#------------------------------------------------------------------------------ #$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $ #$Revision: 176729 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/51/61/1516147.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1516147 loop_ _publ_author_name 'Zipfel, Hannes F.' 'Carreira, Erick M.' _publ_section_title ; An efficient synthesis strategy to the core structure of 6-5-6-5-6-membered epipolythiodiketopiperazines. ; _journal_issue 11 _journal_name_full 'Organic letters' _journal_page_first 2854 _journal_page_last 2857 _journal_paper_doi 10.1021/ol500990f _journal_volume 16 _journal_year 2014 _chemical_absolute_configuration ad _chemical_formula_moiety 'C7 H9 Br O2' _chemical_formula_sum 'C7 H9 Br O2' _chemical_formula_weight 205.05 _chemical_name_systematic ((1S,2R,4S)-2-bromo-7-oxabicyclo[2.2.1]hept-5-en-2-yl)methanol _space_group_crystal_system trigonal _space_group_IT_number 145 _space_group_name_Hall 'P 32' _space_group_name_H-M_alt 'P 32' _symmetry_cell_setting trigonal _symmetry_Int_Tables_number 145 _symmetry_space_group_name_Hall 'P 32' _symmetry_space_group_name_H-M 'P 32' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2013-11-11 _audit_creation_method ; Olex2 1.2 (compiled 2013.09.17 svn.r2790 for OlexSys, GUI svn.r4601) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 9 _cell_length_a 17.8119(15) _cell_length_b 17.8119(15) _cell_length_c 6.2589(5) _cell_measurement_reflns_used 7903 _cell_measurement_temperature 99.99 _cell_measurement_theta_max 30.058 _cell_measurement_theta_min 3.49 _cell_volume 1719.7(2) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'SAINT v8.27A (Bruker, 2012)' _computing_molecular_graphics OLEX2 _computing_publication_material OLEX2 _computing_structure_refinement 'SHELXL-97 (Sheldrick, 2008)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _diffrn_ambient_temperature 100.0(2) _diffrn_detector 'Bruker APEX2 area detector' _diffrn_detector_area_resol_mean 8.33 _diffrn_detector_type 'CCD area detector' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device 'kappa-stage diffractometer' _diffrn_measurement_device_type 'Bruker Kappa Apex2 Duo' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator 'focusing graphite' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_xray_symbol K-L~3~ _diffrn_reflns_av_R_equivalents 0.0301 _diffrn_reflns_av_unetI/netI 0.0425 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 25 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 18642 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.513 _diffrn_reflns_theta_min 1.320 _diffrn_source 'sealed tube' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 5.313 _exptl_absorpt_correction_T_max 0.8134 _exptl_absorpt_correction_T_min 0.6022 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0805 before and 0.0528 after correction. The Ratio of minimum to maximum transmission is 0.7403. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.782 _exptl_crystal_description needle _exptl_crystal_F_000 918 _exptl_crystal_recrystallization_method 'crystallized from a diethyether/pentane mixture' _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.742 _refine_diff_density_min -0.476 _refine_diff_density_rms 0.070 _refine_ls_abs_structure_details ; Flack x determined using 2628 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.008(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 275 _refine_ls_number_reflns 6360 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0255 _refine_ls_R_factor_gt 0.0235 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0129P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0456 _refine_ls_wR_factor_ref 0.0467 _reflns_Friedel_coverage 0.998 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.998 _reflns_number_gt 6143 _reflns_number_total 6360 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ol500990f_si_002.cif _cod_data_source_block mo_ca041113_0m _cod_depositor_comments 'Adding full bibliography for 1516147--1516149.cif.' _cod_original_cell_volume 1719.7(3) _cod_database_code 1516147 #BEGIN Tags that were not found in dictionaries: _shelxl_version_number 2013-4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All O(H) groups 2.a Ternary CH refined with riding coordinates: C2(H2A), C5(H5), C2A(H2AB), C5A(H5A), C2B(H2BA), C5B(H5B) 2.b Secondary CH2 refined with riding coordinates: C6(H6A,H6B), C7(H7A,H7B), C6A(H6AA,H6AB), C7A(H7AA,H7AB), C6B(H6BA,H6BB), C7B(H7BA,H7BB) 2.c Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C3A(H3A), C4A(H4A), C3B(H3B), C4B(H4B) 2.d Idealised tetrahedral OH refined as rotating group: O2(H2), O2A(H2AA), O2B(H2B) ; _shelx_res_file ; TITL mo_ca041113_0m in P31 #144 CELL 0.71073 17.8119 17.8119 6.2589 90 90 120 ZERR 9 0.0015 0.0015 0.0005 0 0 0 LATT -1 SYMM -Y,+X-Y,0.667+Z SYMM +Y-X,-X,0.333+Z SFAC C H Br O UNIT 63 81 9 18 L.S. 4 0 0 PLAN 20 TEMP -173.16 REM reset to P31 #144 BOND$H HTAB fmap 2 53 acta TWIN 0 -1 0 -1 0 0 0 0 -1 2 REM D:/SMoCC_Strukturen/ca041113/work/mo_ca041113_0m.hkl WGHT 0.012900 BASF 0.33776 FVAR 0.42972 BR1 3 0.820023 0.814294 0.639100 11.00000 0.01199 0.02026 = 0.01714 -0.00109 0.00145 0.00858 O1 4 1.001781 0.778388 0.339544 11.00000 0.01427 0.01624 = 0.01996 -0.00074 0.00391 0.00902 O2 4 1.013963 0.954075 0.715219 11.00000 0.01711 0.01023 = 0.01336 0.00033 0.00306 0.00511 AFIX 147 H2 2 0.984600 0.963288 0.805499 11.00000 -1.50000 AFIX 0 C1 1 0.923470 0.803142 0.588770 11.00000 0.01057 0.01059 = 0.01308 0.00249 0.00400 0.00609 C2 1 0.949594 0.819814 0.346501 11.00000 0.01399 0.01132 = 0.01295 0.00042 0.00072 0.00459 AFIX 13 H2A 2 0.979988 0.882017 0.301544 11.00000 -1.20000 AFIX 0 C3 1 0.872560 0.759862 0.212585 11.00000 0.01386 0.02562 = 0.01093 -0.00197 0.00039 0.00794 AFIX 43 H3 2 0.838609 0.775394 0.126106 11.00000 -1.20000 AFIX 0 C4 1 0.861266 0.680459 0.239170 11.00000 0.02532 0.01694 = 0.01531 -0.00547 0.00121 0.00577 AFIX 43 H4 2 0.818224 0.628005 0.175641 11.00000 -1.20000 AFIX 0 C5 1 0.932081 0.692351 0.392721 11.00000 0.02355 0.01456 = 0.02067 0.00065 0.00503 0.01068 AFIX 13 H5 2 0.947868 0.645830 0.386999 11.00000 -1.20000 AFIX 0 C6 1 0.907336 0.709757 0.619438 11.00000 0.02185 0.01355 = 0.01538 0.00306 0.00014 0.00804 AFIX 23 H6A 2 0.845992 0.668367 0.654523 11.00000 -1.20000 H6B 2 0.945243 0.707340 0.731654 11.00000 -1.20000 AFIX 0 C7 1 0.995662 0.866667 0.733836 11.00000 0.01321 0.01445 = 0.01312 -0.00014 -0.00111 0.00787 AFIX 23 H7A 2 0.979678 0.847647 0.883777 11.00000 -1.20000 H7B 2 1.049065 0.864798 0.700897 11.00000 -1.20000 AFIX 0 BR1A 3 0.499756 0.370286 0.557219 11.00000 0.01456 0.02220 = 0.01830 -0.00217 -0.00037 0.00124 O1A 4 0.701302 0.559852 0.889448 11.00000 0.01586 0.01714 = 0.02187 -0.00429 -0.00165 0.00643 O2A 4 0.686490 0.396172 0.482679 11.00000 0.02387 0.01965 = 0.01487 -0.00435 -0.00500 0.01419 AFIX 147 H2AA 2 0.657526 0.362989 0.382259 11.00000 -1.50000 AFIX 0 C1A 1 0.613182 0.472068 0.624281 11.00000 0.01292 0.01143 = 0.01381 0.00250 -0.00078 0.00494 C2A 1 0.636977 0.469885 0.861737 11.00000 0.01853 0.01228 = 0.01371 -0.00008 -0.00198 0.00800 AFIX 13 H2AB 2 0.657199 0.427946 0.894938 11.00000 -1.20000 AFIX 0 C3A 1 0.563423 0.461559 1.001310 11.00000 0.01938 0.02233 = 0.01199 -0.00041 0.00163 0.00861 AFIX 43 H3A 2 0.522771 0.411944 1.079109 11.00000 -1.20000 AFIX 0 C4A 1 0.567790 0.537344 0.991923 11.00000 0.02253 0.02732 = 0.02054 0.00040 0.00574 0.01471 AFIX 43 H4A 2 0.531250 0.554055 1.062756 11.00000 -1.20000 AFIX 0 C5A 1 0.643404 0.592791 0.844279 11.00000 0.02482 0.01289 = 0.02545 -0.00075 0.00315 0.01121 AFIX 13 H5A 2 0.669335 0.656778 0.863254 11.00000 -1.20000 AFIX 0 C6A 1 0.613408 0.559473 0.614705 11.00000 0.02465 0.01953 = 0.02216 0.00733 0.00345 0.01539 AFIX 23 H6AA 2 0.654757 0.599210 0.506580 11.00000 -1.20000 H6AB 2 0.554898 0.550536 0.585022 11.00000 -1.20000 AFIX 0 C7A 1 0.681254 0.472994 0.473013 11.00000 0.01429 0.01466 = 0.01342 0.00065 0.00061 0.00540 AFIX 23 H7AA 2 0.667172 0.481078 0.324816 11.00000 -1.20000 H7AB 2 0.738644 0.523114 0.509008 11.00000 -1.20000 AFIX 0 BR1B 3 0.359689 0.493671 0.235271 11.00000 0.01502 0.03392 = 0.02543 0.00489 0.00290 0.01288 O1B 4 0.138680 0.432081 0.558293 11.00000 0.02347 0.02131 = 0.02315 0.00427 0.00786 0.01229 O2B 4 0.277996 0.612947 0.167902 11.00000 0.02892 0.01170 = 0.01921 0.00217 0.00777 0.00947 AFIX 147 H2B 2 0.320497 0.626809 0.086672 11.00000 -1.50000 AFIX 0 C1B 1 0.241074 0.468376 0.297958 11.00000 0.01101 0.01090 = 0.01511 -0.00109 0.00193 0.00540 C2B 1 0.231586 0.484285 0.538639 11.00000 0.02017 0.01341 = 0.01237 0.00086 0.00169 0.00786 AFIX 13 H2BA 2 0.256632 0.546483 0.580257 11.00000 -1.20000 AFIX 0 C3B 1 0.262280 0.433120 0.672181 11.00000 0.03051 0.02936 = 0.01103 0.00113 -0.00289 0.01848 AFIX 43 H3B 2 0.314441 0.455421 0.752155 11.00000 -1.20000 AFIX 0 C4B 1 0.201460 0.351988 0.653094 11.00000 0.03922 0.02248 = 0.01617 0.00462 0.00218 0.01794 AFIX 43 H4B 2 0.199998 0.303378 0.719878 11.00000 -1.20000 AFIX 0 C5B 1 0.134393 0.350571 0.505151 11.00000 0.02463 0.01264 = 0.02055 0.00474 0.00694 0.00529 AFIX 13 H5B 2 0.075482 0.298063 0.517108 11.00000 -1.20000 AFIX 0 C6B 1 0.173112 0.370834 0.276652 11.00000 0.01814 0.01083 = 0.01878 -0.00104 -0.00099 0.00404 AFIX 23 H6BA 2 0.200646 0.336042 0.240350 11.00000 -1.20000 H6BB 2 0.128597 0.360784 0.168136 11.00000 -1.20000 AFIX 0 C7B 1 0.219348 0.523090 0.150326 11.00000 0.01902 0.01288 = 0.01518 0.00070 0.00258 0.00769 AFIX 23 H7BA 2 0.219177 0.504917 0.000762 11.00000 -1.20000 H7BB 2 0.160244 0.511709 0.183882 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_ca041113_0m in P31 #144 REM R1 = 0.0235 for 6143 Fo > 4sig(Fo) and 0.0255 for all 6360 data REM 275 parameters refined using 1 restraints END WGHT 0.0129 0.0000 REM Instructions for potential hydrogen bonds EQIV $1 x, y, z-1 HTAB C4 O1A_$1 EQIV $2 x, y, z+1 HTAB C3A Br1A_$2 HTAB C4A Br1B_$2 EQIV $3 -y+1, x-y+1, z+2/3 HTAB C4A O1B_$3 HTAB C5A Br1 HTAB C3B Br1B_$2 EQIV $4 -y+1, x-y, z+2/3 HTAB C4B O1_$4 EQIV $5 -y+1, x-y, z-1/3 HTAB C6B O1_$5 REM Highest difference peak 0.742, deepest hole -0.476, 1-sigma level 0.070 Q1 1 0.8201 0.8189 0.7669 11.00000 0.05 0.74 Q2 1 0.3813 0.5383 0.3180 11.00000 0.05 0.71 Q3 1 0.8212 0.8165 0.5131 11.00000 0.05 0.68 Q4 1 0.5024 0.3678 0.6859 11.00000 0.05 0.65 Q5 1 0.5026 0.3761 0.4241 11.00000 0.05 0.63 Q6 1 0.3614 0.5006 0.3660 11.00000 0.05 0.59 Q7 1 0.3639 0.4931 0.0960 11.00000 0.05 0.59 Q8 1 0.7845 0.7656 0.5937 11.00000 0.05 0.43 Q9 1 0.8316 0.7755 0.6842 11.00000 0.05 0.41 Q10 1 0.4834 0.4064 0.5206 11.00000 0.05 0.41 Q11 1 0.8586 0.8622 0.6871 11.00000 0.05 0.39 Q12 1 0.3793 0.4629 0.2708 11.00000 0.05 0.36 Q13 1 0.2223 0.4847 0.2138 11.00000 0.05 0.35 Q14 1 0.4034 0.4862 0.1729 11.00000 0.05 0.32 Q15 1 0.3053 0.4748 0.2741 11.00000 0.05 0.31 Q16 1 0.3447 0.4426 0.2626 11.00000 0.05 0.30 Q17 1 0.5463 0.3825 0.5064 11.00000 0.05 0.30 Q18 1 0.2036 0.4227 0.2679 11.00000 0.05 0.30 Q19 1 0.3437 0.5374 0.2020 11.00000 0.05 0.30 Q20 1 0.2396 0.4789 0.4236 11.00000 0.05 0.30 ; _shelx_res_checksum 22389 _shelx_hkl_file ; -1 1 0 -1.2640 0.35164 2 0 1 0 -0.2425 0.34619 2 -1 0 0 0.93644 0.30849 2 1 -2 0 427.444 17.6139 2 -2 1 0 439.961 17.5111 2 1 1 0 432.396 17.5305 2 -1 -1 0 426.316 17.5242 2 2 -1 0 417.207 17.5086 2 -1 2 0 427.035 17.6500 2 0 -2 0 4.59977 1.39582 2 -2 2 0 4.02842 1.38481 2 2 0 0 3.75987 1.29156 2 0 2 0 4.27521 1.46439 2 2 -2 0 3.98634 1.28932 2 -2 0 0 2.75562 1.19823 2 -3 1 0 510.160 20.6441 2 1 2 0 486.545 20.7216 2 2 -3 0 490.175 20.7845 2 -3 2 0 315.900 13.4373 2 1 -3 0 308.135 13.4174 1 2 1 0 320.458 13.4455 2 1 -3 0 301.080 13.5752 2 0 -3 0 7074.65 271.585 2 -3 3 0 7178.46 270.926 2 0 3 0 6696.82 270.926 2 -3 0 0 6640.45 271.747 2 3 -3 0 6535.38 270.867 2 1 3 0 898.006 40.4499 2 -4 1 0 930.579 40.4052 2 3 -4 0 914.793 40.5481 2 -3 4 0 1131.18 40.7605 2 4 -1 0 1115.17 40.5767 2 2 -4 0 1304.64 53.0326 2 -4 2 0 1329.62 52.7963 2 2 -4 0 1297.80 54.6382 1 2 2 0 1285.78 52.8069 2 -2 -2 0 1333.38 52.8747 2 -2 4 0 1311.22 53.0744 2 -4 3 0 903.461 32.7222 2 1 -4 0 861.995 32.8522 2 3 1 0 883.582 32.6562 2 -1 4 0 714.543 32.7192 2 4 -3 0 726.404 32.5474 2 -3 -1 0 695.056 32.4806 2 4 0 0 320.738 13.3583 2 0 -4 0 338.009 13.5926 2 -4 4 0 313.720 13.5254 2 0 4 0 277.598 13.4967 2 4 -4 0 263.976 13.3030 2 -4 0 0 281.161 13.2204 2 -5 1 0 2422.52 96.8243 2 1 4 0 2369.05 96.9101 2 4 -5 0 2399.38 96.9822 2 -1 -4 0 2464.86 96.9873 2 5 -1 0 2435.11 96.8306 2 3 -5 0 538.546 24.5848 2 2 3 0 542.752 24.3898 2 -5 2 0 538.180 24.2584 2 -2 -3 0 615.232 24.4484 2 5 -2 0 616.348 24.4721 2 -3 5 0 628.301 24.7987 2 3 2 0 824.268 32.9052 2 2 -5 0 827.590 33.1484 2 2 -5 0 794.166 33.4119 1 -2 5 0 767.649 33.1335 2 5 -3 0 762.871 32.8153 2 1 -5 0 2493.11 102.718 2 -5 4 0 2634.15 102.634 2 4 1 0 2555.30 102.527 2 -1 5 0 2567.98 102.818 2 5 0 0 103.471 6.13408 2 0 -5 0 94.8074 6.29473 2 -5 5 0 112.527 6.50489 2 5 -5 0 81.5618 6.13607 2 0 5 0 84.4881 6.71169 2 -5 0 0 85.0800 5.94989 2 5 -6 0 741.190 30.5611 2 1 5 0 733.683 30.5134 2 -6 1 0 704.951 30.2678 2 -5 6 0 702.503 30.5663 2 -1 -5 0 694.639 30.4792 2 6 -1 0 741.871 30.3468 2 -6 2 0 4426.21 179.997 2 4 -6 0 4567.78 180.322 2 -2 -4 0 4552.27 180.123 2 6 -2 0 4527.84 180.040 2 -6 3 0 655.071 27.6424 2 3 3 0 653.133 27.6894 2 3 -6 0 670.647 27.9742 1 3 -6 0 645.883 27.9959 2 6 -3 0 667.863 27.7766 2 -3 -3 0 653.866 27.6953 2 -3 6 0 664.356 28.0435 2 2 -6 0 4009.70 165.845 2 2 -6 0 4011.42 172.110 1 -6 4 0 4122.11 165.668 2 4 2 0 4084.06 165.618 2 6 -4 0 4351.13 165.780 2 -2 6 0 4258.82 166.014 2 -4 -2 0 4242.35 165.731 2 -6 5 0 1035.35 43.2216 2 1 -6 0 1040.07 43.3940 2 5 1 0 1039.81 43.1213 2 -1 6 0 1070.87 43.5059 2 6 0 0 5651.65 219.482 2 0 -6 0 5469.09 219.632 2 -6 6 0 5324.81 219.524 2 0 6 0 5550.11 219.717 2 -6 0 0 5487.85 219.467 2 6 -6 0 5590.27 219.642 2 1 6 0 323.176 15.5684 2 -7 1 0 320.177 15.1301 2 6 -7 0 304.940 15.3731 2 -6 7 0 341.300 15.6172 2 -1 -6 0 327.871 15.4223 2 -7 2 0 243.700 11.8878 2 5 -7 0 250.969 12.3090 2 2 5 0 232.822 12.2528 2 -5 7 0 233.696 12.5071 2 7 -2 0 245.736 11.9752 2 -2 -5 0 234.524 12.0338 2 3 4 0 1807.24 71.4457 2 4 -7 0 1736.58 71.6363 2 -7 3 0 1709.44 71.2447 2 4 -7 0 1774.78 73.6287 1 -3 -4 0 1745.32 71.3696 2 7 -3 0 1786.64 71.3256 2 -4 7 0 1753.63 71.6796 2 -7 4 0 2005.13 75.8112 2 3 -7 0 1839.58 77.8894 1 4 3 0 1829.05 75.6769 2 3 -7 0 1829.57 76.0023 2 7 -4 0 1842.58 75.7096 2 -3 7 0 1861.70 76.0564 2 -4 -3 0 1888.19 75.7453 2 2 -7 0 392.973 18.3080 2 5 2 0 397.418 17.9555 2 -7 5 0 393.452 18.0149 2 -5 -2 0 413.556 17.9996 2 -2 7 0 396.699 18.5101 2 7 -5 0 399.156 18.1033 2 -7 6 0 268.211 13.4075 2 1 -7 0 279.503 13.6429 2 6 1 0 284.527 13.4700 2 -1 7 0 265.404 13.6979 2 7 -6 0 265.915 13.3557 2 0 -7 0 88.1157 7.00426 2 -7 7 0 80.3204 6.88667 2 7 0 0 84.4430 6.80157 2 -7 0 0 63.3557 5.68239 2 0 7 0 64.0786 6.21882 2 7 -7 0 67.0169 6.20542 2 -8 1 0 1314.12 51.5887 2 1 7 0 1348.87 51.9727 2 7 -8 0 1373.04 51.9853 2 8 -1 0 1144.90 51.3348 2 -1 -7 0 1179.83 51.6115 2 -7 8 0 1120.59 51.5559 2 -8 2 0 421.211 20.2626 2 6 -8 0 401.809 20.5531 2 2 6 0 413.253 20.4526 2 -6 8 0 517.159 21.0428 2 8 -2 0 511.184 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1678.79 69.5928 2 7 4 0 165.447 10.6056 2 4 -11 0 156.682 10.9885 2 -11 7 0 174.057 10.9834 2 11 -7 0 143.420 10.4863 2 -7 -4 0 134.476 10.2375 2 -4 11 0 123.511 10.9388 2 8 3 0 1027.68 42.3346 2 3 -11 0 985.393 42.7118 2 -11 8 0 987.998 42.4349 2 -3 11 0 955.068 42.8209 2 -8 -3 0 981.963 42.1623 2 -11 9 0 647.827 30.1903 2 9 2 0 654.475 29.9674 2 2 -11 0 641.826 30.4789 2 11 -9 0 698.421 30.2461 2 -2 11 0 668.158 30.7223 2 -9 -2 0 712.453 30.0731 2 1 -11 0 801.117 34.0156 2 -11 10 0 826.979 33.8564 2 10 1 0 763.178 33.3942 2 -10 -1 0 704.486 33.2513 2 -1 11 0 731.267 33.9238 2 11 -10 0 702.626 33.3977 2 -11 11 0 121.431 11.0971 2 0 -11 0 103.814 9.84048 2 11 0 0 118.659 10.9303 2 11 -11 0 160.627 11.6327 2 0 11 0 162.671 11.9354 2 -11 0 0 156.527 11.0561 2 11 -12 0 710.077 32.0368 2 1 11 0 663.257 32.1212 2 -12 1 0 707.241 31.4470 2 12 -1 0 700.085 31.6203 2 -11 12 0 687.205 32.1842 2 -1 -11 0 683.741 31.7887 2 -12 2 0 3008.09 121.509 2 2 10 0 2968.19 121.868 2 10 -12 0 2982.12 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1290.05 54.4141 2 4 -12 0 1380.99 55.1080 2 -4 12 0 1270.16 54.8752 2 12 -8 0 1223.66 54.2428 2 -8 -4 0 1287.11 54.3454 2 -12 9 0 130.451 11.0838 2 3 -12 0 118.626 10.3827 2 9 3 0 135.776 11.2370 2 12 -9 0 166.426 11.1387 2 -9 -3 0 153.055 10.9813 2 -3 12 0 142.816 12.1259 2 10 2 0 2526.57 103.696 2 2 -12 0 2438.02 104.017 2 -12 10 0 2582.33 103.894 2 12 -10 0 2599.49 103.968 2 -10 -2 0 2533.95 103.655 2 -2 12 0 2541.73 104.243 2 11 1 0 1011.63 44.6243 2 -12 11 0 1052.33 45.1095 2 1 -12 0 1026.76 45.1130 2 -1 12 0 1031.73 45.3465 2 12 -11 0 1052.60 45.0032 2 -11 -1 0 1022.25 44.6724 2 -12 12 0 87.9844 9.04499 2 0 -12 0 77.8833 8.60881 2 12 0 0 74.1709 7.90766 2 0 12 0 53.3534 8.31147 2 12 -12 0 60.7091 8.00936 2 -12 0 0 65.1388 7.71674 2 12 -13 0 123.991 10.6755 2 -13 1 0 90.0051 8.96901 2 1 12 0 94.2420 10.2903 2 -1 -12 0 106.553 10.1554 2 -12 13 0 83.5835 9.80845 2 13 -1 0 82.3352 9.09962 2 2 11 0 193.752 14.2254 2 -13 2 0 193.615 13.0191 2 11 -13 0 177.127 13.4587 2 -11 13 0 178.753 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525.121 26.8026 2 -13 8 0 546.192 26.7778 2 5 -13 0 521.157 27.1742 2 13 -8 0 589.042 26.9563 2 -5 13 0 621.255 27.8341 2 -8 -5 0 611.724 26.7205 2 4 -13 0 885.697 38.9275 2 -13 9 0 893.453 38.5494 2 9 4 0 851.588 38.2929 2 13 -9 0 886.755 38.5587 2 -9 -4 0 845.892 38.2007 2 -4 13 0 843.269 38.9369 2 3 -13 0 413.854 21.4171 2 10 3 0 417.746 20.7325 2 -13 10 0 402.568 21.1691 2 -3 13 0 396.054 21.6145 2 13 -10 0 409.846 21.0634 2 -10 -3 0 386.430 20.3665 2 2 -13 0 135.974 12.2424 2 11 2 0 139.004 12.0396 2 -13 11 0 128.018 11.1475 2 -11 -2 0 161.367 12.2366 2 -2 13 0 162.442 12.6007 2 13 -11 0 177.507 12.3674 2 12 1 0 45.3868 7.35713 2 -13 12 0 51.7524 8.26688 2 1 -13 0 38.4656 7.52395 2 -12 -1 0 46.2874 7.27905 2 13 -12 0 56.8507 7.96016 2 -1 13 0 70.7079 9.14852 2 -13 13 0 139.446 12.0044 2 13 0 0 155.781 12.6497 2 0 -13 0 172.399 13.2940 2 -13 0 0 149.867 12.4366 2 13 -13 0 145.587 12.8113 2 0 13 0 143.269 12.3018 2 1 13 0 545.079 26.7392 2 -14 1 0 561.625 25.2813 2 13 -14 0 537.654 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344.161 21.1612 2 -1 14 0 379.591 21.4095 2 14 -13 0 388.330 21.1872 2 -13 -1 0 412.206 20.4792 2 -14 14 0 598.252 28.9308 2 0 -14 0 583.724 28.4360 2 14 0 0 596.917 28.2177 2 0 14 0 561.266 28.9756 2 -14 0 0 498.658 27.2053 2 14 -14 0 533.897 27.9468 2 14 -15 0 93.9825 10.9619 2 -15 1 0 113.296 11.0582 2 1 14 0 97.8063 11.8678 2 -1 -14 0 116.444 11.5938 2 15 -1 0 92.4682 10.4710 2 -14 15 0 101.268 11.3918 2 2 13 0 580.782 29.1971 2 13 -15 0 576.770 28.4809 2 -15 2 0 600.364 27.8129 2 -2 -13 0 512.381 28.0943 2 15 -2 0 520.245 27.6484 2 3 12 0 279.475 17.8540 2 -15 3 0 246.901 16.5070 2 12 -15 0 246.865 17.3915 2 15 -3 0 254.693 16.8480 2 -12 15 0 237.550 17.8216 2 -3 -12 0 236.973 16.7573 2 11 -15 0 266.914 14.7431 1 4 11 0 267.847 17.5891 2 11 -15 0 287.298 17.6729 2 -15 4 0 256.222 16.4760 2 -11 15 0 257.389 18.0963 2 -4 -11 0 266.712 16.9898 2 15 -4 0 245.343 16.9335 2 10 -15 0 256.995 17.7236 2 5 10 0 264.533 17.9527 2 -15 5 0 256.447 16.4027 2 -15 5 0 281.850 16.8104 2 10 -15 0 262.388 14.0512 1 -5 -10 0 267.481 16.7987 2 15 -5 0 276.772 16.6262 2 -10 15 0 276.440 18.1468 2 -15 6 0 96.4014 9.97671 2 9 -15 0 93.8830 10.1773 2 9 -15 0 94.5119 7.12747 1 6 9 0 110.867 10.7103 2 -6 -9 0 99.5243 10.1324 2 -9 15 0 104.125 11.0871 2 15 -6 0 85.1935 9.36095 2 8 -15 0 1316.69 56.2518 2 7 8 0 1336.80 55.9367 2 8 -15 0 1238.10 54.5742 1 -15 7 0 1294.98 55.5686 2 -7 -8 0 1277.03 55.7497 2 15 -7 0 1265.29 55.4399 2 -8 15 0 1332.76 56.2439 2 -15 8 0 1086.96 47.2469 2 7 -15 0 1073.33 47.6543 2 8 7 0 1081.03 47.2748 2 -8 -7 0 1045.76 46.9924 2 15 -8 0 1087.99 47.0721 2 -7 15 0 1052.89 47.5097 2 9 6 0 117.886 10.9832 2 6 -15 0 118.164 11.1524 2 -15 9 0 85.7593 9.88799 2 15 -9 0 142.095 11.2937 2 -6 15 0 122.024 11.5502 2 -9 -6 0 93.1138 9.61736 2 10 5 0 304.179 17.8266 2 -15 10 0 288.904 17.6273 2 5 -15 0 297.449 18.3521 2 -5 15 0 253.465 18.4219 2 15 -10 0 297.370 17.3030 2 -10 -5 0 272.479 16.9903 2 -15 11 0 206.854 15.6569 2 11 4 0 204.792 15.1865 2 4 -15 0 207.907 15.5898 2 -4 15 0 205.535 16.4485 2 15 -11 0 214.258 15.3665 2 -11 -4 0 201.949 14.5169 2 -15 12 0 178.840 15.2768 2 3 -15 0 203.312 15.1149 2 12 3 0 202.626 14.7231 2 15 -12 0 204.208 15.1805 2 -3 15 0 183.705 15.7215 2 -12 -3 0 184.614 14.2068 2 2 -15 0 772.899 36.4330 2 13 2 0 772.392 35.8412 2 -15 13 0 784.359 36.3694 2 -2 15 0 744.023 36.3616 2 -13 -2 0 747.973 35.3824 2 15 -13 0 768.270 35.9137 2 14 1 0 100.918 10.8060 2 1 -15 0 123.170 11.9752 2 -15 14 0 116.500 11.5830 2 15 -14 0 102.538 11.2139 2 -1 15 0 88.0322 11.4063 2 -14 -1 0 110.217 11.0523 2 15 0 0 18.4286 7.80241 2 0 -15 0 29.4699 8.80053 2 -15 15 0 23.0068 9.15460 2 0 15 0 26.0516 9.40939 2 -15 0 0 10.0845 7.18670 2 15 -15 0 35.7573 8.79956 2 15 -16 0 131.385 12.7850 2 1 15 0 99.2255 12.5520 2 -16 1 0 106.239 11.2961 2 16 -1 0 117.413 11.8221 2 -15 16 0 89.2770 11.8863 2 -1 -15 0 102.932 11.7672 2 14 -16 0 140.629 13.0925 2 2 14 0 135.169 13.3557 2 -16 2 0 126.343 11.9458 2 -14 16 0 118.621 12.5920 2 -2 -14 0 122.474 12.4021 2 16 -2 0 115.706 11.6756 2 3 13 0 130.450 13.3820 2 -16 3 0 133.904 12.2315 2 13 -16 0 148.323 12.2209 1 13 -16 0 165.772 14.0455 2 -3 -13 0 153.743 13.3610 2 -13 16 0 156.404 13.8898 2 16 -3 0 155.226 12.7735 2 -16 4 0 432.747 22.6231 2 12 -16 0 402.522 23.7057 2 12 -16 0 413.569 20.9490 1 4 12 0 418.837 23.9659 2 16 -4 0 399.636 22.8611 2 -12 16 0 404.862 23.6098 2 -4 -12 0 438.454 23.5080 2 11 -16 0 219.230 13.1951 1 -16 5 0 214.210 16.2264 2 -16 5 0 215.509 16.4650 2 11 -16 0 232.290 16.9066 2 5 11 0 218.374 17.5968 2 -5 -11 0 275.077 17.1753 2 -11 16 0 270.453 17.7414 2 16 -5 0 271.168 16.9308 2 6 10 0 376.354 22.2701 2 -16 6 0 348.250 20.8955 2 10 -16 0 350.894 21.7775 2 -6 -10 0 402.425 21.6097 2 -10 16 0 378.972 22.4227 2 16 -6 0 391.048 21.4044 2 -16 7 0 282.761 17.8682 2 9 -16 0 284.531 18.5798 2 7 9 0 290.017 19.0990 2 16 -7 0 290.597 17.9476 2 -9 16 0 297.150 18.9393 2 -7 -9 0 288.200 18.4271 2 -16 8 0 514.363 26.5297 2 8 -16 0 519.949 26.9417 2 8 8 0 527.103 26.7763 2 -8 -8 0 530.764 26.3369 2 16 -8 0 494.633 25.8796 2 -8 16 0 496.434 27.0878 2 -16 9 0 151.017 12.7790 2 9 7 0 159.715 12.7906 2 7 -16 0 156.784 13.3806 2 16 -9 0 158.539 13.3582 2 -7 16 0 135.945 12.8802 2 -9 -7 0 143.542 12.0308 2 -16 10 0 500.324 25.5771 2 6 -16 0 484.669 26.0569 2 10 6 0 499.265 25.9402 2 -6 16 0 469.009 26.3458 2 -10 -6 0 495.720 25.0661 2 16 -10 0 492.837 25.2743 2 -16 11 0 136.463 12.0569 2 11 5 0 148.989 12.2019 2 5 -16 0 145.575 12.3504 2 16 -11 0 111.401 11.1697 2 -5 16 0 117.726 12.0949 2 -11 -5 0 88.3232 10.3052 2 12 4 0 314.227 19.6960 2 4 -16 0 346.426 19.8454 2 -16 12 0 287.214 19.8058 2 16 -12 0 336.265 19.7286 2 -4 16 0 299.302 20.1731 2 -12 -4 0 307.946 19.1342 2 -16 13 0 206.051 16.8832 2 13 3 0 195.667 16.0901 2 3 -16 0 197.533 16.6784 2 -3 16 0 201.377 17.4732 2 -13 -3 0 191.952 15.0508 2 16 -13 0 201.211 15.6338 2 -16 14 0 139.196 13.3264 2 2 -16 0 114.560 12.6734 2 14 2 0 129.752 12.6733 2 -14 -2 0 149.096 12.6487 2 -2 16 0 167.043 14.2415 2 16 -14 0 181.305 14.9364 2 -16 15 0 179.661 14.7997 2 15 1 0 168.671 14.9839 2 1 -16 0 176.328 14.9061 2 -15 -1 0 144.374 13.0258 2 -1 16 0 161.341 14.7024 2 16 -15 0 172.480 14.6532 2 -16 16 0 1450.57 62.2415 2 0 -16 0 1375.66 61.9431 2 16 0 0 1464.74 61.4610 2 16 -16 0 1413.53 61.9420 2 -16 0 0 1357.97 61.0486 2 0 16 0 1355.20 62.2352 2 -17 1 0 132.399 13.1560 2 16 -17 0 168.598 14.9002 2 1 16 0 137.956 14.8226 2 -1 -16 0 156.978 14.6210 2 17 -1 0 157.086 14.0746 2 -16 17 0 162.292 15.0644 2 15 -17 0 121.621 12.9375 2 -17 2 0 104.649 11.6393 2 2 15 0 112.276 13.4114 2 -15 17 0 97.3566 12.6617 2 -2 -15 0 115.821 12.5830 2 17 -2 0 106.139 11.8851 2 3 14 0 523.811 29.9879 2 14 -17 0 534.432 27.4358 1 14 -17 0 548.910 29.2533 2 -17 3 0 514.991 28.3849 2 -14 17 0 611.484 30.1546 2 17 -3 0 563.460 28.8267 2 -3 -14 0 580.570 29.4588 2 -17 4 0 211.112 15.8679 2 13 -17 0 181.237 14.9781 2 -17 4 0 209.394 16.1748 2 4 13 0 162.131 14.8073 2 13 -17 0 167.854 12.5331 1 17 -4 0 164.601 14.2020 2 -4 -13 0 160.251 14.0180 2 -13 17 0 167.576 14.9321 2 -17 5 0 338.085 20.5048 2 12 -17 0 320.826 21.1625 2 -17 5 0 327.149 20.6039 2 5 12 0 352.137 21.9441 2 -12 17 0 350.137 21.9018 2 17 -5 0 391.277 21.3402 2 -5 -12 0 344.042 21.0096 2 6 11 0 189.623 15.0673 2 -17 6 0 180.109 14.6165 2 11 -17 0 165.175 14.4429 2 -6 -11 0 170.911 15.1222 2 17 -6 0 178.264 14.0749 2 -11 17 0 185.386 16.4682 2 10 -17 0 236.750 17.7422 2 7 10 0 264.865 18.0437 2 -17 7 0 243.749 16.8864 2 -10 17 0 182.553 15.8108 2 -7 -10 0 207.971 16.2921 2 17 -7 0 192.936 16.2714 2 8 9 0 65.7477 10.1857 2 9 -17 0 72.1848 10.1055 2 -17 8 0 67.0819 9.87967 2 -8 -9 0 63.5919 9.51426 2 -9 17 0 68.2247 10.5868 2 17 -8 0 80.2970 10.0674 2 9 8 0 91.6496 11.4223 2 8 -17 0 93.8256 11.1119 2 -17 9 0 107.085 11.3004 2 -8 17 0 76.7863 11.0145 2 17 -9 0 81.6082 10.2726 2 -9 -8 0 76.4742 9.78663 2 7 -17 0 272.840 19.0142 2 10 7 0 243.832 19.0598 2 -17 10 0 271.968 18.9636 2 -10 -7 0 314.125 18.9187 2 -7 17 0 308.935 20.2286 2 17 -10 0 301.472 18.7098 2 6 -17 0 226.656 17.4424 2 -17 11 0 210.724 16.9024 2 11 6 0 227.380 17.4237 2 -6 17 0 218.588 18.1420 2 -11 -6 0 242.844 16.6213 2 17 -11 0 217.095 16.4669 2 5 -17 0 553.627 26.8681 2 -17 12 0 504.968 26.5910 2 12 5 0 486.304 26.3471 2 -5 17 0 474.309 27.0773 2 -12 -5 0 444.500 25.2871 2 17 -12 0 465.691 25.9082 2 -17 13 0 103.540 11.8536 2 13 4 0 89.2598 11.2943 2 4 -17 0 97.7620 11.8889 2 -4 17 0 103.691 12.4592 2 17 -13 0 110.814 11.5089 2 -13 -4 0 103.791 11.3267 2 -17 14 0 376.243 24.1439 2 3 -17 0 434.688 24.2571 2 14 3 0 466.852 24.4815 2 -14 -3 0 396.312 23.3282 2 -3 17 0 426.139 25.1802 2 17 -14 0 378.502 23.8331 2 2 -17 0 204.367 17.8130 2 15 2 0 222.552 17.5799 2 -17 15 0 226.131 18.0576 2 17 -15 0 211.483 17.1617 2 -2 17 0 191.398 16.5322 2 -15 -2 0 200.100 16.7496 2 16 1 0 208.694 18.0818 2 1 -17 0 246.894 19.6178 2 -17 16 0 240.362 19.4248 2 -16 -1 0 222.520 17.8823 2 -1 17 0 240.522 20.5818 2 17 -16 0 259.455 19.2213 2 0 -17 0 204.050 17.0037 2 17 0 0 170.192 15.3859 2 -17 17 0 180.959 16.5214 2 -17 0 0 214.913 16.9995 2 17 -17 0 209.162 17.1172 2 0 17 0 194.027 17.0015 2 1 17 0 97.3452 14.0757 2 -18 1 0 75.2672 11.4021 2 17 -18 0 71.8266 11.9123 2 18 -1 0 90.5740 11.8839 2 -1 -17 0 62.6635 11.4997 2 -17 18 0 87.5942 12.9862 2 2 16 0 285.346 21.6467 2 16 -18 0 288.939 18.9170 1 -18 2 0 289.500 20.2510 2 16 -18 0 272.151 21.1410 2 -2 -16 0 275.777 20.4408 2 -16 18 0 278.083 21.4601 2 18 -2 0 281.106 19.9974 2 15 -18 0 233.040 19.5384 2 3 15 0 251.468 20.0594 2 -18 3 0 228.645 18.3064 2 -3 -15 0 243.434 19.1011 2 -15 18 0 215.772 18.0226 2 18 -3 0 244.028 18.8284 2 14 -18 0 328.875 22.0686 2 4 14 0 323.259 22.7563 2 -18 4 0 321.721 20.2400 2 -18 4 0 318.999 20.3997 2 18 -4 0 281.434 20.1997 2 -14 18 0 290.272 21.2900 2 -4 -14 0 318.611 21.1560 2 -18 5 0 153.395 14.0913 2 13 -18 0 186.645 15.2092 2 5 13 0 140.022 14.5827 2 -18 5 0 164.701 14.4005 2 18 -5 0 131.772 13.1873 2 -13 18 0 157.055 14.8933 2 -5 -13 0 153.149 14.1100 2 12 -18 0 551.837 28.7563 2 -18 6 0 536.911 28.3240 2 6 12 0 493.631 29.2274 2 -12 18 0 537.272 29.5908 2 -6 -12 0 546.981 28.6588 2 18 -6 0 522.547 28.2466 2 11 -18 0 330.566 21.5320 2 7 11 0 337.676 21.9488 2 -18 7 0 301.262 20.3970 2 -11 18 0 305.975 21.6151 2 18 -7 0 321.829 20.1919 2 -7 -11 0 294.961 20.2330 2 -18 8 0 648.595 32.2925 2 8 10 0 651.232 32.6819 2 10 -18 0 656.631 32.7797 2 18 -8 0 619.132 31.9480 2 -8 -10 0 615.167 31.7830 2 -10 18 0 648.766 33.1549 2 9 -18 0 420.891 24.8277 2 -18 9 0 429.928 24.1931 2 9 9 0 398.176 24.6963 2 -9 -9 0 408.216 24.0041 2 18 -9 0 440.714 24.4297 2 -9 18 0 466.968 25.0406 2 -18 10 0 362.447 22.4372 2 8 -18 0 358.169 23.0059 2 10 8 0 379.105 23.1461 2 -8 18 0 356.782 23.5583 2 18 -10 0 381.492 22.1307 2 -10 -8 0 382.355 21.9510 2 7 -18 0 450.605 25.8212 2 -18 11 0 447.704 25.5430 2 11 7 0 445.961 25.7963 2 -7 18 0 491.304 26.5470 2 -11 -7 0 432.412 24.9046 2 18 -11 0 452.767 24.9376 2 12 6 0 520.075 27.3866 2 -18 12 0 556.060 28.3629 2 6 -18 0 520.092 28.4781 2 -6 18 0 524.475 28.6969 2 18 -12 0 489.110 27.4976 2 -12 -6 0 476.653 27.0490 2 13 5 0 227.674 18.0582 2 5 -18 0 221.215 18.1950 2 -18 13 0 231.778 18.6328 2 -5 18 0 207.033 17.1721 2 -13 -5 0 213.745 17.1192 2 18 -13 0 198.624 16.9096 2 14 4 0 280.179 20.3399 2 4 -18 0 256.689 20.4565 2 -18 14 0 244.772 20.5027 2 -4 18 0 290.935 21.1181 2 -14 -4 0 276.430 18.9733 2 18 -14 0 340.229 20.5999 2 3 -18 0 325.980 21.7287 2 -18 15 0 295.826 21.7463 2 15 3 0 277.093 20.3928 2 18 -15 0 299.838 20.7036 2 -3 18 0 270.746 21.6555 2 -15 -3 0 287.061 19.9535 2 16 2 0 191.765 15.8975 2 -18 16 0 212.550 18.5000 2 2 -18 0 212.622 18.6178 2 -16 -2 0 169.969 15.1073 2 -2 18 0 161.881 16.1402 2 18 -16 0 191.867 16.3436 2 -18 17 0 98.4195 13.4819 2 17 1 0 98.2781 12.7401 2 1 -18 0 117.635 13.7493 2 18 -17 0 110.137 13.0666 2 -17 -1 0 128.814 13.2712 2 -1 18 0 128.611 14.8690 2 -18 18 0 21.1712 11.2503 2 0 -18 0 6.37201 9.82224 2 18 0 0 19.5411 10.1385 2 18 -18 0 19.5320 9.90954 2 -18 0 0 15.1399 9.35723 2 0 18 0 1.78025 11.0528 2 -19 1 0 114.699 13.4173 2 18 -19 0 96.9862 13.7556 2 1 18 0 90.0126 14.7372 2 -1 -18 0 86.9080 13.3224 2 19 -1 0 132.241 14.0902 2 -18 19 0 125.672 15.3424 2 17 -19 0 192.014 17.1145 2 2 17 0 158.059 17.0832 2 -19 2 0 200.149 17.5021 2 -17 19 0 217.678 18.2963 2 -2 -17 0 168.834 16.1072 2 19 -2 0 186.293 16.2382 2 16 -19 0 302.592 22.5934 2 -19 3 0 298.444 21.1483 2 3 16 0 313.417 23.8634 2 -3 -16 0 324.979 22.1409 2 -16 19 0 314.177 23.4981 2 19 -3 0 283.028 21.4424 2 -19 4 0 66.0911 10.7211 2 4 15 0 61.1248 12.5663 2 -19 4 0 43.9648 10.2906 2 15 -19 0 75.9861 11.9158 2 -15 19 0 69.3466 12.4059 2 -4 -15 0 50.4708 10.9274 2 19 -4 0 60.3365 11.0028 2 5 14 0 244.546 20.6797 2 -19 5 0 235.780 18.4892 2 -19 5 0 201.947 18.5378 2 14 -19 0 247.353 19.8712 2 -14 19 0 213.472 18.1170 2 -5 -14 0 219.654 19.0598 2 19 -5 0 251.807 18.3313 2 13 -19 0 149.726 14.7367 2 -19 6 0 144.770 14.2007 2 6 13 0 162.455 15.5059 2 -13 19 0 186.186 16.1621 2 19 -6 0 160.501 14.5689 2 -6 -13 0 152.397 14.7077 2 7 12 0 31.0503 10.5202 2 -19 7 0 22.3953 9.07721 2 12 -19 0 36.5878 9.88600 2 -12 19 0 17.1652 9.89676 2 -7 -12 0 23.4789 9.45945 2 19 -7 0 15.2311 9.09705 2 -19 8 0 101.126 12.4164 2 11 -19 0 102.151 12.7736 2 8 11 0 106.026 13.0161 2 19 -8 0 115.160 12.3089 2 -11 19 0 91.1346 12.8628 2 -8 -11 0 119.962 13.1848 2 -19 9 0 12.0349 9.13984 2 10 -19 0 20.7868 9.11299 2 9 10 0 12.5905 9.41490 2 -9 -10 0 23.5941 8.73101 2 -10 19 0 25.1501 10.0361 2 19 -9 0 19.7675 8.71946 2 10 9 0 5.39835 9.26248 2 -19 10 0 22.3414 9.24696 2 9 -19 0 17.9432 9.07848 2 -9 19 0 15.2597 10.2350 2 19 -10 0 0.41622 7.71087 2 -10 -9 0 8.47880 7.99470 2 11 8 0 119.996 13.5076 2 -19 11 0 144.659 13.9082 2 8 -19 0 127.834 13.6316 2 -8 19 0 109.591 13.3542 2 19 -11 0 116.758 12.5964 2 -11 -8 0 129.703 13.0870 2 -19 12 0 44.2208 10.3445 2 12 7 0 52.9713 10.4954 2 7 -19 0 46.2053 10.4642 2 -12 -7 0 44.7017 9.57189 2 19 -12 0 38.1489 9.61843 2 -7 19 0 49.3173 10.9605 2 13 6 0 155.732 14.4885 2 6 -19 0 152.961 14.8596 2 -19 13 0 172.365 15.3008 2 19 -13 0 139.699 13.7293 2 -6 19 0 146.435 14.9885 2 -13 -6 0 136.377 13.4642 2 5 -19 0 209.677 17.4885 2 14 5 0 223.011 18.9281 2 -19 14 0 198.714 16.9860 2 -14 -5 0 207.827 17.7944 2 -5 19 0 219.890 18.0290 2 19 -14 0 224.183 17.7706 2 -19 15 0 46.4449 11.2861 2 15 4 0 69.6519 11.5574 2 4 -19 0 46.4371 10.9893 2 19 -15 0 59.7223 10.7943 2 -15 -4 0 46.2135 10.0673 2 -4 19 0 73.1955 12.3190 2 3 -19 0 245.251 20.4958 2 -19 16 0 270.293 21.4467 2 16 3 0 262.911 20.3429 2 -3 19 0 244.640 21.6226 2 19 -16 0 241.130 19.8979 2 -16 -3 0 221.412 18.6872 2 2 -19 0 181.205 16.8006 2 17 2 0 176.395 15.6521 2 -19 17 0 167.365 16.9722 2 19 -17 0 202.598 16.6855 2 -2 19 0 160.188 16.9756 2 -17 -2 0 165.799 15.2791 2 -19 18 0 64.0244 12.8635 2 18 1 0 75.5186 12.5861 2 1 -19 0 75.5365 12.7941 2 -18 -1 0 73.6523 11.8136 2 -1 19 0 82.3462 13.6699 2 19 -18 0 87.2086 12.9485 2 19 0 0 301.488 22.7381 2 0 -19 0 319.178 23.3827 2 -19 19 0 279.936 24.0981 2 -19 0 0 312.993 22.3752 2 19 -19 0 288.074 23.1649 2 0 19 0 279.788 24.7695 2 1 19 0 221.028 20.8894 2 -20 1 0 259.298 21.0048 2 19 -20 0 256.793 22.4496 2 -1 -19 0 239.305 19.9849 2 20 -1 0 227.931 19.0832 2 -19 20 0 245.068 20.7275 2 18 -20 0 251.113 20.3310 2 2 18 0 230.214 20.3267 2 -20 2 0 266.300 20.6029 2 20 -2 0 233.847 21.1677 2 -2 -18 0 235.901 19.7044 2 -18 20 0 272.889 23.8567 2 3 17 0 160.615 16.8281 2 17 -20 0 175.034 16.4095 2 -20 3 0 134.595 14.4101 2 -20 3 0 148.088 14.9578 2 -3 -17 0 130.302 14.7704 2 -17 20 0 111.257 15.2796 2 20 -3 0 128.339 14.5284 2 4 16 0 213.106 18.6125 2 -20 4 0 207.553 17.5584 2 -20 4 0 199.019 18.0087 2 16 -20 0 205.979 18.0250 2 -4 -16 0 189.139 17.2602 2 20 -4 0 221.612 17.6115 2 -16 20 0 225.440 18.8040 2 -20 5 0 90.5010 12.2506 2 5 15 0 77.5023 13.6110 2 15 -20 0 96.5904 13.0860 2 -20 5 0 97.3485 12.6906 2 20 -5 0 66.9390 11.7052 2 -15 20 0 118.718 14.5766 2 -5 -15 0 84.9382 12.6732 2 -20 6 0 156.130 15.0438 2 6 14 0 163.955 16.8450 2 14 -20 0 182.581 16.5174 2 -6 -14 0 158.191 15.5238 2 -14 20 0 175.534 16.4677 2 20 -6 0 207.527 16.6762 2 -20 7 0 319.718 21.8475 2 7 13 0 307.573 23.3432 2 13 -20 0 298.037 21.4425 2 -13 20 0 304.807 23.0562 2 20 -7 0 289.425 21.5396 2 -7 -13 0 285.042 21.8919 2 8 12 0 112.539 13.6661 2 -20 8 0 86.1666 12.3791 2 12 -20 0 94.5968 12.6388 2 -8 -12 0 103.978 12.9627 2 -12 20 0 92.4730 13.2353 2 20 -8 0 101.948 12.5719 2 9 11 0 95.9346 12.8678 2 -20 9 0 83.0956 12.2241 2 11 -20 0 100.453 12.5577 2 -11 20 0 74.1781 12.4120 2 20 -9 0 84.1613 11.8243 2 -9 -11 0 72.0344 11.3699 2 10 10 0 668.357 34.6481 2 10 -20 0 677.937 34.5254 2 -20 10 0 699.965 34.0286 2 -10 -10 0 615.254 33.1676 2 -10 20 0 614.398 34.7409 2 20 -10 0 653.852 33.5771 2 11 9 0 152.933 15.1760 2 -20 11 0 131.898 14.3894 2 9 -20 0 139.535 14.7035 2 20 -11 0 140.114 13.9507 2 -9 20 0 148.950 15.0701 2 -11 -9 0 135.922 14.0059 2 12 8 0 120.521 13.8528 2 8 -20 0 138.270 14.3201 2 -20 12 0 119.199 14.0273 2 -12 -8 0 121.818 13.1982 2 -8 20 0 130.002 14.4545 2 20 -12 0 109.754 13.0151 2 -20 13 0 299.294 21.7780 2 7 -20 0 321.744 22.4060 2 13 7 0 292.684 22.1902 2 -13 -7 0 322.244 21.4599 2 20 -13 0 276.762 21.3158 2 -7 20 0 334.313 23.2405 2 -20 14 0 101.439 13.4426 2 6 -20 0 122.153 14.1443 2 14 6 0 112.165 13.7486 2 -6 20 0 128.670 14.9830 2 -14 -6 0 118.987 13.4087 2 20 -14 0 147.441 14.5760 2 5 -20 0 31.1537 10.9531 2 15 5 0 41.2719 10.9965 2 -20 15 0 45.3832 12.0965 2 -5 20 0 40.2032 11.9987 2 20 -15 0 48.2127 11.0458 2 -15 -5 0 39.7361 10.2614 2 16 4 0 258.944 21.3370 2 -20 16 0 271.267 22.6868 2 4 -20 0 275.913 21.6422 2 -16 -4 0 286.775 20.9065 2 20 -16 0 265.301 21.4747 2 -4 20 0 305.012 23.3875 2 -20 17 0 257.274 20.2750 2 17 3 0 176.221 17.1073 2 3 -20 0 230.837 19.0409 2 -17 -3 0 259.762 20.0134 2 -3 20 0 210.054 19.1208 2 20 -17 0 215.872 17.9822 2 2 -20 0 175.470 17.0532 2 -20 18 0 166.629 17.1977 2 18 2 0 159.811 16.2812 2 -2 20 0 178.413 17.8295 2 20 -18 0 173.551 16.5919 2 -18 -2 0 188.253 16.4377 2 1 -20 0 112.292 15.1079 2 -20 19 0 106.898 15.4731 2 19 1 0 125.332 15.0551 2 -1 20 0 107.625 15.9435 2 -19 -1 0 135.234 14.6761 2 20 -19 0 148.583 15.7827 2 0 -20 0 18.1085 11.1706 2 -20 20 0 11.0683 12.4268 2 20 -20 0 19.8532 11.5123 2 -20 0 0 5.91334 10.1607 2 20 -21 0 28.5531 12.2123 2 -21 1 0 23.0263 11.4540 2 -1 -20 0 57.0707 13.2258 2 -21 2 0 157.103 16.1515 2 19 -21 0 175.367 17.9165 2 -19 21 0 191.015 18.9720 2 -2 -19 0 175.830 17.6303 2 -21 3 0 140.497 14.6727 2 18 -21 0 127.992 15.5948 2 -21 3 0 122.153 14.7399 2 -3 -18 0 115.887 15.0016 2 21 -3 0 109.702 14.7395 2 -18 21 0 123.650 16.1631 2 17 -21 0 116.806 14.6906 2 -21 4 0 100.453 13.9862 2 4 17 0 109.699 15.9259 2 -21 4 0 98.8157 13.2452 2 21 -4 0 115.526 14.2354 2 -17 21 0 82.3103 14.8442 2 -4 -17 0 99.8975 14.1910 2 16 -21 0 22.7266 11.1582 2 5 16 0 15.0138 12.1997 2 -21 5 0 21.1101 10.6972 2 -5 -16 0 28.1353 10.9666 2 -16 21 0 27.3878 12.0454 2 21 -5 0 12.7625 10.1715 2 6 15 0 104.623 15.1840 2 -21 6 0 137.765 14.7981 2 15 -21 0 124.636 14.9304 2 -6 -15 0 106.173 14.0632 2 21 -6 0 101.621 13.3917 2 -15 21 0 73.0693 13.6202 2 14 -21 0 44.1578 11.4993 2 7 14 0 50.5530 12.3338 2 -21 7 0 45.0628 11.6233 2 -7 -14 0 55.5972 11.9171 2 -14 21 0 41.4562 12.6304 2 21 -7 0 51.2932 11.4142 2 13 -21 0 191.395 17.5778 2 -21 8 0 229.326 18.3171 2 8 13 0 213.718 18.7503 2 21 -8 0 225.310 17.8888 2 -13 21 0 189.112 18.0308 2 -8 -13 0 234.020 18.6353 2 9 12 0 347.257 25.2999 2 12 -21 0 343.021 24.4451 2 -21 9 0 380.923 24.9835 2 -9 -12 0 385.836 24.4750 2 -12 21 0 375.081 25.9014 2 21 -9 0 403.884 24.8537 2 10 11 0 135.419 15.6490 2 11 -21 0 186.341 17.0055 2 -21 10 0 148.287 15.3785 2 21 -10 0 168.080 15.1405 2 -11 21 0 147.102 16.1353 2 -10 -11 0 164.572 15.4987 2 10 -21 0 179.474 16.3097 2 -21 11 0 190.868 16.6845 2 11 10 0 165.126 16.2462 2 -11 -10 0 163.062 15.2945 2 -10 21 0 128.628 15.7430 2 21 -11 0 143.984 14.8519 2 12 9 0 238.282 18.6399 2 -21 12 0 218.985 18.4024 2 9 -21 0 187.680 17.5668 2 -9 21 0 176.324 17.3370 2 21 -12 0 253.315 19.8303 2 -12 -9 0 210.803 18.7673 2 13 8 0 219.191 18.0852 2 8 -21 0 212.566 18.0838 2 -21 13 0 217.217 18.0593 2 -8 21 0 176.113 17.5887 2 -13 -8 0 234.954 19.6147 2 21 -13 0 226.264 18.2633 2 7 -21 0 76.3725 12.5090 2 14 7 0 81.7537 12.8185 2 -21 14 0 71.4476 12.6754 2 -14 -7 0 56.5748 11.1591 2 -7 21 0 42.2550 12.7714 2 21 -14 0 71.0338 11.9877 2 15 6 0 126.138 14.9587 2 -21 15 0 124.511 15.4832 2 6 -21 0 118.216 14.9816 2 -6 21 0 137.722 16.0235 2 -15 -6 0 147.300 14.6830 2 21 -15 0 156.998 15.2217 2 16 5 0 29.6883 11.4726 2 -21 16 0 41.2939 12.4284 2 5 -21 0 39.6623 11.9942 2 -5 21 0 24.8634 11.9858 2 21 -16 0 39.7965 11.0190 2 -16 -5 0 34.2100 10.8480 2 -21 17 0 143.177 16.4383 2 4 -21 0 185.208 17.4237 2 17 4 0 145.393 15.9253 2 21 -17 0 178.623 16.6128 2 -17 -4 0 146.268 15.3409 2 -4 21 0 139.621 16.6613 2 18 3 0 84.1804 13.8857 2 -21 18 0 68.0692 14.3796 2 3 -21 0 91.4269 14.3787 2 -3 21 0 94.8941 15.9851 2 -18 -3 0 92.7538 12.9757 2 21 -18 0 89.1896 13.9901 2 2 -21 0 118.206 15.3762 2 -21 19 0 122.258 16.0111 2 21 -19 0 120.402 15.4761 2 -19 -2 0 89.7646 13.8520 2 1 -21 0 28.0610 12.2797 2 -21 20 0 36.2563 13.6571 2 -20 -1 0 21.8714 11.1567 2 21 -20 0 12.5389 11.6815 2 0 -21 0 15.0346 11.8223 2 -21 0 0 5.46265 10.6431 2 21 -21 0 5.36514 11.7499 2 -22 1 0 66.5710 13.8543 2 -1 -21 0 85.4628 14.8589 2 -22 2 0 67.5926 13.2929 2 -22 2 0 75.2774 14.2808 2 20 -22 0 87.3607 15.5463 2 -2 -20 0 65.1268 14.0025 2 -22 3 0 68.1465 13.1021 2 19 -22 0 71.7757 14.0926 2 -22 3 0 79.0320 14.1672 2 -3 -19 0 82.9267 14.3802 2 18 -22 0 26.2779 12.0406 2 -22 4 0 7.38380 11.3242 2 -22 4 0 23.4842 11.1759 2 -18 22 0 25.0378 13.8802 2 -4 -18 0 26.1283 11.6166 2 -22 5 0 141.001 16.0211 2 17 -22 0 115.464 15.4698 2 -5 -17 0 146.781 16.4144 2 22 -5 0 107.090 15.7494 2 -17 22 0 130.472 16.5782 2 16 -22 0 340.133 25.4801 2 -22 6 0 316.868 24.8700 2 -6 -16 0 333.078 25.3282 2 -16 22 0 354.062 26.5308 2 22 -6 0 360.285 24.9451 2 7 15 0 69.9248 14.6139 2 -22 7 0 43.1911 12.1640 2 15 -22 0 55.4862 12.4550 2 -7 -15 0 45.2056 12.3394 2 22 -7 0 29.0566 11.2602 2 -15 22 0 43.7634 13.1752 2 14 -22 0 151.905 16.2970 2 -22 8 0 178.730 16.9207 2 8 14 0 141.303 17.1222 2 -8 -14 0 157.860 16.3734 2 22 -8 0 181.852 16.4778 2 -14 22 0 131.243 16.4600 2 9 13 0 75.8327 13.8288 2 -22 9 0 67.2169 13.0396 2 13 -22 0 74.9055 12.7816 2 22 -9 0 85.3986 13.0475 2 -9 -13 0 76.7999 12.5624 2 -13 22 0 81.2460 13.8956 2 -22 10 0 64.3302 12.7861 2 10 12 0 68.2307 13.5649 2 12 -22 0 50.7392 12.2613 2 22 -10 0 72.9883 12.0429 2 -12 22 0 71.5527 13.9381 2 -10 -12 0 76.0087 12.6450 2 11 11 0 22.6276 11.8009 2 11 -22 0 13.0604 10.6455 2 -22 11 0 36.8380 11.6935 2 22 -11 0 29.1270 10.9150 2 -11 22 0 29.0371 12.2598 2 -11 -11 0 45.9687 11.2810 2 -22 12 0 79.9468 13.2827 2 12 10 0 78.1691 13.6519 2 10 -22 0 83.0824 13.3012 2 -10 22 0 64.3015 13.3809 2 22 -12 0 49.7878 11.8684 2 -12 -10 0 65.4146 11.9366 2 9 -22 0 43.2797 11.7616 2 -22 13 0 40.4377 12.1081 2 13 9 0 51.7346 12.3299 2 -9 22 0 32.9012 12.4977 2 22 -13 0 36.6823 11.1139 2 -13 -9 0 37.8826 10.9882 2 -22 14 0 186.214 17.8677 2 14 8 0 194.486 17.9058 2 8 -22 0 200.085 17.9198 2 -14 -8 0 191.317 17.4117 2 -8 22 0 180.491 17.9738 2 22 -14 0 164.643 16.6685 2 7 -22 0 48.9885 12.5122 2 15 7 0 42.7441 12.8631 2 -22 15 0 56.6683 13.1352 2 22 -15 0 51.4631 11.6872 2 -15 -7 0 53.1537 11.6716 2 -7 22 0 40.6485 13.1240 2 6 -22 0 381.919 26.3328 2 -22 16 0 391.761 27.4829 2 -16 -6 0 379.809 25.1180 2 22 -16 0 398.238 25.5330 2 -6 22 0 354.144 28.6747 2 5 -22 0 70.3572 13.5944 2 -22 17 0 83.1343 14.4855 2 22 -17 0 61.2055 12.8604 2 -17 -5 0 58.5090 12.3321 2 4 -22 0 19.0367 11.9510 2 -22 18 0 30.0113 13.3192 2 -18 -4 0 13.9027 10.5711 2 22 -18 0 12.4565 11.0561 2 3 -22 0 113.538 15.8085 2 -22 19 0 107.069 17.7932 2 -19 -3 0 115.638 14.4561 2 22 -19 0 98.5016 14.7345 2 2 -22 0 107.352 15.6432 2 -20 -2 0 112.229 15.1089 2 1 -22 0 80.1689 15.0600 2 -21 -1 0 103.670 15.2043 2 -3 -20 0 72.7283 14.3660 2 -23 4 0 131.296 16.7638 2 -4 -19 0 97.0177 15.9600 2 -23 5 0 82.1090 14.6563 2 18 -23 0 76.3395 14.6033 2 -5 -18 0 79.2101 14.7405 2 -23 6 0 66.4891 13.9623 2 17 -23 0 62.7719 13.3349 2 -6 -17 0 71.9246 14.2785 2 16 -23 0 66.4916 13.2259 2 -23 7 0 59.1153 13.6848 2 -7 -16 0 63.1437 13.4906 2 15 -23 0 46.0953 12.5063 2 -23 8 0 76.6034 13.9063 2 -8 -15 0 73.3823 13.6406 2 14 -23 0 84.5665 14.1344 2 -23 9 0 126.394 15.6355 2 -9 -14 0 124.915 14.7992 2 -14 23 0 121.590 16.9487 2 23 -9 0 98.3561 14.6890 2 13 -23 0 8.90681 11.2776 2 -23 10 0 13.7337 11.4734 2 -10 -13 0 9.82444 10.7308 2 -13 23 0 3.49960 12.7252 2 23 -10 0 9.67806 10.5090 2 12 -23 0 78.8236 13.8549 2 -23 11 0 101.698 14.8863 2 -11 -12 0 83.0015 13.0485 2 -12 23 0 60.3890 14.1257 2 23 -11 0 71.0716 12.9235 2 11 -23 0 96.3628 14.8275 2 -23 12 0 103.305 15.2191 2 -12 -11 0 132.875 15.0634 2 23 -12 0 109.504 14.4098 2 10 -23 0 20.6105 11.2449 2 -23 13 0 8.87157 11.2551 2 -13 -10 0 15.5483 10.4356 2 23 -13 0 13.9140 10.9756 2 -23 14 0 134.715 16.4008 2 9 -23 0 137.416 16.2448 2 -14 -9 0 158.902 16.2883 2 23 -14 0 132.815 15.6547 2 8 -23 0 46.3885 13.0679 2 -23 15 0 74.2843 13.9151 2 23 -15 0 26.8204 11.5992 2 -15 -8 0 54.0617 12.0346 2 -23 16 0 40.3167 13.6918 2 7 -23 0 39.1520 12.6999 2 23 -16 0 44.8004 11.9580 2 -16 -7 0 46.3858 11.7843 2 6 -23 0 163.868 17.4892 2 -23 17 0 139.156 17.8283 2 23 -17 0 125.877 16.3395 2 -17 -6 0 133.247 15.8270 2 5 -23 0 114.029 16.1309 2 -18 -5 0 97.7211 14.6594 2 4 -23 0 106.373 16.1131 2 -19 -4 0 94.4546 14.4241 2 3 -23 0 62.1363 14.6900 2 -20 -3 0 55.7765 13.1967 2 -5 -19 0 17.3469 13.1469 2 -6 -18 0 159.620 18.2181 2 -7 -17 0 43.7772 13.6641 2 -24 8 0 43.3719 13.6876 2 16 -24 0 64.6225 13.8161 2 -8 -16 0 50.3387 13.6820 2 15 -24 0 331.693 25.6929 2 -24 9 0 309.906 25.9090 2 -9 -15 0 312.144 25.0494 2 -24 10 0 73.0294 14.2585 2 14 -24 0 72.6265 14.1316 2 -10 -14 0 60.9138 13.2060 2 -24 11 0 61.0471 14.1889 2 13 -24 0 58.9620 13.3102 2 -11 -13 0 19.2578 11.6014 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5000.33 205.471 1 -1 -1 1 5009.19 196.145 2 -1 -1 1 4999.37 240.512 3 2 0 -1 777.816 34.4846 2 -2 2 -1 784.784 34.5420 2 0 -2 -1 778.609 34.3613 2 0 -2 -1 771.709 34.4192 2 -2 2 -1 764.472 34.4270 2 2 0 -1 745.548 34.4355 2 2 -2 1 984.928 42.7804 3 -2 0 1 916.286 34.4073 2 2 -2 1 909.294 36.8927 1 2 -2 1 948.387 34.4277 2 0 2 1 975.022 36.3956 1 -2 0 1 972.263 43.0946 3 -1 -2 -1 262.581 10.1833 2 3 -1 -1 257.511 10.1641 2 -2 3 -1 247.421 10.2224 2 -1 -2 -1 249.327 10.1914 2 1 2 1 213.796 9.77590 2 2 -3 1 206.469 10.0215 2 2 -3 1 204.859 11.1735 1 1 2 1 229.653 11.0362 1 -3 1 1 218.959 12.9388 3 2 -3 1 232.666 12.8027 3 -3 1 1 207.815 9.96167 2 -2 -2 -1 4100.01 165.725 2 4 -2 -1 4105.99 165.718 2 -2 4 -1 4090.19 165.881 2 -4 2 1 4303.81 202.548 3 2 2 1 4116.63 165.527 2 2 -4 1 4058.79 173.520 1 -4 2 1 4247.15 165.695 2 2 -4 1 4285.35 202.695 3 2 -4 1 4226.37 165.792 2 -2 5 -1 1582.16 68.7224 2 5 -3 -1 1718.73 68.5180 2 -3 -2 -1 1628.01 68.4379 2 2 -5 1 1652.17 71.6844 1 -5 3 1 1773.23 68.5167 2 3 2 1 1734.30 68.3023 2 -5 3 1 1876.19 83.5420 3 2 -5 1 1642.36 68.5709 2 4 -3 -1 1090.27 46.2477 2 -1 4 -1 1110.93 46.5754 2 -3 -1 -1 1087.78 46.2154 2 -4 3 1 1192.87 56.3947 3 -4 3 1 1164.19 46.2932 2 1 -4 1 1174.93 46.3269 2 1 -4 1 1161.28 48.6485 1 3 1 1 1177.12 46.1158 2 3 -3 -1 3501.70 126.315 2 -3 0 -1 3391.45 126.248 2 0 3 -1 3378.69 126.538 2 3 0 1 2945.02 126.042 2 0 -3 1 2936.78 132.288 1 0 -3 1 3016.81 126.178 2 -3 3 1 3133.13 154.154 3 -3 3 1 3082.18 126.256 2 2 -3 -1 2872.16 109.490 2 -3 1 -1 2836.79 109.449 2 1 2 -1 2873.20 109.674 2 -2 3 1 2711.44 109.396 2 3 -1 1 2556.02 109.321 2 -1 -2 1 2667.41 109.399 2 -3 2 -1 3267.30 134.482 2 1 -3 -1 3196.33 134.509 2 2 1 -1 3247.83 134.574 2 3 -2 1 3532.31 164.617 3 -1 3 1 3518.82 134.391 2 -2 -1 1 3451.42 134.466 2 3 -2 1 3423.14 134.503 2 -1 3 1 3457.87 140.552 1 -3 3 -1 3588.18 157.893 2 3 0 -1 3698.57 157.939 2 0 -3 -1 3616.28 157.973 2 3 -3 1 4227.93 193.078 3 -3 0 1 4159.30 157.908 2 0 3 1 4151.75 157.793 2 0 3 1 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739.664 29.5052 2 -5 7 -1 772.884 29.8328 2 -2 -5 -1 743.257 29.6126 2 -7 2 1 680.079 29.2069 2 5 -7 1 656.977 30.6358 1 -7 2 1 652.791 29.1015 2 5 -7 1 663.798 29.4689 2 5 -7 1 671.785 34.9277 3 2 5 1 654.570 29.0693 2 -5 8 -1 2083.45 82.3901 2 8 -3 -1 2084.71 81.9865 2 -3 -5 -1 2079.48 82.0839 2 5 -8 1 1945.28 85.2890 1 -8 3 1 2032.52 81.8172 2 3 5 1 2005.16 81.7139 2 5 -8 1 1976.52 99.2550 3 5 -8 1 1957.17 82.1091 2 -5 9 -1 850.309 40.3095 2 -4 -5 -1 830.555 39.8499 2 9 -4 -1 831.723 39.8828 2 5 -9 1 1027.31 48.3898 3 5 -9 1 1015.66 41.3981 1 4 5 1 994.549 39.9127 2 -9 4 1 1031.29 40.0969 2 5 -9 1 1024.17 40.4839 2 -5 -5 -1 1109.41 47.2038 2 10 -5 -1 1138.98 47.1753 2 -5 10 -1 1177.79 47.9094 2 5 5 1 1113.20 46.8440 2 5 -10 1 1118.97 48.3215 1 5 -10 1 1106.61 47.3625 2 -10 5 1 1097.29 46.9858 2 11 -6 -1 605.450 27.9788 2 -6 -5 -1 597.504 27.8683 2 -5 11 -1 600.312 28.8320 2 5 -11 1 636.476 28.3201 2 -11 6 1 651.035 28.0595 2 6 5 1 637.488 27.8026 2 5 -11 1 632.001 27.8937 1 10 -6 -1 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885.538 35.9101 2 -6 0 2 901.161 35.9615 2 0 6 2 879.776 37.5073 1 -1 -6 -2 1151.67 51.8904 2 -6 7 -2 1149.69 51.8788 2 7 -1 -2 1168.05 51.7997 2 6 -7 2 1284.36 51.6550 2 1 6 2 1297.54 51.1316 2 6 -7 2 1336.52 63.4707 3 6 -7 2 1338.49 55.4366 1 1 6 2 1332.66 53.8634 1 -7 1 2 1289.97 51.4422 2 -2 -6 -2 442.098 18.7671 2 8 -2 -2 440.817 18.6099 2 -6 8 -2 430.307 18.8421 2 6 -8 2 385.800 22.3995 3 -8 2 2 386.810 17.9071 2 6 -8 2 385.123 18.0867 2 2 6 2 384.463 18.8555 1 6 -8 2 398.313 20.2551 1 2 6 2 369.075 17.4550 2 -8 2 2 367.736 23.1997 3 -3 -6 -2 230.570 12.3572 2 -6 9 -2 243.535 13.0107 2 9 -3 -2 224.953 12.3496 2 3 6 2 221.563 11.2542 2 6 -9 2 227.632 11.9869 2 -9 3 2 208.970 11.6127 2 -9 3 2 211.147 15.4629 3 6 -9 2 226.183 14.8896 3 6 -9 2 212.168 13.2359 1 10 -4 -2 652.027 28.5677 2 -4 -6 -2 613.482 28.4768 2 -6 10 -2 624.996 29.0293 2 6 -10 2 633.893 29.9217 1 6 -10 2 679.446 34.6321 3 -10 4 2 665.769 34.8042 3 4 6 2 643.574 27.5555 2 -10 4 2 652.256 28.0002 2 6 -10 2 609.282 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43.2083 2 -7 1 -2 999.947 43.0788 2 1 6 -2 967.499 43.5566 2 7 -1 2 1062.79 42.6361 2 -6 7 2 1103.90 43.0424 2 -1 -6 2 1110.92 42.9645 2 -7 2 -2 1972.15 80.7890 2 5 -7 -2 1918.25 80.8828 2 2 5 -2 1883.93 81.1814 2 -5 7 2 2130.17 80.6156 2 -2 -5 2 2079.19 80.6003 2 7 -2 2 2013.29 80.3954 2 -7 3 -2 1470.57 62.1590 2 4 -7 -2 1447.59 62.2970 2 3 4 -2 1512.04 62.5783 2 -3 -4 2 1582.69 61.9834 2 7 -3 2 1554.53 61.8712 2 -4 7 2 1612.51 61.9068 2 4 3 -2 1000.29 40.2708 2 3 -7 -2 1034.29 40.2525 2 -7 4 -2 999.947 39.9819 2 7 -4 2 899.770 39.5340 2 -4 -3 2 930.220 39.5445 2 -3 7 2 929.493 39.3661 2 -7 5 -2 1926.73 80.1082 2 2 -7 -2 2015.31 80.4335 2 5 2 -2 2060.99 80.4062 2 -7 5 -2 1980.59 80.1179 2 7 -5 2 1947.78 79.8725 2 -2 7 2 2017.10 79.5913 2 -5 -2 2 1973.71 79.7511 2 -2 7 2 1915.97 82.9334 1 7 -5 2 2005.28 85.4566 1 -7 6 -2 1103.32 44.1043 2 6 1 -2 1105.22 44.1692 2 1 -7 -2 1119.12 44.3198 2 7 -6 2 1008.06 47.3046 1 7 -6 2 1028.32 53.6097 3 7 -6 2 1039.06 43.7302 2 -6 -1 2 1061.97 43.5658 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52.0556 15.8704 2 4 -23 -2 20.8558 13.1639 2 19 4 -2 59.2494 15.4502 2 23 -19 2 36.9969 14.0410 1 7 17 -2 20.7132 15.5786 2 17 -24 -2 17.9986 12.9221 2 -24 7 -2 23.1202 13.7519 2 8 16 -2 110.751 18.2374 2 16 -24 -2 97.9718 16.5168 2 -24 8 -2 115.703 16.8182 2 9 15 -2 52.5241 16.1070 2 15 -24 -2 35.0810 13.2898 2 -24 9 -2 71.7306 15.3407 2 -24 10 -2 131.806 17.8793 2 10 14 -2 113.731 18.4436 2 14 -24 -2 137.088 16.9473 2 11 13 -2 67.5650 16.3074 2 13 -24 -2 89.4467 15.2793 2 -24 11 -2 82.1841 15.7090 2 12 -24 -2 25.6520 12.7887 2 -24 12 -2 17.4440 13.5312 2 12 12 -2 35.3149 14.5614 2 13 11 -2 26.8273 14.9191 2 11 -24 -2 46.7870 13.5645 2 -24 13 -2 71.9725 15.4174 2 -24 14 -2 70.7308 15.9405 2 14 10 -2 60.8977 15.7066 2 10 -24 -2 63.3125 14.9544 2 15 9 -2 71.6369 16.1901 2 -24 15 -2 97.9517 16.6102 2 9 -24 -2 111.808 16.0685 2 -24 16 -2 87.4864 16.5659 2 16 8 -2 94.8426 16.6524 2 8 -24 -2 95.6028 15.9177 2 7 -24 -2 19.2586 13.2040 2 17 7 -2 5.05863 13.6578 2 -24 17 -2 7.55200 13.8154 2 24 -17 2 24.0258 14.8337 1 0 0 3 8883.14 376.213 1 0 0 3 9202.86 439.598 3 1 0 3 1879.57 96.6473 3 0 -1 3 1949.17 96.8022 3 1 0 3 1947.16 82.8222 1 -1 1 3 1943.93 96.6666 3 0 -1 3 1917.97 82.8714 1 -1 1 3 1963.22 82.6698 1 0 1 3 1724.20 73.9155 1 -1 0 3 1720.88 74.1079 1 -1 0 3 1723.09 86.6019 3 0 1 3 1713.88 86.5534 3 1 -1 3 1736.07 86.6001 3 1 -1 3 1717.60 74.1744 1 -2 1 3 322.410 20.3035 3 -2 1 3 351.340 17.5066 1 1 -2 3 321.791 17.4775 1 1 1 3 316.025 20.4096 3 1 1 3 345.302 17.2920 1 1 -2 3 312.067 20.3346 3 -1 3 -3 325.817 13.1083 2 -1 3 -3 342.922 13.0730 2 -3 2 3 300.469 19.3675 3 2 1 3 291.308 16.5845 1 1 -3 3 285.248 16.8977 1 1 -3 3 288.786 19.5194 3 2 0 3 25.6940 5.29770 1 0 -2 3 20.0737 5.13322 1 -2 2 3 34.2975 5.15027 1 -2 2 3 26.0789 6.63803 3 0 -2 3 25.8721 6.27739 3 2 0 3 38.8814 7.37781 3 -1 2 3 106.196 10.5672 3 -1 -1 3 98.5328 11.0050 3 -1 -1 3 115.949 9.47993 1 -1 2 3 97.9965 8.76454 1 2 -1 3 115.508 11.3771 3 2 -1 3 109.851 9.44694 1 0 2 3 60.7346 6.35033 1 2 -2 3 71.1198 7.53098 1 -2 0 3 70.5670 7.39471 1 2 -2 3 87.6967 9.40311 3 -2 0 3 74.6347 8.90700 3 0 2 3 73.1189 8.94328 3 3 -1 -3 238.801 10.4112 2 -2 3 -3 235.399 10.3746 2 -2 3 -3 230.179 10.3672 2 3 -1 -3 246.364 10.4690 2 2 -3 3 265.492 16.9698 3 1 2 3 277.151 14.0188 1 2 -3 3 259.781 14.3053 1 -3 1 3 280.502 17.0680 3 -2 -2 -3 2840.54 111.516 2 4 -2 -3 2856.36 111.918 2 -2 4 -3 2733.70 111.906 2 -2 -2 -3 2820.26 111.631 2 -2 4 -3 2786.40 111.905 2 4 -2 -3 2798.79 111.802 2 2 2 3 2830.56 118.871 1 2 -4 3 2853.94 139.170 3 -4 2 3 2801.45 138.914 3 2 -4 3 2768.59 119.257 1 5 -3 -3 160.048 8.27639 2 -2 5 -3 156.378 8.72231 2 5 -3 -3 162.128 8.39154 2 -2 5 -3 157.089 8.28469 2 -3 -2 -3 169.523 8.09300 2 -3 -2 -3 171.103 7.83487 2 2 -5 3 152.567 11.6498 1 2 -5 3 159.906 13.5281 3 3 2 3 169.905 11.4380 1 -5 3 3 151.803 12.8517 3 4 -3 -3 206.968 9.40074 2 -1 4 -3 185.340 9.55676 2 -3 -1 -3 196.000 8.78983 2 -3 -1 -3 203.956 8.91597 2 -1 4 -3 200.060 9.27641 2 4 -3 -3 205.173 9.16981 2 1 -4 3 199.357 14.5578 3 3 1 3 192.846 12.6518 1 1 -4 3 202.405 12.9800 1 -4 3 3 204.843 14.5620 3 0 3 -3 1614.44 67.5166 2 3 -3 -3 1658.74 67.3612 2 0 3 -3 1592.30 67.6239 2 3 -3 -3 1621.72 67.2627 2 3 0 3 1767.43 73.1730 1 0 -3 3 1722.92 73.1284 1 0 -3 3 1822.97 85.6437 3 -3 3 3 1773.02 85.0118 3 1 2 -3 1368.55 52.5666 2 1 2 -3 1384.22 52.7255 2 -2 3 3 1336.49 66.9702 3 -1 -2 3 1305.60 57.6438 1 3 -1 3 1235.82 57.4514 1 3 -1 3 1307.03 67.0923 3 -2 3 3 1291.29 56.9535 1 -1 -2 3 1268.62 67.1817 3 2 1 -3 1064.74 43.6442 2 2 1 -3 1068.50 43.5237 2 -2 -1 3 1069.98 48.0700 1 -2 -1 3 1092.72 56.3493 3 -1 3 3 1117.86 56.1183 3 3 -2 3 1141.53 56.3235 3 -1 3 3 1087.18 47.6052 1 3 -2 3 1063.87 48.2618 1 -3 3 -3 1803.57 70.5358 2 3 0 -3 1793.45 70.6655 2 3 0 -3 1813.74 70.6102 2 -3 3 -3 1807.11 70.4792 2 0 3 3 1751.86 75.5976 1 3 -3 3 1737.64 88.7936 3 3 -3 3 1719.61 76.3484 1 -3 0 3 1703.65 88.7977 3 4 -1 -3 150.570 7.63515 2 -3 4 -3 147.778 7.62869 2 4 -1 -3 155.803 7.74935 2 -1 -3 -3 154.873 7.11693 2 -3 4 -3 154.667 7.71301 2 -1 -3 -3 154.594 7.28182 2 1 3 3 173.350 10.4802 1 3 -4 3 182.304 13.5170 3 -4 1 3 171.689 13.4125 3 3 -4 3 164.580 10.9018 1 -2 -3 -3 183.620 8.49034 2 -2 -3 -3 167.569 8.10049 2 5 -2 -3 169.491 8.49793 2 -3 5 -3 171.911 8.61990 2 -3 5 -3 163.239 8.73693 2 5 -2 -3 182.702 8.67695 2 3 -5 3 168.122 11.9721 1 3 -5 3 148.865 13.4820 3 2 3 3 153.579 11.1817 1 -5 2 3 157.854 13.3859 3 6 -3 -3 142.717 8.17450 2 -3 6 -3 150.993 8.77978 2 -3 -3 -3 150.238 8.02540 2 -3 -3 -3 143.228 7.67596 2 3 3 3 149.658 10.8989 1 3 -6 3 139.687 11.2030 1 -6 3 3 135.080 12.3011 3 3 -6 3 156.592 13.1414 3 -4 -3 -3 1575.03 65.5035 2 7 -4 -3 1602.53 65.6250 2 -3 7 -3 1624.92 66.1420 2 -7 4 3 1698.20 81.5736 3 3 -7 3 1542.87 70.1949 1 4 3 3 1587.34 70.0933 1 3 -7 3 1674.05 82.2156 3 -4 -2 -3 1356.92 53.5346 2 6 -4 -3 1290.62 53.5912 2 -2 6 -3 1313.31 54.0722 2 -4 -2 -3 1351.27 53.3434 2 2 -6 3 1305.53 67.7972 3 4 2 3 1344.86 58.0680 1 2 -6 3 1291.26 58.0123 1 -6 4 3 1281.76 66.9391 3 -1 5 -3 479.682 21.0000 2 -4 -1 -3 491.586 20.3118 2 -4 -1 -3 481.743 20.1577 2 5 -4 -3 476.919 20.4036 2 5 -4 -3 501.109 20.6132 2 1 -5 3 483.334 23.8780 1 4 1 3 452.578 23.9280 1 1 -5 3 478.923 27.9729 3 -5 4 3 459.372 27.1498 3 0 4 -3 775.518 31.6807 2 -4 0 -3 742.970 31.3446 2 -4 0 -3 756.768 31.3377 2 0 4 -3 760.651 32.0033 2 4 -4 -3 720.283 31.4030 2 4 -4 -3 792.373 31.7501 2 0 -4 3 770.852 35.4737 1 -4 4 3 827.723 40.9388 3 0 -4 3 802.078 41.7407 3 4 0 3 764.730 35.5467 1 -4 1 -3 1108.08 44.8853 2 1 3 -3 1119.74 45.4015 2 1 3 -3 1123.44 45.1361 2 3 -4 -3 1125.18 44.9788 2 3 -4 -3 1108.63 44.8459 2 -4 1 -3 1088.38 44.8216 2 -1 -3 3 1145.24 58.0678 3 -1 -3 3 1097.97 49.6112 1 4 -1 3 1153.72 49.8150 1 -3 4 3 1094.10 57.2112 3 -4 2 -3 255.214 11.0230 2 2 -4 -3 248.604 10.8907 2 2 2 -3 252.307 11.6696 2 2 2 -3 255.566 11.3056 2 2 -4 -3 253.224 10.9399 2 -4 2 -3 230.293 11.0805 2 4 -2 3 278.764 15.4487 1 -2 4 3 277.670 14.0887 1 -2 -2 3 265.391 17.8113 3 4 -2 3 260.328 17.2423 3 -2 4 3 264.233 16.9971 3 1 -4 -3 1052.59 42.3997 2 -4 3 -3 1035.63 42.7224 2 -4 3 -3 1041.18 42.5600 2 1 -4 -3 1068.41 42.3973 2 3 1 -3 1044.38 42.8687 2 3 1 -3 1044.72 42.7065 2 4 -3 3 1101.36 54.8209 3 4 -3 3 1051.67 47.2831 1 -1 4 3 1069.13 46.2106 1 -3 -1 3 1056.73 55.0177 3 4 0 -3 830.992 34.1039 2 0 -4 -3 837.918 33.9152 2 -4 4 -3 817.822 34.1835 2 4 0 -3 838.207 34.2203 2 -4 4 -3 817.386 34.0448 2 0 -4 -3 850.940 33.7994 2 -4 0 3 824.588 44.3208 3 0 4 3 827.828 37.1169 1 4 -4 3 844.786 44.1021 3 4 -4 3 839.225 38.2480 1 -4 5 -3 446.800 20.5252 2 5 -1 -3 479.158 20.6327 2 5 -1 -3 470.356 20.4717 2 -1 -4 -3 477.797 20.5212 2 -4 5 -3 465.501 20.6320 2 -1 -4 -3 458.941 20.1159 2 -5 1 3 511.235 27.9696 3 4 -5 3 531.218 27.8417 3 4 -5 3 511.699 24.2894 1 1 4 3 500.519 23.0258 1 -4 6 -3 1194.82 49.4223 2 -2 -4 -3 1166.49 48.8928 2 -2 -4 -3 1183.38 49.1947 2 6 -2 -3 1205.53 49.2746 2 2 4 3 1220.93 52.7455 1 4 -6 3 1209.15 53.5127 1 4 -6 3 1253.53 62.1519 3 -6 2 3 1224.76 62.1919 3 -4 7 -3 2015.79 81.4436 2 7 -3 -3 1959.08 81.1017 2 -3 -4 -3 1924.51 81.0215 2 4 -7 3 2072.06 100.943 3 -7 3 3 2075.10 100.693 3 4 -7 3 2017.79 86.6581 1 3 4 3 1995.96 85.9352 1 8 -4 -3 111.004 8.25973 2 -4 -4 -3 119.552 8.02753 2 -4 8 -3 123.971 9.15737 2 4 -8 3 117.805 10.6021 1 4 -8 3 106.121 11.3313 3 4 4 3 115.928 10.3749 1 -8 4 3 102.479 10.7229 3 -5 -4 -3 374.959 17.8733 2 -4 9 -3 359.613 18.8936 2 9 -5 -3 412.708 18.3590 2 5 4 3 369.130 20.5234 1 4 -9 3 351.028 20.1596 1 4 -9 3 389.120 24.2249 3 -9 5 3 392.450 23.0927 3 -3 8 -3 366.103 18.7246 2 8 -5 -3 377.919 18.0392 2 -5 -3 -3 391.868 17.8315 2 -8 5 3 398.562 23.3191 3 5 3 3 405.982 20.7588 1 3 -8 3 380.790 20.5769 1 3 -8 3 401.632 24.3598 3 -2 7 -3 458.229 20.7158 2 7 -5 -3 444.520 19.8492 2 -5 -2 -3 458.238 19.7692 2 5 2 3 449.647 22.9696 1 2 -7 3 421.224 26.7303 3 -7 5 3 441.090 25.6521 3 2 -7 3 444.647 22.7533 1 6 -5 -3 1405.54 57.2970 2 -1 6 -3 1428.62 57.9053 2 -5 -1 -3 1396.64 57.2022 2 -5 -1 -3 1493.97 57.4572 2 1 -6 3 1318.33 61.6633 1 -6 5 3 1421.09 71.4050 3 1 -6 3 1437.28 72.6268 3 5 1 3 1360.49 61.9735 1 5 -5 -3 1782.40 69.6340 2 -5 0 -3 1760.36 69.2546 2 -5 0 -3 1722.58 69.2932 2 5 -5 -3 1737.12 69.3731 2 0 5 -3 1766.48 69.9618 2 -5 5 3 1694.18 86.2737 3 0 -5 3 1679.69 87.2475 3 0 -5 3 1677.12 74.6079 1 5 0 3 1650.59 74.6915 1 -5 1 -3 550.496 23.6353 2 4 -5 -3 548.703 23.6706 2 -5 1 -3 569.058 23.6667 2 4 -5 -3 568.834 23.9939 2 1 4 -3 548.688 24.3221 2 -1 -4 3 592.012 32.5276 3 -4 5 3 610.651 31.3409 3 -1 -4 3 556.996 27.4137 1 5 -1 3 566.739 27.6528 1 3 -5 -3 1317.70 54.6841 2 2 3 -3 1361.27 55.2427 2 3 -5 -3 1355.65 54.8421 2 2 3 -3 1344.44 54.9413 2 -5 2 -3 1336.85 54.7126 2 -5 2 -3 1326.33 54.7845 2 -3 5 3 1388.58 69.1248 3 -2 -3 3 1388.20 69.9434 3 5 -2 3 1412.29 60.0280 1 3 2 -3 1280.35 52.3168 2 -5 3 -3 1307.41 52.1163 2 -5 3 -3 1305.49 51.9590 2 2 -5 -3 1296.65 51.9163 2 3 2 -3 1327.32 52.1527 2 2 -5 -3 1265.37 51.8736 2 5 -3 3 1231.76 56.8044 1 -3 -2 3 1286.69 66.3890 3 5 -3 3 1268.63 65.7318 3 -2 5 3 1277.42 55.5513 1 4 1 -3 723.252 29.5112 2 4 1 -3 723.604 29.5230 2 1 -5 -3 703.219 29.1666 2 1 -5 -3 715.010 29.0709 2 -5 4 -3 690.135 29.1971 2 -5 4 -3 717.318 29.4240 2 -1 5 3 685.969 31.7009 1 5 -4 3 715.334 33.4240 1 -4 -1 3 699.806 38.6793 3 5 -4 3 675.374 37.7926 3 5 0 -3 1563.62 64.7357 2 0 -5 -3 1536.34 64.3245 2 0 -5 -3 1546.03 64.5947 2 -5 5 -3 1535.05 64.6085 2 -5 0 3 1628.48 81.2606 3 0 5 3 1679.62 68.5820 1 5 -5 3 1622.27 69.8659 1 5 -5 3 1701.32 80.9563 3 -1 -5 -3 1647.86 69.7948 2 -1 -5 -3 1712.86 69.5216 2 6 -1 -3 1672.83 69.8659 2 -5 6 -3 1664.76 69.8740 2 -6 1 3 1743.94 87.3456 3 5 -6 3 1772.11 75.1312 1 5 -6 3 1786.95 87.0511 3 1 5 3 1808.86 73.8956 1 -2 -5 -3 337.679 16.9460 2 -5 7 -3 348.199 17.2545 2 7 -2 -3 346.881 17.0471 2 2 5 3 391.267 18.9481 1 5 -7 3 390.560 20.4009 1 5 -7 3 414.799 22.9205 3 -7 2 3 398.680 23.0774 3 -3 -5 -3 185.924 11.2207 2 8 -3 -3 211.797 11.3035 2 -5 8 -3 187.083 11.9369 2 5 -8 3 224.663 14.2753 1 3 5 3 204.755 12.9418 1 5 -8 3 234.339 16.2345 3 -8 3 3 222.482 16.0949 3 -4 -5 -3 713.485 31.4709 2 9 -4 -3 698.055 31.4854 2 -5 9 -3 729.500 32.2493 2 4 5 3 740.778 33.9523 1 5 -9 3 759.956 34.7701 1 5 -9 3 737.904 40.1233 3 -9 4 3 730.438 39.6497 3 10 -5 -3 469.430 21.6212 2 -5 10 -3 458.588 22.4982 2 -5 -5 -3 436.243 21.1940 2 5 5 3 461.510 23.5263 1 5 -10 3 469.411 23.7761 1 -10 5 3 452.642 26.7432 3 5 -10 3 433.464 20.0689 2 5 -10 3 465.967 27.5028 3 11 -6 -3 89.3202 8.03724 2 -6 -5 -3 105.301 8.35852 2 -5 11 -3 88.7872 9.16521 2 5 -11 3 70.3985 10.8481 3 6 5 3 83.9647 9.44172 1 5 -11 3 70.7046 8.74887 1 5 -11 3 84.0475 7.48931 2 -11 6 3 92.1664 10.2962 3 -4 10 -3 1485.92 64.9577 2 -6 -4 -3 1506.06 64.1537 2 10 -6 -3 1495.04 64.2205 2 -10 6 3 1600.24 78.7273 3 6 4 3 1551.63 68.5782 1 4 -10 3 1587.82 63.3149 2 4 -10 3 1611.60 80.0831 3 4 -10 3 1593.80 68.3688 1 -6 -3 -3 463.035 21.6057 2 -3 9 -3 474.707 22.6764 2 9 -6 -3 448.761 21.6609 2 -9 6 3 483.373 27.0843 3 3 -9 3 474.590 24.0291 1 6 3 3 478.692 24.8212 1 3 -9 3 500.262 28.9480 3 -6 -2 -3 141.312 8.62310 2 -2 8 -3 144.496 10.0102 2 8 -6 -3 127.530 8.74051 2 6 2 3 122.014 10.8307 1 2 -8 3 126.923 13.1708 3 -8 6 3 107.963 11.4731 3 2 -8 3 123.133 10.9216 1 -1 7 -3 66.1086 6.40505 2 -6 -1 -3 67.5231 5.43013 2 7 -6 -3 71.1410 5.62863 2 1 -7 3 61.7508 9.91362 3 6 1 3 44.7763 7.69601 1 1 -7 3 53.3740 7.10321 1 -7 6 3 36.7068 7.22725 3 0 6 -3 1438.08 57.7025 2 -6 0 -3 1395.08 56.9199 2 6 -6 -3 1382.86 57.0276 2 6 0 3 1373.95 61.9280 1 -6 6 3 1380.70 70.7868 3 0 -6 3 1395.16 61.5556 1 0 -6 3 1420.46 72.4734 3 -6 1 -3 209.640 10.6696 2 1 5 -3 232.999 11.7613 2 5 -6 -3 209.740 10.7788 2 -5 6 3 223.171 15.0658 3 6 -1 3 203.950 14.4898 1 -1 -5 3 222.868 17.2791 3 -6 2 -3 835.845 33.3771 2 -6 2 -3 809.691 33.2602 2 4 -6 -3 808.716 33.3315 2 4 -6 -3 809.092 33.5368 2 2 4 -3 792.417 33.8382 2 -2 -4 3 787.768 43.7978 3 6 -2 3 767.443 37.4808 1 3 -6 -3 980.958 40.3316 2 -6 3 -3 1003.70 40.5334 2 3 -6 -3 1012.59 40.4667 2 -6 3 -3 953.424 40.2664 2 3 3 -3 993.681 40.7765 2 6 -3 3 903.183 44.5645 1 -3 -3 3 1031.21 52.5265 3 4 2 -3 962.473 40.4622 2 2 -6 -3 1007.22 40.1541 2 2 -6 -3 977.576 40.1833 2 -6 4 -3 974.222 40.1230 2 -4 -2 3 986.353 51.8512 3 6 -4 3 980.881 44.4456 1 6 -4 3 973.137 51.0196 3 -2 6 3 956.997 42.6502 1 1 -6 -3 190.644 10.0343 2 -6 5 -3 172.311 9.73979 2 1 -6 -3 201.862 9.71706 2 5 1 -3 189.128 10.2178 2 -6 5 -3 183.956 9.88756 2 6 -5 3 206.697 13.6443 1 -1 6 3 183.490 11.0441 1 6 -5 3 196.185 14.7774 3 -5 -1 3 183.549 15.4676 3 6 0 -3 1359.82 55.2083 2 0 -6 -3 1330.18 55.1685 2 -6 6 -3 1330.00 55.1336 2 6 -6 3 1349.82 68.7848 3 -6 0 3 1350.67 69.6149 3 6 -6 3 1345.65 59.8067 1 0 6 3 1365.58 58.0730 1 -1 -6 -3 35.2051 4.73736 2 7 -1 -3 37.2339 4.82484 2 -6 7 -3 32.5655 4.72819 2 1 6 3 48.1084 5.49295 1 -7 1 3 46.6453 8.80962 3 6 -7 3 32.9545 7.19417 3 6 -7 3 44.5504 7.14992 1 -2 -6 -3 71.7564 6.57420 2 -6 8 -3 84.3268 7.03867 2 8 -2 -3 85.2343 7.02652 2 6 -8 3 93.1093 9.98181 3 6 -8 3 93.0353 9.22703 1 2 6 3 95.7360 7.74306 1 -8 2 3 94.4489 10.6771 3 -3 -6 -3 413.409 18.9038 2 -6 9 -3 415.451 19.4436 2 9 -3 -3 433.266 19.1273 2 6 -9 3 375.772 21.1544 1 -9 3 3 377.978 24.5280 3 6 -9 3 387.864 24.2229 3 3 6 3 360.276 20.0138 1 -4 -6 -3 1965.50 78.4206 2 10 -4 -3 1898.76 78.3537 2 -6 10 -3 2032.75 79.0889 2 6 -10 3 1852.99 83.0162 1 6 -10 3 1866.85 96.4540 3 -10 4 3 1838.83 96.2557 3 6 -10 3 1916.48 77.3655 2 4 6 3 1911.12 82.3020 1 -6 11 -3 66.3297 8.46155 2 -5 -6 -3 78.2597 7.62744 2 11 -5 -3 59.1607 7.34884 2 6 -11 3 95.2024 9.40511 1 5 6 3 88.4045 8.86280 1 6 -11 3 92.6245 7.72624 2 6 -11 3 90.6950 11.1908 3 -11 5 3 88.5428 10.4854 3 12 -6 -3 1394.56 57.7975 2 -6 12 -3 1399.71 58.7386 2 -6 -6 -3 1380.80 57.7509 2 6 6 3 1397.74 61.2009 1 6 -12 3 1330.92 60.7669 1 6 -12 3 1326.73 71.0211 3 -12 6 3 1343.40 70.2910 3 13 -7 -3 145.772 12.0760 2 -7 -6 -3 140.708 11.6008 2 -6 13 -3 133.561 11.6991 2 6 -13 3 117.895 13.5767 3 -13 7 3 131.704 13.3632 3 7 6 3 117.120 11.7442 1 6 -13 3 113.286 10.8209 1 -7 -5 -3 282.495 16.5292 2 12 -7 -3 299.034 16.9552 2 -5 12 -3 290.822 18.2717 2 5 -12 3 327.996 22.5346 3 7 5 3 315.065 19.6047 1 5 -12 3 318.711 18.4625 1 -12 7 3 323.980 20.3234 3 11 -7 -3 359.100 18.0070 2 -4 11 -3 345.549 19.1980 2 -7 -4 -3 338.589 17.7520 2 -11 7 3 350.504 21.6127 3 4 -11 3 352.776 19.6565 1 4 -11 3 332.167 23.8115 3 7 4 3 352.287 20.9213 1 4 -11 3 338.147 16.6132 2 -3 10 -3 513.044 24.8841 2 10 -7 -3 483.502 23.7160 2 -7 -3 -3 507.238 23.6579 2 3 -10 3 509.642 26.1121 1 -10 7 3 532.741 29.1960 3 3 -10 3 479.043 31.2713 3 7 3 3 530.856 27.1025 1 3 -10 3 558.307 22.7364 2 -2 9 -3 801.002 34.9493 2 9 -7 -3 751.404 33.9389 2 -7 -2 -3 768.329 33.7863 2 2 -9 3 777.928 43.8584 3 2 -9 3 796.718 32.8789 2 7 2 3 757.623 37.6676 1 -9 7 3 828.438 41.8135 3 2 -9 3 813.659 36.8893 1 8 -7 -3 994.395 43.1214 2 -1 8 -3 964.043 43.8403 2 -7 -1 -3 1049.92 43.1046 2 -8 7 3 1046.48 53.1512 3 7 1 3 1014.47 47.4453 1 1 -8 3 1089.17 55.5720 3 1 -8 3 1061.67 46.7713 1 0 7 -3 198.934 12.4880 2 -7 0 -3 206.206 11.2749 2 7 -7 -3 191.673 11.3399 2 0 -7 3 220.144 18.0382 3 7 0 3 235.293 15.6570 1 -7 7 3 245.553 15.3909 3 -7 1 -3 343.732 15.8412 2 1 6 -3 324.797 16.8170 2 6 -7 -3 337.511 15.9603 2 -1 -6 3 342.378 23.3474 3 7 -1 3 356.402 19.7180 1 -6 7 3 349.244 20.6926 3 -7 2 -3 444.268 19.5981 2 5 -7 -3 456.594 19.7963 2 2 5 -3 438.091 20.4186 2 7 -2 3 431.453 23.7154 1 -2 -5 3 441.454 27.7698 3 4 -7 -3 72.7483 6.32885 2 -7 3 -3 67.1112 6.12809 2 3 4 -3 69.6915 6.12934 2 7 -3 3 78.8362 8.95091 1 -3 -4 3 71.2729 10.5149 3 -7 4 -3 63.2238 5.12567 2 3 -7 -3 69.8867 5.46528 2 4 3 -3 70.5643 5.92243 2 7 -4 3 50.0041 7.77910 1 -4 -3 3 60.5386 10.0700 3 5 2 -3 426.469 19.2948 2 -7 5 -3 423.076 18.9678 2 2 -7 -3 425.183 19.0993 2 -2 7 3 410.605 19.9659 1 -5 -2 3 412.530 26.4960 3 7 -5 3 448.391 22.7936 1 6 1 -3 485.732 21.3366 2 -7 6 -3 493.974 21.2521 2 1 -7 -3 475.269 21.2563 2 7 -6 3 464.798 24.6099 1 7 -6 3 433.517 27.0282 3 -1 7 3 470.740 22.0082 1 -6 -1 3 472.626 28.8391 3 0 -7 -3 210.759 11.1259 2 -7 7 -3 206.041 11.0495 2 7 0 -3 202.453 11.1485 2 7 -7 3 174.343 13.9381 1 7 -7 3 171.489 14.5361 3 0 7 3 171.517 11.0307 1 -7 0 3 167.677 16.4529 3 -7 8 -3 1234.12 51.7583 2 8 -1 -3 1217.28 51.6681 2 -1 -7 -3 1209.81 51.7338 2 1 7 3 1275.89 53.9091 1 7 -8 3 1258.34 63.9193 3 -8 1 3 1213.19 64.8450 3 7 -8 3 1297.92 55.9626 1 -7 9 -3 505.857 23.8728 2 9 -2 -3 531.446 23.7200 2 -2 -7 -3 531.116 23.8016 2 -9 2 3 521.302 30.7269 3 2 7 3 494.152 24.4662 1 7 -9 3 528.975 29.6710 3 7 -9 3 501.284 26.2272 1 -7 10 -3 272.615 15.5498 2 10 -3 -3 316.315 15.3977 2 -3 -7 -3 292.114 15.0710 2 7 -10 3 242.386 13.4197 2 7 -10 3 286.134 19.2559 3 3 7 3 300.576 15.8559 1 -10 3 3 271.825 19.9577 3 7 -10 3 267.278 17.3451 1 -10 3 3 272.145 13.5773 2 11 -4 -3 359.880 20.2325 2 -7 11 -3 404.034 21.4399 2 -4 -7 -3 416.477 20.4852 2 7 -11 3 411.236 19.2630 2 4 7 3 436.654 21.6598 1 7 -11 3 426.797 22.3645 1 7 -11 3 443.328 25.9320 3 -11 4 3 429.889 26.0397 3 12 -5 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3 43.5459 8.40717 3 -4 12 -3 306.924 19.5394 2 12 -8 -3 320.809 18.4573 2 -8 -4 -3 320.452 18.3567 2 -12 8 3 390.562 21.9351 3 4 -12 3 393.199 20.3292 1 4 -12 3 361.983 24.5230 3 11 -8 -3 315.204 16.9165 2 -3 11 -3 290.309 18.0753 2 -8 -3 -3 321.409 16.7239 2 3 -11 3 327.426 18.7267 1 3 -11 3 302.342 15.5472 2 -11 8 3 320.627 19.9992 3 3 -11 3 355.666 23.3406 3 -2 10 -3 238.603 15.8722 2 -8 -2 -3 250.391 14.5205 2 10 -8 -3 244.611 14.6087 2 2 -10 3 287.473 16.9572 1 2 -10 3 310.608 21.3720 3 2 -10 3 271.062 13.4661 2 -10 8 3 306.565 18.0379 3 9 -8 -3 808.518 34.4436 2 -1 9 -3 776.858 35.2530 2 -8 -1 -3 783.208 34.2425 2 -9 8 3 794.068 41.8702 3 1 -9 3 791.856 44.6828 3 1 -9 3 801.783 33.2901 2 0 8 -3 1871.57 75.5709 2 -8 0 -3 1852.72 74.7254 2 8 -8 -3 1931.17 75.0172 2 8 0 3 1746.57 80.5357 1 -8 8 3 1832.99 91.5233 3 0 -8 3 1809.41 74.0633 2 0 -8 3 1756.46 93.9794 3 7 -8 -3 156.973 10.0148 2 1 7 -3 166.403 11.2028 2 -8 1 -3 170.383 9.83093 2 -1 -7 3 146.409 16.3981 3 8 -1 3 158.275 14.1518 1 2 6 -3 643.484 28.2415 2 -8 2 -3 645.911 27.4563 2 6 -8 -3 671.468 27.6835 2 8 -2 3 582.044 31.5025 1 -2 -6 3 608.509 37.0522 3 -8 3 -3 614.625 26.8442 2 5 -8 -3 599.196 26.9672 2 3 5 -3 624.770 27.5856 2 8 -3 3 613.654 31.0097 1 -3 -5 3 670.579 36.5969 3 4 -8 -3 1354.44 55.2048 2 -8 4 -3 1328.17 54.9999 2 4 4 -3 1308.76 55.4010 2 -4 -4 3 1397.21 70.8384 3 8 -4 3 1317.41 60.1599 1 5 3 -3 386.126 18.1950 2 3 -8 -3 392.090 17.9795 2 -8 5 -3 376.857 17.7745 2 8 -5 3 372.650 21.6094 1 -5 -3 3 393.831 25.8460 3 -8 6 -3 672.612 29.8514 2 6 2 -3 688.794 30.1259 2 -8 6 -3 649.433 29.7311 2 2 -8 -3 697.547 30.0720 2 8 -6 3 706.586 33.7786 1 -2 8 3 697.842 30.7846 1 -6 -2 3 751.944 40.1045 3 -8 7 -3 84.3679 7.24934 2 1 -8 -3 103.648 8.36633 2 7 1 -3 78.2191 7.23621 2 -1 8 3 107.698 7.75415 1 -7 -1 3 96.5650 12.1862 3 8 -7 3 101.164 10.1956 1 8 -7 3 108.432 10.4872 3 8 0 -3 1701.96 69.9943 2 -8 8 -3 1659.28 69.9398 2 0 -8 -3 1672.42 69.9926 2 8 -8 3 1714.74 74.9045 1 0 8 3 1709.95 72.4274 1 8 -8 3 1718.12 85.8833 3 -8 0 3 1741.01 87.6102 3 -8 9 -3 959.311 40.5390 2 9 -1 -3 946.523 40.3382 2 -1 -8 -3 958.632 40.3404 2 8 -9 3 945.296 49.3961 3 -9 1 3 922.875 50.8403 3 8 -9 3 907.447 43.6553 1 1 8 3 950.421 41.3381 1 -9 1 3 919.144 39.0040 2 -2 -8 -3 324.720 16.6804 2 -8 10 -3 339.103 17.2587 2 10 -2 -3 334.834 16.6706 2 8 -10 3 318.205 20.4195 3 8 -10 3 300.305 18.5395 1 -10 2 3 302.319 22.2086 3 2 8 3 314.504 16.5448 1 -10 2 3 321.902 15.2140 2 8 -10 3 282.168 14.8728 2 11 -3 -3 567.583 26.7396 2 -3 -8 -3 564.539 26.6839 2 -8 11 -3 595.890 27.3677 2 8 -11 3 580.453 32.6577 3 3 8 3 559.535 27.2075 1 -11 3 3 576.893 33.8613 3 8 -11 3 587.815 29.2752 1 -4 -8 -3 233.892 14.7342 2 -8 12 -3 217.130 16.0074 2 12 -4 -3 238.951 14.8579 2 8 -12 3 231.746 15.8099 1 8 -12 3 257.084 18.1590 3 4 8 3 237.163 14.9026 1 -12 4 3 261.823 19.1912 3 -8 13 -3 44.8329 8.56743 2 13 -5 -3 31.9695 7.11314 2 -5 -8 -3 35.2813 6.99750 2 -13 5 3 39.5894 9.33811 3 5 8 3 31.4757 6.91781 1 8 -13 3 32.2981 8.57603 3 8 -13 3 34.2604 7.56243 1 -6 -8 -3 95.8223 9.83902 2 14 -6 -3 82.9459 9.54879 2 -8 14 -3 71.4128 10.3972 2 8 -14 3 117.999 12.7135 3 6 8 3 107.605 10.4313 1 -14 6 3 102.886 11.9303 3 8 -14 3 97.7259 10.2161 1 -8 15 -3 843.315 41.3788 2 -7 -8 -3 858.561 40.3467 2 15 -7 -3 888.121 40.6366 2 8 -15 3 900.547 41.8785 1 -15 7 3 851.492 48.1740 3 7 8 3 955.311 42.7563 1 8 -15 3 933.011 49.3464 3 16 -8 -3 221.336 15.9331 2 -8 16 -3 201.142 16.2783 2 -8 -8 -3 220.172 15.7717 2 -16 8 3 198.082 17.5631 3 8 -16 3 185.414 15.0534 1 8 -16 3 170.004 18.0346 3 17 -9 -3 52.0132 9.67686 2 -9 -8 -3 34.5405 8.83303 2 -8 17 -3 49.5007 11.0247 2 8 -17 3 43.8181 8.46380 1 8 -17 3 62.9150 11.9709 3 -9 -7 -3 176.745 14.9919 2 -7 16 -3 166.042 15.0589 2 16 -9 -3 175.818 15.4420 2 7 -16 3 188.360 14.9677 1 7 -16 3 202.691 18.7022 3 -16 9 3 187.868 16.2668 3 -9 -6 -3 158.721 13.5165 2 15 -9 -3 168.118 14.1391 2 -6 15 -3 159.701 13.9297 2 -15 9 3 144.597 14.3046 3 6 -15 3 133.930 12.0208 1 6 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25.6612 1 9 -13 3 543.375 27.5497 1 -13 4 3 537.722 31.9569 3 9 -13 3 546.835 30.5754 3 -9 14 -3 143.267 12.9150 2 -5 -9 -3 160.134 13.2034 2 14 -5 -3 148.040 11.8451 2 9 -14 3 127.609 12.0511 1 9 -14 3 131.121 14.4182 3 -14 5 3 116.369 13.7261 3 5 9 3 129.071 10.9225 1 -6 -9 -3 265.140 17.9995 2 -9 15 -3 315.609 20.5534 2 15 -6 -3 288.398 18.5579 2 6 9 3 306.166 18.4028 1 -15 6 3 263.695 21.0774 3 9 -15 3 267.844 21.0917 3 9 -15 3 299.203 18.6976 1 -7 -9 -3 320.079 20.0621 2 16 -7 -3 300.327 20.2767 2 -9 16 -3 320.000 21.4298 2 7 9 3 329.928 20.9452 1 9 -16 3 360.625 23.8961 3 -16 7 3 324.087 23.2398 3 9 -16 3 353.429 20.3967 1 -9 17 -3 57.8188 11.3968 2 17 -8 -3 47.4988 9.84322 2 -8 -9 -3 45.5326 9.22989 2 9 -17 3 52.1970 11.1667 3 -17 8 3 64.5812 10.7873 3 9 -17 3 44.1458 8.60226 1 8 9 3 44.1783 9.78054 1 -9 -9 -3 187.210 17.0563 2 -9 18 -3 195.124 17.1112 2 18 -9 -3 201.753 17.7046 2 9 -18 3 205.177 15.9348 1 9 -18 3 231.978 20.3252 3 -10 -9 -3 80.4048 11.8135 2 19 -10 -3 73.0262 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724.863 33.4196 2 -3 -8 -5 772.619 33.3114 2 3 8 5 736.704 36.1284 1 8 -11 5 722.927 38.3934 1 8 -11 5 695.875 43.3707 3 -11 3 5 691.617 43.8215 3 12 -4 -5 82.5441 9.79988 2 -4 -8 -5 103.327 9.90427 2 -8 12 -5 98.0465 11.2966 2 4 8 5 117.551 11.6424 1 -12 4 5 94.4333 15.3264 3 8 -12 5 122.233 14.1722 1 8 -12 5 108.444 15.5945 3 13 -5 -5 228.812 16.2879 2 -5 -8 -5 202.808 15.2381 2 -8 13 -5 189.149 17.1685 2 8 -13 5 227.126 20.2738 1 8 -13 5 244.886 22.8168 3 -13 5 5 215.324 22.7281 3 5 8 5 229.482 18.0917 1 14 -6 -5 240.792 17.2224 2 -6 -8 -5 244.491 16.5636 2 -8 14 -5 221.084 19.1839 2 6 8 5 227.841 19.1779 1 8 -14 5 226.725 23.3492 3 8 -14 5 217.210 20.0678 1 -14 6 5 245.296 23.3398 3 -8 15 -5 47.8154 10.8947 2 15 -7 -5 63.4896 9.93272 2 -7 -8 -5 55.9981 9.33507 2 -15 7 5 39.7997 13.3288 3 8 -15 5 61.6842 11.7989 1 7 8 5 70.6988 11.4480 1 8 -15 5 46.7707 13.6480 3 -8 -8 -5 163.499 14.0631 2 16 -8 -5 158.990 14.2727 2 -8 16 -5 178.014 16.2451 2 8 8 5 172.946 15.9410 1 -16 8 5 176.951 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54.7919 11.3731 2 8 -15 -7 45.2782 10.4676 2 15 -7 7 53.6017 18.7926 1 -7 -8 7 39.7408 22.7382 3 -15 8 -7 70.0428 11.8936 2 7 -15 -7 68.7316 10.8838 2 8 7 -7 65.5165 12.1131 2 15 -8 7 61.7696 18.8081 1 -8 -7 7 34.9858 22.4804 3 6 -15 -7 61.9798 11.1849 2 9 6 -7 56.7389 12.4129 2 -15 9 -7 47.3387 11.5244 2 -9 -6 7 25.8920 21.0507 3 15 -9 7 43.6014 17.8736 1 -15 10 -7 92.2993 13.3420 2 5 -15 -7 102.560 12.7384 2 10 5 -7 58.1892 12.4365 2 -10 -5 7 70.7141 24.3200 3 15 -10 7 92.9058 18.7599 1 11 4 -7 69.1549 12.7929 2 4 -15 -7 89.6919 12.5413 2 -15 11 -7 109.666 13.9825 2 -11 -4 7 75.8578 24.7353 3 15 -11 7 80.1632 19.1148 1 0 0 8 0.57239 15.1458 3 1 0 8 24.1839 14.5146 1 0 -1 8 21.2121 16.1127 3 -1 1 8 27.3774 17.6849 3 -1 0 8 30.6585 17.2468 3 1 -1 8 28.9554 16.3781 3 1 -1 8 52.2656 15.5060 1 -2 1 8 110.093 21.3704 3 1 -2 8 90.5812 20.2291 3 1 1 8 142.095 19.1486 1 1 -2 8 96.3840 17.6151 1 -3 2 8 32.3730 18.1865 3 2 1 8 25.1663 14.1231 1 1 -3 8 33.8932 18.3950 3 2 0 8 66.1232 15.6093 1 0 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7.16274 2 4 0 -8 79.5322 7.23257 2 4 -4 8 86.5775 17.6021 1 -4 0 8 32.8365 17.8606 3 5 -1 -8 137.971 10.7883 2 -4 5 -8 122.316 9.90489 2 -5 1 8 163.434 23.7592 3 1 4 8 164.035 19.0881 1 4 -5 8 147.263 20.6835 1 4 -5 8 145.647 23.1993 3 6 -2 -8 139.316 11.1421 2 -4 6 -8 142.180 10.9416 2 4 -6 8 140.118 22.6170 3 -6 2 8 120.745 21.6355 3 2 4 8 158.037 19.1409 1 4 -6 8 133.285 19.3741 1 -3 -4 -8 29.7112 5.60913 2 -4 7 -8 30.6320 8.17561 2 7 -3 -8 26.2840 6.64493 2 4 -7 8 18.9934 17.3028 3 -7 3 8 29.2010 18.1478 3 3 4 8 16.8945 14.4016 1 4 -7 8 35.7804 15.6808 1 -4 -4 -8 16.9550 5.79283 2 -4 8 -8 27.0331 8.46248 2 8 -4 -8 17.2820 6.72606 2 4 4 8 21.5789 14.6913 1 -8 4 8 11.0088 17.1646 3 4 -8 8 19.8042 17.6745 3 4 -8 8 9.73872 14.5962 1 -5 -4 -8 293.032 16.0775 2 9 -5 -8 309.447 17.6876 2 -4 9 -8 291.699 19.4340 2 4 -9 8 196.801 27.2858 3 5 4 8 306.426 26.0389 1 -9 5 8 290.185 30.6505 3 4 -9 8 246.059 25.3512 1 -3 8 -8 154.821 12.6280 2 8 -5 -8 154.216 12.6325 2 -5 -3 -8 135.757 11.2543 2 3 -8 8 151.458 24.6479 3 -8 5 8 117.994 21.9484 3 5 3 8 159.799 20.4483 1 -5 -2 -8 24.5103 5.56478 2 -2 7 -8 9.19671 7.58201 2 7 -5 -8 25.7232 6.40161 2 -7 5 8 6.66877 16.5652 3 5 2 8 21.6392 15.3330 1 2 -7 8 1.36212 16.0732 3 6 -5 -8 143.055 10.7135 2 -1 6 -8 130.993 10.7922 2 5 1 8 118.503 19.6818 1 -6 5 8 117.342 21.8557 3 1 -6 8 101.704 21.0461 3 0 5 -8 98.5723 8.99852 2 5 -5 -8 104.588 9.05888 2 0 -5 8 83.1266 20.8910 3 5 0 8 89.5994 18.3436 1 1 4 -8 121.011 9.55601 2 5 -1 8 153.930 20.7268 1 -1 -4 8 113.739 22.5231 3 2 3 -8 111.020 8.85851 2 -2 -3 8 96.4446 22.1909 3 5 -2 8 130.024 19.9726 1 3 2 -8 145.928 11.2573 2 5 -3 8 136.072 20.1857 1 -3 -2 8 136.316 23.4894 3 -5 4 -8 149.872 10.9508 2 4 1 -8 151.911 11.1525 2 -4 -1 8 97.6977 21.9511 3 5 -4 8 117.595 19.5891 1 -5 5 -8 162.285 12.2083 2 5 0 -8 172.252 12.1373 2 -5 0 8 131.228 23.0239 3 5 -5 8 185.429 22.4743 1 -5 6 -8 166.555 13.6016 2 6 -1 -8 199.938 12.8248 2 1 5 8 195.233 20.2849 1 5 -6 8 124.458 23.0549 3 -6 1 8 144.378 23.7398 3 5 -6 8 191.039 22.5742 1 7 -2 -8 16.2868 6.52643 2 -5 7 -8 16.5036 7.68034 2 -2 -5 -8 11.5069 5.33721 2 2 5 8 -6.7840 12.4513 1 -7 2 8 17.2934 17.6280 3 5 -7 8 21.2278 14.7285 1 5 -7 8 12.9357 16.4282 3 -3 -5 -8 102.270 8.52609 2 -5 8 -8 91.1713 11.0079 2 8 -3 -8 112.085 9.93949 2 -8 3 8 102.046 20.9005 3 3 5 8 117.618 18.3268 1 5 -8 8 103.067 19.0731 1 5 -8 8 105.609 21.0908 3 -4 -5 -8 143.540 12.1531 2 -5 9 -8 163.176 13.4263 2 9 -4 -8 168.590 13.7659 2 5 -9 8 169.298 25.0352 3 5 -9 8 165.039 21.8673 1 4 5 8 144.920 19.6600 1 -9 4 8 145.761 23.2727 3 -5 -5 -8 5.79655 6.36892 2 10 -5 -8 4.26579 7.32501 2 -5 10 -8 -2.3014 8.98639 2 5 -10 8 26.2733 17.2008 3 5 5 8 10.1527 14.8614 1 5 -10 8 11.6503 15.8431 1 -10 5 8 12.0196 17.1974 3 -5 11 -8 27.7730 10.4411 2 -6 -5 -8 37.6138 7.98222 2 11 -6 -8 27.8075 8.65648 2 6 5 8 32.1494 15.9004 1 -11 6 8 2.47270 17.5199 3 5 -11 8 31.3539 18.0796 3 5 -11 8 23.1217 15.8587 1 -4 10 -8 22.5952 9.59816 2 -6 -4 -8 20.8330 7.04968 2 10 -6 -8 30.1874 8.10311 2 4 -10 8 22.3168 17.6749 3 -10 6 8 23.1268 17.4846 3 6 4 8 20.3956 15.8783 1 -3 9 -8 16.5677 9.16578 2 -6 -3 -8 35.8714 6.94556 2 9 -6 -8 35.2081 7.74106 2 3 -9 8 28.4550 17.7766 3 -9 6 8 41.8196 18.9470 3 6 3 8 56.0472 16.8895 1 8 -6 -8 115.800 9.76594 2 -2 8 -8 108.210 11.1781 2 -6 -2 -8 115.756 8.94944 2 -8 6 8 86.2518 20.4295 3 6 2 8 81.5146 18.8186 1 2 -8 8 125.726 23.7473 3 -6 -1 -8 154.663 11.2183 2 7 -6 -8 166.540 12.3599 2 -1 7 -8 165.182 14.3692 2 1 -7 8 174.115 26.0801 3 6 1 8 162.526 21.7206 1 0 6 -8 43.0994 8.13368 2 6 -6 -8 53.4282 6.75319 2 -6 0 -8 46.5246 6.27387 2 0 -6 8 35.0309 19.3239 3 6 0 8 56.0716 17.5482 1 1 5 -8 118.352 9.93693 2 5 -6 -8 108.594 9.52477 2 -6 1 -8 109.817 9.29699 2 6 -1 8 94.2180 18.6735 1 -1 -5 8 81.8942 20.5862 3 4 -6 -8 115.021 9.52874 2 -6 2 -8 125.485 9.85704 2 2 4 -8 122.484 9.94947 2 6 -2 8 147.120 20.2284 1 -2 -4 8 133.141 23.9093 3 3 3 -8 66.2234 7.90797 2 -6 3 -8 60.4876 6.99315 2 6 -3 8 37.3236 17.0977 1 -3 -3 8 67.0285 20.5882 3 4 2 -8 96.1428 8.92668 2 -6 4 -8 110.836 8.76314 2 -4 -2 8 77.1904 21.1596 3 6 -4 8 74.8697 17.8796 1 5 1 -8 141.037 12.3285 2 -6 5 -8 134.025 10.2963 2 -5 -1 8 123.687 23.1754 3 6 -5 8 151.883 21.3283 1 -6 6 -8 38.8670 7.83852 2 6 0 -8 37.4397 7.32910 2 0 -6 -8 49.6696 6.59325 2 6 -6 8 25.7904 15.9257 1 -6 0 8 29.8310 18.1849 3 -1 -6 -8 134.236 10.6855 2 7 -1 -8 121.580 10.3397 2 -6 7 -8 126.821 10.9862 2 6 -7 8 97.2114 21.6233 3 1 6 8 122.303 17.4116 1 -7 1 8 125.261 23.5028 3 6 -7 8 96.9696 18.9710 1 -2 -6 -8 175.459 12.1900 2 8 -2 -8 147.000 11.9789 2 -6 8 -8 161.696 13.1879 2 -8 2 8 142.533 24.1359 3 6 -8 8 207.180 26.4412 3 2 6 8 158.280 18.8173 1 6 -8 8 197.370 23.3550 1 -6 9 -8 55.9939 10.2188 2 9 -3 -8 55.9947 8.67701 2 -3 -6 -8 58.3385 7.71199 2 3 6 8 26.5926 14.0388 1 6 -9 8 34.6661 17.7449 3 6 -9 8 37.7030 15.9337 1 -9 3 8 29.5080 18.4081 3 -6 10 -8 33.4583 10.0029 2 -4 -6 -8 43.8422 7.78678 2 10 -4 -8 42.0273 8.67508 2 -10 4 8 21.4275 18.0866 3 4 6 8 49.0143 15.7591 1 6 -10 8 34.9751 19.6160 3 6 -10 8 47.5337 16.7805 1 11 -5 -8 32.0649 8.76616 2 -5 -6 -8 36.5225 8.03558 2 -6 11 -8 38.8210 10.8920 2 -11 5 8 27.8221 18.2949 3 6 -11 8 25.6090 18.2584 3 5 6 8 24.2482 15.3578 1 6 -11 8 45.7128 17.3429 1 11 -7 -8 29.8649 8.58659 2 -7 -4 -8 26.8035 7.63783 2 -4 11 -8 38.8150 10.7976 2 7 4 8 19.0612 16.0334 1 4 -11 8 2.41813 16.7202 3 -11 7 8 27.5974 18.0376 3 -3 10 -8 26.1466 9.89002 2 -7 -3 -8 39.7454 7.75601 2 10 -7 -8 38.9130 8.27756 2 -10 7 8 37.3384 18.1692 3 7 3 8 64.0697 17.7679 1 3 -10 8 25.9677 17.5829 3 -2 9 -8 97.0343 11.5628 2 9 -7 -8 107.516 10.2066 2 -7 -2 -8 104.964 9.21855 2 7 2 8 102.839 19.2523 1 2 -9 8 83.5256 21.3431 3 -1 8 -8 113.418 11.3659 2 8 -7 -8 131.425 10.1819 2 -7 -1 -8 101.347 8.96976 2 7 1 8 94.2209 18.9675 1 1 -8 8 55.1380 19.4337 3 0 7 -8 6.28224 7.71708 2 -7 0 -8 14.1547 5.85085 2 7 -7 -8 9.55458 6.21375 2 7 0 8 23.1473 16.1473 1 0 -7 8 16.1004 16.8891 3 -7 1 -8 126.189 10.4870 2 6 -7 -8 121.969 9.50991 2 1 6 -8 120.086 11.0121 2 -1 -6 8 109.461 22.2088 3 7 -1 8 113.085 19.9755 1 -7 2 -8 202.305 12.6372 2 2 5 -8 187.815 14.4931 2 5 -7 -8 195.633 12.6437 2 7 -2 8 193.993 23.5216 1 -2 -5 8 183.031 26.2634 3 4 -7 -8 53.6247 6.71343 2 -7 3 -8 51.1871 7.18832 2 -7 3 -8 69.4229 7.18767 2 3 4 -8 49.8893 8.18463 2 7 -3 8 57.5404 18.0077 1 -3 -4 8 38.6543 19.4288 3 3 -7 -8 37.8567 6.44967 2 4 3 -8 36.9947 7.57591 2 -7 4 -8 39.5989 7.18433 2 7 -4 8 43.7491 17.5186 1 -4 -3 8 31.0156 18.9132 3 2 -7 -8 144.221 11.2341 2 5 2 -8 152.962 12.8444 2 -7 5 -8 154.032 12.7216 2 7 -5 8 124.231 20.0129 1 -5 -2 8 116.980 22.1535 3 -7 6 -8 124.879 10.6463 2 1 -7 -8 124.655 9.61405 2 6 1 -8 132.283 10.7815 2 7 -6 8 101.407 19.3204 1 -6 -1 8 118.032 22.8467 3 7 0 -8 14.0978 7.31670 2 -7 7 -8 8.07524 7.70875 2 0 -7 -8 14.7410 6.22364 2 -7 0 8 -8.4035 16.7927 3 7 -7 8 -3.3484 14.9282 1 -1 -7 -8 92.6432 9.05368 2 8 -1 -8 88.4776 9.69556 2 -7 8 -8 89.8156 10.6429 2 -8 1 8 77.6366 20.8079 3 7 -8 8 108.508 19.8158 1 1 7 8 130.641 17.0428 1 -7 9 -8 127.561 12.7997 2 9 -2 -8 138.435 11.8049 2 -2 -7 -8 130.971 10.6250 2 7 -9 8 103.298 22.0073 3 2 7 8 140.330 18.1502 1 7 -9 8 127.810 20.0245 1 -9 2 8 100.458 22.5947 3 -3 -7 -8 47.9990 7.98338 2 -7 10 -8 67.2722 11.0872 2 10 -3 -8 32.4337 8.65110 2 3 7 8 32.9913 13.9821 1 7 -10 8 9.89175 16.4262 3 7 -10 8 29.8313 16.2142 1 -10 3 8 50.9585 19.6184 3 -4 -7 -8 60.9011 8.91618 2 -7 11 -8 49.2410 11.2378 2 11 -4 -8 52.6767 9.74202 2 7 -11 8 56.2352 18.9618 3 7 -11 8 67.9833 18.0933 1 -11 4 8 39.5893 19.1039 3 4 7 8 50.0339 16.0772 1 3 -11 8 40.3535 18.9822 3 8 3 8 83.3401 18.5720 1 -2 10 -8 202.750 15.7134 2 10 -8 -8 186.200 15.3352 2 -8 -2 -8 197.451 14.4635 2 8 2 8 179.465 23.1982 1 2 -10 8 183.366 27.4389 3 -8 -1 -8 20.5868 6.96387 2 -1 9 -8 19.3165 9.16974 2 9 -8 -8 21.6459 7.45256 2 1 -9 8 12.5578 16.9757 3 8 1 8 11.9064 16.2994 1 8 -8 -8 99.3801 9.56973 2 0 8 -8 96.5117 11.1195 2 -8 0 -8 95.9012 8.99715 2 0 -8 8 57.2574 20.3787 3 8 0 8 90.4409 19.2551 1 1 7 -8 21.6616 8.49800 2 -8 1 -8 19.3487 6.52652 2 7 -8 -8 18.9806 6.71228 2 -1 -7 8 27.1957 18.5079 3 8 -1 8 36.3108 17.5179 1 2 6 -8 40.8237 8.63563 2 6 -8 -8 60.3326 7.56474 2 -8 2 -8 60.2908 7.40944 2 -2 -6 8 38.4354 19.3353 3 8 -2 8 23.8315 17.3203 1 3 5 -8 48.6170 8.65698 2 5 -8 -8 43.9047 7.03872 2 -8 3 -8 51.2234 7.36623 2 8 -3 8 33.2687 17.1309 1 -3 -5 8 19.6412 18.0040 3 4 -8 -8 205.649 13.5724 2 -8 4 -8 212.149 14.4445 2 4 4 -8 219.910 15.5176 2 -4 -4 8 167.970 26.0506 3 8 -4 8 220.128 24.5795 1 3 -8 -8 24.5131 6.70208 2 5 3 -8 22.1765 7.70554 2 -8 5 -8 22.1183 7.50711 2 8 -5 8 17.1326 16.6600 1 -5 -3 8 5.82485 17.1512 3 -8 6 -8 98.4019 10.0158 2 2 -8 -8 91.7659 9.09226 2 6 2 -8 81.6801 9.93947 2 8 -6 8 84.0310 19.0486 1 -6 -2 8 97.9973 23.1572 3 7 1 -8 29.5717 8.05682 2 -8 7 -8 29.3304 8.25522 2 1 -8 -8 16.7468 6.74999 2 -7 -1 8 16.3990 19.2412 3 8 -7 8 6.96476 15.7760 1 0 -8 -8 54.4814 8.07166 2 -8 8 -8 37.8878 9.36531 2 8 0 -8 51.4809 9.12206 2 -8 0 8 43.9332 20.4974 3 8 -8 8 69.4246 17.9695 1 -1 -8 -8 12.6653 7.17081 2 -8 9 -8 20.5866 9.17852 2 9 -1 -8 20.6049 8.19708 2 8 -9 8 34.4508 16.9834 1 -9 1 8 28.6035 18.2209 3 -8 10 -8 92.4362 12.1522 2 -2 -8 -8 99.2988 10.2634 2 10 -2 -8 116.185 11.6317 2 2 8 8 95.9975 16.8515 1 -10 2 8 98.0322 21.8347 3 8 -10 8 100.380 19.4164 1 8 -11 8 86.5947 20.5888 3 -11 3 8 60.8262 20.6832 3 8 -11 8 76.9016 19.1002 1 -1 10 -8 109.169 12.9095 2 10 -9 -8 139.122 11.7735 2 -9 -1 -8 136.223 11.1834 2 9 1 8 129.719 21.0459 1 1 -10 8 61.0981 21.0605 3 9 -9 -8 43.5067 8.50278 2 0 9 -8 41.8892 10.2589 2 -9 0 -8 47.1299 8.05844 2 0 -9 8 43.8009 19.9648 3 9 0 8 41.7889 18.0769 1 -9 1 -8 108.666 9.91656 2 8 -9 -8 123.207 10.6589 2 1 8 -8 101.267 11.8492 2 9 -1 8 106.677 20.7803 1 -1 -8 8 69.0825 21.5613 3 2 7 -8 173.129 13.4994 2 -9 2 -8 165.132 12.9029 2 7 -9 -8 154.068 13.0750 2 9 -2 8 145.629 22.6599 1 -2 -7 8 122.845 23.6696 3 -9 3 -8 158.994 12.9911 2 3 6 -8 138.944 12.5178 2 6 -9 -8 143.792 12.4695 2 -3 -6 8 157.162 27.0361 3 9 -3 8 173.132 22.9905 1 5 -9 -8 210.670 14.6152 2 -9 4 -8 213.909 15.5811 2 4 5 -8 200.109 16.7862 2 -4 -5 8 230.969 29.6094 3 9 -4 8 297.566 27.5196 1 -9 5 -8 159.884 11.9871 2 4 -9 -8 147.259 11.4676 2 5 4 -8 149.630 12.4688 2 -5 -4 8 118.004 25.6837 3 9 -5 8 120.176 21.4002 1 6 3 -8 168.763 13.1960 2 -9 6 -8 162.277 12.6263 2 3 -9 -8 146.281 11.6887 2 -6 -3 8 150.623 25.9603 3 9 -6 8 165.273 22.1580 1 2 -9 -8 170.580 13.6173 2 7 2 -8 164.362 13.3273 2 -9 7 -8 163.392 13.2802 2 9 -7 8 146.421 21.7670 1 -7 -2 8 161.870 26.8962 3 1 -9 -8 157.525 12.2604 2 8 1 -8 160.151 13.2179 2 -9 8 -8 143.448 12.9517 2 9 -8 8 151.232 22.3378 1 -8 -1 8 149.754 26.2336 3 9 0 -8 74.9777 10.3215 2 -9 9 -8 67.0619 10.7858 2 0 -9 -8 57.3046 8.94550 2 -9 0 8 42.4380 20.6353 3 9 -9 8 56.9136 17.8028 1 -9 10 -8 205.941 16.0185 2 -1 -9 -8 206.671 15.5093 2 10 -1 -8 186.763 14.7363 2 9 -10 8 184.905 23.4826 1 -10 1 8 142.962 26.0215 3 1 9 -8 119.575 12.8714 2 -10 1 -8 120.668 10.7063 2 9 -10 -8 108.203 10.9271 2 -1 -9 8 86.3237 21.6813 3 10 -1 8 94.5186 20.2559 1 2 8 -8 41.3186 9.98744 2 -10 2 -8 35.0787 7.95490 2 8 -10 -8 37.7476 8.08902 2 10 -2 8 9.94456 17.7001 1 -2 -8 8 11.4590 18.3581 3 3 7 -8 35.4129 9.77601 2 7 -10 -8 45.5667 8.25244 2 -10 3 -8 44.7025 8.30476 2 10 -3 8 69.8596 19.4232 1 -3 -7 8 59.9022 22.1878 3 -10 4 -8 26.3590 8.21066 2 4 6 -8 26.6101 9.14360 2 -10 4 -8 26.8993 7.67635 2 6 -10 -8 23.4176 7.43397 2 -4 -6 8 18.4387 18.9559 3 10 -4 8 1.85832 16.4607 1 5 -10 -8 27.2353 7.75387 2 5 5 -8 12.4816 8.63976 2 -10 5 -8 22.2190 8.28121 2 10 -5 8 16.9592 17.6650 1 -5 -5 8 28.8938 19.4792 3 -10 6 -8 44.3855 9.28531 2 4 -10 -8 46.4960 8.32334 2 6 4 -8 26.4410 8.95082 2 -6 -4 8 20.6141 20.3060 3 10 -6 8 51.1134 17.7824 1 3 -10 -8 84.6957 10.0027 2 -10 7 -8 100.938 11.3746 2 7 3 -8 90.1190 11.1208 2 -7 -3 8 65.6512 22.2850 3 10 -7 8 76.1141 19.0442 1 2 -10 -8 10.9929 7.67621 2 8 2 -8 10.3393 8.71016 2 -10 8 -8 12.6872 8.93828 2 -8 -2 8 37.5572 21.0195 3 10 -8 8 14.1341 16.1348 1 1 -10 -8 146.305 12.3802 2 9 1 -8 126.862 12.7368 2 -10 9 -8 133.754 13.0306 2 10 -9 8 119.554 21.7843 1 -9 -1 8 71.7113 23.3928 3 11 -3 8 75.1005 20.6086 1 -3 -8 8 54.0258 21.8467 3 -11 4 -8 40.7341 8.43969 2 4 7 -8 48.3466 10.5306 2 -11 4 -8 32.9448 8.94209 2 7 -11 -8 37.3019 8.38640 2 -4 -7 8 15.8806 19.5339 3 11 -4 8 27.5329 19.1806 1 5 6 -8 47.0040 10.2074 2 -11 5 -8 37.4161 9.48386 2 6 -11 -8 55.1420 9.01494 2 11 -5 8 40.8932 19.1038 1 -5 -6 8 27.0029 19.4143 3 -11 6 -8 46.5043 9.63018 2 6 5 -8 34.4387 10.0439 2 5 -11 -8 58.6487 9.42703 2 11 -6 8 39.6264 18.4858 1 -6 -5 8 26.4300 19.8256 3 4 -11 -8 97.3303 10.6651 2 -11 7 -8 72.7472 11.0698 2 7 4 -8 80.3161 11.4884 2 11 -7 8 63.3039 18.9559 1 -7 -4 8 43.6614 22.2655 3 -8 -3 8 50.7724 21.4668 3 11 -8 8 76.1516 19.2382 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 69484 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z+2/3' '-x+y, -x, z+1/3' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Br1 Br 0.82002(3) 0.81429(3) 0.63910(5) 0.01623(8) Uani 1 1 d . . O1 O 1.0018(2) 0.7784(2) 0.3395(5) 0.0162(6) Uani 1 1 d . . O2 O 1.01396(19) 0.95407(18) 0.7152(5) 0.0143(6) Uani 1 1 d . . H2 H 0.9846 0.9633 0.8055 0.021 Uiso 1 1 calc R U C1 C 0.9235(3) 0.8031(3) 0.5888(6) 0.0111(8) Uani 1 1 d . . C2 C 0.9496(3) 0.8198(3) 0.3465(6) 0.0135(8) Uani 1 1 d . . H2A H 0.9800 0.8820 0.3015 0.016 Uiso 1 1 calc R U C3 C 0.8726(3) 0.7599(3) 0.2126(7) 0.0177(9) Uani 1 1 d . . H3 H 0.8386 0.7754 0.1261 0.021 Uiso 1 1 calc R U C4 C 0.8613(3) 0.6805(3) 0.2392(7) 0.0213(9) Uani 1 1 d . . H4 H 0.8182 0.6280 0.1756 0.026 Uiso 1 1 calc R U C5 C 0.9321(3) 0.6924(3) 0.3927(7) 0.0191(9) Uani 1 1 d . . H5 H 0.9479 0.6458 0.3870 0.023 Uiso 1 1 calc R U C6 C 0.9073(3) 0.7098(3) 0.6194(7) 0.0173(9) Uani 1 1 d . . H6A H 0.8460 0.6684 0.6545 0.021 Uiso 1 1 calc R U H6B H 0.9452 0.7073 0.7317 0.021 Uiso 1 1 calc R U C7 C 0.9957(3) 0.8667(3) 0.7338(7) 0.0132(7) Uani 1 1 d . . H7A H 0.9797 0.8476 0.8838 0.016 Uiso 1 1 calc R U H7B H 1.0491 0.8648 0.7009 0.016 Uiso 1 1 calc R U Br1A Br 0.49976(3) 0.37029(3) 0.55722(7) 0.02189(10) Uani 1 1 d . . O1A O 0.7013(2) 0.5599(2) 0.8894(6) 0.0191(6) Uani 1 1 d . . O2A O 0.6865(2) 0.3962(2) 0.4827(5) 0.0180(6) Uani 1 1 d . . H2AA H 0.6575 0.3630 0.3823 0.027 Uiso 1 1 calc R U C1A C 0.6132(3) 0.4721(3) 0.6243(6) 0.0132(8) Uani 1 1 d . . C2A C 0.6370(3) 0.4699(3) 0.8617(6) 0.0147(8) Uani 1 1 d . . H2AB H 0.6572 0.4279 0.8949 0.018 Uiso 1 1 calc R U C3A C 0.5634(3) 0.4616(3) 1.0013(6) 0.0187(9) Uani 1 1 d . . H3A H 0.5228 0.4119 1.0791 0.022 Uiso 1 1 calc R U C4A C 0.5678(3) 0.5373(3) 0.9919(7) 0.0225(10) Uani 1 1 d . . H4A H 0.5312 0.5541 1.0628 0.027 Uiso 1 1 calc R U C5A C 0.6434(3) 0.5928(3) 0.8443(7) 0.0203(9) Uani 1 1 d . . H5A H 0.6693 0.6568 0.8633 0.024 Uiso 1 1 calc R U C6A C 0.6134(3) 0.5595(3) 0.6147(7) 0.0202(9) Uani 1 1 d . . H6AA H 0.6548 0.5992 0.5066 0.024 Uiso 1 1 calc R U H6AB H 0.5549 0.5505 0.5850 0.024 Uiso 1 1 calc R U C7A C 0.6813(3) 0.4730(3) 0.4730(7) 0.0149(8) Uani 1 1 d . . H7AA H 0.6672 0.4811 0.3248 0.018 Uiso 1 1 calc R U H7AB H 0.7386 0.5231 0.5090 0.018 Uiso 1 1 calc R U Br1B Br 0.35969(3) 0.49367(4) 0.23527(7) 0.02450(11) Uani 1 1 d . . O1B O 0.1387(2) 0.4321(2) 0.5583(5) 0.0222(7) Uani 1 1 d . . O2B O 0.2780(2) 0.6129(2) 0.1679(5) 0.0202(7) Uani 1 1 d . . H2B H 0.3205 0.6268 0.0867 0.030 Uiso 1 1 calc R U C1B C 0.2411(3) 0.4684(3) 0.2980(7) 0.0124(8) Uani 1 1 d . . C2B C 0.2316(3) 0.4843(3) 0.5386(7) 0.0156(8) Uani 1 1 d . . H2BA H 0.2566 0.5465 0.5803 0.019 Uiso 1 1 calc R U C3B C 0.2623(3) 0.4331(3) 0.6722(7) 0.0221(10) Uani 1 1 d . . H3B H 0.3144 0.4554 0.7522 0.026 Uiso 1 1 calc R U C4B C 0.2015(4) 0.3520(3) 0.6531(7) 0.0248(11) Uani 1 1 d . . H4B H 0.2000 0.3034 0.7199 0.030 Uiso 1 1 calc R U C5B C 0.1344(3) 0.3506(3) 0.5052(7) 0.0211(9) Uani 1 1 d . . H5B H 0.0755 0.2981 0.5171 0.025 Uiso 1 1 calc R U C6B C 0.1731(3) 0.3708(3) 0.2767(7) 0.0173(9) Uani 1 1 d . . H6BA H 0.2006 0.3360 0.2404 0.021 Uiso 1 1 calc R U H6BB H 0.1286 0.3608 0.1681 0.021 Uiso 1 1 calc R U C7B C 0.2193(3) 0.5231(3) 0.1503(7) 0.0158(9) Uani 1 1 d . . H7BA H 0.2192 0.5049 0.0008 0.019 Uiso 1 1 calc R U H7BB H 0.1602 0.5117 0.1839 0.019 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0120(2) 0.0203(2) 0.01714(17) -0.00109(16) 0.00145(16) 0.00858(17) O1 0.0143(15) 0.0162(15) 0.0200(14) -0.0007(12) 0.0039(13) 0.0090(14) O2 0.0171(17) 0.0102(14) 0.0134(13) 0.0003(10) 0.0031(11) 0.0051(13) C1 0.0106(19) 0.0106(18) 0.0131(17) 0.0025(14) 0.0040(14) 0.0061(16) C2 0.014(2) 0.011(2) 0.0129(18) 0.0004(14) 0.0007(15) 0.0046(16) C3 0.014(2) 0.026(3) 0.0109(17) -0.0020(16) 0.0004(16) 0.0079(19) C4 0.025(3) 0.017(2) 0.0153(19) -0.0055(17) 0.0012(18) 0.006(2) C5 0.024(2) 0.015(2) 0.021(2) 0.0007(17) 0.0050(18) 0.011(2) C6 0.022(2) 0.014(2) 0.0154(19) 0.0031(16) 0.0001(16) 0.0080(19) C7 0.0132(19) 0.014(2) 0.0131(14) -0.0001(15) -0.0011(18) 0.0079(19) Br1A 0.0146(2) 0.0222(3) 0.01830(19) -0.0022(2) -0.00037(18) 0.0012(2) O1A 0.0159(16) 0.0171(16) 0.0219(15) -0.0043(13) -0.0016(12) 0.0064(13) O2A 0.0239(18) 0.0196(16) 0.0149(14) -0.0044(11) -0.0050(13) 0.0142(15) C1A 0.013(2) 0.011(2) 0.0138(18) 0.0025(15) -0.0008(14) 0.0049(17) C2A 0.019(2) 0.012(2) 0.0137(18) -0.0001(14) -0.0020(15) 0.0080(18) C3A 0.019(2) 0.022(2) 0.0120(18) -0.0004(16) 0.0016(16) 0.0086(19) C4A 0.023(2) 0.027(3) 0.021(2) 0.0004(18) 0.0057(18) 0.015(2) C5A 0.025(2) 0.013(2) 0.025(2) -0.0007(17) 0.0031(18) 0.0112(19) C6A 0.025(3) 0.020(2) 0.022(2) 0.0073(17) 0.0035(18) 0.015(2) C7A 0.014(2) 0.015(2) 0.0134(18) 0.0006(15) 0.0006(15) 0.0054(17) Br1B 0.0150(2) 0.0339(3) 0.0254(2) 0.0049(2) 0.0029(2) 0.0129(2) O1B 0.0235(18) 0.0213(18) 0.0232(16) 0.0043(13) 0.0079(14) 0.0123(15) O2B 0.0289(19) 0.0117(15) 0.0192(16) 0.0022(12) 0.0078(13) 0.0095(14) C1B 0.011(2) 0.0109(19) 0.0151(18) -0.0011(15) 0.0019(14) 0.0054(17) C2B 0.020(2) 0.013(2) 0.0124(18) 0.0009(15) 0.0017(15) 0.0079(18) C3B 0.031(3) 0.029(3) 0.0110(19) 0.0011(17) -0.0029(17) 0.018(2) C4B 0.039(3) 0.022(3) 0.016(2) 0.0046(18) 0.0022(19) 0.018(2) C5B 0.025(2) 0.013(2) 0.021(2) 0.0047(16) 0.0069(18) 0.0053(19) C6B 0.018(2) 0.0108(19) 0.0188(19) -0.0010(16) -0.0010(16) 0.0040(18) C7B 0.019(2) 0.013(2) 0.0152(18) 0.0007(15) 0.0026(16) 0.0077(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 O1 C5 95.9(3) C7 O2 H2 109.5 C2 C1 Br1 109.8(3) C6 C1 Br1 114.0(3) C6 C1 C2 101.6(3) C7 C1 Br1 108.4(3) C7 C1 C2 112.1(3) C7 C1 C6 111.0(3) O1 C2 C1 97.9(3) O1 C2 H2A 115.2 O1 C2 C3 102.2(3) C1 C2 H2A 115.2 C3 C2 C1 109.0(3) C3 C2 H2A 115.2 C2 C3 H3 126.8 C4 C3 C2 106.5(4) C4 C3 H3 126.8 C3 C4 H4 127.6 C3 C4 C5 104.9(4) C5 C4 H4 127.6 O1 C5 C4 102.4(3) O1 C5 H5 114.9 O1 C5 C6 100.2(3) C4 C5 H5 114.9 C4 C5 C6 107.8(4) C6 C5 H5 114.9 C1 C6 C5 100.4(3) C1 C6 H6A 111.7 C1 C6 H6B 111.7 C5 C6 H6A 111.7 C5 C6 H6B 111.7 H6A C6 H6B 109.5 O2 C7 C1 114.3(3) O2 C7 H7A 108.7 O2 C7 H7B 108.7 C1 C7 H7A 108.7 C1 C7 H7B 108.7 H7A C7 H7B 107.6 C2A O1A C5A 95.5(3) C7A O2A H2AA 109.5 C2A C1A Br1A 110.4(3) C2A C1A C6A 101.4(3) C6A C1A Br1A 113.6(3) C7A C1A Br1A 108.7(3) C7A C1A C2A 111.6(4) C7A C1A C6A 111.1(3) O1A C2A C1A 99.4(3) O1A C2A H2AB 115.0 O1A C2A C3A 101.9(3) C1A C2A H2AB 115.0 C3A C2A C1A 108.7(4) C3A C2A H2AB 115.0 C2A C3A H3A 127.2 C4A C3A C2A 105.6(4) C4A C3A H3A 127.2 C3A C4A H4A 127.1 C3A C4A C5A 105.8(4) C5A C4A H4A 127.1 O1A C5A C4A 101.4(4) O1A C5A H5A 115.0 O1A C5A C6A 101.9(3) C4A C5A H5A 115.0 C4A C5A C6A 107.0(4) C6A C5A H5A 115.0 C1A C6A H6AA 111.7 C1A C6A H6AB 111.7 C5A C6A C1A 100.1(3) C5A C6A H6AA 111.7 C5A C6A H6AB 111.7 H6AA C6A H6AB 109.5 O2A C7A C1A 113.4(3) O2A C7A H7AA 108.9 O2A C7A H7AB 108.9 C1A C7A H7AA 108.9 C1A C7A H7AB 108.9 H7AA C7A H7AB 107.7 C2B O1B C5B 95.4(3) C7B O2B H2B 109.5 C2B C1B Br1B 110.7(3) C6B C1B Br1B 112.8(3) C6B C1B C2B 101.1(3) C7B C1B Br1B 108.6(3) C7B C1B C2B 112.6(3) C7B C1B C6B 111.0(3) O1B C2B C1B 99.2(3) O1B C2B H2BA 115.1 O1B C2B C3B 101.9(4) C1B C2B H2BA 115.1 C3B C2B C1B 108.5(4) C3B C2B H2BA 115.1 C2B C3B H3B 127.4 C4B C3B C2B 105.3(4) C4B C3B H3B 127.4 C3B C4B H4B 126.7 C3B C4B C5B 106.7(4) C5B C4B H4B 126.7 O1B C5B C4B 101.4(4) O1B C5B H5B 115.1 O1B C5B C6B 100.6(3) C4B C5B H5B 115.1 C4B C5B C6B 107.9(4) C6B C5B H5B 115.1 C1B C6B C5B 100.9(3) C1B C6B H6BA 111.6 C1B C6B H6BB 111.6 C5B C6B H6BA 111.6 C5B C6B H6BB 111.6 H6BA C6B H6BB 109.4 O2B C7B C1B 113.4(4) O2B C7B H7BA 108.9 O2B C7B H7BB 108.9 C1B C7B H7BA 108.9 C1B C7B H7BB 108.9 H7BA C7B H7BB 107.7 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Br1 C1 1.975(4) O1 C2 1.448(5) O1 C5 1.448(6) O2 H2 0.8400 O2 C7 1.427(5) C1 C2 1.570(6) C1 C6 1.552(6) C1 C7 1.518(6) C2 H2A 1.0000 C2 C3 1.503(6) C3 H3 0.9500 C3 C4 1.336(7) C4 H4 0.9500 C4 C5 1.514(7) C5 H5 1.0000 C5 C6 1.562(6) C6 H6A 0.9900 C6 H6B 0.9900 C7 H7A 0.9900 C7 H7B 0.9900 Br1A C1A 1.970(4) O1A C2A 1.440(5) O1A C5A 1.447(6) O2A H2AA 0.8400 O2A C7A 1.419(5) C1A C2A 1.551(6) C1A C6A 1.556(6) C1A C7A 1.532(6) C2A H2AB 1.0000 C2A C3A 1.519(6) C3A H3A 0.9500 C3A C4A 1.314(7) C4A H4A 0.9500 C4A C5A 1.521(7) C5A H5A 1.0000 C5A C6A 1.544(6) C6A H6AA 0.9900 C6A H6AB 0.9900 C7A H7AA 0.9900 C7A H7AB 0.9900 Br1B C1B 1.967(4) O1B C2B 1.442(6) O1B C5B 1.454(6) O2B H2B 0.8400 O2B C7B 1.412(5) C1B C2B 1.558(6) C1B C6B 1.549(6) C1B C7B 1.527(6) C2B H2BA 1.0000 C2B C3B 1.525(6) C3B H3B 0.9500 C3B C4B 1.308(7) C4B H4B 0.9500 C4B C5B 1.502(7) C5B H5B 1.0000 C5B C6B 1.550(6) C6B H6BA 0.9900 C6B H6BB 0.9900 C7B H7BA 0.9900 C7B H7BB 0.9900