Crystallography Open Database

Information card for entry 1507371

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Structure parameters

Formula	C14 H25 N O4 Si
Calculated formula	C14 H25 N O4 Si
SMILES	[Si]1(OC[C@@H](OC=O)[C@@H](O1)C1=NC1)(C(C)(C)C)C(C)(C)C
Title of publication	Fragmentation of carbohydrate anomeric alkoxyl radicals. A new synthesis of chiral beta-iodo azides, vinyl azides, and 2H-azirines.
Authors of publication	Alonso-Cruz, Carmen R; Kennedy, Alan R.; Rodríguez, María S; Suárez, Ernesto
Journal of publication	Organic letters
Year of publication	2003
Journal volume	5
Journal issue	20
Pages of publication	3729 - 3732
a	16.4478 ± 0.0008 Å
b	6.2864 ± 0.0003 Å
c	16.1368 ± 0.0008 Å
α	90°
β	95.529 ± 0.002°
γ	90°
Cell volume	1660.74 ± 0.14 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	5
Hermann-Mauguin space group symbol	C 1 2 1
Hall space group symbol	C 2y
Residual factor for all reflections	0.0614
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for significantly intense reflections	0.0734
Weighted residual factors for all reflections included in the refinement	0.0798
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
201954 (current)	2017-10-13	cif/ Marking COD entries in range 1 that are known to be related to ChemSpider entries using the _cod_related_entry data loop.	1507371.cif
176729	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1507371.cif
120071	2014-07-11	Adding DOIs to range 1 structures.	1507371.cif
53865	2012-04-20	cif/ Adding structures of 1507371 via cif-deposit CGI script.	1507371.cif