#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/79/7207942.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7207942
loop_
_publ_author_name
'Ma, Jie'
'Jiang, Feilong'
'Chen, Lian'
'Wu, Mingyan'
'Zhang, Shuquan'
'Xiong, Kecai'
'Han, Dong'
'Hong, Maochun'
_publ_section_title
;
 Temperature-controlled reduction of Cu(ii) and structural transformation
 on the assembly of coordination network
;
_journal_issue                   12
_journal_name_full               CrystEngComm
_journal_page_first              4181
_journal_paper_doi               10.1039/c2ce00004k
_journal_volume                  14
_journal_year                    2012
_chemical_formula_moiety         'C28.50 H22.50 Cu2 N4.50 O13.50'
_chemical_formula_sum            'C28.5 H22.5 Cu2 N4.5 O13.5'
_chemical_formula_weight         771.09
_chemical_name_systematic
;
?
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 109.477(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.039(2)
_cell_length_b                   8.7560(6)
_cell_length_c                   21.7481(19)
_cell_measurement_reflns_used    8942
_cell_measurement_temperature    293.1500
_cell_measurement_theta_max      27.4642
_cell_measurement_theta_min      2.2313
_cell_volume                     4136.2(6)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku, 2000)'
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 2008)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293.1500
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'Saturn70 CCD area-detector'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0478
_diffrn_reflns_av_sigmaI/netI    0.0400
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            25537
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.53
_exptl_absorpt_coefficient_mu    1.086
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.7332
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(CrystalClear; Rigaku, 2000)'
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    1.238
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1564
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.070
_refine_diff_density_min         -0.891
_refine_diff_density_rms         0.114
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.074
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     480
_refine_ls_number_reflns         7217
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.074
_refine_ls_R_factor_all          0.0785
_refine_ls_R_factor_gt           0.0678
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1385P)²+1.8306P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1918
_refine_ls_wR_factor_ref         0.2056
_reflns_number_gt                6027
_reflns_number_total             7217
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2ce00004k.txt
_cod_data_source_block           complex2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P2/c
_cod_original_formula_sum        'C28.50 H22.50 Cu2 N4.50 O13.50'
_cod_database_code               7207942
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cu1 Cu 0.25290(2) 0.62591(5) 0.371934(19) 0.03039(19) Uani 1 1 d .
O1 O 0.24745(14) 0.6324(3) 0.46172(13) 0.0392(7) Uani 1 1 d .
N1 N 0.26477(18) 0.2248(4) 0.56703(16) 0.0428(8) Uani 1 1 d .
C1 C 0.2391(3) 0.6417(5) 0.5843(2) 0.0493(12) Uani 1 1 d .
H1 H 0.2335 0.7323 0.5589 0.059 Uiso 1 1 calc R
Cu2 Cu 0.19609(3) 0.19685(6) 0.47981(2) 0.0462(2) Uani 1 1 d .
O2 O 0.22752(16) 0.3858(3) 0.45085(13) 0.0473(8) Uani 1 1 d .
N2 N 0.1274(2) 0.1670(5) 0.39684(19) 0.0570(10) Uani 1 1 d .
C2 C 0.2463(2) 0.5031(4) 0.55629(18) 0.0361(9) Uani 1 1 d .
O3 O 0.2377(2) 0.6445(4) 0.77835(16) 0.0647(11) Uani 1 1 d .
N3 N 0.16060(16) 0.6519(5) 0.32974(17) 0.0429(8) Uani 1 1 d .
C3 C 0.25597(19) 0.3706(4) 0.59494(18) 0.0345(9) Uani 1 1 d .
O4 O 0.26183(13) 0.3999(3) 0.78580(12) 0.0372(6) Uani 1 1 d .
N4 N 0.34219(15) 0.5761(4) 0.41633(15) 0.0376(7) Uani 1 1 d .
C4 C 0.2565(2) 0.3812(4) 0.65862(19) 0.0364(9) Uani 1 1 d .
H4 H 0.2625 0.2914 0.6844 0.044 Uiso 1 1 calc R
O5 O 0.3712(2) 0.0663(6) 0.4935(2) 0.0905(15) Uani 1 1 d .
N5 N -0.0809(5) 0.4201(14) 0.4499(6) 0.086(3) Uani 0.50 1 d P
C5 C 0.24870(19) 0.5199(4) 0.68571(18) 0.0362(9) Uani 1 1 d .
O6 O 0.26920(19) 0.0615(4) 0.46461(17) 0.0683(11) Uani 1 1 d .
C6 C 0.2399(3) 0.6511(5) 0.6477(2) 0.0497(12) Uani 1 1 d .
H6 H 0.2344 0.7470 0.6655 0.060 Uiso 1 1 calc R
O7 O 0.1543(2) 0.0936(5) 0.53233(17) 0.0732(12) Uani 1 1 d .
C7 C 0.24017(19) 0.5057(5) 0.48469(19) 0.0377(9) Uani 1 1 d .
O8 O 0.1694(2) 0.0108(6) 0.6321(2) 0.0921(15) Uani 1 1 d .
C8 C 0.2493(2) 0.5255(5) 0.75545(18) 0.0375(9) Uani 1 1 d .
O9 O 0.26862(17) 0.8729(3) 0.36699(14) 0.0504(8) Uani 1 1 d .
C9 C 0.3253(2) 0.2154(6) 0.5558(2) 0.0534(12) Uani 1 1 d .
H9A H 0.3574 0.1807 0.5963 0.064 Uiso 1 1 calc R
H9B H 0.3370 0.3181 0.5449 0.064 Uiso 1 1 calc R
O10 O -0.1025(6) 0.5664(12) 0.5201(5) 0.106(4) Uani 0.50 1 d P
C10 C 0.3220(3) 0.1030(7) 0.4996(3) 0.0647(15) Uani 1 1 d .
O11 O 0.0393(7) 0.0919(18) 0.5762(9) 0.157(6) Uani 0.50 1 d P
C11 C 0.2552(3) 0.0894(5) 0.6039(2) 0.0553(13) Uani 1 1 d .
H11A H 0.2737 -0.0021 0.5911 0.066 Uiso 1 1 calc R
H11B H 0.2757 0.1062 0.6513 0.066 Uiso 1 1 calc R
C12 C 0.1888(3) 0.0639(6) 0.5903(3) 0.0655(15) Uani 1 1 d .
O13 O 0.4070(4) 0.0428(9) 0.3813(4) 0.154(3) Uani 1 1 d .
C13 C 0.0729(3) 0.1210(8) 0.3961(3) 0.0767(19) Uani 1 1 d .
H13 H 0.0681 0.0893 0.4359 0.092 Uiso 1 1 calc R
O14 O 0.5243(6) -0.042(3) 0.4104(10) 0.218(10) Uani 0.50 1 d P
C14 C 0.0214(3) 0.1166(9) 0.3390(3) 0.081(2) Uani 1 1 d .
H14 H -0.0174 0.0858 0.3411 0.097 Uiso 1 1 calc R
C15 C 0.0269(3) 0.1562(8) 0.2808(2) 0.0676(15) Uani 1 1 d .
O16 O 0.3659(6) 0.1886(16) 0.7835(6) 0.125(5) Uani 0.50 1 d P
C16 C 0.0854(3) 0.1991(10) 0.2813(3) 0.090(2) Uani 1 1 d .
H16 H 0.0918 0.2252 0.2416 0.108 Uiso 1 1 calc R
C17 C 0.1342(3) 0.2038(9) 0.3396(2) 0.080(2) Uani 1 1 d .
H17 H 0.1737 0.2337 0.3390 0.096 Uiso 1 1 calc R
C18 C 0.1206(3) 0.6087(10) 0.3573(3) 0.093(3) Uani 1 1 d .
H18 H 0.1360 0.5649 0.3997 0.112 Uiso 1 1 calc R
C19 C 0.0577(3) 0.6228(11) 0.3290(3) 0.102(3) Uani 1 1 d .
H19 H 0.0314 0.5965 0.3530 0.122 Uiso 1 1 calc R
C20 C 0.0334(2) 0.6747(6) 0.2666(2) 0.0514(11) Uani 1 1 d .
C21 C 0.0750(3) 0.7265(8) 0.2381(3) 0.0692(16) Uani 1 1 d .
H21 H 0.0604 0.7720 0.1961 0.083 Uiso 1 1 calc R
C22 C 0.1373(2) 0.7133(7) 0.2699(3) 0.0644(15) Uani 1 1 d .
H22 H 0.1648 0.7487 0.2488 0.077 Uiso 1 1 calc R
C23 C 0.3800(2) 0.6804(6) 0.4550(3) 0.0719(18) Uani 1 1 d .
H23 H 0.3634 0.7769 0.4602 0.086 Uiso 1 1 calc R
C24 C 0.4398(3) 0.6549(7) 0.4864(4) 0.079(2) Uani 1 1 d .
H24 H 0.4642 0.7343 0.5120 0.095 Uiso 1 1 calc R
C25 C 0.46721(19) 0.5156(5) 0.4826(2) 0.0432(10) Uani 1 1 d .
C26 C 0.4279(2) 0.4067(6) 0.4446(3) 0.0683(17) Uani 1 1 d .
H26 H 0.4430 0.3076 0.4405 0.082 Uiso 1 1 calc R
C27 C 0.3674(2) 0.4408(6) 0.4128(3) 0.0626(14) Uani 1 1 d .
H27 H 0.3418 0.3637 0.3867 0.075 Uiso 1 1 calc R
C28 C -0.0769(10) 0.387(3) 0.3843(10) 0.133(7) Uani 0.50 1 d P
H28A H -0.0943 0.4722 0.3548 0.199 Uiso 0.50 1 calc PR
H28B H -0.1000 0.2933 0.3669 0.199 Uiso 0.50 1 calc PR
H28C H -0.0337 0.3724 0.3879 0.199 Uiso 0.50 1 calc PR
C29 C -0.0733(12) 0.290(3) 0.4883(12) 0.143(8) Uani 0.50 1 d P
H29A H -0.1137 0.2512 0.4867 0.215 Uiso 0.50 1 calc PR
H29B H -0.0489 0.3148 0.5335 0.215 Uiso 0.50 1 calc PR
H29C H -0.0519 0.2112 0.4718 0.215 Uiso 0.50 1 calc PR
C30 C -0.0904(7) 0.5461(15) 0.4741(7) 0.082(4) Uani 0.50 1 d P
H30 H -0.0868 0.6352 0.4507 0.098 Uiso 0.50 1 calc PR
O12 O 0.2321(4) 1.0465(5) 0.2588(2) 0.144(3) Uani 1 1 d .
O15 O 0.4138(10) 0.698(2) 0.7047(10) 0.186(7) Uani 0.50 1 d PU
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O4 Cu1 O1 174.54(12) 4_565 .
O4 Cu1 N4 91.00(13) 4_565 .
O1 Cu1 N4 85.66(13) . .
O4 Cu1 N3 90.51(13) 4_565 .
O1 Cu1 N3 92.35(14) . .
N4 Cu1 N3 173.50(15) . .
O4 Cu1 O9 89.71(12) 4_565 .
O1 Cu1 O9 94.85(12) . .
N4 Cu1 O9 94.47(14) . .
N3 Cu1 O9 91.86(15) . .
C7 O1 Cu1 115.2(3) . .
C3 N1 C11 114.0(3) . .
C3 N1 C9 112.5(4) . .
C11 N1 C9 111.0(4) . .
C3 N1 Cu2 108.7(2) . .
C11 N1 Cu2 101.4(3) . .
C9 N1 Cu2 108.6(3) . .
C6 C1 C2 121.8(4) . .
C6 C1 H1 119.1 . .
C2 C1 H1 119.1 . .
O7 Cu2 N2 94.11(17) . .
O7 Cu2 O2 151.13(17) . .
N2 Cu2 O2 94.93(16) . .
O7 Cu2 N1 83.81(16) . .
N2 Cu2 N1 177.88(17) . .
O2 Cu2 N1 86.75(14) . .
O7 Cu2 O6 113.37(19) . .
N2 Cu2 O6 102.37(16) . .
O2 Cu2 O6 91.31(15) . .
N1 Cu2 O6 78.84(14) . .
C7 O2 Cu2 123.1(3) . .
C13 N2 C17 117.9(5) . .
C13 N2 Cu2 121.5(4) . .
C17 N2 Cu2 120.4(4) . .
C1 C2 C3 118.4(4) . .
C1 C2 C7 116.9(4) . .
C3 C2 C7 124.6(3) . .
C18 N3 C22 116.3(4) . .
C18 N3 Cu1 123.5(3) . .
C22 N3 Cu1 120.2(3) . .
C4 C3 C2 119.3(3) . .
C4 C3 N1 121.3(3) . .
C2 C3 N1 119.4(3) . .
C8 O4 Cu1 121.3(2) . 4_566
C27 N4 C23 115.8(4) . .
C27 N4 Cu1 124.1(3) . .
C23 N4 Cu1 120.0(3) . .
C3 C4 C5 121.7(3) . .
C3 C4 H4 119.2 . .
C5 C4 H4 119.2 . .
C30 N5 C29 117.8(16) . .
C30 N5 C28 129.9(15) . .
C29 N5 C28 112.3(16) . .
C4 C5 C6 119.0(4) . .
C4 C5 C8 119.7(3) . .
C6 C5 C8 121.3(4) . .
C10 O6 Cu2 113.2(3) . .
C1 C6 C5 119.8(4) . .
C1 C6 H6 120.1 . .
C5 C6 H6 120.1 . .
C12 O7 Cu2 114.1(4) . .
O1 C7 O2 122.8(4) . .
O1 C7 C2 116.4(4) . .
O2 C7 C2 120.8(4) . .
O3 C8 O4 124.8(4) . .
O3 C8 C5 120.4(4) . .
O4 C8 C5 114.8(3) . .
N1 C9 C10 111.1(4) . .
N1 C9 H9A 109.4 . .
C10 C9 H9A 109.4 . .
N1 C9 H9B 109.4 . .
C10 C9 H9B 109.4 . .
H9A C9 H9B 108.0 . .
O5 C10 O6 127.1(5) . .
O5 C10 C9 116.5(5) . .
O6 C10 C9 116.4(5) . .
C12 C11 N1 110.1(4) . .
C12 C11 H11A 109.6 . .
N1 C11 H11A 109.6 . .
C12 C11 H11B 109.6 . .
N1 C11 H11B 109.6 . .
H11A C11 H11B 108.2 . .
O8 C12 O7 123.2(6) . .
O8 C12 C11 121.2(5) . .
O7 C12 C11 115.6(5) . .
N2 C13 C14 122.8(5) . .
N2 C13 H13 118.6 . .
C14 C13 H13 118.6 . .
C15 C14 C13 120.3(6) . .
C15 C14 H14 119.9 . .
C13 C14 H14 119.9 . .
C14 C15 C16 116.8(5) . .
C14 C15 C15 122.1(7) . 2
C16 C15 C15 121.1(6) . 2
C17 C16 C15 120.1(6) . .
C17 C16 H16 119.9 . .
C15 C16 H16 119.9 . .
N2 C17 C16 121.9(6) . .
N2 C17 H17 119.0 . .
C16 C17 H17 119.0 . .
N3 C18 C19 124.4(5) . .
N3 C18 H18 117.8 . .
C19 C18 H18 117.8 . .
C20 C19 C18 119.8(6) . .
C20 C19 H19 120.1 . .
C18 C19 H19 120.1 . .
C19 C20 C21 116.1(5) . .
C19 C20 C20 120.4(6) . 2
C21 C20 C20 123.5(5) . 2
C22 C21 C20 120.8(5) . .
C22 C21 H21 119.6 . .
C20 C21 H21 119.6 . .
N3 C22 C21 122.3(5) . .
N3 C22 H22 118.9 . .
C21 C22 H22 118.9 . .
C24 C23 N4 123.2(5) . .
C24 C23 H23 118.4 . .
N4 C23 H23 118.4 . .
C23 C24 C25 121.9(5) . .
C23 C24 H24 119.0 . .
C25 C24 H24 119.0 . .
C26 C25 C24 114.8(4) . .
C26 C25 C25 122.3(5) . 3_666
C24 C25 C25 122.8(5) . 3_666
C27 C26 C25 120.4(5) . .
C27 C26 H26 119.8 . .
C25 C26 H26 119.8 . .
N4 C27 C26 123.7(4) . .
N4 C27 H27 118.1 . .
C26 C27 H27 118.1 . .
N5 C28 H28A 109.5 . .
N5 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
N5 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
N5 C29 H29A 109.5 . .
N5 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
N5 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
O10 C30 N5 128.8(14) . .
O10 C30 H30 115.6 . .
N5 C30 H30 115.6 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 O4 1.964(3) 4_565
Cu1 O1 1.999(3) .
Cu1 N4 2.007(3) .
Cu1 N3 2.028(4) .
Cu1 O9 2.202(3) .
O1 C7 1.251(5) .
N1 C3 1.456(5) .
N1 C11 1.489(6) .
N1 C9 1.496(7) .
N1 Cu2 2.040(3) .
C1 C6 1.376(6) .
C1 C2 1.393(6) .
C1 H1 0.9500 .
Cu2 O7 1.945(4) .
Cu2 N2 1.981(4) .
Cu2 O2 1.991(3) .
Cu2 O6 2.173(4) .
O2 C7 1.259(5) .
N2 C13 1.314(8) .
N2 C17 1.346(7) .
C2 C3 1.406(5) .
C2 C7 1.516(5) .
O3 C8 1.223(5) .
N3 C18 1.313(7) .
N3 C22 1.344(6) .
C3 C4 1.384(6) .
O4 C8 1.266(5) .
O4 Cu1 1.964(3) 4_566
N4 C27 1.332(6) .
N4 C23 1.345(6) .
C4 C5 1.388(6) .
C4 H4 0.9500 .
O5 C10 1.227(7) .
N5 C30 1.273(17) .
N5 C29 1.39(2) .
N5 C28 1.49(2) .
C5 C6 1.390(6) .
C5 C8 1.512(5) .
O6 C10 1.254(7) .
C6 H6 0.9500 .
O7 C12 1.274(6) .
O8 C12 1.229(7) .
C9 C10 1.552(7) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
O10 C30 1.138(14) .
C11 C12 1.473(8) .
C11 H11A 0.9900 .
C11 H11B 0.9900 .
C13 C14 1.402(8) .
C13 H13 0.9500 .
C14 C15 1.358(9) .
C14 H14 0.9500 .
C15 C16 1.397(9) .
C15 C15 1.490(10) 2
C16 C17 1.386(8) .
C16 H16 0.9500 .
C17 H17 0.9500 .
C18 C19 1.377(9) .
C18 H18 0.9500 .
C19 C20 1.364(8) .
C19 H19 0.9500 .
C20 C21 1.379(8) .
C20 C20 1.464(9) 2
C21 C22 1.375(8) .
C21 H21 0.9500 .
C22 H22 0.9500 .
C23 C24 1.336(8) .
C23 H23 0.9500 .
C24 C25 1.388(7) .
C24 H24 0.9500 .
C25 C26 1.384(7) .
C25 C25 1.472(8) 3_666
C26 C27 1.367(7) .
C26 H26 0.9500 .
C27 H27 0.9500 .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 H29A 0.9800 .
C29 H29B 0.9800 .
C29 H29C 0.9800 .
C30 H30 0.9500 .
