#------------------------------------------------------------------------------
#$Date: 2020-11-06 14:23:16 +0200 (Fri, 06 Nov 2020) $
#$Revision: 258865 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/53/7705338.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7705338
loop_
_publ_author_name
'Petrovskii, Stanislav K.'
'Paderina, Aleksandra V.'
'Sizova, Anastasia A.'
'Baranov, Andrey Yu'
'Artem'ev, Alexander A.'
'Sizov, Vladimir V.'
'Grachova, Elena V.'
_publ_section_title
;
 Luminescence behaviour of Au(I)-Cu(I) heterobimetallic coordination
 polymers based on alkynyl-tris(2-pyridyl)phosphine Au(I) complexes.
;
_journal_issue                   38
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13430
_journal_page_last               13439
_journal_paper_doi               10.1039/d0dt02583f
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C30 H23 Au N3 O P'
_chemical_formula_sum            'C30 H23 Au N3 O P'
_chemical_formula_weight         669.46
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_block_doi                 10.5517/ccdc.csd.cc25k7gg
_audit_creation_date             2020-04-24
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2020-06-27 deposited with the CCDC.	2020-09-02 downloaded from the CCDC.
;
_cell_angle_alpha                109.897(4)
_cell_angle_beta                 111.317(4)
_cell_angle_gamma                100.110(4)
_cell_formula_units_Z            2
_cell_length_a                   10.4121(5)
_cell_length_b                   11.9530(5)
_cell_length_c                   12.0119(5)
_cell_measurement_reflns_used    5088
_cell_measurement_temperature    100(11)
_cell_measurement_theta_max      30.7410
_cell_measurement_theta_min      3.2290
_cell_volume                     1230.75(12)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      100(11)
_diffrn_detector_area_resol_mean 16.2096
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.875
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
  1 omega  -81.00    2.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -      -22.4241  -77.0000   30.0000 83

#__ type_ start__ end____ width___ exp.time_
  2 omega   65.00   93.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -       23.3616   77.0000  -30.0000 28

#__ type_ start__ end____ width___ exp.time_
  3 omega  -44.00   38.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -       23.3616  -57.0000   90.0000 82

#__ type_ start__ end____ width___ exp.time_
  4 omega   -7.00   42.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -       23.3616   77.0000  -30.0000 49

#__ type_ start__ end____ width___ exp.time_
  5 omega  -24.00   64.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -       23.3616  -99.0000 -150.0000 88

#__ type_ start__ end____ width___ exp.time_
  6 omega   42.00   81.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -       23.3616   57.0000  -30.0000 39

#__ type_ start__ end____ width___ exp.time_
  7 omega   56.00   92.00   1.0000    5.3700
omega____ theta____ kappa____ phi______ frames
    -       23.3616   57.0000 -120.0000 36
;
_diffrn_measurement_device_type  'Xcalibur, Eos'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      -0.0592347000
_diffrn_orient_matrix_UB_12      -0.0054877000
_diffrn_orient_matrix_UB_13      -0.0571349000
_diffrn_orient_matrix_UB_21      0.0114836000
_diffrn_orient_matrix_UB_22      -0.0521741000
_diffrn_orient_matrix_UB_23      -0.0406646000
_diffrn_orient_matrix_UB_31      -0.0491254000
_diffrn_orient_matrix_UB_32      -0.0419120000
_diffrn_orient_matrix_UB_33      0.0082497000
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0330
_diffrn_reflns_av_unetI/netI     0.0602
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.875
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            11477
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.875
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.892
_diffrn_reflns_theta_min         2.860
_diffrn_source                   'Enhance (Mo) X-ray Source'
_exptl_absorpt_coefficient_mu    6.071
_exptl_absorpt_correction_T_max  0.807
_exptl_absorpt_correction_T_min  0.261
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'clear colourless'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.809
_exptl_crystal_description       needle
_exptl_crystal_F_000             654
_exptl_crystal_size_max          0.302
_exptl_crystal_size_mid          0.254
_exptl_crystal_size_min          0.037
_refine_diff_density_max         1.753
_refine_diff_density_min         -1.375
_refine_diff_density_rms         0.169
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     320
_refine_ls_number_reflns         6807
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.0341
_refine_ls_R_factor_gt           0.0300
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0141P)²+0.0265P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0596
_refine_ls_wR_factor_ref         0.0620
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6282
_reflns_number_total             6807
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d0dt02583f3.cif
_cod_data_source_block           ps-002
_cod_depositor_comments
'Adding full bibliography for 7705338--7705340.cif.'
_cod_original_cell_volume        1230.74(11)
_cod_database_code               7705338
_shelx_shelxl_version_number     2014/7
_chemical_oxdiff_formula         'P1 Au1 C32 O1 N3'
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.807
_shelx_estimated_absorpt_t_min   0.261
_reflns_odcompleteness_completeness 99.90
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     28.51
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All O(H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(C16) = Uanis(C17)
3.a Aromatic/amide H refined with riding coordinates:
 C1(H1A), C2(H2), C3(H3), C4(H4), C6(H6), C7(H7), C8(H8), C9(H9), C11(H11),
 C12(H12), C13(H13), C14(H14), C20(H20), C21(H21), C22(H22), C23(H23), C24(H24),
  C26(H26), C27(H27), C28(H28), C29(H29), C30(H30)
3.b Idealised tetrahedral OH refined as rotating group:
 O1(H1)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.35028(2) 0.27441(2) 0.62989(2) 0.00959(4) Uani 1 1 d . . . . .
P1 P 0.39458(9) 0.20387(8) 0.78776(9) 0.00809(17) Uani 1 1 d . . . . .
O1 O 0.3603(3) 0.4648(2) 0.2837(3) 0.0116(5) Uani 1 1 d . . . . .
H1 H 0.4400 0.5104 0.3482 0.017 Uiso 1 1 calc GR . . . .
N1 N 0.1215(3) 0.0644(3) 0.6815(3) 0.0137(6) Uani 1 1 d . . . . .
N2 N 0.5620(3) 0.2949(3) 1.0548(3) 0.0132(6) Uani 1 1 d . . . . .
N3 N 0.5036(3) 0.0438(3) 0.6628(3) 0.0115(6) Uani 1 1 d . . . . .
C1 C -0.0046(4) 0.0049(3) 0.6739(4) 0.0175(8) Uani 1 1 d . . . . .
H1A H -0.0821 -0.0498 0.5904 0.021 Uiso 1 1 calc R . . . .
C2 C -0.0250(4) 0.0215(3) 0.7865(4) 0.0186(9) Uani 1 1 d . . . . .
H2 H -0.1139 -0.0223 0.7779 0.022 Uiso 1 1 calc R . . . .
C3 C 0.0878(4) 0.1032(3) 0.9095(4) 0.0145(7) Uani 1 1 d . . . . .
H3 H 0.0765 0.1160 0.9857 0.017 Uiso 1 1 calc R . . . .
C4 C 0.2199(4) 0.1670(3) 0.9192(4) 0.0114(7) Uani 1 1 d . . . . .
H4 H 0.2982 0.2238 1.0014 0.014 Uiso 1 1 calc R . . . .
C5 C 0.2303(4) 0.1428(3) 0.8023(4) 0.0095(7) Uani 1 1 d . . . . .
C6 C 0.6715(4) 0.3787(3) 1.1728(4) 0.0179(8) Uani 1 1 d . . . . .
H6 H 0.6878 0.3611 1.2455 0.021 Uiso 1 1 calc R . . . .
C7 C 0.7630(4) 0.4916(3) 1.1932(4) 0.0159(8) Uani 1 1 d . . . . .
H7 H 0.8392 0.5472 1.2771 0.019 Uiso 1 1 calc R . . . .
C8 C 0.7384(4) 0.5189(3) 1.0865(4) 0.0152(8) Uani 1 1 d . . . . .
H8 H 0.7981 0.5933 1.0971 0.018 Uiso 1 1 calc R . . . .
C9 C 0.6227(4) 0.4337(3) 0.9623(4) 0.0119(7) Uani 1 1 d . . . . .
H9 H 0.6022 0.4503 0.8886 0.014 Uiso 1 1 calc R . . . .
C10 C 0.5387(3) 0.3227(3) 0.9521(4) 0.0091(7) Uani 1 1 d . . . . .
C11 C 0.5509(4) -0.0553(3) 0.6382(4) 0.0150(8) Uani 1 1 d . . . . .
H11 H 0.5826 -0.0743 0.5731 0.018 Uiso 1 1 calc R . . . .
C12 C 0.5551(4) -0.1303(3) 0.7037(4) 0.0144(8) Uani 1 1 d . . . . .
H12 H 0.5889 -0.1979 0.6830 0.017 Uiso 1 1 calc R . . . .
C13 C 0.5083(4) -0.1036(3) 0.8012(4) 0.0142(7) Uani 1 1 d . . . . .
H13 H 0.5116 -0.1517 0.8482 0.017 Uiso 1 1 calc R . . . .
C14 C 0.4562(4) -0.0027(3) 0.8267(4) 0.0111(7) Uani 1 1 d . . . . .
H14 H 0.4217 0.0168 0.8897 0.013 Uiso 1 1 calc R . . . .
C15 C 0.4570(3) 0.0676(3) 0.7569(3) 0.0076(6) Uani 1 1 d . . . . .
C16 C 0.3116(4) 0.3450(3) 0.4972(4) 0.0100(5) Uani 1 1 d . . . . .
C17 C 0.2882(4) 0.3927(3) 0.4221(4) 0.0100(5) Uani 1 1 d . . . . .
C18 C 0.2499(3) 0.4490(3) 0.3276(3) 0.0087(7) Uani 1 1 d . . . . .
C19 C 0.2272(4) 0.5748(3) 0.3899(3) 0.0091(7) Uani 1 1 d . . . . .
C20 C 0.1567(4) 0.5875(3) 0.4704(4) 0.0125(7) Uani 1 1 d . . . . .
H20 H 0.1338 0.5234 0.4945 0.015 Uiso 1 1 calc R . . . .
C21 C 0.1204(4) 0.6952(3) 0.5148(4) 0.0161(8) Uani 1 1 d . . . . .
H21 H 0.0745 0.7034 0.5692 0.019 Uiso 1 1 calc R . . . .
C22 C 0.1531(4) 0.7912(3) 0.4775(4) 0.0168(8) Uani 1 1 d . . . . .
H22 H 0.1273 0.8627 0.5054 0.020 Uiso 1 1 calc R . . . .
C23 C 0.2236(4) 0.7788(3) 0.3990(4) 0.0163(8) Uani 1 1 d . . . . .
H23 H 0.2456 0.8427 0.3743 0.020 Uiso 1 1 calc R . . . .
C24 C 0.2624(4) 0.6725(3) 0.3561(4) 0.0126(7) Uani 1 1 d . . . . .
H24 H 0.3119 0.6664 0.3047 0.015 Uiso 1 1 calc R . . . .
C25 C 0.1069(4) 0.3634(3) 0.2014(3) 0.0092(7) Uani 1 1 d . . . . .
C26 C 0.0696(4) 0.3900(3) 0.0924(4) 0.0142(7) Uani 1 1 d . . . . .
H26 H 0.1347 0.4571 0.0965 0.017 Uiso 1 1 calc R . . . .
C27 C -0.0610(4) 0.3201(3) -0.0213(4) 0.0167(8) Uani 1 1 d . . . . .
H27 H -0.0828 0.3383 -0.0940 0.020 Uiso 1 1 calc R . . . .
C28 C -0.1600(4) 0.2218(3) -0.0263(4) 0.0180(8) Uani 1 1 d . . . . .
H28 H -0.2492 0.1746 -0.1025 0.022 Uiso 1 1 calc R . . . .
C29 C -0.1271(4) 0.1939(3) 0.0804(4) 0.0175(8) Uani 1 1 d . . . . .
H29 H -0.1938 0.1278 0.0764 0.021 Uiso 1 1 calc R . . . .
C30 C 0.0065(4) 0.2647(3) 0.1949(4) 0.0126(7) Uani 1 1 d . . . . .
H30 H 0.0285 0.2458 0.2673 0.015 Uiso 1 1 calc R . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C16 Au1 P1 177.06(9) . . ?
C5 P1 Au1 113.27(12) . . ?
C5 P1 C10 109.16(16) . . ?
C10 P1 Au1 113.19(11) . . ?
C15 P1 Au1 115.15(12) . . ?
C15 P1 C5 101.34(14) . . ?
C15 P1 C10 103.69(15) . . ?
C18 O1 H1 109.5 . . ?
C5 N1 C1 117.4(3) . . ?
C6 N2 C10 117.5(3) . . ?
C11 N3 C15 116.4(3) . . ?
N1 C1 H1A 118.7 . . ?
N1 C1 C2 122.6(4) . . ?
C2 C1 H1A 118.7 . . ?
C1 C2 H2 120.5 . . ?
C3 C2 C1 119.0(3) . . ?
C3 C2 H2 120.5 . . ?
C2 C3 H3 120.4 . . ?
C2 C3 C4 119.2(3) . . ?
C4 C3 H3 120.4 . . ?
C3 C4 H4 121.2 . . ?
C5 C4 C3 117.6(3) . . ?
C5 C4 H4 121.2 . . ?
N1 C5 P1 109.3(3) . . ?
N1 C5 C4 124.2(3) . . ?
C4 C5 P1 126.4(3) . . ?
N2 C6 H6 118.3 . . ?
N2 C6 C7 123.4(4) . . ?
C7 C6 H6 118.3 . . ?
C6 C7 H7 120.7 . . ?
C8 C7 C6 118.6(3) . . ?
C8 C7 H7 120.7 . . ?
C7 C8 H8 120.4 . . ?
C7 C8 C9 119.1(3) . . ?
C9 C8 H8 120.4 . . ?
C8 C9 H9 121.1 . . ?
C8 C9 C10 117.8(3) . . ?
C10 C9 H9 121.1 . . ?
N2 C10 P1 117.7(2) . . ?
N2 C10 C9 123.6(3) . . ?
C9 C10 P1 118.7(3) . . ?
N3 C11 H11 118.1 . . ?
N3 C11 C12 123.8(3) . . ?
C12 C11 H11 118.1 . . ?
C11 C12 H12 120.5 . . ?
C11 C12 C13 119.0(3) . . ?
C13 C12 H12 120.5 . . ?
C12 C13 H13 120.9 . . ?
C12 C13 C14 118.2(3) . . ?
C14 C13 H13 120.9 . . ?
C13 C14 H14 120.6 . . ?
C15 C14 C13 118.7(3) . . ?
C15 C14 H14 120.6 . . ?
N3 C15 P1 114.9(3) . . ?
N3 C15 C14 123.9(3) . . ?
C14 C15 P1 121.3(3) . . ?
C17 C16 Au1 176.7(3) . . ?
C16 C17 C18 176.5(4) . . ?
O1 C18 C17 110.3(3) . . ?
O1 C18 C19 111.6(3) . . ?
O1 C18 C25 105.5(3) . . ?
C17 C18 C19 110.9(3) . . ?
C17 C18 C25 112.1(3) . . ?
C25 C18 C19 106.3(3) . . ?
C20 C19 C18 120.0(3) . . ?
C24 C19 C18 120.7(3) . . ?
C24 C19 C20 119.0(3) . . ?
C19 C20 H20 119.7 . . ?
C21 C20 C19 120.5(3) . . ?
C21 C20 H20 119.7 . . ?
C20 C21 H21 120.0 . . ?
C20 C21 C22 119.9(3) . . ?
C22 C21 H21 120.0 . . ?
C21 C22 H22 120.3 . . ?
C23 C22 C21 119.4(3) . . ?
C23 C22 H22 120.3 . . ?
C22 C23 H23 119.5 . . ?
C22 C23 C24 121.0(3) . . ?
C24 C23 H23 119.5 . . ?
C19 C24 H24 120.0 . . ?
C23 C24 C19 120.1(3) . . ?
C23 C24 H24 120.0 . . ?
C26 C25 C18 119.3(3) . . ?
C26 C25 C30 118.3(3) . . ?
C30 C25 C18 122.2(3) . . ?
C25 C26 H26 119.1 . . ?
C27 C26 C25 121.9(3) . . ?
C27 C26 H26 119.1 . . ?
C26 C27 H27 120.4 . . ?
C26 C27 C28 119.2(4) . . ?
C28 C27 H27 120.4 . . ?
C27 C28 H28 119.8 . . ?
C29 C28 C27 120.4(3) . . ?
C29 C28 H28 119.8 . . ?
C28 C29 H29 120.0 . . ?
C28 C29 C30 120.0(3) . . ?
C30 C29 H29 120.0 . . ?
C25 C30 C29 120.3(4) . . ?
C25 C30 H30 119.9 . . ?
C29 C30 H30 119.9 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 P1 2.2601(10) . ?
Au1 C16 1.996(4) . ?
P1 C5 1.831(3) . ?
P1 C10 1.831(4) . ?
P1 C15 1.830(3) . ?
O1 H1 0.8200 . ?
O1 C18 1.438(4) . ?
N1 C1 1.334(4) . ?
N1 C5 1.332(4) . ?
N2 C6 1.330(4) . ?
N2 C10 1.335(5) . ?
N3 C11 1.343(4) . ?
N3 C15 1.350(4) . ?
C1 H1A 0.9300 . ?
C1 C2 1.398(6) . ?
C2 H2 0.9300 . ?
C2 C3 1.367(5) . ?
C3 H3 0.9300 . ?
C3 C4 1.393(5) . ?
C4 H4 0.9300 . ?
C4 C5 1.383(5) . ?
C6 H6 0.9300 . ?
C6 C7 1.394(5) . ?
C7 H7 0.9300 . ?
C7 C8 1.375(5) . ?
C8 H8 0.9300 . ?
C8 C9 1.394(5) . ?
C9 H9 0.9300 . ?
C9 C10 1.395(4) . ?
C11 H11 0.9300 . ?
C11 C12 1.377(5) . ?
C12 H12 0.9300 . ?
C12 C13 1.388(5) . ?
C13 H13 0.9300 . ?
C13 C14 1.393(4) . ?
C14 H14 0.9300 . ?
C14 C15 1.375(5) . ?
C16 C17 1.199(5) . ?
C17 C18 1.478(5) . ?
C18 C19 1.537(4) . ?
C18 C25 1.527(5) . ?
C19 C20 1.398(5) . ?
C19 C24 1.394(5) . ?
C20 H20 0.9300 . ?
C20 C21 1.391(5) . ?
C21 H21 0.9300 . ?
C21 C22 1.399(5) . ?
C22 H22 0.9300 . ?
C22 C23 1.377(5) . ?
C23 H23 0.9300 . ?
C23 C24 1.390(5) . ?
C24 H24 0.9300 . ?
C25 C26 1.386(5) . ?
C25 C30 1.392(4) . ?
C26 H26 0.9300 . ?
C26 C27 1.374(5) . ?
C27 H27 0.9300 . ?
C27 C28 1.388(5) . ?
C28 H28 0.9300 . ?
C28 C29 1.373(6) . ?
C29 H29 0.9300 . ?
C29 C30 1.395(5) . ?
C30 H30 0.9300 . ?
