#------------------------------------------------------------------------------
#$Date: 2016-02-05 00:13:20 +0200 (Fri, 05 Feb 2016) $
#$Revision: 175940 $
#$URL: svn://www.crystallography.net/cod/cif/7/22/33/7223326.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7223326
loop_
_publ_author_name
'Sha, Jing-Quan'
'Sun, Long-Jiang'
'Zhu, Pei-Pei'
'Jiang, Jianzhuang'
_publ_section_title
;
 The first two-fold interpenetrating polyoxometalate-based coordination
 polymer with helical channels: structure and catalytic activities
;
_journal_issue                   2
_journal_name_full               CrystEngComm
_journal_page_first              283
_journal_paper_doi               10.1039/C5CE02021B
_journal_volume                  18
_journal_year                    2016
_chemical_formula_moiety         'C18 H12 Ag4 Mo12 N14 Na O40 P'
_chemical_formula_sum            'C18 H12 Ag4 Mo12 N14 Na O40 P'
_chemical_formula_weight         2701.17
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-11-10 deposited with the CCDC.
2015-11-23 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 129.598(14)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.442(5)
_cell_length_b                   22.524(5)
_cell_length_c                   21.414(5)
_cell_measurement_temperature    293(2)
_cell_volume                     5367(3)
_computing_cell_refinement       'Bruker FRAMBO'
_computing_data_collection       'Bruker FRAMBO'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0292
_diffrn_reflns_av_sigmaI/netI    0.0491
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            16979
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         3.26
_exptl_absorpt_coefficient_mu    4.275
_exptl_absorpt_correction_T_max  0.574
_exptl_absorpt_correction_T_min  0.354
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs(Sheldrick,1996)
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    3.340
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             5016
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.13
_refine_diff_density_max         3.363
_refine_diff_density_min         -2.805
_refine_diff_density_rms         0.216
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.063
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     856
_refine_ls_number_reflns         9421
_refine_ls_number_restraints     30
_refine_ls_restrained_S_all      1.099
_refine_ls_R_factor_all          0.0717
_refine_ls_R_factor_gt           0.0557
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0559P)²+95.2255P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1340
_refine_ls_wR_factor_ref         0.1444
_reflns_number_gt                7647
_reflns_number_total             9456
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5ce02021b2.cif
_cod_data_source_block           sha
_cod_depositor_comments          'Adding full bibliography for 7223326.cif.'
_cod_original_sg_symbol_Hall     '  -P 2ybc '
_cod_original_sg_symbol_H-M      '  P 21/c '
_cod_database_code               7223326
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C -0.4831(12) -0.2957(5) 0.5330(8) 0.035(3) Uani 1 1 d .
H1 H -0.4826 -0.2586 0.5523 0.042 Uiso 1 1 calc R
C2 C -0.5061(10) -0.3632(5) 0.4570(7) 0.027(3) Uani 1 1 d .
C3 C -0.5282(12) -0.3923(6) 0.3864(8) 0.034(3) Uani 1 1 d .
C4 C -0.5611(11) -0.4028(6) 0.2778(8) 0.034(3) Uani 1 1 d .
C5 C -0.5881(12) -0.3882(6) 0.1996(8) 0.037(3) Uani 1 1 d .
C7 C -0.5842(14) -0.4325(8) 0.1548(10) 0.055(4) Uani 1 1 d .
H7 H -0.5667 -0.4720 0.1713 0.067 Uiso 1 1 calc R
C8 C -0.6093(14) -0.4122(11) 0.0825(10) 0.067(6) Uani 1 1 d .
H8 H -0.6053 -0.4394 0.0515 0.080 Uiso 1 1 calc R
C9 C -0.6371(14) -0.3580(8) 0.0580(9) 0.049(4) Uani 1 1 d .
H9 H -0.6561 -0.3477 0.0090 0.059 Uiso 1 1 calc R
N1 N -0.6173(14) -0.3310(7) 0.1714(9) 0.075(4) Uani 1 1 d D
C10 C -0.7667(13) -0.1588(6) 0.1991(9) 0.045(3) Uani 1 1 d .
H10 H -0.8399 -0.1744 0.1807 0.054 Uiso 1 1 calc R
C11 C -0.5839(14) -0.1451(5) 0.2609(9) 0.039(3) Uani 1 1 d .
C12 C -0.4559(13) -0.1567(5) 0.3142(8) 0.038(3) Uani 1 1 d .
C13 C -0.2726(13) -0.1523(6) 0.3666(8) 0.038(3) Uani 1 1 d .
C14 C -0.1575(12) -0.1393(6) 0.3863(8) 0.038(3) Uani 1 1 d .
C15 C -0.0536(15) -0.1386(8) 0.4624(9) 0.057(4) Uani 1 1 d .
H15 H -0.0526 -0.1455 0.5056 0.069 Uiso 1 1 calc R
C16 C 0.0538(14) -0.1274(8) 0.4764(11) 0.062(5) Uani 1 1 d .
H16 H 0.1264 -0.1258 0.5291 0.074 Uiso 1 1 calc R
C17 C 0.0513(14) -0.1189(7) 0.4132(10) 0.052(4) Uani 1 1 d .
H17 H 0.1214 -0.1128 0.4207 0.062 Uiso 1 1 calc R
C18 C -0.0596(14) -0.1196(6) 0.3369(9) 0.042(3) Uani 1 1 d .
H18 H -0.0625 -0.1124 0.2929 0.051 Uiso 1 1 calc R
Ag1A Ag -0.32757(13) -0.13928(6) 0.19880(8) 0.0539(4) Uani 0.90 1 d P
Ag4 Ag -0.52323(10) -0.52709(4) 0.43335(6) 0.0389(3) Uani 1 1 d .
Mo1 Mo 0.15710(9) -0.47764(5) 0.29237(6) 0.0290(2) Uani 1 1 d .
Mo2 Mo 0.00729(10) -0.53408(5) 0.35276(7) 0.0323(3) Uani 1 1 d .
Mo3 Mo -0.20444(10) -0.43634(5) 0.34844(7) 0.0322(3) Uani 1 1 d .
Mo4 Mo -0.28549(9) -0.30213(5) 0.25253(6) 0.0263(2) Uani 1 1 d .
Mo5 Mo -0.00904(10) -0.31885(5) 0.43796(6) 0.0311(3) Uani 1 1 d .
Mo6 Mo -0.12174(10) -0.24329(5) 0.18563(7) 0.0311(3) Uani 1 1 d .
Mo7 Mo 0.07456(10) -0.33195(5) 0.19024(7) 0.0298(2) Uani 1 1 d .
Mo8 Mo 0.15543(10) -0.27430(5) 0.36527(7) 0.0347(3) Uani 1 1 d .
Mo9 Mo 0.20954(10) -0.42185(5) 0.46058(6) 0.0331(3) Uani 1 1 d .
Mo11 Mo -0.29356(10) -0.49919(5) 0.15766(7) 0.0347(3) Uani 1 1 d .
Mo12 Mo -0.14234(10) -0.45756(5) 0.09055(6) 0.0300(3) Uani 1 1 d .
Mo10 Mo -0.34494(9) -0.36408(5) 0.06849(6) 0.0294(2) Uani 1 1 d .
C6 C -0.6393(15) -0.3188(10) 0.0983(10) 0.071(5) Uani 1 1 d .
H6 H -0.6562 -0.2800 0.0793 0.085 Uiso 1 1 calc R
N2 N -0.4539(10) -0.3446(5) 0.5737(6) 0.039(3) Uani 1 1 d .
N3 N -0.4691(10) -0.3903(5) 0.5247(6) 0.034(2) Uani 1 1 d .
N4 N -0.5142(10) -0.3047(4) 0.4599(6) 0.035(2) Uani 1 1 d .
N5 N -0.5216(9) -0.4504(4) 0.3795(6) 0.029(2) Uani 1 1 d .
N6 N -0.5442(10) -0.4563(5) 0.3071(7) 0.035(2) Uani 1 1 d .
N7 N -0.5538(10) -0.3607(4) 0.3253(6) 0.034(2) Uani 1 1 d D
N8 N -0.7553(13) -0.1103(6) 0.1690(9) 0.060(4) Uani 1 1 d .
N9 N -0.6348(12) -0.1014(6) 0.2097(8) 0.050(3) Uani 1 1 d .
N10 N -0.6627(11) -0.1815(5) 0.2574(8) 0.046(3) Uani 1 1 d .
N11 N -0.4059(11) -0.1981(5) 0.3692(7) 0.041(3) Uani 1 1 d D
N12 N -0.2872(11) -0.1944(5) 0.4041(7) 0.046(3) Uani 1 1 d .
N13 N -0.3801(10) -0.1264(5) 0.3093(6) 0.036(3) Uani 1 1 d .
N14 N -0.1627(11) -0.1300(5) 0.3221(7) 0.041(3) Uani 1 1 d .
O1 O 0.0111(8) -0.6017(4) 0.3876(6) 0.040(2) Uani 1 1 d .
O2 O -0.1388(8) -0.5341(4) 0.2463(5) 0.033(2) Uani 1 1 d .
O3 O 0.0991(8) -0.5429(3) 0.3207(5) 0.033(2) Uani 1 1 d .
O4 O 0.1462(7) -0.4972(4) 0.4524(5) 0.0314(19) Uani 1 1 d .
O5 O 0.3408(8) -0.4228(4) 0.5554(5) 0.041(2) Uani 1 1 d .
O6 O 0.2610(7) -0.4584(4) 0.4020(5) 0.034(2) Uani 1 1 d .
O7 O 0.1577(7) -0.4029(4) 0.2576(5) 0.0305(19) Uani 1 1 d .
O8 O 0.2209(7) -0.3472(4) 0.4193(5) 0.035(2) Uani 1 1 d .
O9 O -0.2918(7) -0.4654(4) 0.2374(5) 0.0314(19) Uani 1 1 d .
O10 O -0.1669(7) -0.4148(3) 0.1828(4) 0.0233(17) Uani 1 1 d .
O11 O -0.0263(8) -0.2652(4) 0.1512(5) 0.0303(19) Uani 1 1 d .
O12 O 0.0279(8) -0.2204(4) 0.2846(5) 0.0321(19) Uani 1 1 d .
O13 O 0.0668(7) -0.2781(4) 0.4068(5) 0.0324(19) Uani 1 1 d .
O14 O 0.1844(7) -0.2893(4) 0.2932(5) 0.0313(19) Uani 1 1 d .
O15 O 0.0327(7) -0.4349(3) 0.3190(5) 0.0249(17) Uani 1 1 d .
O16 O -0.0879(7) -0.4898(4) 0.3755(5) 0.033(2) Uani 1 1 d .
O17 O -0.1186(7) -0.3696(4) 0.3071(5) 0.0280(18) Uani 1 1 d .
O18 O -0.2400(7) -0.2989(4) 0.1029(5) 0.0302(19) Uani 1 1 d .
O19 O -0.1033(7) -0.3842(4) 0.4349(5) 0.033(2) Uani 1 1 d .
O20 O -0.1935(7) -0.2533(3) 0.2318(5) 0.0305(19) Uani 1 1 d .
O21 O -0.1553(7) -0.2788(4) 0.3659(5) 0.0311(19) Uani 1 1 d .
O22 O -0.3507(7) -0.3369(4) 0.1533(5) 0.0293(18) Uani 1 1 d .
O23 O -0.3132(7) -0.3661(4) 0.2920(5) 0.0303(19) Uani 1 1 d .
O24 O -0.3931(8) -0.2530(4) 0.2279(5) 0.035(2) Uani 1 1 d .
O25 O 0.0469(9) -0.2873(4) 0.5262(5) 0.042(2) Uani 1 1 d .
O26 O -0.2820(7) -0.4042(4) 0.0271(5) 0.0299(18) Uani 1 1 d .
O27 O -0.1503(9) -0.4850(4) 0.0148(6) 0.047(2) Uani 1 1 d .
O28 O 0.1092(7) -0.3825(4) 0.4723(5) 0.0318(19) Uani 1 1 d .
O29 O 0.1442(9) -0.3211(4) 0.1515(6) 0.042(2) Uani 1 1 d .
O30 O 0.2649(9) -0.2255(4) 0.4307(6) 0.045(2) Uani 1 1 d .
O31 O -0.0134(7) -0.3334(3) 0.2561(5) 0.0236(17) Uani 1 1 d .
O32 O -0.0486(7) -0.3841(4) 0.1168(5) 0.0294(18) Uani 1 1 d .
O33 O -0.2768(9) -0.4714(4) 0.3746(6) 0.045(2) Uani 1 1 d .
O34 O 0.2457(8) -0.5183(4) 0.2825(6) 0.042(2) Uani 1 1 d .
O35 O 0.0000(7) -0.4875(3) 0.1834(5) 0.0301(19) Uani 1 1 d .
O36 O -0.2381(8) -0.5109(4) 0.0934(5) 0.0328(19) Uani 1 1 d .
O37 O -0.3869(9) -0.5568(4) 0.1258(6) 0.048(3) Uani 1 1 d .
O38 O -0.1774(8) -0.1772(4) 0.1377(6) 0.041(2) Uani 1 1 d .
O39 O -0.3951(7) -0.4400(4) 0.0807(5) 0.034(2) Uani 1 1 d .
O40 O -0.4778(8) -0.3376(4) -0.0135(5) 0.040(2) Uani 1 1 d .
P1 P -0.0662(2) -0.38826(12) 0.26661(17) 0.0199(6) Uani 1 1 d .
Ag3A Ag -0.5662(2) -0.54445(10) 0.26015(15) 0.0600(6) Uani 0.70 1 d PU
Ag3B Ag -0.4923(6) -0.5412(3) 0.2916(3) 0.084(2) Uani 0.30 1 d P
Ag2A Ag -0.58671(14) -0.25159(6) 0.35043(9) 0.0538(4) Uani 0.80 1 d PD
Ag2B Ag -0.4573(11) -0.2494(5) 0.4103(7) 0.065(4) Uani 0.10 1 d PD
Ag2C Ag -0.6279(12) -0.2815(5) 0.2493(7) 0.082(5) Uani 0.10 1 d PD
Ag1B Ag -0.4185(12) -0.1308(6) 0.1851(8) 0.055(3) Uani 0.10 1 d PU
Na1A Na -0.1496(7) -0.2487(3) 0.5103(5) 0.0383(18) Uani 0.67 1 d PU
Na1B Na -0.2129(15) -0.3015(8) 0.4839(10) 0.046(4) Uani 0.33 1 d PU
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 C1 N4 112.3(11) . .
N2 C1 H1 123.9 . .
N4 C1 H1 123.9 . .
N3 C2 N4 113.0(11) . .
N3 C2 C3 125.6(11) . .
N4 C2 C3 121.2(11) . .
N7 C3 N5 114.6(11) . .
N7 C3 C2 121.0(11) . .
N5 C3 C2 124.4(11) . .
N6 C4 N7 112.7(11) . .
N6 C4 C5 125.3(12) . .
N7 C4 C5 122.0(12) . .
N1 C5 C7 120.0(14) . .
N1 C5 C4 119.3(12) . .
C7 C5 C4 120.7(13) . .
C5 C7 C8 114.9(16) . .
C5 C7 H7 122.5 . .
C8 C7 H7 122.5 . .
C9 C8 C7 122.9(16) . .
C9 C8 H8 118.5 . .
C7 C8 H8 118.5 . .
C6 C9 C8 121.9(16) . .
C6 C9 H9 119.0 . .
C8 C9 H9 119.0 . .
C5 N1 C6 117.4(15) . .
C5 N1 Ag2C 107.9(10) . .
C6 N1 Ag2C 134.6(15) . .
N10 C10 N8 111.4(13) . .
N10 C10 H10 124.3 . .
N8 C10 H10 124.3 . .
N9 C11 N10 113.9(13) . .
N9 C11 C12 123.7(13) . .
N10 C11 C12 122.3(11) . .
N11 C12 N13 115.0(13) . .
N11 C12 C11 122.4(13) . .
N13 C12 C11 122.6(12) . .
N12 C13 N13 108.6(12) . .
N12 C13 C14 123.5(12) . .
N13 C13 C14 127.8(12) . .
C15 C14 N14 122.1(14) . .
C15 C14 C13 122.8(13) . .
N14 C14 C13 115.1(12) . .
C14 C15 C16 119.5(14) . .
C14 C15 H15 120.3 . .
C16 C15 H15 120.3 . .
C17 C16 C15 119.6(15) . .
C17 C16 H16 120.2 . .
C15 C16 H16 120.2 . .
C16 C17 C18 117.3(15) . .
C16 C17 H17 121.4 . .
C18 C17 H17 121.4 . .
N14 C18 C17 124.2(14) . .
N14 C18 H18 117.9 . .
C17 C18 H18 117.9 . .
Ag1B Ag1A N2 77.5(7) . 4
Ag1B Ag1A N14 118.6(7) . .
N2 Ag1A N14 163.8(5) 4 .
Ag1B Ag1A Ag3A 42.9(6) . 2_455
N2 Ag1A Ag3A 107.4(3) 4 2_455
N14 Ag1A Ag3A 86.9(3) . 2_455
Ag1B Ag1A Ag4 69.4(6) . 2_455
N2 Ag1A Ag4 59.1(3) 4 2_455
N14 Ag1A Ag4 124.9(3) . 2_455
Ag3A Ag1A Ag4 63.11(5) 2_455 2_455
N5 Ag4 N3 173.2(4) . 3_446
N5 Ag4 Ag4 97.1(3) . 3_446
N3 Ag4 Ag4 89.6(3) 3_446 3_446
N5 Ag4 Ag1B 105.2(4) . 2_445
N3 Ag4 Ag1B 68.1(4) 3_446 2_445
Ag4 Ag4 Ag1B 157.7(2) 3_446 2_445
N5 Ag4 Ag3B 61.5(3) . .
N3 Ag4 Ag3B 112.2(3) 3_446 .
Ag4 Ag4 Ag3B 153.07(15) 3_446 .
Ag1B Ag4 Ag3B 47.2(3) 2_445 .
N5 Ag4 Ag1A 112.7(3) . 2_445
N3 Ag4 Ag1A 60.9(3) 3_446 2_445
Ag4 Ag4 Ag1A 143.68(6) 3_446 2_445
Ag1B Ag4 Ag1A 20.3(2) 2_445 2_445
Ag3B Ag4 Ag1A 63.25(14) . 2_445
N5 Ag4 Ag3A 63.1(3) . .
N3 Ag4 Ag3A 110.2(3) 3_446 .
Ag4 Ag4 Ag3A 160.13(7) 3_446 .
Ag1B Ag4 Ag3A 42.2(2) 2_445 .
Ag3B Ag4 Ag3A 14.10(11) . .
Ag1A Ag4 Ag3A 54.26(5) 2_445 .
O34 Mo1 O7 104.2(4) . .
O34 Mo1 O6 102.6(4) . .
O7 Mo1 O6 95.1(4) . .
O34 Mo1 O3 97.9(4) . .
O7 Mo1 O3 156.8(3) . .
O6 Mo1 O3 86.9(4) . .
O34 Mo1 O35 100.5(4) . .
O7 Mo1 O35 85.6(3) . .
O6 Mo1 O35 156.0(3) . .
O3 Mo1 O35 83.4(3) . .
O34 Mo1 O15 169.9(4) . .
O7 Mo1 O15 85.8(3) . .
O6 Mo1 O15 74.4(3) . .
O3 Mo1 O15 72.4(3) . .
O35 Mo1 O15 81.7(3) . .
O1 Mo2 O3 103.8(4) . .
O1 Mo2 O2 103.4(4) . .
O3 Mo2 O2 93.8(4) . .
O1 Mo2 O4 100.4(4) . .
O3 Mo2 O4 88.4(4) . .
O2 Mo2 O4 154.8(3) . .
O1 Mo2 O16 100.2(4) . .
O3 Mo2 O16 155.9(4) . .
O2 Mo2 O16 83.1(4) . .
O4 Mo2 O16 84.7(3) . .
O1 Mo2 O15 171.7(4) . .
O3 Mo2 O15 73.2(3) . .
O2 Mo2 O15 84.6(3) . .
O4 Mo2 O15 72.0(3) . .
O16 Mo2 O15 82.7(3) . .
O33 Mo3 O16 103.2(4) . .
O33 Mo3 O19 103.1(4) . .
O16 Mo3 O19 96.8(4) . .
O33 Mo3 O9 101.1(4) . .
O16 Mo3 O9 85.2(4) . .
O19 Mo3 O9 154.6(3) . .
O33 Mo3 O23 99.1(4) . .
O16 Mo3 O23 156.4(3) . .
O19 Mo3 O23 85.4(4) . .
O9 Mo3 O23 83.2(3) . .
O33 Mo3 O17 169.9(4) . .
O16 Mo3 O17 86.8(3) . .
O19 Mo3 O17 73.5(3) . .
O9 Mo3 O17 81.3(3) . .
O23 Mo3 O17 71.3(3) . .
O24 Mo4 O23 103.3(4) . .
O24 Mo4 O22 102.9(4) . .
O23 Mo4 O22 95.5(4) . .
O24 Mo4 O21 100.1(4) . .
O23 Mo4 O21 87.6(4) . .
O22 Mo4 O21 155.4(3) . .
O24 Mo4 O20 100.4(4) . .
O23 Mo4 O20 155.7(3) . .
O22 Mo4 O20 84.3(3) . .
O21 Mo4 O20 83.0(3) . .
O24 Mo4 O17 172.1(4) . .
O23 Mo4 O17 74.2(3) . .
O22 Mo4 O17 84.9(3) . .
O21 Mo4 O17 72.5(3) . .
O20 Mo4 O17 81.6(3) . .
O25 Mo5 O13 103.1(4) . .
O25 Mo5 O21 101.9(4) . .
O13 Mo5 O21 94.6(4) . .
O25 Mo5 O19 100.4(4) . .
O13 Mo5 O19 155.7(3) . .
O21 Mo5 O19 86.6(4) . .
O25 Mo5 O28 102.0(4) . .
O13 Mo5 O28 85.7(4) . .
O21 Mo5 O28 155.4(3) . .
O19 Mo5 O28 83.4(3) . .
O25 Mo5 O17 170.8(4) . .
O13 Mo5 O17 85.3(3) . .
O21 Mo5 O17 73.4(3) . .
O19 Mo5 O17 71.7(3) . .
O28 Mo5 O17 82.1(3) . .
O25 Mo5 Na1A 47.6(4) . .
O13 Mo5 Na1A 124.2(3) . .
O21 Mo5 Na1A 59.7(3) . .
O19 Mo5 Na1A 77.1(3) . .
O28 Mo5 Na1A 138.3(3) . .
O17 Mo5 Na1A 124.4(2) . .
O25 Mo5 Na1B 62.8(4) . .
O13 Mo5 Na1B 143.6(4) . .
O21 Mo5 Na1B 59.6(4) . .
O19 Mo5 Na1B 55.7(4) . .
O28 Mo5 Na1B 128.8(4) . .
O17 Mo5 Na1B 108.2(3) . .
Na1A Mo5 Na1B 21.9(3) . .
O38 Mo6 O20 102.8(4) . .
O38 Mo6 O12 101.6(4) . .
O20 Mo6 O12 93.7(4) . .
O38 Mo6 O18 102.3(4) . .
O20 Mo6 O18 86.7(3) . .
O12 Mo6 O18 155.4(4) . .
O38 Mo6 O11 99.5(4) . .
O20 Mo6 O11 157.4(3) . .
O12 Mo6 O11 85.2(3) . .
O18 Mo6 O11 85.2(3) . .
O38 Mo6 O31 170.4(4) . .
O20 Mo6 O31 85.6(3) . .
O12 Mo6 O31 73.0(3) . .
O18 Mo6 O31 82.6(3) . .
O11 Mo6 O31 72.5(3) . .
O38 Mo6 Na1A 73.2(3) . 4
O20 Mo6 Na1A 147.6(3) . 4
O12 Mo6 Na1A 118.7(3) . 4
O18 Mo6 Na1A 63.7(3) . 4
O11 Mo6 Na1A 39.5(3) . 4
O31 Mo6 Na1A 102.2(2) . 4
O29 Mo7 O32 103.0(4) . .
O29 Mo7 O11 101.7(4) . .
O32 Mo7 O11 94.4(4) . .
O29 Mo7 O14 100.0(4) . .
O32 Mo7 O14 156.1(3) . .
O11 Mo7 O14 87.1(4) . .
O29 Mo7 O7 101.7(4) . .
O32 Mo7 O7 85.1(3) . .
O11 Mo7 O7 156.1(3) . .
O14 Mo7 O7 84.0(4) . .
O29 Mo7 O31 171.4(4) . .
O32 Mo7 O31 84.9(3) . .
O11 Mo7 O31 74.0(3) . .
O14 Mo7 O31 72.6(3) . .
O7 Mo7 O31 82.2(3) . .
O29 Mo7 Na1A 79.0(4) . 4
O32 Mo7 Na1A 71.8(3) . 4
O11 Mo7 Na1A 36.9(3) . 4
O14 Mo7 Na1A 119.5(3) . 4
O7 Mo7 Na1A 156.3(3) . 4
O31 Mo7 Na1A 100.6(2) . 4
O30 Mo8 O14 102.6(4) . .
O30 Mo8 O8 102.7(4) . .
O14 Mo8 O8 93.5(4) . .
O30 Mo8 O12 100.7(4) . .
O14 Mo8 O12 87.9(4) . .
O8 Mo8 O12 155.6(4) . .
O30 Mo8 O13 100.9(4) . .
O14 Mo8 O13 156.3(3) . .
O8 Mo8 O13 84.3(4) . .
O12 Mo8 O13 84.8(3) . .
O30 Mo8 O31 171.6(4) . .
O14 Mo8 O31 73.9(3) . .
O8 Mo8 O31 85.2(3) . .
O12 Mo8 O31 71.8(3) . .
O13 Mo8 O31 82.4(3) . .
O5 Mo9 O28 102.8(4) . .
O5 Mo9 O4 102.0(4) . .
O28 Mo9 O4 93.9(4) . .
O5 Mo9 O8 101.7(4) . .
O28 Mo9 O8 87.0(4) . .
O4 Mo9 O8 155.4(4) . .
O5 Mo9 O6 99.7(4) . .
O28 Mo9 O6 157.1(4) . .
O4 Mo9 O6 85.6(4) . .
O8 Mo9 O6 84.1(4) . .
O5 Mo9 O15 170.2(4) . .
O28 Mo9 O15 86.3(3) . .
O4 Mo9 O15 73.4(3) . .
O8 Mo9 O15 82.2(3) . .
O6 Mo9 O15 71.5(3) . .
O37 Mo11 O9 103.2(4) . .
O37 Mo11 O39 102.5(4) . .
O9 Mo11 O39 93.5(4) . .
O37 Mo11 O2 102.1(4) . .
O9 Mo11 O2 86.2(4) . .
O39 Mo11 O2 154.8(4) . .
O37 Mo11 O36 100.9(4) . .
O9 Mo11 O36 155.5(3) . .
O39 Mo11 O36 85.5(4) . .
O2 Mo11 O36 84.5(4) . .
O37 Mo11 O10 171.0(4) . .
O9 Mo11 O10 84.8(3) . .
O39 Mo11 O10 72.5(3) . .
O2 Mo11 O10 82.4(3) . .
O36 Mo11 O10 71.5(3) . .
O27 Mo12 O35 104.5(4) . .
O27 Mo12 O36 101.6(4) . .
O35 Mo12 O36 94.0(4) . .
O27 Mo12 O26 98.6(4) . .
O35 Mo12 O26 156.0(3) . .
O36 Mo12 O26 87.7(4) . .
O27 Mo12 O32 101.3(4) . .
O35 Mo12 O32 84.8(3) . .
O36 Mo12 O32 156.6(3) . .
O26 Mo12 O32 84.2(3) . .
O27 Mo12 O10 170.3(4) . .
O35 Mo12 O10 84.8(3) . .
O36 Mo12 O10 74.4(3) . .
O26 Mo12 O10 72.6(3) . .
O32 Mo12 O10 82.2(3) . .
O40 Mo10 O26 104.7(4) . .
O40 Mo10 O18 103.3(4) . .
O26 Mo10 O18 92.8(4) . .
O40 Mo10 O39 100.2(4) . .
O26 Mo10 O39 88.5(4) . .
O18 Mo10 O39 155.3(4) . .
O40 Mo10 O22 99.3(4) . .
O26 Mo10 O22 155.9(3) . .
O18 Mo10 O22 83.9(3) . .
O39 Mo10 O22 84.9(3) . .
O40 Mo10 O10 172.4(4) . .
O26 Mo10 O10 74.1(3) . .
O18 Mo10 O10 84.3(3) . .
O39 Mo10 O10 72.3(3) . .
O22 Mo10 O10 81.8(3) . .
C9 C6 N1 122.8(19) . .
C9 C6 H6 118.6 . .
N1 C6 H6 118.6 . .
C1 N2 N3 107.2(10) . .
C1 N2 Ag1A 130.6(9) . 4_556
N3 N2 Ag1A 115.3(8) . 4_556
C1 N2 Ag1B 134.7(10) . 4_556
N3 N2 Ag1B 117.1(9) . 4_556
Ag1A N2 Ag1B 31.6(4) 4_556 4_556
C2 N3 N2 104.1(10) . .
C2 N3 Ag4 141.2(9) . 3_446
N2 N3 Ag4 111.2(8) . 3_446
C2 N4 C1 103.4(10) . .
C2 N4 Ag2B 119.2(9) . .
C1 N4 Ag2B 123.3(9) . .
C2 N4 Ag2A 118.9(8) . .
C1 N4 Ag2A 137.3(8) . .
Ag2B N4 Ag2A 38.9(4) . .
C3 N5 N6 103.8(10) . .
C3 N5 Ag4 136.8(9) . .
N6 N5 Ag4 117.7(7) . .
C4 N6 N5 106.9(10) . .
C4 N6 Ag3B 136.0(9) . .
N5 N6 Ag3B 113.9(8) . .
C4 N6 Ag3A 134.2(9) . .
N5 N6 Ag3A 118.3(8) . .
Ag3B N6 Ag3A 22.1(2) . .
C3 N7 C4 101.9(10) . .
C3 N7 Ag2C 151.1(10) . .
C4 N7 Ag2C 104.4(8) . .
C3 N7 Ag2A 105.9(8) . .
C4 N7 Ag2A 151.5(8) . .
Ag2C N7 Ag2A 47.1(4) . .
C10 N8 N9 108.0(12) . .
C11 N9 N8 103.4(12) . .
C11 N9 Ag3B 115.5(10) . 2_455
N8 N9 Ag3B 140.9(9) . 2_455
C10 N10 C11 103.2(12) . .
C10 N10 Ag2A 138.9(11) . .
C11 N10 Ag2A 117.6(9) . .
C10 N10 Ag2C 118.6(10) . .
C11 N10 Ag2C 111.8(9) . .
Ag2A N10 Ag2C 51.1(4) . .
C12 N11 N12 103.3(11) . .
C12 N11 Ag2B 135.3(11) . .
N12 N11 Ag2B 121.1(9) . .
C13 N12 N11 109.6(11) . .
C13 N12 Na1A 128.8(10) . .
N11 N12 Na1A 121.5(9) . .
C13 N12 Na1B 147.4(10) . .
N11 N12 Na1B 98.2(8) . .
Na1A N12 Na1B 29.9(4) . .
C12 N13 C13 103.4(11) . .
C12 N13 Ag3A 121.8(9) . 2_455
C13 N13 Ag3A 133.5(9) . 2_455
C12 N13 Ag1B 116.7(9) . .
C13 N13 Ag1B 108.4(9) . .
Ag3A N13 Ag1B 62.5(4) 2_455 .
C12 N13 Ag3B 105.0(8) . 2_455
C13 N13 Ag3B 150.9(9) . 2_455
Ag3A N13 Ag3B 17.44(14) 2_455 2_455
Ag1B N13 Ag3B 63.6(4) . 2_455
C18 N14 C14 117.3(12) . .
C18 N14 Ag1A 120.1(9) . .
C14 N14 Ag1A 122.3(10) . .
Mo2 O2 Mo11 152.4(5) . .
Mo2 O3 Mo1 125.4(4) . .
Mo9 O4 Mo2 125.8(4) . .
Mo1 O6 Mo9 124.4(4) . .
Mo1 O7 Mo7 151.7(5) . .
Mo8 O8 Mo9 151.1(5) . .
Mo11 O9 Mo3 150.9(5) . .
P1 O10 Mo12 125.9(4) . .
P1 O10 Mo10 126.9(4) . .
Mo12 O10 Mo10 88.6(2) . .
P1 O10 Mo11 125.2(4) . .
Mo12 O10 Mo11 89.4(2) . .
Mo10 O10 Mo11 88.9(2) . .
Mo7 O11 Mo6 123.8(4) . .
Mo7 O11 Na1A 114.5(4) . 4
Mo6 O11 Na1A 107.8(4) . 4
Mo6 O12 Mo8 125.6(4) . .
Mo5 O13 Mo8 152.7(5) . .
Mo8 O14 Mo7 124.8(4) . .
P1 O15 Mo1 126.0(4) . .
P1 O15 Mo9 125.1(4) . .
Mo1 O15 Mo9 89.7(3) . .
P1 O15 Mo2 126.5(4) . .
Mo1 O15 Mo2 88.8(3) . .
Mo9 O15 Mo2 88.7(3) . .
Mo3 O16 Mo2 152.4(5) . .
P1 O17 Mo4 126.7(4) . .
P1 O17 Mo3 125.8(5) . .
Mo4 O17 Mo3 89.0(3) . .
P1 O17 Mo5 125.8(4) . .
Mo4 O17 Mo5 88.7(3) . .
Mo3 O17 Mo5 88.8(3) . .
Mo10 O18 Mo6 151.4(5) . .
Mo3 O19 Mo5 126.0(4) . .
Mo6 O20 Mo4 150.9(5) . .
Mo5 O21 Mo4 125.3(4) . .
Mo4 O22 Mo10 153.7(5) . .
Mo4 O23 Mo3 125.5(4) . .
Mo5 O25 Na1A 106.0(5) . .
Mo10 O26 Mo12 124.5(4) . .
Mo9 O28 Mo5 149.7(5) . .
P1 O31 Mo6 125.5(4) . .
P1 O31 Mo7 125.9(4) . .
Mo6 O31 Mo7 89.8(2) . .
P1 O31 Mo8 125.8(4) . .
Mo6 O31 Mo8 89.7(2) . .
Mo7 O31 Mo8 88.6(2) . .
Mo7 O32 Mo12 151.8(5) . .
Mo12 O35 Mo1 151.9(4) . .
Mo12 O36 Mo11 124.7(4) . .
Mo11 O39 Mo10 126.3(4) . .
O17 P1 O15 109.9(4) . .
O17 P1 O10 109.1(4) . .
O15 P1 O10 109.5(4) . .
O17 P1 O31 109.4(4) . .
O15 P1 O31 109.8(4) . .
O10 P1 O31 109.2(4) . .
Ag3B Ag3A N6 78.9(5) . .
Ag3B Ag3A N13 110.3(5) . 2_445
N6 Ag3A N13 168.8(4) . 2_445
Ag3B Ag3A Ag1B 98.6(6) . 2_445
N6 Ag3A Ag1B 124.1(4) . 2_445
N13 Ag3A Ag1B 62.3(4) 2_445 2_445
Ag3B Ag3A Ag1A 116.8(6) . 2_445
N6 Ag3A Ag1A 117.3(3) . 2_445
N13 Ag3A Ag1A 65.2(3) 2_445 2_445
Ag1B Ag3A Ag1A 19.7(3) 2_445 2_445
Ag3B Ag3A Ag4 81.7(4) . .
N6 Ag3A Ag4 60.7(3) . .
N13 Ag3A Ag4 125.8(3) 2_445 .
Ag1B Ag3A Ag4 63.7(3) 2_445 .
Ag1A Ag3A Ag4 62.63(5) 2_445 .
Ag3A Ag3B N6 79.1(5) . .
Ag3A Ag3B N9 124.3(6) . 2_445
N6 Ag3B N9 152.2(6) . 2_445
Ag3A Ag3B N13 52.3(5) . 2_445
N6 Ag3B N13 131.0(5) . 2_445
N9 Ag3B N13 72.5(4) 2_445 2_445
Ag3A Ag3B Ag1B 63.1(6) . 2_445
N6 Ag3B Ag1B 113.2(5) . 2_445
N9 Ag3B Ag1B 92.4(5) 2_445 2_445
N13 Ag3B Ag1B 53.8(4) 2_445 2_445
Ag3A Ag3B Ag4 84.2(5) . .
N6 Ag3B Ag4 61.1(3) . .
N9 Ag3B Ag4 129.5(4) 2_445 .
N13 Ag3B Ag4 113.1(4) 2_445 .
Ag1B Ag3B Ag4 62.2(3) 2_445 .
Ag2B Ag2A Ag2C 107.6(6) . .
Ag2B Ag2A N10 113.2(5) . .
Ag2C Ag2A N10 67.9(5) . .
Ag2B Ag2A N4 66.9(5) . .
Ag2C Ag2A N4 126.1(4) . .
N10 Ag2A N4 165.8(4) . .
Ag2B Ag2A N7 85.0(5) . .
Ag2C Ag2A N7 54.5(4) . .
N10 Ag2A N7 122.4(4) . .
N4 Ag2A N7 71.7(3) . .
Ag2A Ag2B N11 106.3(8) . .
Ag2A Ag2B N4 74.2(5) . .
N11 Ag2B N4 177.7(8) . .
Ag2A Ag2B Ag2C 42.6(4) . .
N11 Ag2B Ag2C 83.1(6) . .
N4 Ag2B Ag2C 98.6(6) . .
Ag2A Ag2B Na1B 149.9(7) . .
N11 Ag2B Na1B 78.7(6) . .
N4 Ag2B Na1B 102.0(6) . .
Ag2C Ag2B Na1B 111.3(6) . .
Ag2A Ag2B Na1A 164.9(6) . .
N11 Ag2B Na1A 63.5(5) . .
N4 Ag2B Na1A 116.4(6) . .
Ag2C Ag2B Na1A 122.7(5) . .
Na1B Ag2B Na1A 23.1(4) . .
Ag2A Ag2C N1 159.7(8) . .
Ag2A Ag2C N7 78.4(5) . .
N1 Ag2C N7 84.7(6) . .
Ag2A Ag2C N10 61.0(4) . .
N1 Ag2C N10 134.5(8) . .
N7 Ag2C N10 139.4(7) . .
Ag2A Ag2C Ag2B 29.8(3) . .
N1 Ag2C Ag2B 132.3(7) . .
N7 Ag2C Ag2B 70.2(5) . .
N10 Ag2C Ag2B 73.6(5) . .
Ag1A Ag1B N2 70.9(7) . 4
Ag1A Ag1B N13 107.9(9) . .
N2 Ag1B N13 167.6(8) 4 .
Ag1A Ag1B Ag3A 117.4(8) . 2_455
N2 Ag1B Ag3A 136.8(7) 4 2_455
N13 Ag1B Ag3A 55.3(4) . 2_455
Ag1A Ag1B Ag3B 134.0(9) . 2_455
N2 Ag1B Ag3B 127.6(7) 4 2_455
N13 Ag1B Ag3B 62.6(4) . 2_455
Ag3A Ag1B Ag3B 18.24(15) 2_455 2_455
Ag1A Ag1B Ag4 90.3(7) . 2_455
N2 Ag1B Ag4 63.2(4) 4 2_455
N13 Ag1B Ag4 129.2(6) . 2_455
Ag3A Ag1B Ag4 74.1(3) 2_455 2_455
Ag3B Ag1B Ag4 70.6(3) 2_455 2_455
Na1B Na1A N12 97.4(9) . .
Na1B Na1A O11 113.7(9) . 4_556
N12 Na1A O11 134.2(5) . 4_556
Na1B Na1A O25 98.0(8) . .
N12 Na1A O25 118.7(5) . .
O11 Na1A O25 90.3(4) 4_556 .
Na1B Na1A Ag2B 59.6(8) . .
N12 Na1A Ag2B 53.9(4) . .
O11 Na1A Ag2B 114.4(4) 4_556 .
O25 Na1A Ag2B 151.2(4) . .
Na1B Na1A Mo6 89.3(8) . 4_556
N12 Na1A Mo6 122.9(4) . 4_556
O11 Na1A Mo6 32.7(2) 4_556 4_556
O25 Na1A Mo6 116.2(3) . 4_556
Ag2B Na1A Mo6 83.6(2) . 4_556
Na1B Na1A Mo7 142.0(8) . 4_556
N12 Na1A Mo7 115.6(4) . 4_556
O11 Na1A Mo7 28.6(2) 4_556 4_556
O25 Na1A Mo7 82.8(3) . 4_556
Ag2B Na1A Mo7 126.0(3) . 4_556
Mo6 Na1A Mo7 57.67(13) 4_556 4_556
Na1B Na1A Mo5 81.6(8) . .
N12 Na1A Mo5 100.7(4) . .
O11 Na1A Mo5 115.9(3) 4_556 .
O25 Na1A Mo5 26.4(2) . .
Ag2B Na1A Mo5 125.4(3) . .
Mo6 Na1A Mo5 136.3(2) 4_556 .
Mo7 Na1A Mo5 108.4(2) 4_556 .
Na1A Na1B N12 52.7(7) . .
Na1A Na1B Ag2B 97.3(9) . .
N12 Na1B Ag2B 58.3(5) . .
Na1A Na1B Mo5 76.5(8) . .
N12 Na1B Mo5 89.4(5) . .
Ag2B Na1B Mo5 140.1(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N2 1.297(16) .
C1 N4 1.341(16) .
C1 H1 0.9300 .
C2 N3 1.331(15) .
C2 N4 1.328(15) .
C2 C3 1.484(17) .
C3 N7 1.319(16) .
C3 N5 1.326(16) .
C4 N6 1.307(17) .
C4 N7 1.345(16) .
C4 C5 1.493(18) .
C5 N1 1.37(2) .
C5 C7 1.41(2) .
C7 C8 1.42(2) .
C7 H7 0.9300 .
C8 C9 1.29(2) .
C8 H8 0.9300 .
C9 C6 1.25(2) .
C9 H9 0.9300 .
N1 C6 1.41(2) .
N1 Ag2C 2.092(15) .
C10 N10 1.299(18) .
C10 N8 1.331(19) .
C10 H10 0.9300 .
C11 N9 1.297(17) .
C11 N10 1.366(18) .
C11 C12 1.45(2) .
C12 N11 1.302(17) .
C12 N13 1.349(17) .
C13 N12 1.343(17) .
C13 N13 1.352(17) .
C13 C14 1.46(2) .
C14 C15 1.34(2) .
C14 N14 1.344(17) .
C15 C16 1.40(2) .
C15 H15 0.9300 .
C16 C17 1.34(2) .
C16 H16 0.9300 .
C17 C18 1.38(2) .
C17 H17 0.9300 .
C18 N14 1.332(18) .
C18 H18 0.9300 .
Ag1A Ag1B 1.164(13) .
Ag1A N2 2.099(11) 4
Ag1A N14 2.161(12) .
Ag1A Ag3A 3.067(3) 2_455
Ag1A Ag4 3.3560(18) 2_455
Ag4 N5 2.086(10) .
Ag4 N3 2.099(10) 3_446
Ag4 Ag4 2.765(2) 3_446
Ag4 Ag1B 3.142(13) 2_445
Ag4 Ag3B 3.352(6) .
Ag4 Ag1A 3.3560(18) 2_445
Ag4 Ag3A 3.371(3) .
Mo1 O34 1.693(8) .
Mo1 O7 1.843(8) .
Mo1 O6 1.860(8) .
Mo1 O3 1.969(8) .
Mo1 O35 1.973(8) .
Mo1 O15 2.405(8) .
Mo2 O1 1.682(9) .
Mo2 O3 1.852(8) .
Mo2 O2 1.875(9) .
Mo2 O4 1.953(8) .
Mo2 O16 1.994(8) .
Mo2 O15 2.447(8) .
Mo3 O33 1.665(8) .
Mo3 O16 1.837(8) .
Mo3 O19 1.869(9) .
Mo3 O9 1.962(8) .
Mo3 O23 2.004(8) .
Mo3 O17 2.445(8) .
Mo4 O24 1.695(8) .
Mo4 O23 1.838(8) .
Mo4 O22 1.861(8) .
Mo4 O21 1.971(8) .
Mo4 O20 1.981(8) .
Mo4 O17 2.429(8) .
Mo5 O25 1.667(8) .
Mo5 O13 1.848(9) .
Mo5 O21 1.871(8) .
Mo5 O19 1.978(9) .
Mo5 O28 1.978(8) .
Mo5 O17 2.452(8) .
Mo5 Na1A 3.608(8) .
Mo5 Na1B 3.670(17) .
Mo6 O38 1.693(9) .
Mo6 O20 1.845(8) .
Mo6 O12 1.895(8) .
Mo6 O18 1.942(8) .
Mo6 O11 1.994(8) .
Mo6 O31 2.415(8) .
Mo6 Na1A 3.518(8) 4
Mo7 O29 1.682(9) .
Mo7 O32 1.858(8) .
Mo7 O11 1.879(8) .
Mo7 O14 1.960(8) .
Mo7 O7 1.967(8) .
Mo7 O31 2.427(7) .
Mo7 Na1A 3.568(8) 4
Mo8 O30 1.687(9) .
Mo8 O14 1.869(8) .
Mo8 O8 1.881(9) .
Mo8 O12 1.948(9) .
Mo8 O13 1.973(9) .
Mo8 O31 2.432(8) .
Mo9 O5 1.676(9) .
Mo9 O28 1.847(8) .
Mo9 O4 1.882(8) .
Mo9 O8 1.954(9) .
Mo9 O6 1.999(8) .
Mo9 O15 2.436(8) .
Mo11 O37 1.672(9) .
Mo11 O9 1.855(8) .
Mo11 O39 1.888(9) .
Mo11 O2 1.952(9) .
Mo11 O36 2.003(8) .
Mo11 O10 2.449(7) .
Mo12 O27 1.670(9) .
Mo12 O35 1.850(8) .
Mo12 O36 1.861(8) .
Mo12 O26 1.965(8) .
Mo12 O32 1.979(8) .
Mo12 O10 2.419(7) .
Mo10 O40 1.681(9) .
Mo10 O26 1.860(8) .
Mo10 O18 1.889(8) .
Mo10 O39 1.938(9) .
Mo10 O22 1.968(8) .
Mo10 O10 2.425(8) .
C6 H6 0.9300 .
N2 N3 1.385(15) .
N2 Ag1A 2.099(11) 4_556
N2 Ag1B 2.169(17) 4_556
N3 Ag4 2.099(10) 3_446
N4 Ag2B 2.114(14) .
N4 Ag2A 2.212(11) .
N5 N6 1.372(14) .
N6 Ag3B 2.155(11) .
N6 Ag3A 2.156(10) .
N7 Ag2C 2.180(13) .
N7 Ag2A 2.623(10) .
N8 N9 1.376(18) .
N9 Ag3B 2.298(14) 2_455
N10 Ag2A 2.209(11) .
N10 Ag2C 2.339(15) .
N11 N12 1.367(16) .
N11 Ag2B 1.869(12) .
N12 Na1A 2.203(14) .
N12 Na1B 2.75(2) .
N13 Ag3A 2.180(10) 2_455
N13 Ag1B 2.348(17) .
N13 Ag3B 2.584(12) 2_455
O10 P1 1.538(8) .
O11 Na1A 2.352(11) 4
O15 P1 1.536(8) .
O17 P1 1.528(8) .
O25 Na1A 2.773(12) .
O31 P1 1.542(8) .
Ag3A Ag3B 0.825(6) .
Ag3A N13 2.180(10) 2_445
Ag3A Ag1B 2.353(13) 2_445
Ag3A Ag1A 3.067(3) 2_445
Ag3B N9 2.298(14) 2_445
Ag3B N13 2.584(12) 2_445
Ag3B Ag1B 2.608(15) 2_445
Ag2A Ag2B 1.444(12) .
Ag2A Ag2C 1.963(12) .
Ag2B Ag2C 2.766(14) .
Ag2B Na1B 3.04(2) .
Ag2B Na1A 3.493(14) .
Ag1B N2 2.169(17) 4
Ag1B Ag3A 2.353(13) 2_455
Ag1B Ag3B 2.608(15) 2_455
Ag1B Ag4 3.142(13) 2_455
Na1A Na1B 1.382(18) .
Na1A O11 2.352(11) 4_556
Na1A Mo6 3.518(8) 4_556
Na1A Mo7 3.568(8) 4_556
