Crystallography Open Database

Information card for entry 1518020

Preview

Coordinates	1518020.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C120 H156 B2 Cl18 P4 Pb2 Pt2
Calculated formula	C120 H156 B2 Cl18 P4 Pb2 Pt2
Title of publication	Stepwise isolation of low-valent, low-coordinate Sn and Pb mono- and dications in the coordination sphere of platinum
Authors of publication	Braunschweig, Holger; Celik, Mehmet Ali; Dewhurst, Rian D.; Heid, Magdalena; Hupp, Florian; Sen, Sakya S.
Journal of publication	Chem. Sci.
Year of publication	2015
Journal volume	6
Journal issue	1
Pages of publication	425
a	10.5092 ± 0.0006 Å
b	15.3892 ± 0.001 Å
c	20.0776 ± 0.0012 Å
α	109.785 ± 0.002°
β	90.439 ± 0.002°
γ	90.796 ± 0.002°
Cell volume	3054.9 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0275
Residual factor for significantly intense reflections	0.0209
Weighted residual factors for significantly intense reflections	0.0435
Weighted residual factors for all reflections included in the refinement	0.0454
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1518020.cif
130961	2015-02-04	cif/ Updating files of 1518019, 1518020, 1518021, 1518022, 1518023, 1518024, 1518025, 1518026, 1518027 Original log message: Adding full bibliography for 1518019--1518027.cif.	1518020.cif
125441	2014-10-16	cif/ Adding structures of 1518019, 1518020, 1518021, 1518022, 1518023, 1518024, 1518025, 1518026, 1518027 via cif-deposit CGI script.	1518020.cif