#------------------------------------------------------------------------------
#$Date: 2019-11-28 14:09:37 +0200 (Thu, 28 Nov 2019) $
#$Revision: 243921 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/26/7702602.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7702602
loop_
_publ_author_name
'Seisenbaeva, Gulaim A.'
'Shevelkov, Andrei V.'
'Tegenfeldt, Jörgen'
'Kloo, Lars'
'Drobot, Dmitrii V.'
'Kessler, Vadim G.'
_publ_section_title
;
 Homo- and hetero-metallic rhenium oxomethoxide complexes with a
 M4(µ-O)2(µ-OMe)4 planar core---a new family of metal
 alkoxides displaying a peculiar structural disorder. Preparation and
 X-ray single crystal study
;
_journal_issue                   19
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2762
_journal_paper_doi               10.1039/b103287a
_journal_year                    2001
_chemical_formula_sum            'C12 H36 O18 Re4'
_chemical_formula_weight         1213.21
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                113.434(2)
_cell_angle_beta                 93.048(2)
_cell_angle_gamma                92.736(2)
_cell_formula_units_Z            3
_cell_length_a                   7.8993(8)
_cell_length_b                   15.994(2)
_cell_length_c                   17.501(1)
_cell_measurement_reflns_used    '999 (I>10sigma(I))'
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      28.28
_cell_measurement_theta_min      1.39
_cell_volume                     2020.1(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINTPLUS'
_computing_molecular_graphics    'Bruker SHELXTL-NT'
_computing_publication_material  'Bruker SHELXTL-NT'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.861
_diffrn_measured_fraction_theta_max 0.861
_diffrn_measurement_device_type  'Bruker SMART CCD 1K'
_diffrn_measurement_method       'Bruker SMART'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0255
_diffrn_reflns_av_sigmaI/netI    0.0745
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            12007
_diffrn_reflns_theta_full        28.28
_diffrn_reflns_theta_max         28.28
_diffrn_reflns_theta_min         1.39
_exptl_absorpt_coefficient_mu    17.799
_exptl_absorpt_correction_T_max  0.0624
_exptl_absorpt_correction_T_min  0.0460
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'Bruker SADABS'
_exptl_crystal_colour            'reddish black'
_exptl_crystal_density_diffrn    2.960
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1656
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.35
_refine_diff_density_max         2.176
_refine_diff_density_min         -1.626
_refine_diff_density_rms         0.232
_refine_ls_extinction_coef       0.000325(18)
_refine_ls_extinction_expression Fc^*^==kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.832
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     479
_refine_ls_number_reflns         8746
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.832
_refine_ls_R_factor_all          0.0574
_refine_ls_R_factor_gt           0.0348
_refine_ls_shift/su_max          0.144
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w==1/[σ²(Fo²)+(0.0256P)²+0.0000P] where P==(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0664
_refine_ls_wR_factor_ref         0.0701
_reflns_number_gt                5990
_reflns_number_total             8746
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b103287a.txt
_cod_data_source_block           reomem
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        2020.1(6)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7702602
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Re1 Re 0.41991(5) 0.16099(3) 0.04948(3) 0.03178(11) Uani 1 1 d .
Re2 Re 0.36326(5) -0.04495(3) -0.14787(2) 0.03092(11) Uani 1 1 d .
Re3 Re 0.19812(5) 0.31247(3) 0.79540(2) 0.02868(10) Uani 1 1 d .
Re4 Re -0.01065(5) 0.46234(2) 0.73358(2) 0.02876(10) Uani 1 1 d .
Re5 Re 0.10074(5) 0.33101(3) 0.51690(2) 0.03027(11) Uani 1 1 d .
Re6 Re 0.30294(5) 0.17974(3) 0.57972(2) 0.03107(11) Uani 1 1 d .
O1 O 0.4302(7) 0.0551(4) -0.0483(4) 0.0290(15) Uani 1 1 d .
O2 O 0.3372(8) 0.2968(4) 0.5603(4) 0.0334(16) Uani 1 1 d .
O3 O 0.0820(9) 0.3990(4) 0.6308(4) 0.0349(17) Uani 1 1 d .
O4 O 0.2302(8) 0.4351(4) 0.7826(4) 0.0333(16) Uani 1 1 d .
O5 O -0.0424(8) 0.3468(4) 0.7572(4) 0.0342(17) Uani 1 1 d .
O6 O 0.0651(8) 0.2075(4) 0.5273(4) 0.0359(17) Uani 1 1 d .
O7 O 0.3896(8) 0.0877(4) 0.1226(4) 0.0332(16) Uani 1 1 d .
O8 O -0.0556(9) 0.5228(4) 0.8472(4) 0.0425(19) Uani 1 1 d .
O9 O 0.2045(8) 0.2434(4) 0.6811(4) 0.0306(16) Uani 1 1 d .
O10 O 0.1410(9) 0.3806(4) 0.9067(4) 0.0398(18) Uani 1 1 d .
O11 O 0.1711(9) 0.2665(4) 0.4079(4) 0.0407(18) Uani 1 1 d .
O12 O 0.3366(8) -0.1272(4) -0.0836(4) 0.0365(17) Uani 1 1 d .
O13 O 0.3458(8) -0.1563(4) -0.2434(4) 0.0396(17) Uani 1 1 d .
O14 O 0.3509(9) 0.1211(4) 0.4658(4) 0.0436(19) Uani 1 1 d .
O15 O 0.0864(9) 0.2095(4) 0.8050(4) 0.0359(17) Uani 1 1 d .
O16 O 0.2138(9) 0.4352(4) 0.5119(4) 0.0395(18) Uani 1 1 d .
O17 O 0.4059(9) 0.3112(5) 0.8178(4) 0.0446(19) Uani 1 1 d .
O18 O 0.0853(9) 0.5772(4) 0.7440(4) 0.0384(17) Uani 1 1 d .
O19 O -0.2095(9) 0.4541(5) 0.6917(5) 0.048(2) Uani 1 1 d .
O20 O 0.4558(9) 0.2704(4) 0.1504(4) 0.0467(19) Uani 1 1 d .
O21 O 0.5267(9) 0.2283(4) -0.0037(4) 0.0405(18) Uani 1 1 d .
O22 O -0.1051(9) 0.3310(4) 0.4886(4) 0.0443(19) Uani 1 1 d .
O23 O 0.1592(8) -0.0211(5) -0.1470(4) 0.0454(19) Uani 1 1 d .
O24 O 0.2030(9) 0.0656(4) 0.5672(4) 0.047(2) Uani 1 1 d .
O25 O 0.2087(9) 0.1664(5) 0.0365(4) 0.0418(18) Uani 1 1 d .
O26 O 0.4983(9) 0.1874(5) 0.6239(5) 0.052(2) Uani 1 1 d .
O27 O 0.4594(9) 0.0075(4) -0.2163(4) 0.0425(18) Uani 1 1 d .
C1 C 0.3911(12) 0.4636(7) 0.7618(6) 0.040(3) Uani 1 1 d .
H1A H 0.4822 0.4506 0.7929 0.060 Uiso 1 1 calc R
H1B H 0.3962 0.5277 0.7750 0.060 Uiso 1 1 calc R
H1C H 0.4017 0.4312 0.7035 0.060 Uiso 1 1 calc R
C2 C -0.0999(12) 0.1826(7) 0.5508(7) 0.042(3) Uani 1 1 d .
H2A H -0.1225 0.2278 0.6036 0.063 Uiso 1 1 calc R
H2B H -0.0966 0.1245 0.5543 0.063 Uiso 1 1 calc R
H2C H -0.1882 0.1793 0.5097 0.063 Uiso 1 1 calc R
C3 C 0.4979(13) 0.3169(7) 0.5322(7) 0.052(3) Uani 1 1 d .
H3A H 0.5896 0.2999 0.5600 0.078 Uiso 1 1 calc R
H3B H 0.5128 0.3808 0.5448 0.078 Uiso 1 1 calc R
H3C H 0.4974 0.2831 0.4734 0.078 Uiso 1 1 calc R
C4 C -0.1986(13) 0.3293(7) 0.7896(7) 0.049(3) Uani 1 1 d .
H4A H -0.2024 0.3731 0.8455 0.073 Uiso 1 1 calc R
H4B H -0.2028 0.2692 0.7891 0.073 Uiso 1 1 calc R
H4C H -0.2942 0.3341 0.7558 0.073 Uiso 1 1 calc R
C5 C 0.2377(13) 0.0291(7) 0.1095(7) 0.048(3) Uani 1 1 d .
H5A H 0.1431 0.0552 0.0929 0.073 Uiso 1 1 calc R
H5B H 0.2169 0.0224 0.1600 0.073 Uiso 1 1 calc R
H5C H 0.2517 -0.0294 0.0667 0.073 Uiso 1 1 calc R
C6 C 0.5183(15) 0.1026(7) -0.1921(7) 0.052(3) Uani 1 1 d .
H6A H 0.4484 0.1288 -0.2219 0.078 Uiso 1 1 calc R
H6B H 0.6342 0.1065 -0.2048 0.078 Uiso 1 1 calc R
H6C H 0.5110 0.1352 -0.1336 0.078 Uiso 1 1 calc R
C7 C 0.1890(13) -0.1927(7) -0.1050(7) 0.049(3) Uani 1 1 d .
H7A H 0.0872 -0.1620 -0.1039 0.073 Uiso 1 1 calc R
H7B H 0.1868 -0.2203 -0.0656 0.073 Uiso 1 1 calc R
H7C H 0.1958 -0.2388 -0.1596 0.073 Uiso 1 1 calc R
C8 C 0.1091(14) 0.1804(7) 0.3490(6) 0.046(3) Uani 1 1 d .
H8A H 0.0855 0.1406 0.3764 0.069 Uiso 1 1 calc R
H8B H 0.1928 0.1558 0.3103 0.069 Uiso 1 1 calc R
H8C H 0.0067 0.1859 0.3199 0.069 Uiso 1 1 calc R
C9 C 0.1670(15) 0.6009(7) 0.6835(7) 0.057(3) Uani 1 1 d .
H9A H 0.2021 0.5469 0.6410 0.086 Uiso 1 1 calc R
H9B H 0.2647 0.6425 0.7100 0.086 Uiso 1 1 calc R
H9C H 0.0888 0.6291 0.6591 0.086 Uiso 1 1 calc R
C10 C 0.3694(14) 0.0275(7) 0.4170(6) 0.051(3) Uani 1 1 d .
H10A H 0.4865 0.0153 0.4212 0.076 Uiso 1 1 calc R
H10B H 0.3329 0.0137 0.3601 0.076 Uiso 1 1 calc R
H10C H 0.3011 -0.0096 0.4368 0.076 Uiso 1 1 calc R
C11 C 0.2141(14) 0.4692(7) 0.9585(6) 0.046(3) Uani 1 1 d .
H11A H 0.3341 0.4671 0.9687 0.069 Uiso 1 1 calc R
H11B H 0.1625 0.4905 1.0102 0.069 Uiso 1 1 calc R
H11C H 0.1949 0.5099 0.9315 0.069 Uiso 1 1 calc R
C12 C 0.2673(15) 0.4491(7) 0.4413(7) 0.054(3) Uani 1 1 d .
H12A H 0.2065 0.4050 0.3918 0.082 Uiso 1 1 calc R
H12B H 0.3871 0.4424 0.4381 0.082 Uiso 1 1 calc R
H12C H 0.2442 0.5092 0.4465 0.082 Uiso 1 1 calc R
C13 C 0.1253(16) 0.0422(7) 0.6291(7) 0.060(4) Uani 1 1 d .
H13A H 0.2064 0.0156 0.6537 0.090 Uiso 1 1 calc R
H13B H 0.0288 -0.0006 0.6036 0.090 Uiso 1 1 calc R
H13C H 0.0891 0.0961 0.6713 0.090 Uiso 1 1 calc R
C14 C 0.3791(15) -0.1716(7) -0.3249(6) 0.053(3) Uani 1 1 d .
H14A H 0.3400 -0.1229 -0.3381 0.080 Uiso 1 1 calc R
H14B H 0.3210 -0.2282 -0.3623 0.080 Uiso 1 1 calc R
H14C H 0.4993 -0.1743 -0.3300 0.080 Uiso 1 1 calc R
C15 C 0.0455(15) 0.1982(8) 0.8780(7) 0.055(3) Uani 1 1 d .
H15A H 0.1441 0.2156 0.9170 0.083 Uiso 1 1 calc R
H15B H 0.0092 0.1356 0.8643 0.083 Uiso 1 1 calc R
H15C H -0.0443 0.2358 0.9022 0.083 Uiso 1 1 calc R
C16 C 0.3748(15) 0.2896(7) 0.2239(7) 0.050(3) Uani 1 1 d .
H16A H 0.2559 0.2707 0.2104 0.076 Uiso 1 1 calc R
H16B H 0.3887 0.3538 0.2571 0.076 Uiso 1 1 calc R
H16C H 0.4246 0.2574 0.2543 0.076 Uiso 1 1 calc R
C17 C -0.0813(16) 0.6162(6) 0.8929(7) 0.056(4) Uani 1 1 d .
H17A H 0.0186 0.6532 0.8939 0.084 Uiso 1 1 calc R
H17B H -0.1032 0.6257 0.9487 0.084 Uiso 1 1 calc R
H17C H -0.1768 0.6328 0.8671 0.084 Uiso 1 1 calc R
C18 C 0.5626(17) 0.3252(7) 0.0242(8) 0.073(4) Uani 1 1 d .
H18A H 0.4906 0.3561 0.0672 0.110 Uiso 1 1 calc R
H18B H 0.5417 0.3427 -0.0214 0.110 Uiso 1 1 calc R
H18C H 0.6795 0.3412 0.0456 0.110 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O25 Re1 O21 107.7(3) .
O25 Re1 O1 95.1(3) .
O21 Re1 O1 88.4(3) .
O25 Re1 O20 95.6(3) .
O21 Re1 O20 86.7(3) .
O1 Re1 O20 169.2(3) .
O25 Re1 O7 92.0(3) .
O21 Re1 O7 160.0(3) .
O1 Re1 O7 93.2(2) .
O20 Re1 O7 88.2(3) .
O25 Re1 O12 162.4(3) 2_655
O21 Re1 O12 89.8(3) 2_655
O1 Re1 O12 84.0(2) 2_655
O20 Re1 O12 86.3(3) 2_655
O7 Re1 O12 70.6(2) 2_655
O23 Re2 O1 93.9(3) .
O23 Re2 O27 104.7(3) .
O1 Re2 O27 94.8(3) .
O23 Re2 O13 99.3(3) .
O1 Re2 O13 166.2(3) .
O27 Re2 O13 85.8(3) .
O23 Re2 O12 95.1(3) .
O1 Re2 O12 90.1(2) .
O27 Re2 O12 159.2(3) .
O13 Re2 O12 84.6(3) .
O23 Re2 O7 164.5(3) 2_655
O1 Re2 O7 82.1(2) 2_655
O27 Re2 O7 90.6(3) 2_655
O13 Re2 O7 84.2(3) 2_655
O12 Re2 O7 70.0(2) 2_655
O17 Re3 O9 94.7(3) .
O17 Re3 O15 107.5(3) .
O9 Re3 O15 89.0(3) .
O17 Re3 O10 97.3(3) .
O9 Re3 O10 168.0(3) .
O15 Re3 O10 86.1(3) .
O17 Re3 O4 92.7(3) .
O9 Re3 O4 93.1(2) .
O15 Re3 O4 159.5(3) .
O10 Re3 O4 87.7(2) .
O17 Re3 O5 162.9(3) .
O9 Re3 O5 83.3(2) .
O15 Re3 O5 89.5(3) .
O10 Re3 O5 85.7(3) .
O4 Re3 O5 70.5(2) .
O19 Re4 O18 105.2(3) .
O19 Re4 O3 94.9(3) .
O18 Re4 O3 93.4(3) .
O19 Re4 O8 97.6(3) .
O18 Re4 O8 85.7(3) .
O3 Re4 O8 167.2(3) .
O19 Re4 O5 95.0(3) .
O18 Re4 O5 158.2(3) .
O3 Re4 O5 93.0(2) .
O8 Re4 O5 83.5(3) .
O19 Re4 O4 164.6(3) .
O18 Re4 O4 90.2(3) .
O3 Re4 O4 82.0(3) .
O8 Re4 O4 85.2(3) .
O5 Re4 O4 70.1(2) .
O22 Re5 O3 95.0(3) .
O22 Re5 O16 107.1(3) .
O3 Re5 O16 88.6(3) .
O22 Re5 O11 97.1(3) .
O3 Re5 O11 167.7(3) .
O16 Re5 O11 85.8(3) .
O22 Re5 O6 92.8(3) .
O3 Re5 O6 93.3(2) .
O16 Re5 O6 159.8(3) .
O11 Re5 O6 88.3(3) .
O22 Re5 O2 162.8(3) .
O3 Re5 O2 83.6(3) .
O16 Re5 O2 90.0(3) .
O11 Re5 O2 85.5(3) .
O6 Re5 O2 70.3(2) .
O26 Re6 O24 105.7(3) .
O26 Re6 O9 95.1(3) .
O24 Re6 O9 93.6(3) .
O26 Re6 O14 98.6(3) .
O24 Re6 O14 86.1(3) .
O9 Re6 O14 165.9(3) .
O26 Re6 O2 95.1(3) .
O24 Re6 O2 158.2(3) .
O9 Re6 O2 91.1(2) .
O14 Re6 O2 84.1(3) .
O26 Re6 O6 164.6(3) .
O24 Re6 O6 89.6(3) .
O9 Re6 O6 81.9(2) .
O14 Re6 O6 84.0(3) .
O2 Re6 O6 70.0(2) .
Re2 O1 Re1 161.0(3) .
C3 O2 Re6 119.0(5) .
C3 O2 Re5 121.0(6) .
Re6 O2 Re5 110.8(3) .
Re5 O3 Re4 161.9(4) .
C1 O4 Re3 120.6(5) .
C1 O4 Re4 121.5(5) .
Re3 O4 Re4 108.7(3) .
C4 O5 Re4 119.1(5) .
C4 O5 Re3 121.6(6) .
Re4 O5 Re3 110.3(3) .
C2 O6 Re5 119.0(5) .
C2 O6 Re6 120.5(5) .
Re5 O6 Re6 108.6(3) .
C5 O7 Re1 119.6(6) .
C5 O7 Re2 120.5(5) 2_655
Re1 O7 Re2 108.5(3) 2_655
C17 O8 Re4 129.1(6) .
Re3 O9 Re6 157.5(4) .
C11 O10 Re3 124.4(6) .
C8 O11 Re5 128.4(6) .
C7 O12 Re2 119.1(6) .
C7 O12 Re1 120.5(5) 2_655
Re2 O12 Re1 110.5(3) 2_655
C14 O13 Re2 129.0(6) .
C10 O14 Re6 129.8(6) .
C15 O15 Re3 128.6(6) .
C12 O16 Re5 129.2(6) .
C9 O18 Re4 128.9(6) .
C16 O20 Re1 127.0(7) .
C18 O21 Re1 129.8(6) .
C13 O24 Re6 127.7(6) .
C6 O27 Re2 126.7(6) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Re1 O25 1.682(7) .
Re1 O21 1.886(6) .
Re1 O1 1.891(6) .
Re1 O20 1.936(7) .
Re1 O7 2.074(6) .
Re1 O12 2.140(6) 2_655
Re2 O23 1.675(7) .
Re2 O1 1.876(6) .
Re2 O27 1.892(6) .
Re2 O13 1.901(7) .
Re2 O12 2.062(6) .
Re2 O7 2.180(6) 2_655
Re3 O17 1.669(7) .
Re3 O9 1.881(6) .
Re3 O15 1.907(6) .
Re3 O10 1.923(6) .
Re3 O4 2.074(6) .
Re3 O5 2.148(6) .
Re4 O19 1.674(7) .
Re4 O18 1.894(6) .
Re4 O3 1.901(6) .
Re4 O8 1.911(6) .
Re4 O5 2.062(6) .
Re4 O4 2.179(6) .
Re5 O22 1.674(7) .
Re5 O3 1.886(6) .
Re5 O16 1.893(6) .
Re5 O11 1.917(6) .
Re5 O6 2.069(6) .
Re5 O2 2.155(6) .
Re6 O26 1.665(8) .
Re6 O24 1.883(7) .
Re6 O9 1.905(5) .
Re6 O14 1.919(6) .
Re6 O2 2.046(6) .
Re6 O6 2.189(7) .
O2 C3 1.456(11) .
O4 C1 1.445(10) .
O5 C4 1.450(10) .
O6 C2 1.474(10) .
O7 C5 1.437(11) .
O7 Re2 2.180(6) 2_655
O8 C17 1.425(10) .
O10 C11 1.423(12) .
O11 C8 1.403(11) .
O12 C7 1.457(11) .
O12 Re1 2.140(6) 2_655
O13 C14 1.400(11) .
O14 C10 1.425(11) .
O15 C15 1.420(11) .
O16 C12 1.431(10) .
O18 C9 1.440(11) .
O20 C16 1.407(11) .
O21 C18 1.440(11) .
O24 C13 1.444(11) .
O27 C6 1.457(11) .
