data_1100116
_chemical_formula_sum 'C10 H26 Al1 F5 N2'
_chemical_formula_moiety
;
(C10 H26 N2 2+)n,n(Al1 F5 2-)
;
_journal_volume 4
_journal_year 2002
_journal_page_first 1213
_journal_name_full 'Solid State Sciences '
loop_
_publ_author_name
"E.Goreshnik"
"M.Leblanc"
"E.Gaudin"
"F.Taulelle"
"V.Maisonneuve"
_chemical_name_systematic
;
catena-(1,10-Decanediammonium (\m~2~-fluoro)-tetrafluoro-aluminium)
;
_cell_volume    735.303
_exptl_crystal_density_diffrn 1.331
_diffrn_ambient_temperature ?
_diffrn_special_details
;
The study was carried out at room temperature,in the range 283-303K

;
_refine_ls_R_factor_gt 0.0892
_refine_ls_wR_factor_gt 0.0892
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'P 21'
_symmetry_Int_Tables_number 4
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,1/2+y,-z
_cell_length_a 7.881(5)
_cell_length_b 5.489(2)
_cell_length_c 18.36(1)
_cell_angle_alpha 90
_cell_angle_beta 112.21(6)
_cell_angle_gamma 90
_cell_formula_units_Z 2
loop_
_atom_type_symbol
_atom_type_radius_bond
C 0.68
Al 1.35
F 0.64
N 0.68
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Al1 Al 0.3250(4) 0.00000 -0.0295(2)
F1 F 0.3416(7) -0.002(3) 0.0713(3)
F2 F 0.3391(8) -0.013(2) -0.1235(3)
F3 F 0.510(2) 0.244(2) -0.004(6)
F4 F 0.1549(7) 0.232(2) -0.0598(3)
F5 F 0.150(1) -0.230(1) -0.0546(4)
N1 N 0.189(1) 0.526(2) 0.0771(4)
N2 N 0.283(1) 0.505(3) 0.8459(5)
C1 C 0.266(2) 0.418(3) 0.1580(6)
C2 C 0.214(2) 0.562(3) 0.2139(6)
C3 C 0.292(2) 0.449(3) 0.2962(6)
C4 C 0.218(2) 0.573(3) 0.3539(8)
C5 C 0.292(2) 0.455(3) 0.4357(7)
C6 C 0.216(2) 0.564(3) 0.4926(7)
C7 C 0.289(2) 0.458(3) 0.5740(7)
C8 C 0.205(2) 0.563(3) 0.6294(7)
C9 C 0.285(2) 0.475(4) 0.7127(6)
C10 C 0.189(2) 0.573(3) 0.7627(6)
Al1A* Al 0.6750(4) 0.50000 0.0295(2)
F3A* F 0.490(2) -0.256(2) 0.004(6)