 50.80(5) .
S4 Ag5 Ag1 133.99(7) .
S4 Ag5 Ag11 52.67(6) .
S4 Ag5 Ag4 50.16(6) .
S4 Ag5 S1 92.39(8) .
Ag11 Ag10 Ag4 94.42(3) .
S4 Ag10 Ag11 54.51(6) .
S4 Ag10 Ag4 56.30(7) .
S10 Ag10 Ag11 128.70(8) .
S10 Ag10 Ag4 85.31(7) .
S10 Ag10 S4 140.42(10) .
O10 Ag10 Ag11 82.5(2) .
O10 Ag10 Ag4 161.0(3) .
O10 Ag10 S4 108.2(2) .
O10 Ag10 S10 111.3(2) .
Ag3 Ag4 Ag5 87.30(3) .
Ag3 Ag4 Ag10 135.24(4) .
Ag10 Ag4 Ag5 85.38(3) .
S1 Ag4 Ag3 51.44(6) .
S1 Ag4 Ag5 49.76(6) .
S1 Ag4 Ag10 92.22(6) .
S9 Ag4 Ag3 82.64(6) .
S9 Ag4 Ag5 167.18(7) .
S9 Ag4 Ag10 107.37(7) .
S9 Ag4 S1 126.33(9) .
S9 Ag4 S4 140.19(9) .
S4 Ag4 Ag3 136.91(6) .
S4 Ag4 Ag5 49.66(6) .
S4 Ag4 Ag10 51.78(6) .
S4 Ag4 S1 91.06(8) .
Ag26 Ag18 Ag13 134.75(4) .
Ag12 Ag18 Ag13 61.32(3) .
Ag12 Ag18 Ag26 101.78(4) .
S13 Ag18 Ag13 48.77(7) .
S13 Ag18 Ag26 129.71(7) .
S13 Ag18 Ag12 109.82(8) .
S13 Ag18 S12 162.36(10) .
S12 Ag18 Ag13 113.89(8) .
S12 Ag18 Ag26 62.88(7) .
S12 Ag18 Ag12 52.64(7) .
Ag2 Ag8 Ag14 135.72(4) .
S8 Ag8 Ag2 122.34(7) .
S8 Ag8 Ag14 55.42(7) .
S7 Ag8 Ag2 69.36(7) .
S7 Ag8 Ag14 119.94(8) .
S7 Ag8 S8 167.78(10) .
Ag7 Ag13 Ag18 85.95(3) .
Ag7 Ag13 Ag12 94.65(3) .
Ag12 Ag13 Ag18 56.68(3) .
S6 Ag13 Ag18 82.97(6) .
S6 Ag13 Ag7 51.43(6) .
S6 Ag13 Ag12 50.47(6) .
S13 Ag13 Ag18 47.03(6) .
S13 Ag13 Ag7 86.12(7) .
S13 Ag13 Ag12 103.47(7) .
S13 Ag13 S6 118.26(9) .
O20 Ag13 Ag18 159.4(3) .
O20 Ag13 Ag7 114.7(3) .
O20 Ag13 Ag12 118.1(3) .
O20 Ag13 S6 109.4(3) .
O20 Ag13 S13 130.2(3) .
S3 Ag20 Ag30 51.05(5) .
S19 Ag20 Ag30 58.83(7) .
S19 Ag20 S3 99.72(8) .
S14 Ag20 Ag30 126.16(8) .
S14 Ag20 S3 95.00(9) .
S14 Ag20 S19 161.79(10) .
Ag1 Ag6 Ag7 89.69(3) .
Ag17 Ag6 Ag1 90.02(3) .
Ag17 Ag6 Ag7 145.42(4) .
S5 Ag6 Ag1 77.12(6) .
S5 Ag6 Ag17 52.39(6) .
S5 Ag6 Ag7 158.86(7) .
S5 Ag6 S2 119.05(9) .
S5 Ag6 S6 146.36(9) .
S2 Ag6 Ag1 47.46(6) .
S2 Ag6 Ag17 98.18(6) .
S2 Ag6 Ag7 57.94(6) .
S6 Ag6 Ag1 136.21(7) .
S6 Ag6 Ag17 118.77(7) .
S6 Ag6 Ag7 47.58(6) .
S6 Ag6 S2 93.46(8) .
Ag3 Ag30 Ag2 54.18(3) .
Ag3 Ag30 Ag20 104.01(3) .
Ag2 Ag30 Ag20 66.11(3) .
Ag29 Ag30 Ag3 88.70(3) .
Ag29 Ag30 Ag2 59.81(3) .
Ag29 Ag30 Ag20 98.89(4) .
Ag27 Ag30 Ag3 65.21(3) .
Ag27 Ag30 Ag2 102.87(3) .
Ag27 Ag30 Ag20 90.12(3) .
Ag27 Ag30 Ag29 153.80(4) .
S3 Ag30 Ag3 49.36(6) .
S3 Ag30 Ag2 50.90(6) .
S3 Ag30 Ag20 57.75(6) .
S3 Ag30 Ag29 110.62(7) .
S3 Ag30 Ag27 54.45(6) .
S3 Ag30 S19 95.55(8) .
S20 Ag30 Ag3 82.67(6) .
S20 Ag30 Ag2 100.04(7) .
S20 Ag30 Ag20 153.63(7) .
S20 Ag30 Ag29 55.32(6) .
S20 Ag30 Ag27 115.45(7) .
S20 Ag30 S3 131.72(9) .
S20 Ag30 S19 107.51(9) .
S19 Ag30 Ag3 121.35(6) .
S19 Ag30 Ag2 67.20(6) .
S19 Ag30 Ag20 47.09(6) .
S19 Ag30 Ag29 58.21(6) .
S19 Ag30 Ag27 137.02(6) .
O13 Ag30 Ag3 136.2(2) .
O13 Ag30 Ag2 156.9(3) .
O13 Ag30 Ag20 90.8(3) .
O13 Ag30 Ag29 130.0(2) .
O13 Ag30 Ag27 73.9(2) .
O13 Ag30 S3 115.8(2) .
O13 Ag30 S20 101.9(3) .
O13 Ag30 S19 99.1(3) .
Ag26 Ag17 Ag6 71.90(3) .
Ag16 Ag17 Ag6 102.60(3) .
Ag16 Ag17 Ag26 89.92(4) .
S5 Ag17 Ag6 50.02(6) .
S5 Ag17 Ag26 96.89(6) .
S5 Ag17 Ag16 59.64(6) .
S12 Ag17 Ag6 82.03(7) .
S12 Ag17 Ag26 64.13(7) .
S12 Ag17 Ag16 151.13(8) .
S12 Ag17 S5 132.04(9) .
O6 Ag17 Ag6 154.4(3) .
O6 Ag17 Ag26 133.7(3) .
O6 Ag17 Ag16 81.5(3) .
O6 Ag17 S5 116.5(3) .
O6 Ag17 S12 106.7(2) .
S9 Ag23 Ag22 54.11(6) .
S16 Ag23 Ag22 75.11(7) .
S16 Ag23 S9 105.42(9) .
S10 Ag23 Ag22 156.82(8) .
S10 Ag23 S9 102.90(9) .
S10 Ag23 S16 118.80(10) .
O4 Ag23 Ag22 87.8(2) .
O4 Ag23 S9 113.2(3) .
O4 Ag23 S16 115.3(3) .
O4 Ag23 S10 100.9(3) .
Ag25 Ag24 Ag31 90.70(3) .
S10 Ag24 Ag25 130.78(8) .
S10 Ag24 Ag31 121.62(7) .
S10 Ag24 S17 177.88(11) .
S17 Ag24 Ag25 50.68(7) .
S17 Ag24 Ag31 58.92(7) .
Ag13 Ag7 Ag6 92.57(3) .
S2 Ag7 Ag13 94.54(5) .
S2 Ag7 Ag6 50.79(5) .
S6 Ag7 Ag13 55.17(6) .
S6 Ag7 Ag6 49.88(7) .
S6 Ag7 S2 89.36(8) .
S7 Ag7 Ag13 106.34(8) .
S7 Ag7 Ag6 145.62(8) .
S7 Ag7 S2 98.34(9) .
S7 Ag7 S6 160.71(10) .
Ag24 Ag25 Ag28 95.54(4) .
S11 Ag25 Ag24 129.16(7) .
S11 Ag25 Ag28 117.60(8) .
S11 Ag25 S17 175.21(10) .
S17 Ag25 Ag24 51.04(7) .
S17 Ag25 Ag28 66.36(7) .
Ag1 Ag26 Ag28 53.24(3) .
Ag18 Ag26 Ag1 111.08(3) .
Ag18 Ag26 Ag28 151.86(4) .
Ag17 Ag26 Ag1 93.88(3) .
Ag17 Ag26 Ag18 91.21(4) .
Ag17 Ag26 Ag29 154.97(4) .
Ag17 Ag26 Ag28 111.53(4) .
Ag29 Ag26 Ag1 62.86(3) .
Ag29 Ag26 Ag18 89.10(3) .
Ag29 Ag26 Ag28 63.22(3) .
S2 Ag26 Ag1 48.72(6) .
S2 Ag26 Ag18 63.32(6) .
S2 Ag26 Ag17 103.54(6) .
S2 Ag26 Ag29 54.80(6) .
S2 Ag26 Ag28 94.29(6) .
S2 Ag26 S12 95.30(8) .
S12 Ag26 Ag1 123.96(6) .
S12 Ag26 Ag18 47.25(6) .
S12 Ag26 Ag17 48.48(6) .
S12 Ag26 Ag29 136.30(6) .
S12 Ag26 Ag28 159.52(6) .
S18 Ag26 Ag1 80.81(7) .
S18 Ag26 Ag18 162.15(8) .
S18 Ag26 Ag17 74.28(7) .
S18 Ag26 Ag29 108.46(8) .
S18 Ag26 Ag28 45.98(7) .
S18 Ag26 S2 129.50(9) .
S18 Ag26 S12 115.24(9) .
O8 Ag26 Ag1 140.2(2) .
O8 Ag26 Ag18 58.7(2) .
O8 Ag26 Ag17 122.9(2) .
O8 Ag26 Ag29 78.0(2) .
O8 Ag26 Ag28 115.7(2) .
O8 Ag26 S2 103.0(2) .
O8 Ag26 S12 79.5(2) .
O8 Ag26 S18 120.7(2) .
S5 Ag16 Ag17 53.87(6) .
S11 Ag16 Ag17 163.02(7) .
S11 Ag16 S5 109.45(8) .
S11 Ag16 S18 108.61(10) .
S18 Ag16 Ag17 75.11(7) .
S18 Ag16 S5 101.65(8) .
O7 Ag16 Ag17 81.8(2) .
O7 Ag16 S5 112.0(3) .
O7 Ag16 S11 110.3(2) .
O7 Ag16 S18 114.4(2) .
Ag9 Ag15 Ag21 106.88(3) .
Ag14 Ag15 Ag9 100.53(3) .
Ag14 Ag15 Ag21 78.50(3) .
S8 Ag15 Ag9 52.36(6) .
S8 Ag15 Ag14 56.61(7) .
S8 Ag15 Ag21 118.11(7) .
S15 Ag15 Ag9 91.95(7) .
S15 Ag15 Ag14 129.53(7) .
S15 Ag15 Ag21 51.15(7) .
S15 Ag15 S8 140.89(9) .
O1 Ag15 Ag9 141.9(3) .
O1 Ag15 Ag14 81.4(2) .
O1 Ag15 Ag21 110.7(3) .
O1 Ag15 S8 102.7(3) .
O1 Ag15 S15 116.3(3) .
S15 Ag21 Ag15 48.53(7) .
S14 Ag21 Ag15 84.73(7) .
S14 Ag21 S15 130.85(10) .
N1 Ag21 Ag15 138.8(3) .
N1 Ag21 S15 110.9(3) .
N1 Ag21 S14 115.4(3) .
S19 Ag19 Ag2 69.32(6) .
S19 Ag19 S7 105.14(9) .
S13 Ag19 Ag2 127.51(7) .
S13 Ag19 S19 148.25(10) .
S13 Ag19 S7 106.60(9) .
S7 Ag19 Ag2 62.52(7) .
Ag1 Ag29 Ag28 52.65(3) .
Ag2 Ag29 Ag1 53.86(2) .
Ag2 Ag29 Ag28 100.10(3) .
Ag30 Ag29 Ag1 89.29(3) .
Ag30 Ag29 Ag2 61.84(3) .
Ag30 Ag29 Ag28 90.58(4) .
Ag26 Ag29 Ag1 60.19(3) .
Ag26 Ag29 Ag2 102.27(3) .
Ag26 Ag29 Ag30 147.71(4) .
Ag26 Ag29 Ag28 63.33(3) .
S20 Ag29 Ag1 83.10(6) .
S20 Ag29 Ag2 99.66(6) .
S20 Ag29 Ag30 52.66(6) .
S20 Ag29 Ag26 108.93(7) .
S20 Ag29 Ag28 46.54(6) .
S20 Ag29 S19 103.89(8) .
S2 Ag29 Ag1 47.63(6) .
S2 Ag29 Ag2 52.05(5) .
S2 Ag29 Ag30 113.53(6) .
S2 Ag29 Ag26 54.58(6) .
S2 Ag29 Ag28 94.23(6) .
S2 Ag29 S20 130.59(8) .
S2 Ag29 S19 100.03(8) .
S19 Ag29 Ag1 121.26(6) .
S19 Ag29 Ag2 67.58(6) .
S19 Ag29 Ag30 56.83(6) .
S19 Ag29 Ag26 146.91(7) .
S19 Ag29 Ag28 147.37(6) .
O9 Ag29 Ag1 138.8(2) .
O9 Ag29 Ag2 155.3(3) .
O9 Ag29 Ag30 127.1(2) .
O9 Ag29 Ag26 79.7(2) .
O9 Ag29 Ag28 102.6(3) .
O9 Ag29 S20 102.9(2) .
O9 Ag29 S2 116.2(2) .
O9 Ag29 S19 97.2(2) .
Ag23 Ag22 Ag9 100.02(4) .
Ag23 Ag22 Ag27 89.87(4) .
Ag27 Ag22 Ag9 76.24(3) .
S9 Ag22 Ag9 51.02(6) .
S9 Ag22 Ag23 57.61(6) .
S9 Ag22 Ag27 103.14(7) .
S15 Ag22 Ag9 92.03(7) .
S15 Ag22 Ag23 149.72(8) .
S15 Ag22 Ag27 66.03(7) .
S15 Ag22 S9 142.80(10) .
O3 Ag22 Ag9 148.3(3) .
O3 Ag22 Ag23 74.7(2) .
O3 Ag22 Ag27 134.0(3) .
O3 Ag22 S9 104.1(3) .
O3 Ag22 S15 108.3(3) .
Ag18 Ag12 Ag13 61.99(3) .
S6 Ag12 Ag18 87.14(7) .
S6 Ag12 Ag13 51.39(6) .
S12 Ag12 Ag18 50.26(7) .
S12 Ag12 Ag13 112.19(7) .
S12 Ag12 S6 117.27(9) .
N3 Ag12 Ag18 94.2(3) .
N3 Ag12 Ag13 70.0(3) .
N3 Ag12 S6 111.9(3) .
N3 Ag12 S12 114.4(3) .
N3 Ag12 N4 95.6(4) .
N4 Ag12 Ag18 151.1(3) .
N4 Ag12 Ag13 146.7(3) .
N4 Ag12 S6 113.9(3) .
N4 Ag12 S12 101.1(3) .
Ag3 Ag31 Ag24 93.82(4) .
S20 Ag31 Ag3 85.01(6) .
S20 Ag31 Ag24 134.88(7) .
S20 Ag31 S17 95.13(9) .
S16 Ag31 Ag3 81.70(7) .
S16 Ag31 Ag24 85.17(7) .
S16 Ag31 S20 138.61(10) .
S16 Ag31 S17 125.41(10) .
S17 Ag31 Ag3 119.78(7) .
S17 Ag31 Ag24 47.17(6) .
Ag30 Ag27 Ag3 59.76(3) .
Ag30 Ag27 Ag22 146.80(5) .
Ag22 Ag27 Ag3 88.27(4) .
S3 Ag27 Ag3 47.30(6) .
S3 Ag27 Ag30 55.46(6) .
S3 Ag27 Ag22 97.15(6) .
S16 Ag27 Ag3 75.75(7) .
S16 Ag27 Ag30 103.64(7) .
S16 Ag27 Ag22 74.05(7) .
S16 Ag27 S3 122.89(10) .
O12 Ag27 Ag3 146.2(2) .
O12 Ag27 Ag30 86.4(2) .
O12 Ag27 Ag22 125.2(2) .
O12 Ag27 S3 115.4(3) .
O12 Ag27 S16 115.0(3) .
Ag1 Ag28 Ag25 98.07(4) .
Ag1 Ag28 Ag26 59.27(3) .
Ag1 Ag28 Ag29 61.03(3) .
Ag25 Ag28 Ag26 122.57(4) .
Ag25 Ag28 Ag29 158.43(4) .
Ag29 Ag28 Ag26 53.45(3) .
S20 Ag28 Ag1 92.54(7) .
S20 Ag28 Ag25 131.51(8) .
S20 Ag28 Ag26 103.50(8) .
S20 Ag28 Ag29 50.93(7) .
S18 Ag28 Ag1 86.14(7) .
S18 Ag28 Ag25 82.73(7) .
S18 Ag28 Ag26 47.14(7) .
S18 Ag28 Ag29 99.92(8) .
S18 Ag28 S20 145.39(11) .
Ag5 S5 Ag6 100.95(9) .
Ag5 S5 Ag17 137.25(11) .
Ag5 S5 Ag16 85.02(8) .
Ag6 S5 Ag17 77.59(7) .
Ag6 S5 Ag16 130.51(10) .
Ag17 S5 Ag16 66.49(7) .
C11 S5 Ag5 110.8(3) .
C11 S5 Ag6 114.9(4) .
C11 S5 Ag17 108.2(3) .
C11 S5 Ag16 108.2(4) .
Ag3 S3 Ag2 70.40(7) .
Ag3 S3 Ag9 75.71(7) .
Ag3 S3 Ag20 140.57(10) .
Ag3 S3 Ag30 76.68(7) .
Ag3 S3 Ag27 82.02(8) .
Ag2 S3 Ag9 107.58(9) .
Ag2 S3 Ag20 80.01(7) .
Ag2 S3 Ag30 76.04(7) .
Ag2 S3 Ag27 140.32(11) .
Ag9 S3 Ag20 139.80(10) .
Ag30 S3 Ag9 148.82(11) .
Ag30 S3 Ag20 71.21(7) .
Ag27 S3 Ag9 91.91(8) .
Ag27 S3 Ag20 107.12(9) .
Ag27 S3 Ag30 70.09(7) .
Ag30 S20 Ag29 72.02(7) .
Ag31 S20 Ag30 84.60(8) .
Ag31 S20 Ag29 135.32(10) .
Ag28 S20 Ag30 131.14(11) .
Ag28 S20 Ag29 82.53(9) .
Ag28 S20 Ag31 85.44(9) .
C2 S20 Ag30 113.6(4) .
C2 S20 Ag29 112.9(3) .
C2 S20 Ag31 111.3(3) .
C2 S20 Ag28 114.6(4) .
Ag1 S1 Ag3 74.11(7) .
Ag1 S1 Ag5 69.76(7) .
Ag1 S1 Ag4 111.11(9) .
Ag3 S1 Ag5 119.31(10) .
Ag3 S1 Ag4 70.30(6) .
Ag5 S1 Ag4 79.44(7) .
Ag1 S2 Ag2 70.32(7) .
Ag1 S2 Ag6 77.30(7) .
Ag1 S2 Ag7 116.91(9) .
Ag1 S2 Ag26 76.91(7) .
Ag1 S2 Ag29 79.13(7) .
Ag2 S2 Ag6 114.83(9) .
Ag2 S2 Ag7 75.58(7) .
Ag2 S2 Ag26 135.02(10) .
Ag2 S2 Ag29 73.58(7) .
Ag6 S2 Ag7 71.28(6) .
Ag26 S2 Ag6 85.97(8) .
Ag26 S2 Ag7 148.61(10) .
Ag26 S2 Ag29 70.62(7) .
Ag29 S2 Ag6 149.92(11) .
Ag29 S2 Ag7 137.17(10) .
Ag9 S9 Ag4 93.62(9) .
Ag9 S9 Ag23 127.13(10) .
Ag9 S9 Ag22 75.11(8) .
Ag4 S9 Ag23 91.85(8) .
Ag4 S9 Ag22 141.00(11) .
Ag22 S9 Ag23 68.27(7) .
C9 S9 Ag9 111.5(4) .
C9 S9 Ag4 110.6(4) .
C9 S9 Ag23 115.4(4) .
C9 S9 Ag22 108.2(4) .
Ag6 S6 Ag13 126.02(10) .
Ag6 S6 Ag12 85.18(8) .
Ag7 S6 Ag13 73.40(8) .
Ag7 S6 Ag6 82.55(8) .
Ag7 S6 Ag12 133.19(11) .
Ag12 S6 Ag13 78.14(8) .
C15 S6 Ag13 109.3(4) .
C15 S6 Ag6 124.7(4) .
C15 S6 Ag7 113.8(4) .
C15 S6 Ag12 110.3(4) .
Ag20 S19 Ag30 74.08(7) .
Ag20 S19 Ag19 101.80(10) .
Ag20 S19 Ag29 127.03(10) .
Ag30 S19 Ag29 64.96(6) .
Ag19 S19 Ag30 126.81(10) .
Ag19 S19 Ag29 79.19(8) .
C13 S19 Ag20 106.9(4) .
C13 S19 Ag30 122.6(4) .
C13 S19 Ag19 109.5(4) .
C13 S19 Ag29 122.8(4) .
Ag9 S8 Ag14 130.55(10) .
Ag8 S8 Ag9 92.85(9) .
Ag8 S8 Ag14 75.60(8) .
Ag8 S8 Ag15 123.86(11) .
Ag15 S8 Ag9 76.40(8) .
Ag15 S8 Ag14 71.67(7) .
C8 S8 Ag9 115.6(4) .
C8 S8 Ag14 111.7(4) .
C8 S8 Ag8 119.5(4) .
C8 S8 Ag15 114.6(4) .
Ag31 S16 Ag23 113.28(11) .
Ag31 S16 Ag27 94.70(10) .
Ag27 S16 Ag23 114.64(11) .
C3 S16 Ag23 109.5(4) .
C3 S16 Ag31 113.1(4) .
C3 S16 Ag27 111.0(4) .
Ag11 S4 Ag5 71.51(7) .
Ag11 S4 Ag4 115.80(11) .
Ag5 S4 Ag4 80.17(8) .
Ag10 S4 Ag11 71.80(8) .
Ag10 S4 Ag5 116.58(11) .
Ag10 S4 Ag4 71.92(8) .
C23 S4 Ag11 110.0(4) .
C23 S4 Ag5 133.1(4) .
C23 S4 Ag10 107.5(4) .
C23 S4 Ag4 130.6(4) .
Ag15 S15 Ag21 80.32(9) .
Ag15 S15 Ag22 93.27(10) .
Ag22 S15 Ag21 139.20(11) .
C4 S15 Ag15 106.9(4) .
C4 S15 Ag21 110.4(4) .
C4 S15 Ag22 110.1(4) .
Ag18 S13 Ag13 84.19(9) .
Ag18 S13 Ag19 104.94(10) .
Ag19 S13 Ag13 115.31(10) .
C17 S13 Ag18 112.4(3) .
C17 S13 Ag13 113.1(4) .
C17 S13 Ag19 120.5(4) .
Ag20 S14 Ag14 109.99(11) .
Ag20 S14 Ag21 106.57(11) .
Ag21 S14 Ag14 105.09(10) .
C5 S14 Ag14 110.5(4) .
C5 S14 Ag20 113.6(3) .
C5 S14 Ag21 110.6(4) .
Ag11 S11 Ag16 118.90(11) .
Ag25 S11 Ag11 96.34(10) .
Ag25 S11 Ag16 99.15(10) .
C6 S11 Ag11 113.5(4) .
C6 S11 Ag25 110.7(4) .
C6 S11 Ag16 115.0(4) .
Ag10 S10 Ag23 122.03(11) .
Ag24 S10 Ag10 97.89(10) .
Ag24 S10 Ag23 91.69(10) .
C20 S10 Ag10 112.1(4) .
C20 S10 Ag23 116.2(4) .
C20 S10 Ag24 112.5(4) .
Ag8 S7 Ag7 106.69(12) .
Ag8 S7 Ag19 124.69(11) .
Ag7 S7 Ag19 83.96(8) .
C29 S7 Ag8 107.4(4) .
C29 S7 Ag7 111.3(4) .
C29 S7 Ag19 118.9(4) .
Ag18 S12 Ag17 127.63(11) .
Ag18 S12 Ag26 69.87(7) .
Ag18 S12 Ag12 77.10(8) .
Ag17 S12 Ag26 67.39(7) .
Ag17 S12 Ag12 102.46(10) .
Ag12 S12 Ag26 123.03(9) .
C1 S12 Ag18 110.7(4) .
C1 S12 Ag17 116.7(4) .
C1 S12 Ag26 121.3(4) .
C1 S12 Ag12 113.3(4) .
Ag26 S18 Ag16 112.36(11) .
Ag28 S18 Ag26 86.88(10) .
Ag28 S18 Ag16 117.90(11) .
C42 S18 Ag26 114.0(4) .
C42 S18 Ag16 113.7(4) .
C42 S18 Ag28 109.3(4) .
C33 O10 Ag10 118.7(7) .
C28 O13 Ag30 128.9(8) .
C7 O9 Ag29 121.6(7) .
C44 O3 Ag22 129.9(9) .
C14 O2 Ag14 122.0(8) .
C7 O8 Ag26 121.7(8) .
C28 O12 Ag27 112.4(9) .
C38 O6 Ag17 123.9(8) .
C38 O7 Ag16 121.3(8) .
C10 C9 S9 107.5(8) .
C41 C9 S9 108.6(8) .
C41 C9 C10 110.7(10) .
C63 C9 S9 105.9(8) .
C63 C9 C10 111.4(11) .
C63 C9 C41 112.4(11) .
C12 C11 S5 107.5(7) .
C25 C11 S5 107.8(7) .
C25 C11 C12 109.2(10) .
C26 C11 S5 107.7(8) .
C26 C11 C12 111.1(10) .
C26 C11 C25 113.3(10) .
C21 C13 S19 108.3(8) .
C21 C13 C58 109.0(10) .
C22 C13 S19 108.9(8) .
C22 C13 C21 112.4(10) .
C22 C13 C58 110.7(11) .
C58 C13 S19 107.2(8) .
C27 C4 S15 109.5(7) .
C27 C4 C40 110.1(10) .
C40 C4 S15 107.9(9) .
C65 C4 S15 106.6(8) .
C65 C4 C27 111.3(11) .
C65 C4 C40 111.3(12) .
C14 O1 Ag15 122.3(8) .
C50 C3 S16 107.9(8) .
C70 C3 S16 108.2(9) .
C70 C3 C50 109.2(12) .
C76 C3 S16 108.0(9) .
C76 C3 C50 109.8(12) .
C76 C3 C70 113.5(12) .
C30 C8 S8 108.2(8) .
C31 C8 S8 107.1(8) .
C31 C8 C30 112.5(10) .
C31 C8 C36 112.0(10) .
C36 C8 S8 105.5(8) .
C36 C8 C30 111.1(10) .
C44 O4 Ag23 116.7(9) .
C32 C5 S14 108.5(8) .
C32 C5 C59 109.9(10) .
C59 C5 S14 107.3(8) .
C67 C5 S14 107.9(9) .
C67 C5 C32 112.7(12) .
C67 C5 C59 110.3(11) .
O9 C7 C55 113.1(10) .
O8 C7 O9 131.4(11) .
O8 C7 C55 115.5(10) .
C11 C12 H12A 109.5 .
C11 C12 H12B 109.5 .
C11 C12 H12C 109.5 .
H12A C12 H12B 109.5 .
H12A C12 H12C 109.5 .
H12B C12 H12C 109.5 .
C57 C2 S20 106.7(8) .
C74 C2 S20 108.0(8) .
C74 C2 C57 108.7(13) .
C75 C2 S20 108.4(9) .
C75 C2 C57 110.2(14) .
C75 C2 C74 114.4(13) .
C33 O11 Ag11 124.4(9) .
C9 C10 H10A 109.5 .
C9 C10 H10B 109.5 .
C9 C10 H10C 109.5 .
H10A C10 H10B 109.5 .
H10A C10 H10C 109.5 .
H10B C10 H10C 109.5 .
C39 C1 S12 108.1(8) .
C39 C1 C52 109.8(11) .
C39 C1 C51 111.8(12) .
C52 C1 S12 108.0(8) .
C51 C1 S12 108.0(8) .
C51 C1 C52 111.1(11) .
C37 C6 S11 110.1(8) .
C37 C6 C77 108.5(12) .
C77 C6 S11 104.7(9) .
C82 C6 S11 107.7(9) .
C82 C6 C37 114.1(13) .
C82 C6 C77 111.4(14) .
H19A C19 H19B 109.5 .
H19A C19 H19C 109.5 .
H19B C19 H19C 109.5 .
C17 C19 H19A 109.5 .
C17 C19 H19B 109.5 .
C17 C19 H19C 109.5 .
C4 C27 H27A 109.5 .
C4 C27 H27B 109.5 .
C4 C27 H27C 109.5 .
H27A C27 H27B 109.5 .
H27A C27 H27C 109.5 .
H27B C27 H27C 109.5 .
C8 C30 H30A 109.5 .
C8 C30 H30B 109.5 .
C8 C30 H30C 109.5 .
H30A C30 H30B 109.5 .
H30A C30 H30C 109.5 .
H30B C30 H30C 109.5 .
C16 C15 S6 108.0(8) .
C16 C15 C46 110.9(11) .
C45 C15 S6 109.1(9) .
C45 C15 C16 110.0(12) .
C45 C15 C46 110.4(12) .
C46 C15 S6 108.4(8) .
O2 C14 C62 114.7(11) .
O1 C14 O2 132.1(12) .
O1 C14 C62 112.9(11) .
C24 C23 S4 108.5(9) .
C24 C23 C64 110.4(10) .
C35 C23 S4 107.8(8) .
C35 C23 C24 111.9(11) .
C35 C23 C64 112.4(12) .
C64 C23 S4 105.5(8) .
C11 C25 H25A 109.5 .
C11 C25 H25B 109.5 .
C11 C25 H25C 109.5 .
H25A C25 H25B 109.5 .
H25A C25 H25C 109.5 .
H25B C25 H25C 109.5 .
C15 C16 H16A 109.5 .
C15 C16 H16B 109.5 .
C15 C16 H16C 109.5 .
H16A C16 H16B 109.5 .
H16A C16 H16C 109.5 .
H16B C16 H16C 109.5 .
C19 C17 S13 109.8(8) .
C19 C17 C18 110.1(10) .
C18 C17 S13 105.1(7) .
C34 C17 S13 108.3(8) .
C34 C17 C19 111.6(10) .
C34 C17 C18 111.7(10) .
C47 C29 S7 108.3(8) .
C47 C29 C69 109.4(12) .
C69 C29 S7 107.6(8) .
C71 C29 S7 107.0(10) .
C71 C29 C47 112.4(11) .
C71 C29 C69 112.0(12) .
C8 C31 H31A 109.5 .
C8 C31 H31B 109.5 .
C8 C31 H31C 109.5 .
H31A C31 H31B 109.5 .
H31A C31 H31C 109.5 .
H31B C31 H31C 109.5 .
C13 C21 H21A 109.5 .
C13 C21 H21B 109.5 .
C13 C21 H21C 109.5 .
H21A C21 H21B 109.5 .
H21A C21 H21C 109.5 .
H21B C21 H21C 109.5 .
C13 C22 H22A 109.5 .
C13 C22 H22B 109.5 .
C13 C22 H22C 109.5 .
H22A C22 H22B 109.5 .
H22A C22 H22C 109.5 .
H22B C22 H22C 109.5 .
C11 C26 H26A 109.5 .
C11 C26 H26B 109.5 .
C11 C26 H26C 109.5 .
H26A C26 H26B 109.5 .
H26A C26 H26C 109.5 .
H26B C26 H26C 109.5 .
O13 C28 C68 113.1(10) .
O12 C28 O13 132.2(13) .
O12 C28 C68 114.5(12) .
C23 C24 H24A 109.5 .
C23 C24 H24B 109.5 .
C23 C24 H24C 109.5 .
H24A C24 H24B 109.5 .
H24A C24 H24C 109.5 .
H24B C24 H24C 109.5 .
C56 C20 S10 106.3(9) .
C61 C20 S10 110.1(9) .
C61 C20 C56 109.6(12) .
C61 C20 C72 110.8(12) .
C72 C20 S10 107.5(9) .
C72 C20 C56 112.4(13) .
C17 C18 H18A 109.5 .
C17 C18 H18B 109.5 .
C17 C18 H18C 109.5 .
H18A C18 H18B 109.5 .
H18A C18 H18C 109.5 .
H18B C18 H18C 109.5 .
C48 O100 Ag2 125.3(10) .
H43A C43 H43B 109.5 .
H43A C43 H43C 109.5 .
H43B C43 H43C 109.5 .
C42 C43 H43A 109.5 .
C42 C43 H43B 109.5 .
C42 C43 H43C 109.5 .
N1 C201 C203 176.1(16) .
O3 C44 C73 115.1(12) .
O4 C44 O3 130.4(13) .
O4 C44 C73 114.5(13) .
C201 N1 Ag21 171.8(11) .
C8 C36 H36A 109.5 .
C8 C36 H36B 109.5 .
C8 C36 H36C 109.5 .
H36A C36 H36B 109.5 .
H36A C36 H36C 109.5 .
H36B C36 H36C 109.5 .
C43 C42 S18 111.3(8) .
C53 C42 S18 107.5(8) .
C53 C42 C43 110.2(11) .
C54 C42 S18 109.2(8) .
C54 C42 C43 109.4(10) .
C54 C42 C53 109.1(11) .
C1 C39 H39A 109.5 .
C1 C39 H39B 109.5 .
C1 C39 H39C 109.5 .
H39A C39 H39B 109.5 .
H39A C39 H39C 109.5 .
H39B C39 H39C 109.5 .
C23 C35 H35A 109.5 .
C23 C35 H35B 109.5 .
C23 C35 H35C 109.5 .
H35A C35 H35B 109.5 .
H35A C35 H35C 109.5 .
H35B C35 H35C 109.5 .
C4 C40 H40A 109.5 .
C4 C40 H40B 109.5 .
C4 C40 H40C 109.5 .
H40A C40 H40B 109.5 .
H40A C40 H40C 109.5 .
H40B C40 H40C 109.5 .
C6 C37 H37A 109.5 .
C6 C37 H37B 109.5 .
C6 C37 H37C 109.5 .
H37A C37 H37B 109.5 .
H37A C37 H37C 109.5 .
H37B C37 H37C 109.5 .
C9 C41 H41A 109.5 .
C9 C41 H41B 109.5 .
C9 C41 H41C 109.5 .
H41A C41 H41B 109.5 .
H41A C41 H41C 109.5 .
H41B C41 H41C 109.5 .
C17 C34 H34A 109.5 .
C17 C34 H34B 109.5 .
C17 C34 H34C 109.5 .
H34A C34 H34B 109.5 .
H34A C34 H34C 109.5 .
H34B C34 H34C 109.5 .
O6 C38 O7 129.2(12) .
O6 C38 C66 117.3(12) .
O7 C38 C66 113.5(13) .
O10 C33 O11 130.9(12) .
O10 C33 C60 116.4(11) .
O11 C33 C60 112.7(12) .
C5 C32 H32A 109.5 .
C5 C32 H32B 109.5 .
C5 C32 H32C 109.5 .
H32A C32 H32B 109.5 .
H32A C32 H32C 109.5 .
H32B C32 H32C 109.5 .
C202 N2 Ag14 173.6(11) .
F3 C49 F2 107.0(11) .
F3 C49 C48 110.9(10) .
F1 C49 F3 108.2(11) .
F1 C49 F2 109.1(11) .
F1 C49 C48 113.0(11) .
F2 C49 C48 108.4(10) .
C15 C45 H45A 109.5 .
C15 C45 H45B 109.5 .
C15 C45 H45C 109.5 .
H45A C45 H45B 109.5 .
H45A C45 H45C 109.5 .
H45B C45 H45C 109.5 .
O101 C48 C49 117.0(11) .
O100 C48 O101 128.2(14) .
O100 C48 C49 113.5(11) .
C42 C53 H53A 109.5 .
C42 C53 H53B 109.5 .
C42 C53 H53C 109.5 .
H53A C53 H53B 109.5 .
H53A C53 H53C 109.5 .
H53B C53 H53C 109.5 .
N2 C202 C204 179.3(17) .
C1 C52 H52A 109.5 .
C1 C52 H52B 109.5 .
C1 C52 H52C 109.5 .
H52A C52 H52B 109.5 .
H52A C52 H52C 109.5 .
H52B C52 H52C 109.5 .
F4 C55 C7 113.6(10) .
F4 C55 F5 105.2(13) .
F4 C55 F6 109.9(12) .
F5 C55 C7 111.9(11) .
F6 C55 C7 109.5(12) .
F6 C55 F5 106.5(11) .
C13 C58 H58A 109.5 .
C13 C58 H58B 109.5 .
C13 C58 H58C 109.5 .
H58A C58 H58B 109.5 .
H58A C58 H58C 109.5 .
H58B C58 H58C 109.5 .
C3 C50 H50A 109.5 .
C3 C50 H50B 109.5 .
C3 C50 H50C 109.5 .
H50A C50 H50B 109.5 .
H50A C50 H50C 109.5 .
H50B C50 H50C 109.5 .
C1 C51 H51A 109.5 .
C1 C51 H51B 109.5 .
C1 C51 H51C 109.5 .
H51A C51 H51B 109.5 .
H51A C51 H51C 109.5 .
H51B C51 H51C 109.5 .
C20 C56 H56A 109.5 .
C20 C56 H56B 109.5 .
C20 C56 H56C 109.5 .
H56A C56 H56B 109.5 .
H56A C56 H56C 109.5 .
H56B C56 H56C 109.5 .
C29 C47 H47A 109.5 .
C29 C47 H47B 109.5 .
C29 C47 H47C 109.5 .
H47A C47 H47B 109.5 .
H47A C47 H47C 109.5 .
H47B C47 H47C 109.5 .
C42 C54 H54A 109.5 .
C42 C54 H54B 109.5 .
C42 C54 H54C 109.5 .
H54A C54 H54B 109.5 .
H54A C54 H54C 109.5 .
H54B C54 H54C 109.5 .
C15 C46 H46A 109.5 .
C15 C46 H46B 109.5 .
C15 C46 H46C 109.5 .
H46A C46 H46B 109.5 .
H46A C46 H46C 109.5 .
H46B C46 H46C 109.5 .
C2 C57 H57A 109.5 .
C2 C57 H57B 109.5 .
C2 C57 H57C 109.5 .
H57A C57 H57B 109.5 .
H57A C57 H57C 109.5 .
H57B C57 H57C 109.5 .
C5 C59 H59A 109.5 .
C5 C59 H59B 109.5 .
C5 C59 H59C 109.5 .
H59A C59 H59B 109.5 .
H59A C59 H59C 109.5 .
H59B C59 H59C 109.5 .
C205 N3 Ag12 172.3(12) .
F7 C60 C33 113.0(12) .
F8 C60 C33 115.2(13) .
F8 C60 F7 105.9(12) .
F8 C60 F9 108.6(15) .
F9 C60 C33 109.2(11) .
F9 C60 F7 104.3(13) .
F16 C68 C28 117.7(13) .
F16 C68 F17 101.4(16) .
F17 C68 C28 113.9(14) .
F18 C68 C28 113.4(14) .
F18 C68 F16 104.6(19) .
F18 C68 F17 104.2(19) .
N3 C205 C206 178.0(17) .
C5 C67 H67A 109.5 .
C5 C67 H67B 109.5 .
C5 C67 H67C 109.5 .
H67A C67 H67B 109.5 .
H67A C67 H67C 109.5 .
H67B C67 H67C 109.5 .
C20 C61 H61A 109.5 .
C20 C61 H61B 109.5 .
C20 C61 H61C 109.5 .
H61A C61 H61B 109.5 .
H61A C61 H61C 109.5 .
H61B C61 H61C 109.5 .
C23 C64 H64A 109.5 .
C23 C64 H64B 109.5 .
C23 C64 H64C 109.5 .
H64A C64 H64B 109.5 .
H64A C64 H64C 109.5 .
H64B C64 H64C 109.5 .
C9 C63 H63A 109.5 .
C9 C63 H63B 109.5 .
C9 C63 H63C 109.5 .
H63A C63 H63B 109.5 .
H63A C63 H63C 109.5 .
H63B C63 H63C 109.5 .
F10 C62 C14 112.6(12) .
F10 C62 F12 106.5(12) .
F11 C62 C14 114.6(11) .
F11 C62 F10 109.8(14) .
F11 C62 F12 103.2(12) .
F12 C62 C14 109.3(12) .
C29 C69 H69A 109.5 .
C29 C69 H69B 109.5 .
C29 C69 H69C 109.5 .
H69A C69 H69B 109.5 .
H69A C69 H69C 109.5 .
H69B C69 H69C 109.5 .
C202 C204 H20A 109.5 .
C202 C204 H20B 109.5 .
C202 C204 H20C 109.5 .
H20A C204 H20B 109.5 .
H20A C204 H20C 109.5 .
H20B C204 H20C 109.5 .
C201 C203 H20D 109.5 .
C201 C203 H20E 109.5 .
C201 C203 H20F 109.5 .
H20D C203 H20E 109.5 .
H20D C203 H20F 109.5 .
H20E C203 H20F 109.5 .
C4 C65 H65A 109.5 .
C4 C65 H65B 109.5 .
C4 C65 H65C 109.5 .
H65A C65 H65B 109.5 .
H65A C65 H65C 109.5 .
H65B C65 H65C 109.5 .
C3 C70 H70A 109.5 .
C3 C70 H70B 109.5 .
C3 C70 H70C 109.5 .
H70A C70 H70B 109.5 .
H70A C70 H70C 109.5 .
H70B C70 H70C 109.5 .
F14 C66 C38 115.9(13) .
F14 C66 F13 103.4(15) .
F14 C66 F15 112.9(18) .
F13 C66 C38 111.7(15) .
F15 C66 C38 111.9(13) .
F15 C66 F13 99.3(16) .
C207 N4 Ag12 153.3(15) .
C205 C206 H20G 109.5 .
C205 C206 H20H 109.5 .
C205 C206 H20I 109.5 .
H20G C206 H20H 109.5 .
H20G C206 H20I 109.5 .
H20H C206 H20I 109.5 .
N4 C207 C208 178.6(19) .
C2 C74 H74A 109.5 .
C2 C74 H74B 109.5 .
C2 C74 H74C 109.5 .
H74A C74 H74B 109.5 .
H74A C74 H74C 109.5 .
H74B C74 H74C 109.5 .
C20 C72 H72A 109.5 .
C20 C72 H72B 109.5 .
C20 C72 H72C 109.5 .
H72A C72 H72B 109.5 .
H72A C72 H72C 109.5 .
H72B C72 H72C 109.5 .
C29 C71 H71A 109.5 .
C29 C71 H71B 109.5 .
C29 C71 H71C 109.5 .
H71A C71 H71B 109.5 .
H71A C71 H71C 109.5 .
H71B C71 H71C 109.5 .
C3 C76 H76A 109.5 .
C3 C76 H76B 109.5 .
C3 C76 H76C 109.5 .
H76A C76 H76B 109.5 .
H76A C76 H76C 109.5 .
H76B C76 H76C 109.5 .
F20 C73 C44 115.7(15) .
F20 C73 F19 105.2(15) .
F20 C73 F22 107.3(17) .
F19 C73 C44 107.9(13) .
F22 C73 C44 112.6(14) .
F22 C73 F19 107.7(18) .
C2 C75 H75A 109.5 .
C2 C75 H75B 109.5 .
C2 C75 H75C 109.5 .
H75A C75 H75B 109.5 .
H75A C75 H75C 109.5 .
H75B C75 H75C 109.5 .
C207 C208 H20J 109.5 .
C207 C208 H20K 109.5 .
C207 C208 H20L 109.5 .
H20J C208 H20K 109.5 .
H20J C208 H20L 109.5 .
H20K C208 H20L 109.5 .
Ag24 S17 Ag31 73.91(8) .
Ag25 S17 Ag24 78.28(9) .
Ag25 S17 Ag31 115.18(10) .
C78 S17 Ag24 109.1(4) .
C78 S17 Ag25 111.3(4) .
C78 S17 Ag31 132.8(4) .
C209 O20 Ag13 122.5(9) .
C80 C78 S17 107.5(8) .
C80 C78 C79 109.4(11) .
C81 C78 S17 106.9(8) .
C81 C78 C80 111.6(11) .
C81 C78 C79 111.6(12) .
C79 C78 S17 109.7(8) .
C78 C80 H80A 109.5 .
C78 C80 H80B 109.5 .
C78 C80 H80C 109.5 .
H80A C80 H80B 109.5 .
H80A C80 H80C 109.5 .
H80B C80 H80C 109.5 .
O20 C209 O21 129.8(12) .
O20 C209 C100 116.0(12) .
O21 C209 C100 114.2(11) .
C78 C81 H81A 109.5 .
C78 C81 H81B 109.5 .
C78 C81 H81C 109.5 .
H81A C81 H81B 109.5 .
H81A C81 H81C 109.5 .
H81B C81 H81C 109.5 .
C78 C79 H79A 109.5 .
C78 C79 H79B 109.5 .
C78 C79 H79C 109.5 .
H79A C79 H79B 109.5 .
H79A C79 H79C 109.5 .
H79B C79 H79C 109.5 .
C6 C77 H77A 109.5 .
C6 C77 H77B 109.5 .
C6 C77 H77C 109.5 .
H77A C77 H77B 109.5 .
H77A C77 H77C 109.5 .
H77B C77 H77C 109.5 .
C6 C82 H82A 109.5 .
C6 C82 H82B 109.5 .
C6 C82 H82C 109.5 .
H82A C82 H82B 109.5 .
H82A C82 H82C 109.5 .
H82B C82 H82C 109.5 .
F26 C100 C209 115.3(11) .
F26 C100 F27 107.3(10) .
F26 C100 F28 103.5(11) .
F27 C100 C209 109.5(11) .
F27 C100 F28 107.9(11) .
F28 C100 C209 112.9(10) .
N5 C501 C502 171(3) .
O5 C89 O58 92(5) 2_557
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 Ag3 2.9395(11) .
Ag1 Ag2 2.8609(11) .
Ag1 Ag5 2.8925(11) .
Ag1 Ag6 3.2037(12) .
Ag1 Ag26 3.1360(12) .
Ag1 Ag29 3.2163(12) .
Ag1 Ag28 2.9227(13) .
Ag1 S1 2.438(2) .
Ag1 S2 2.420(3) .
Ag3 Ag2 2.8635(11) .
Ag3 Ag9 3.1373(11) .
Ag3 Ag4 2.9380(12) .
Ag3 Ag30 3.1301(12) .
Ag3 Ag31 3.0257(14) .
Ag3 Ag27 3.2890(15) .
Ag3 S3 2.441(3) .
Ag3 S1 2.440(2) .
Ag2 Ag8 3.0501(12) .
Ag2 Ag30 3.1581(12) .
Ag2 Ag19 3.2658(12) .
Ag2 Ag29 3.0965(11) .
Ag2 S3 2.526(3) .
Ag2 S2 2.546(2) .
Ag2 O100 2.585(9) .
Ag11 Ag5 2.9856(12) .
Ag11 Ag10 2.9206(12) .
Ag11 S4 2.503(3) .
Ag11 S11 2.415(3) .
Ag11 O11 2.336(9) .
Ag9 Ag15 3.0998(13) .
Ag9 Ag22 3.0670(14) .
Ag9 S3 2.663(3) .
Ag9 S9 2.467(3) .
Ag9 S8 2.525(3) .
Ag14 Ag8 3.1123(12) .
Ag14 Ag15 3.0079(13) .
Ag14 S8 2.646(3) .
Ag14 S14 2.474(3) .
Ag14 O2 2.398(8) .
Ag14 N2 2.343(11) .
Ag5 Ag4 3.3666(11) .
Ag5 S5 2.457(3) .
Ag5 S1 2.614(3) .
Ag5 S4 2.604(3) .
Ag10 Ag4 2.9978(12) .
Ag10 S4 2.478(3) .
Ag10 S10 2.394(3) .
Ag10 O10 2.372(9) .
Ag4 S1 2.654(2) .
Ag4 S9 2.491(3) .
Ag4 S4 2.624(3) .
Ag18 Ag13 3.2492(13) .
Ag18 Ag26 3.1020(13) .
Ag18 Ag12 3.0753(13) .
Ag18 S13 2.390(3) .
Ag18 S12 2.426(3) .
Ag8 S8 2.424(3) .
Ag8 S7 2.403(3) .
Ag13 Ag7 3.0095(12) .
Ag13 Ag12 3.2287(14) .
Ag13 S6 2.578(3) .
Ag13 S13 2.456(3) .
Ag13 O20 2.252(9) .
Ag20 Ag30 3.1663(13) .
Ag20 S3 2.828(3) .
Ag20 S19 2.411(3) .
Ag20 S14 2.382(3) .
Ag6 Ag17 3.1540(13) .
Ag6 Ag7 3.2980(12) .
Ag6 S5 2.475(3) .
Ag6 S2 2.698(3) .
Ag6 S6 2.543(3) .
Ag30 Ag29 3.0493(13) .
Ag30 Ag27 2.9689(14) .
Ag30 S3 2.601(3) .
Ag30 S20 2.549(3) .
Ag30 S19 2.817(3) .
Ag30 O13 2.360(9) .
Ag17 Ag26 3.0171(14) .
Ag17 Ag16 2.9044(13) .
Ag17 S5 2.558(2) .
Ag17 S12 2.447(3) .
Ag17 O6 2.299(9) .
Ag23 Ag22 2.9391(13) .
Ag23 S9 2.672(3) .
Ag23 S16 2.524(3) .
Ag23 S10 2.519(3) .
Ag23 O4 2.323(10) .
Ag24 Ag25 3.0344(13) .
Ag24 Ag31 3.1571(15) .
Ag24 S10 2.374(3) .
Ag24 S17 2.410(3) .
Ag7 S2 2.951(3) .
Ag7 S6 2.455(3) .
Ag7 S7 2.426(3) .
Ag25 Ag28 3.1590(16) .
Ag25 S11 2.371(3) .
Ag25 S17 2.397(3) .
Ag26 Ag29 3.0294(14) .
Ag26 Ag28 3.3700(16) .
Ag26 S2 2.617(3) .
Ag26 S12 2.941(3) .
Ag26 S18 2.474(3) .
Ag26 O8 2.386(8) .
Ag16 S5 2.733(3) .
Ag16 S11 2.508(3) .
Ag16 S18 2.563(3) .
Ag16 O7 2.330(9) .
Ag15 Ag21 3.1720(13) .
Ag15 S8 2.487(3) .
Ag15 S15 2.411(3) .
Ag15 O1 2.341(9) .
Ag21 S15 2.506(3) .
Ag21 S14 2.454(3) .
Ag21 N1 2.341(13) .
Ag19 S19 2.449(3) .
Ag19 S13 2.440(3) .
Ag19 S7 2.739(3) .
Ag29 Ag28 3.3669(17) .
Ag29 S20 2.636(3) .
Ag29 S2 2.624(3) .
Ag29 S19 2.861(3) .
Ag29 O9 2.342(8) .
Ag22 Ag27 3.0269(13) .
Ag22 S9 2.563(3) .
Ag22 S15 2.448(3) .
Ag22 O3 2.408(11) .
Ag12 S6 2.545(3) .
Ag12 S12 2.508(3) .
Ag12 N3 2.350(13) .
Ag12 N4 2.420(12) .
Ag31 S20 2.538(3) .
Ag31 S16 2.437(3) .
Ag31 S17 2.814(3) .
Ag27 S3 2.569(3) .
Ag27 S16 2.483(3) .
Ag27 O12 2.391(9) .
Ag28 S20 2.465(3) .
Ag28 S18 2.427(3) .
S5 C11 1.881(10) .
S20 C2 1.882(10) .
S9 C9 1.879(11) .
S6 C15 1.866(11) .
S19 C13 1.869(10) .
S8 C8 1.880(10) .
S16 C3 1.868(11) .
S4 C23 1.904(12) .
S15 C4 1.861(10) .
S13 C17 1.856(11) .
S14 C5 1.863(11) .
S11 C6 1.858(12) .
S10 C20 1.856(12) .
S7 C29 1.865(12) .
S12 C1 1.867(10) .
S18 C42 1.837(11) .
O10 C33 1.226(15) .
O13 C28 1.243(15) .
O9 C7 1.230(13) .
O3 C44 1.222(15) .
O2 C14 1.242(15) .
O8 C7 1.214(13) .
O12 C28 1.225(14) .
O6 C38 1.233(16) .
O7 C38 1.240(16) .
C9 C10 1.532(17) .
C9 C41 1.511(16) .
C9 C63 1.511(18) .
C11 C12 1.514(15) .
C11 C25 1.511(16) .
C11 C26 1.493(15) .
C13 C21 1.517(16) .
C13 C22 1.480(15) .
C13 C58 1.533(17) .
C4 C27 1.515(15) .
C4 C40 1.524(18) .
C4 C65 1.506(18) .
O1 C14 1.212(14) .
C3 C50 1.515(17) .
C3 C70 1.511(18) .
C3 C76 1.481(17) .
C8 C30 1.541(16) .
C8 C31 1.503(16) .
C8 C36 1.526(15) .
O4 C44 1.219(15) .
C5 C32 1.503(17) .
C5 C59 1.553(17) .
C5 C67 1.492(17) .
C7 C55 1.553(16) .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C2 C57 1.516(18) .
C2 C74 1.486(18) .
C2 C75 1.468(17) .
O11 C33 1.245(15) .
C10 H10A 0.9600 .
C10 H10B 0.9600 .
C10 H10C 0.9600 .
C1 C39 1.512(17) .
C1 C52 1.532(17) .
C1 C51 1.518(16) .
C6 C37 1.509(17) .
C6 C77 1.55(2) .
C6 C82 1.50(2) .
C19 H19A 0.9600 .
C19 H19B 0.9600 .
C19 H19C 0.9600 .
C19 C17 1.517(16) .
C27 H27A 0.9600 .
C27 H27B 0.9600 .
C27 H27C 0.9600 .
C30 H30A 0.9600 .
C30 H30B 0.9600 .
C30 H30C 0.9600 .
C15 C16 1.531(16) .
C15 C45 1.497(18) .
C15 C46 1.535(17) .
C14 C62 1.557(17) .
C23 C24 1.501(16) .
C23 C35 1.499(18) .
C23 C64 1.519(17) .
C25 H25A 0.9600 .
C25 H25B 0.9600 .
C25 H25C 0.9600 .
C16 H16A 0.9600 .
C16 H16B 0.9600 .
C16 H16C 0.9600 .
C17 C18 1.528(15) .
C17 C34 1.514(16) .
C29 C47 1.529(18) .
C29 C69 1.548(17) .
C29 C71 1.50(2) .
C31 H31A 0.9600 .
C31 H31B 0.9600 .
C31 H31C 0.9600 .
C21 H21A 0.9600 .
C21 H21B 0.9600 .
C21 H21C 0.9600 .
C22 H22A 0.9600 .
C22 H22B 0.9600 .
C22 H22C 0.9600 .
C26 H26A 0.9600 .
C26 H26B 0.9600 .
C26 H26C 0.9600 .
C28 C68 1.527(19) .
C24 H24A 0.9600 .
C24 H24B 0.9600 .
C24 H24C 0.9600 .
C20 C56 1.520(19) .
C20 C61 1.496(18) .
C20 C72 1.508(19) .
C18 H18A 0.9600 .
C18 H18B 0.9600 .
C18 H18C 0.9600 .
O101 C48 1.234(15) .
O100 C48 1.217(15) .
C43 H43A 0.9600 .
C43 H43B 0.9600 .
C43 H43C 0.9600 .
C43 C42 1.549(17) .
C201 N1 1.116(17) .
C201 C203 1.475(19) .
C44 C73 1.550(19) .
C36 H36A 0.9600 .
C36 H36B 0.9600 .
C36 H36C 0.9600 .
C42 C53 1.532(17) .
C42 C54 1.522(17) .
C39 H39A 0.9600 .
C39 H39B 0.9600 .
C39 H39C 0.9600 .
C35 H35A 0.9600 .
C35 H35B 0.9600 .
C35 H35C 0.9600 .
C40 H40A 0.9600 .
C40 H40B 0.9600 .
C40 H40C 0.9600 .
C37 H37A 0.9600 .
C37 H37B 0.9600 .
C37 H37C 0.9600 .
C41 H41A 0.9600 .
C41 H41B 0.9600 .
C41 H41C 0.9600 .
C34 H34A 0.9600 .
C34 H34B 0.9600 .
C34 H34C 0.9600 .
C38 C66 1.530(18) .
C33 C60 1.528(17) .
C32 H32A 0.9600 .
C32 H32B 0.9600 .
C32 H32C 0.9600 .
F4 C55 1.297(15) .
F5 C55 1.350(17) .
F3 C49 1.316(14) .
N2 C202 1.128(15) .
F1 C49 1.306(15) .
F2 C49 1.321(14) .
F6 C55 1.315(17) .
C49 C48 1.548(17) .
C45 H45A 0.9600 .
C45 H45B 0.9600 .
C45 H45C 0.9600 .
C53 H53A 0.9600 .
C53 H53B 0.9600 .
C53 H53C 0.9600 .
C202 C204 1.460(18) .
C52 H52A 0.9600 .
C52 H52B 0.9600 .
C52 H52C 0.9600 .
C58 H58A 0.9600 .
C58 H58B 0.9600 .
C58 H58C 0.9600 .
C50 H50A 0.9600 .
C50 H50B 0.9600 .
C50 H50C 0.9600 .
C51 H51A 0.9600 .
C51 H51B 0.9600 .
C51 H51C 0.9600 .
C56 H56A 0.9600 .
C56 H56B 0.9600 .
C56 H56C 0.9600 .
C47 H47A 0.9600 .
C47 H47B 0.9600 .
C47 H47C 0.9600 .
C54 H54A 0.9600 .
C54 H54B 0.9600 .
C54 H54C 0.9600 .
C46 H46A 0.9600 .
C46 H46B 0.9600 .
C46 H46C 0.9600 .
C57 H57A 0.9600 .
C57 H57B 0.9600 .
C57 H57C 0.9600 .
C59 H59A 0.9600 .
C59 H59B 0.9600 .
C59 H59C 0.9600 .
F7 C60 1.345(16) .
F10 C62 1.304(17) .
F11 C62 1.304(16) .
F12 C62 1.363(17) .
F16 C68 1.242(16) .
F14 C66 1.260(18) .
F8 C60 1.271(17) .
F9 C60 1.334(17) .
N3 C205 1.127(17) .
C68 F17 1.243(19) .
C68 F18 1.22(2) .
C205 C206 1.45(2) .
C67 H67A 0.9600 .
C67 H67B 0.9600 .
C67 H67C 0.9600 .
F13 C66 1.32(2) .
C61 H61A 0.9600 .
C61 H61B 0.9600 .
C61 H61C 0.9600 .
C64 H64A 0.9600 .
C64 H64B 0.9600 .
C64 H64C 0.9600 .
C63 H63A 0.9600 .
C63 H63B 0.9600 .
C63 H63C 0.9600 .
C69 H69A 0.9600 .
C69 H69B 0.9600 .
C69 H69C 0.9600 .
C204 H20A 0.9600 .
C204 H20B 0.9600 .
C204 H20C 0.9600 .
F15 C66 1.26(2) .
C203 H20D 0.9600 .
C203 H20E 0.9600 .
C203 H20F 0.9600 .
C65 H65A 0.9600 .
C65 H65B 0.9600 .
C65 H65C 0.9600 .
C70 H70A 0.9600 .
C70 H70B 0.9600 .
C70 H70C 0.9600 .
F20 C73 1.272(19) .
N4 C207 1.119(19) .
F19 C73 1.320(19) .
C206 H20G 0.9600 .
C206 H20H 0.9600 .
C206 H20I 0.9600 .
C207 C208 1.46(2) .
C74 H74A 0.9600 .
C74 H74B 0.9600 .
C74 H74C 0.9600 .
C72 H72A 0.9600 .
C72 H72B 0.9600 .
C72 H72C 0.9600 .
C71 H71A 0.9600 .
C71 H71B 0.9600 .
C71 H71C 0.9600 .
F22 C73 1.30(2) .
C76 H76A 0.9600 .
C76 H76B 0.9600 .
C76 H76C 0.9600 .
C75 H75A 0.9600 .
C75 H75B 0.9600 .
C75 H75C 0.9600 .
C208 H20J 0.9600 .
C208 H20K 0.9600 .
C208 H20L 0.9600 .
S17 C78 1.874(11) .
O20 C209 1.233(15) .
O21 C209 1.254(16) .
C78 C80 1.514(17) .
C78 C81 1.515(17) .
C78 C79 1.522(17) .
C80 H80A 0.9600 .
C80 H80B 0.9600 .
C80 H80C 0.9600 .
C209 C100 1.524(17) .
C81 H81A 0.9600 .
C81 H81B 0.9600 .
C81 H81C 0.9600 .
C79 H79A 0.9600 .
C79 H79B 0.9600 .
C79 H79C 0.9600 .
C77 H77A 0.9600 .
C77 H77B 0.9600 .
C77 H77C 0.9600 .
C82 H82A 0.9600 .
C82 H82B 0.9600 .
C82 H82C 0.9600 .
F26 C100 1.300(14) .
F27 C100 1.321(14) .
F28 C100 1.362(15) .
C501 N5 1.12(3) .
C501 C502 1.47(3) .
O5 C89 1.67(8) .
O58 C89 2.50(9) 2_557
C89 O58 2.50(9) 2_557
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
Ag2 O100 C48 O101 27(2)
Ag2 O100 C48 C49 -166.9(8)
Ag11 S11 C6 C37 -57.2(10)
Ag11 S11 C6 C77 59.2(10)
Ag11 S11 C6 C82 177.8(11)
Ag11 O11 C33 O10 -5(2)
Ag11 O11 C33 C60 176.8(9)
Ag9 S9 C9 C10 172.9(8)
Ag9 S9 C9 C41 -67.3(9)
Ag9 S9 C9 C63 53.7(9)
Ag9 S8 C8 C30 -176.3(7)
Ag9 S8 C8 C31 62.2(9)
Ag9 S8 C8 C36 -57.3(9)
Ag14 S8 C8 C30 18.5(9)
Ag14 S8 C8 C31 -103.0(8)
Ag14 S8 C8 C36 137.5(7)
Ag14 S14 C5 C32 177.3(7)
Ag14 S14 C5 C59 -64.0(8)
Ag14 S14 C5 C67 54.8(10)
Ag14 O2 C14 O1 12(2)
Ag14 O2 C14 C62 -162.9(9)
Ag5 S5 C11 C12 172.2(7)
Ag5 S5 C11 C25 54.6(8)
Ag5 S5 C11 C26 -68.0(8)
Ag10 S10 C20 C56 -65.7(10)
Ag10 S10 C20 C61 52.9(11)
Ag10 S10 C20 C72 173.7(9)
Ag10 O10 C33 O11 -13(2)
Ag10 O10 C33 C60 164.6(8)
Ag4 S9 C9 C10 70.2(9)
Ag4 S9 C9 C41 -170.0(8)
Ag4 S9 C9 C63 -49.1(9)
Ag18 S13 C17 C19 53.5(9)
Ag18 S13 C17 C18 171.9(7)
Ag18 S13 C17 C34 -68.6(9)
Ag18 S12 C1 C39 -137.4(9)
Ag18 S12 C1 C52 103.9(8)
Ag18 S12 C1 C51 -16.2(11)
Ag8 S8 C8 C30 -66.8(8)
Ag8 S8 C8 C31 171.7(7)
Ag8 S8 C8 C36 52.2(9)
Ag8 S7 C29 C47 -45.9(10)
Ag8 S7 C29 C69 -164.0(9)
Ag8 S7 C29 C71 75.5(10)
Ag13 S6 C15 C16 53.0(9)
Ag13 S6 C15 C45 -66.5(10)
Ag13 S6 C15 C46 173.2(8)
Ag13 S13 C17 C19 -39.8(9)
Ag13 S13 C17 C18 78.6(8)
Ag13 S13 C17 C34 -161.9(8)
Ag13 O20 C209 O21 17(2)
Ag13 O20 C209 C100 -165.1(8)
Ag20 S19 C13 C21 -57.7(8)
Ag20 S19 C13 C22 179.8(8)
Ag20 S19 C13 C58 59.9(9)
Ag20 S14 C5 C32 -58.5(9)
Ag20 S14 C5 C59 60.2(8)
Ag20 S14 C5 C67 179.0(9)
Ag6 S5 C11 C12 58.6(9)
Ag6 S5 C11 C25 -59.0(8)
Ag6 S5 C11 C26 178.5(7)
Ag6 S6 C15 C16 -129.6(8)
Ag6 S6 C15 C45 110.9(10)
Ag6 S6 C15 C46 -9.4(11)
Ag30 S20 C2 C57 75.1(11)
Ag30 S20 C2 C74 -41.7(10)
Ag30 S20 C2 C75 -166.2(12)
Ag30 S19 C13 C21 -139.3(7)
Ag30 S19 C13 C22 98.1(8)
Ag30 S19 C13 C58 -21.8(10)
Ag30 O13 C28 O12 19(2)
Ag30 O13 C28 C68 -166.0(9)
Ag17 S5 C11 C12 -25.8(9)
Ag17 S5 C11 C25 -143.4(7)
Ag17 S5 C11 C26 94.0(7)
Ag17 S12 C1 C39 65.7(10)
Ag17 S12 C1 C52 -53.0(10)
Ag17 S12 C1 C51 -173.2(9)
Ag17 O6 C38 O7 16(2)
Ag17 O6 C38 C66 -163.2(10)
Ag23 S9 C9 C10 -32.4(10)
Ag23 S9 C9 C41 87.5(9)
Ag23 S9 C9 C63 -151.6(7)
Ag23 S16 C3 C50 -69.3(10)
Ag23 S16 C3 C70 172.7(9)
Ag23 S16 C3 C76 49.4(10)
Ag23 S10 C20 C56 81.2(10)
Ag23 S10 C20 C61 -160.2(9)
Ag23 S10 C20 C72 -39.4(11)
Ag23 O4 C44 O3 -10(2)
Ag23 O4 C44 C73 169.6(10)
Ag24 S10 C20 C56 -174.9(8)
Ag24 S10 C20 C61 -56.3(11)
Ag24 S10 C20 C72 64.5(11)
Ag24 S17 C78 C80 -85.0(8)
Ag24 S17 C78 C81 155.0(8)
Ag24 S17 C78 C79 33.8(10)
Ag7 S6 C15 C16 132.8(8)
Ag7 S6 C15 C45 13.3(11)
Ag7 S6 C15 C46 -107.0(9)
Ag7 S7 C29 C47 70.6(9)
Ag7 S7 C29 C69 -47.5(11)
Ag7 S7 C29 C71 -168.1(8)
Ag25 S11 C6 C37 49.8(10)
Ag25 S11 C6 C77 166.2(9)
Ag25 S11 C6 C82 -75.2(13)
Ag25 S17 C78 C80 -169.5(7)
Ag25 S17 C78 C81 70.5(9)
Ag25 S17 C78 C79 -50.7(10)
Ag26 S12 C1 C39 144.3(8)
Ag26 S12 C1 C52 25.5(10)
Ag26 S12 C1 C51 -94.6(10)
Ag26 S18 C42 C43 21.5(10)
Ag26 S18 C42 C53 -99.3(9)
Ag26 S18 C42 C54 142.4(8)
Ag26 O8 C7 O9 -15.3(19)
Ag26 O8 C7 C55 164.3(8)
Ag16 S5 C11 C12 -96.3(8)
Ag16 S5 C11 C25 146.1(7)
Ag16 S5 C11 C26 23.6(8)
Ag16 S11 C6 C37 161.1(8)
Ag16 S11 C6 C77 -82.4(10)
Ag16 S11 C6 C82 36.2(13)
Ag16 S18 C42 C43 152.0(7)
Ag16 S18 C42 C53 31.2(10)
Ag16 S18 C42 C54 -87.0(9)
Ag16 O7 C38 O6 -20(2)
Ag16 O7 C38 C66 159.6(10)
Ag15 S8 C8 C30 97.6(8)
Ag15 S8 C8 C31 -23.9(9)
Ag15 S8 C8 C36 -143.5(7)
Ag15 S15 C4 C27 -59.0(9)
Ag15 S15 C4 C40 60.8(10)
Ag15 S15 C4 C65 -179.6(9)
Ag15 O1 C14 O2 6(2)
Ag15 O1 C14 C62 -179.1(9)
Ag21 S15 C4 C27 26.7(9)
Ag21 S15 C4 C40 146.5(9)
Ag21 S15 C4 C65 -93.9(9)
Ag21 S14 C5 C32 61.3(9)
Ag21 S14 C5 C59 180.0(7)
Ag21 S14 C5 C67 -61.2(10)
Ag19 S19 C13 C21 51.9(8)
Ag19 S19 C13 C22 -70.7(9)
Ag19 S19 C13 C58 169.4(8)
Ag19 S13 C17 C19 178.0(7)
Ag19 S13 C17 C18 -63.6(9)
Ag19 S13 C17 C34 55.9(9)
Ag19 S7 C29 C47 165.5(7)
Ag19 S7 C29 C69 47.4(11)
Ag19 S7 C29 C71 -73.1(10)
Ag29 S20 C2 C57 154.7(10)
Ag29 S20 C2 C74 37.9(10)
Ag29 S20 C2 C75 -86.6(12)
Ag29 S19 C13 C21 141.4(7)
Ag29 S19 C13 C22 18.9(10)
Ag29 S19 C13 C58 -101.0(8)
Ag29 O9 C7 O8 -12.0(19)
Ag29 O9 C7 C55 168.4(8)
Ag22 S9 C9 C10 -106.4(9)
Ag22 S9 C9 C41 13.5(9)
Ag22 S9 C9 C63 134.4(8)
Ag22 S15 C4 C27 -159.1(7)
Ag22 S15 C4 C40 -39.2(10)
Ag22 S15 C4 C65 80.4(10)
Ag22 O3 C44 O4 6(2)
Ag22 O3 C44 C73 -173.0(10)
Ag12 S6 C15 C16 -31.1(10)
Ag12 S6 C15 C45 -150.6(9)
Ag12 S6 C15 C46 89.1(9)
Ag12 S12 C1 C39 -53.0(10)
Ag12 S12 C1 C52 -171.7(7)
Ag12 S12 C1 C51 68.2(10)
Ag31 S20 C2 C57 -18.3(11)
Ag31 S20 C2 C74 -135.1(9)
Ag31 S20 C2 C75 100.4(12)
Ag31 S16 C3 C50 163.4(9)
Ag31 S16 C3 C70 45.3(10)
Ag31 S16 C3 C76 -78.0(10)
Ag31 S17 C78 C80 0.5(11)
Ag31 S17 C78 C81 -119.5(9)
Ag31 S17 C78 C79 119.3(9)
Ag27 S16 C3 C50 58.3(10)
Ag27 S16 C3 C70 -59.7(10)
Ag27 S16 C3 C76 177.0(9)
Ag27 O12 C28 O13 5.3(19)
Ag27 O12 C28 C68 -169.3(9)
Ag28 S20 C2 C57 -113.2(10)
Ag28 S20 C2 C74 130.0(9)
Ag28 S20 C2 C75 5.5(13)
Ag28 S18 C42 C43 -73.9(9)
Ag28 S18 C42 C53 165.3(8)
Ag28 S18 C42 C54 47.1(9)
O10 C33 C60 F7 13.3(18)
O10 C33 C60 F8 135.2(15)
O10 C33 C60 F9 -102.3(16)
O13 C28 C68 F16 -171.8(16)
O13 C28 C68 F17 70(2)
O13 C28 C68 F18 -49(2)
O9 C7 C55 F4 -43.8(17)
O9 C7 C55 F5 -162.8(12)
O9 C7 C55 F6 79.4(14)
O3 C44 C73 F20 -14(2)
O3 C44 C73 F19 103.4(17)
O3 C44 C73 F22 -137.9(17)
O2 C14 C62 F10 101.7(15)
O2 C14 C62 F11 -24.8(19)
O2 C14 C62 F12 -140.2(13)
O8 C7 C55 F4 136.5(13)
O8 C7 C55 F5 17.6(17)
O8 C7 C55 F6 -100.2(14)
O12 C28 C68 F16 4(2)
O12 C28 C68 F17 -114.6(19)
O12 C28 C68 F18 126(2)
O6 C38 C66 F14 -143.7(17)
O6 C38 C66 F13 -26(2)
O6 C38 C66 F15 85(2)
O7 C38 C66 F14 37(2)
O7 C38 C66 F13 154.9(15)
O7 C38 C66 F15 -95(2)
O1 C14 C62 F10 -74.1(17)
O1 C14 C62 F11 159.4(14)
O1 C14 C62 F12 44.1(16)
O4 C44 C73 F20 166.6(15)
O4 C44 C73 F19 -76.0(19)
O4 C44 C73 F22 43(2)
O11 C33 C60 F7 -168.3(12)
O11 C33 C60 F8 -46.4(18)
O11 C33 C60 F9 76.1(17)
F3 C49 C48 O101 17.4(17)
F3 C49 C48 O100 -150.4(13)
F1 C49 C48 O101 139.1(13)
F1 C49 C48 O100 -28.7(17)
F2 C49 C48 O101 -99.8(14)
F2 C49 C48 O100 92.4(15)
O20 C209 C100 F26 -29.6(17)
O20 C209 C100 F27 91.4(14)
O20 C209 C100 F28 -148.3(12)
O21 C209 C100 F26 148.4(12)
O21 C209 C100 F27 -90.6(14)
O21 C209 C100 F28 29.7(16)
