#------------------------------------------------------------------------------
#$Date: 2024-03-04 22:07:46 +0200 (Mon, 04 Mar 2024) $
#$Revision: 290146 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/24/79/7247984.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7247984
loop_
_publ_author_name
'Yakubovich, Olga'
'Kiriukhina, Galina'
'Volkov, Anatoly'
'Simonov, Sergey'
'Yapaskurt, Vasiliy'
'Dimitrova, Olga'
_publ_section_title
;
 Crystal chemistry and predicted ionic conductivity of hydrothermally
 synthesized Na9Zn2(PO4)4Cl
;
_journal_issue                   6
_journal_name_full               CrystEngComm
_journal_page_first              848
_journal_page_last               855
_journal_paper_doi               10.1039/D3CE01242E
_journal_volume                  26
_journal_year                    2024
_chemical_formula_sum            'Cl0.5 Na4.5 O8 P2 Zn'
_chemical_formula_weight         376.49
_chemical_name_common            'sodiun zincophosphate chloride'
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2023-11-08 deposited with the CCDC.	2024-01-09 downloaded from the CCDC.
;
_cell_angle_alpha                100.539(3)
_cell_angle_beta                 104.874(3)
_cell_angle_gamma                90.936(2)
_cell_formula_units_Z            2
_cell_length_a                   5.15540(10)
_cell_length_b                   8.9641(3)
_cell_length_c                   9.1377(4)
_cell_measurement_reflns_used    5691
_cell_measurement_temperature    168(2)
_cell_measurement_theta_max      37.45
_cell_measurement_theta_min      2.34
_cell_volume                     400.36(2)
_computing_cell_refinement       'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)'
_computing_data_collection       'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)'
_computing_data_reduction        'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)'
_computing_molecular_graphics    Diamond
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    SHELXT
_diffrn_ambient_temperature      168(2)
_diffrn_detector_area_resol_mean 5.2283
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Xcalibur, AtlasS2, Gemini'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0207
_diffrn_reflns_av_unetI/netI     0.0168
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            9783
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.999
_diffrn_reflns_theta_min         2.316
_diffrn_source                   'fine-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    3.897
_exptl_absorpt_correction_T_max  1.220
_exptl_absorpt_correction_T_min  0.880
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.42.84a (Rigaku Oxford Diffraction, 2023)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.123
_exptl_crystal_description       prism
_exptl_crystal_F_000             364
_exptl_crystal_size_max          0.170
_exptl_crystal_size_mid          0.081
_exptl_crystal_size_min          0.062
_exptl_transmission_factor_max   1.000
_exptl_transmission_factor_min   0.859
_refine_diff_density_max         0.515
_refine_diff_density_min         -0.455
_refine_diff_density_rms         0.099
_refine_ls_extinction_coef       0.0242(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.188
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     149
_refine_ls_number_reflns         2342
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.188
_refine_ls_R_factor_all          0.0175
_refine_ls_R_factor_gt           0.0167
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0190P)²+0.2000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0450
_refine_ls_wR_factor_ref         0.0454
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2254
_reflns_number_total             2342
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d3ce01242e2.cif
_cod_data_source_block           shelx
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_atom_sites_solution_primary' value 'Direct' was changed
to 'direct' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_atom_sites_solution_secondary' value 'Diffmap' was
changed to 'difmap'.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 7247984.cif.
;
_cod_original_formula_sum        'Cl0.50 Na4.50 O8 P2 Zn'
_cod_database_code               7247984
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.557
_shelx_estimated_absorpt_t_max   0.794
_exptl_absorpt_special_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Zn1 Zn 0.29757(3) 0.92352(2) 0.17799(2) 0.00709(6) Uani 1 1 d . . . . .
Cl1 Cl 0.5000 1.0000 0.5000 0.01181(10) Uani 1 2 d S . P . .
P1 P 0.82692(7) 1.12466(4) 0.20034(4) 0.00463(7) Uani 1 1 d . . . . .
P2 P 0.37657(7) 0.59981(4) 0.24772(4) 0.00560(8) Uani 1 1 d . . . . .
Na1 Na -0.10655(12) 0.81416(7) 0.40323(7) 0.00911(12) Uani 1 1 d . . . . .
Na2 Na 0.26671(12) 0.22743(7) -0.01873(7) 0.00922(12) Uani 1 1 d . . . . .
Na3 Na 1.0000 0.5000 0.5000 0.01194(17) Uani 1 2 d S . P . .
Na4 Na -0.18345(12) 0.44183(7) 0.11932(8) 0.01215(13) Uani 1 1 d . . . . .
Na5 Na 0.54123(13) 0.69817(7) 0.61839(8) 0.01465(14) Uani 1 1 d . . . . .
O1 O 0.8764(2) 1.16977(12) 0.05454(12) 0.00764(19) Uani 1 1 d . . . . .
O2 O 0.9505(2) 0.97142(11) 0.22262(12) 0.00648(19) Uani 1 1 d . . . . .
O3 O 0.4838(2) 0.73908(12) 0.19445(13) 0.0088(2) Uani 1 1 d . . . . .
O4 O 0.5175(2) 1.10337(12) 0.17572(12) 0.00756(19) Uani 1 1 d . . . . .
O5 O 0.9441(2) 1.25085(12) 0.33979(12) 0.0092(2) Uani 1 1 d . . . . .
O6 O 0.5950(2) 0.56759(14) 0.38355(14) 0.0150(2) Uani 1 1 d . . . . .
O7 O 0.3256(2) 0.46270(12) 0.11369(13) 0.0135(2) Uani 1 1 d . . . . .
O8 O 0.1161(2) 0.63387(13) 0.29349(15) 0.0167(2) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 Zn1 O4 115.98(4) . . ?
O3 Zn1 O2 127.84(4) . 1_455 ?
O4 Zn1 O2 113.66(4) . 1_455 ?
O3 Zn1 O1 88.16(4) . 2_675 ?
O4 Zn1 O1 104.76(4) . 2_675 ?
O2 Zn1 O1 94.06(4) 1_455 2_675 ?
O3 Zn1 Cl1 85.42(3) . . ?
O4 Zn1 Cl1 85.09(3) . . ?
O2 Zn1 Cl1 83.78(3) 1_455 . ?
O1 Zn1 Cl1 169.89(3) 2_675 . ?
O3 Zn1 Na2 97.40(3) . 2_565 ?
O4 Zn1 Na2 138.69(3) . 2_565 ?
O2 Zn1 Na2 50.25(3) 1_455 2_565 ?
O1 Zn1 Na2 50.14(3) 2_675 2_565 ?
Cl1 Zn1 Na2 123.062(13) . 2_565 ?
O3 Zn1 Na2 47.75(3) . 2_665 ?
O4 Zn1 Na2 78.68(3) . 2_665 ?
O2 Zn1 Na2 161.76(3) 1_455 2_665 ?
O1 Zn1 Na2 69.11(3) 2_675 2_665 ?
Cl1 Zn1 Na2 111.514(13) . 2_665 ?
Na2 Zn1 Na2 111.549(19) 2_565 2_665 ?
O3 Zn1 Na1 42.35(3) . 1_655 ?
O4 Zn1 Na1 84.95(3) . 1_655 ?
O2 Zn1 Na1 131.78(3) 1_455 1_655 ?
O1 Zn1 Na1 125.07(3) 2_675 1_655 ?
Cl1 Zn1 Na1 52.533(11) . 1_655 ?
Na2 Zn1 Na1 135.574(16) 2_565 1_655 ?
Na2 Zn1 Na1 59.985(15) 2_665 1_655 ?
O3 Zn1 Na2 139.16(3) . 1_565 ?
O4 Zn1 Na2 40.18(3) . 1_565 ?
O2 Zn1 Na2 90.57(3) 1_455 1_565 ?
O1 Zn1 Na2 74.14(3) 2_675 1_565 ?
Cl1 Zn1 Na2 115.673(12) . 1_565 ?
Na2 Zn1 Na2 98.566(14) 2_565 1_565 ?
Na2 Zn1 Na2 91.409(15) 2_665 1_565 ?
Na1 Zn1 Na2 123.873(15) 1_655 1_565 ?
O3 Zn1 Na1 89.06(3) . . ?
O4 Zn1 Na1 137.96(3) . . ?
O2 Zn1 Na1 41.44(3) 1_455 . ?
O1 Zn1 Na1 109.50(3) 2_675 . ?
Cl1 Zn1 Na1 62.661(11) . . ?
Na2 Zn1 Na1 60.556(15) 2_565 . ?
Na2 Zn1 Na1 136.303(16) 2_665 . ?
Na1 Zn1 Na1 94.524(15) 1_655 . ?
Na2 Zn1 Na1 131.346(14) 1_565 . ?
O3 Zn1 Na5 132.11(4) . 2_676 ?
O4 Zn1 Na5 41.17(3) . 2_676 ?
O2 Zn1 Na5 80.16(3) 1_455 2_676 ?
O1 Zn1 Na5 132.57(3) 2_675 2_676 ?
Cl1 Zn1 Na5 56.869(12) . 2_676 ?
Na2 Zn1 Na5 126.753(17) 2_565 2_676 ?
Na2 Zn1 Na5 116.166(16) 2_665 2_676 ?
Na1 Zn1 Na5 89.759(16) 1_655 2_676 ?
Na2 Zn1 Na5 59.024(16) 1_565 2_676 ?
Na1 Zn1 Na5 96.858(15) . 2_676 ?
Zn1 Cl1 Zn1 180.0 2_676 . ?
Zn1 Cl1 Na1 76.231(13) 2_676 2_576 ?
Zn1 Cl1 Na1 103.769(13) . 2_576 ?
Zn1 Cl1 Na1 103.769(13) 2_676 1_655 ?
Zn1 Cl1 Na1 76.231(13) . 1_655 ?
Na1 Cl1 Na1 180.00(2) 2_576 1_655 ?
Zn1 Cl1 Na5 106.540(14) 2_676 2_676 ?
Zn1 Cl1 Na5 73.460(14) . 2_676 ?
Na1 Cl1 Na5 66.915(17) 2_576 2_676 ?
Na1 Cl1 Na5 113.085(17) 1_655 2_676 ?
Zn1 Cl1 Na5 73.459(14) 2_676 . ?
Zn1 Cl1 Na5 106.540(14) . . ?
Na1 Cl1 Na5 113.084(17) 2_576 . ?
Na1 Cl1 Na5 66.916(17) 1_655 . ?
Na5 Cl1 Na5 180.0 2_676 . ?
Zn1 Cl1 Na1 69.195(11) 2_676 2_676 ?
Zn1 Cl1 Na1 110.805(11) . 2_676 ?
Na1 Cl1 Na1 112.134(19) 2_576 2_676 ?
Na1 Cl1 Na1 67.866(19) 1_655 2_676 ?
Na5 Cl1 Na1 69.810(16) 2_676 2_676 ?
Na5 Cl1 Na1 110.189(16) . 2_676 ?
Zn1 Cl1 Na1 110.806(11) 2_676 . ?
Zn1 Cl1 Na1 69.194(11) . . ?
Na1 Cl1 Na1 67.866(19) 2_576 . ?
Na1 Cl1 Na1 112.134(19) 1_655 . ?
Na5 Cl1 Na1 110.189(16) 2_676 . ?
Na5 Cl1 Na1 69.811(16) . . ?
Na1 Cl1 Na1 180.0 2_676 . ?
O5 P1 O1 109.67(6) . . ?
O5 P1 O2 111.62(6) . . ?
O1 P1 O2 109.80(6) . . ?
O5 P1 O4 109.38(6) . . ?
O1 P1 O4 107.83(6) . . ?
O2 P1 O4 108.45(6) . . ?
O5 P1 Na4 66.85(4) . 1_665 ?
O1 P1 Na4 52.25(4) . 1_665 ?
O2 P1 Na4 154.67(4) . 1_665 ?
O4 P1 Na4 95.20(4) . 1_665 ?
O5 P1 Na5 59.05(4) . 2_676 ?
O1 P1 Na5 122.07(4) . 2_676 ?
O2 P1 Na5 127.55(4) . 2_676 ?
O4 P1 Na5 50.36(4) . 2_676 ?
Na4 P1 Na5 74.774(19) 1_665 2_676 ?
O5 P1 Na2 153.68(5) . 2_665 ?
O1 P1 Na2 88.57(4) . 2_665 ?
O2 P1 Na2 42.55(4) . 2_665 ?
O4 P1 Na2 81.29(4) . 2_665 ?
Na4 P1 Na2 137.78(2) 1_665 2_665 ?
Na5 P1 Na2 127.194(19) 2_676 2_665 ?
O5 P1 Na2 110.32(5) . 1_565 ?
O1 P1 Na2 68.95(4) . 1_565 ?
O2 P1 Na2 135.25(4) . 1_565 ?
O4 P1 Na2 41.26(4) . 1_565 ?
Na4 P1 Na2 60.644(17) 1_665 1_565 ?
Na5 P1 Na2 65.355(19) 2_676 1_565 ?
Na2 P1 Na2 93.657(17) 2_665 1_565 ?
O6 P2 O8 111.03(7) . . ?
O6 P2 O7 109.71(7) . . ?
O8 P2 O7 109.78(7) . . ?
O6 P2 O3 107.31(6) . . ?
O8 P2 O3 110.54(6) . . ?
O7 P2 O3 108.39(6) . . ?
O6 P2 Na4 126.74(5) . . ?
O8 P2 Na4 49.41(5) . . ?
O7 P2 Na4 60.38(5) . . ?
O3 P2 Na4 125.76(4) . . ?
O6 P2 Na4 72.28(5) . 1_655 ?
O8 P2 Na4 163.68(5) . 1_655 ?
O7 P2 Na4 55.33(5) . 1_655 ?
O3 P2 Na4 82.61(4) . 1_655 ?
Na4 P2 Na4 115.27(2) . 1_655 ?
O6 P2 Na1 57.24(5) . 1_655 ?
O8 P2 Na1 120.22(5) . 1_655 ?
O7 P2 Na1 129.77(5) . 1_655 ?
O3 P2 Na1 50.62(4) . 1_655 ?
Na4 P2 Na1 169.02(2) . 1_655 ?
Na4 P2 Na1 75.424(18) 1_655 1_655 ?
O6 P2 Na5 50.90(5) . 2_666 ?
O8 P2 Na5 95.07(5) . 2_666 ?
O7 P2 Na5 70.98(5) . 2_666 ?
O3 P2 Na5 152.16(4) . 2_666 ?
Na4 P2 Na5 79.170(19) . 2_666 ?
Na4 P2 Na5 74.404(19) 1_655 2_666 ?
Na1 P2 Na5 107.25(2) 1_655 2_666 ?
O6 P2 Na4 144.99(5) . 2_565 ?
O8 P2 Na4 102.05(5) . 2_565 ?
O7 P2 Na4 45.56(5) . 2_565 ?
O3 P2 Na4 69.78(4) . 2_565 ?
Na4 P2 Na4 68.46(2) . 2_565 ?
Na4 P2 Na4 72.76(2) 1_655 2_565 ?
Na1 P2 Na4 114.702(19) 1_655 2_565 ?
Na5 P2 Na4 116.45(2) 2_666 2_565 ?
O6 P2 Na5 42.36(5) . . ?
O8 P2 Na5 73.67(5) . . ?
O7 P2 Na5 143.64(5) . . ?
O3 P2 Na5 103.49(4) . . ?
Na4 P2 Na5 112.71(2) . . ?
Na4 P2 Na5 113.65(2) 1_655 . ?
Na1 P2 Na5 62.338(18) 1_655 . ?
Na5 P2 Na5 72.66(2) 2_666 . ?
Na4 P2 Na5 170.55(2) 2_565 . ?
O8 Na1 O2 89.70(4) . 1_455 ?
O8 Na1 O3 91.43(5) . 1_455 ?
O2 Na1 O3 78.62(4) 1_455 1_455 ?
O8 Na1 O5 93.20(5) . 2_676 ?
O2 Na1 O5 148.11(4) 1_455 2_676 ?
O3 Na1 O5 132.95(4) 1_455 2_676 ?
O8 Na1 O6 78.34(4) . 1_455 ?
O2 Na1 O6 134.79(4) 1_455 1_455 ?
O3 Na1 O6 58.57(4) 1_455 1_455 ?
O5 Na1 O6 76.67(4) 2_676 1_455 ?
O8 Na1 Cl1 166.48(4) . 1_455 ?
O2 Na1 Cl1 92.64(3) 1_455 1_455 ?
O3 Na1 Cl1 76.01(3) 1_455 1_455 ?
O5 Na1 Cl1 91.83(3) 2_676 1_455 ?
O6 Na1 Cl1 90.64(3) 1_455 1_455 ?
O8 Na1 P2 86.73(4) . 1_455 ?
O2 Na1 P2 107.81(3) 1_455 1_455 ?
O3 Na1 P2 29.61(3) 1_455 1_455 ?
O5 Na1 P2 104.05(3) 2_676 1_455 ?
O6 Na1 P2 29.19(3) 1_455 1_455 ?
Cl1 Na1 P2 79.870(17) 1_455 1_455 ?
O8 Na1 Na3 55.09(3) . 1_455 ?
O2 Na1 Na3 144.76(3) 1_455 1_455 ?
O3 Na1 Na3 98.82(3) 1_455 1_455 ?
O5 Na1 Na3 49.33(3) 2_676 1_455 ?
O6 Na1 Na3 44.79(3) 1_455 1_455 ?
Cl1 Na1 Na3 121.16(2) 1_455 1_455 ?
P2 Na1 Na3 72.201(15) 1_455 1_455 ?
O8 Na1 Na5 114.67(4) . 1_455 ?
O2 Na1 Na5 150.64(3) 1_455 1_455 ?
O3 Na1 Na5 84.39(3) 1_455 1_455 ?
O5 Na1 Na5 51.51(3) 2_676 1_455 ?
O6 Na1 Na5 44.88(3) 1_455 1_455 ?
Cl1 Na1 Na5 59.839(16) 1_455 1_455 ?
P2 Na1 Na5 60.424(18) 1_455 1_455 ?
Na3 Na1 Na5 61.317(16) 1_455 1_455 ?
O8 Na1 Na2 67.35(4) . 2_565 ?
O2 Na1 Na2 44.77(3) 1_455 2_565 ?
O3 Na1 Na2 44.74(3) 1_455 2_565 ?
O5 Na1 Na2 159.01(4) 2_676 2_565 ?
O6 Na1 Na2 91.12(3) 1_455 2_565 ?
Cl1 Na1 Na2 105.50(2) 1_455 2_565 ?
P2 Na1 Na2 68.424(17) 1_455 2_565 ?
Na3 Na1 Na2 110.26(2) 1_455 2_565 ?
Na5 Na1 Na2 128.30(2) 1_455 2_565 ?
O8 Na1 Cl1 80.98(3) . . ?
O2 Na1 Cl1 66.32(3) 1_455 . ?
O3 Na1 Cl1 144.04(3) 1_455 . ?
O5 Na1 Cl1 82.79(3) 2_676 . ?
O6 Na1 Cl1 149.79(3) 1_455 . ?
Cl1 Na1 Cl1 112.134(19) 1_455 . ?
P2 Na1 Cl1 166.29(2) 1_455 . ?
Na3 Na1 Cl1 105.053(17) 1_455 . ?
Na5 Na1 Cl1 130.73(2) 1_455 . ?
Na2 Na1 Cl1 100.966(19) 2_565 . ?
O8 Na1 Na1 130.24(4) . 2_576 ?
O2 Na1 Na1 69.65(3) 1_455 2_576 ?
O3 Na1 Na1 125.37(4) 1_455 2_576 ?
O5 Na1 Na1 84.58(3) 2_676 2_576 ?
O6 Na1 Na1 147.00(4) 1_455 2_576 ?
Cl1 Na1 Na1 62.766(18) 1_455 2_576 ?
P2 Na1 Na1 142.04(3) 1_455 2_576 ?
Na3 Na1 Na1 132.31(3) 1_455 2_576 ?
Na5 Na1 Na1 102.40(3) 1_455 2_576 ?
Na2 Na1 Na1 113.67(3) 2_565 2_576 ?
Cl1 Na1 Na1 49.368(16) . 2_576 ?
O7 Na2 O3 97.60(4) . 2_665 ?
O7 Na2 O1 94.31(4) . 1_445 ?
O3 Na2 O1 155.21(5) 2_665 1_445 ?
O7 Na2 O2 154.80(5) . 2_665 ?
O3 Na2 O2 81.80(4) 2_665 2_665 ?
O1 Na2 O2 78.24(4) 1_445 2_665 ?
O7 Na2 O4 99.01(5) . 1_545 ?
O3 Na2 O4 110.76(4) 2_665 1_545 ?
O1 Na2 O4 88.60(4) 1_445 1_545 ?
O2 Na2 O4 104.77(4) 2_665 1_545 ?
O7 Na2 Zn1 121.33(4) . 2_565 ?
O3 Na2 Zn1 112.87(3) 2_665 2_565 ?
O1 Na2 Zn1 42.92(3) 1_445 2_565 ?
O2 Na2 Zn1 40.05(3) 2_665 2_565 ?
O4 Na2 Zn1 113.56(3) 1_545 2_565 ?
O7 Na2 Zn1 122.22(4) . 2_665 ?
O3 Na2 Zn1 37.47(3) 2_665 2_665 ?
O1 Na2 Zn1 142.56(4) 1_445 2_665 ?
O2 Na2 Zn1 71.51(3) 2_665 2_665 ?
O4 Na2 Zn1 78.57(3) 1_545 2_665 ?
Zn1 Na2 Zn1 111.549(19) 2_565 2_665 ?
O7 Na2 Na4 51.38(3) . 1_655 ?
O3 Na2 Na4 63.52(3) 2_665 1_655 ?
O1 Na2 Na4 138.76(4) 1_445 1_655 ?
O2 Na2 Na4 142.67(4) 2_665 1_655 ?
O4 Na2 Na4 77.21(3) 1_545 1_655 ?
Zn1 Na2 Na4 168.84(3) 2_565 1_655 ?
Zn1 Na2 Na4 72.494(17) 2_665 1_655 ?
O7 Na2 P1 177.31(4) . 2_665 ?
O3 Na2 P1 84.92(3) 2_665 2_665 ?
O1 Na2 P1 83.71(3) 1_445 2_665 ?
O2 Na2 P1 26.39(3) 2_665 2_665 ?
O4 Na2 P1 79.16(3) 1_545 2_665 ?
Zn1 Na2 P1 58.138(13) 2_565 2_665 ?
Zn1 Na2 P1 59.496(13) 2_665 2_665 ?
Na4 Na2 P1 129.61(2) 1_655 2_665 ?
O7 Na2 Na4 46.94(4) . 2_565 ?
O3 Na2 Na4 68.63(3) 2_665 2_565 ?
O1 Na2 Na4 105.39(3) 1_445 2_565 ?
O2 Na2 Na4 111.42(3) 2_665 2_565 ?
O4 Na2 Na4 143.07(4) 1_545 2_565 ?
Zn1 Na2 Na4 99.08(2) 2_565 2_565 ?
Zn1 Na2 Na4 105.84(2) 2_665 2_565 ?
Na4 Na2 Na4 69.76(2) 1_655 2_565 ?
P1 Na2 Na4 135.36(2) 2_665 2_565 ?
O7 Na2 P1 92.82(4) . 1_545 ?
O3 Na2 P1 87.23(3) 2_665 1_545 ?
O1 Na2 P1 113.88(3) 1_445 1_545 ?
O2 Na2 P1 112.26(3) 2_665 1_545 ?
O4 Na2 P1 25.57(3) 1_545 1_545 ?
Zn1 Na2 P1 135.33(2) 2_565 1_545 ?
Zn1 Na2 P1 61.015(13) 2_665 1_545 ?
Na4 Na2 P1 55.830(16) 1_655 1_545 ?
P1 Na2 P1 86.344(17) 2_665 1_545 ?
Na4 Na2 P1 125.58(2) 2_565 1_545 ?
O7 Na2 Na1 116.50(4) . 2_565 ?
O3 Na2 Na1 46.90(3) 2_665 2_565 ?
O1 Na2 Na1 108.32(3) 1_445 2_565 ?
O2 Na2 Na1 46.48(3) 2_665 2_565 ?
O4 Na2 Na1 138.46(4) 1_545 2_565 ?
Zn1 Na2 Na1 66.523(16) 2_565 2_565 ?
Zn1 Na2 Na1 64.849(16) 2_665 2_565 ?
Na4 Na2 Na1 107.80(2) 1_655 2_565 ?
P1 Na2 Na1 65.949(17) 2_665 2_565 ?
Na4 Na2 Na1 69.76(2) 2_565 2_565 ?
P1 Na2 Na1 125.86(2) 1_545 2_565 ?
O6 Na3 O6 180.0 2_766 . ?
O6 Na3 O5 94.30(4) 2_766 2_776 ?
O6 Na3 O5 85.70(4) . 2_776 ?
O6 Na3 O5 85.70(4) 2_766 1_545 ?
O6 Na3 O5 94.30(4) . 1_545 ?
O5 Na3 O5 180.0 2_776 1_545 ?
O6 Na3 O8 78.93(4) 2_766 2_666 ?
O6 Na3 O8 101.07(4) . 2_666 ?
O5 Na3 O8 93.92(4) 2_776 2_666 ?
O5 Na3 O8 86.08(4) 1_545 2_666 ?
O6 Na3 O8 101.07(4) 2_766 1_655 ?
O6 Na3 O8 78.93(4) . 1_655 ?
O5 Na3 O8 86.08(4) 2_776 1_655 ?
O5 Na3 O8 93.92(4) 1_545 1_655 ?
O8 Na3 O8 180.0 2_666 1_655 ?
O6 Na3 Na5 128.16(3) 2_766 2_666 ?
O6 Na3 Na5 51.84(3) . 2_666 ?
O5 Na3 Na5 124.11(3) 2_776 2_666 ?
O5 Na3 Na5 55.89(3) 1_545 2_666 ?
O8 Na3 Na5 66.30(3) 2_666 2_666 ?
O8 Na3 Na5 113.70(3) 1_655 2_666 ?
O6 Na3 Na5 51.84(3) 2_766 1_655 ?
O6 Na3 Na5 128.16(3) . 1_655 ?
O5 Na3 Na5 55.89(3) 2_776 1_655 ?
O5 Na3 Na5 124.11(3) 1_545 1_655 ?
O8 Na3 Na5 113.70(3) 2_666 1_655 ?
O8 Na3 Na5 66.30(3) 1_655 1_655 ?
Na5 Na3 Na5 180.0 2_666 1_655 ?
O6 Na3 Na1 124.19(3) 2_766 1_655 ?
O6 Na3 Na1 55.81(3) . 1_655 ?
O5 Na3 Na1 50.96(3) 2_776 1_655 ?
O5 Na3 Na1 129.04(3) 1_545 1_655 ?
O8 Na3 Na1 135.11(3) 2_666 1_655 ?
O8 Na3 Na1 44.89(3) 1_655 1_655 ?
Na5 Na3 Na1 107.480(17) 2_666 1_655 ?
Na5 Na3 Na1 72.520(17) 1_655 1_655 ?
O6 Na3 Na1 55.81(3) 2_766 2_666 ?
O6 Na3 Na1 124.19(3) . 2_666 ?
O5 Na3 Na1 129.04(3) 2_776 2_666 ?
O5 Na3 Na1 50.96(3) 1_545 2_666 ?
O8 Na3 Na1 44.89(3) 2_666 2_666 ?
O8 Na3 Na1 135.11(3) 1_655 2_666 ?
Na5 Na3 Na1 72.520(17) 2_666 2_666 ?
Na5 Na3 Na1 107.480(17) 1_655 2_666 ?
Na1 Na3 Na1 180.0 1_655 2_666 ?
O6 Na3 Na5 45.60(3) 2_766 2_766 ?
O6 Na3 Na5 134.40(3) . 2_766 ?
O5 Na3 Na5 128.04(3) 2_776 2_766 ?
O5 Na3 Na5 51.96(3) 1_545 2_766 ?
O8 Na3 Na5 105.26(3) 2_666 2_766 ?
O8 Na3 Na5 74.74(3) 1_655 2_766 ?
Na5 Na3 Na5 107.786(19) 2_666 2_766 ?
Na5 Na3 Na5 72.214(19) 1_655 2_766 ?
Na1 Na3 Na5 118.214(16) 1_655 2_766 ?
Na1 Na3 Na5 61.786(16) 2_666 2_766 ?
O6 Na3 Na5 134.40(3) 2_766 . ?
O6 Na3 Na5 45.60(3) . . ?
O5 Na3 Na5 51.96(3) 2_776 . ?
O5 Na3 Na5 128.04(3) 1_545 . ?
O8 Na3 Na5 74.74(3) 2_666 . ?
O8 Na3 Na5 105.26(3) 1_655 . ?
Na5 Na3 Na5 72.214(19) 2_666 . ?
Na5 Na3 Na5 107.786(19) 1_655 . ?
Na1 Na3 Na5 61.786(16) 1_655 . ?
Na1 Na3 Na5 118.214(16) 2_666 . ?
Na5 Na3 Na5 180.00(2) 2_766 . ?
O8 Na4 O7 105.34(5) . 2_565 ?
O8 Na4 O1 128.82(5) . 1_445 ?
O7 Na4 O1 108.86(4) 2_565 1_445 ?
O8 Na4 O7 115.78(4) . 1_455 ?
O7 Na4 O7 81.90(4) 2_565 1_455 ?
O1 Na4 O7 105.87(4) 1_445 1_455 ?
O8 Na4 O7 59.81(4) . . ?
O7 Na4 O7 91.66(4) 2_565 . ?
O1 Na4 O7 82.11(4) 1_445 . ?
O7 Na4 O7 171.01(6) 1_455 . ?
O8 Na4 O5 89.17(4) . 1_445 ?
O7 Na4 O5 164.27(4) 2_565 1_445 ?
O1 Na4 O5 56.05(3) 1_445 1_445 ?
O7 Na4 O5 97.44(4) 1_455 1_445 ?
O7 Na4 O5 90.46(4) . 1_445 ?
O8 Na4 O6 69.58(4) . 1_455 ?
O7 Na4 O6 118.77(4) 2_565 1_455 ?
O1 Na4 O6 120.96(4) 1_445 1_455 ?
O7 Na4 O6 53.21(4) 1_455 1_455 ?
O7 Na4 O6 126.40(4) . 1_455 ?
O5 Na4 O6 71.62(3) 1_445 1_455 ?
O8 Na4 P2 29.50(3) . . ?
O7 Na4 P2 100.00(3) 2_565 . ?
O1 Na4 P2 106.63(3) 1_445 . ?
O7 Na4 P2 144.78(4) 1_455 . ?
O7 Na4 P2 30.31(3) . . ?
O5 Na4 P2 89.62(3) 1_445 . ?
O6 Na4 P2 97.67(3) 1_455 . ?
O8 Na4 P1 117.11(4) . 1_445 ?
O7 Na4 P1 134.67(4) 2_565 1_445 ?
O1 Na4 P1 29.86(3) 1_445 1_445 ?
O7 Na4 P1 92.91(3) 1_455 1_445 ?
O7 Na4 P1 96.08(3) . 1_445 ?
O5 Na4 P1 29.62(2) 1_445 1_445 ?
O6 Na4 P1 91.54(3) 1_455 1_445 ?
P2 Na4 P1 108.90(2) . 1_445 ?
O8 Na4 P2 85.94(3) . 1_455 ?
O7 Na4 P2 91.77(3) 2_565 1_455 ?
O1 Na4 P2 128.89(3) 1_445 1_455 ?
O7 Na4 P2 29.93(3) 1_455 1_455 ?
O7 Na4 P2 145.20(3) . 1_455 ?
O5 Na4 P2 95.35(3) 1_445 1_455 ?
O6 Na4 P2 29.13(2) 1_455 1_455 ?
P2 Na4 P2 115.27(2) . 1_455 ?
P1 Na4 P2 105.77(2) 1_445 1_455 ?
O8 Na4 P2 127.58(4) . 2_565 ?
O7 Na4 P2 27.33(3) 2_565 2_565 ?
O1 Na4 P2 81.69(3) 1_445 2_565 ?
O7 Na4 P2 86.24(3) 1_455 2_565 ?
O7 Na4 P2 90.91(3) . 2_565 ?
O5 Na4 P2 137.06(3) 1_445 2_565 ?
O6 Na4 P2 136.35(3) 1_455 2_565 ?
P2 Na4 P2 111.54(2) . 2_565 ?
P1 Na4 P2 107.73(2) 1_445 2_565 ?
P2 Na4 P2 107.24(2) 1_455 2_565 ?
O8 Na4 Na2 156.30(4) . 1_455 ?
O7 Na4 Na2 84.05(3) 2_565 1_455 ?
O1 Na4 Na2 64.86(3) 1_445 1_455 ?
O7 Na4 Na2 42.93(3) 1_455 1_455 ?
O7 Na4 Na2 142.93(4) . 1_455 ?
O5 Na4 Na2 84.87(3) 1_445 1_455 ?
O6 Na4 Na2 86.79(3) 1_455 1_455 ?
P2 Na4 Na2 171.46(3) . 1_455 ?
P1 Na4 Na2 63.526(18) 1_445 1_455 ?
P2 Na4 Na2 71.854(18) 1_455 1_455 ?
P2 Na4 Na2 68.997(19) 2_565 1_455 ?
O6 Na5 O4 163.11(5) . 2_676 ?
O6 Na5 O6 76.90(5) . 2_666 ?
O4 Na5 O6 118.84(5) 2_676 2_666 ?
O6 Na5 O5 79.33(4) . 2_776 ?
O4 Na5 O5 98.01(4) 2_676 2_776 ?
O6 Na5 O5 113.89(4) 2_666 2_776 ?
O6 Na5 O5 121.47(5) . 2_676 ?
O4 Na5 O5 59.03(4) 2_676 2_676 ?
O6 Na5 O5 83.05(4) 2_666 2_676 ?
O5 Na5 O5 156.81(5) 2_776 2_676 ?
O6 Na5 O7 117.12(4) . 2_666 ?
O4 Na5 O7 79.20(4) 2_676 2_666 ?
O6 Na5 O7 53.30(4) 2_666 2_666 ?
O5 Na5 O7 87.67(4) 2_776 2_666 ?
O5 Na5 O7 90.75(4) 2_676 2_666 ?
O6 Na5 Cl1 91.04(4) . . ?
O4 Na5 Cl1 72.07(3) 2_676 . ?
O6 Na5 Cl1 155.28(4) 2_666 . ?
O5 Na5 Cl1 84.26(3) 2_776 . ?
O5 Na5 Cl1 85.15(3) 2_676 . ?
O7 Na5 Cl1 148.67(3) 2_666 . ?
O6 Na5 P1 148.43(4) . 2_676 ?
O4 Na5 P1 29.61(3) 2_676 2_676 ?
O6 Na5 P1 101.45(4) 2_666 2_676 ?
O5 Na5 P1 127.60(3) 2_776 2_676 ?
O5 Na5 P1 29.43(2) 2_676 2_676 ?
O7 Na5 P1 83.67(3) 2_666 2_676 ?
Cl1 Na5 P1 77.585(17) . 2_676 ?
O6 Na5 Na3 80.55(3) . 1_455 ?
O4 Na5 Na3 105.77(3) 2_676 1_455 ?
O6 Na5 Na3 45.40(3) 2_666 1_455 ?
O5 Na5 Na3 154.37(3) 2_776 1_455 ?
O5 Na5 Na3 48.43(3) 2_676 1_455 ?
O7 Na5 Na3 87.51(3) 2_666 1_455 ?
Cl1 Na5 Na3 111.86(2) . 1_455 ?
P1 Na5 Na3 76.761(16) 2_676 1_455 ?
O6 Na5 P2 90.01(3) . 2_666 ?
O4 Na5 P2 106.81(3) 2_676 2_666 ?
O6 Na5 P2 28.59(3) 2_666 2_666 ?
O5 Na5 P2 92.16(3) 2_776 2_666 ?
O5 Na5 P2 97.58(3) 2_676 2_666 ?
O7 Na5 P2 28.90(2) 2_666 2_666 ?
Cl1 Na5 P2 176.02(3) . 2_666 ?
P1 Na5 P2 103.38(2) 2_676 2_666 ?
Na3 Na5 P2 72.101(15) 1_455 2_666 ?
O6 Na5 P2 26.06(3) . . ?
O4 Na5 P2 141.47(4) 2_676 . ?
O6 Na5 P2 85.52(3) 2_666 . ?
O5 Na5 P2 98.02(3) 2_776 . ?
O5 Na5 P2 99.06(3) 2_676 . ?
O7 Na5 P2 136.24(3) 2_666 . ?
Cl1 Na5 P2 74.976(17) . . ?
P1 Na5 P2 123.01(2) 2_676 . ?
Na3 Na5 P2 68.984(16) 1_455 . ?
P2 Na5 P2 107.34(2) 2_666 . ?
O6 Na5 Na3 43.17(3) . . ?
O4 Na5 Na3 142.12(4) 2_676 . ?
O6 Na5 Na3 75.63(3) 2_666 . ?
O5 Na5 Na3 46.70(3) 2_776 . ?
O5 Na5 Na3 156.10(3) 2_676 . ?
O7 Na5 Na3 85.16(3) 2_666 . ?
Cl1 Na5 Na3 110.141(19) . . ?
P1 Na5 Na3 167.75(3) 2_676 . ?
Na3 Na5 Na3 107.785(19) 1_455 . ?
P2 Na5 Na3 68.258(15) 2_666 . ?
P2 Na5 Na3 68.958(15) . . ?
P1 O1 Zn1 129.79(6) . 2_675 ?
P1 O1 Na2 133.70(6) . 1_665 ?
Zn1 O1 Na2 86.94(4) 2_675 1_665 ?
P1 O1 Na4 97.89(5) . 1_665 ?
Zn1 O1 Na4 112.82(5) 2_675 1_665 ?
Na2 O1 Na4 89.50(4) 1_665 1_665 ?
P1 O2 Zn1 121.11(6) . 1_655 ?
P1 O2 Na2 111.06(6) . 2_665 ?
Zn1 O2 Na2 89.69(4) 1_655 2_665 ?
P1 O2 Na1 127.87(6) . 1_655 ?
Zn1 O2 Na1 106.01(4) 1_655 1_655 ?
Na2 O2 Na1 88.76(4) 2_665 1_655 ?
P2 O3 Zn1 124.08(6) . . ?
P2 O3 Na2 135.43(6) . 2_665 ?
Zn1 O3 Na2 94.78(4) . 2_665 ?
P2 O3 Na1 99.77(5) . 1_655 ?
Zn1 O3 Na1 105.39(5) . 1_655 ?
Na2 O3 Na1 88.37(4) 2_665 1_655 ?
P1 O4 Zn1 129.53(6) . . ?
P1 O4 Na2 113.17(6) . 1_565 ?
Zn1 O4 Na2 107.67(5) . 1_565 ?
P1 O4 Na5 100.03(5) . 2_676 ?
Zn1 O4 Na5 106.65(5) . 2_676 ?
Na2 O4 Na5 92.47(4) 1_565 2_676 ?
P1 O5 Na3 157.83(7) . 1_565 ?
P1 O5 Na1 119.38(6) . 2_676 ?
Na3 O5 Na1 79.70(4) 1_565 2_676 ?
P1 O5 Na5 111.30(6) . 2_776 ?
Na3 O5 Na5 81.34(3) 1_565 2_776 ?
Na1 O5 Na5 80.70(4) 2_676 2_776 ?
P1 O5 Na5 91.52(5) . 2_676 ?
Na3 O5 Na5 75.69(3) 1_565 2_676 ?
Na1 O5 Na5 91.96(4) 2_676 2_676 ?
Na5 O5 Na5 156.80(5) 2_776 2_676 ?
P1 O5 Na4 83.53(5) . 1_665 ?
Na3 O5 Na4 77.62(3) 1_565 1_665 ?
Na1 O5 Na4 157.06(5) 2_676 1_665 ?
Na5 O5 Na4 92.46(4) 2_776 1_665 ?
Na5 O5 Na4 85.81(4) 2_676 1_665 ?
P2 O6 Na3 155.23(8) . . ?
P2 O6 Na5 111.57(7) . . ?
Na3 O6 Na5 91.23(5) . . ?
P2 O6 Na5 100.51(6) . 2_666 ?
Na3 O6 Na5 82.76(4) . 2_666 ?
Na5 O6 Na5 103.09(5) . 2_666 ?
P2 O6 Na1 93.58(5) . 1_655 ?
Na3 O6 Na1 79.41(4) . 1_655 ?
Na5 O6 Na1 82.62(4) . 1_655 ?
Na5 O6 Na1 161.40(6) 2_666 1_655 ?
P2 O6 Na4 78.59(5) . 1_655 ?
Na3 O6 Na4 77.13(4) . 1_655 ?
Na5 O6 Na4 164.11(5) . 1_655 ?
Na5 O6 Na4 86.32(4) 2_666 1_655 ?
Na1 O6 Na4 84.61(4) 1_655 1_655 ?
P2 O7 Na2 162.03(8) . . ?
P2 O7 Na4 107.11(6) . 2_565 ?
Na2 O7 Na4 90.57(5) . 2_565 ?
P2 O7 Na4 94.74(5) . 1_655 ?
Na2 O7 Na4 85.70(4) . 1_655 ?
Na4 O7 Na4 98.10(4) 2_565 1_655 ?
P2 O7 Na4 89.31(5) . . ?
Na2 O7 Na4 87.98(4) . . ?
Na4 O7 Na4 88.34(4) 2_565 . ?
Na4 O7 Na4 171.01(6) 1_655 . ?
P2 O7 Na5 80.12(5) . 2_666 ?
Na2 O7 Na5 82.04(4) . 2_666 ?
Na4 O7 Na5 171.88(5) 2_565 2_666 ?
Na4 O7 Na5 84.76(4) 1_655 2_666 ?
Na4 O7 Na5 88.04(4) . 2_666 ?
P2 O8 Na1 144.79(7) . . ?
P2 O8 Na4 101.10(6) . . ?
Na1 O8 Na4 110.98(5) . . ?
P2 O8 Na3 118.74(7) . 1_455 ?
Na1 O8 Na3 80.02(4) . 1_455 ?
Na4 O8 Na3 83.53(4) . 1_455 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Zn1 O3 1.9356(10) . ?
Zn1 O4 1.9620(10) . ?
Zn1 O2 1.9719(10) 1_455 ?
Zn1 O1 2.0895(11) 2_675 ?
Zn1 Cl1 2.8070(2) . ?
Zn1 Na2 3.0642(6) 2_565 ?
Zn1 Na2 3.1705(6) 2_665 ?
Zn1 Na1 3.4964(6) 1_655 ?
Zn1 Na2 3.5124(6) 1_565 ?
Zn1 Na1 3.5228(6) . ?
Zn1 Na5 3.5297(7) 2_676 ?
Cl1 Zn1 2.8069(2) 2_676 ?
Cl1 Na1 2.8573(6) 2_576 ?
Cl1 Na1 2.8573(6) 1_655 ?
Cl1 Na5 3.0834(7) 2_676 ?
Cl1 Na5 3.0834(7) . ?
Cl1 Na1 3.3476(6) 2_676 ?
Cl1 Na1 3.3476(6) . ?
P1 O5 1.5243(11) . ?
P1 O1 1.5400(11) . ?
P1 O2 1.5486(10) . ?
P1 O4 1.5563(11) . ?
P1 Na4 3.0642(7) 1_665 ?
P1 Na5 3.1013(7) 2_676 ?
P1 Na2 3.2513(7) 2_665 ?
P1 Na2 3.3152(7) 1_565 ?
P2 O6 1.5219(12) . ?
P2 O8 1.5251(12) . ?
P2 O7 1.5340(11) . ?
P2 O3 1.5618(11) . ?
P2 Na4 3.0393(7) . ?
P2 Na4 3.0644(7) 1_655 ?
P2 Na1 3.1148(7) 1_655 ?
P2 Na5 3.1270(8) 2_666 ?
P2 Na4 3.1929(8) 2_565 ?
P2 Na5 3.2214(8) . ?
Na1 O8 2.2348(13) . ?
Na1 O2 2.4257(12) 1_455 ?
Na1 O3 2.4429(13) 1_455 ?
Na1 O5 2.4621(12) 2_676 ?
Na1 O6 2.6244(13) 1_455 ?
Na1 Cl1 2.8573(6) 1_455 ?
Na1 P2 3.1148(7) 1_455 ?
Na1 Na3 3.1187(6) 1_455 ?
Na1 Na5 3.2807(9) 1_455 ?
Na1 Na2 3.3446(9) 2_565 ?
Na1 Na1 3.4875(12) 2_576 ?
Na2 O7 2.2048(12) . ?
Na2 O3 2.3551(12) 2_665 ?
Na2 O1 2.3556(12) 1_445 ?
Na2 O2 2.3561(12) 2_665 ?
Na2 O4 2.3782(12) 1_545 ?
Na2 Zn1 3.0642(6) 2_565 ?
Na2 Zn1 3.1705(6) 2_665 ?
Na2 Na4 3.2280(9) 1_655 ?
Na2 P1 3.2514(7) 2_665 ?
Na2 Na4 3.2641(8) 2_565 ?
Na2 P1 3.3152(7) 1_545 ?
Na2 Na1 3.3447(9) 2_565 ?
Na3 O6 2.2352(11) 2_766 ?
Na3 O6 2.2352(11) . ?
Na3 O5 2.4042(10) 2_776 ?
Na3 O5 2.4042(10) 1_545 ?
Na3 O8 2.5970(13) 2_666 ?
Na3 O8 2.5970(13) 1_655 ?
Na3 Na5 3.1140(7) 2_666 ?
Na3 Na5 3.1140(7) 1_655 ?
Na3 Na1 3.1187(6) 1_655 ?
Na3 Na1 3.1187(6) 2_666 ?
Na3 Na5 3.2662(7) 2_766 ?
Na3 Na5 3.2662(7) . ?
Na4 O8 2.3518(14) . ?
Na4 O7 2.3852(14) 2_565 ?
Na4 O1 2.4461(12) 1_445 ?
Na4 O7 2.5290(13) 1_455 ?
Na4 O7 2.6423(13) . ?
Na4 O5 2.8355(12) 1_445 ?
Na4 O6 2.9779(14) 1_455 ?
Na4 P1 3.0642(7) 1_445 ?
Na4 P2 3.0644(7) 1_455 ?
Na4 P2 3.1929(8) 2_565 ?
Na4 Na2 3.2280(9) 1_455 ?
Na5 O6 2.3343(14) . ?
Na5 O4 2.4252(13) 2_676 ?
Na5 O6 2.4682(14) 2_666 ?
Na5 O5 2.6021(13) 2_776 ?
Na5 O5 2.6607(13) 2_676 ?
Na5 O7 3.0008(14) 2_666 ?
Na5 P1 3.1013(7) 2_676 ?
Na5 Na3 3.1140(7) 1_455 ?
Na5 P2 3.1270(8) 2_666 ?
O1 Zn1 2.0895(11) 2_675 ?
O1 Na2 2.3556(12) 1_665 ?
O1 Na4 2.4461(12) 1_665 ?
O2 Zn1 1.9719(10) 1_655 ?
O2 Na2 2.3561(12) 2_665 ?
O2 Na1 2.4257(12) 1_655 ?
O3 Na2 2.3551(12) 2_665 ?
O3 Na1 2.4430(12) 1_655 ?
O4 Na2 2.3782(12) 1_565 ?
O4 Na5 2.4252(13) 2_676 ?
O5 Na3 2.4043(10) 1_565 ?
O5 Na1 2.4621(12) 2_676 ?
O5 Na5 2.6021(13) 2_776 ?
O5 Na5 2.6607(13) 2_676 ?
O5 Na4 2.8355(12) 1_665 ?
O6 Na5 2.4682(14) 2_666 ?
O6 Na1 2.6244(13) 1_655 ?
O6 Na4 2.9779(14) 1_655 ?
O7 Na4 2.3851(14) 2_565 ?
O7 Na4 2.5290(13) 1_655 ?
O7 Na5 3.0009(14) 2_666 ?
O8 Na3 2.5970(13) 1_455 ?
