#------------------------------------------------------------------------------
#$Date: 2016-03-26 22:09:08 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180492 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/61/7216168.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7216168
loop_
_publ_author_name
'Jia, Li'
'Hui, Yan-Chun'
'Li, Zongsheng'
'Sun, Hao-Ling'
'Wang, Zhenqiang'
_publ_section_title
;
 Luminescent lanthanide-2-phenylpyrimidine-carboxylate frameworks:
 structure and luminescence tuning
;
_journal_issue                   28
_journal_name_full               CrystEngComm
_journal_page_first              6483
_journal_paper_doi               10.1039/c4ce00360h
_journal_volume                  16
_journal_year                    2014
_chemical_formula_sum            'C35 H24 Eu N6 O7'
_chemical_formula_weight         792.56
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                100.2320(10)
_cell_angle_beta                 99.5760(10)
_cell_angle_gamma                98.7850(10)
_cell_formula_units_Z            2
_cell_length_a                   7.6660(10)
_cell_length_b                   13.1780(10)
_cell_length_c                   16.1230(10)
_cell_measurement_reflns_used    4416
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      26.77
_cell_measurement_theta_min      2.62
_cell_volume                     1552.4(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.957
_diffrn_measured_fraction_theta_max 0.957
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0218
_diffrn_reflns_av_sigmaI/netI    0.0471
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            9514
_diffrn_reflns_theta_full        27.63
_diffrn_reflns_theta_max         27.63
_diffrn_reflns_theta_min         1.31
_exptl_absorpt_coefficient_mu    2.082
_exptl_absorpt_correction_T_max  0.8188
_exptl_absorpt_correction_T_min  0.5211
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.696
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       columnar
_exptl_crystal_F_000             790
_exptl_crystal_size_max          0.36
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.602
_refine_diff_density_min         -0.825
_refine_diff_density_rms         0.202
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     449
_refine_ls_number_reflns         6896
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      1.041
_refine_ls_R_factor_all          0.0362
_refine_ls_R_factor_gt           0.0311
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0539P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0828
_refine_ls_wR_factor_ref         0.0910
_reflns_number_gt                6252
_reflns_number_total             6896
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4ce00360h2.cif
_cod_data_source_block           110403b_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 7216165--7216170.cif.
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7216168
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.3015(6) 0.2736(3) -0.1279(3) 0.0366(9) Uani 1 1 d .
H1 H 0.3125 0.2054 -0.1509 0.044 Uiso 1 1 calc R
C2 C 0.3184(7) 0.3488(4) -0.1779(3) 0.0478(11) Uani 1 1 d .
H2 H 0.3363 0.3303 -0.2339 0.057 Uiso 1 1 calc R
C3 C 0.3086(7) 0.4501(4) -0.1444(3) 0.0462(11) Uani 1 1 d .
H3 H 0.3227 0.5014 -0.1769 0.055 Uiso 1 1 calc R
C4 C 0.2774(6) 0.4759(3) -0.0610(3) 0.0388(10) Uani 1 1 d .
C5 C 0.2653(7) 0.5804(3) -0.0215(3) 0.0489(12) Uani 1 1 d .
H5 H 0.2781 0.6340 -0.0518 0.059 Uiso 1 1 calc R
C6 C 0.2357(7) 0.6014(3) 0.0585(4) 0.0522(13) Uani 1 1 d .
H6 H 0.2280 0.6697 0.0828 0.063 Uiso 1 1 calc R
C7 C 0.2153(6) 0.5216(3) 0.1082(3) 0.0401(10) Uani 1 1 d .
C8 C 0.1845(7) 0.5410(4) 0.1922(3) 0.0532(13) Uani 1 1 d .
H8 H 0.1779 0.6084 0.2192 0.064 Uiso 1 1 calc R
C9 C 0.1640(7) 0.4598(4) 0.2346(3) 0.0509(12) Uani 1 1 d .
H9 H 0.1408 0.4712 0.2899 0.061 Uiso 1 1 calc R
C10 C 0.1784(6) 0.3593(3) 0.1934(3) 0.0398(10) Uani 1 1 d .
H10 H 0.1659 0.3051 0.2231 0.048 Uiso 1 1 calc R
C11 C 0.2258(5) 0.4179(3) 0.0716(3) 0.0305(8) Uani 1 1 d .
C12 C 0.2592(5) 0.3949(3) -0.0145(3) 0.0290(8) Uani 1 1 d .
C13 C 0.6556(5) 0.2336(3) 0.1791(2) 0.0301(8) Uani 1 1 d .
C14 C 0.6702(5) 0.2408(3) 0.2759(3) 0.0327(8) Uani 1 1 d .
C15 C 0.5237(6) 0.2021(4) 0.3061(3) 0.0489(12) Uani 1 1 d .
H15 H 0.4157 0.1692 0.2691 0.059 Uiso 1 1 calc R
C16 C 0.5424(7) 0.2136(5) 0.3938(3) 0.0609(15) Uani 1 1 d .
H16 H 0.4453 0.1858 0.4158 0.073 Uiso 1 1 calc R
C17 C 0.8295(6) 0.2957(4) 0.4126(3) 0.0407(10) Uani 1 1 d .
C18 C 1.0011(6) 0.3463(4) 0.4733(3) 0.0425(10) Uani 1 1 d .
C19 C 1.1639(7) 0.3519(4) 0.4477(4) 0.0565(13) Uani 1 1 d .
H19 H 1.1676 0.3251 0.3908 0.068 Uiso 1 1 calc R
C20 C 1.3221(8) 0.3970(5) 0.5059(4) 0.0733(18) Uani 1 1 d .
H20 H 1.4320 0.3992 0.4884 0.088 Uiso 1 1 calc R
C21 C 1.3171(9) 0.4392(5) 0.5906(4) 0.0780(19) Uani 1 1 d .
H21 H 1.4231 0.4707 0.6298 0.094 Uiso 1 1 calc R
C22 C 1.1555(9) 0.4339(5) 0.6158(4) 0.0736(18) Uani 1 1 d .
H22 H 1.1513 0.4621 0.6724 0.088 Uiso 1 1 calc R
C23 C 0.9996(8) 0.3877(5) 0.5584(3) 0.0600(14) Uani 1 1 d .
H23 H 0.8904 0.3839 0.5768 0.072 Uiso 1 1 calc R
C24 C -0.0097(5) 0.0343(3) 0.1563(2) 0.0250(7) Uani 1 1 d .
C25 C -0.0682(5) 0.0284(3) 0.2414(2) 0.0279(8) Uani 1 1 d .
C26 C 0.0493(6) 0.0726(4) 0.3178(3) 0.0431(11) Uani 1 1 d .
H26 H 0.1626 0.1111 0.3195 0.052 Uiso 1 1 calc R
C27 C -0.0085(7) 0.0573(4) 0.3923(3) 0.0547(13) Uani 1 1 d .
H27 H 0.0709 0.0827 0.4447 0.066 Uiso 1 1 calc R
C28 C -0.2810(6) -0.0284(3) 0.3142(3) 0.0350(9) Uani 1 1 d .
C29 C -0.4691(6) -0.0796(3) 0.3121(3) 0.0386(9) Uani 1 1 d .
C30 C -0.5243(8) -0.0959(5) 0.3871(3) 0.0638(16) Uani 1 1 d .
H30 H -0.4419 -0.0774 0.4391 0.077 Uiso 1 1 calc R
C31 C -0.7012(8) -0.1396(6) 0.3851(4) 0.0764(19) Uani 1 1 d .
H31 H -0.7380 -0.1479 0.4361 0.092 Uiso 1 1 calc R
C32 C -0.8216(7) -0.1704(4) 0.3094(3) 0.0532(12) Uani 1 1 d .
H32 H -0.9391 -0.2023 0.3084 0.064 Uiso 1 1 calc R
C33 C -0.7705(6) -0.1547(4) 0.2343(3) 0.0427(10) Uani 1 1 d .
H33 H -0.8536 -0.1745 0.1826 0.051 Uiso 1 1 calc R
C34 C -0.5950(6) -0.1092(3) 0.2360(3) 0.0383(9) Uani 1 1 d .
H34 H -0.5609 -0.0984 0.1851 0.046 Uiso 1 1 calc R
C35 C 0.5403(5) 0.0360(3) -0.0278(2) 0.0225(7) Uani 1 1 d .
Eu1 Eu 0.23695(2) 0.152353(12) 0.038944(10) 0.02092(7) Uani 1 1 d .
N1 N 0.2704(4) 0.2949(2) -0.0487(2) 0.0285(7) Uani 1 1 d .
N2 N 0.2090(4) 0.3381(2) 0.1146(2) 0.0299(7) Uani 1 1 d .
N3 N 0.6922(6) 0.2623(4) 0.4477(2) 0.0544(11) Uani 1 1 d .
N4 N 0.8274(5) 0.2868(3) 0.3278(2) 0.0351(7) Uani 1 1 d .
N5 N -0.1730(5) 0.0077(3) 0.3916(2) 0.0495(10) Uani 1 1 d .
N6 N -0.2337(4) -0.0225(2) 0.2383(2) 0.0307(7) Uani 1 1 d .
O1 O 0.4976(4) 0.2259(2) 0.13838(18) 0.0381(7) Uani 1 1 d .
O2 O 0.7947(4) 0.2375(3) 0.1500(2) 0.0513(9) Uani 1 1 d .
O3 O 0.1165(3) 0.1087(2) 0.15825(17) 0.0306(6) Uani 1 1 d .
O4 O -0.0856(4) -0.0339(2) 0.09100(16) 0.0317(6) Uani 1 1 d .
O5 O 0.6680(3) 0.00791(19) -0.06040(17) 0.0274(5) Uani 1 1 d .
O6 O 0.4782(3) 0.11617(19) -0.03471(17) 0.0275(5) Uani 1 1 d .
O7 O -0.0705(3) 0.1841(2) 0.00457(17) 0.0284(5) Uani 1 1 d D
H7A H -0.119(7) 0.200(4) 0.053(2) 0.079(14) Uiso 1 1 d D
H7B H -0.150(6) 0.134(4) -0.037(2) 0.079(14) Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 C1 C2 122.7(4) . .
N1 C1 H1 118.7 . .
C2 C1 H1 118.7 . .
C3 C2 C1 119.6(4) . .
C3 C2 H2 120.2 . .
C1 C2 H2 120.2 . .
C2 C3 C4 119.4(4) . .
C2 C3 H3 120.3 . .
C4 C3 H3 120.3 . .
C3 C4 C12 117.7(4) . .
C3 C4 C5 122.7(4) . .
C12 C4 C5 119.6(4) . .
C6 C5 C4 120.5(4) . .
C6 C5 H5 119.7 . .
C4 C5 H5 119.7 . .
C5 C6 C7 121.9(4) . .
C5 C6 H6 119.0 . .
C7 C6 H6 119.0 . .
C8 C7 C11 117.3(4) . .
C8 C7 C6 123.4(4) . .
C11 C7 C6 119.3(4) . .
C9 C8 C7 119.5(4) . .
C9 C8 H8 120.2 . .
C7 C8 H8 120.2 . .
C8 C9 C10 119.2(4) . .
C8 C9 H9 120.4 . .
C10 C9 H9 120.4 . .
N2 C10 C9 123.1(4) . .
N2 C10 H10 118.5 . .
C9 C10 H10 118.5 . .
N2 C11 C7 122.9(4) . .
N2 C11 C12 118.1(3) . .
C7 C11 C12 119.1(4) . .
N1 C12 C4 122.0(4) . .
N1 C12 C11 118.4(3) . .
C4 C12 C11 119.6(4) . .
O2 C13 O1 127.4(4) . .
O2 C13 C14 118.5(3) . .
O1 C13 C14 114.1(3) . .
N4 C14 C15 122.5(4) . .
N4 C14 C13 118.0(3) . .
C15 C14 C13 119.5(4) . .
C14 C15 C16 117.2(4) . .
C14 C15 H15 121.4 . .
C16 C15 H15 121.4 . .
N3 C16 C15 122.6(5) . .
N3 C16 H16 118.7 . .
C15 C16 H16 118.7 . .
N3 C17 N4 126.2(4) . .
N3 C17 C18 116.1(4) . .
N4 C17 C18 117.7(4) . .
C19 C18 C23 118.5(5) . .
C19 C18 C17 121.5(4) . .
C23 C18 C17 120.0(4) . .
C18 C19 C20 120.5(5) . .
C18 C19 H19 119.8 . .
C20 C19 H19 119.8 . .
C19 C20 C21 120.0(6) . .
C19 C20 H20 120.0 . .
C21 C20 H20 120.0 . .
C22 C21 C20 119.4(5) . .
C22 C21 H21 120.3 . .
C20 C21 H21 120.3 . .
C21 C22 C23 120.4(6) . .
C21 C22 H22 119.8 . .
C23 C22 H22 119.8 . .
C22 C23 C18 121.2(6) . .
C22 C23 H23 119.4 . .
C18 C23 H23 119.4 . .
O4 C24 O3 124.8(3) . .
O4 C24 C25 119.0(3) . .
O3 C24 C25 116.1(3) . .
N6 C25 C26 122.1(3) . .
N6 C25 C24 117.6(3) . .
C26 C25 C24 120.2(3) . .
C25 C26 C27 116.9(4) . .
C25 C26 H26 121.5 . .
C27 C26 H26 121.5 . .
N5 C27 C26 122.4(4) . .
N5 C27 H27 118.8 . .
C26 C27 H27 118.8 . .
N5 C28 N6 125.5(4) . .
N5 C28 C29 117.2(4) . .
N6 C28 C29 117.3(4) . .
C34 C29 C30 118.1(4) . .
C34 C29 C28 121.1(4) . .
C30 C29 C28 120.7(4) . .
C31 C30 C29 120.4(5) . .
C31 C30 H30 119.8 . .
C29 C30 H30 119.8 . .
C32 C31 C30 120.5(5) . .
C32 C31 H31 119.8 . .
C30 C31 H31 119.8 . .
C31 C32 C33 120.2(5) . .
C31 C32 H32 119.9 . .
C33 C32 H32 119.9 . .
C32 C33 C34 119.6(4) . .
C32 C33 H33 120.2 . .
C34 C33 H33 120.2 . .
C33 C34 C29 121.1(4) . .
C33 C34 H34 119.4 . .
C29 C34 H34 119.4 . .
O6 C35 O5 126.0(3) . .
O6 C35 C35 118.2(4) . 2_655
O5 C35 C35 115.8(4) . 2_655
O6 C35 Eu1 41.61(16) . .
O5 C35 Eu1 167.5(2) . .
C35 C35 Eu1 76.6(2) 2_655 .
O6 C35 Eu1 166.3(2) . 2_655
O5 C35 Eu1 40.29(16) . 2_655
C35 C35 Eu1 75.5(2) 2_655 2_655
Eu1 C35 Eu1 152.10(11) . 2_655
O1 Eu1 O4 149.90(10) . 2
O1 Eu1 O3 85.49(10) . .
O4 Eu1 O3 110.77(9) 2 .
O1 Eu1 O5 82.36(10) . 2_655
O4 Eu1 O5 78.29(9) 2 2_655
O3 Eu1 O5 74.29(9) . 2_655
O1 Eu1 O6 74.97(10) . .
O4 Eu1 O6 76.41(9) 2 .
O3 Eu1 O6 138.88(9) . .
O5 Eu1 O6 67.58(8) 2_655 .
O1 Eu1 O7 138.01(10) . .
O4 Eu1 O7 71.66(9) 2 .
O3 Eu1 O7 78.23(9) . .
O5 Eu1 O7 128.18(8) 2_655 .
O6 Eu1 O7 138.64(9) . .
O1 Eu1 N1 94.25(11) . .
O4 Eu1 N1 87.65(10) 2 .
O3 Eu1 N1 142.50(10) . .
O5 Eu1 N1 142.95(9) 2_655 .
O6 Eu1 N1 75.88(9) . .
O7 Eu1 N1 77.20(9) . .
O1 Eu1 N2 71.13(10) . .
O4 Eu1 N2 134.76(10) 2 .
O3 Eu1 N2 80.64(10) . .
O5 Eu1 N2 144.70(10) 2_655 .
O6 Eu1 N2 124.13(9) . .
O7 Eu1 N2 68.18(9) . .
N1 Eu1 N2 64.08(10) . .
O1 Eu1 C35 74.89(9) . .
O4 Eu1 C35 75.03(9) 2 .
O3 Eu1 C35 120.16(9) . .
O5 Eu1 C35 47.74(8) 2_655 .
O6 Eu1 C35 19.85(8) . .
O7 Eu1 C35 146.13(9) . .
N1 Eu1 C35 95.64(9) . .
N2 Eu1 C35 138.30(9) . .
O1 Eu1 C35 77.78(10) . 2_655
O4 Eu1 C35 76.19(9) 2 2_655
O3 Eu1 C35 93.27(9) . 2_655
O5 Eu1 C35 19.84(8) 2_655 2_655
O6 Eu1 C35 47.75(8) . 2_655
O7 Eu1 C35 140.91(8) . 2_655
N1 Eu1 C35 123.41(9) . 2_655
N2 Eu1 C35 148.66(10) . 2_655
C35 Eu1 C35 27.90(11) . 2_655
C1 N1 C12 118.6(3) . .
C1 N1 Eu1 121.0(3) . .
C12 N1 Eu1 120.4(3) . .
C10 N2 C11 117.9(3) . .
C10 N2 Eu1 123.0(3) . .
C11 N2 Eu1 119.0(2) . .
C16 N3 C17 116.1(4) . .
C14 N4 C17 115.3(4) . .
C27 N5 C28 116.3(4) . .
C25 N6 C28 116.5(3) . .
C13 O1 Eu1 157.7(3) . .
C24 O3 Eu1 127.0(2) . .
C24 O4 Eu1 175.2(3) . 2
C35 O5 Eu1 119.9(2) . 2_655
C35 O6 Eu1 118.5(2) . .
Eu1 O7 H7A 112(4) . .
Eu1 O7 H7B 116(4) . .
H7A O7 H7B 111(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N1 1.327(5) .
C1 C2 1.389(6) .
C1 H1 0.9300 .
C2 C3 1.367(7) .
C2 H2 0.9300 .
C3 C4 1.397(7) .
C3 H3 0.9300 .
C4 C12 1.412(5) .
C4 C5 1.435(6) .
C5 C6 1.335(7) .
C5 H5 0.9300 .
C6 C7 1.436(7) .
C6 H6 0.9300 .
C7 C8 1.399(7) .
C7 C11 1.409(5) .
C8 C9 1.371(7) .
C8 H8 0.9300 .
C9 C10 1.400(6) .
C9 H9 0.9300 .
C10 N2 1.320(5) .
C10 H10 0.9300 .
C11 N2 1.361(5) .
C11 C12 1.442(6) .
C12 N1 1.357(5) .
C13 O2 1.232(5) .
C13 O1 1.258(5) .
C13 C14 1.530(5) .
C14 N4 1.335(5) .
C14 C15 1.361(6) .
C15 C16 1.375(7) .
C15 H15 0.9300 .
C16 N3 1.316(6) .
C16 H16 0.9300 .
C17 N3 1.331(6) .
C17 N4 1.348(5) .
C17 C18 1.485(6) .
C18 C19 1.374(7) .
C18 C23 1.386(6) .
C19 C20 1.381(8) .
C19 H19 0.9300 .
C20 C21 1.390(9) .
C20 H20 0.9300 .
C21 C22 1.362(9) .
C21 H21 0.9300 .
C22 C23 1.366(7) .
C22 H22 0.9300 .
C23 H23 0.9300 .
C24 O4 1.247(4) .
C24 O3 1.259(4) .
C24 C25 1.524(5) .
C25 N6 1.330(5) .
C25 C26 1.373(6) .
C26 C27 1.383(6) .
C26 H26 0.9300 .
C27 N5 1.326(6) .
C27 H27 0.9300 .
C28 N5 1.339(6) .
C28 N6 1.346(5) .
C28 C29 1.488(6) .
C29 C34 1.382(6) .
C29 C30 1.387(6) .
C30 C31 1.383(7) .
C30 H30 0.9300 .
C31 C32 1.357(8) .
C31 H31 0.9300 .
C32 C33 1.373(6) .
C32 H32 0.9300 .
C33 C34 1.380(6) .
C33 H33 0.9300 .
C34 H34 0.9300 .
C35 O6 1.238(4) .
C35 O5 1.259(4) .
C35 C35 1.548(7) 2_655
C35 Eu1 3.202(3) .
C35 Eu1 3.217(3) 2_655
Eu1 O1 2.301(3) .
Eu1 O4 2.377(3) 2
Eu1 O3 2.389(3) .
Eu1 O5 2.399(2) 2_655
Eu1 O6 2.420(2) .
Eu1 O7 2.447(3) .
Eu1 N1 2.551(3) .
Eu1 N2 2.591(3) .
Eu1 C35 3.217(3) 2_655
O4 Eu1 2.377(3) 2
O5 Eu1 2.399(2) 2_655
O7 H7A 0.927(19) .
O7 H7B 0.922(19) .
