Crystallography Open Database

Information card for entry 1503324

Preview

Coordinates	1503324.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H24 O4
Calculated formula	C18.998 H24 O4
Title of publication	Studies directed toward the synthesis of hamigeran B: a catalytic oxidative cyclization.
Authors of publication	Cai, Zhengxin; Harmata, Michael
Journal of publication	Organic letters
Year of publication	2010
Journal volume	12
Journal issue	24
Pages of publication	5668 - 5670
a	11.135 ± 0.004 Å
b	12.976 ± 0.004 Å
c	13.502 ± 0.005 Å
α	66.977 ± 0.003°
β	72.14 ± 0.004°
γ	78.98 ± 0.004°
Cell volume	1703.3 ± 1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0565
Residual factor for significantly intense reflections	0.0469
Weighted residual factors for significantly intense reflections	0.1209
Weighted residual factors for all reflections included in the refinement	0.1294
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1503324.cif
91932	2013-12-28	cif/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the range 1 CIFs.	1503324.cif
37199	2012-03-01	../uploads/cif-deposit/cod/cif Adding structures of 1503324 via cif-deposit CGI script.	1503324.cif