#------------------------------------------------------------------------------ #$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $ #$Revision: 176729 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/51/64/1516476.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1516476 loop_ _publ_author_name 'Liu, Siqian' 'Du, Gaixia' 'He, Jianyun' 'Long, Yingyun' 'Zhang, Shaowen' 'Li, Xiaofang' _publ_section_title ; Cationic Tropidinyl Scandium Catalyst: A Perfectly Acceptable Substitute for Cationic Half-Sandwich Scandium Catalysts incis-1,4-Polymerization of Isoprene and Copolymerization with Norbornene ; _journal_issue 11 _journal_name_full Macromolecules _journal_page_first 3567 _journal_paper_doi 10.1021/ma500740m _journal_volume 47 _journal_year 2014 _chemical_formula_sum 'C16 H31 Lu N O Si' _chemical_formula_weight 456.48 _chemical_name_systematic ; ? ; _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 19.256(2) _cell_length_b 10.1640(10) _cell_length_c 18.2180(18) _cell_measurement_temperature 173(2) _cell_volume 3565.6(6) _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _diffrn_ambient_temperature 173(2) _diffrn_measured_fraction_theta_full 0.985 _diffrn_measured_fraction_theta_max 0.984 _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0324 _diffrn_reflns_av_unetI/netI 0.0363 _diffrn_reflns_Laue_measured_fraction_full 0.985 _diffrn_reflns_Laue_measured_fraction_max 0.984 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 24520 _diffrn_reflns_point_group_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.402 _diffrn_reflns_theta_min 5.587 _exptl_absorpt_coefficient_mu 5.601 _exptl_crystal_density_diffrn 1.701 _exptl_crystal_F_000 1816 _exptl_crystal_size_max 0.450 _exptl_crystal_size_mid 0.430 _exptl_crystal_size_min 0.420 _refine_diff_density_max 1.139 _refine_diff_density_min -0.886 _refine_diff_density_rms 0.113 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.510(11) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 369 _refine_ls_number_reflns 8722 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.046 _refine_ls_R_factor_all 0.0306 _refine_ls_R_factor_gt 0.0245 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0092P)^2^+6.0782P] where P=(Fo^2^+2Fc^2^)/3 ; _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0448 _refine_ls_wR_factor_ref 0.0466 _reflns_Friedel_coverage 0.942 _reflns_Friedel_fraction_full 0.988 _reflns_Friedel_fraction_max 0.986 _reflns_number_gt 8002 _reflns_number_total 8722 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ma500740m_si_003.cif _cod_data_source_block aa _cod_depositor_comments 'Adding full bibliography for 1516474--1516476.cif.' _cod_original_cell_volume 3565.7(6) _cod_database_code 1516476 #BEGIN Tags that were not found in dictionaries: _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.187 _shelx_estimated_absorpt_t_max 0.202 _shelxl_version_number 2013-2 _shelx_res_file ; TITL aa in Pna2(1) CELL 0.71073 19.2564 10.1640 18.2180 90.000 90.000 90.000 ZERR 8 0.0020 0.0010 0.0018 0.000 0.000 0.000 LATT -1 SYMM -X, -Y, 0.5+Z SYMM 0.5+X, 0.5-Y, Z SYMM 0.5-X, 0.5+Y, 0.5+Z SFAC C H N O Si Lu UNIT 128 248 8 8 8 8 REM OMIT -3.00 50.04 L.S. 40 ACTA BOND $H FMAP 2 PLAN 5 SIZE 0.45 0.43 0.42 TEMP -100 CONF TWIN WGHT 0.009200 6.078200 BASF 0.51021 FVAR 0.07180 LU1 6 0.058395 0.542251 0.211388 11.00000 0.01449 0.01520 = 0.01686 0.00024 -0.00006 0.00134 LU2 6 0.195685 0.329100 0.167143 11.00000 0.01443 0.01429 = 0.01486 -0.00035 0.00056 0.00085 SI1 5 0.032307 0.796016 0.359202 11.00000 0.02444 0.02136 = 0.01914 -0.00323 0.00514 0.00155 SI2 5 0.211676 0.074337 0.012102 11.00000 0.02402 0.01609 = 0.01696 -0.00155 0.00131 0.00079 N1 3 0.109653 0.354065 0.257440 11.00000 0.01514 0.01588 = 0.01877 0.00076 0.00402 -0.00050 N2 3 0.143636 0.520026 0.122977 11.00000 0.01796 0.01423 = 0.02001 0.00254 0.00060 -0.00081 O1 4 0.011958 0.715125 0.138465 11.00000 0.02291 0.01950 = 0.03080 0.00509 -0.00945 0.00140 O2 4 0.236498 0.157188 0.241378 11.00000 0.02233 0.01915 = 0.02160 0.00320 -0.00719 0.00282 C1 1 0.089802 0.702354 0.297935 11.00000 0.02629 0.01749 = 0.01756 0.00045 -0.00331 0.00141 AFIX 23 H1A 2 0.123831 0.658803 0.330629 11.00000 -1.20000 H1B 2 0.116231 0.769328 0.270069 11.00000 -1.20000 AFIX 0 C2 1 0.007357 0.697200 0.440936 11.00000 0.05264 0.03798 = 0.02300 -0.00643 0.01202 -0.00411 AFIX 137 H2A 2 -0.021547 0.622832 0.425481 11.00000 -1.50000 H2B 2 -0.018831 0.752520 0.475212 11.00000 -1.50000 H2C 2 0.049299 0.664161 0.465196 11.00000 -1.50000 AFIX 0 C3 1 -0.049304 0.854873 0.312256 11.00000 0.02897 0.04666 = 0.03664 -0.00341 -0.00027 0.02007 AFIX 137 H3A 2 -0.038378 0.930629 0.281047 11.00000 -1.50000 H3B 2 -0.083554 0.880766 0.349330 11.00000 -1.50000 H3C 2 -0.068373 0.783800 0.282006 11.00000 -1.50000 AFIX 0 C4 1 0.074125 0.948058 0.397260 11.00000 0.03824 0.02957 = 0.03454 -0.00728 0.00365 0.00251 AFIX 137 H4A 2 0.116727 0.923955 0.423434 11.00000 -1.50000 H4B 2 0.042005 0.991437 0.431251 11.00000 -1.50000 H4C 2 0.085493 1.008231 0.356983 11.00000 -1.50000 AFIX 0 C5 1 0.052054 0.256681 0.246313 11.00000 0.02726 0.01272 = 0.02880 0.00244 0.01263 0.00272 AFIX 3 H5 2 0.073134 0.167071 0.242193 11.00000 -1.20000 AFIX 0 C6 1 0.015088 0.288085 0.173837 11.00000 0.01990 0.02534 = 0.02782 -0.00291 -0.00132 -0.00459 AFIX 43 H6 2 0.030716 0.242361 0.131462 11.00000 -1.20000 AFIX 0 C7 1 -0.037249 0.373936 0.164366 11.00000 0.01969 0.02973 = 0.02072 -0.00175 -0.00142 -0.00987 AFIX 43 H7 2 -0.058021 0.371409 0.117088 11.00000 -1.20000 AFIX 0 C8 1 -0.066920 0.468158 0.213152 11.00000 0.01833 0.02515 = 0.03068 0.00227 0.00031 0.00228 AFIX 43 H8 2 -0.096651 0.532508 0.192111 11.00000 -1.20000 AFIX 0 C9 1 -0.056254 0.474969 0.290243 11.00000 0.01440 0.02040 = 0.03382 -0.00258 0.00414 -0.00201 AFIX 43 H9 2 -0.074465 0.550731 0.313952 11.00000 -1.20000 AFIX 0 C10 1 -0.023842 0.388360 0.333785 11.00000 0.02387 0.02705 = 0.03247 -0.00102 0.00875 -0.00791 AFIX 23 H10A 2 -0.054716 0.375202 0.376612 11.00000 -1.20000 H10B 2 0.017996 0.433945 0.352509 11.00000 -1.20000 AFIX 0 C11 1 -0.000451 0.254752 0.311266 11.00000 0.02225 0.02391 = 0.02954 0.00420 0.00421 -0.00034 AFIX 23 H11A 2 -0.041511 0.202109 0.296883 11.00000 -1.20000 H11B 2 0.021495 0.210846 0.353868 11.00000 -1.20000 AFIX 0 C12 1 0.139250 0.349201 0.331766 11.00000 0.02651 0.03125 = 0.01769 0.00288 0.00072 0.00797 AFIX 33 H12A 2 0.102058 0.359885 0.367996 11.00000 -1.50000 H12B 2 0.173211 0.420255 0.337570 11.00000 -1.50000 H12C 2 0.162215 0.264218 0.339283 11.00000 -1.50000 AFIX 0 C13 1 -0.047591 0.704035 0.089620 11.00000 0.03073 0.04110 = 0.04750 0.01475 -0.01748 -0.00380 AFIX 23 H13A 2 -0.091529 0.709955 0.117643 11.00000 -1.20000 H13B 2 -0.046641 0.619227 0.062913 11.00000 -1.20000 AFIX 0 C14 1 -0.041115 0.816241 0.037657 11.00000 0.03466 0.04305 = 0.04968 0.02188 -0.01819 -0.00320 AFIX 23 H14A 2 -0.086861 0.841609 0.017294 11.00000 -1.20000 H14B 2 -0.009110 0.795024 -0.003190 11.00000 -1.20000 AFIX 0 C15 1 -0.011472 0.924586 0.086665 11.00000 0.03827 0.02621 = 0.03810 0.01091 -0.00128 0.00878 AFIX 23 H15A 2 0.012823 0.992326 0.057250 11.00000 -1.20000 H15B 2 -0.048474 0.967213 0.115953 11.00000 -1.20000 AFIX 0 C16 1 0.038987 0.850200 0.135626 11.00000 0.02758 0.02394 = 0.03077 0.00460 -0.00486 -0.00397 AFIX 23 H16A 2 0.086373 0.851662 0.114563 11.00000 -1.20000 H16B 2 0.040424 0.889445 0.185338 11.00000 -1.20000 AFIX 0 C17 1 0.161405 0.167300 0.080409 11.00000 0.01623 0.01930 = 0.01548 0.00373 0.00168 0.00350 AFIX 23 H17A 2 0.137986 0.098886 0.110132 11.00000 -1.20000 H17B 2 0.124154 0.210204 0.051603 11.00000 -1.20000 AFIX 0 C18 1 0.236423 0.183261 -0.066822 11.00000 0.04664 0.03435 = 0.02101 0.00065 0.01160 -0.01087 AFIX 137 H18A 2 0.195624 0.232850 -0.083210 11.00000 -1.50000 H18B 2 0.253837 0.129152 -0.107363 11.00000 -1.50000 H18C 2 0.272734 0.244675 -0.051117 11.00000 -1.50000 AFIX 0 C19 1 0.163005 -0.066919 -0.029465 11.00000 0.04446 0.02604 = 0.02759 -0.00691 0.00352 -0.00520 AFIX 137 H19A 2 0.153795 -0.133237 0.008350 11.00000 -1.50000 H19B 2 0.190865 -0.106143 -0.068804 11.00000 -1.50000 H19C 2 0.118906 -0.035231 -0.049674 11.00000 -1.50000 AFIX 0 C20 1 0.293363 -0.000182 0.049925 11.00000 0.02807 0.04042 = 0.04208 -0.00283 0.00069 0.01012 AFIX 137 H20A 2 0.317800 0.065168 0.079878 11.00000 -1.50000 H20B 2 0.323340 -0.028066 0.009334 11.00000 -1.50000 H20C 2 0.281599 -0.076559 0.080312 11.00000 -1.50000 AFIX 0 C21 1 0.201735 0.614864 0.134704 11.00000 0.02196 0.02690 = 0.03029 0.00639 0.00381 0.00335 AFIX 3 H21 2 0.182015 0.705704 0.137924 11.00000 -1.20000 AFIX 0 C22 1 0.237551 0.583790 0.207084 11.00000 0.01995 0.02302 = 0.02897 -0.01035 -0.00010 -0.00546 AFIX 43 H22 2 0.220996 0.630242 0.248814 11.00000 -1.20000 AFIX 0 C23 1 0.290821 0.496943 0.219530 11.00000 0.01479 0.03274 = 0.02833 -0.00504 -0.00185 -0.00961 AFIX 43 H23 2 0.309884 0.500371 0.267588 11.00000 -1.20000 AFIX 0 C24 1 0.322224 0.402569 0.172312 11.00000 0.01749 0.01968 = 0.03442 0.00386 -0.00104 0.00049 AFIX 43 H24 2 0.352026 0.339432 0.194361 11.00000 -1.20000 AFIX 0 C25 1 0.312793 0.394455 0.094258 11.00000 0.01819 0.02172 = 0.02816 0.00040 0.01166 -0.00127 AFIX 43 H25 2 0.334210 0.321287 0.071012 11.00000 -1.20000 AFIX 0 C26 1 0.277611 0.476676 0.049318 11.00000 0.03232 0.02355 = 0.02424 -0.00166 0.00908 -0.00526 AFIX 23 H26A 2 0.235230 0.428814 0.034045 11.00000 -1.20000 H26B 2 0.306460 0.486659 0.004685 11.00000 -1.20000 AFIX 0 C27 1 0.254876 0.610635 0.069845 11.00000 0.02897 0.02374 = 0.03341 0.00129 0.00294 -0.00152 AFIX 23 H27A 2 0.233541 0.652934 0.026398 11.00000 -1.20000 H27B 2 0.296239 0.662974 0.083587 11.00000 -1.20000 AFIX 0 C28 1 0.112531 0.527424 0.049000 11.00000 0.02896 0.02985 = 0.01553 0.00176 0.00109 0.00129 AFIX 137 H28A 2 0.103018 0.619537 0.036689 11.00000 -1.50000 H28B 2 0.069053 0.477329 0.048218 11.00000 -1.50000 H28C 2 0.144880 0.490315 0.013002 11.00000 -1.50000 AFIX 0 C29 1 0.214092 0.019929 0.239532 11.00000 0.03083 0.01960 = 0.02649 0.00628 -0.00151 0.00047 AFIX 23 H29A 2 0.223990 -0.019258 0.190895 11.00000 -1.20000 H29B 2 0.163573 0.013634 0.248981 11.00000 -1.20000 AFIX 0 C30 1 0.254033 -0.050742 0.298403 11.00000 0.02313 0.02778 = 0.04097 0.01445 -0.00056 -0.00219 AFIX 23 H30A 2 0.296291 -0.092726 0.278174 11.00000 -1.20000 H30B 2 0.225067 -0.118680 0.322464 11.00000 -1.20000 AFIX 0 C31 1 0.272563 0.059154 0.351740 11.00000 0.02436 0.04499 = 0.02665 0.01262 -0.00517 0.00026 AFIX 23 H31A 2 0.233503 0.078537 0.385379 11.00000 -1.20000 H31B 2 0.314214 0.036532 0.380991 11.00000 -1.20000 AFIX 0 C32 1 0.286602 0.172956 0.301161 11.00000 0.02152 0.03092 = 0.02269 -0.00414 -0.00508 0.00431 AFIX 23 H32A 2 0.279478 0.257744 0.326826 11.00000 -1.20000 H32B 2 0.334778 0.169648 0.282278 11.00000 -1.20000 AFIX 0 HKLF 4 REM aa in Pna2(1) REM R1 = 0.0245 for 8002 Fo > 4sig(Fo) and 0.0306 for all 8722 data REM 369 parameters refined using 1 restraints END WGHT 0.0098 6.1561 REM Highest difference peak 1.139, deepest hole -0.886, 1-sigma level 0.113 Q1 1 -0.0741 0.7565 0.2563 11.00000 0.05 1.14 Q2 1 -0.0753 0.7521 0.1671 11.00000 0.05 0.98 Q3 1 0.2539 0.3271 0.1649 11.00000 0.05 0.89 Q4 1 -0.0763 0.3332 0.2560 11.00000 0.05 0.88 Q5 1 0.3327 0.5512 0.1199 11.00000 0.05 0.80 ; _shelx_res_checksum 61397 _shelx_hkl_file ; 0 -3 0 -0.26 0.26 0 4 0 3.13 0.67 0 -4 0 3.16 0.45 0 -4 0 4.71 0.83 0 5 0 4.16 0.85 0 -5 0 3.94 0.94 0 6 0 230.82 5.87 0 6 0 234.37 5.94 0 -6 0 220.56 5.98 0 -6 0 228.43 5.29 0 7 0 -0.80 0.83 0 -7 0 0.32 1.09 0 7 0 2.11 0.93 0 -7 0 0.97 0.61 0 8 0 219.31 6.23 0 -8 0 229.39 5.36 0 -8 0 228.16 6.55 0 -9 0 -2.60 0.76 0 -9 0 -0.89 1.50 0 9 0 0.09 1.19 0 -10 0 80.53 4.13 0 10 0 77.88 3.56 0 -10 0 80.79 2.42 0 11 0 4.36 1.55 0 -11 0 -0.39 2.05 0 -12 0 -0.80 2.38 0 -3 1 152.44 3.45 0 -3 -1 150.37 3.45 0 -4 -1 0.77 0.63 0 -4 -1 0.87 0.39 0 -4 1 0.04 0.60 0 4 1 0.85 0.51 0 4 -1 0.71 0.51 0 -4 1 1.55 0.38 0 -5 -1 763.86 16.48 0 -5 1 750.68 15.99 0 -5 -1 748.88 16.01 0 5 1 747.49 16.59 0 5 -1 762.12 16.54 0 -5 1 725.09 16.50 0 -6 -1 1.04 0.93 0 -6 1 -0.08 0.52 0 6 -1 -0.23 0.76 0 6 -1 0.09 0.72 0 6 1 0.48 0.81 0 -6 1 -0.78 0.87 0 6 1 0.69 0.79 0 -6 -1 0.71 0.57 0 7 1 19.36 1.74 0 -7 1 21.48 1.93 0 7 1 18.77 1.72 0 -7 -1 19.19 1.80 0 7 -1 20.39 1.74 0 7 -1 17.18 1.54 0 -7 1 19.46 1.16 0 -7 -1 21.69 1.19 0 -8 1 1.79 1.37 0 8 1 1.17 1.07 0 8 -1 0.86 1.06 0 -8 1 -1.25 0.64 0 -8 -1 -0.13 0.72 0 -8 -1 2.47 1.36 0 -9 -1 54.30 3.31 0 9 -1 52.27 2.79 0 -9 1 54.17 3.42 0 -9 1 53.37 1.91 0 -9 -1 52.46 1.99 0 9 1 52.76 2.86 0 -10 1 3.94 1.94 0 10 1 5.69 1.58 0 -10 -1 3.97 1.90 0 -10 -1 0.69 0.89 0 10 -1 4.94 1.49 0 -11 -1 77.72 4.31 0 11 -1 79.80 3.70 0 -11 1 80.04 4.45 0 11 1 78.78 3.73 0 -12 -1 -0.12 2.23 0 12 -1 1.91 1.62 0 -13 -1 94.16 5.19 0 -3 2 0.18 0.27 0 -3 -2 0.80 0.32 0 4 2 28.14 1.55 0 -4 -2 28.52 1.08 0 4 2 29.66 1.51 0 4 -2 31.79 1.37 0 -4 2 27.62 1.05 0 -4 2 27.81 1.56 0 -4 -2 25.52 1.50 0 -5 -2 4.28 0.87 0 5 -2 2.69 0.72 0 5 2 4.09 0.82 0 -5 2 2.88 0.53 0 -5 2 2.46 0.83 0 6 2 232.88 5.93 0 -6 -2 221.70 5.95 0 -6 2 223.86 6.16 0 -6 2 229.67 5.27 0 -6 -2 225.62 5.31 0 6 -2 227.98 5.86 0 6 2 235.19 6.04 0 6 -2 226.79 5.82 0 -7 -2 1.04 1.04 0 7 2 -0.45 0.86 0 -7 -2 -0.75 0.63 0 -7 2 -1.29 1.10 0 7 -2 1.38 0.86 0 7 -2 -0.84 0.80 0 7 2 0.19 0.89 0 -7 2 0.52 0.57 0 -8 2 72.52 3.62 0 -8 -2 79.45 2.41 0 -8 -2 77.84 3.47 0 8 2 75.88 3.18 0 8 -2 73.66 3.04 0 -8 2 75.33 2.31 0 -9 2 1.68 1.67 0 9 -2 -0.28 1.11 0 9 2 0.37 1.22 0 -9 2 0.13 0.72 0 -9 -2 -1.14 0.85 0 -9 -2 1.88 1.59 0 -10 -2 116.24 3.18 0 10 2 109.57 4.31 0 10 -2 110.19 4.21 0 -10 -2 115.12 4.72 0 -10 2 105.98 4.79 0 -11 -2 -0.76 1.95 0 11 -2 2.19 1.46 0 11 2 0.73 1.48 0 -12 -2 21.40 3.03 0 12 -2 21.69 2.46 0 -13 -2 4.88 2.72 0 -3 -3 300.87 6.62 0 -3 3 302.47 6.60 0 4 -3 0.42 0.51 0 -4 3 0.72 0.69 0 -4 3 0.48 0.39 0 -4 -3 0.61 0.42 0 4 3 0.73 0.65 0 -5 3 665.52 15.10 0 -5 -3 683.03 14.51 0 5 3 675.98 15.01 0 5 -3 672.48 14.94 0 -5 -3 684.60 14.84 0 5 3 687.76 15.16 0 5 3 648.80 15.06 0 -5 3 678.32 14.46 0 6 3 0.06 0.73 0 -6 3 1.14 0.53 0 6 3 -1.04 0.73 0 -6 -3 -0.56 0.60 0 6 -3 0.17 0.75 0 -6 -3 -1.40 0.85 0 -6 3 0.11 1.01 0 6 -3 0.87 0.73 0 7 3 59.33 2.63 0 -7 -3 56.73 2.77 0 7 -3 59.96 2.52 0 -7 3 60.03 1.88 0 -7 3 53.80 2.86 0 7 3 56.77 2.64 0 -7 -3 61.71 2.01 0 -8 -3 1.48 0.81 0 -8 3 -0.08 1.40 0 -8 -3 -1.01 1.19 0 8 -3 -0.36 1.01 0 8 3 -1.04 1.03 0 -8 3 -0.02 0.65 0 -9 -3 73.83 3.65 0 9 3 72.34 3.33 0 9 -3 67.55 3.12 0 -9 3 73.16 2.23 0 -9 -3 70.57 2.41 0 10 3 3.76 1.49 0 10 -3 4.32 1.43 0 -10 -3 2.29 1.91 0 -10 -3 1.05 0.98 0 -11 -3 21.13 2.73 0 11 3 16.88 2.19 0 11 -3 17.90 2.14 0 -12 -3 -0.27 2.18 0 12 -3 0.30 1.60 0 -2 -4 389.44 8.43 0 -2 4 389.92 8.44 0 3 -4 0.61 0.44 0 -3 4 1.12 0.38 0 -3 -4 0.63 0.42 0 4 4 83.83 2.83 0 4 -4 87.72 2.61 0 -4 4 89.19 2.31 0 4 4 87.88 2.72 0 -4 -4 89.72 2.36 0 5 4 1.46 0.76 0 5 4 1.73 0.92 0 -5 -4 2.31 0.60 0 -5 4 1.66 0.49 0 5 -4 1.43 0.69 0 -6 -4 132.24 3.42 0 6 4 128.50 4.12 0 6 4 129.78 4.10 0 6 -4 132.22 3.84 0 -6 -4 133.48 4.03 0 6 -4 130.26 3.87 0 6 4 133.65 3.99 0 -6 4 137.23 3.34 0 -7 4 0.82 0.58 0 -7 -4 0.15 0.70 0 -7 -4 0.19 1.04 0 7 4 0.62 0.87 0 7 4 0.20 0.93 0 7 -4 0.90 0.86 0 8 -4 115.34 3.97 0 -8 4 118.93 3.13 0 8 4 116.59 4.15 0 -8 -4 117.31 4.21 0 -8 -4 122.41 3.32 0 8 4 121.09 4.07 0 9 4 -0.83 1.26 0 -9 -4 -0.28 1.54 0 -9 -4 -1.10 0.90 0 -9 4 -0.32 0.66 0 9 -4 0.69 1.22 0 10 4 97.38 4.04 0 -10 -4 96.25 2.93 0 -10 -4 94.46 4.25 0 10 -4 90.00 3.81 0 11 -4 -0.20 1.38 0 -11 -4 0.38 1.97 0 -12 -4 19.43 2.89 0 12 -4 19.86 2.39 0 -1 5 193.43 4.47 0 -2 5 0.53 0.35 0 -2 -5 0.16 0.36 0 -3 5 90.84 2.35 0 3 -5 87.98 2.53 0 3 5 88.78 2.68 0 -3 -5 91.25 2.38 0 -4 5 1.22 0.45 0 4 -5 0.86 0.55 0 -4 -5 0.22 0.50 0 4 5 0.92 0.74 0 4 5 1.13 0.65 0 5 5 291.77 7.24 0 -5 -5 296.89 6.75 0 5 5 292.64 7.37 0 5 -5 296.48 7.12 0 -5 5 300.11 6.68 0 6 5 0.54 1.01 0 -6 5 0.98 0.54 0 -6 -5 0.24 0.65 0 6 5 1.11 0.94 0 6 -5 1.26 0.79 0 6 5 -0.25 0.81 0 6 -5 0.72 0.77 0 -6 -5 0.43 0.90 0 -7 -5 151.66 3.96 0 7 5 154.40 4.76 0 7 5 161.70 4.72 0 7 -5 148.32 4.48 0 -7 5 155.01 3.80 0 -7 -5 141.50 4.51 0 8 5 1.52 1.12 0 -8 5 0.63 0.67 0 -8 -5 0.08 1.22 0 8 -5 0.51 1.05 0 -8 -5 1.80 0.89 0 8 5 1.50 1.09 0 9 -5 65.66 3.08 0 -9 -5 63.04 3.43 0 -9 5 72.65 2.10 0 -9 -5 67.36 2.47 0 9 5 65.52 3.28 0 -10 -5 1.28 1.04 0 -10 -5 1.75 1.73 0 10 -5 1.74 1.39 0 10 5 2.37 1.52 0 11 -5 36.59 2.78 0 -11 -5 28.88 3.00 0 12 -5 1.53 1.69 0 0 6 561.91 12.22 0 1 6 0.69 0.46 0 -1 6 0.71 0.41 0 -2 6 584.58 12.60 0 -2 -6 587.20 12.57 0 2 6 576.58 12.84 0 3 -6 0.30 0.47 0 -3 -6 1.03 0.49 0 3 6 0.94 0.64 0 -3 6 0.68 0.44 0 -4 -6 152.00 3.69 0 4 6 149.92 4.11 0 4 6 142.37 4.15 0 -4 6 145.87 3.61 0 4 -6 142.79 3.92 0 5 -6 0.20 0.65 0 -5 6 -0.03 0.48 0 5 6 0.65 0.87 0 -5 -6 0.03 0.60 0 5 6 0.21 0.74 0 5 -6 0.30 0.61 0 6 -6 83.39 2.90 0 -6 -6 79.31 2.48 0 6 6 82.14 3.10 0 6 -6 82.54 2.90 0 -6 6 82.53 2.37 0 6 6 84.34 3.30 0 7 6 0.94 1.27 0 -7 -6 1.31 0.83 0 -7 -6 1.09 1.04 0 7 6 0.82 1.08 0 7 -6 0.21 0.89 0 -7 6 2.20 0.66 0 7 6 -0.34 1.00 0 -8 6 100.98 2.79 0 8 -6 97.79 3.65 0 8 6 103.37 3.80 0 8 6 99.52 3.90 0 -8 -6 95.51 3.79 0 -8 -6 105.78 3.11 0 -9 -6 0.24 1.59 0 9 6 2.02 1.40 0 9 -6 -0.64 1.15 0 -9 -6 0.12 0.98 0 10 6 41.81 2.91 0 -10 -6 39.76 1.99 0 -10 -6 41.16 3.19 0 10 -6 33.70 2.60 0 11 -6 1.26 1.51 0 12 -6 80.18 4.03 0 0 7 0.70 0.46 0 0 -7 0.02 0.45 0 -1 7 243.78 5.78 0 1 7 254.32 5.93 0 2 -7 2.32 0.61 0 -2 -7 1.47 0.54 0 2 7 0.85 0.62 0 -2 7 2.52 0.51 0 -3 -7 125.82 3.21 0 3 -7 122.34 3.39 0 -3 7 126.82 3.20 0 3 7 132.32 3.62 0 3 7 115.76 3.62 0 4 7 1.17 0.87 0 -4 7 0.05 0.46 0 4 -7 1.03 0.59 0 4 7 0.61 0.77 0 4 -7 0.62 0.64 0 -4 -7 0.73 0.59 0 -5 -7 135.07 3.53 0 -5 7 131.99 3.39 0 5 7 132.15 4.06 0 5 7 127.41 4.09 0 5 -7 133.92 3.86 0 5 -7 134.28 3.78 0 6 -7 1.70 0.85 0 6 7 0.40 1.06 0 -6 -7 1.44 0.80 0 6 -7 1.82 0.86 0 6 7 0.05 0.88 0 -6 7 1.50 0.63 0 7 7 264.28 6.92 0 7 7 233.57 6.88 0 -7 -7 260.96 6.17 0 -7 -7 244.74 6.60 0 7 7 255.03 7.06 0 -7 7 266.15 5.94 0 7 -7 245.88 6.66 0 8 7 2.82 1.40 0 -8 -7 3.23 1.04 0 8 -7 1.59 1.17 0 -8 7 2.61 0.73 0 8 7 1.88 1.30 0 -8 -7 2.94 1.46 0 -9 -7 25.66 2.41 0 9 7 23.29 2.32 0 -9 -7 22.86 1.76 0 9 -7 24.25 2.23 0 -10 -7 0.04 1.10 0 -10 -7 0.24 1.67 0 10 -7 0.85 1.38 0 -11 -7 24.37 1.77 0 11 -7 23.06 2.42 0 0 8 229.25 5.49 0 0 -8 226.47 5.37 0 1 -8 0.25 0.52 0 1 -8 0.49 0.59 0 1 8 -0.23 0.51 0 -1 8 0.66 0.51 0 -2 8 375.84 8.38 0 -2 -8 372.61 8.34 0 2 -8 366.52 8.41 0 2 8 370.86 8.65 0 2 -8 371.59 8.56 0 3 8 0.44 0.82 0 3 -8 0.82 0.65 0 3 8 0.27 0.65 0 -3 -8 1.98 0.64 0 -3 8 1.85 0.55 0 3 -8 0.98 0.63 0 4 8 112.72 3.53 0 -4 8 111.58 2.99 0 -4 -8 109.02 3.06 0 4 -8 104.72 3.16 0 4 8 109.01 3.67 0 4 -8 113.17 3.34 0 5 -8 1.60 0.81 0 5 8 0.98 0.93 0 -5 -8 0.24 0.73 0 -5 8 0.32 0.59 0 5 8 1.20 0.89 0 5 -8 0.02 0.72 0 6 8 167.14 4.91 0 -6 8 157.26 4.02 0 6 8 164.88 5.08 0 -6 -8 162.64 4.23 0 6 -8 152.31 4.61 0 7 8 2.90 1.43 0 7 -8 1.58 1.03 0 7 8 0.70 1.18 0 -7 8 0.70 0.69 0 -7 -8 1.97 1.00 0 -8 -8 29.65 1.81 0 8 8 28.29 2.54 0 8 -8 25.24 2.16 0 -8 8 27.90 1.47 0 -8 -8 23.99 2.13 0 8 8 22.14 2.16 0 8 8 30.56 2.37 0 -9 -8 -0.65 1.47 0 -9 -8 -1.92 1.01 0 9 -8 -0.15 1.22 0 -10 -8 22.63 1.84 0 10 -8 24.09 2.31 0 -11 -8 1.52 1.18 0 11 -8 2.05 1.61 0 0 -9 -0.45 0.62 0 0 -9 -0.21 0.54 0 0 9 -0.83 0.51 0 -1 9 289.15 6.71 0 1 -9 290.21 6.88 0 1 -9 287.28 6.68 0 1 9 275.45 6.81 0 2 -9 1.20 0.59 0 -2 -9 0.04 0.62 0 2 9 -0.26 0.63 0 -2 9 1.06 0.54 0 2 -9 0.54 0.60 0 3 -9 146.00 4.01 0 -3 9 150.36 3.87 0 -3 -9 153.76 3.88 0 3 9 152.19 4.27 0 3 -9 153.32 4.15 0 3 9 140.00 4.36 0 4 9 0.49 0.88 0 4 -9 -0.44 0.71 0 4 9 -0.24 0.79 0 -4 9 0.47 0.60 0 4 -9 0.63 0.78 0 -4 -9 -0.77 0.66 0 -5 -9 82.29 2.66 0 5 -9 81.35 2.95 0 5 9 85.33 3.21 0 5 9 84.07 3.39 0 5 -9 83.82 2.92 0 -5 9 84.44 2.52 0 -6 -9 3.17 0.93 0 -6 9 2.40 0.72 0 6 9 3.34 1.28 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1.66 1.06 0 -7 11 345.19 7.75 0 7 -11 334.49 8.70 0 7 11 331.01 8.90 0 -7 -11 338.94 8.14 0 8 -11 0.15 1.25 0 8 11 -1.32 1.39 0 -8 -11 1.68 1.20 0 9 11 31.76 2.67 0 9 -11 33.05 2.63 0 -9 -11 29.31 2.05 0 -10 -11 -0.57 1.34 0 10 -11 0.67 1.53 0 -11 -11 12.96 1.64 0 0 -12 7.27 1.17 0 0 12 6.23 1.01 0 0 -12 6.21 0.99 0 1 -12 1.07 0.84 0 1 -12 0.87 0.85 0 -1 -12 1.07 0.95 0 -1 12 0.40 0.72 0 1 12 1.56 0.84 0 -2 -12 386.74 9.25 0 2 12 376.99 9.22 0 2 -12 391.55 9.31 0 -2 12 386.65 8.95 0 -2 -12 391.79 8.96 0 2 -12 374.15 9.05 0 3 -12 1.71 0.96 0 3 12 2.67 1.01 0 -3 -12 2.07 0.94 0 -3 12 2.54 0.79 0 3 -12 2.69 0.99 0 4 -12 215.78 5.80 0 -4 12 222.41 5.48 0 -4 -12 229.31 5.67 0 4 12 211.68 6.04 0 4 -12 215.85 5.94 0 -5 -12 -1.47 0.99 0 5 -12 0.22 0.98 0 5 12 -0.33 1.05 0 -5 12 -1.00 0.72 0 -6 -12 69.16 2.72 0 6 12 66.18 3.27 0 -6 12 72.26 2.41 0 6 -12 70.74 3.09 0 -7 -12 1.66 1.16 0 7 -12 1.27 1.27 0 7 12 0.28 1.29 0 -7 12 0.75 0.81 0 8 -12 4.75 1.52 0 -8 -12 5.64 1.43 0 8 12 3.70 1.58 0 -9 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42.22 2.13 -2 -6 -7 39.55 2.23 2 6 -7 42.91 2.20 -2 6 7 44.13 2.31 -2 6 7 44.28 2.49 -2 -6 -7 43.68 1.95 2 -6 -7 42.81 1.66 2 6 7 41.90 2.47 -2 6 -7 39.80 1.99 2 6 7 41.66 2.60 -2 -6 7 38.32 1.77 2 6 7 35.81 2.17 -2 -7 -7 105.93 3.63 2 7 -7 106.08 3.69 -2 7 7 101.35 3.86 2 7 -7 101.82 3.66 -2 -7 -7 103.64 3.22 -2 -7 7 106.66 3.09 -2 7 -7 102.71 3.46 2 7 7 96.60 3.68 2 7 7 94.31 3.73 2 -7 -7 105.28 2.88 -2 -8 -7 31.87 1.98 -2 8 7 31.22 2.63 2 8 -7 31.15 2.36 -2 8 7 31.90 2.48 2 8 -7 27.98 2.22 -2 8 -7 24.68 2.04 -2 -8 7 28.74 1.76 2 -8 -7 31.77 2.73 2 -8 -7 29.53 1.55 2 8 7 25.28 2.25 -2 9 7 40.12 2.77 2 9 -7 37.86 2.51 -2 -9 -7 41.63 2.15 -2 -9 7 41.16 2.02 2 -9 -7 41.14 1.70 -2 9 -7 39.66 2.59 2 9 7 43.23 2.87 2 -9 -7 39.73 3.00 -2 -10 -7 18.39 1.74 -2 10 7 19.75 2.27 -2 10 -7 21.18 2.16 2 -10 -7 24.23 2.68 -2 -10 7 19.44 1.67 2 10 7 20.08 2.27 -2 11 7 35.40 2.92 -2 -11 -7 33.37 2.27 2 11 7 36.25 3.10 2 -11 -7 38.92 3.33 -2 11 -7 36.74 2.81 -2 -12 -7 46.35 2.58 -2 12 -7 50.34 3.34 -2 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65.79 2.26 -2 5 -8 66.75 2.45 2 6 -8 77.91 3.04 -2 6 8 81.21 3.19 2 6 -8 79.45 2.96 -2 6 8 82.54 3.33 -2 -6 -8 80.50 2.74 -2 6 -8 77.67 2.85 2 6 8 76.41 3.19 -2 -6 8 80.52 2.59 2 6 8 77.64 3.37 2 -6 -8 84.88 2.50 2 6 8 74.10 3.21 -2 7 8 137.34 4.71 -2 -7 -8 138.01 3.98 2 7 -8 129.71 4.28 2 7 -8 137.72 4.46 2 -7 -8 135.42 3.63 2 7 8 146.21 4.65 -2 7 -8 136.02 4.22 -2 -7 8 136.99 3.79 -2 -8 -8 96.40 3.17 2 8 -8 92.16 3.67 -2 8 8 100.33 4.05 -2 8 -8 85.15 3.42 -2 -8 8 95.61 2.99 2 -8 -8 91.26 2.79 2 8 8 87.05 3.70 2 9 -8 8.57 1.63 -2 9 8 8.16 1.97 -2 -9 -8 9.01 1.39 -2 9 8 6.92 1.79 2 -9 -8 8.54 1.96 -2 -9 8 6.88 1.13 2 -9 -8 7.32 1.03 2 9 8 8.74 1.71 -2 9 -8 9.12 1.64 -2 10 8 40.03 3.03 -2 -10 -8 34.76 2.22 -2 -10 8 34.63 1.87 2 10 8 36.97 2.99 -2 10 -8 32.57 2.57 2 -10 -8 33.03 2.99 -2 -11 -8 5.39 1.54 2 11 8 7.82 2.01 -2 11 -8 4.36 1.77 2 -11 -8 7.04 2.34 -2 -12 -8 8.48 1.64 -2 12 -8 13.26 2.27 2 12 8 11.70 2.37 -2 0 -9 0.96 0.58 -2 0 9 0.07 0.56 -2 0 -9 1.43 0.68 2 0 9 1.55 0.57 -2 1 9 36.51 1.85 -2 -1 -9 38.47 1.78 2 -1 9 37.73 1.52 -2 1 9 39.65 1.72 2 1 -9 38.77 1.64 -2 -1 9 41.06 1.70 2 -1 -9 39.86 1.60 -2 1 -9 39.68 1.77 2 1 9 35.95 1.69 -2 -2 -9 170.60 4.31 2 -2 9 173.08 4.19 2 2 -9 168.71 4.57 -2 2 9 171.93 4.83 -2 -2 -9 175.96 4.56 2 2 -9 177.40 4.48 -2 2 9 171.04 4.55 2 -2 -9 174.57 4.28 2 2 9 173.22 4.59 -2 -2 9 167.39 4.36 -2 2 -9 172.26 4.49 2 3 -9 81.28 2.63 -2 -3 -9 82.12 2.54 2 3 -9 82.94 2.77 -2 3 9 77.96 3.00 -2 3 9 77.17 2.72 2 -3 9 79.05 2.23 -2 -3 -9 83.34 2.78 2 -3 -9 79.80 2.41 -2 -3 9 78.97 2.51 2 3 9 76.22 2.79 -2 3 -9 79.37 2.62 -2 -4 -9 41.69 2.00 2 -4 9 42.67 1.44 -2 4 9 42.81 2.41 2 4 -9 42.73 2.02 -2 4 9 43.31 2.19 -2 -4 -9 46.57 1.94 2 4 -9 41.83 1.99 2 4 9 47.82 2.51 2 4 9 41.43 2.19 2 -4 -9 42.91 1.76 -2 4 -9 43.68 1.96 -2 -4 9 43.75 1.83 -2 -5 -9 228.79 5.65 -2 5 9 221.37 6.05 2 5 -9 219.65 5.86 2 5 -9 227.82 6.04 -2 5 9 230.12 6.34 2 5 9 234.31 6.44 2 -5 -9 226.07 5.46 -2 -5 9 224.44 5.58 2 5 9 233.53 6.18 -2 5 -9 222.74 5.84 2 6 -9 58.09 2.64 -2 6 9 56.29 2.95 -2 -6 -9 59.87 2.36 -2 6 9 53.85 2.64 2 6 -9 50.05 2.49 2 6 9 54.54 2.75 2 -6 -9 59.40 2.11 -2 -6 9 52.21 2.09 -2 6 -9 54.50 2.53 -2 7 9 13.22 1.77 2 7 -9 12.94 1.66 -2 -7 -9 10.47 1.37 2 7 -9 10.89 1.52 -2 7 -9 13.55 1.56 2 -7 -9 9.28 1.11 2 7 9 9.72 1.57 -2 -7 9 10.37 1.15 -2 -8 -9 11.66 1.44 2 8 -9 12.42 1.78 2 8 9 11.89 1.79 -2 -8 9 9.41 1.18 2 -8 -9 12.12 1.23 -2 8 -9 12.30 1.61 -2 -9 -9 29.73 2.05 -2 9 9 37.29 3.09 -2 9 9 32.05 2.74 2 9 -9 27.48 2.54 2 -9 -9 29.97 1.71 2 9 9 31.28 2.75 -2 -9 9 30.64 1.84 -2 9 -9 32.05 2.49 2 -9 -9 33.31 2.73 -2 -10 -9 12.83 1.77 -2 10 9 12.86 2.16 -2 -10 9 12.25 1.29 2 -10 -9 13.80 2.33 2 10 9 16.71 2.29 -2 10 -9 17.37 2.09 -2 -11 -9 19.27 1.97 2 11 9 21.24 2.57 -2 11 -9 20.52 2.35 -2 -12 -9 42.59 2.55 -2 12 -9 38.11 3.23 2 12 9 48.85 3.57 -2 0 -10 331.28 7.76 -2 0 10 323.95 7.67 -2 0 10 319.34 7.94 2 0 10 318.90 7.56 -2 0 -10 329.04 7.56 -2 -1 -10 100.32 3.10 -2 1 10 100.47 3.34 -2 1 10 101.03 3.09 2 1 -10 101.58 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2.30 -2 1 11 51.57 2.52 -2 1 11 50.36 2.15 -2 -1 11 49.84 2.10 2 1 11 48.67 2.14 -2 1 -11 52.14 2.24 2 -1 -11 53.99 1.99 -2 1 -11 50.13 2.11 -2 -2 -11 180.49 4.97 2 2 -11 185.82 5.09 -2 -2 -11 187.38 4.77 2 -2 11 188.90 4.62 -2 2 11 194.25 5.40 -2 2 11 183.33 5.01 2 2 -11 186.22 4.87 2 -2 -11 186.71 4.74 2 2 11 181.17 4.99 -2 2 -11 183.46 4.81 -2 2 -11 181.16 4.97 -2 -2 11 180.55 4.83 2 -3 11 55.77 1.85 -2 -3 -11 53.61 2.41 -2 3 11 46.92 2.27 -2 -3 -11 53.23 2.19 2 3 -11 50.82 2.39 -2 3 11 58.30 2.75 2 3 -11 47.80 2.21 -2 -3 11 50.94 2.09 2 -3 -11 54.80 2.06 -2 3 -11 53.26 2.28 2 3 11 48.06 2.34 2 4 -11 41.36 2.28 2 -4 11 46.39 1.62 -2 4 11 43.67 2.36 2 4 -11 41.79 2.27 -2 -4 -11 43.97 2.10 -2 4 11 47.22 2.71 -2 4 -11 45.84 2.18 2 -4 -11 44.02 1.99 2 4 11 43.06 2.24 -2 -4 11 47.89 2.05 2 5 -11 178.69 5.18 -2 5 11 189.85 5.73 -2 -5 -11 195.86 5.01 2 5 -11 182.94 5.31 -2 5 11 184.98 5.42 -2 5 -11 182.61 5.14 -2 -5 11 178.76 4.81 2 5 11 172.19 5.27 2 -5 -11 186.01 4.79 2 6 -11 65.02 3.00 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26.88 1.67 -8 -5 -4 24.06 1.82 -8 -5 4 29.96 1.86 -8 5 -4 26.51 1.33 -8 -5 4 30.46 1.70 8 5 4 27.20 1.66 -8 -6 -4 89.82 2.95 -8 6 4 90.08 3.04 -8 -6 -4 91.18 3.28 8 6 -4 87.84 3.19 8 -6 4 88.99 3.73 8 6 4 87.88 3.11 -8 6 -4 86.95 2.68 -8 -6 4 90.39 3.22 -8 -6 4 90.52 2.95 -8 7 4 45.17 2.39 8 7 -4 51.24 2.54 -8 -7 -4 45.70 2.23 8 -7 4 42.52 3.08 -8 7 -4 45.08 1.98 8 7 4 45.99 2.49 -8 -7 4 48.71 2.22 8 8 -4 63.97 3.19 -8 -8 -4 62.09 2.73 8 -8 4 61.70 3.44 -8 8 4 68.53 3.03 -8 -8 4 66.29 2.79 -8 8 -4 66.00 2.60 8 8 4 62.34 3.04 8 -8 -4 68.26 3.28 -8 9 4 4.53 1.59 -8 -9 -4 3.12 1.40 8 -9 4 2.70 1.92 -8 9 4 2.51 1.42 8 9 -4 2.24 1.46 8 -9 -4 4.17 1.92 -8 9 -4 0.96 1.07 8 9 4 0.60 1.44 -8 -9 4 2.66 1.35 8 -10 4 86.54 4.47 8 10 -4 80.53 3.89 -8 -10 -4 75.87 3.36 -8 10 4 71.87 3.50 8 -10 -4 85.76 4.32 -8 -10 4 75.69 3.23 -8 10 -4 74.39 3.26 8 10 4 81.91 3.81 8 11 -4 8.49 2.11 8 -11 4 4.20 2.56 -8 -11 -4 3.10 1.73 -8 11 4 6.96 1.84 -8 -11 4 3.87 1.58 8 -11 -4 5.15 2.50 -8 11 -4 5.25 1.59 8 11 4 4.47 1.94 -8 12 4 32.88 3.00 8 -12 4 36.82 3.81 8 12 -4 33.93 3.19 -8 -12 -4 28.00 2.59 8 -12 -4 35.06 3.67 -8 -12 4 30.37 2.61 8 12 4 31.47 2.99 -8 12 -4 29.90 2.74 -8 0 -5 5.44 0.61 -8 0 5 6.80 0.77 -8 1 5 105.47 2.92 -8 -1 -5 105.14 2.87 -8 1 -5 110.19 2.65 -8 -1 5 105.60 3.04 -8 2 5 5.24 0.72 8 -2 5 6.93 0.92 -8 -2 -5 3.69 0.78 8 2 -5 5.94 0.60 -8 -2 5 5.99 0.84 -8 2 -5 5.91 0.49 -8 3 5 112.14 3.22 -8 -3 -5 107.44 3.26 8 -3 5 109.23 3.44 8 3 -5 115.40 3.08 8 3 5 116.43 2.80 -8 -3 5 110.82 3.11 -8 -3 5 114.18 3.33 -8 3 -5 113.35 2.72 -8 -4 -5 20.56 1.62 -8 -4 -5 19.68 1.39 8 4 -5 23.32 1.48 8 -4 5 21.97 1.98 -8 4 5 21.55 1.53 -8 4 -5 21.50 1.06 -8 -4 5 22.30 1.38 8 4 5 20.19 1.34 -8 -4 5 25.01 1.65 8 -5 5 283.41 7.43 -8 -5 -5 284.54 6.87 8 5 -5 285.63 7.03 -8 5 5 291.24 7.01 -8 -5 -5 286.84 7.19 -8 -5 5 267.97 7.08 8 5 5 292.83 6.98 -8 5 -5 290.02 6.58 -8 -5 5 287.38 6.92 -8 -6 -5 17.62 1.56 8 6 -5 16.26 1.53 -8 6 5 16.83 1.49 -8 -6 -5 18.02 1.70 8 -6 5 18.62 1.96 -8 6 -5 17.46 1.30 -8 -6 5 17.46 1.60 8 6 5 17.19 1.54 -8 -6 5 15.56 1.35 8 -7 5 160.40 5.43 -8 7 5 155.88 4.74 -8 -7 -5 156.16 4.53 8 7 -5 166.62 4.95 8 7 5 164.22 4.86 -8 7 -5 154.91 4.30 -8 -7 5 157.55 4.52 -8 -8 -5 -0.29 1.26 -8 8 5 5.33 1.49 8 8 -5 4.30 1.49 8 -8 5 3.28 1.80 -8 8 -5 1.46 0.96 8 8 5 3.19 1.40 -8 -8 5 2.53 1.20 -8 9 5 44.88 2.89 8 -9 5 42.82 3.22 -8 9 5 43.25 2.64 8 9 -5 38.39 2.74 -8 -9 -5 42.43 2.45 -8 9 -5 44.64 2.37 8 9 5 43.59 2.85 -8 -9 5 42.48 2.45 8 -9 -5 48.09 3.35 8 10 -5 3.67 1.79 -8 10 5 2.84 1.61 -8 -10 -5 3.94 1.63 8 -10 5 5.27 2.06 -8 -10 5 2.11 1.51 -8 10 -5 3.38 1.37 8 -10 -5 5.11 2.29 8 10 5 3.95 1.72 -8 -11 -5 25.15 2.38 8 11 -5 30.79 2.84 8 -11 5 31.22 3.45 -8 11 5 25.09 2.49 8 -11 -5 29.81 3.28 -8 11 -5 26.53 2.46 -8 -11 5 30.28 2.48 8 11 5 28.72 2.72 8 -12 5 15.75 3.28 8 12 -5 16.68 2.67 -8 12 5 13.85 2.30 -8 -12 -5 15.96 2.22 8 12 5 20.31 2.64 -8 12 -5 16.55 2.23 -8 -12 5 15.73 2.04 8 -12 -5 19.41 3.30 -8 0 6 349.55 8.07 -8 0 -6 348.85 7.81 8 1 -6 48.22 1.35 -8 -1 -6 45.83 1.72 -8 1 6 45.68 1.83 -8 -1 6 43.27 1.84 -8 1 -6 45.37 1.56 8 -2 6 179.01 4.63 -8 -2 -6 174.54 4.53 -8 2 6 177.03 4.58 8 2 -6 186.78 4.29 -8 -2 6 179.39 4.70 -8 2 -6 178.99 4.18 8 3 -6 1.68 0.66 -8 3 6 2.55 0.83 8 -3 6 1.76 0.90 -8 -3 -6 0.34 0.78 -8 3 -6 2.02 0.52 -8 -3 6 1.97 0.81 -8 -3 6 1.16 0.69 8 3 6 2.01 0.52 8 4 -6 146.50 4.05 -8 4 6 150.51 4.19 8 -4 6 141.76 4.43 -8 -4 -6 149.93 4.26 -8 -4 6 150.97 4.05 -8 4 -6 148.97 3.67 8 4 6 155.97 3.94 -8 -4 6 144.24 4.20 8 -5 6 8.06 1.42 -8 5 6 8.42 1.16 -8 -5 -6 8.47 1.25 8 5 -6 7.38 1.15 -8 -5 -6 8.69 1.06 -8 5 -6 8.38 0.86 -8 -5 6 7.23 1.21 -8 -5 6 7.00 1.05 8 5 6 7.58 1.09 -8 6 6 115.20 3.69 8 -6 6 115.10 4.22 -8 -6 -6 106.02 3.65 8 6 -6 107.84 3.70 -8 -6 -6 105.66 3.38 -8 -6 6 110.44 3.44 8 6 6 108.68 3.62 -8 6 -6 109.54 3.18 8 7 -6 9.87 1.57 -8 -7 -6 8.60 1.41 -8 7 6 12.24 1.59 8 -7 6 10.21 1.80 -8 -7 6 7.43 1.31 8 7 6 6.65 1.39 -8 7 -6 10.34 1.15 8 8 -6 62.60 3.22 8 -8 6 57.88 3.74 -8 8 6 64.80 3.18 -8 -8 -6 65.98 2.91 -8 -8 6 64.69 2.82 -8 8 -6 65.46 2.62 8 8 6 66.59 3.10 8 -9 6 6.08 2.00 -8 -9 -6 5.33 1.58 8 9 -6 5.55 1.68 -8 9 6 8.97 1.88 8 9 6 7.39 1.69 8 -9 -6 5.61 2.02 -8 -9 6 6.02 1.46 -8 9 -6 7.64 1.35 -8 10 6 47.18 3.06 8 10 -6 48.14 3.15 -8 -10 -6 48.08 2.81 8 -10 6 45.50 3.85 -8 10 6 47.09 3.02 -8 -10 6 42.33 2.61 8 10 6 51.76 3.25 -8 10 -6 47.54 2.66 8 -10 -6 47.09 3.60 -8 -11 -6 7.42 1.92 8 -11 6 9.88 2.77 -8 11 6 5.86 1.87 8 11 -6 6.83 2.17 8 11 6 6.80 2.03 -8 -11 6 6.59 1.68 -8 11 -6 7.62 1.73 8 -11 -6 5.37 2.52 8 12 -6 73.58 4.26 8 -12 6 75.47 4.94 -8 -12 -6 62.04 3.54 -8 12 6 77.81 3.94 -8 -12 6 68.57 3.37 -8 12 -6 76.25 3.74 8 12 6 71.19 4.02 8 -12 -6 75.85 4.67 -8 0 -7 116.18 3.09 -8 0 7 112.14 3.32 -8 -1 -7 189.99 4.81 -8 1 7 193.10 5.01 8 1 -7 199.96 4.48 -8 1 -7 194.68 4.68 -8 -1 7 194.03 5.04 8 2 -7 11.74 1.05 8 -2 7 10.72 1.10 -8 -2 -7 9.17 1.03 -8 2 7 9.58 1.06 -8 -2 7 10.64 1.13 -8 -2 7 10.84 0.95 -8 2 -7 13.09 0.97 -8 -3 -7 56.13 2.26 -8 3 7 56.22 2.34 8 3 -7 52.18 2.07 8 -3 7 49.23 2.34 -8 3 -7 50.02 1.76 8 3 7 54.81 1.73 -8 -3 7 57.18 2.35 -8 -3 7 54.34 2.04 -8 -4 -7 7.30 0.98 8 -4 7 6.83 1.27 8 4 -7 8.09 1.06 -8 -4 -7 5.89 1.13 -8 -4 7 6.60 1.05 -8 4 -7 8.31 0.82 8 4 7 7.11 0.92 -8 -4 7 7.05 1.01 8 5 -7 139.59 4.08 -8 5 7 128.95 4.08 -8 -5 -7 132.24 4.18 -8 -5 -7 134.59 3.83 8 -5 7 141.64 4.55 -8 -5 7 144.56 4.26 -8 -5 7 134.74 3.93 8 5 7 138.08 3.95 -8 5 -7 133.79 3.63 -8 -6 -7 7.97 1.28 -8 6 7 8.40 1.40 8 6 -7 6.94 1.29 -8 -6 -7 5.79 1.29 8 -6 7 8.23 1.68 -8 6 -7 6.28 0.94 -8 -6 7 10.22 1.25 8 6 7 6.31 1.22 8 -7 7 281.91 7.93 8 7 -7 278.82 7.40 -8 -7 -7 274.52 7.08 -8 7 7 270.44 7.32 -8 -7 7 279.32 7.04 8 7 7 278.06 7.29 -8 7 -7 275.12 6.87 -8 -8 -7 15.42 1.71 -8 8 7 14.65 1.94 8 -8 7 17.53 2.50 8 8 -7 18.82 1.99 8 8 7 16.43 1.89 -8 -8 7 13.74 1.65 -8 8 -7 16.60 1.58 -8 9 7 25.22 2.43 8 -9 7 28.88 3.00 8 9 -7 22.54 2.31 -8 -9 -7 23.57 2.10 8 9 7 25.10 2.28 -8 9 -7 26.34 2.06 8 -10 7 0.94 2.25 -8 10 7 -0.05 1.79 -8 -10 -7 1.93 1.60 -8 10 7 0.83 1.67 8 10 -7 0.56 1.78 8 -10 -7 -0.15 2.10 -8 10 -7 0.17 1.24 8 10 7 1.17 1.61 -8 -10 7 2.06 1.47 -8 11 7 16.55 2.41 8 11 -7 17.83 2.56 8 -11 7 18.43 3.05 -8 -11 -7 13.14 2.14 -8 11 -7 15.01 2.04 8 -11 -7 15.90 2.94 8 11 7 15.04 2.31 -8 -11 7 15.43 2.01 8 12 -7 11.46 2.54 -8 -12 -7 4.53 1.96 -8 12 7 7.76 2.15 8 12 7 7.00 2.24 -8 -12 7 7.37 1.89 -8 12 -7 8.29 1.94 8 -12 -7 11.50 3.02 8 0 -8 96.02 2.38 -8 0 8 96.94 3.09 -8 0 -8 94.45 2.82 -8 1 8 14.25 1.29 -8 -1 -8 13.57 1.16 -8 -1 8 15.03 1.32 -8 -1 8 15.23 1.19 -8 1 -8 13.51 1.16 -8 -2 -8 227.24 5.72 -8 2 8 219.75 5.83 8 2 -8 230.43 5.45 -8 2 -8 221.82 5.42 -8 -2 8 228.73 5.91 -8 -2 8 234.99 5.64 8 3 -8 0.73 0.72 -8 3 8 0.51 0.87 -8 -3 -8 0.44 0.85 -8 -3 8 0.38 0.71 -8 -3 8 0.36 0.87 8 3 8 0.50 0.54 -8 3 -8 -0.10 0.60 8 4 -8 116.53 3.57 -8 4 8 115.20 3.74 8 -4 8 120.35 3.95 -8 -4 -8 111.98 3.37 -8 -4 -8 122.04 3.78 -8 -4 8 118.39 3.50 -8 4 -8 117.09 3.24 8 4 8 124.11 3.39 -8 -4 8 113.57 3.77 -8 5 8 25.90 2.14 -8 -5 -8 27.75 1.71 8 5 -8 25.03 1.80 8 -5 8 26.42 2.41 -8 -5 -8 25.30 2.00 -8 -5 8 24.40 1.77 8 5 8 25.77 1.75 -8 5 -8 26.49 1.55 -8 -5 8 23.01 1.79 -8 -6 -8 110.56 3.56 8 6 -8 111.52 3.85 -8 -6 -8 109.60 3.94 -8 6 8 117.60 4.05 8 -6 8 111.80 4.37 -8 -6 8 114.62 3.65 -8 6 -8 114.96 3.40 8 6 8 108.81 3.68 -8 -7 -8 0.85 1.20 8 -7 8 1.92 1.49 8 7 -8 1.00 1.24 -8 7 8 0.76 1.40 8 7 8 1.68 1.20 -8 -7 8 1.65 1.20 -8 7 -8 2.08 1.02 -8 8 8 21.17 2.24 8 8 -8 21.65 2.14 -8 -8 -8 22.60 1.99 8 -8 8 20.41 2.58 8 8 8 19.09 1.96 -8 -8 8 19.16 1.80 -8 8 -8 18.64 1.65 8 9 -8 2.72 1.70 -8 9 8 1.22 1.66 8 -9 8 3.51 2.12 -8 -9 -8 2.25 1.51 8 9 8 2.18 1.47 -8 -9 8 0.42 1.34 -8 9 -8 2.24 1.22 -8 -10 -8 25.20 2.31 -8 10 8 27.91 2.79 8 10 -8 28.98 2.76 -8 10 -8 25.75 2.30 8 10 8 25.71 2.45 8 -10 -8 27.98 3.04 -8 -10 8 25.12 2.32 8 11 -8 13.95 2.45 -8 -11 -8 13.47 2.18 -8 11 8 12.85 2.30 -8 11 -8 16.23 2.08 -8 -11 8 17.01 2.03 8 -11 -8 17.30 3.07 8 11 8 19.03 2.47 -8 12 8 104.73 4.69 8 12 -8 109.74 4.97 -8 -12 -8 96.93 4.23 -8 12 -8 100.56 4.32 8 -12 -8 104.11 5.48 -8 -12 8 96.39 3.93 8 12 8 95.90 4.57 -8 0 9 66.42 2.60 -8 0 -9 63.76 2.35 -8 0 9 65.86 2.28 8 0 -9 69.36 1.96 -8 1 9 164.98 4.73 -8 -1 -9 174.50 4.59 -8 1 -9 168.90 4.43 -8 -1 9 170.43 4.77 -8 -1 9 173.30 4.48 8 -1 -9 173.32 3.84 8 2 -9 18.72 1.41 -8 2 9 17.32 1.49 -8 -2 -9 16.85 1.53 -8 -2 9 16.16 1.41 -8 2 -9 15.87 1.37 -8 -2 9 17.32 1.47 8 3 -9 39.65 1.94 -8 -3 -9 44.97 2.25 -8 3 9 40.21 2.39 -8 3 -9 42.54 1.81 -8 -3 9 43.10 1.96 -8 -3 9 39.33 2.10 8 3 9 44.97 1.64 -8 -4 -9 2.43 1.15 8 4 -9 2.99 1.00 -8 -4 -9 2.93 0.91 -8 4 9 2.66 1.16 -8 -4 9 3.64 1.00 -8 -4 9 3.65 1.12 8 4 9 2.61 0.86 -8 4 -9 5.08 0.88 -8 -5 -9 57.90 2.80 -8 -5 -9 57.66 2.49 -8 5 9 62.28 2.98 8 5 -9 60.52 2.59 -8 -5 9 66.72 2.60 -8 5 -9 58.29 2.23 8 5 9 56.32 2.43 -8 -6 -9 36.16 2.51 -8 6 9 33.41 2.69 -8 -6 -9 36.95 2.25 8 6 -9 34.10 2.41 -8 6 -9 36.76 1.93 8 6 9 37.46 2.27 -8 -6 9 37.51 2.20 8 7 -9 232.43 6.56 -8 7 9 228.25 6.71 -8 -7 -9 238.06 6.36 -8 7 -9 236.29 6.16 8 7 9 244.11 6.57 -8 -7 9 237.66 6.33 -8 8 9 7.93 1.78 8 8 -9 5.40 1.60 -8 -8 -9 8.55 1.58 8 8 9 7.37 1.61 -8 8 -9 7.05 1.28 8 9 -9 19.31 2.33 -8 -9 -9 21.04 2.05 -8 9 9 24.00 2.60 -8 -9 9 18.79 1.90 8 9 9 25.49 2.31 -8 9 -9 23.78 2.10 -8 10 9 5.91 2.33 8 10 -9 10.76 2.19 -8 -10 -9 5.84 1.73 -8 10 -9 8.12 1.65 8 10 9 8.67 1.96 8 -10 -9 5.27 2.41 -8 -10 9 7.63 1.71 -8 11 9 11.42 2.37 -8 -11 -9 7.01 1.89 8 11 -9 12.15 2.43 -8 11 9 9.70 2.56 8 -11 -9 9.02 2.77 8 11 9 9.79 2.19 -8 11 -9 9.86 1.93 -8 -11 9 8.45 1.85 -8 0 -10 58.81 2.34 -8 0 10 58.71 2.56 8 0 -10 62.56 1.96 -8 0 10 60.75 2.34 -8 1 10 39.40 2.15 -8 -1 -10 36.18 1.88 -8 -1 10 35.91 1.84 -8 -1 10 36.74 2.09 8 -1 -10 32.45 1.33 -8 1 -10 33.88 1.81 -8 2 10 278.03 7.20 -8 -2 -10 286.42 7.03 -8 -2 10 276.51 6.86 -8 2 -10 280.07 6.76 -8 -2 10 277.82 7.20 -8 3 10 14.52 1.56 -8 -3 -10 16.00 1.55 8 3 -10 13.41 1.27 -8 -3 10 14.30 1.32 -8 3 -10 14.32 1.23 -8 -3 10 15.35 1.55 8 3 10 13.52 1.19 -8 4 10 75.36 3.10 -8 -4 -10 70.38 2.88 8 4 -10 69.36 2.78 8 4 10 75.96 2.56 -8 4 -10 73.27 2.53 -8 -4 10 74.85 3.08 -8 -4 10 70.31 2.67 -8 -5 -10 51.23 2.34 8 5 -10 53.11 2.51 -8 5 10 51.92 2.93 -8 -5 -10 54.23 2.76 8 5 10 51.62 2.34 -8 5 -10 51.20 2.21 -8 -5 10 53.08 2.36 8 6 -10 84.51 3.40 -8 6 10 82.58 3.63 -8 -6 -10 79.91 3.54 -8 -6 -10 84.88 3.22 8 6 10 84.68 3.22 -8 6 -10 84.59 3.02 -8 -6 10 87.07 3.19 -8 7 10 5.70 1.75 -8 -7 -10 0.33 1.39 8 7 -10 3.31 1.49 8 7 10 1.63 1.24 -8 -7 10 1.41 1.19 -8 7 -10 2.85 1.11 -8 8 10 4.98 1.77 8 8 -10 6.48 1.69 -8 -8 -10 3.68 1.45 -8 8 -10 4.74 1.31 8 8 10 7.16 1.57 -8 -8 10 7.17 1.50 -8 9 10 4.47 2.00 -8 -9 -10 2.40 1.51 8 9 -10 4.83 1.91 -8 9 -10 1.61 1.33 -8 -9 10 3.59 1.47 8 9 10 4.76 1.71 -8 10 10 21.86 2.80 8 10 -10 20.64 2.59 -8 -10 -10 16.43 2.15 -8 -10 10 19.77 2.00 8 10 10 18.03 2.30 -8 10 -10 21.29 2.17 8 11 -10 2.06 2.18 -8 11 10 5.50 2.50 -8 -11 -10 1.66 1.81 -8 11 10 1.96 2.00 8 11 10 3.40 1.97 8 -11 -10 6.13 2.85 -8 11 -10 4.81 1.80 -8 -11 10 3.04 1.70 -8 0 11 29.12 1.85 -8 0 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137.31 3.83 -10 1 -7 132.01 3.45 -10 -1 7 135.79 3.93 10 -2 7 70.94 2.63 -10 -2 -7 72.44 2.54 -10 2 7 75.06 2.63 -10 -2 7 77.22 2.75 -10 2 -7 76.41 2.19 10 3 -7 37.07 1.58 -10 -3 -7 35.91 1.94 10 -3 7 31.94 2.00 -10 3 7 29.44 1.88 -10 -3 7 35.91 2.01 -10 3 -7 35.12 1.40 -10 -3 7 37.70 1.81 -10 4 7 9.12 1.26 10 4 -7 9.12 1.08 -10 -4 -7 9.20 1.32 10 -4 7 9.15 1.45 -10 -4 7 8.24 1.12 -10 -4 7 7.96 1.25 -10 4 -7 9.98 0.86 10 5 -7 204.68 5.32 -10 5 7 202.63 5.54 10 -5 7 193.67 5.80 -10 -5 -7 199.93 5.62 -10 -5 7 191.59 5.28 -10 5 -7 194.43 4.86 -10 -5 7 199.99 5.66 10 5 7 206.38 5.01 10 6 -7 22.47 2.02 -10 -6 -7 22.62 2.06 10 -6 7 21.11 2.24 -10 -6 7 25.00 2.01 -10 6 -7 23.89 1.55 10 6 7 23.95 1.84 -10 7 7 67.54 2.99 -10 -7 -7 64.83 2.90 10 -7 7 60.73 3.38 10 7 -7 65.97 3.03 -10 -7 7 67.16 2.92 -10 7 -7 66.48 2.53 10 7 7 68.59 2.95 -10 -8 -7 1.02 1.44 10 -8 7 3.41 1.99 -10 8 7 -0.11 1.36 10 8 -7 0.35 1.39 -10 -8 7 1.51 1.36 -10 8 -7 2.49 1.07 10 8 7 1.26 1.24 10 -9 7 28.79 3.05 10 9 -7 24.95 2.41 -10 -9 -7 28.63 2.31 -10 9 7 26.36 2.49 10 9 7 29.58 2.39 -10 -9 7 24.05 2.16 -10 9 -7 26.88 2.10 -10 -10 -7 10.97 2.01 10 -10 7 14.69 2.92 -10 10 7 13.69 2.44 10 10 -7 17.00 2.39 -10 -10 7 13.43 1.97 10 10 7 13.53 2.10 10 -10 -7 16.90 2.88 -10 10 -7 16.98 1.85 10 -11 7 61.97 4.43 10 11 -7 62.84 3.84 -10 -11 -7 55.62 3.33 -10 11 7 59.49 3.59 10 -11 -7 63.19 4.29 -10 11 -7 62.16 3.19 10 11 7 59.26 3.44 -10 0 -8 550.47 12.28 -10 0 8 554.08 12.61 -10 1 8 8.93 1.16 -10 -1 -8 7.00 1.02 -10 -1 8 7.05 1.10 -10 1 -8 8.33 0.92 -10 -2 -8 69.60 2.54 -10 2 8 67.71 2.63 10 -2 8 68.22 2.53 -10 2 -8 66.83 2.20 -10 -2 8 66.99 2.69 -10 3 8 15.69 1.47 10 3 -8 14.93 1.11 10 -3 8 14.78 1.49 -10 -3 -8 16.60 1.51 -10 -3 8 14.62 1.26 -10 3 -8 13.24 1.09 -10 -3 8 15.27 1.48 -10 -4 -8 1.36 1.10 10 4 -8 1.22 0.87 10 -4 8 3.38 1.26 -10 4 8 1.63 1.04 -10 4 -8 1.72 0.71 -10 -4 8 1.74 1.09 -10 -4 8 1.90 0.90 10 5 -8 18.27 1.58 -10 -5 -8 18.03 1.82 10 -5 8 17.41 1.95 -10 5 8 16.48 1.70 -10 -5 8 24.30 2.10 10 5 8 17.62 1.45 -10 -5 8 18.43 1.67 -10 5 -8 17.90 1.40 -10 -6 -8 93.63 3.68 -10 6 8 89.31 3.56 10 -6 8 84.71 3.92 10 6 -8 90.64 3.38 -10 -6 8 88.63 3.24 -10 6 -8 91.18 2.94 10 6 8 97.83 3.19 10 7 -8 32.46 2.42 10 -7 8 36.52 2.96 -10 -7 -8 30.90 2.15 -10 7 8 28.32 2.50 -10 -7 8 32.86 2.17 -10 7 -8 31.26 1.88 10 7 8 30.00 2.12 -10 8 8 85.24 3.74 10 8 -8 87.93 3.68 10 -8 8 89.51 4.40 -10 -8 -8 83.47 3.36 10 8 8 82.05 3.40 -10 8 -8 83.89 3.10 -10 -8 8 86.45 3.43 -10 -9 -8 14.65 2.01 10 -9 8 13.42 2.68 -10 9 8 12.80 2.16 10 9 -8 13.95 2.13 -10 9 -8 16.71 1.72 10 9 8 15.16 1.94 -10 -9 8 13.18 1.86 10 10 -8 42.26 3.24 -10 10 8 45.14 3.42 10 -10 8 42.94 3.67 -10 -10 -8 37.68 2.72 10 10 8 45.27 3.01 -10 10 -8 45.16 2.73 -10 -10 8 42.14 2.80 10 -10 -8 47.23 3.72 10 11 -8 3.46 2.24 -10 11 8 7.16 2.43 -10 11 8 5.86 2.03 -10 -11 -8 2.30 1.86 -10 11 -8 5.90 1.71 -10 -11 8 5.95 1.95 10 -11 -8 8.14 2.84 10 11 8 6.15 2.02 -10 0 -9 68.82 2.47 -10 0 9 70.72 2.76 -10 -1 -9 73.57 2.60 10 1 -9 76.63 2.03 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3.33 -10 -8 -14 49.42 3.24 -10 -8 14 54.85 3.08 -10 8 -14 54.87 3.00 10 8 14 49.46 2.78 10 9 -14 6.85 2.22 -10 9 14 3.63 2.36 -10 -9 -14 2.72 1.87 -10 9 -14 7.67 1.86 10 9 14 8.20 1.81 -10 -9 14 3.83 1.82 -10 0 15 12.25 2.00 -10 0 -15 11.81 1.82 10 0 -15 10.51 1.22 10 1 -15 56.38 2.40 -10 -1 -15 57.27 3.09 -10 1 15 61.49 3.38 -10 -1 15 60.48 3.33 10 -1 -15 57.47 2.08 -10 1 -15 59.72 2.81 10 2 -15 18.36 1.62 -10 2 15 19.01 2.29 -10 -2 -15 16.29 2.07 -10 2 -15 17.00 1.91 -10 -2 15 19.63 1.97 -10 -3 -15 42.28 2.91 -10 3 15 42.99 3.06 -10 -3 15 38.78 2.62 -10 3 -15 39.38 2.50 -10 -4 -15 4.57 1.83 -10 4 15 4.98 1.96 -10 4 -15 5.40 1.48 -10 -4 15 5.71 1.56 10 5 -15 126.75 4.38 -10 5 15 131.84 5.28 -10 -5 15 126.04 4.37 -10 5 -15 120.17 4.25 -10 6 15 8.27 2.25 10 6 -15 5.37 1.70 10 6 15 6.55 1.21 -10 -6 15 6.44 1.64 -10 6 -15 7.39 1.64 10 7 -15 28.75 2.58 -10 7 15 29.60 3.08 -10 -7 15 37.10 2.71 -10 7 -15 36.50 2.59 10 7 15 33.22 2.22 10 8 -15 2.55 2.07 -10 8 15 1.74 2.16 -10 -8 -15 -1.76 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23.97 2.27 -11 -6 -10 28.14 2.52 -11 6 -10 25.74 1.85 -11 -6 10 23.81 2.05 11 6 10 22.39 1.65 -11 7 10 -3.57 1.45 11 7 -10 0.38 1.43 -11 -7 10 -1.66 1.32 11 7 10 0.43 1.13 -11 7 -10 -0.86 0.98 11 8 -10 5.07 1.67 -11 -8 -10 4.08 1.66 -11 8 10 4.34 1.91 11 8 10 2.57 1.36 -11 8 -10 2.77 1.25 -11 -8 10 4.24 1.64 -11 9 10 40.64 3.41 -11 -9 -10 47.82 2.95 11 9 -10 50.40 3.23 11 9 10 51.24 2.91 -11 9 -10 50.38 2.76 -11 -9 10 52.64 3.03 -11 10 10 64.75 3.95 -11 -10 -10 58.67 3.40 11 10 -10 63.21 3.70 -11 -10 10 57.19 3.22 11 10 10 54.16 3.15 -11 10 -10 62.64 3.17 -11 0 11 2.13 1.17 -11 0 -11 -0.83 1.04 11 1 -11 131.89 3.20 -11 -1 -11 131.55 4.07 -11 1 11 130.54 4.28 -11 -1 11 128.72 4.33 -11 1 -11 128.10 3.85 11 2 -11 1.38 0.80 -11 2 11 1.34 1.21 -11 -2 -11 1.74 1.19 -11 2 -11 3.07 1.06 -11 -2 11 2.43 1.25 -11 3 11 14.38 1.84 -11 -3 -11 13.32 1.75 -11 -3 11 16.86 1.88 -11 3 -11 11.99 1.32 11 4 -11 135.54 4.05 -11 4 11 135.22 4.61 -11 -4 -11 137.58 4.73 -11 4 -11 137.80 4.00 -11 -4 11 140.94 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26.42 3.20 -12 9 -8 29.48 2.14 -12 -9 8 27.99 2.58 12 9 8 26.07 2.34 12 -10 8 5.65 2.78 12 10 -8 3.51 2.06 -12 10 8 3.56 2.07 -12 -10 -8 0.51 1.75 -12 -10 8 1.72 1.83 12 10 8 2.45 1.63 -12 10 -8 3.37 1.48 12 -10 -8 1.51 2.51 12 11 -8 11.04 2.47 -12 11 8 15.32 2.52 -12 -11 -8 7.42 2.17 -12 11 8 8.93 2.30 12 -11 8 10.16 3.02 -12 -11 8 9.99 2.18 12 11 8 9.84 2.03 -12 11 -8 9.04 1.81 12 -11 -8 10.97 3.10 -12 0 -9 419.71 9.76 -12 0 9 426.77 10.16 -12 -1 -9 38.82 2.03 -12 1 9 35.66 2.09 -12 1 -9 33.17 1.80 -12 -1 9 36.39 2.19 -12 -2 -9 31.43 2.05 -12 2 9 32.60 2.01 -12 -2 9 29.31 2.13 -12 2 -9 31.76 1.66 -12 -3 -9 0.74 1.17 -12 3 9 0.48 1.16 -12 3 -9 1.12 0.81 -12 -3 9 0.18 1.15 -12 -4 -9 4.69 1.48 12 -4 9 2.96 1.43 -12 4 9 4.08 1.29 -12 -4 9 4.40 1.41 -12 4 -9 3.93 0.91 -12 -5 -9 16.74 2.00 12 -5 9 19.53 2.12 -12 5 9 16.32 1.83 -12 5 -9 17.77 1.50 -12 -5 9 14.18 1.83 12 6 -9 52.50 2.68 12 -6 9 54.75 3.38 -12 -6 -9 55.58 3.09 -12 6 9 57.83 2.99 -12 6 -9 52.45 2.24 -12 -6 9 57.12 2.83 -12 -7 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12.95 1.91 -13 7 -2 12.12 1.18 13 7 2 14.69 1.42 -13 8 2 57.77 2.68 13 8 -2 53.22 2.73 13 -8 2 61.00 3.72 13 8 2 52.28 2.63 13 -8 -2 52.10 3.28 -13 8 -2 57.47 2.39 -13 -8 2 51.26 2.88 -13 9 2 46.64 2.65 13 9 -2 43.82 2.81 13 -9 2 46.05 3.71 -13 9 2 47.59 2.62 -13 -9 -2 41.61 2.72 -13 -9 2 42.14 2.72 13 -9 -2 44.85 3.58 -13 9 -2 48.80 2.46 13 9 2 40.67 2.73 -13 -10 -2 38.79 2.78 13 10 -2 33.84 2.84 -13 10 2 42.77 2.69 13 -10 2 37.09 3.70 13 10 2 34.56 2.74 -13 -10 2 37.06 2.73 -13 10 -2 41.00 2.48 13 -10 -2 36.40 3.55 -13 -11 -2 19.60 2.42 -13 11 2 15.75 2.10 13 -11 2 25.29 3.42 13 11 -2 15.68 2.35 13 -11 -2 20.86 3.13 -13 11 -2 20.85 2.11 -13 -11 2 19.04 2.41 13 11 2 15.51 2.33 -13 0 -3 0.32 0.59 -13 0 3 0.21 0.61 -13 1 3 184.90 4.48 -13 -1 -3 185.19 4.62 -13 -1 3 191.14 4.76 -13 1 -3 179.92 4.17 -13 1 -3 176.66 4.13 -13 -2 -3 109.22 3.30 -13 2 3 106.18 2.87 -13 -2 3 106.69 3.34 -13 3 3 49.77 1.76 -13 -3 -3 51.31 2.34 13 -3 3 50.78 2.39 -13 -3 3 48.56 2.35 13 -4 3 68.52 3.14 -13 4 3 67.36 2.25 -13 -4 -3 72.96 2.96 -13 -4 3 70.53 2.87 -13 5 3 6.68 1.02 13 5 -3 6.81 0.78 13 -5 3 3.71 1.42 -13 -5 -3 6.22 1.42 -13 5 -3 5.64 0.63 -13 -5 3 6.23 1.38 -13 -6 -3 1.45 1.38 -13 6 3 2.89 1.06 13 -6 3 3.34 1.54 13 6 -3 2.54 0.98 -13 -6 3 2.96 1.38 -13 6 -3 1.44 0.73 13 6 3 0.34 0.71 13 7 -3 8.11 1.34 -13 -7 -3 6.72 1.74 13 -7 3 9.62 2.05 -13 7 3 8.02 1.34 13 7 3 6.34 1.17 -13 -7 3 4.26 1.58 -13 7 -3 6.67 0.97 13 8 -3 43.24 2.58 -13 8 3 48.16 2.50 13 -8 3 45.19 3.52 13 8 3 45.16 2.43 -13 -8 3 48.35 2.78 -13 8 -3 45.02 2.14 13 -8 -3 52.11 3.45 -13 -9 -3 55.52 2.99 13 9 -3 53.77 3.06 -13 9 3 63.40 3.03 13 -9 3 55.99 3.98 -13 -9 3 55.45 3.11 -13 9 -3 63.04 2.69 13 9 3 52.08 2.93 13 -9 -3 60.71 3.87 -13 10 3 46.14 2.86 -13 -10 -3 45.75 3.06 13 -10 3 44.26 3.85 13 10 -3 43.90 3.07 -13 10 -3 48.78 2.59 13 10 3 35.69 2.83 13 -10 -3 35.91 3.52 -13 -10 3 41.73 2.96 13 11 -3 21.50 2.55 13 -11 3 21.97 3.45 -13 11 3 21.05 2.37 -13 -11 -3 17.38 2.48 -13 11 -3 19.32 2.04 13 11 3 18.62 2.33 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32.31 2.70 14 -11 2 30.96 3.64 14 11 -2 26.59 2.64 -14 -11 -2 23.88 2.69 14 11 2 27.97 2.54 -14 11 -2 28.83 2.45 -14 -11 2 25.04 2.65 14 -11 -2 28.80 3.59 -14 0 -3 367.54 8.27 -14 0 3 366.11 8.45 -14 1 3 34.80 1.57 -14 -1 -3 34.60 1.73 -14 -1 3 36.77 1.87 -14 1 -3 33.51 1.29 -14 2 3 21.83 1.25 -14 -2 -3 20.11 1.58 -14 -2 3 20.20 1.55 -14 -3 -3 11.44 1.41 14 -3 3 14.70 1.50 -14 3 3 12.87 1.16 -14 -3 3 11.95 1.38 14 -4 3 19.88 1.85 -14 4 3 19.58 1.38 -14 -4 -3 17.04 1.69 -14 -4 3 16.98 1.68 -14 5 3 24.26 1.61 -14 -5 -3 15.56 1.88 14 -5 3 16.08 1.98 -14 -5 3 18.60 1.91 14 6 -3 104.33 2.85 14 -6 3 101.69 4.18 -14 6 3 98.79 3.17 -14 -6 -3 96.82 3.98 -14 6 -3 97.32 2.76 -14 -6 3 102.87 3.95 14 -7 3 17.16 2.33 -14 7 3 19.16 1.62 -14 -7 -3 14.80 2.04 14 7 -3 13.27 1.43 -14 7 -3 12.52 1.18 -14 -7 3 16.59 2.11 14 -8 3 62.26 3.88 14 8 -3 66.03 2.93 -14 8 3 72.82 3.01 -14 8 -3 69.25 2.59 14 8 3 67.70 2.69 14 -8 -3 68.67 3.88 -14 9 3 3.29 1.62 14 9 -3 0.95 1.52 14 -9 3 -0.22 2.24 -14 9 -3 0.93 1.15 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86.32 4.14 -14 7 4 87.82 3.22 -14 -7 4 83.90 3.80 -14 7 -4 87.41 2.69 14 -8 4 6.84 2.10 -14 8 4 5.97 1.49 14 8 -4 4.80 1.47 -14 8 -4 5.94 1.14 14 8 4 4.66 1.22 14 -9 4 26.36 3.22 -14 9 4 33.06 2.51 14 9 -4 31.08 2.57 14 -9 -4 30.25 3.14 14 9 4 25.84 2.26 -14 -9 4 32.11 2.56 -14 9 -4 34.52 2.08 -14 10 4 2.17 1.70 14 10 -4 0.62 1.72 -14 10 4 5.82 1.95 14 -10 4 4.44 2.61 -14 -10 -4 2.55 1.92 -14 -10 4 2.78 1.92 14 -10 -4 4.74 2.60 -14 10 -4 4.49 1.40 14 10 4 2.19 1.65 -14 -11 -4 21.96 2.66 14 11 -4 26.91 2.65 -14 11 4 21.29 2.37 14 -11 4 28.24 3.61 -14 11 -4 27.34 2.37 -14 -11 4 23.55 2.64 14 -11 -4 25.62 3.29 14 11 4 26.14 2.39 -14 0 5 290.30 7.06 -14 0 -5 291.24 6.77 -14 1 5 4.37 0.91 -14 -1 -5 0.88 0.92 -14 -1 5 4.54 1.01 -14 1 -5 3.57 0.70 -14 2 5 64.04 2.32 -14 -2 -5 70.96 2.62 -14 2 -5 63.47 1.83 -14 -2 5 60.49 2.54 -14 3 5 3.95 0.97 -14 -3 -5 4.40 1.21 14 -3 5 2.77 1.16 -14 -3 5 4.71 1.18 -14 4 5 51.58 2.20 14 -4 5 52.99 2.96 -14 -4 -5 48.89 2.58 -14 -4 5 51.67 2.63 -14 -5 -5 3.61 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10 25.62 2.19 -14 3 -10 25.77 1.76 -14 -3 10 26.18 2.29 -14 4 10 2.77 1.46 -14 -4 -10 3.14 1.61 -14 4 -10 1.74 1.00 -14 -4 10 1.51 1.47 -14 -5 -10 13.32 2.02 -14 5 10 13.04 1.88 -14 -5 10 13.15 1.99 -14 5 -10 14.83 1.36 -14 -6 -10 0.44 1.75 -14 6 10 4.15 1.67 14 6 -10 -1.55 1.15 14 -6 10 3.27 1.88 -14 6 -10 2.66 1.08 -14 7 10 183.67 5.97 14 -7 10 203.52 6.59 14 7 -10 177.30 5.38 -14 -7 -10 192.28 6.27 -14 7 -10 191.58 5.17 14 -8 10 5.40 2.36 -14 8 10 4.59 2.00 14 8 -10 7.03 1.82 -14 8 -10 7.65 1.50 -14 -8 10 6.14 1.82 14 9 -10 8.76 2.04 -14 9 10 5.22 2.14 -14 -9 10 8.55 2.11 -14 9 -10 11.00 1.69 -14 0 -11 1.61 1.26 -14 0 11 3.39 1.39 -14 -1 -11 0.06 1.30 -14 1 11 1.36 1.39 -14 1 -11 2.00 1.21 -14 -1 11 1.72 1.36 -14 2 11 130.94 4.51 -14 -2 -11 134.97 4.43 -14 -2 11 136.60 4.72 -14 2 -11 134.94 4.02 -14 3 11 3.00 1.54 -14 -3 -11 3.67 1.56 -14 -3 11 3.77 1.56 -14 3 -11 0.57 1.06 -14 -4 -11 50.63 2.94 -14 4 11 47.87 2.83 -14 -4 11 49.60 3.07 -14 4 -11 49.26 2.29 -14 -5 -11 16.66 2.22 -14 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39.89 2.93 -15 10 -5 41.37 2.45 15 -10 -5 34.42 3.68 -15 -10 5 39.35 3.09 -15 0 6 -1.92 0.87 -15 0 -6 3.29 0.96 -15 1 6 48.71 2.29 -15 -1 -6 51.36 2.26 -15 -1 6 52.77 2.45 -15 1 -6 50.52 1.92 -15 2 6 38.32 2.05 -15 -2 -6 39.29 2.16 -15 -2 6 40.79 2.25 -15 2 -6 37.90 1.55 -15 3 6 123.38 3.60 -15 -3 -6 116.92 3.90 -15 -3 6 110.67 3.91 -15 3 -6 109.87 2.88 -15 4 6 21.77 1.71 -15 -4 -6 22.01 1.98 15 -4 6 21.53 2.08 -15 4 -6 21.32 1.09 -15 -4 6 22.39 2.03 -15 -5 -6 41.65 2.68 -15 5 6 40.26 2.24 15 -5 6 38.21 2.85 -15 -5 6 40.21 2.65 -15 5 -6 39.55 1.49 15 -6 6 53.25 3.51 -15 6 6 55.46 2.64 -15 -6 -6 54.57 3.10 -15 6 -6 49.24 1.87 -15 -6 6 49.90 3.03 15 -7 6 14.36 2.31 15 7 -6 8.52 1.28 -15 7 6 9.19 1.61 -15 -7 -6 11.96 2.13 -15 7 -6 9.98 1.11 -15 8 6 24.38 2.22 15 -8 6 26.50 3.03 15 8 -6 21.73 1.88 -15 8 -6 26.29 1.79 15 -9 6 36.70 3.59 -15 9 6 42.37 2.87 15 9 -6 36.13 2.63 -15 -9 6 33.18 2.87 -15 9 -6 38.57 2.21 -15 10 6 21.04 2.53 15 -10 6 14.21 3.12 15 10 -6 15.09 2.15 -15 -10 6 13.61 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47.25 3.34 -21 2 -12 46.18 2.83 -21 -2 12 46.94 3.65 -21 3 12 34.08 3.02 -21 -3 -12 26.06 2.98 -21 3 -12 35.80 2.54 -21 -3 12 28.92 3.12 -21 -4 -12 3.07 2.30 -21 4 12 2.66 2.15 -21 -4 12 -0.17 2.11 -21 4 -12 0.60 1.61 -21 0 13 -4.11 1.94 -21 0 -13 -0.09 1.89 -21 1 13 19.19 2.68 -21 -1 -13 17.42 2.62 -21 -1 13 20.47 2.81 -21 1 -13 19.14 2.32 -21 2 13 26.81 2.94 -21 -2 -13 25.62 2.95 -21 2 -13 30.09 2.64 -21 -2 13 21.25 2.95 -21 -3 -13 48.36 3.65 -21 3 13 44.40 3.42 -21 3 -13 45.96 2.91 -21 -3 13 51.86 3.81 -21 0 -14 0.49 2.02 -21 0 14 0.82 2.06 -21 1 14 3.89 2.28 -21 -1 14 0.60 2.25 -22 0 0 29.41 2.35 -22 -1 0 31.38 2.42 -22 1 0 35.16 2.05 -22 -2 0 1.49 1.55 -22 2 0 0.14 0.96 -22 -3 0 43.23 2.91 -22 3 0 37.84 1.79 -22 4 0 -2.25 0.81 -22 -4 0 1.54 1.83 -22 -5 0 159.54 5.76 22 -6 0 5.87 2.40 -22 -6 0 6.01 2.29 -22 -7 0 1.06 2.35 22 -7 0 -2.65 2.27 -22 0 1 232.35 6.26 -22 0 -1 229.71 6.19 -22 1 1 6.73 1.30 -22 -1 -1 -0.93 1.49 -22 1 -1 6.00 1.24 -22 -1 1 3.93 1.54 -22 2 1 6.13 1.16 -22 -2 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3 3.58 1.50 -22 1 -3 3.78 1.26 -22 -2 -3 10.72 1.91 -22 2 3 13.34 1.52 -22 -2 3 12.65 1.96 -22 2 -3 11.68 1.26 -22 3 3 0.89 1.17 -22 -3 -3 2.26 1.70 -22 -3 3 2.22 1.73 -22 3 -3 -0.31 0.78 -22 -4 -3 1.52 1.88 -22 4 3 0.89 1.18 -22 -4 3 3.53 1.95 -22 5 3 5.64 1.42 -22 -5 -3 5.31 2.15 -22 -5 3 4.29 2.18 -22 -6 -3 18.91 2.69 -22 6 3 21.57 1.97 -22 -6 3 20.84 2.81 -22 0 4 14.96 1.82 -22 0 -4 9.59 1.75 -22 1 4 30.24 2.18 -22 -1 -4 34.21 2.59 -22 1 -4 31.21 2.08 -22 -1 4 37.83 2.60 -22 2 4 6.71 1.45 -22 -2 -4 7.65 1.82 -22 -2 4 8.06 1.79 -22 2 -4 5.51 1.15 -22 -3 -4 27.03 2.50 -22 3 4 24.90 2.05 -22 -3 4 25.23 2.55 -22 -4 -4 1.86 1.93 -22 4 4 -2.18 1.20 -22 -4 4 -0.70 1.89 -22 -5 -4 85.57 4.32 -22 5 4 86.27 3.22 -22 -5 4 86.94 4.27 -22 -6 -4 5.48 2.29 -22 -6 4 3.13 2.16 -22 0 5 120.33 4.19 -22 0 -5 116.64 4.04 -22 -1 -5 2.00 1.59 -22 1 5 1.36 1.36 -22 1 -5 0.52 1.28 -22 -1 5 4.29 1.52 -22 2 5 30.79 2.25 -22 -2 -5 32.36 2.66 -22 -2 5 34.42 2.71 -22 2 -5 33.08 1.91 -22 -3 -5 0.55 1.80 -22 3 5 0.01 1.33 -22 -3 5 1.58 1.75 -22 4 5 15.39 1.75 -22 -4 -5 12.18 2.30 -22 -4 5 13.09 2.29 -22 5 5 1.37 1.50 -22 -5 -5 -0.27 2.06 -22 -5 5 4.60 2.19 -22 -6 -5 23.24 2.99 -22 6 5 25.81 2.31 -22 -6 5 26.31 2.99 -22 0 6 12.80 1.89 -22 0 -6 10.58 1.72 -22 1 6 41.82 2.60 -22 -1 -6 39.20 2.68 -22 1 -6 39.09 2.35 -22 -1 6 39.79 2.74 -22 2 6 3.48 1.49 -22 -2 -6 3.38 1.74 -22 2 -6 4.41 1.27 -22 -2 6 5.30 1.83 -22 -3 -6 36.14 2.84 -22 3 6 31.94 2.35 -22 -3 6 31.91 2.93 -22 3 -6 29.90 1.79 -22 -4 -6 0.32 1.98 -22 4 6 3.25 1.50 -22 -4 6 1.52 2.05 -22 -5 -6 51.63 3.49 -22 5 6 51.70 2.86 -22 -5 6 52.08 3.76 -22 -6 -6 0.71 2.25 -22 6 6 -1.34 1.53 -22 -6 6 2.08 2.29 -22 0 7 58.14 3.20 -22 0 -7 66.69 3.05 -22 1 7 6.74 1.75 -22 -1 -7 4.16 1.71 -22 1 -7 5.15 1.53 -22 -1 7 5.88 1.77 -22 2 7 88.65 3.61 -22 -2 -7 85.68 3.83 -22 -2 7 89.53 4.04 -22 3 7 0.89 1.49 -22 -3 -7 -0.05 1.86 -22 -3 7 0.94 1.95 -22 3 -7 0.80 1.17 -22 -4 -7 18.56 2.56 -22 4 7 21.49 2.16 -22 -4 7 21.10 2.70 -22 5 7 0.42 1.59 -22 -5 -7 4.86 2.32 -22 -5 7 1.32 2.13 -22 0 -8 2.15 1.65 -22 0 8 1.94 1.71 -22 -1 -8 40.85 2.85 -22 1 8 38.92 2.71 -22 -1 8 38.83 2.94 -22 1 -8 44.70 2.54 -22 -2 -8 4.50 1.89 -22 2 8 3.71 1.67 -22 -2 8 6.21 1.97 -22 2 -8 3.92 1.46 -22 -3 -8 19.59 2.54 -22 3 8 18.51 2.16 -22 3 -8 16.59 1.59 -22 -3 8 18.22 2.58 -22 4 8 -0.30 1.64 -22 -4 -8 2.77 2.11 -22 4 -8 2.57 1.19 -22 -4 8 2.11 2.18 -22 -5 -8 12.68 2.56 -22 5 8 13.95 2.09 -22 5 -8 16.41 1.46 -22 -5 8 14.99 2.75 -22 0 9 13.17 2.18 -22 0 -9 13.37 1.96 -22 1 9 5.51 1.91 -22 -1 -9 7.03 1.92 -22 1 -9 5.65 1.69 -22 -1 9 7.42 2.04 -22 -2 -9 75.48 3.65 -22 2 9 69.45 3.52 -22 2 -9 78.30 3.12 -22 -2 9 77.16 4.01 -22 3 9 2.52 1.72 -22 -3 -9 3.71 2.03 -22 -3 9 -0.06 2.02 -22 3 -9 1.33 1.40 -22 -4 -9 22.39 2.87 -22 4 9 25.56 2.48 -22 4 -9 32.21 1.98 -22 -4 9 29.22 3.11 -22 0 10 0.72 1.74 -22 0 -10 1.55 1.76 -22 1 10 65.85 3.65 -22 -1 -10 68.14 3.48 -22 -1 10 62.52 3.70 -22 1 -10 69.17 3.26 -22 2 10 13.08 2.22 -22 -2 -10 10.96 2.31 -22 2 -10 13.70 1.87 -22 -2 10 12.85 2.44 -22 3 10 19.09 2.42 -22 -3 -10 17.55 2.61 -22 -3 10 24.26 2.82 -22 3 -10 20.57 1.96 -22 -4 -10 0.95 2.12 -22 4 10 1.34 1.84 -22 -4 10 0.33 2.14 -22 4 -10 1.36 1.42 -22 0 11 -0.66 1.88 -22 0 -11 2.88 1.79 -22 1 11 6.24 2.06 -22 -1 -11 5.19 2.08 -22 1 -11 5.48 1.88 -22 -1 11 5.90 2.16 -22 -2 -11 66.06 3.71 -22 2 11 68.32 3.66 -22 -2 11 67.38 3.94 -22 2 -11 74.55 3.24 -22 3 11 1.13 1.84 -22 -3 -11 2.60 2.15 -22 3 -11 1.90 1.65 -22 -3 11 1.67 2.24 -22 0 -12 -0.77 1.88 -22 0 12 -0.80 2.02 -22 1 12 43.09 3.38 -22 -1 -12 57.53 3.49 -22 1 -12 50.48 3.14 -22 -1 12 52.31 3.71 -22 -2 -12 4.73 2.29 -22 2 12 10.57 2.35 -22 2 -12 6.69 1.98 -22 -2 12 9.34 2.45 -23 0 0 -2.70 1.24 -23 -1 0 76.84 3.46 -23 1 0 83.33 3.04 -23 2 0 6.66 1.23 -23 -2 0 5.48 1.82 -23 3 0 8.11 1.14 -23 -3 0 9.09 2.00 -23 -4 0 15.79 2.51 -23 -5 0 11.48 2.54 -23 -6 0 36.38 3.49 -23 0 1 2.04 1.36 -23 0 -1 0.87 1.35 -23 -1 -1 45.99 2.80 -23 1 1 51.76 2.47 -23 1 -1 49.64 2.42 -23 -1 1 46.30 2.83 -23 2 1 12.94 1.45 -23 -2 -1 12.52 1.97 -23 2 -1 12.94 1.37 -23 -2 1 10.21 1.90 -23 -3 -1 7.00 1.92 -23 3 1 6.51 1.21 -23 3 -1 8.40 1.08 -23 -3 1 11.15 2.15 -23 -4 -1 72.01 3.91 -23 4 1 70.34 2.57 -23 -4 1 74.56 4.03 -23 5 1 5.69 1.18 -23 -5 -1 2.95 2.24 -23 -5 1 5.71 2.21 -23 -6 -1 4.26 2.46 -23 6 1 4.75 1.17 -23 -6 1 2.49 2.41 -23 0 2 0.26 1.34 -23 0 -2 -1.45 1.30 -23 1 2 58.78 2.67 -23 -1 -2 51.98 2.89 -23 -1 2 54.00 2.95 -23 1 -2 53.02 2.51 -23 2 2 10.94 1.46 -23 -2 -2 10.75 1.99 -23 2 -2 12.29 1.31 -23 -2 2 12.31 2.06 -23 -3 -2 20.72 2.35 -23 3 2 19.60 1.62 -23 3 -2 18.54 1.39 -23 -3 2 19.22 2.36 -23 -4 -2 29.16 2.83 -23 4 2 26.95 1.93 -23 -4 2 28.54 2.86 -23 -5 -2 18.03 2.63 -23 5 2 20.68 1.63 -23 -5 2 19.64 2.76 -23 6 2 28.73 1.90 -23 -6 -2 22.45 3.04 -23 -6 2 17.11 2.78 -23 0 -3 0.47 1.36 -23 0 3 0.95 1.39 -23 -1 -3 18.19 2.10 -23 1 3 24.89 2.10 -23 1 -3 18.06 1.74 -23 -1 3 21.71 2.17 -23 -2 -3 17.59 2.15 -23 2 3 16.79 1.72 -23 -2 3 15.06 2.07 -23 2 -3 14.94 1.42 -23 3 3 19.01 1.71 -23 -3 -3 17.25 2.27 -23 -3 3 19.80 2.41 -23 -4 -3 80.94 4.03 -23 4 3 81.44 2.96 -23 -4 3 74.61 3.90 -23 5 3 -0.23 1.27 -23 -5 -3 -1.59 2.04 -23 -5 3 -0.84 2.09 -23 0 -4 -0.55 1.41 -23 0 4 -0.51 1.45 -23 1 4 39.23 2.43 -23 -1 -4 31.72 2.64 -23 -1 4 33.72 2.53 -23 2 4 8.58 1.54 -23 -2 -4 5.47 1.81 -23 2 -4 5.11 1.28 -23 -2 4 9.22 1.89 -23 3 4 42.21 2.41 -23 -3 -4 43.97 3.16 -23 3 -4 36.50 1.78 -23 -3 4 41.85 3.10 -23 4 4 17.79 1.78 -23 -4 -4 17.14 2.56 -23 -4 4 17.40 2.63 -23 -5 -4 15.31 2.65 -23 5 4 17.86 1.82 -23 -5 4 18.47 2.71 -23 0 -5 -1.53 1.40 -23 0 5 1.71 1.52 -23 -1 -5 26.47 2.38 -23 1 5 32.37 2.35 -23 1 -5 27.49 2.19 -23 -1 5 29.73 2.61 -23 2 5 28.17 2.24 -23 -2 -5 29.24 2.70 -23 -2 5 27.55 2.57 -23 2 -5 28.61 1.94 -23 3 5 24.47 2.16 -23 -3 -5 16.66 2.31 -23 3 -5 16.85 1.38 -23 -3 5 23.00 2.64 -23 4 5 44.84 2.56 -23 -4 -5 40.94 3.29 -23 -4 5 44.54 3.45 -23 5 5 -0.56 1.47 -23 -5 -5 1.19 2.18 -23 -5 5 -2.11 2.17 -23 0 6 -1.52 1.47 -23 0 -6 -3.87 1.44 -23 1 6 29.76 2.43 -23 -1 -6 26.02 2.38 -23 1 -6 28.06 2.24 -23 -1 6 33.29 2.74 -23 -2 -6 5.08 1.87 -23 2 6 7.85 1.68 -23 2 -6 5.99 1.37 -23 -2 6 5.68 1.93 -23 3 6 58.06 2.90 -23 -3 -6 59.80 3.58 -23 -3 6 63.79 3.68 -23 3 -6 57.85 2.34 -23 4 6 14.06 1.95 -23 -4 -6 12.68 2.44 -23 -4 6 18.65 2.72 -23 5 6 6.49 1.76 -23 -5 -6 9.20 2.35 -23 -5 6 7.43 2.46 -23 0 7 -1.63 1.61 -23 0 -7 -0.37 1.49 -23 1 7 21.96 2.25 -23 -1 -7 19.85 2.26 -23 1 -7 18.67 1.91 -23 -1 7 22.73 2.44 -23 -2 -7 45.01 3.06 -23 2 7 40.44 2.68 -23 2 -7 40.66 2.31 -23 -2 7 41.65 3.13 -23 -3 -7 10.25 2.18 -23 3 7 9.44 1.82 -23 -3 7 14.84 2.55 -23 3 -7 9.64 1.40 -23 4 7 22.28 2.26 -23 -4 -7 22.62 2.75 -23 -4 7 19.06 2.76 -23 0 -8 0.01 1.56 -23 0 8 -2.15 1.55 -23 -1 -8 4.97 1.83 -23 1 8 7.01 1.90 -23 1 -8 4.92 1.60 -23 -1 8 5.64 1.96 -23 2 8 11.28 1.94 -23 -2 -8 5.95 2.00 -23 2 -8 7.22 1.58 -23 -2 8 7.32 2.15 -23 3 8 67.11 3.26 -23 -3 -8 62.22 3.62 -23 -3 8 61.31 3.86 -23 3 -8 62.02 2.62 -23 -4 -8 19.43 2.66 -23 4 8 24.94 2.40 -23 4 -8 24.09 1.78 -23 -4 8 27.54 3.10 -23 0 -9 -0.25 1.67 -23 0 9 -0.55 1.83 -23 1 9 27.00 2.58 -23 -1 -9 23.11 2.47 -23 -1 9 28.23 2.81 -23 1 -9 28.29 2.46 -23 2 9 43.99 3.03 -23 -2 -9 42.48 3.06 -23 2 -9 48.44 2.64 -23 -2 9 47.04 3.45 -23 -3 -9 10.96 2.42 -23 3 9 14.84 2.17 -23 3 -9 10.08 1.66 -23 -3 9 11.17 2.56 -23 0 -10 0.06 1.80 -23 0 10 -1.88 1.77 -23 -1 -10 0.93 1.88 -23 1 10 1.62 1.84 -23 -1 10 3.79 2.08 -23 1 -10 -0.07 1.71 -23 2 10 4.93 1.91 -23 -2 -10 6.25 2.18 -23 -2 10 5.37 2.28 -24 0 0 42.28 2.57 -24 -1 0 32.08 2.62 -24 1 0 29.78 2.15 -24 2 0 12.46 1.45 -24 -2 0 13.07 2.16 -24 -3 0 2.97 1.93 -24 3 0 2.65 1.11 -24 -4 0 0.81 2.09 -24 4 0 1.69 1.00 -24 0 1 11.93 1.76 -24 0 -1 9.86 1.75 -24 1 1 1.37 1.30 -24 -1 -1 -0.65 1.59 -24 1 -1 1.13 1.32 -24 -1 1 2.02 1.65 -24 -2 -1 41.49 2.97 -24 2 1 40.32 2.18 -24 -2 1 40.28 2.93 -24 2 -1 37.77 2.08 -24 -3 -1 12.39 2.28 -24 3 1 9.91 1.37 -24 -3 1 11.46 2.24 -24 3 -1 10.35 1.20 -24 -4 -1 20.86 2.72 -24 4 1 23.88 1.74 -24 -4 1 22.58 2.79 -24 0 2 67.52 3.07 -24 0 -2 57.89 2.97 -24 -1 -2 46.56 2.86 -24 1 2 47.69 2.54 -24 -1 2 41.97 2.79 -24 1 -2 45.21 2.41 -24 2 2 16.81 1.68 -24 -2 -2 12.54 2.12 -24 2 -2 13.57 1.47 -24 -2 2 15.44 2.22 -24 3 2 6.50 1.38 -24 -3 -2 7.06 2.12 -24 3 -2 7.18 1.06 -24 -3 2 4.16 1.97 -24 4 2 4.32 1.25 -24 -4 -2 3.36 2.14 -24 -4 2 2.76 2.11 -24 0 3 23.67 2.18 -24 0 -3 16.88 2.00 -24 1 3 2.84 1.44 -24 -1 -3 2.21 1.66 -24 -1 3 2.51 1.65 -24 1 -3 1.93 1.39 -24 -2 -3 23.06 2.44 -24 2 3 28.68 2.11 -24 2 -3 22.62 1.84 -24 -2 3 26.35 2.56 -24 -3 -3 17.29 2.45 -24 3 3 13.19 1.64 -24 3 -3 14.03 1.22 -24 -3 3 15.06 2.34 -24 4 3 27.34 2.02 -24 -4 3 29.82 3.00 -24 0 4 45.19 2.78 -24 0 -4 47.25 2.76 -24 1 4 32.15 2.40 -24 -1 -4 30.44 2.63 -24 -1 4 34.06 2.69 -24 1 -4 35.02 2.34 -24 -2 -4 8.59 2.07 -24 2 4 8.27 1.64 -24 -2 4 6.87 1.97 -24 2 -4 5.69 1.32 -24 -3 -4 2.11 1.93 -24 3 4 4.77 1.48 -24 3 -4 1.98 0.97 -24 -3 4 5.66 2.09 -24 4 4 4.62 1.46 -24 -4 -4 5.52 2.28 -24 -4 4 4.10 2.14 -24 0 5 47.43 2.91 -24 0 -5 46.64 2.81 -24 1 5 3.32 1.63 -24 -1 -5 4.22 1.81 -24 -1 5 4.50 1.84 -24 1 -5 2.22 1.46 -24 -2 -5 24.73 2.54 -24 2 5 25.88 2.27 -24 -2 5 29.63 2.76 -24 2 -5 23.06 2.00 -24 3 5 23.21 2.08 -24 -3 -5 24.32 2.71 -24 -3 5 20.49 2.64 -24 3 -5 21.06 1.65 -24 4 5 8.03 1.71 -24 -4 -5 8.46 2.32 -24 -4 5 10.94 2.47 -24 0 -6 29.02 2.47 -24 0 6 24.94 2.41 -24 -1 -6 15.42 2.16 -24 1 6 16.18 2.07 -24 -1 6 16.74 2.32 -24 1 -6 15.46 1.81 -24 -2 -6 14.63 2.29 -24 2 6 15.65 1.99 -24 2 -6 13.89 1.66 -24 -2 6 19.61 2.47 -24 3 6 6.90 1.68 -24 -3 -6 7.03 2.16 -24 -3 6 8.24 2.27 -24 3 -6 5.71 1.27 -24 0 7 44.46 3.02 -24 0 -7 45.37 2.81 -24 -1 -7 1.79 1.83 -24 1 7 2.96 1.71 -24 1 -7 5.22 1.57 -24 -1 7 4.46 1.90 -24 2 7 13.24 2.03 -24 -2 -7 7.92 2.14 -24 2 -7 12.36 1.64 -24 -2 7 14.10 2.41 -24 3 7 7.64 1.86 -24 -3 -7 6.55 2.21 -24 -3 7 9.38 2.37 -24 3 -7 4.94 1.31 -24 0 -8 19.05 2.19 -24 1 8 26.47 2.58 -24 -1 -8 31.37 2.83 -24 -1 8 26.68 2.75 -24 1 -8 32.10 2.46 -24 2 8 25.26 2.45 -24 2 -8 30.02 2.29 -24 -2 8 26.93 2.83 -25 0 0 -0.56 1.43 -25 -1 0 15.31 2.05 -25 1 0 13.78 1.71 -25 2 0 24.78 2.01 -25 -2 0 23.57 2.55 -25 3 0 56.53 2.34 -25 -3 0 62.14 3.63 -25 0 1 -0.99 1.41 -25 0 -1 -0.67 1.44 -25 -1 -1 2.33 1.72 -25 1 1 2.28 1.42 -25 -1 1 3.75 1.70 -25 1 -1 3.61 1.44 -25 2 1 46.48 2.37 -25 -2 -1 43.47 3.11 -25 2 -1 41.49 2.21 -25 -2 1 41.56 3.05 -25 3 1 18.75 1.63 -25 -3 -1 19.22 2.63 -25 -3 1 17.92 2.52 -25 3 -1 18.56 1.59 -25 0 2 0.19 1.49 -25 0 -2 -0.20 1.47 -25 -1 -2 17.51 2.16 -25 1 2 16.26 1.85 -25 -1 2 18.93 2.19 -25 1 -2 16.70 1.80 -25 2 2 9.84 1.61 -25 -2 -2 13.62 2.30 -25 2 -2 9.05 1.41 -25 -2 2 15.83 2.28 -25 -3 -2 70.31 3.91 -25 3 2 73.15 2.86 -25 3 -2 71.56 2.44 -25 -3 2 70.47 3.85 -25 0 -3 -2.00 1.42 -25 0 3 0.72 1.54 -25 1 3 2.67 1.50 -25 -1 -3 2.54 1.66 -25 1 -3 -1.25 1.33 -25 -1 3 2.43 1.76 -25 -2 -3 36.06 2.99 -25 2 3 38.12 2.39 -25 2 -3 33.92 2.14 -25 -2 3 37.94 2.98 -25 0 4 -2.20 1.50 -25 0 -4 -0.47 1.44 -25 -1 -4 19.61 2.27 -25 1 4 19.70 2.07 -25 1 -4 18.13 1.87 -25 -1 4 17.46 2.24 -25 -2 -4 4.65 2.04 -25 2 4 6.39 1.67 -25 2 -4 5.45 1.37 -25 -2 4 8.25 2.02 -25 0 -5 0.09 1.55 -25 0 5 -0.98 1.58 -25 1 5 1.48 1.62 -25 -1 -5 -1.24 1.64 -25 1 -5 -2.24 1.38 -25 -1 5 1.80 1.71 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 39258 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Lu1 Lu 0.05840(2) 0.54225(2) 0.21139(2) 0.01552(6) Uani 1 1 d . . Lu2 Lu 0.19568(2) 0.32910(2) 0.16714(2) 0.01453(5) Uani 1 1 d . . Si1 Si 0.03231(11) 0.79602(18) 0.35920(10) 0.0216(4) Uani 1 1 d . . Si2 Si 0.21168(10) 0.07434(17) 0.01210(10) 0.0190(4) Uani 1 1 d . . N1 N 0.1097(3) 0.3541(5) 0.2574(3) 0.0166(11) Uani 1 1 d . . N2 N 0.1436(3) 0.5200(5) 0.1230(3) 0.0174(11) Uani 1 1 d . . O1 O 0.0120(3) 0.7151(5) 0.1385(3) 0.0244(11) Uani 1 1 d . . O2 O 0.2365(3) 0.1572(4) 0.2414(2) 0.0210(10) Uani 1 1 d . . C1 C 0.0898(4) 0.7024(6) 0.2979(4) 0.0204(14) Uani 1 1 d . . H1A H 0.1238 0.6588 0.3306 0.025 Uiso 1 1 calc R U H1B H 0.1162 0.7693 0.2701 0.025 Uiso 1 1 calc R U C2 C 0.0074(5) 0.6972(8) 0.4409(4) 0.038(2) Uani 1 1 d . . H2A H -0.0215 0.6228 0.4255 0.057 Uiso 1 1 calc R U H2B H -0.0188 0.7525 0.4752 0.057 Uiso 1 1 calc R U H2C H 0.0493 0.6642 0.4652 0.057 Uiso 1 1 calc R U C3 C -0.0493(5) 0.8549(9) 0.3123(5) 0.037(2) Uani 1 1 d . . H3A H -0.0384 0.9306 0.2810 0.056 Uiso 1 1 calc R U H3B H -0.0836 0.8808 0.3493 0.056 Uiso 1 1 calc R U H3C H -0.0684 0.7838 0.2820 0.056 Uiso 1 1 calc R U C4 C 0.0741(4) 0.9481(7) 0.3973(4) 0.0341(18) Uani 1 1 d . . H4A H 0.1167 0.9240 0.4234 0.051 Uiso 1 1 calc R U H4B H 0.0420 0.9914 0.4313 0.051 Uiso 1 1 calc R U H4C H 0.0855 1.0082 0.3570 0.051 Uiso 1 1 calc R U C5 C 0.0521(4) 0.2567(6) 0.2463(4) 0.0229(15) Uani 1 1 d . . H5 H 0.0731 0.1671 0.2422 0.028 Uiso 1 1 d R U C6 C 0.0151(3) 0.2881(6) 0.1738(5) 0.0244(14) Uani 1 1 d . . H6 H 0.0307 0.2424 0.1315 0.029 Uiso 1 1 calc R U C7 C -0.0372(3) 0.3739(6) 0.1644(5) 0.0234(13) Uani 1 1 d . . H7 H -0.0580 0.3714 0.1171 0.028 Uiso 1 1 calc R U C8 C -0.0669(3) 0.4682(6) 0.2132(6) 0.0247(12) Uani 1 1 d . . H8 H -0.0967 0.5325 0.1921 0.030 Uiso 1 1 calc R U C9 C -0.0563(4) 0.4750(7) 0.2902(4) 0.0229(14) Uani 1 1 d . . H9 H -0.0745 0.5507 0.3140 0.027 Uiso 1 1 calc R U C10 C -0.0238(4) 0.3884(7) 0.3338(4) 0.0278(17) Uani 1 1 d . . H10A H -0.0547 0.3752 0.3766 0.033 Uiso 1 1 calc R U H10B H 0.0180 0.4339 0.3525 0.033 Uiso 1 1 calc R U C11 C -0.0005(4) 0.2548(7) 0.3113(4) 0.0252(16) Uani 1 1 d . . H11A H -0.0415 0.2021 0.2969 0.030 Uiso 1 1 calc R U H11B H 0.0215 0.2108 0.3539 0.030 Uiso 1 1 calc R U C12 C 0.1393(4) 0.3492(7) 0.3318(4) 0.0251(16) Uani 1 1 d . . H12A H 0.1021 0.3599 0.3680 0.038 Uiso 1 1 calc R U H12B H 0.1732 0.4203 0.3376 0.038 Uiso 1 1 calc R U H12C H 0.1622 0.2642 0.3393 0.038 Uiso 1 1 calc R U C13 C -0.0476(4) 0.7040(9) 0.0896(5) 0.040(2) Uani 1 1 d . . H13A H -0.0915 0.7100 0.1176 0.048 Uiso 1 1 calc R U H13B H -0.0466 0.6192 0.0629 0.048 Uiso 1 1 calc R U C14 C -0.0411(5) 0.8162(9) 0.0377(5) 0.042(2) Uani 1 1 d . . H14A H -0.0869 0.8416 0.0173 0.051 Uiso 1 1 calc R U H14B H -0.0091 0.7950 -0.0032 0.051 Uiso 1 1 calc R U C15 C -0.0115(5) 0.9246(8) 0.0867(5) 0.0342(18) Uani 1 1 d . . H15A H 0.0128 0.9923 0.0572 0.041 Uiso 1 1 calc R U H15B H -0.0485 0.9672 0.1160 0.041 Uiso 1 1 calc R U C16 C 0.0390(4) 0.8502(7) 0.1356(4) 0.0274(16) Uani 1 1 d . . H16A H 0.0864 0.8517 0.1146 0.033 Uiso 1 1 calc R U H16B H 0.0404 0.8894 0.1853 0.033 Uiso 1 1 calc R U C17 C 0.1614(3) 0.1673(6) 0.0804(3) 0.0170(12) Uani 1 1 d . . H17A H 0.1380 0.0989 0.1101 0.020 Uiso 1 1 calc R U H17B H 0.1242 0.2102 0.0516 0.020 Uiso 1 1 calc R U C18 C 0.2364(5) 0.1833(8) -0.0668(4) 0.0340(18) Uani 1 1 d . . H18A H 0.1956 0.2328 -0.0832 0.051 Uiso 1 1 calc R U H18B H 0.2538 0.1292 -0.1074 0.051 Uiso 1 1 calc R U H18C H 0.2727 0.2447 -0.0511 0.051 Uiso 1 1 calc R U C19 C 0.1630(5) -0.0669(7) -0.0295(4) 0.0327(18) Uani 1 1 d . . H19A H 0.1538 -0.1332 0.0083 0.049 Uiso 1 1 calc R U H19B H 0.1909 -0.1061 -0.0688 0.049 Uiso 1 1 calc R U H19C H 0.1189 -0.0352 -0.0497 0.049 Uiso 1 1 calc R U C20 C 0.2934(4) -0.0002(9) 0.0499(5) 0.0369(19) Uani 1 1 d . . H20A H 0.3178 0.0652 0.0799 0.055 Uiso 1 1 calc R U H20B H 0.3233 -0.0281 0.0093 0.055 Uiso 1 1 calc R U H20C H 0.2816 -0.0766 0.0803 0.055 Uiso 1 1 calc R U C21 C 0.2017(4) 0.6149(7) 0.1347(4) 0.0264(16) Uani 1 1 d . . H21 H 0.1820 0.7057 0.1379 0.032 Uiso 1 1 d R U C22 C 0.2376(3) 0.5838(6) 0.2071(5) 0.0240(14) Uani 1 1 d . . H22 H 0.2210 0.6302 0.2488 0.029 Uiso 1 1 calc R U C23 C 0.2908(3) 0.4969(6) 0.2195(4) 0.0253(15) Uani 1 1 d . . H23 H 0.3099 0.5004 0.2676 0.030 Uiso 1 1 calc R U C24 C 0.3222(3) 0.4026(6) 0.1723(5) 0.0239(13) Uani 1 1 d . . H24 H 0.3520 0.3394 0.1944 0.029 Uiso 1 1 calc R U C25 C 0.3128(4) 0.3945(7) 0.0943(4) 0.0227(14) Uani 1 1 d . . H25 H 0.3342 0.3213 0.0710 0.027 Uiso 1 1 calc R U C26 C 0.2776(4) 0.4767(7) 0.0493(4) 0.0267(16) Uani 1 1 d . . H26A H 0.2352 0.4288 0.0340 0.032 Uiso 1 1 calc R U H26B H 0.3065 0.4867 0.0047 0.032 Uiso 1 1 calc R U C27 C 0.2549(4) 0.6106(7) 0.0698(5) 0.0287(17) Uani 1 1 d . . H27A H 0.2335 0.6529 0.0264 0.034 Uiso 1 1 calc R U H27B H 0.2962 0.6630 0.0836 0.034 Uiso 1 1 calc R U C28 C 0.1125(4) 0.5274(7) 0.0490(4) 0.0248(15) Uani 1 1 d . . H28A H 0.1030 0.6195 0.0367 0.037 Uiso 1 1 calc R U H28B H 0.0691 0.4773 0.0482 0.037 Uiso 1 1 calc R U H28C H 0.1449 0.4903 0.0130 0.037 Uiso 1 1 calc R U C29 C 0.2141(4) 0.0199(7) 0.2395(4) 0.0256(16) Uani 1 1 d . . H29A H 0.2240 -0.0193 0.1909 0.031 Uiso 1 1 calc R U H29B H 0.1636 0.0136 0.2490 0.031 Uiso 1 1 calc R U C30 C 0.2540(4) -0.0507(7) 0.2984(5) 0.0306(17) Uani 1 1 d . . H30A H 0.2963 -0.0927 0.2782 0.037 Uiso 1 1 calc R U H30B H 0.2251 -0.1187 0.3225 0.037 Uiso 1 1 calc R U C31 C 0.2726(4) 0.0592(8) 0.3517(4) 0.0320(18) Uani 1 1 d . . H31A H 0.2335 0.0785 0.3854 0.038 Uiso 1 1 calc R U H31B H 0.3142 0.0365 0.3810 0.038 Uiso 1 1 calc R U C32 C 0.2866(4) 0.1730(7) 0.3012(4) 0.0250(15) Uani 1 1 d . . H32A H 0.2795 0.2577 0.3268 0.030 Uiso 1 1 calc R U H32B H 0.3348 0.1696 0.2823 0.030 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Lu1 0.01449(11) 0.01520(10) 0.01686(11) 0.00024(12) -0.00006(13) 0.00134(10) Lu2 0.01443(10) 0.01429(10) 0.01486(10) -0.00035(12) 0.00056(13) 0.00085(10) Si1 0.0244(10) 0.0214(9) 0.0191(9) -0.0032(7) 0.0051(8) 0.0015(8) Si2 0.0240(10) 0.0161(8) 0.0170(8) -0.0016(7) 0.0013(8) 0.0008(7) N1 0.015(3) 0.016(3) 0.019(3) 0.001(2) 0.004(2) -0.001(2) N2 0.018(3) 0.014(3) 0.020(3) 0.003(2) 0.001(2) -0.001(2) O1 0.023(3) 0.020(2) 0.031(3) 0.005(2) -0.009(2) 0.001(2) O2 0.022(3) 0.019(2) 0.022(2) 0.0032(19) -0.007(2) 0.0028(19) C1 0.026(4) 0.017(3) 0.018(3) 0.000(3) -0.003(3) 0.001(3) C2 0.053(6) 0.038(5) 0.023(4) -0.006(3) 0.012(4) -0.004(4) C3 0.029(5) 0.047(5) 0.037(5) -0.003(4) 0.000(4) 0.020(4) C4 0.038(5) 0.030(4) 0.035(4) -0.007(3) 0.004(4) 0.003(3) C5 0.027(4) 0.013(3) 0.029(4) 0.002(3) 0.013(3) 0.003(3) C6 0.020(3) 0.025(3) 0.028(4) -0.003(4) -0.001(4) -0.005(3) C7 0.020(3) 0.030(3) 0.021(3) -0.002(4) -0.001(3) -0.010(2) C8 0.018(3) 0.025(3) 0.031(3) 0.002(4) 0.000(4) 0.002(3) C9 0.014(3) 0.020(3) 0.034(4) -0.003(3) 0.004(3) -0.002(3) C10 0.024(4) 0.027(4) 0.032(4) -0.001(3) 0.009(3) -0.008(3) C11 0.022(4) 0.024(4) 0.030(4) 0.004(3) 0.004(3) 0.000(3) C12 0.027(4) 0.031(4) 0.018(3) 0.003(3) 0.001(3) 0.008(3) C13 0.031(5) 0.041(4) 0.048(5) 0.015(4) -0.017(4) -0.004(4) C14 0.035(5) 0.043(5) 0.050(5) 0.022(4) -0.018(4) -0.003(4) C15 0.038(5) 0.026(4) 0.038(4) 0.011(3) -0.001(4) 0.009(3) C16 0.028(4) 0.024(3) 0.031(4) 0.005(3) -0.005(3) -0.004(3) C17 0.016(3) 0.019(3) 0.015(3) 0.004(3) 0.002(3) 0.004(3) C18 0.047(5) 0.034(4) 0.021(3) 0.001(3) 0.012(3) -0.011(4) C19 0.044(5) 0.026(4) 0.028(4) -0.007(3) 0.004(4) -0.005(3) C20 0.028(5) 0.040(4) 0.042(5) -0.003(4) 0.001(4) 0.010(4) C21 0.022(4) 0.027(4) 0.030(4) 0.006(3) 0.004(3) 0.003(3) C22 0.020(3) 0.023(3) 0.029(4) -0.010(4) 0.000(4) -0.005(2) C23 0.015(3) 0.033(3) 0.028(4) -0.005(3) -0.002(3) -0.010(2) C24 0.017(3) 0.020(3) 0.034(4) 0.004(3) -0.001(4) 0.000(2) C25 0.018(3) 0.022(3) 0.028(4) 0.000(3) 0.012(3) -0.001(3) C26 0.032(4) 0.024(4) 0.024(4) -0.002(3) 0.009(3) -0.005(3) C27 0.029(4) 0.024(4) 0.033(4) 0.001(3) 0.003(4) -0.002(3) C28 0.029(4) 0.030(4) 0.016(3) 0.002(3) 0.001(3) 0.001(3) C29 0.031(4) 0.020(3) 0.026(4) 0.006(3) -0.002(3) 0.000(3) C30 0.023(4) 0.028(4) 0.041(4) 0.014(3) -0.001(3) -0.002(3) C31 0.024(4) 0.045(5) 0.027(4) 0.013(3) -0.005(3) 0.000(3) C32 0.022(4) 0.031(4) 0.023(3) -0.004(3) -0.005(3) 0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Lu Lu -0.4720 5.8584 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N1 Lu1 N2 82.46(18) N1 Lu1 C1 102.7(2) N2 Lu1 C1 110.7(2) N1 Lu1 O1 167.32(18) N2 Lu1 O1 87.13(18) C1 Lu1 O1 87.70(19) N1 Lu1 C8 99.0(2) N2 Lu1 C8 131.1(3) C1 Lu1 C8 116.4(3) O1 Lu1 C8 82.4(2) N1 Lu1 C7 83.1(2) N2 Lu1 C7 101.8(2) C1 Lu1 C7 147.4(2) O1 Lu1 C7 92.01(19) C8 Lu1 C7 31.8(2) N1 Lu1 C9 87.0(2) N2 Lu1 C9 156.9(2) C1 Lu1 C9 91.6(2) O1 Lu1 C9 100.11(19) C8 Lu1 C9 31.1(3) C7 Lu1 C9 56.3(2) N1 Lu1 C6 56.8(2) N2 Lu1 C6 87.2(2) C1 Lu1 C6 151.8(2) O1 Lu1 C6 115.7(2) C8 Lu1 C6 56.2(2) C7 Lu1 C6 28.37(19) C9 Lu1 C6 69.8(2) N1 Lu1 C5 29.7(2) N2 Lu1 C5 94.75(18) C1 Lu1 C5 123.0(2) O1 Lu1 C5 145.6(2) C8 Lu1 C5 70.6(2) C7 Lu1 C5 54.0(2) C9 Lu1 C5 67.0(2) C6 Lu1 C5 30.6(2) N1 Lu1 Lu2 41.49(13) N2 Lu1 Lu2 40.97(13) C1 Lu1 Lu2 112.85(17) O1 Lu1 Lu2 127.65(13) C8 Lu1 Lu2 122.53(14) C7 Lu1 Lu2 92.90(15) C9 Lu1 Lu2 125.23(14) C6 Lu1 Lu2 66.35(14) C5 Lu1 Lu2 58.53(14) N2 Lu2 O2 164.76(18) N2 Lu2 N1 81.27(18) O2 Lu2 N1 85.01(18) N2 Lu2 C17 103.2(2) O2 Lu2 C17 87.76(18) N1 Lu2 C17 110.2(2) N2 Lu2 C24 100.37(19) O2 Lu2 C24 82.9(2) N1 Lu2 C24 128.1(2) C17 Lu2 C24 119.5(2) N2 Lu2 C23 83.5(2) O2 Lu2 C23 92.3(2) N1 Lu2 C23 99.4(2) C17 Lu2 C23 150.3(2) C24 Lu2 C23 31.5(2) N2 Lu2 C25 89.1(2) O2 Lu2 C25 100.78(19) N1 Lu2 C25 155.11(19) C17 Lu2 C25 94.3(2) C24 Lu2 C25 31.6(2) C23 Lu2 C25 56.5(2) N2 Lu2 C22 56.3(2) O2 Lu2 C22 116.2(2) N1 Lu2 C22 85.5(2) C17 Lu2 C22 153.0(2) C24 Lu2 C22 56.4(2) C23 Lu2 C22 28.8(2) C25 Lu2 C22 70.2(2) N2 Lu2 C21 29.7(2) O2 Lu2 C21 146.23(19) N1 Lu2 C21 93.52(19) C17 Lu2 C21 123.8(2) C24 Lu2 C21 71.5(2) C23 Lu2 C21 54.6(2) C25 Lu2 C21 68.2(2) C22 Lu2 C21 30.4(2) N2 Lu2 Lu1 40.61(14) O2 Lu2 Lu1 125.42(12) N1 Lu2 Lu1 40.67(13) C17 Lu2 Lu1 111.76(16) C24 Lu2 Lu1 122.02(14) C23 Lu2 Lu1 92.30(15) C25 Lu2 Lu1 126.15(15) C22 Lu2 Lu1 65.66(13) C21 Lu2 Lu1 58.08(15) C1 Si1 C2 111.2(3) C1 Si1 C4 113.1(3) C2 Si1 C4 105.1(4) C1 Si1 C3 113.0(4) C2 Si1 C3 108.6(4) C4 Si1 C3 105.3(4) C17 Si2 C19 113.8(3) C17 Si2 C18 110.4(3) C19 Si2 C18 105.6(4) C17 Si2 C20 113.6(4) C19 Si2 C20 105.0(4) C18 Si2 C20 107.9(4) C12 N1 C5 112.9(5) C12 N1 Lu1 121.9(4) C5 N1 Lu1 100.4(4) C12 N1 Lu2 111.6(4) C5 N1 Lu2 110.8(4) Lu1 N1 Lu2 97.8(2) C28 N2 C21 113.7(5) C28 N2 Lu1 110.1(4) C21 N2 Lu1 111.7(4) C28 N2 Lu2 122.2(4) C21 N2 Lu2 99.6(4) Lu1 N2 Lu2 98.4(2) C13 O1 C16 109.3(5) C13 O1 Lu1 125.5(4) C16 O1 Lu1 125.2(4) C29 O2 C32 108.4(5) C29 O2 Lu2 126.8(4) C32 O2 Lu2 124.6(4) Si1 C1 Lu1 127.8(4) Si1 C1 H1A 105.4 Lu1 C1 H1A 105.4 Si1 C1 H1B 105.4 Lu1 C1 H1B 105.4 H1A C1 H1B 106.0 Si1 C2 H2A 109.5 Si1 C2 H2B 109.5 H2A C2 H2B 109.5 Si1 C2 H2C 109.5 H2A C2 H2C 109.5 H2B C2 H2C 109.5 Si1 C3 H3A 109.5 Si1 C3 H3B 109.5 H3A C3 H3B 109.5 Si1 C3 H3C 109.5 H3A C3 H3C 109.5 H3B C3 H3C 109.5 Si1 C4 H4A 109.5 Si1 C4 H4B 109.5 H4A C4 H4B 109.5 Si1 C4 H4C 109.5 H4A C4 H4C 109.5 H4B C4 H4C 109.5 N1 C5 C6 108.8(5) N1 C5 C11 112.7(6) C6 C5 C11 110.8(6) N1 C5 Lu1 49.8(3) C6 C5 Lu1 68.4(3) C11 C5 Lu1 101.6(4) N1 C5 H5 108.1 C6 C5 H5 108.3 C11 C5 H5 108.0 Lu1 C5 H5 148.9 C7 C6 C5 126.4(7) C7 C6 Lu1 69.9(4) C5 C6 Lu1 81.0(4) C7 C6 H6 116.8 C5 C6 H6 116.8 Lu1 C6 H6 123.8 C6 C7 C8 131.0(8) C6 C7 Lu1 81.8(4) C8 C7 Lu1 69.2(3) C6 C7 H7 114.5 C8 C7 H7 114.5 Lu1 C7 H7 127.0 C9 C8 C7 126.2(7) C9 C8 Lu1 82.0(4) C7 C8 Lu1 79.0(4) C9 C8 H8 116.9 C7 C8 H8 116.9 Lu1 C8 H8 111.4 C10 C9 C8 128.4(7) C10 C9 Lu1 95.7(5) C8 C9 Lu1 66.9(4) C10 C9 H9 115.8 C8 C9 H9 115.8 Lu1 C9 H9 109.6 C9 C10 C11 125.3(7) C9 C10 H10A 106.0 C11 C10 H10A 106.0 C9 C10 H10B 106.0 C11 C10 H10B 106.0 H10A C10 H10B 106.3 C10 C11 C5 113.2(6) C10 C11 H11A 108.9 C5 C11 H11A 108.9 C10 C11 H11B 108.9 C5 C11 H11B 108.9 H11A C11 H11B 107.7 N1 C12 H12A 109.5 N1 C12 H12B 109.5 H12A C12 H12B 109.5 N1 C12 H12C 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 O1 C13 C14 105.3(7) O1 C13 H13A 110.7 C14 C13 H13A 110.7 O1 C13 H13B 110.7 C14 C13 H13B 110.7 H13A C13 H13B 108.8 C13 C14 C15 102.2(7) C13 C14 H14A 111.3 C15 C14 H14A 111.3 C13 C14 H14B 111.3 C15 C14 H14B 111.3 H14A C14 H14B 109.2 C16 C15 C14 102.9(6) C16 C15 H15A 111.2 C14 C15 H15A 111.2 C16 C15 H15B 111.2 C14 C15 H15B 111.2 H15A C15 H15B 109.1 O1 C16 C15 105.0(6) O1 C16 H16A 110.7 C15 C16 H16A 110.7 O1 C16 H16B 110.7 C15 C16 H16B 110.7 H16A C16 H16B 108.8 Si2 C17 Lu2 131.3(3) Si2 C17 H17A 104.4 Lu2 C17 H17A 104.4 Si2 C17 H17B 104.4 Lu2 C17 H17B 104.4 H17A C17 H17B 105.6 Si2 C18 H18A 109.5 Si2 C18 H18B 109.5 H18A C18 H18B 109.5 Si2 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 Si2 C19 H19A 109.5 Si2 C19 H19B 109.5 H19A C19 H19B 109.5 Si2 C19 H19C 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 Si2 C20 H20A 109.5 Si2 C20 H20B 109.5 H20A C20 H20B 109.5 Si2 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 N2 C21 C22 109.3(5) N2 C21 C27 111.4(6) C22 C21 C27 110.6(6) N2 C21 Lu2 50.7(3) C22 C21 Lu2 69.0(3) C27 C21 Lu2 98.6(4) N2 C21 H21 108.7 C22 C21 H21 108.2 C27 C21 H21 108.6 Lu2 C21 H21 151.3 C23 C22 C21 128.0(7) C23 C22 Lu2 70.4(4) C21 C22 Lu2 80.6(4) C23 C22 H22 116.0 C21 C22 H22 116.0 Lu2 C22 H22 124.7 C22 C23 C24 130.6(7) C22 C23 Lu2 80.8(4) C24 C23 Lu2 69.3(3) C22 C23 H23 114.7 C24 C23 H23 114.7 Lu2 C23 H23 128.0 C23 C24 C25 125.7(6) C23 C24 Lu2 79.3(4) C25 C24 Lu2 80.0(4) C23 C24 H24 117.2 C25 C24 H24 117.2 Lu2 C24 H24 113.3 C26 C25 C24 128.9(6) C26 C25 Lu2 91.8(5) C24 C25 Lu2 68.5(3) C26 C25 H25 115.6 C24 C25 H25 115.6 Lu2 C25 H25 112.9 C25 C26 C27 124.4(7) C25 C26 H26A 106.2 C27 C26 H26A 106.2 C25 C26 H26B 106.2 C27 C26 H26B 106.2 H26A C26 H26B 106.4 C26 C27 C21 114.2(6) C26 C27 H27A 108.7 C21 C27 H27A 108.7 C26 C27 H27B 108.7 C21 C27 H27B 108.7 H27A C27 H27B 107.6 N2 C28 H28A 109.5 N2 C28 H28B 109.5 H28A C28 H28B 109.5 N2 C28 H28C 109.5 H28A C28 H28C 109.5 H28B C28 H28C 109.5 O2 C29 C30 106.8(6) O2 C29 H29A 110.4 C30 C29 H29A 110.4 O2 C29 H29B 110.4 C30 C29 H29B 110.4 H29A C29 H29B 108.6 C29 C30 C31 103.0(6) C29 C30 H30A 111.2 C31 C30 H30A 111.2 C29 C30 H30B 111.2 C31 C30 H30B 111.2 H30A C30 H30B 109.1 C32 C31 C30 102.4(6) C32 C31 H31A 111.3 C30 C31 H31A 111.3 C32 C31 H31B 111.3 C30 C31 H31B 111.3 H31A C31 H31B 109.2 O2 C32 C31 104.7(6) O2 C32 H32A 110.8 C31 C32 H32A 110.8 O2 C32 H32B 110.8 C31 C32 H32B 110.8 H32A C32 H32B 108.9 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Lu1 N1 2.310(5) Lu1 N2 2.311(6) Lu1 C1 2.345(6) Lu1 O1 2.377(5) Lu1 C8 2.528(6) Lu1 C7 2.656(6) Lu1 C9 2.721(7) Lu1 C6 2.799(7) Lu1 C5 2.974(6) Lu1 Lu2 3.5118(4) Lu2 N2 2.328(5) Lu2 O2 2.345(4) Lu2 N1 2.348(5) Lu2 C17 2.374(6) Lu2 C24 2.550(6) Lu2 C23 2.679(6) Lu2 C25 2.700(7) Lu2 C22 2.807(6) Lu2 C21 2.966(7) Si1 C1 1.838(7) Si1 C2 1.859(8) Si1 C4 1.875(8) Si1 C3 1.887(9) Si2 C17 1.838(6) Si2 C19 1.874(7) Si2 C18 1.876(7) Si2 C20 1.877(8) N1 C12 1.470(9) N1 C5 1.500(9) N2 C28 1.477(9) N2 C21 1.492(9) O1 C13 1.456(9) O1 C16 1.469(8) O2 C29 1.461(8) O2 C32 1.464(8) C1 H1A 0.9900 C1 H1B 0.9900 C2 H2A 0.9800 C2 H2B 0.9800 C2 H2C 0.9800 C3 H3A 0.9800 C3 H3B 0.9800 C3 H3C 0.9800 C4 H4A 0.9800 C4 H4B 0.9800 C4 H4C 0.9800 C5 C6 1.534(10) C5 C11 1.557(10) C5 H5 1.0000 C6 C7 1.344(9) C6 H6 0.9500 C7 C8 1.426(10) C7 H7 0.9500 C8 C9 1.421(12) C8 H8 0.9500 C9 C10 1.339(10) C9 H9 0.9500 C10 C11 1.488(10) C10 H10A 0.9900 C10 H10B 0.9900 C11 H11A 0.9900 C11 H11B 0.9900 C12 H12A 0.9800 C12 H12B 0.9800 C12 H12C 0.9800 C13 C14 1.487(11) C13 H13A 0.9900 C13 H13B 0.9900 C14 C15 1.528(13) C14 H14A 0.9900 C14 H14B 0.9900 C15 C16 1.520(10) C15 H15A 0.9900 C15 H15B 0.9900 C16 H16A 0.9900 C16 H16B 0.9900 C17 H17A 0.9900 C17 H17B 0.9900 C18 H18A 0.9800 C18 H18B 0.9800 C18 H18C 0.9800 C19 H19A 0.9800 C19 H19B 0.9800 C19 H19C 0.9800 C20 H20A 0.9800 C20 H20B 0.9800 C20 H20C 0.9800 C21 C22 1.521(11) C21 C27 1.564(11) C21 H21 1.0001 C22 C23 1.372(9) C22 H22 0.9500 C23 C24 1.423(10) C23 H23 0.9500 C24 C25 1.436(11) C24 H24 0.9500 C25 C26 1.352(10) C25 H25 0.9500 C26 C27 1.478(10) C26 H26A 0.9900 C26 H26B 0.9900 C27 H27A 0.9900 C27 H27B 0.9900 C28 H28A 0.9800 C28 H28B 0.9800 C28 H28C 0.9800 C29 C30 1.503(10) C29 H29A 0.9900 C29 H29B 0.9900 C30 C31 1.523(12) C30 H30A 0.9900 C30 H30B 0.9900 C31 C32 1.503(10) C31 H31A 0.9900 C31 H31B 0.9900 C32 H32A 0.9900 C32 H32B 0.9900 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C2 Si1 C1 Lu1 80.2(5) C4 Si1 C1 Lu1 -161.8(4) C3 Si1 C1 Lu1 -42.2(6) C12 N1 C5 C6 168.5(5) Lu1 N1 C5 C6 37.2(5) Lu2 N1 C5 C6 -65.4(6) C12 N1 C5 C11 45.2(7) Lu1 N1 C5 C11 -86.1(5) Lu2 N1 C5 C11 171.2(4) C12 N1 C5 Lu1 131.3(6) Lu2 N1 C5 Lu1 -102.6(3) N1 C5 C6 C7 -86.4(8) C11 C5 C6 C7 38.0(9) Lu1 C5 C6 C7 -56.6(6) N1 C5 C6 Lu1 -29.8(4) C11 C5 C6 Lu1 94.7(5) C5 C6 C7 C8 8.5(11) Lu1 C6 C7 C8 -53.0(7) C5 C6 C7 Lu1 61.5(6) C6 C7 C8 C9 -13.7(11) Lu1 C7 C8 C9 -71.4(6) C6 C7 C8 Lu1 57.7(7) C7 C8 C9 C10 -8.5(11) Lu1 C8 C9 C10 -78.5(7) C7 C8 C9 Lu1 70.0(6) C8 C9 C10 C11 -9.4(12) Lu1 C9 C10 C11 -74.3(7) C9 C10 C11 C5 59.2(10) N1 C5 C11 C10 48.0(9) C6 C5 C11 C10 -74.2(8) Lu1 C5 C11 C10 -3.1(7) C16 O1 C13 C14 20.0(9) Lu1 O1 C13 C14 -159.9(6) O1 C13 C14 C15 -36.0(9) C13 C14 C15 C16 38.2(9) C13 O1 C16 C15 4.6(8) Lu1 O1 C16 C15 -175.5(5) C14 C15 C16 O1 -26.5(8) C19 Si2 C17 Lu2 167.9(4) C18 Si2 C17 Lu2 -73.5(5) C20 Si2 C17 Lu2 47.8(5) C28 N2 C21 C22 -170.7(5) Lu1 N2 C21 C22 64.1(6) Lu2 N2 C21 C22 -39.1(6) C28 N2 C21 C27 -48.1(8) Lu1 N2 C21 C27 -173.4(4) Lu2 N2 C21 C27 83.5(5) C28 N2 C21 Lu2 -131.6(6) Lu1 N2 C21 Lu2 103.1(3) N2 C21 C22 C23 87.3(8) C27 C21 C22 C23 -35.7(9) Lu2 C21 C22 C23 55.9(6) N2 C21 C22 Lu2 31.5(5) C27 C21 C22 Lu2 -91.5(5) C21 C22 C23 C24 -7.8(12) Lu2 C22 C23 C24 52.3(7) C21 C22 C23 Lu2 -60.1(7) C22 C23 C24 C25 12.7(11) Lu2 C23 C24 C25 69.2(6) C22 C23 C24 Lu2 -56.6(7) C23 C24 C25 C26 5.1(11) Lu2 C24 C25 C26 74.0(7) C23 C24 C25 Lu2 -68.9(6) C24 C25 C26 C27 15.1(12) Lu2 C25 C26 C27 78.6(8) C25 C26 C27 C21 -62.8(10) N2 C21 C27 C26 -48.8(9) C22 C21 C27 C26 72.9(8) Lu2 C21 C27 C26 2.2(7) C32 O2 C29 C30 -2.1(8) Lu2 O2 C29 C30 -178.7(4) O2 C29 C30 C31 24.4(8) C29 C30 C31 C32 -36.8(8) C29 O2 C32 C31 -21.5(7) Lu2 O2 C32 C31 155.2(5) C30 C31 C32 O2 36.0(7)