#------------------------------------------------------------------------------
#$Date: 2020-10-06 11:54:57 +0300 (Tue, 06 Oct 2020) $
#$Revision: 257545 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/52/7705257.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7705257
loop_
_publ_author_name
'Onn, Chee S.'
'Hill, Anthony F.'
'Olding, Angus'
_publ_section_title
;
 Metal coordination of phosphoniocarbynes.
;
_journal_issue                   36
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12731
_journal_page_last               12741
_journal_paper_doi               10.1039/d0dt02737e
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C36 H51 B N8 O2 P Pt W, F6 P'
_chemical_formula_sum            'C36 H51 B F6 N8 O2 P2 Pt W'
_chemical_formula_weight         1193.53
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_date             2020-07-26
_audit_creation_method
;
Olex2 1.3
(compiled 2020.07.16 svn.r6f6c53a7 for OlexSys, GUI svn.r6139)
;
_audit_update_record
;
2020-08-05 deposited with the CCDC.	2020-08-24 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 97.914(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.6038(3)
_cell_length_b                   14.0280(3)
_cell_length_c                   23.5934(5)
_cell_measurement_reflns_used    9037
_cell_measurement_temperature    150.00(10)
_cell_measurement_theta_max      28.9560
_cell_measurement_theta_min      3.8410
_cell_volume                     4787.36(18)
_computing_cell_refinement       'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)'
_computing_data_collection       'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)'
_computing_data_reduction        'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      150.00(10)
_diffrn_detector_area_resol_mean 8.1297
_diffrn_detector_type            EosS2
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.838
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -52.00  32.00   1.00   11.07    --   15.42 -57.00-150.00   84
  2  ω     39.00  71.00   1.00   11.07    --   15.42 178.00-180.00   32
  3  ω     -6.00  83.00   1.00   11.07    --   15.42  19.00   0.00   89
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at home/near, EosS2'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0270
_diffrn_reflns_av_unetI/netI     0.0460
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.838
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            21286
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.838
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.280
_diffrn_reflns_theta_min         3.293
_exptl_absorpt_coefficient_mu    5.448
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.68657
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.39.46e (Rigaku Oxford Diffraction, 2018)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'clear light yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.656
_exptl_crystal_description       plate
_exptl_crystal_F_000             2320
_exptl_crystal_size_max          0.363
_exptl_crystal_size_mid          0.159
_exptl_crystal_size_min          0.112
_refine_diff_density_max         1.120
_refine_diff_density_min         -0.696
_refine_diff_density_rms         0.126
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.020
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     532
_refine_ls_number_reflns         10954
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.020
_refine_ls_R_factor_all          0.0413
_refine_ls_R_factor_gt           0.0301
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0185P)²+5.7595P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0581
_refine_ls_wR_factor_ref         0.0621
_reflns_Friedel_coverage         0.000
_reflns_number_gt                9116
_reflns_number_total             10954
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d0dt02737e2.cif
_cod_data_source_block           Compound_7
_cod_depositor_comments
'Adding full bibliography for 7705254--7705258.cif.'
_cod_database_code               7705257
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C6(H6), C26(H26), C11(H11), C22(H22), C16(H16), C23(H23), C24(H24), C25(H25)
2.b Idealised Me refined as rotating group:
 C19(H19A,H19B,H19C), C9(H9A,H9B,H9C), C8(H8A,H8B,H8C), C4(H4A,H4B,H4C),
 C20(H20A,H20B,H20C), C14(H14A,H14B,H14C), C18(H18A,H18B,H18C), C34(H34A,H34B,
 H34C), C13(H13A,H13B,H13C), C29(H29A,H29B,H29C), C30(H30A,H30B,H30C), C31(H31A,
 H31B,H31C), C35(H35A,H35B,H35C), C36(H36A,H36B,H36C)
;
_smtbx_masks_special_details
;
A solvent mask was calculated and 124 electrons were 
found in a volume of 622 Ang³ in 1 void per unit cell. 
This is consistent with the presence of 1[CH3CH2OH] per 
Asymmetric Unit which account for 104 electrons per unit cell.
;
_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_reflns_friedel_fraction         is
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.66104(2) 0.27040(2) 0.47537(2) 0.01636(4) Uani 1 1 d . . . . .
Pt1 Pt 0.81884(2) 0.30768(2) 0.42697(2) 0.02063(5) Uani 1 1 d . . . . .
P1 P 0.63246(7) 0.26349(7) 0.32673(4) 0.0175(2) Uani 1 1 d . . . . .
P3 P 0.72935(8) 0.63639(9) 0.24950(5) 0.0324(3) Uani 1 1 d . . . . .
N1 N 0.5843(2) 0.2517(2) 0.55131(13) 0.0211(7) Uani 1 1 d . . . . .
N3 N 0.5747(2) 0.1435(2) 0.44925(13) 0.0202(7) Uani 1 1 d . . . . .
O2 O 0.7720(2) 0.4367(2) 0.54272(13) 0.0333(7) Uani 1 1 d . . . . .
N5 N 0.5355(2) 0.3577(2) 0.44993(13) 0.0182(7) Uani 1 1 d . . . . .
C1 C 0.6898(2) 0.2768(3) 0.39635(16) 0.0172(8) Uani 1 1 d . . . . .
O1 O 0.8243(2) 0.1544(2) 0.54440(14) 0.0415(8) Uani 1 1 d . . . . .
C3 C 0.7328(3) 0.3778(3) 0.51466(17) 0.0208(8) Uani 1 1 d . . . . .
C2 C 0.7658(3) 0.1949(3) 0.51603(18) 0.0258(9) Uani 1 1 d . . . . .
N4 N 0.4816(2) 0.1423(2) 0.45162(13) 0.0197(7) Uani 1 1 d . . . . .
N2 N 0.4895(2) 0.2379(2) 0.54151(14) 0.0182(7) Uani 1 1 d . . . . .
N6 N 0.4482(2) 0.3186(2) 0.44834(13) 0.0201(7) Uani 1 1 d . . . . .
N7 N 0.9870(2) 0.3457(3) 0.52153(15) 0.0308(8) Uani 1 1 d . . . . .
C27 C 0.9275(3) 0.3322(3) 0.48538(17) 0.0262(9) Uani 1 1 d . . . . .
N8 N 0.9243(2) 0.3303(3) 0.32239(15) 0.0306(9) Uani 1 1 d . . . . .
C32 C 0.8854(3) 0.3227(3) 0.36143(18) 0.0280(10) Uani 1 1 d . . . . .
F6 F 0.7594(2) 0.5773(2) 0.30637(13) 0.0715(11) Uani 1 1 d . . . . .
C5 C 0.6069(3) 0.2629(3) 0.60837(16) 0.0231(9) Uani 1 1 d . . . . .
F5 F 0.6986(2) 0.6959(2) 0.19315(13) 0.0671(10) Uani 1 1 d . . . . .
C6 C 0.5278(3) 0.2580(3) 0.63500(17) 0.0245(9) Uani 1 1 d . . . . .
H6 H 0.524532 0.263799 0.673937 0.029 Uiso 1 1 calc R U . . .
C21 C 0.6596(3) 0.1512(3) 0.29538(16) 0.0197(8) Uani 1 1 d . . . . .
C7 C 0.4550(3) 0.2429(3) 0.59193(17) 0.0234(9) Uani 1 1 d . . . . .
C19 C 0.5099(3) 0.2686(3) 0.32296(17) 0.0238(9) Uani 1 1 d . . . . .
H19A H 0.489288 0.218333 0.345739 0.036 Uiso 1 1 calc R U . . .
H19B H 0.482104 0.261164 0.283914 0.036 Uiso 1 1 calc R U . . .
H19C H 0.492355 0.329054 0.337191 0.036 Uiso 1 1 calc R U . . .
C9 C 0.6925(3) 0.0320(3) 0.41962(18) 0.0279(10) Uani 1 1 d . . . . .
H9A H 0.726382 0.087555 0.410882 0.042 Uiso 1 1 calc R U . . .
H9B H 0.691246 -0.013296 0.389036 0.042 Uiso 1 1 calc R U . . .
H9C H 0.722023 0.003973 0.454536 0.042 Uiso 1 1 calc R U . . .
C8 C 0.3548(3) 0.2332(3) 0.59657(18) 0.0289(10) Uani 1 1 d . . . . .
H8A H 0.322010 0.287395 0.579114 0.043 Uiso 1 1 calc R U . . .
H8B H 0.346462 0.229928 0.636178 0.043 Uiso 1 1 calc R U . . .
H8C H 0.331246 0.176128 0.577394 0.043 Uiso 1 1 calc R U . . .
C17 C 0.3847(3) 0.3809(3) 0.42389(16) 0.0217(9) Uani 1 1 d . . . . .
C4 C 0.7039(3) 0.2765(4) 0.63726(18) 0.0363(11) Uani 1 1 d . . . . .
H4A H 0.738709 0.219296 0.633695 0.054 Uiso 1 1 calc R U . . .
H4B H 0.703098 0.290419 0.677028 0.054 Uiso 1 1 calc R U . . .
H4C H 0.731985 0.328485 0.619581 0.054 Uiso 1 1 calc R U . . .
C12 C 0.4452(3) 0.0590(3) 0.42976(16) 0.0225(9) Uani 1 1 d . . . . .
C26 C 0.5909(3) 0.0863(3) 0.27590(19) 0.0321(10) Uani 1 1 d . . . . .
H26 H 0.529355 0.100974 0.277911 0.038 Uiso 1 1 calc R U . . .
C10 C 0.5959(3) 0.0599(3) 0.42646(16) 0.0241(9) Uani 1 1 d . . . . .
C20 C 0.6647(3) 0.3573(3) 0.28140(17) 0.0278(10) Uani 1 1 d . . . . .
H20A H 0.650228 0.417955 0.296831 0.042 Uiso 1 1 calc R U . . .
H20B H 0.631231 0.350201 0.243671 0.042 Uiso 1 1 calc R U . . .
H20C H 0.729875 0.353922 0.279513 0.042 Uiso 1 1 calc R U . . .
C11 C 0.5155(3) 0.0065(3) 0.41290(17) 0.0272(10) Uani 1 1 d . . . . .
H11 H 0.510615 -0.053237 0.395692 0.033 Uiso 1 1 calc R U . . .
C14 C 0.6026(3) 0.5107(3) 0.42139(19) 0.0286(10) Uani 1 1 d . . . . .
H14A H 0.623031 0.539919 0.457725 0.043 Uiso 1 1 calc R U . . .
H14B H 0.583043 0.559185 0.393631 0.043 Uiso 1 1 calc R U . . .
H14C H 0.652524 0.474990 0.409271 0.043 Uiso 1 1 calc R U . . .
C18 C 0.2833(3) 0.3574(3) 0.41340(19) 0.0323(10) Uani 1 1 d . . . . .
H18A H 0.273658 0.302681 0.388855 0.048 Uiso 1 1 calc R U . . .
H18B H 0.249679 0.410691 0.395451 0.048 Uiso 1 1 calc R U . . .
H18C H 0.261718 0.343794 0.449187 0.048 Uiso 1 1 calc R U . . .
C22 C 0.7514(3) 0.1267(3) 0.29221(18) 0.0293(10) Uani 1 1 d . . . . .
H22 H 0.798419 0.169081 0.305699 0.035 Uiso 1 1 calc R U . . .
C28 C 1.0571(3) 0.3587(3) 0.57191(17) 0.0295(10) Uani 1 1 d . . . . .
C16 C 0.4305(3) 0.4617(3) 0.41010(18) 0.0268(9) Uani 1 1 d . . . . .
H16 H 0.403818 0.516473 0.392837 0.032 Uiso 1 1 calc R U . . .
C15 C 0.5238(3) 0.4456(3) 0.42687(16) 0.0223(9) Uani 1 1 d . . . . .
C33 C 0.9781(3) 0.3320(4) 0.2747(2) 0.0385(12) Uani 1 1 d . . . . .
C34 C 1.0783(3) 0.3490(4) 0.3001(2) 0.0522(15) Uani 1 1 d . . . . .
H34A H 1.082831 0.407304 0.321558 0.078 Uiso 1 1 calc R U . . .
H34B H 1.115788 0.353462 0.269760 0.078 Uiso 1 1 calc R U . . .
H34C H 1.099597 0.296940 0.324834 0.078 Uiso 1 1 calc R U . . .
B1 B 0.4372(3) 0.2253(3) 0.48067(19) 0.0219(10) Uani 1 1 d . . . . .
C13 C 0.3452(3) 0.0353(3) 0.42529(19) 0.0338(11) Uani 1 1 d . . . . .
H13A H 0.324238 0.045899 0.461583 0.051 Uiso 1 1 calc R U . . .
H13B H 0.336073 -0.030406 0.414591 0.051 Uiso 1 1 calc R U . . .
H13C H 0.310869 0.075062 0.396826 0.051 Uiso 1 1 calc R U . . .
C23 C 0.7733(3) 0.0407(3) 0.2694(2) 0.0387(12) Uani 1 1 d . . . . .
H23 H 0.834690 0.025784 0.266840 0.046 Uiso 1 1 calc R U . . .
C24 C 0.7044(4) -0.0230(3) 0.2503(2) 0.0452(13) Uani 1 1 d . . . . .
H24 H 0.719350 -0.081468 0.235411 0.054 Uiso 1 1 calc R U . . .
C25 C 0.6140(4) -0.0009(3) 0.2533(2) 0.0463(14) Uani 1 1 d . . . . .
H25 H 0.567700 -0.044186 0.240125 0.056 Uiso 1 1 calc R U . . .
C29 C 1.0149(3) 0.4233(4) 0.6131(2) 0.0480(14) Uani 1 1 d . . . . .
H29A H 1.000933 0.484172 0.595451 0.072 Uiso 1 1 calc R U . . .
H29B H 1.058024 0.431564 0.647343 0.072 Uiso 1 1 calc R U . . .
H29C H 0.959157 0.394920 0.622598 0.072 Uiso 1 1 calc R U . . .
C30 C 1.1401(3) 0.4044(4) 0.5520(2) 0.0429(13) Uani 1 1 d . . . . .
H30A H 1.163516 0.363618 0.524593 0.064 Uiso 1 1 calc R U . . .
H30B H 1.187158 0.414095 0.584090 0.064 Uiso 1 1 calc R U . . .
H30C H 1.122705 0.464686 0.534452 0.064 Uiso 1 1 calc R U . . .
C31 C 1.0788(4) 0.2610(4) 0.5971(2) 0.0541(15) Uani 1 1 d . . . . .
H31A H 1.023114 0.232298 0.606469 0.081 Uiso 1 1 calc R U . . .
H31B H 1.122807 0.266719 0.631106 0.081 Uiso 1 1 calc R U . . .
H31C H 1.104201 0.221913 0.569727 0.081 Uiso 1 1 calc R U . . .
C35 C 0.9415(5) 0.4123(5) 0.2353(3) 0.076(2) Uani 1 1 d . . . . .
H35A H 0.878254 0.399790 0.220157 0.114 Uiso 1 1 calc R U . . .
H35B H 0.977762 0.416968 0.204372 0.114 Uiso 1 1 calc R U . . .
H35C H 0.945377 0.471155 0.256227 0.114 Uiso 1 1 calc R U . . .
C36 C 0.9670(4) 0.2351(4) 0.2454(3) 0.0657(18) Uani 1 1 d . . . . .
H36A H 0.983897 0.185768 0.273129 0.099 Uiso 1 1 calc R U . . .
H36B H 1.006256 0.231757 0.216048 0.099 Uiso 1 1 calc R U . . .
H36C H 0.903776 0.226615 0.228720 0.099 Uiso 1 1 calc R U . . .
F1 F 0.7662(3) 0.7295(2) 0.28162(16) 0.0932(14) Uani 1 1 d . . . . .
F2 F 0.6337(2) 0.6506(4) 0.27060(17) 0.134(2) Uani 1 1 d . . . . .
F3 F 0.8267(3) 0.6250(3) 0.2304(2) 0.1194(18) Uani 1 1 d . . . . .
F4 F 0.6957(5) 0.5436(3) 0.21833(16) 0.164(3) Uani 1 1 d . . . . .
H1 H 0.364(3) 0.209(3) 0.4819(16) 0.021(11) Uiso 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_diffrn_refln_index_h
_diffrn_refln_index_k
_diffrn_refln_index_l
_diffrn_refln_intensity_net
_diffrn_refln_intensity_u
0 0 -4 4818.86 88.66
0 0 -5 12.06 3.49
0 0 5 3.32 2.4
0 0 -6 8338 150.53
0 0 6 8174.88 150.44
0 0 -7 59.57 6.72
0 0 7 51.77 5.98
0 0 -8 2409.21 53.77
0 0 8 2322.85 53.59
0 0 -9 5.66 3.37
0 0 9 6.69 3.14
0 0 -10 102.7 8.88
0 0 10 95.1 8.72
0 0 -11 6.72 4.29
0 0 11 7.61 3.97
0 0 -12 509.88 22.34
0 0 12 481.38 22.05
0 0 13 13.73 5.45
0 0 -13 21.01 6.49
0 0 -14 138 12.73
0 0 -15 17.57 6.45
0 0 -16 77.28 10.38
0 0 -17 18.31 7.67
0 0 17 20.55 5.63
0 0 18 1934.25 51.52
0 0 -18 2055.46 60.99
0 0 19 30.15 6.86
0 0 -19 53.04 11.32
0 0 20 3432.21 80.02
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-17 -8 7 96.81 16.18
-17 -8 6 9.94 10.21
-17 -8 5 201.94 22.67
-17 -8 4 175.71 21.68
-17 -8 3 294.53 26.53
-17 -8 2 195.66 22.39
-17 -8 1 130.45 17.89
-17 -8 0 221.72 23.35
-17 -9 8 8.74 9.59
-17 -9 7 70.75 13.8
-17 -9 6 12.89 8.72
-17 -9 5 102.27 16.74
-17 -9 4 53.66 13.53
-17 -9 3 32.04 12.2
-17 -9 2 4.91 9.17
-17 -9 1 2.46 9.31
-17 -10 6 -0.6 11.39
-17 -10 5 19.81 11.53
-17 -10 3 65.08 15.89
-18 0 8 43.05 12.73
-18 0 7 4.35 8.27
-18 0 6 473.89 36.08
-18 0 5 3.38 9.92
-18 0 4 1369.18 62.93
-18 0 3 8.02 11.27
-18 0 2 948.87 51.28
-18 0 1 -5.18 11.67
-18 0 0 140.46 20.07
-18 0 -4 99.05 17.08
-18 1 8 529.98 38.63
-18 -1 8 492.31 37.3
-18 1 7 -0.51 9.54
-18 -1 7 2.68 10.28
-18 1 6 405.84 33.66
-18 -1 6 415.59 33.73
-18 1 5 23.68 10.38
-18 -1 5 11.16 10.1
-18 1 4 -16.78 11.24
-18 -1 4 6.23 10.76
-18 1 3 125.55 19.27
-18 -1 3 102.6 17.12
-18 1 2 422.17 34.69
-18 -1 2 334.53 30.65
-18 1 1 -1.54 11.53
-18 -1 1 0.2 9.78
-18 -1 0 898.07 48.81
-18 -1 -1 -8.61 8.49
-18 1 -4 258.4 26.83
-18 1 -5 24.94 11.08
-18 1 -6 18.61 10.94
-18 1 -7 0.1 8.7
-18 -2 8 40.47 12.45
-18 2 7 204.6 24.28
-18 -2 7 183.86 22.81
-18 2 6 419.97 34.4
-18 -2 6 366 32.23
-18 2 5 65.44 16.46
-18 -2 5 60.51 15.91
-18 2 4 1016.19 54.74
-18 -2 4 995.83 52.26
-18 2 3 23.39 12.7
-18 -2 3 21.19 11.5
-18 -2 2 678.98 42.18
-18 -2 1 250.61 25.79
-18 -2 0 71.06 15.39
-18 -2 -1 117.57 18.26
-18 -2 -2 -6.22 10.55
-18 2 -4 63.25 14.55
-18 2 -5 22.07 12.45
-18 2 -6 17.26 8.67
-18 2 -7 28.83 12.43
-18 2 -8 20.93 11.12
-18 2 -9 5.59 11.46
-18 -3 8 178.02 22.84
-18 -3 7 18.84 9.69
-18 -3 6 88.61 16.53
-18 -3 5 266.27 26.66
-18 3 4 16.53 12.81
-18 -3 4 13.84 11.52
-18 -3 3 514.64 36.8
-18 -3 2 164.28 21.91
-18 -3 1 96.51 17.59
-18 -3 0 206.3 23.27
-18 -3 -1 3.34 9.14
-18 -3 -2 313.84 28.17
-18 -3 -3 131.09 18.8
-18 3 -4 164.06 22.05
-18 3 -5 124.09 20.14
-18 3 -6 60.84 15.05
-18 3 -7 0.72 9.88
-18 3 -8 50.16 15.52
-18 -4 7 406.04 33.85
-18 -4 6 174.8 22.56
-18 -4 5 146.86 20.34
-18 -4 4 392.49 32.45
-18 -4 3 18.98 11
-18 -4 2 165.45 21.01
-18 -4 1 399.19 32.16
-18 -4 0 58.01 13.34
-18 -4 -1 360.42 29.78
-18 -4 -2 91.11 17.07
-18 -4 -3 97.88 16.66
-18 4 -4 37.99 14.41
-18 -4 -4 -1.12 9.62
-18 -5 6 -0.48 9.43
-18 -5 5 503.75 36.57
-18 -5 4 10.19 11.24
-18 -5 3 674.16 42.48
-18 -5 2 23.69 12.16
-18 -5 1 227.4 24.46
-18 -5 0 3.73 9.56
-18 -5 -1 3.61 9.09
-18 -5 -2 92.05 16.9
-18 -5 -3 114.18 17.96
-18 -6 5 100.78 18.19
-18 -6 4 32.96 11.98
-18 -6 3 41.64 12.52
-18 -6 2 0.17 10.3
-18 -6 1 235.31 25.04
-18 -6 0 39.94 12.27
-18 -6 -1 317.73 28.25
-18 -6 -2 264.53 25.65
-18 -7 3 308.68 28.67
-18 -7 2 25.53 10.81
-18 -7 1 108.49 17.74
-18 -7 0 81.57 15.95
-18 -8 2 34.87 11.6
-18 -8 1 17.66 11.49
-19 1 -4 346.97 31.94
-19 2 -4 261.21 28.7
-19 2 -5 117.71 21.57
Q1 1 0.6902 0.7185 0.2688
11.00000 0.05 1.12 Q2 1
0.9750 0.3427 0.3755 11.00000 0.05
1.07 Q3 1 0.6613 0.3392
0.4750 11.00000 0.05 0.97 Q4
1 0.7845 0.5583 0.2340 11.00000
0.05 0.96 Q5 1 0.8118
0.2382 0.4256 11.00000 0.05 0.87
Q6 1 0.6301 0.5810 0.2373
11.00000 0.05 0.87 Q7 1
0.6236 0.2215 0.4770 11.00000 0.05
0.85 Q8 1 0.7086 0.2201
0.4871 11.00000 0.05 0.85 Q9
1 0.8167 0.6849 0.2657 11.00000
0.05 0.80 Q10 1 0.7824
0.3626 0.4331 11.00000 0.05 0.77
Q11 1 0.8592 0.3614 0.4391
11.00000 0.05 0.74 Q12 1
0.7189 0.2660 0.4503 11.00000 0.05
0.70 Q13 1 0.8821 0.3049
0.4070 11.00000 0.05 0.70 Q14
1 0.7572 0.3159 0.4438 11.00000
0.05 0.66 Q15 1 0.6981
0.2932 0.5055 11.00000 0.05 0.65
Q16 1 0.8600 0.2583 0.4221
11.00000 0.05 0.64 Q17 1
0.8657 0.2671 0.4477 11.00000 0.05
0.61 Q18 1 0.5137 0.2393
0.5209 11.00000 0.05 0.61 Q19
1 0.7095 0.3169 0.4856 11.00000
0.05 0.60 Q20 1 0.8553
0.1539 0.6242 11.00000 0.05 0.58
Q21 1 0.7456 0.6721 0.1905
11.00000 0.05 0.56 Q22 1
0.7866 0.2971 0.2796 11.00000 0.05
0.55 Q23 1 0.7390 0.2776
0.4111 11.00000 0.05 0.55 Q24
1 0.6171 0.2981 0.4520 11.00000
0.05 0.54 Q25 1 0.7791
0.2793 0.3945 11.00000 0.05 0.54
Q26 1 0.5960 0.2688 0.4977
11.00000 0.05 0.52 Q27 1
0.7095 0.5195 0.2091 11.00000 0.05
0.50 Q28 1 0.8232 0.6361
0.2099 11.00000 0.05 0.49 Q29
1 0.7427 0.2725 0.6207 11.00000
0.05 0.49 Q30 1 0.7705
0.7483 0.2914 11.00000 0.05 0.49
Q31 1 0.6952 0.5872 0.3098
11.00000 0.05 0.48 Q32 1
0.4377 0.4993 0.3900 11.00000 0.05
0.48 Q33 1 0.9759 0.2659
0.3782 11.00000 0.05 0.48 Q34
1 1.0247 0.5828 0.6207 11.00000
0.05 0.48 Q35 1 0.6219
-0.1209 0.2327 11.00000 0.05 0.47
Q36 1 0.5000 0.5000 0.5000
10.50000 0.05 0.47 Q37 1
0.6394 0.2009 0.2948 11.00000 0.05
0.47 Q38 1 0.8010 0.3202
0.1945 11.00000 0.05 0.47 Q39
1 0.6762 0.2766 0.4321 11.00000
0.05 0.47 Q40 1 0.6789
0.3210 0.4489 11.00000 0.05 0.46
Q41 1 0.7556 0.2588 0.6143
11.00000 0.05 0.46 Q42 1
0.6092 0.1402 0.4774 11.00000 0.05
0.46 Q43 1 0.7145 0.4427
0.5200 11.00000 0.05 0.46 Q44
1 0.5485 0.2191 0.7308 11.00000
0.05 0.46 Q45 1 0.7077
0.1160 0.6695 11.00000 0.05 0.45
Q46 1 0.5008 0.2792 0.7264
11.00000 0.05 0.45 Q47 1
0.6554 0.3182 0.4008 11.00000 0.05
0.44 Q48 1 0.6987 0.5596
0.4918 11.00000 0.05 0.44 Q49
1 0.4691 0.2856 0.5427 11.00000
0.05 0.43 Q50 1 1.0525
0.3077 0.5814 11.00000 0.05 0.43
REM The information below was
added by Olex2. REM REM
R1 = 0.0301 for 9116
Fo > 4sig(Fo) and 0.0413
for all 21825 data REM
532 parameters refined using n/a
restraints REM Highest difference peak
1.12, deepest hole -0.70 REM
Mean Shift 0, Max Shift
0.001. REM +++ Tabular Listing
of Refinement Information +++ REM
R1_all = 0.0413 REM R1_gt
= 0.0301 REM wR_ref =
0.0621 REM GOOF = 1.020
REM Shift_max = 0.001 REM
Shift_mean = 0 REM Reflections_all
= 21825 REM Reflections_gt =
9116 REM Parameters = 532
REM Hole = -0.70 REM
Peak = 1.12 REM Flack
= n/a
;
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction
(ABSPACK) includes: - Absorption correction
using spherical harmonics - Frame
scaling
;

data_Compound_8
_audit_creation_date             2020-07-25
_audit_creation_method           
;
Olex2 1.3 (compiled
2020.07.16 svn.r6f6c53a7 for OlexSys, GUI
svn.r6139)
;
_shelx_SHELXL_version_number     2018/3
_audit_contact_author_address    ?
_audit_contact_author_email      ?
_audit_contact_author_phone      ?
_publ_contact_author_id_orcid    ?
_publ_section_references         
;
Dolomanov, O.V., Bourhis,
L.J., Gildea, R.J, Howard, J.A.K.
& Puschmann, H. (2009), J.
Appl. Cryst. 42, 339-341. Sheldrick,
G.M. (2015). Acta Cryst. C71,
3-8.
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C46 H55 B N8 O2 P Pt W, F6 P, C H Cl3'
_chemical_formula_sum            'C47 H56 B Cl3 F6 N8 O2 P2 Pt W'
_chemical_formula_weight         1437.03
_chemical_melting_point          ?
_chemical_oxdiff_formula         'C46 H54 B1 F6 N8 O2 P2 Pt1 W1'
_chemical_oxdiff_usercomment     'DCM hexane'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed
for this shelxl refinement is
uniquely defined by the following
loop, which should always be
used as a source of
symmetry information in preference to
the above space-group names. They
are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   16.5808(4)
_cell_length_b                   14.4490(4)
_cell_length_c                   22.7627(6)
_cell_angle_alpha                90
_cell_angle_beta                 93.001(2)
_cell_angle_gamma                90
_cell_volume                     5445.9(2)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9479
_cell_measurement_temperature    150.00(10)
_cell_measurement_theta_max      28.9890
_cell_measurement_theta_min      3.8260
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    4.948
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.36691
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.39.46e (Rigaku Oxford
Diffraction, 2018) Empirical absorption correction
using spherical harmonics, implemented in
SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear light yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.753
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       plate
_exptl_crystal_F_000             2808
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
7 0 -31 0.0362
-6 1 31 0.0393
-2 -20 0 0.3415
2 20 -1 0.3399
-7 -2 31 0.0407
-10 1 30 0.0397
-19 1 19 0.0417
20 0 -17 0.0404
-14 0 -25 0.0368
14 0 24 0.0383

_exptl_crystal_size_max          0.692
_exptl_crystal_size_mid          0.092
_exptl_crystal_size_min          0.075
loop_
_exptl_oxdiff_crystal_face_indexfrac_h
_exptl_oxdiff_crystal_face_indexfrac_k
_exptl_oxdiff_crystal_face_indexfrac_l
_exptl_oxdiff_crystal_face_x
_exptl_oxdiff_crystal_face_y
_exptl_oxdiff_crystal_face_z
6.9925 -0.0111 -30.9974 -0.0754 -0.2438 -0.9637
-5.9938 1.0095 30.9960 0.0263 0.2013 0.9674
-1.9977 -19.9661 0.0079 0.2318 0.9282 -0.2316
1.9977 19.9657 -1.0076 -0.2248 -0.9370 0.2025
-6.9925 -1.9855 30.9979 0.0903 0.3375 0.9388
-9.9887 1.0086 30.0008 0.1998 0.1754 0.9736
-18.9769 1.0033 19.0145 0.6512 0.0401 0.7329
19.9756 -0.0041 -17.0166 -0.7142 -0.0651 -0.6711
-13.9814 -0.0113 -24.9760 0.7570 -0.2801 -0.6039
13.9814 0.0109 23.9763 -0.7501 0.2713 0.5748

_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0478
_diffrn_reflns_av_unetI/netI     0.0884
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.834
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            24477
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.834
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.266
_diffrn_reflns_theta_min         3.328
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      150.00(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 8.1297
_diffrn_detector_type            EosS2
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.834
_diffrn_measurement_details      
;
List of Runs (angles in
degrees, time in seconds): 1
\w -11.00 33.00 1.00 47.12
-- 15.57 77.00 60.00 44
2 \w 11.00 72.00 1.00
47.12 -- 15.57 57.00 120.00
61 3 \w -50.00 32.00
1.00 47.12 -- 15.57 -57.00
-60.00 82 4 \w -61.00
-35.00 1.00 47.12 -- -16.59
-38.00 120.00 26
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at home/near, EosS2'
_diffrn_measurement_method       '\w scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0416897000
_diffrn_orient_matrix_UB_12      -0.0074396000
_diffrn_orient_matrix_UB_13      -0.0069693000
_diffrn_orient_matrix_UB_21      0.0042684000
_diffrn_orient_matrix_UB_22      -0.0469100000
_diffrn_orient_matrix_UB_23      0.0088460000
_diffrn_orient_matrix_UB_31      -0.0088027000
_diffrn_orient_matrix_UB_32      0.0124910000
_diffrn_orient_matrix_UB_33      0.0291005000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'micro-focus sealed X-ray tube'
_diffrn_source_type              'SuperNova (Mo) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                9139
_reflns_number_total             12383
_reflns_odcompleteness_completeness 99.31
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     26.32
_reflns_special_details          
;
Reflections
were merged by SHELXL according
to the crystal class for
the calculation of statistics and
refinement.
;
;
;
;
;
;
;
;
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
1 8 30 0.0756
-1 -9 -29 0.0644
-6 -17 16 0.1436
6 17 -16 0.1638
1 9 29 0.0662
-17 -10 15 0.1123
16 9 -17 0.1181
-20 -2 -1 0.0478
21 1 -2 0.0578
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 W1 Pt1 152.31(8) . . ?
N3 W1 Pt1 120.80(8) . . ?
N3 W1 N1 78.58(12) . . ?
N5 W1 Pt1 119.32(8) . . ?
N5 W1 N1 78.26(12) . . ?
N5 W1 N3 87.19(11) . . ?
C1 W1 Pt1 45.57(10) . . ?
C1 W1 N1 162.12(13) . . ?
C1 W1 N3 87.75(13) . . ?
C1 W1 N5 89.73(13) . . ?
C1 W1 C3 103.85(15) . . ?
C1 W1 C2 103.27(16) . . ?
C3 W1 Pt1 68.47(11) . . ?
C3 W1 N1 90.31(14) . . ?
C3 W1 N3 168.34(14) . . ?
C3 W1 N5 94.05(13) . . ?
C3 W1 C2 81.85(17) . . ?
C2 W1 Pt1 70.78(12) . . ?
C2 W1 N1 89.33(14) . . ?
C2 W1 N3 94.37(15) . . ?
C2 W1 N5 166.95(14) . . ?
C1 Pt1 W1 45.52(11) . . ?
C1 Pt1 C27 157.80(16) . . ?
C27 Pt1 W1 112.29(12) . . ?
C32 Pt1 W1 152.33(12) . . ?
C32 Pt1 C1 106.82(16) . . ?
C32 Pt1 C27 95.37(17) . . ?
C1 P1 C21 111.92(18) . . ?
C1 P1 C19 113.02(18) . . ?
C1 P1 C20 110.47(19) . . ?
C19 P1 C21 106.88(19) . . ?
C19 P1 C20 106.5(2) . . ?
C20 P1 C21 107.72(19) . . ?
F5 P3 F6 179.4(2) . . ?
F1 P3 F6 89.43(19) . . ?
F1 P3 F5 90.3(2) . . ?
F2 P3 F6 87.3(2) . . ?
F2 P3 F5 92.2(2) . . ?
F2 P3 F1 90.1(3) . . ?
F3 P3 F6 92.0(2) . . ?
F3 P3 F5 88.6(2) . . ?
F3 P3 F1 87.6(3) . . ?
F3 P3 F2 177.6(3) . . ?
F4 P3 F6 89.7(2) . . ?
F4 P3 F5 90.6(2) . . ?
F4 P3 F1 178.4(3) . . ?
F4 P3 F2 91.1(3) . . ?
F4 P3 F3 91.1(3) . . ?
N2 N1 W1 118.6(2) . . ?
C5 N1 W1 134.3(3) . . ?
C5 N1 N2 106.5(3) . . ?
N4 N3 W1 121.9(2) . . ?
C10 N3 W1 131.2(3) . . ?
C10 N3 N4 106.9(3) . . ?
N6 N5 W1 120.8(2) . . ?
C15 N5 W1 131.9(3) . . ?
C15 N5 N6 106.7(3) . . ?
W1 C1 Pt1 88.91(15) . . ?
P1 C1 W1 138.4(2) . . ?
P1 C1 Pt1 132.7(2) . . ?
O2 C3 W1 173.0(3) . . ?
O1 C2 W1 173.5(4) . . ?
N3 N4 B1 119.4(3) . . ?
C12 N4 N3 109.6(3) . . ?
C12 N4 B1 130.8(3) . . ?
N1 N2 B1 121.8(3) . . ?
C7 N2 N1 109.3(3) . . ?
C7 N2 B1 128.8(3) . . ?
N5 N6 B1 119.0(3) . . ?
C17 N6 N5 109.4(3) . . ?
C17 N6 B1 130.9(3) . . ?
C27 N7 C28 174.1(4) . . ?
N7 C27 Pt1 176.0(4) . . ?
C32 N8 C33 174.7(5) . . ?
N8 C32 Pt1 179.1(4) . . ?
N1 C5 C6 109.9(4) . . ?
N1 C5 C4 123.7(4) . . ?
C6 C5 C4 126.4(4) . . ?
C5 C6 H6 126.9 . . ?
C7 C6 C5 106.2(3) . . ?
C7 C6 H6 126.9 . . ?
C26 C21 P1 121.2(3) . . ?
C26 C21 C22 118.6(4) . . ?
C22 C21 P1 120.2(3) . . ?
N2 C7 C6 108.1(4) . . ?
N2 C7 C8 123.2(4) . . ?
C6 C7 C8 128.6(4) . . ?
P1 C19 H19A 109.5 . . ?
P1 C19 H19B 109.5 . . ?
P1 C19 H19C 109.5 . . ?
H19A C19 H19B 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
H9A C9 H9B 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C10 C9 H9A 109.5 . . ?
C10 C9 H9B 109.5 . . ?
C10 C9 H9C 109.5 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8B 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
N6 C17 C18 122.2(4) . . ?
N6 C17 C16 107.9(4) . . ?
C16 C17 C18 129.8(4) . . ?
C5 C4 H4A 109.5 . . ?
C5 C4 H4B 109.5 . . ?
C5 C4 H4C 109.5 . . ?
H4A C4 H4B 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
N4 C12 C11 107.7(4) . . ?
N4 C12 C13 123.3(4) . . ?
C11 C12 C13 129.0(4) . . ?
C21 C26 H26 120.0 . . ?
C21 C26 C25 120.1(4) . . ?
C25 C26 H26 120.0 . . ?
N3 C10 C9 122.9(4) . . ?
N3 C10 C11 109.2(4) . . ?
C11 C10 C9 127.9(4) . . ?
P1 C20 H20A 109.5 . . ?
P1 C20 H20B 109.5 . . ?
P1 C20 H20C 109.5 . . ?
H20A C20 H20B 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C12 C11 C10 106.7(4) . . ?
C12 C11 H11 126.6 . . ?
C10 C11 H11 126.6 . . ?
H14A C14 H14B 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C15 C14 H14A 109.5 . . ?
C15 C14 H14B 109.5 . . ?
C15 C14 H14C 109.5 . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18B 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C21 C22 H22 119.6 . . ?
C23 C22 C21 120.9(4) . . ?
C23 C22 H22 119.6 . . ?
N7 C28 C29 107.0(4) . . ?
N7 C28 C30 107.6(3) . . ?
N7 C28 C31 106.9(4) . . ?
C30 C28 C29 111.2(4) . . ?
C30 C28 C31 112.1(4) . . ?
C31 C28 C29 111.8(4) . . ?
C17 C16 H16 126.6 . . ?
C17 C16 C15 106.8(4) . . ?
C15 C16 H16 126.6 . . ?
N5 C15 C14 122.7(4) . . ?
N5 C15 C16 109.2(4) . . ?
C16 C15 C14 128.1(4) . . ?
N8 C33 C34 106.9(4) . . ?
N8 C33 C35 107.7(4) . . ?
N8 C33 C36 107.4(4) . . ?
C34 C33 C36 110.8(4) . . ?
C35 C33 C34 111.4(5) . . ?
C35 C33 C36 112.3(5) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34B 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
N4 B1 N2 108.4(3) . . ?
N4 B1 H1 109(2) . . ?
N2 B1 H1 111(2) . . ?
N6 B1 N4 110.1(3) . . ?
N6 B1 N2 107.0(3) . . ?
N6 B1 H1 111(2) . . ?
C12 C13 H13A 109.5 . . ?
C12 C13 H13B 109.5 . . ?
C12 C13 H13C 109.5 . . ?
H13A C13 H13B 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
C22 C23 H23 120.0 . . ?
C24 C23 C22 119.9(5) . . ?
C24 C23 H23 120.0 . . ?
C23 C24 H24 119.9 . . ?
C25 C24 C23 120.3(4) . . ?
C25 C24 H24 119.9 . . ?
C26 C25 H25 119.8 . . ?
C24 C25 C26 120.3(4) . . ?
C24 C25 H25 119.8 . . ?
C28 C29 H29A 109.5 . . ?
C28 C29 H29B 109.5 . . ?
C28 C29 H29C 109.5 . . ?
H29A C29 H29B 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C28 C30 H30A 109.5 . . ?
C28 C30 H30B 109.5 . . ?
C28 C30 H30C 109.5 . . ?
H30A C30 H30B 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C28 C31 H31A 109.5 . . ?
C28 C31 H31B 109.5 . . ?
C28 C31 H31C 109.5 . . ?
H31A C31 H31B 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35B 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36B 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
W1 Pt1 2.7592(2) . ?
W1 N1 2.256(3) . ?
W1 N3 2.219(3) . ?
W1 N5 2.218(3) . ?
W1 C1 1.969(4) . ?
W1 C3 1.990(4) . ?
W1 C2 1.995(4) . ?
Pt1 C1 1.971(4) . ?
Pt1 C27 1.984(4) . ?
Pt1 C32 1.948(4) . ?
P1 C1 1.748(4) . ?
P1 C21 1.808(4) . ?
P1 C19 1.781(4) . ?
P1 C20 1.799(4) . ?
P3 F6 1.587(3) . ?
P3 F5 1.582(3) . ?
P3 F1 1.568(4) . ?
P3 F2 1.560(4) . ?
P3 F3 1.557(4) . ?
P3 F4 1.542(4) . ?
N1 N2 1.385(4) . ?
N1 C5 1.350(5) . ?
N3 N4 1.369(4) . ?
N3 C10 1.344(5) . ?
O2 C3 1.159(5) . ?
N5 N6 1.383(4) . ?
N5 C15 1.348(5) . ?
O1 C2 1.159(5) . ?
N4 C12 1.356(5) . ?
N4 B1 1.539(6) . ?
N2 C7 1.356(5) . ?
N2 B1 1.541(5) . ?
N6 C17 1.345(5) . ?
N6 B1 1.535(6) . ?
N7 C27 1.146(5) . ?
N7 C28 1.469(5) . ?
N8 C32 1.152(5) . ?
N8 C33 1.458(5) . ?
C5 C6 1.391(6) . ?
C5 C4 1.497(6) . ?
C6 H6 0.9300 . ?
C6 C7 1.382(6) . ?
C21 C26 1.385(6) . ?
C21 C22 1.396(5) . ?
C7 C8 1.489(6) . ?
C19 H19A 0.9600 . ?
C19 H19B 0.9600 . ?
C19 H19C 0.9600 . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C9 C10 1.494(6) . ?
C8 H8A 0.9600 . ?
C8 H8B 0.9600 . ?
C8 H8C 0.9600 . ?
C17 C18 1.505(6) . ?
C17 C16 1.376(6) . ?
C4 H4A 0.9600 . ?
C4 H4B 0.9600 . ?
C4 H4C 0.9600 . ?
C12 C11 1.366(6) . ?
C12 C13 1.487(6) . ?
C26 H26 0.9300 . ?
C26 C25 1.395(6) . ?
C10 C11 1.391(6) . ?
C20 H20A 0.9600 . ?
C20 H20B 0.9600 . ?
C20 H20C 0.9600 . ?
C11 H11 0.9300 . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C14 C15 1.489(5) . ?
C18 H18A 0.9600 . ?
C18 H18B 0.9600 . ?
C18 H18C 0.9600 . ?
C22 H22 0.9300 . ?
C22 C23 1.377(6) . ?
C28 C29 1.520(6) . ?
C28 C30 1.503(6) . ?
C28 C31 1.509(7) . ?
C16 H16 0.9300 . ?
C16 C15 1.385(6) . ?
C33 C34 1.521(6) . ?
C33 C35 1.511(7) . ?
C33 C36 1.524(7) . ?
C34 H34A 0.9600 . ?
C34 H34B 0.9600 . ?
C34 H34C 0.9600 . ?
B1 H1 1.09(4) . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C23 H23 0.9300 . ?
C23 C24 1.375(7) . ?
C24 H24 0.9300 . ?
C24 C25 1.367(7) . ?
C25 H25 0.9300 . ?
C29 H29A 0.9600 . ?
C29 H29B 0.9600 . ?
C29 H29C 0.9600 . ?
C30 H30A 0.9600 . ?
C30 H30B 0.9600 . ?
C30 H30C 0.9600 . ?
C31 H31A 0.9600 . ?
C31 H31B 0.9600 . ?
C31 H31C 0.9600 . ?
C35 H35A 0.9600 . ?
C35 H35B 0.9600 . ?
C35 H35C 0.9600 . ?
C36 H36A 0.9600 . ?
C36 H36B 0.9600 . ?
C36 H36C 0.9600 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
W1 N1 N2 C7 -170.7(2) . . . . ?
W1 N1 N2 B1 6.1(4) . . . . ?
W1 N1 C5 C6 169.3(3) . . . . ?
W1 N1 C5 C4 -11.8(6) . . . . ?
W1 N3 N4 C12 176.0(2) . . . . ?
W1 N3 N4 B1 -8.5(4) . . . . ?
W1 N3 C10 C9 6.9(6) . . . . ?
W1 N3 C10 C11 -174.7(3) . . . . ?
W1 N5 N6 C17 -171.1(2) . . . . ?
W1 N5 N6 B1 18.1(4) . . . . ?
W1 N5 C15 C14 -9.6(6) . . . . ?
W1 N5 C15 C16 170.0(3) . . . . ?
P1 C21 C26 C25 -178.3(4) . . . . ?
P1 C21 C22 C23 178.8(3) . . . . ?
N1 N2 C7 C6 -1.3(4) . . . . ?
N1 N2 C7 C8 178.7(3) . . . . ?
N1 N2 B1 N4 55.2(4) . . . . ?
N1 N2 B1 N6 -63.6(4) . . . . ?
N1 C5 C6 C7 0.2(5) . . . . ?
N3 N4 C12 C11 -0.4(4) . . . . ?
N3 N4 C12 C13 -179.2(3) . . . . ?
N3 N4 B1 N2 -53.9(4) . . . . ?
N3 N4 B1 N6 62.9(4) . . . . ?
N3 C10 C11 C12 -1.8(4) . . . . ?
N5 N6 C17 C18 177.1(3) . . . . ?
N5 N6 C17 C16 -0.8(4) . . . . ?
N5 N6 B1 N4 -68.7(4) . . . . ?
N5 N6 B1 N2 49.0(4) . . . . ?
C1 P1 C21 C26 122.0(3) . . . . ?
C1 P1 C21 C22 -55.8(4) . . . . ?
N4 N3 C10 C9 -176.8(3) . . . . ?
N4 N3 C10 C11 1.6(4) . . . . ?
N4 C12 C11 C10 1.3(4) . . . . ?
N2 N1 C5 C6 -1.0(4) . . . . ?
N2 N1 C5 C4 177.9(4) . . . . ?
N6 N5 C15 C14 179.6(4) . . . . ?
N6 N5 C15 C16 -0.8(4) . . . . ?
N6 C17 C16 C15 0.3(4) . . . . ?
C5 N1 N2 C7 1.4(4) . . . . ?
C5 N1 N2 B1 178.2(3) . . . . ?
C5 C6 C7 N2 0.6(4) . . . . ?
C5 C6 C7 C8 -179.3(4) . . . . ?
C21 P1 C1 W1 -104.7(3) . . . . ?
C21 P1 C1 Pt1 76.1(3) . . . . ?
C21 C26 C25 C24 0.2(7) . . . . ?
C21 C22 C23 C24 -1.2(7) . . . . ?
C7 N2 B1 N4 -128.7(4) . . . . ?
C7 N2 B1 N6 112.5(4) . . . . ?
C19 P1 C1 W1 16.0(4) . . . . ?
C19 P1 C1 Pt1 -163.2(3) . . . . ?
C19 P1 C21 C26 -2.3(4) . . . . ?
C19 P1 C21 C22 180.0(3) . . . . ?
C9 C10 C11 C12 176.4(4) . . . . ?
C17 N6 B1 N4 122.7(4) . . . . ?
C17 N6 B1 N2 -119.6(4) . . . . ?
C17 C16 C15 N5 0.4(5) . . . . ?
C17 C16 C15 C14 179.9(4) . . . . ?
C4 C5 C6 C7 -178.6(4) . . . . ?
C12 N4 B1 N2 120.5(4) . . . . ?
C12 N4 B1 N6 -122.7(4) . . . . ?
C26 C21 C22 C23 1.0(6) . . . . ?
C10 N3 N4 C12 -0.8(4) . . . . ?
C10 N3 N4 B1 174.8(3) . . . . ?
C20 P1 C1 W1 135.3(3) . . . . ?
C20 P1 C1 Pt1 -44.0(3) . . . . ?
C20 P1 C21 C26 -116.4(4) . . . . ?
C20 P1 C21 C22 65.8(4) . . . . ?
C18 C17 C16 C15 -177.4(4) . . . . ?
C22 C21 C26 C25 -0.5(6) . . . . ?
C22 C23 C24 C25 0.9(8) . . . . ?
C15 N5 N6 C17 1.0(4) . . . . ?
C15 N5 N6 B1 -169.9(3) . . . . ?
B1 N4 C12 C11 -175.2(4) . . . . ?
B1 N4 C12 C13 6.0(6) . . . . ?
B1 N2 C7 C6 -177.8(4) . . . . ?
B1 N2 C7 C8 2.1(6) . . . . ?
B1 N6 C17 C18 -13.5(6) . . . . ?
B1 N6 C17 C16 168.6(4) . . . . ?
C13 C12 C11 C10 -180.0(4) . . . . ?
C23 C24 C25 C26 -0.4(8) . . . . ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.000 0.000 0.500 311.2 62.1 '2 CH3CH2OH'
2 0.000 0.500 0.000 311.2 62.1 '2 CH3CH2OH'
