#------------------------------------------------------------------------------
#$Date: 2016-03-26 22:23:39 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180503 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/72/7217229.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7217229
loop_
_publ_author_name
'Li, Xinxiong'
'Gong, Yaqiong'
'Zhao, Huaixia'
'Wang, Ruihu'
_publ_section_title
;
 Solvent-mediated crystal-to-crystal transformations from a cationic
 homometallic metal--organic framework to heterometallic frameworks
;
_journal_issue                   37
_journal_name_full               CrystEngComm
_journal_page_first              8818
_journal_paper_doi               10.1039/C4CE01035C
_journal_volume                  16
_journal_year                    2014
_chemical_formula_sum            'C24 H36 Ag9 Cr8 F6 N36 O34 P'
_chemical_formula_weight         2904.69
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                118.924(8)
_cell_angle_beta                 102.910(15)
_cell_angle_gamma                99.902(12)
_cell_formula_units_Z            1
_cell_length_a                   12.83740(10)
_cell_length_b                   13.000
_cell_length_c                   13.2175(5)
_cell_measurement_temperature    293(2)
_cell_volume                     1777.6(3)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean none
_diffrn_measured_fraction_theta_full 0.917
_diffrn_measured_fraction_theta_max 0.917
_diffrn_measurement_method       none
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0141
_diffrn_reflns_av_sigmaI/netI    0.0219
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            13549
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.05
_diffrn_standards_interval_count none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    3.730
_exptl_absorpt_correction_T_max  0.9359
_exptl_absorpt_correction_T_min  0.4941
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.713
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             1388
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.02
_refine_diff_density_max         2.190
_refine_diff_density_min         -1.442
_refine_diff_density_rms         0.114
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.061
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     535
_refine_ls_number_reflns         7474
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.061
_refine_ls_R_factor_all          0.0346
_refine_ls_R_factor_gt           0.0321
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0503P)²+3.1080P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0859
_refine_ls_wR_factor_ref         0.0877
_reflns_number_gt                6969
_reflns_number_total             7474
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4ce01035c2.cif
_cod_data_source_block           a
_cod_depositor_comments
'Adding full bibliography for 7217228--7217229.cif.'
_cod_original_cell_volume        1777.59(7)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7217229
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 1.72776(3) 0.60773(3) 0.76173(2) 0.02908(8) Uani 1 1 d .
Ag2 Ag 2.5000 0.5000 1.0000 0.03458(11) Uani 1 2 d S
Ag3 Ag 1.73033(3) 0.28237(3) 0.60865(3) 0.03045(8) Uani 1 1 d .
Ag4 Ag 1.74916(3) 0.44479(3) 0.94949(3) 0.02993(9) Uani 1 1 d .
Ag5 Ag 1.96829(3) 0.31950(3) 0.54567(3) 0.04473(10) Uani 1 1 d .
Cr1 Cr 2.46148(5) 0.27004(6) 0.66572(6) 0.02776(14) Uani 1 1 d .
Cr2 Cr 2.19825(5) 0.20761(6) 0.53240(6) 0.02568(13) Uani 1 1 d .
Cr3 Cr 1.99090(5) 0.64405(6) 0.68755(6) 0.02996(14) Uani 1 1 d .
Cr4 Cr 1.98514(5) 0.51332(7) 0.83704(6) 0.03121(15) Uani 1 1 d .
N1 N 1.5583(3) -0.2573(3) 0.6692(3) 0.0366(8) Uani 1 1 d .
N2 N 1.6697(3) -0.2307(3) 0.7389(4) 0.0339(8) Uani 1 1 d .
N3 N 1.7693(3) 0.9450(3) 1.2461(3) 0.0243(6) Uani 1 1 d .
N4 N 1.6584(3) -0.0727(3) 0.7264(3) 0.0247(6) Uani 1 1 d .
N5 N 1.6859(3) 0.0429(3) 0.7429(3) 0.0247(6) Uani 1 1 d .
N6 N 1.7266(3) 0.1870(3) 0.7058(3) 0.0233(6) Uani 1 1 d .
N7 N 1.6882(3) 0.4823(3) 0.5569(3) 0.0245(6) Uani 1 1 d .
N8 N 1.7169(3) 0.2395(3) 0.8212(3) 0.0266(7) Uani 1 1 d .
N9 N 1.7544(3) 0.8313(3) 1.1431(3) 0.0232(6) Uani 1 1 d .
N10 N 1.7094(3) 0.3695(3) 0.5028(3) 0.0220(6) Uani 1 1 d .
N11 N 1.6763(2) 0.4223(3) 0.3701(2) 0.0190(6) Uani 1 1 d .
N12 N 1.7441(3) 0.6398(3) 1.0259(3) 0.0235(6) Uani 1 1 d .
N13 N 1.7191(3) 0.6877(3) 0.9527(3) 0.0256(6) Uani 1 1 d .
N14 N 1.6565(2) 0.4179(3) 0.2606(2) 0.0186(6) Uani 1 1 d .
N15 N 1.8492(3) 1.1319(3) 1.4059(3) 0.0313(7) Uani 1 1 d .
N16 N 1.7369(3) 1.0913(3) 1.3949(3) 0.0329(7) Uani 1 1 d .
N17 N 1.5771(3) 0.4244(3) 0.1035(3) 0.0291(7) Uani 1 1 d .
N18 N 1.6838(3) 0.4187(4) 0.1057(3) 0.0325(8) Uani 1 1 d .
C1 C 1.6920(4) 0.1516(4) 0.8413(3) 0.0313(8) Uani 1 1 d .
H1A H 1.6802 0.1616 0.9120 0.038 Uiso 1 1 calc R
C2 C 1.7251(3) 0.8027(3) 1.0247(3) 0.0265(8) Uani 1 1 d .
H2A H 1.7116 0.8562 0.9995 0.032 Uiso 1 1 calc R
C3 C 1.7280(3) -0.1215(4) 0.7704(4) 0.0327(9) Uani 1 1 d .
H3A H 1.8051 -0.0825 0.8159 0.039 Uiso 1 1 calc R
C4 C 1.7072(3) 0.0691(3) 0.6602(3) 0.0249(7) Uani 1 1 d .
H4A H 1.7079 0.0117 0.5832 0.030 Uiso 1 1 calc R
C5 C 1.7655(3) 0.7279(3) 1.1398(3) 0.0249(7) Uani 1 1 d .
H5A H 1.7852 0.7212 1.2079 0.030 Uiso 1 1 calc R
C6 C 1.5543(4) -0.1609(4) 0.6640(4) 0.0350(9) Uani 1 1 d .
H6A H 1.4898 -0.1533 0.6235 0.042 Uiso 1 1 calc R
C7 C 1.7009(3) 0.3347(3) 0.3898(3) 0.0213(7) Uani 1 1 d .
H7A H 1.7102 0.2622 0.3325 0.026 Uiso 1 1 calc R
C8 C 1.6692(3) 0.5123(3) 0.4760(3) 0.0231(7) Uani 1 1 d .
H8A H 1.6533 0.5838 0.4883 0.028 Uiso 1 1 calc R
C9 C 1.8674(3) 1.0434(3) 1.3163(3) 0.0302(8) Uani 1 1 d .
H9A H 1.9354 1.0465 1.3023 0.036 Uiso 1 1 calc R
C10 C 1.6916(3) 0.9792(4) 1.2984(4) 0.0297(8) Uani 1 1 d .
H10A H 1.6170 0.9296 1.2692 0.036 Uiso 1 1 calc R
C11 C 1.5622(3) 0.4229(4) 0.1963(3) 0.0279(8) Uani 1 1 d .
H11A H 1.4968 0.4249 0.2155 0.034 Uiso 1 1 calc R
C12 C 1.7312(3) 0.4171(5) 0.2022(4) 0.0325(9) Uani 1 1 d .
H12A H 1.8043 0.4156 0.2273 0.039 Uiso 1 1 calc R
O1 O 2.0240(5) 0.4029(7) 0.8332(7) 0.107(2) Uani 1 1 d .
O2 O 2.0655(4) 0.6411(6) 0.9595(4) 0.108(2) Uani 1 1 d .
O3 O 2.1569(3) 0.3096(4) 0.6302(3) 0.0521(9) Uani 1 1 d .
O4 O 2.5734(3) 0.3781(3) 0.7017(4) 0.0504(9) Uani 1 1 d .
O5 O 2.3444(3) 0.2746(4) 0.5664(4) 0.0520(9) Uani 1 1 d .
O6 O 1.9270(3) 0.5862(3) 0.5417(3) 0.0445(8) Uani 1 1 d .
O7 O 2.4744(3) 0.1354(3) 0.5914(3) 0.0520(9) Uani 1 1 d .
O8 O 1.9212(3) 0.7173(3) 0.7701(3) 0.0453(8) Uani 1 1 d .
O9 O 2.1183(3) 0.7339(3) 0.7380(4) 0.0484(8) Uani 1 1 d .
O10 O 1.8540(2) 0.4927(3) 0.8250(3) 0.0391(7) Uani 1 1 d .
O11 O 2.1802(3) 0.0879(3) 0.5429(3) 0.0453(8) Uani 1 1 d .
O12 O 2.4369(3) 0.2920(3) 0.7884(3) 0.0469(8) Uani 1 1 d .
O13 O 2.1313(3) 0.1662(3) 0.3940(3) 0.0457(8) Uani 1 1 d .
O14 O 2.0004(2) 0.5156(3) 0.7059(2) 0.0301(6) Uani 1 1 d .
P1 P 1.5000 1.0000 1.0000 0.0341(3) Uani 1 2 d S
F1 F 1.5627(10) 1.0418(16) 1.1264(7) 0.282(8) Uani 1 1 d .
F2 F 1.4824(9) 0.8747(8) 0.9706(17) 0.295(9) Uani 1 1 d .
F3 F 1.6112(5) 0.9952(7) 0.9715(7) 0.129(2) Uani 1 1 d .
O1W O 2.0370(7) 0.8774(7) 1.1123(7) 0.149(3) Uani 1 1 d .
H1WA H 2.0978 0.9100 1.1077 0.179 Uiso 1 1 d R
H1WB H 2.0339 0.8950 1.1822 0.179 Uiso 1 1 d R
O2W O 1.9014(7) 1.0118(7) 1.0612(7) 0.152(4) Uani 1 1 d .
H2WA H 1.9012 1.0504 1.0245 0.182 Uiso 1 1 d R
H2WB H 1.8898 1.0427 1.1292 0.182 Uiso 1 1 d R
O3W O 2.0164(4) -0.1304(5) 0.3134(6) 0.107(2) Uani 1 1 d .
H3WA H 2.0453 -0.1841 0.2735 0.128 Uiso 1 1 d R
H3WB H 1.9469 -0.1528 0.3037 0.128 Uiso 1 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N7 Ag1 N13 162.24(12) . .
N7 Ag1 N2 92.36(12) . 1_565
N13 Ag1 N2 93.30(12) . 1_565
N7 Ag1 O8 86.04(12) . .
N13 Ag1 O8 111.29(12) . .
N2 Ag1 O8 83.94(11) 1_565 .
N17 Ag2 N17 180.00(13) 2_966 1_656
N17 Ag2 O12 86.78(12) 2_966 .
N17 Ag2 O12 93.22(12) 1_656 .
N17 Ag2 O12 93.22(12) 2_966 2_:67
N17 Ag2 O12 86.78(12) 1_656 2_:67
O12 Ag2 O12 180.000(1) . 2_:67
N6 Ag3 N10 172.33(12) . .
N6 Ag3 Ag5 112.89(8) . .
N10 Ag3 Ag5 74.15(8) . .
N12 Ag4 N8 162.69(12) . .
N12 Ag4 N18 95.08(12) . 1_556
N8 Ag4 N18 93.98(12) . 1_556
N12 Ag4 O10 83.67(11) . .
N8 Ag4 O10 90.23(11) . .
N18 Ag4 O10 168.69(11) 1_556 .
N15 Ag5 O14 148.44(12) 1_544 .
N15 Ag5 O6 113.16(12) 1_544 2_966
O14 Ag5 O6 88.03(11) . 2_966
N15 Ag5 O3 110.29(13) 1_544 .
O14 Ag5 O3 95.17(11) . .
O6 Ag5 O3 81.76(12) 2_966 .
N15 Ag5 Ag3 70.32(9) 1_544 .
O14 Ag5 Ag3 78.80(7) . .
O6 Ag5 Ag3 143.70(8) 2_966 .
O3 Ag5 Ag3 132.63(9) . .
O7 Cr1 O4 110.97(19) . .
O7 Cr1 O12 109.5(2) . .
O4 Cr1 O12 110.80(19) . .
O7 Cr1 O5 107.92(19) . .
O4 Cr1 O5 107.91(18) . .
O12 Cr1 O5 109.63(18) . .
O13 Cr2 O11 109.9(2) . .
O13 Cr2 O3 111.19(19) . .
O11 Cr2 O3 109.87(19) . .
O13 Cr2 O5 107.62(18) . .
O11 Cr2 O5 109.29(18) . .
O3 Cr2 O5 108.9(2) . .
O9 Cr3 O8 110.24(19) . .
O9 Cr3 O6 111.83(19) . .
O8 Cr3 O6 111.59(19) . .
O9 Cr3 O14 106.90(16) . .
O8 Cr3 O14 108.27(16) . .
O6 Cr3 O14 107.81(16) . .
O1 Cr4 O2 109.7(4) . .
O1 Cr4 O10 112.0(3) . .
O2 Cr4 O10 111.2(2) . .
O1 Cr4 O14 106.7(2) . .
O2 Cr4 O14 108.8(2) . .
O10 Cr4 O14 108.25(15) . .
C6 N1 N2 106.8(3) . .
C3 N2 N1 108.2(3) . .
C3 N2 Ag1 131.4(3) . 1_545
N1 N2 Ag1 120.0(2) . 1_545
C10 N3 C9 106.9(3) . .
C10 N3 N9 127.2(3) . .
C9 N3 N9 125.9(3) . .
C6 N4 C3 105.9(3) . .
C6 N4 N5 126.3(3) . .
C3 N4 N5 127.8(3) . .
C1 N5 C4 106.4(3) . .
C1 N5 N4 127.2(3) . .
C4 N5 N4 126.4(3) . .
C4 N6 N8 107.5(3) . .
C4 N6 Ag3 127.8(2) . .
N8 N6 Ag3 123.0(2) . .
C8 N7 N10 107.8(3) . .
C8 N7 Ag1 126.8(2) . .
N10 N7 Ag1 123.6(2) . .
C1 N8 N6 107.8(3) . .
C1 N8 Ag4 128.2(2) . .
N6 N8 Ag4 123.9(2) . .
C5 N9 C2 107.0(3) . .
C5 N9 N3 127.2(3) . .
C2 N9 N3 125.7(3) . .
C7 N10 N7 107.7(3) . .
C7 N10 Ag3 134.3(3) . .
N7 N10 Ag3 117.6(2) . .
C7 N11 C8 107.3(3) . .
C7 N11 N14 126.3(3) . .
C8 N11 N14 126.3(3) . .
C5 N12 N13 107.6(3) . .
C5 N12 Ag4 129.3(3) . .
N13 N12 Ag4 123.1(2) . .
C2 N13 N12 107.9(3) . .
C2 N13 Ag1 123.9(3) . .
N12 N13 Ag1 125.1(2) . .
C11 N14 C12 106.7(3) . .
C11 N14 N11 126.5(3) . .
C12 N14 N11 126.6(3) . .
C9 N15 N16 108.7(3) . .
C9 N15 Ag5 126.8(3) . 1_566
N16 N15 Ag5 124.4(2) . 1_566
C10 N16 N15 106.8(3) . .
C11 N17 N18 108.2(3) . .
C11 N17 Ag2 130.9(3) . 1_454
N18 N17 Ag2 116.4(2) . 1_454
C12 N18 N17 107.4(3) . .
C12 N18 Ag4 135.7(3) . 1_554
N17 N18 Ag4 116.2(2) . 1_554
N8 C1 N5 109.1(3) . .
N13 C2 N9 108.5(3) . .
N2 C3 N4 109.1(4) . .
N6 C4 N5 109.2(3) . .
N12 C5 N9 108.9(3) . .
N1 C6 N4 110.0(4) . .
N10 C7 N11 108.4(3) . .
N7 C8 N11 108.8(3) . .
N15 C9 N3 108.0(3) . .
N16 C10 N3 109.6(4) . .
N17 C11 N14 108.9(3) . .
N18 C12 N14 108.8(3) . .
Cr2 O3 Ag5 116.38(19) . .
Cr2 O5 Cr1 126.85(19) . .
Cr3 O6 Ag5 114.02(18) . 2_966
Cr3 O8 Ag1 123.51(18) . .
Cr4 O10 Ag4 129.90(17) . .
Cr1 O12 Ag2 127.53(18) . .
Cr4 O14 Cr3 122.42(15) . .
Cr4 O14 Ag5 110.44(14) . .
Cr3 O14 Ag5 123.65(14) . .
F2 P1 F2 180.00(19) . 2_877
F2 P1 F1 87.2(8) . .
F2 P1 F1 92.8(8) 2_877 .
F2 P1 F1 92.8(8) . 2_877
F2 P1 F1 87.2(8) 2_877 2_877
F1 P1 F1 179.999(6) . 2_877
F2 P1 F3 93.0(5) . 2_877
F2 P1 F3 87.0(5) 2_877 2_877
F1 P1 F3 91.2(5) . 2_877
F1 P1 F3 88.8(5) 2_877 2_877
F2 P1 F3 87.0(5) . .
F2 P1 F3 93.0(5) 2_877 .
F1 P1 F3 88.8(5) . .
F1 P1 F3 91.2(5) 2_877 .
F3 P1 F3 179.998(3) 2_877 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N7 2.253(3) .
Ag1 N13 2.256(3) .
Ag1 N2 2.472(4) 1_565
Ag1 O8 2.592(3) .
Ag2 N17 2.202(3) 2_966
Ag2 N17 2.202(3) 1_656
Ag2 O12 2.590(3) .
Ag2 O12 2.590(3) 2_:67
Ag3 N6 2.176(3) .
Ag3 N10 2.187(3) .
Ag3 Ag5 3.3579(5) .
Ag4 N12 2.250(3) .
Ag4 N8 2.257(3) .
Ag4 N18 2.536(3) 1_556
Ag4 O10 2.569(3) .
Ag5 N15 2.190(3) 1_544
Ag5 O14 2.276(3) .
Ag5 O6 2.478(3) 2_966
Ag5 O3 2.482(4) .
Cr1 O7 1.602(3) .
Cr1 O4 1.618(3) .
Cr1 O12 1.620(3) .
Cr1 O5 1.791(3) .
Cr2 O13 1.601(3) .
Cr2 O11 1.611(3) .
Cr2 O3 1.613(3) .
Cr2 O5 1.779(3) .
Cr3 O9 1.609(3) .
Cr3 O8 1.620(3) .
Cr3 O6 1.623(3) .
Cr3 O14 1.820(3) .
Cr4 O1 1.580(5) .
Cr4 O2 1.583(5) .
Cr4 O10 1.617(3) .
Cr4 O14 1.800(3) .
N1 C6 1.296(6) .
N1 N2 1.396(5) .
N2 C3 1.292(5) .
N2 Ag1 2.472(4) 1_545
N3 C10 1.355(5) .
N3 C9 1.363(5) .
N3 N9 1.383(4) .
N4 C6 1.359(5) .
N4 C3 1.364(5) .
N4 N5 1.378(4) .
N5 C1 1.354(5) .
N5 C4 1.359(5) .
N6 C4 1.297(5) .
N6 N8 1.385(4) .
N7 C8 1.295(5) .
N7 N10 1.394(4) .
N8 C1 1.298(5) .
N9 C5 1.357(5) .
N9 C2 1.362(5) .
N10 C7 1.306(4) .
N11 C7 1.356(5) .
N11 C8 1.358(4) .
N11 N14 1.383(4) .
N12 C5 1.301(4) .
N12 N13 1.393(4) .
N13 C2 1.303(5) .
N14 C11 1.347(5) .
N14 C12 1.357(4) .
N15 C9 1.296(5) .
N15 N16 1.395(5) .
N15 Ag5 2.190(3) 1_566
N16 C10 1.291(5) .
N17 C11 1.291(5) .
N17 N18 1.379(4) .
N17 Ag2 2.202(3) 1_454
N18 C12 1.297(5) .
N18 Ag4 2.536(3) 1_554
O6 Ag5 2.478(3) 2_966
P1 F2 1.441(7) .
P1 F2 1.441(7) 2_877
P1 F1 1.451(7) .
P1 F1 1.451(7) 2_877
P1 F3 1.560(4) 2_877
P1 F3 1.560(4) .
