#------------------------------------------------------------------------------
#$Date: 2020-08-06 16:07:59 +0300 (Thu, 06 Aug 2020) $
#$Revision: 254924 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/12/67/7126733.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7126733
loop_
_publ_author_name
'Kim, Dongwook'
'Seong, Junmo'
'Han, Seungwan'
'Baek, Seung Bin'
'Lah, Myoung Soo'
_publ_section_title
;
 Pore space partition of a fragile Ag(i)-carboxylate framework via
 post-synthetic linker insertion.
;
_journal_issue                   61
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              8615
_journal_page_last               8618
_journal_paper_doi               10.1039/d0cc03472j
_journal_volume                  56
_journal_year                    2020
_chemical_formula_sum            'C252.21 H144.14 Ag24 N6.04 O48'
_chemical_formula_weight         6615.83
_space_group_crystal_system      monoclinic
_space_group_IT_number           5
_space_group_name_Hall           'I 2y'
_space_group_name_H-M_alt        'I 1 2 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-06-04 deposited with the CCDC.	2020-06-19 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 107.21(3)
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   34.592(7)
_cell_length_b                   6.2570(13)
_cell_length_c                   35.505(18)
_cell_measurement_reflns_used    79935
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      23.198
_cell_measurement_theta_min      1.697
_cell_volume                     7341(4)
_computing_cell_refinement       HKL3000
_computing_data_collection       'PAL BL2D-SMDC Program'
_computing_data_reduction        HKL3000
_computing_molecular_graphics    ORTEP
_computing_publication_material  CIFTAB
_computing_structure_refinement  SHELXL
_computing_structure_solution    SHELXS
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.940
_diffrn_measured_fraction_theta_max 0.940
_diffrn_measurement_device_type  'ADSC Q210 CCD area detector'
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.700
_diffrn_reflns_av_R_equivalents  0.0381
_diffrn_reflns_av_unetI/netI     0.0508
_diffrn_reflns_Laue_measured_fraction_full 0.940
_diffrn_reflns_Laue_measured_fraction_max 0.940
_diffrn_reflns_limit_h_max       36
_diffrn_reflns_limit_h_min       -36
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       39
_diffrn_reflns_limit_l_min       -39
_diffrn_reflns_number            20422
_diffrn_reflns_point_group_measured_fraction_full 0.952
_diffrn_reflns_point_group_measured_fraction_max 0.952
_diffrn_reflns_theta_full        23.198
_diffrn_reflns_theta_max         23.198
_diffrn_reflns_theta_min         1.697
_diffrn_source                   'PLSII 2D bending magnet'
_exptl_absorpt_coefficient_mu    1.533
_exptl_absorpt_correction_T_max  0.968
_exptl_absorpt_correction_T_min  0.916
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   HKL3000
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.497
_exptl_crystal_description       plate
_exptl_crystal_F_000             3212
_exptl_crystal_size_max          0.058
_exptl_crystal_size_mid          0.052
_exptl_crystal_size_min          0.021
_refine_diff_density_max         1.042
_refine_diff_density_min         -0.683
_refine_diff_density_rms         0.087
_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.47(5)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.982
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     752
_refine_ls_number_reflns         10393
_refine_ls_number_restraints     152
_refine_ls_restrained_S_all      0.983
_refine_ls_R_factor_all          0.0739
_refine_ls_R_factor_gt           0.0519
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1020P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1420
_refine_ls_wR_factor_ref         0.1557
_reflns_Friedel_coverage         0.831
_reflns_Friedel_fraction_full    0.968
_reflns_Friedel_fraction_max     0.968
_reflns_number_gt                7322
_reflns_number_total             10393
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d0cc03472j2.cif
_cod_data_source_block           2-AgBTB-dpey
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 

 Adding full bibliography for 7126731--7126734.cif.
;
_cod_original_sg_symbol_H-M      'I 2'
_cod_database_code               7126733
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.28150(4) 2.5404(2) 0.49419(5) 0.1149(5) Uani 1 1 d . . . . .
Ag2 Ag 0.20857(4) 2.6092(2) 0.50929(5) 0.1285(6) Uani 1 1 d . . . . .
Ag3 Ag 0.53300(4) 0.2685(3) 0.71532(5) 0.1227(6) Uani 1 1 d . . . . .
Ag4 Ag 0.57175(4) 0.6790(3) 0.71660(4) 0.1143(5) Uani 1 1 d . . . . .
Ag5 Ag 0.03952(4) 0.8267(2) 0.73069(4) 0.1168(6) Uani 1 1 d . . . . .
Ag6 Ag 0.07567(4) 0.4283(3) 0.72178(4) 0.1158(5) Uani 1 1 d . . . . .
O1 O 0.2864(3) 2.261(2) 0.5323(3) 0.102(4) Uani 1 1 d . . . . .
O2 O 0.2250(4) 2.2910(18) 0.5356(4) 0.121(4) Uani 1 1 d . . . . .
O3 O 0.4831(2) 0.5054(15) 0.7156(3) 0.073(2) Uani 1 1 d . . . . .
O4 O 0.5117(3) 0.8042(16) 0.7008(3) 0.090(3) Uani 1 1 d . . . . .
O5 O 0.0967(3) 0.9654(16) 0.7220(3) 0.082(3) Uani 1 1 d . . . . .
O6 O 0.1248(2) 0.6330(18) 0.7262(3) 0.081(3) Uani 1 1 d . . . . .
C1 C 0.2839(3) 1.4381(19) 0.6370(3) 0.052(3) Uani 1 1 d . . . . .
C2 C 0.3204(3) 1.3208(18) 0.6460(3) 0.052(3) Uani 1 1 d . . . . .
H2 H 0.340938 1.366547 0.635960 0.062 Uiso 1 1 calc R U . . .
C3 C 0.3268(3) 1.1275(18) 0.6710(3) 0.049(3) Uani 1 1 d . . . . .
C4 C 0.2986(4) 1.0711(19) 0.6885(4) 0.066(3) Uani 1 1 d . . . . .
H4 H 0.304801 0.967894 0.708267 0.079 Uiso 1 1 calc R U . . .
C5 C 0.2591(3) 1.1681(18) 0.6772(3) 0.054(3) Uani 1 1 d . . . . .
C6 C 0.2539(4) 1.358(2) 0.6527(4) 0.070(4) Uani 1 1 d . . . . .
H6 H 0.229428 1.430913 0.647121 0.084 Uiso 1 1 calc R U . . .
C7 C 0.2771(3) 1.6215(18) 0.6119(3) 0.047(3) Uani 1 1 d . . . . .
C8 C 0.3079(4) 1.702(2) 0.5988(4) 0.077(4) Uani 1 1 d . . . . .
H8 H 0.333458 1.639783 0.605141 0.093 Uiso 1 1 calc R U . . .
C9 C 0.2981(4) 1.885(2) 0.5752(4) 0.072(4) Uani 1 1 d . . . . .
H9 H 0.318464 1.939355 0.565820 0.086 Uiso 1 1 calc R U . . .
C10 C 0.2637(4) 1.988(2) 0.5647(4) 0.072(4) Uani 1 1 d . . . . .
C11 C 0.2360(4) 1.910(2) 0.5833(4) 0.078(4) Uani 1 1 d . . . . .
H11 H 0.211929 1.986376 0.579043 0.093 Uiso 1 1 calc R U . . .
C12 C 0.2407(4) 1.731(2) 0.6075(4) 0.085(4) Uani 1 1 d . . . . .
H12 H 0.221583 1.687468 0.619628 0.103 Uiso 1 1 calc R U . . .
C13 C 0.2553(5) 2.208(2) 0.5428(4) 0.083(4) Uani 1 1 d . . . . .
C14 C 0.3668(4) 1.023(2) 0.6806(4) 0.062(3) Uani 1 1 d . . . . .
C15 C 0.3711(4) 0.816(2) 0.6916(4) 0.070(3) Uani 1 1 d . . . . .
H15 H 0.348740 0.740307 0.693826 0.084 Uiso 1 1 calc R U . . .
C16 C 0.4080(3) 0.716(2) 0.6996(4) 0.075(4) Uani 1 1 d . . . . .
H16 H 0.410304 0.577582 0.709672 0.089 Uiso 1 1 calc R U . . .
C17 C 0.4408(3) 0.8068(19) 0.6937(3) 0.057(3) Uani 1 1 d . . . . .
C18 C 0.4371(4) 1.016(2) 0.6820(4) 0.076(4) Uani 1 1 d . . . . .
H18 H 0.459466 1.090786 0.679647 0.091 Uiso 1 1 calc R U . . .
C19 C 0.4002(3) 1.114(2) 0.6739(4) 0.073(4) Uani 1 1 d . . . . .
H19 H 0.397618 1.251266 0.663200 0.087 Uiso 1 1 calc R U . . .
C20 C 0.4831(4) 0.695(2) 0.7040(3) 0.058(3) Uani 1 1 d . . . . .
C21 C 0.2297(4) 1.096(2) 0.6950(4) 0.077(4) Uani 1 1 d . . . . .
C22 C 0.1969(5) 1.201(2) 0.6986(5) 0.091(5) Uani 1 1 d . . . . .
H22 H 0.197452 1.345933 0.693037 0.109 Uiso 1 1 calc R U . . .
C23 C 0.1645(3) 1.147(3) 0.7080(5) 0.085(5) Uani 1 1 d . . . . .
H23 H 0.145111 1.247098 0.709672 0.102 Uiso 1 1 calc R U . . .
C24 C 0.1607(4) 0.933(2) 0.7154(5) 0.079(4) Uani 1 1 d . . . . .
C25 C 0.1932(4) 0.803(3) 0.7164(4) 0.090(5) Uani 1 1 d . . . . .
H25 H 0.193669 0.660352 0.723544 0.108 Uiso 1 1 calc R U . . .
C26 C 0.2270(3) 0.900(3) 0.7056(4) 0.078(4) Uani 1 1 d . . . . .
H26 H 0.248895 0.811760 0.706576 0.094 Uiso 1 1 calc R U . . .
C27 C 0.1249(6) 0.846(3) 0.7218(5) 0.102(5) Uani 1 1 d . . . . .
O7 O -0.4051(3) 0.144(2) 0.7193(3) 0.098(4) Uani 1 1 d . . . . .
O8 O -0.3773(3) 0.468(2) 0.7210(3) 0.091(3) Uani 1 1 d . . . . .
O9 O -0.2106(3) -1.1294(15) 0.5302(3) 0.095(3) Uani 1 1 d . . . . .
O10 O -0.2715(3) -1.1700(15) 0.5380(3) 0.092(3) Uani 1 1 d . . . . .
O11 O -0.0134(3) 0.6113(19) 0.7221(3) 0.088(3) Uani 1 1 d . . . . .
O12 O 0.0139(2) 0.3182(15) 0.7054(3) 0.084(3) Uani 1 1 d . . . . .
C28 C -0.2355(3) -0.0598(19) 0.6806(4) 0.063(3) Uani 1 1 d . . . . .
C29 C -0.2438(3) -0.2240(19) 0.6563(4) 0.066(4) Uani 1 1 d . . . . .
H29 H -0.268901 -0.290762 0.650060 0.079 Uiso 1 1 calc R U . . .
C30 C -0.2129(3) -0.2976(18) 0.6396(4) 0.061(3) Uani 1 1 d . . . . .
C31 C -0.1759(3) -0.188(2) 0.6506(4) 0.063(3) Uani 1 1 d . . . . .
H31 H -0.155691 -0.234254 0.640061 0.076 Uiso 1 1 calc R U . . .
C32 C -0.1685(3) -0.031(2) 0.6739(4) 0.062(3) Uani 1 1 d . . . . .
C33 C -0.1997(3) 0.0424(19) 0.6901(3) 0.053(3) Uani 1 1 d . . . . .
H33 H -0.195210 0.159470 0.706981 0.063 Uiso 1 1 calc R U . . .
C34 C -0.2721(3) 0.020(2) 0.6939(3) 0.060(3) Uani 1 1 d . . . . .
C35 C -0.3000(4) -0.115(2) 0.6956(5) 0.088(5) Uani 1 1 d . . . . .
H35 H -0.297461 -0.259632 0.690672 0.106 Uiso 1 1 calc R U . . .
C36 C -0.3356(6) -0.035(3) 0.7056(7) 0.139(8) Uani 1 1 d . . . . .
H36 H -0.356283 -0.126974 0.706710 0.167 Uiso 1 1 calc R U . . .
C37 C -0.3378(4) 0.196(2) 0.7138(4) 0.071(4) Uani 1 1 d . . . . .
C38 C -0.3045(3) 0.310(2) 0.7148(4) 0.084(4) Uani 1 1 d . . . . .
H38 H -0.304933 0.454269 0.721058 0.100 Uiso 1 1 calc R U . . .
C39 C -0.2700(4) 0.238(2) 0.7075(4) 0.071(4) Uani 1 1 d . . . . .
H39 H -0.247140 0.322590 0.711030 0.085 Uiso 1 1 calc R U . . .
C40 C -0.3790(4) 0.274(3) 0.7203(4) 0.070(4) Uani 1 1 d . . . . .
C41 C -0.2211(4) -0.5044(19) 0.6133(4) 0.069(4) Uani 1 1 d . . . . .
C42 C -0.1959(5) -0.564(3) 0.5898(5) 0.103(5) Uani 1 1 d . . . . .
H42 H -0.173831 -0.476804 0.590712 0.123 Uiso 1 1 calc R U . . .
C43 C -0.2020(5) -0.736(3) 0.5665(6) 0.118(7) Uani 1 1 d . . . . .
H43 H -0.184802 -0.760412 0.551149 0.142 Uiso 1 1 calc R U . . .
C44 C -0.2314(5) -0.873(3) 0.5645(5) 0.081(5) Uani 1 1 d . . . . .
C45 C -0.2581(8) -0.819(3) 0.5774(7) 0.149(10) Uani 1 1 d . . . . .
H45 H -0.281826 -0.899542 0.570789 0.178 Uiso 1 1 calc R U . . .
C46 C -0.2554(4) -0.628(2) 0.6041(5) 0.100(6) Uani 1 1 d . . . . .
H46 H -0.276639 -0.593923 0.613999 0.120 Uiso 1 1 calc R U . . .
C47 C -0.2373(5) -1.068(2) 0.5432(4) 0.074(4) Uani 1 1 d . . . . .
C48 C -0.1297(3) 0.0942(17) 0.6824(3) 0.051(3) Uani 1 1 d . . . . .
C49 C -0.1253(3) 0.299(2) 0.6973(3) 0.061(3) Uani 1 1 d . . . . .
H49 H -0.147398 0.368003 0.701635 0.074 Uiso 1 1 calc R U . . .
C50 C -0.0871(3) 0.4066(19) 0.7062(3) 0.065(4) Uani 1 1 d . . . . .
H50 H -0.084486 0.547226 0.715064 0.078 Uiso 1 1 calc R U . . .
C51 C -0.0558(3) 0.302(2) 0.7015(4) 0.068(4) Uani 1 1 d . . . . .
C52 C -0.0573(3) 0.100(2) 0.6912(5) 0.082(4) Uani 1 1 d . . . . .
H52 H -0.033550 0.029109 0.691579 0.098 Uiso 1 1 calc R U . . .
C53 C -0.0931(3) -0.0094(18) 0.6800(4) 0.064(3) Uani 1 1 d . . . . .
H53 H -0.093954 -0.149246 0.670968 0.077 Uiso 1 1 calc R U . . .
C54 C -0.0152(4) 0.432(3) 0.7124(4) 0.073(4) Uani 1 1 d . . . . .
N1D N 0.1407(3) 2.615(3) 0.5119(4) 0.146(5) Uani 0.957 1 d G U P . .
C1D C 0.1162(5) 2.788(2) 0.4960(5) 0.182(6) Uani 0.957 1 d G U P . .
H1D H 0.126975 2.905635 0.486573 0.218 Uiso 0.957 1 calc R U P . .
C2D C 0.0754(5) 2.786(3) 0.4941(5) 0.184(6) Uani 0.957 1 d G U P . .
H2D H 0.059028 2.902131 0.483437 0.221 Uiso 0.957 1 calc R U P . .
C3D C 0.0593(4) 2.611(4) 0.5081(5) 0.161(6) Uani 0.957 1 d G U P . .
C4D C 0.0838(6) 2.437(3) 0.5241(5) 0.175(6) Uani 0.957 1 d G U P . .
H4D H 0.072969 2.320062 0.533484 0.210 Uiso 0.957 1 calc R U P . .
C5D C 0.1245(5) 2.440(2) 0.5260(4) 0.185(6) Uani 0.957 1 d G U P . .
H5D H 0.140916 2.323562 0.536620 0.222 Uiso 0.957 1 calc R U P . .
C6D C 0.0168(6) 2.647(4) 0.5004(7) 0.151(7) Uani 0.957 1 d . U P . .
N11D N 0.5094(5) 0.242(3) 0.6374(3) 0.093(5) Uani 0.5517 1 d G U P . .
C11D C 0.4901(5) 0.413(2) 0.6145(4) 0.092(5) Uani 0.5517 1 d G U P . .
H11D H 0.478943 0.521628 0.625884 0.111 Uiso 0.5517 1 calc R U P . .
C12D C 0.4873(5) 0.422(2) 0.5747(4) 0.100(5) Uani 0.5517 1 d DG U P . .
H12D H 0.474376 0.536168 0.559413 0.120 Uiso 0.5517 1 calc R U P . .
C13D C 0.5039(5) 0.259(3) 0.5577(3) 0.096(5) Uani 0.5517 1 d DG U P . .
C14D C 0.5233(5) 0.088(2) 0.5806(4) 0.100(5) Uani 0.5517 1 d DG U P . .
H14D H 0.534403 -0.020732 0.569211 0.120 Uiso 0.5517 1 calc R U P . .
C15D C 0.5260(5) 0.079(2) 0.6204(4) 0.096(5) Uani 0.5517 1 d G U P . .
H15D H 0.538970 -0.035276 0.635682 0.115 Uiso 0.5517 1 calc R U P . .
C16D C 0.5008(8) 0.267(4) 0.5148(4) 0.097(6) Uani 0.5517 1 d D U P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0030 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.9078 1.0766 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0059 0.0032 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0105 0.0059 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O10 Ag1 O1 171.7(5) 2_596 . ?
O10 Ag1 Ag2 87.6(3) 2_596 . ?
O1 Ag1 Ag2 85.0(3) . . ?
O9 Ag2 O2 154.6(5) 2_596 . ?
O9 Ag2 N1D 103.6(5) 2_596 . ?
O2 Ag2 N1D 97.5(6) . . ?
O9 Ag2 Ag1 77.6(3) 2_596 . ?
O2 Ag2 Ag1 78.8(3) . . ?
N1D Ag2 Ag1 168.2(4) . . ?
O7 Ag3 O3 159.5(4) 1_655 . ?
O7 Ag3 Ag4 83.0(3) 1_655 . ?
O3 Ag3 Ag4 76.7(2) . . ?
O4 Ag4 O8 161.6(4) . 1_655 ?
O4 Ag4 Ag3 84.9(3) . . ?
O8 Ag4 Ag3 79.8(3) 1_655 . ?
O11 Ag5 O5 158.8(4) . . ?
O11 Ag5 O3 86.9(3) . 4_556 ?
O5 Ag5 O3 114.3(3) . 4_556 ?
O11 Ag5 Ag6 79.9(3) . . ?
O5 Ag5 Ag6 83.7(3) . . ?
O3 Ag5 Ag6 135.7(2) 4_556 . ?
O6 Ag6 O12 158.9(4) . . ?
O6 Ag6 Ag5 80.2(3) . . ?
O12 Ag6 Ag5 82.9(2) . . ?
C13 O1 Ag1 118.1(10) . . ?
C13 O2 Ag2 128.1(12) . . ?
C20 O3 Ag3 122.6(7) . . ?
C20 O3 Ag5 134.2(7) . 4_546 ?
Ag3 O3 Ag5 96.9(3) . 4_546 ?
C20 O4 Ag4 121.2(8) . . ?
C27 O5 Ag5 119.6(11) . . ?
C27 O6 Ag6 128.9(10) . . ?
C6 C1 C2 116.0(11) . . ?
C6 C1 C7 121.9(10) . . ?
C2 C1 C7 122.0(9) . . ?
C1 C2 C3 121.8(9) . . ?
C1 C2 H2 119.1 . . ?
C3 C2 H2 119.1 . . ?
C4 C3 C2 119.4(9) . . ?
C4 C3 C14 122.3(11) . . ?
C2 C3 C14 117.7(9) . . ?
C3 C4 C5 121.0(11) . . ?
C3 C4 H4 119.5 . . ?
C5 C4 H4 119.5 . . ?
C21 C5 C4 119.2(11) . . ?
C21 C5 C6 123.2(10) . . ?
C4 C5 C6 116.9(10) . . ?
C1 C6 C5 123.6(12) . . ?
C1 C6 H6 118.2 . . ?
C5 C6 H6 118.2 . . ?
C8 C7 C12 122.9(12) . . ?
C8 C7 C1 120.2(8) . . ?
C12 C7 C1 116.0(10) . . ?
C7 C8 C9 115.1(10) . . ?
C7 C8 H8 122.4 . . ?
C9 C8 H8 122.4 . . ?
C10 C9 C8 128.1(12) . . ?
C10 C9 H9 116.0 . . ?
C8 C9 H9 116.0 . . ?
C9 C10 C11 112.6(11) . . ?
C9 C10 C13 126.7(13) . . ?
C11 C10 C13 119.1(12) . . ?
C12 C11 C10 126.6(11) . . ?
C12 C11 H11 116.7 . . ?
C10 C11 H11 116.7 . . ?
C11 C12 C7 113.6(13) . . ?
C11 C12 H12 123.2 . . ?
C7 C12 H12 123.2 . . ?
O2 C13 O1 128.0(16) . . ?
O2 C13 C10 122.7(15) . . ?
O1 C13 C10 109.0(14) . . ?
C15 C14 C19 115.3(12) . . ?
C15 C14 C3 120.4(11) . . ?
C19 C14 C3 123.6(12) . . ?
C14 C15 C16 120.9(12) . . ?
C14 C15 H15 119.6 . . ?
C16 C15 H15 119.6 . . ?
C17 C16 C15 123.4(13) . . ?
C17 C16 H16 118.3 . . ?
C15 C16 H16 118.3 . . ?
C16 C17 C18 116.5(11) . . ?
C16 C17 C20 123.4(11) . . ?
C18 C17 C20 119.8(12) . . ?
C17 C18 C19 119.6(12) . . ?
C17 C18 H18 120.2 . . ?
C19 C18 H18 120.2 . . ?
C18 C19 C14 123.7(14) . . ?
C18 C19 H19 118.2 . . ?
C14 C19 H19 118.2 . . ?
O4 C20 O3 129.0(11) . . ?
O4 C20 C17 116.8(12) . . ?
O3 C20 C17 114.1(11) . . ?
C26 C21 C22 107.2(13) . . ?
C26 C21 C5 123.5(10) . . ?
C22 C21 C5 128.6(14) . . ?
C23 C22 C21 135.3(16) . . ?
C23 C22 H22 112.3 . . ?
C21 C22 H22 112.3 . . ?
C22 C23 C24 115.8(14) . . ?
C22 C23 H23 122.1 . . ?
C24 C23 H23 122.1 . . ?
C25 C24 C23 117.1(11) . . ?
C25 C24 C27 120.7(15) . . ?
C23 C24 C27 122.3(14) . . ?
C24 C25 C26 117.3(14) . . ?
C24 C25 H25 121.4 . . ?
C26 C25 H25 121.4 . . ?
C21 C26 C25 126.9(12) . . ?
C21 C26 H26 116.6 . . ?
C25 C26 H26 116.6 . . ?
O5 C27 O6 124.9(15) . . ?
O5 C27 C24 119.7(18) . . ?
O6 C27 C24 115.4(17) . . ?
C40 O7 Ag3 117.3(11) . 1_455 ?
C40 O8 Ag4 125.0(10) . 1_455 ?
C47 O9 Ag2 131.4(9) . 2_516 ?
C47 O10 Ag1 119.4(10) . 2_516 ?
C54 O11 Ag5 126.3(10) . . ?
C54 O12 Ag6 121.9(9) . . ?
C29 C28 C33 122.7(11) . . ?
C29 C28 C34 114.2(10) . . ?
C33 C28 C34 122.8(11) . . ?
C28 C29 C30 118.4(9) . . ?
C28 C29 H29 120.8 . . ?
C30 C29 H29 120.8 . . ?
C31 C30 C29 117.2(10) . . ?
C31 C30 C41 123.8(10) . . ?
C29 C30 C41 118.8(10) . . ?
C32 C31 C30 123.7(11) . . ?
C32 C31 H31 118.2 . . ?
C30 C31 H31 118.2 . . ?
C31 C32 C33 118.5(11) . . ?
C31 C32 C48 122.2(10) . . ?
C33 C32 C48 119.0(11) . . ?
C28 C33 C32 119.5(11) . . ?
C28 C33 H33 120.2 . . ?
C32 C33 H33 120.2 . . ?
C35 C34 C39 124.4(10) . . ?
C35 C34 C28 119.1(12) . . ?
C39 C34 C28 116.1(11) . . ?
C34 C35 C36 118.4(13) . . ?
C34 C35 H35 120.8 . . ?
C36 C35 H35 120.8 . . ?
C35 C36 C37 118.6(13) . . ?
C35 C36 H36 120.7 . . ?
C37 C36 H36 120.7 . . ?
C38 C37 C36 115.3(12) . . ?
C38 C37 C40 129.2(14) . . ?
C36 C37 C40 115.5(14) . . ?
C37 C38 C39 127.3(14) . . ?
C37 C38 H38 116.4 . . ?
C39 C38 H38 116.4 . . ?
C38 C39 C34 114.6(12) . . ?
C38 C39 H39 122.7 . . ?
C34 C39 H39 122.7 . . ?
O7 C40 O8 134.8(14) . . ?
O7 C40 C37 119.0(15) . . ?
O8 C40 C37 105.7(13) . . ?
C46 C41 C42 110.4(12) . . ?
C46 C41 C30 126.7(11) . . ?
C42 C41 C30 121.9(12) . . ?
C43 C42 C41 124.1(15) . . ?
C43 C42 H42 117.9 . . ?
C41 C42 H42 117.9 . . ?
C44 C43 C42 122.4(16) . . ?
C44 C43 H43 118.8 . . ?
C42 C43 H43 118.8 . . ?
C45 C44 C43 118.0(19) . . ?
C45 C44 C47 116.1(19) . . ?
C43 C44 C47 125.2(15) . . ?
C44 C45 C46 123(2) . . ?
C44 C45 H45 118.3 . . ?
C46 C45 H45 118.3 . . ?
C41 C46 C45 119.1(14) . . ?
C41 C46 H46 120.4 . . ?
C45 C46 H46 120.4 . . ?
O9 C47 O10 123.4(14) . . ?
O9 C47 C44 118.1(13) . . ?
O10 C47 C44 118.6(16) . . ?
C49 C48 C53 116.1(9) . . ?
C49 C48 C32 123.4(10) . . ?
C53 C48 C32 120.0(10) . . ?
C48 C49 C50 120.8(11) . . ?
C48 C49 H49 119.6 . . ?
C50 C49 H49 119.6 . . ?
C51 C50 C49 118.6(12) . . ?
C51 C50 H50 120.7 . . ?
C49 C50 H50 120.7 . . ?
C52 C51 C50 123.0(10) . . ?
C52 C51 C54 121.9(11) . . ?
C50 C51 C54 114.9(14) . . ?
C51 C52 C53 121.4(11) . . ?
C51 C52 H52 119.3 . . ?
C53 C52 H52 119.3 . . ?
C52 C53 C48 119.5(10) . . ?
C52 C53 H53 120.2 . . ?
C48 C53 H53 120.2 . . ?
O11 C54 O12 126.8(14) . . ?
O11 C54 C51 122.3(13) . . ?
O12 C54 C51 110.5(14) . . ?
C1D N1D C5D 120.0 . . ?
C1D N1D Ag2 119.1(10) . . ?
C5D N1D Ag2 120.6(10) . . ?
N1D C1D C2D 120.0 . . ?
N1D C1D H1D 120.0 . . ?
C2D C1D H1D 120.0 . . ?
C3D C2D C1D 120.0 . . ?
C3D C2D H2D 120.0 . . ?
C1D C2D H2D 120.0 . . ?
C4D C3D C2D 120.0 . . ?
C4D C3D C6D 132.1(18) . . ?
C2D C3D C6D 107.8(18) . . ?
C3D C4D C5D 120.0 . . ?
C3D C4D H4D 120.0 . . ?
C5D C4D H4D 120.0 . . ?
C4D C5D N1D 120.0 . . ?
C4D C5D H5D 120.0 . . ?
N1D C5D H5D 120.0 . . ?
C6D C6D C3D 167(3) 2_556 . ?
C11D N11D C15D 120.0 . . ?
C12D C11D N11D 120.0 . . ?
C12D C11D H11D 120.0 . . ?
N11D C11D H11D 120.0 . . ?
C13D C12D C11D 120.0 . . ?
C13D C12D H12D 120.0 . . ?
C11D C12D H12D 120.0 . . ?
C12D C13D C14D 120.0 . . ?
C12D C13D C16D 120.3(7) . . ?
C14D C13D C16D 119.7(7) . . ?
C15D C14D C13D 120.0 . . ?
C15D C14D H14D 120.0 . . ?
C13D C14D H14D 120.0 . . ?
C14D C15D N11D 120.0 . . ?
C14D C15D H15D 120.0 . . ?
N11D C15D H15D 120.0 . . ?
C16D C16D C13D 178(2) 2_656 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O10 2.116(8) 2_596 ?
Ag1 O1 2.186(11) . ?
Ag1 Ag2 2.764(2) . ?
Ag2 O9 2.168(9) 2_596 ?
Ag2 O2 2.201(11) . ?
Ag2 N1D 2.378(11) . ?
Ag3 O7 2.246(10) 1_655 ?
Ag3 O3 2.278(7) . ?
Ag3 Ag4 2.891(2) . ?
Ag4 O4 2.135(8) . ?
Ag4 O8 2.171(10) 1_655 ?
Ag5 O11 2.221(9) . ?
Ag5 O5 2.263(9) . ?
Ag5 O3 2.525(9) 4_556 ?
Ag5 Ag6 2.848(2) . ?
Ag6 O6 2.096(9) . ?
Ag6 O12 2.155(8) . ?
O1 C13 1.282(17) . ?
O2 C13 1.131(18) . ?
O3 C20 1.256(15) . ?
O4 C20 1.234(16) . ?
O5 C27 1.23(2) . ?
O6 C27 1.34(2) . ?
C1 C6 1.407(15) . ?
C1 C2 1.413(14) . ?
C1 C7 1.429(16) . ?
C2 C3 1.477(15) . ?
C2 H2 0.9300 . ?
C3 C4 1.350(16) . ?
C3 C14 1.479(15) . ?
C4 C5 1.439(15) . ?
C4 H4 0.9300 . ?
C5 C21 1.419(17) . ?
C5 C6 1.452(17) . ?
C6 H6 0.9300 . ?
C7 C8 1.381(16) . ?
C7 C12 1.398(16) . ?
C8 C9 1.396(16) . ?
C8 H8 0.9300 . ?
C9 C10 1.308(17) . ?
C9 H9 0.9300 . ?
C10 C11 1.403(17) . ?
C10 C13 1.56(2) . ?
C11 C12 1.40(2) . ?
C11 H11 0.9300 . ?
C12 H12 0.9300 . ?
C14 C15 1.346(17) . ?
C14 C19 1.371(15) . ?
C15 C16 1.375(16) . ?
C15 H15 0.9300 . ?
C16 C17 1.341(17) . ?
C16 H16 0.9300 . ?
C17 C18 1.367(18) . ?
C17 C20 1.563(15) . ?
C18 C19 1.368(18) . ?
C18 H18 0.9300 . ?
C19 H19 0.9300 . ?
C21 C26 1.30(2) . ?
C21 C22 1.350(17) . ?
C22 C23 1.305(17) . ?
C22 H22 0.9300 . ?
C23 C24 1.38(2) . ?
C23 H23 0.9300 . ?
C24 C25 1.38(2) . ?
C24 C27 1.432(19) . ?
C25 C26 1.464(18) . ?
C25 H25 0.9300 . ?
C26 H26 0.9300 . ?
O7 C40 1.207(18) . ?
O8 C40 1.216(19) . ?
O9 C47 1.212(17) . ?
O10 C47 1.308(16) . ?
O11 C54 1.168(18) . ?
O12 C54 1.317(16) . ?
C28 C29 1.317(15) . ?
C28 C33 1.345(15) . ?
C28 C34 1.558(15) . ?
C29 C30 1.442(15) . ?
C29 H29 0.9300 . ?
C30 C31 1.401(16) . ?
C30 C41 1.571(16) . ?
C31 C32 1.266(16) . ?
C31 H31 0.9300 . ?
C32 C33 1.441(15) . ?
C32 C48 1.504(15) . ?
C33 H33 0.9300 . ?
C34 C35 1.297(18) . ?
C34 C39 1.441(18) . ?
C35 C36 1.47(2) . ?
C35 H35 0.9300 . ?
C36 C37 1.48(2) . ?
C36 H36 0.9300 . ?
C37 C38 1.349(18) . ?
C37 C40 1.586(17) . ?
C38 C39 1.368(16) . ?
C38 H38 0.9300 . ?
C39 H39 0.9300 . ?
C41 C46 1.371(17) . ?
C41 C42 1.42(2) . ?
C42 C43 1.34(2) . ?
C42 H42 0.9300 . ?
C43 C44 1.31(2) . ?
C43 H43 0.9300 . ?
C44 C45 1.20(3) . ?
C44 C47 1.42(2) . ?
C45 C46 1.51(3) . ?
C45 H45 0.9300 . ?
C46 H46 0.9300 . ?
C48 C49 1.376(17) . ?
C48 C53 1.446(15) . ?
C49 C50 1.433(15) . ?
C49 H49 0.9300 . ?
C50 C51 1.317(16) . ?
C50 H50 0.9300 . ?
C51 C52 1.316(19) . ?
C51 C54 1.568(19) . ?
C52 C53 1.365(15) . ?
C52 H52 0.9300 . ?
C53 H53 0.9300 . ?
N1D C1D 1.3900 . ?
N1D C5D 1.3900 . ?
C1D C2D 1.3900 . ?
C1D H1D 0.9300 . ?
C2D C3D 1.3900 . ?
C2D H2D 0.9300 . ?
C3D C4D 1.3900 . ?
C3D C6D 1.43(2) . ?
C4D C5D 1.3900 . ?
C4D H4D 0.9300 . ?
C5D H5D 0.9300 . ?
C6D C6D 1.15(4) 2_556 ?
N11D C11D 1.3900 . ?
N11D C15D 1.3900 . ?
C11D C12D 1.3900 . ?
C11D H11D 0.9300 . ?
C12D C13D 1.3900 . ?
C12D H12D 0.9300 . ?
C13D C14D 1.3900 . ?
C13D C16D 1.495(9) . ?
C14D C15D 1.3900 . ?
C14D H14D 0.9300 . ?
C15D H15D 0.9300 . ?
C16D C16D 1.04(2) 2_656 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6 C1 C2 C3 -0.8(16) . . . . ?
C7 C1 C2 C3 -178.1(10) . . . . ?
C1 C2 C3 C4 -5.9(16) . . . . ?
C1 C2 C3 C14 -176.7(11) . . . . ?
C2 C3 C4 C5 12.9(17) . . . . ?
C14 C3 C4 C5 -176.7(11) . . . . ?
C3 C4 C5 C21 176.9(12) . . . . ?
C3 C4 C5 C6 -12.9(17) . . . . ?
C2 C1 C6 C5 0.5(17) . . . . ?
C7 C1 C6 C5 177.8(10) . . . . ?
C21 C5 C6 C1 175.8(13) . . . . ?
C4 C5 C6 C1 6.0(16) . . . . ?
C6 C1 C7 C8 176.4(13) . . . . ?
C2 C1 C7 C8 -6.5(17) . . . . ?
C6 C1 C7 C12 7.0(16) . . . . ?
C2 C1 C7 C12 -175.9(12) . . . . ?
C12 C7 C8 C9 -10(2) . . . . ?
C1 C7 C8 C9 -178.5(11) . . . . ?
C7 C8 C9 C10 1(2) . . . . ?
C8 C9 C10 C11 6(2) . . . . ?
C8 C9 C10 C13 171.7(14) . . . . ?
C9 C10 C11 C12 -6(2) . . . . ?
C13 C10 C11 C12 -172.7(14) . . . . ?
C10 C11 C12 C7 -1(2) . . . . ?
C8 C7 C12 C11 10(2) . . . . ?
C1 C7 C12 C11 178.9(12) . . . . ?
Ag2 O2 C13 O1 -12(3) . . . . ?
Ag2 O2 C13 C10 174.9(10) . . . . ?
Ag1 O1 C13 O2 -2(2) . . . . ?
Ag1 O1 C13 C10 172.2(9) . . . . ?
C9 C10 C13 O2 -177.8(17) . . . . ?
C11 C10 C13 O2 -13(2) . . . . ?
C9 C10 C13 O1 8(2) . . . . ?
C11 C10 C13 O1 172.2(13) . . . . ?
C4 C3 C14 C15 31.1(19) . . . . ?
C2 C3 C14 C15 -158.4(12) . . . . ?
C4 C3 C14 C19 -158.1(13) . . . . ?
C2 C3 C14 C19 12.4(18) . . . . ?
C19 C14 C15 C16 7(2) . . . . ?
C3 C14 C15 C16 178.4(11) . . . . ?
C14 C15 C16 C17 -6(2) . . . . ?
C15 C16 C17 C18 5(2) . . . . ?
C15 C16 C17 C20 178.2(11) . . . . ?
C16 C17 C18 C19 -5.5(19) . . . . ?
C20 C17 C18 C19 -178.6(11) . . . . ?
C17 C18 C19 C14 7(2) . . . . ?
C15 C14 C19 C18 -8(2) . . . . ?
C3 C14 C19 C18 -178.7(12) . . . . ?
Ag4 O4 C20 O3 -0.5(19) . . . . ?
Ag4 O4 C20 C17 176.9(7) . . . . ?
Ag3 O3 C20 O4 -21.4(19) . . . . ?
Ag5 O3 C20 O4 123.7(12) 4_546 . . . ?
Ag3 O3 C20 C17 161.2(7) . . . . ?
Ag5 O3 C20 C17 -53.6(16) 4_546 . . . ?
C16 C17 C20 O4 -172.8(12) . . . . ?
C18 C17 C20 O4 -0.1(18) . . . . ?
C16 C17 C20 O3 4.9(18) . . . . ?
C18 C17 C20 O3 177.6(12) . . . . ?
C4 C5 C21 C26 -34(2) . . . . ?
C6 C5 C21 C26 156.8(14) . . . . ?
C4 C5 C21 C22 157.3(15) . . . . ?
C6 C5 C21 C22 -12(2) . . . . ?
C26 C21 C22 C23 -4(3) . . . . ?
C5 C21 C22 C23 166.7(18) . . . . ?
C21 C22 C23 C24 -2(3) . . . . ?
C22 C23 C24 C25 7(2) . . . . ?
C22 C23 C24 C27 -172.9(15) . . . . ?
C23 C24 C25 C26 -6(2) . . . . ?
C27 C24 C25 C26 173.9(13) . . . . ?
C22 C21 C26 C25 5(2) . . . . ?
C5 C21 C26 C25 -166.2(13) . . . . ?
C24 C25 C26 C21 0(2) . . . . ?
Ag5 O5 C27 O6 0(2) . . . . ?
Ag5 O5 C27 C24 178.7(11) . . . . ?
Ag6 O6 C27 O5 16(3) . . . . ?
Ag6 O6 C27 C24 -162.9(10) . . . . ?
C25 C24 C27 O5 177.8(15) . . . . ?
C23 C24 C27 O5 -2(3) . . . . ?
C25 C24 C27 O6 -4(2) . . . . ?
C23 C24 C27 O6 176.1(16) . . . . ?
C33 C28 C29 C30 0.6(19) . . . . ?
C34 C28 C29 C30 174.6(11) . . . . ?
C28 C29 C30 C31 0.1(18) . . . . ?
C28 C29 C30 C41 175.1(11) . . . . ?
C29 C30 C31 C32 -0.1(18) . . . . ?
C41 C30 C31 C32 -174.9(12) . . . . ?
C30 C31 C32 C33 -0.5(18) . . . . ?
C30 C31 C32 C48 -174.8(11) . . . . ?
C29 C28 C33 C32 -1.2(19) . . . . ?
C34 C28 C33 C32 -174.8(10) . . . . ?
C31 C32 C33 C28 1.1(18) . . . . ?
C48 C32 C33 C28 175.6(11) . . . . ?
C29 C28 C34 C35 29.0(18) . . . . ?
C33 C28 C34 C35 -157.0(13) . . . . ?
C29 C28 C34 C39 -157.5(12) . . . . ?
C33 C28 C34 C39 16.6(17) . . . . ?
C39 C34 C35 C36 11(2) . . . . ?
C28 C34 C35 C36 -175.9(15) . . . . ?
C34 C35 C36 C37 -1(3) . . . . ?
C35 C36 C37 C38 -6(3) . . . . ?
C35 C36 C37 C40 174.4(15) . . . . ?
C36 C37 C38 C39 3(2) . . . . ?
C40 C37 C38 C39 -177.3(13) . . . . ?
C37 C38 C39 C34 6(2) . . . . ?
C35 C34 C39 C38 -14(2) . . . . ?
C28 C34 C39 C38 173.1(12) . . . . ?
Ag3 O7 C40 O8 3(2) 1_455 . . . ?
Ag3 O7 C40 C37 -166.9(8) 1_455 . . . ?
Ag4 O8 C40 O7 -4(3) 1_455 . . . ?
Ag4 O8 C40 C37 166.4(7) 1_455 . . . ?
C38 C37 C40 O7 -178.1(14) . . . . ?
C36 C37 C40 O7 2(2) . . . . ?
C38 C37 C40 O8 10(2) . . . . ?
C36 C37 C40 O8 -170.5(16) . . . . ?
C31 C30 C41 C46 174.7(15) . . . . ?
C29 C30 C41 C46 0(2) . . . . ?
C31 C30 C41 C42 -18(2) . . . . ?
C29 C30 C41 C42 167.6(14) . . . . ?
C46 C41 C42 C43 -9(2) . . . . ?
C30 C41 C42 C43 -178.9(16) . . . . ?
C41 C42 C43 C44 -3(3) . . . . ?
C42 C43 C44 C45 16(3) . . . . ?
C42 C43 C44 C47 -174.3(16) . . . . ?
C43 C44 C45 C46 -15(3) . . . . ?
C47 C44 C45 C46 174.2(16) . . . . ?
C42 C41 C46 C45 10(2) . . . . ?
C30 C41 C46 C45 178.6(14) . . . . ?
C44 C45 C46 C41 2(3) . . . . ?
Ag2 O9 C47 O10 7(2) 2_516 . . . ?
Ag2 O9 C47 C44 -171.8(10) 2_516 . . . ?
Ag1 O10 C47 O9 0.4(18) 2_516 . . . ?
Ag1 O10 C47 C44 179.4(9) 2_516 . . . ?
C45 C44 C47 O9 -178.8(18) . . . . ?
C43 C44 C47 O9 11(2) . . . . ?
C45 C44 C47 O10 2(2) . . . . ?
C43 C44 C47 O10 -168.2(17) . . . . ?
C31 C32 C48 C49 159.4(12) . . . . ?
C33 C32 C48 C49 -14.9(18) . . . . ?
C31 C32 C48 C53 -28.9(18) . . . . ?
C33 C32 C48 C53 156.8(11) . . . . ?
C53 C48 C49 C50 5.6(17) . . . . ?
C32 C48 C49 C50 177.6(11) . . . . ?
C48 C49 C50 C51 -3.0(19) . . . . ?
C49 C50 C51 C52 -4(2) . . . . ?
C49 C50 C51 C54 -179.3(10) . . . . ?
C50 C51 C52 C53 8(2) . . . . ?
C54 C51 C52 C53 -177.0(12) . . . . ?
C51 C52 C53 C48 -5(2) . . . . ?
C49 C48 C53 C52 -1.9(18) . . . . ?
C32 C48 C53 C52 -174.1(12) . . . . ?
Ag5 O11 C54 O12 2(2) . . . . ?
Ag5 O11 C54 C51 -171.3(8) . . . . ?
Ag6 O12 C54 O11 12(2) . . . . ?
Ag6 O12 C54 C51 -174.0(7) . . . . ?
C52 C51 C54 O11 -178.9(16) . . . . ?
C50 C51 C54 O11 -4(2) . . . . ?
C52 C51 C54 O12 7.2(18) . . . . ?
C50 C51 C54 O12 -177.6(11) . . . . ?
C5D N1D C1D C2D 0.0 . . . . ?
Ag2 N1D C1D C2D 174.4(9) . . . . ?
N1D C1D C2D C3D 0.0 . . . . ?
C1D C2D C3D C4D 0.0 . . . . ?
C1D C2D C3D C6D -176.6(16) . . . . ?
C2D C3D C4D C5D 0.0 . . . . ?
C6D C3D C4D C5D 176(2) . . . . ?
C3D C4D C5D N1D 0.0 . . . . ?
C1D N1D C5D C4D 0.0 . . . . ?
Ag2 N1D C5D C4D -174.3(9) . . . . ?
C4D C3D C6D C6D 24(13) . . . 2_556 ?
C2D C3D C6D C6D -160(11) . . . 2_556 ?
C15D N11D C11D C12D 0.0 . . . . ?
N11D C11D C12D C13D 0.0 . . . . ?
C11D C12D C13D C14D 0.0 . . . . ?
C11D C12D C13D C16D 179.5(19) . . . . ?
C12D C13D C14D C15D 0.0 . . . . ?
C16D C13D C14D C15D -179.5(19) . . . . ?
C13D C14D C15D N11D 0.0 . . . . ?
C11D N11D C15D C14D 0.0 . . . . ?
