#------------------------------------------------------------------------------ #$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $ #$Revision: 176729 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/51/84/1518465.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1518465 loop_ _publ_author_name 'Xu, Jin-Fang' 'Zhao, Hui-Jun' 'Wang, Xiao-Bing' 'Li, Zhong-Rui' 'Luo, Jun' 'Yang, Ming-Hua' 'Yang, Lei' 'Yu, Wen-Ying' 'Yao, He-Quan' 'Luo, Jian-Guang' 'Kong, Ling-Yi' _publ_section_title ; (+-)-Melicolones A and B, Rearranged Prenylated Acetophenone Stereoisomers with an Unusual 9-Oxatricyclo[3.2.1.1(3,8)]nonane Core from the Leaves of Melicope ptelefolia. ; _journal_issue 1 _journal_name_full 'Organic letters' _journal_page_first 146 _journal_page_last 149 _journal_paper_doi 10.1021/ol5033738 _journal_volume 17 _journal_year 2015 _chemical_absolute_configuration ad _chemical_formula_sum 'C19 H26 O7' _chemical_formula_weight 366.40 _chemical_name_systematic ; ? ; _space_group_crystal_system trigonal _space_group_IT_number 145 _space_group_name_Hall 'P 32' _space_group_name_H-M_alt 'P 32' _symmetry_space_group_name_Hall 'P 32' _symmetry_space_group_name_H-M 'P 32' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 3 _cell_length_a 9.26830(10) _cell_length_b 9.26830(10) _cell_length_c 18.5901(3) _cell_measurement_reflns_used 8336 _cell_measurement_temperature 291(2) _cell_measurement_theta_max 62.1871 _cell_measurement_theta_min 4.7535 _cell_volume 1382.97(3) _computing_cell_refinement 'CrysAlisPro (Agilent Technologies)' _computing_data_collection 'CrysAlisPro (Agilent Technologies)' _computing_data_reduction 'CrysAlisPro (Agilent Technologies)' _computing_molecular_graphics 'Ortep-3 (L. J. Farrugia, 2001)' _computing_publication_material SHELXL-2013 _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1997)' _diffrn_ambient_temperature 291(2) _diffrn_detector_area_resol_mean 15.9149 _diffrn_measured_fraction_theta_full 0.872 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device_type 'Gemini S Ultra, Agilent Technologies' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0155 _diffrn_reflns_av_unetI/netI 0.0126 _diffrn_reflns_Laue_measured_fraction_full 0.872 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 10427 _diffrn_reflns_point_group_measured_fraction_full 0.777 _diffrn_reflns_point_group_measured_fraction_max 0.879 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 62.278 _diffrn_reflns_theta_min 9.043 _diffrn_source 'Enhance Ultra (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.836 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.80731 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.36.21 (release 14-08-2012 CrysAlis171 .NET) (compiled Sep 14 2012,17:21:16) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.320 _exptl_crystal_description block _exptl_crystal_F_000 588 _exptl_crystal_size_max 0.410 _exptl_crystal_size_mid 0.360 _exptl_crystal_size_min 0.300 _refine_diff_density_max 0.126 _refine_diff_density_min -0.114 _refine_diff_density_rms 0.022 _refine_ls_abs_structure_details ; Flack x determined using 1117 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.03(5) _refine_ls_extinction_coef 0.0230(19) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.061 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 242 _refine_ls_number_reflns 2582 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.060 _refine_ls_R_factor_all 0.0241 _refine_ls_R_factor_gt 0.0240 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0395P)^2^+0.1328P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0643 _refine_ls_wR_factor_ref 0.0644 _reflns_Friedel_coverage 0.783 _reflns_Friedel_fraction_full 0.683 _reflns_Friedel_fraction_max 0.772 _reflns_number_gt 2573 _reflns_number_total 2582 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ol5033738_si_002.cif _cod_data_source_block shelxl _cod_depositor_comments 'Adding full bibliography for 1518464--1518465.cif.' _cod_original_cell_volume 1382.97(4) _cod_database_code 1518465 #BEGIN Tags that were not found in dictionaries: _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.726 _shelx_estimated_absorpt_t_max 0.788 _shelxl_version_number 2013-4 _shelx_res_file ; TITL mp-17a in P3(1) CELL 1.54184 9.2683 9.2683 18.5901 90.000 90.000 120.000 ZERR 3.00 0.0001 0.0001 0.0003 0.000 0.000 0.000 LATT -1 SYMM - Y, X - Y, 2/3 + Z SYMM - X + Y, - X, 1/3 + Z SFAC C H O UNIT 57 78 21 MERG 2 HTAB O1 O6 EQIV $1 x-1, y-1, z HTAB O7 O1_$1 FMAP 2 PLAN 25 SIZE 0.30 0.36 0.41 ACTA BOND $H CONF L.S. 4 WGHT 0.039500 0.132800 EXTI 0.022996 FVAR 17.70946 O3 3 0.667034 0.873051 0.088561 11.00000 0.03808 0.04967 = 0.04805 -0.00246 -0.00134 0.02569 O2 3 0.144114 0.835574 0.126475 11.00000 0.02999 0.03306 = 0.05728 0.00521 0.00153 0.01340 O5 3 0.789665 0.995443 0.216622 11.00000 0.03594 0.06891 = 0.05257 -0.00013 -0.01221 0.02141 O1 3 0.714002 1.231698 0.125700 11.00000 0.03471 0.03099 = 0.06643 0.00140 -0.01088 0.00661 AFIX 83 H1 2 0.713131 1.311433 0.107048 11.00000 -1.50000 AFIX 0 O7 3 0.030448 0.417282 0.197195 11.00000 0.04146 0.03542 = 0.07219 0.01441 -0.00445 0.00748 AFIX 83 H7 2 -0.070492 0.372300 0.190973 11.00000 -1.50000 AFIX 0 O6 3 0.502965 1.341739 0.087576 11.00000 0.05191 0.03168 = 0.11846 0.00747 -0.01260 0.01440 O4 3 0.546390 0.956617 0.257803 11.00000 0.04681 0.06545 = 0.04422 -0.00721 -0.00370 0.02267 C15 1 0.298554 0.642067 0.166696 11.00000 0.03667 0.03117 = 0.04923 -0.00016 -0.00724 0.01411 AFIX 23 H15A 2 0.335197 0.563156 0.155636 11.00000 -1.20000 H15B 2 0.323926 0.674568 0.216745 11.00000 -1.20000 AFIX 0 C3 1 0.307884 0.901183 0.119428 11.00000 0.03118 0.03136 = 0.03267 -0.00247 -0.00257 0.01433 C4 1 0.387689 0.794542 0.118386 11.00000 0.03058 0.02949 = 0.03869 -0.00324 -0.00416 0.01407 C2 1 0.416881 1.062130 0.105274 11.00000 0.03452 0.03302 = 0.03717 -0.00232 -0.00437 0.01568 C16 1 0.112158 0.562654 0.153724 11.00000 0.03631 0.03012 = 0.04488 0.00262 -0.00357 0.01044 AFIX 13 H16 2 0.088654 0.530365 0.103017 11.00000 -1.20000 AFIX 0 C6 1 0.632466 0.957998 0.209052 11.00000 0.03301 0.03132 = 0.04613 0.00264 -0.00537 0.01058 C5 1 0.575405 0.924264 0.132296 11.00000 0.03065 0.03336 = 0.04128 -0.00002 -0.00188 0.01512 C10 1 0.403226 0.747421 0.039347 11.00000 0.04542 0.04477 = 0.04328 -0.01092 -0.00569 0.02274 AFIX 23 H10A 2 0.379066 0.633007 0.036070 11.00000 -1.20000 H10B 2 0.328935 0.762631 0.007530 11.00000 -1.20000 AFIX 0 C8 1 0.386164 1.201569 0.099422 11.00000 0.04507 0.03392 = 0.04954 -0.00381 -0.00953 0.01885 C12 1 0.627371 1.052773 0.014892 11.00000 0.03820 0.05525 = 0.04363 0.00733 0.00509 0.02180 C1 1 0.587811 1.081928 0.094334 11.00000 0.02954 0.03180 = 0.04277 0.00231 -0.00327 0.01080 C17 1 0.050773 0.684983 0.171624 11.00000 0.03144 0.03210 = 0.04755 0.00269 0.00355 0.00809 C11 1 0.586150 0.870048 0.021436 11.00000 0.04382 0.06119 = 0.04054 -0.00631 0.00138 0.03003 AFIX 13 H11 2 0.627113 0.833873 -0.019409 11.00000 -1.20000 AFIX 0 C19 1 -0.127330 0.620714 0.148135 11.00000 0.03377 0.04412 = 0.07420 0.00328 0.00649 0.01466 AFIX 137 H19A 2 -0.140221 0.584625 0.098968 11.00000 -1.50000 H19B 2 -0.153876 0.708067 0.152432 11.00000 -1.50000 H19C 2 -0.200950 0.528651 0.178093 11.00000 -1.50000 AFIX 0 C9 1 0.214779 1.176212 0.107932 11.00000 0.05624 0.04577 = 0.07623 -0.00326 -0.00332 0.03256 AFIX 137 H9A 2 0.218098 1.280661 0.101732 11.00000 -1.50000 H9B 2 0.173579 1.133268 0.155114 11.00000 -1.50000 H9C 2 0.142487 1.098408 0.072420 11.00000 -1.50000 AFIX 0 C18 1 0.078105 0.739672 0.249335 11.00000 0.06236 0.05698 = 0.05422 -0.00608 0.00670 0.02500 AFIX 137 H18A 2 0.032783 0.811304 0.257924 11.00000 -1.50000 H18B 2 0.195336 0.798873 0.259562 11.00000 -1.50000 H18C 2 0.023572 0.643610 0.279928 11.00000 -1.50000 AFIX 0 C13 1 0.814458 1.162304 -0.001708 11.00000 0.04716 0.07413 = 0.07191 0.01812 0.02051 0.02692 AFIX 137 H13A 2 0.843214 1.277182 -0.003143 11.00000 -1.50000 H13B 2 0.838526 1.130961 -0.047436 11.00000 -1.50000 H13C 2 0.878244 1.147040 0.035109 11.00000 -1.50000 AFIX 0 C14 1 0.528306 1.081937 -0.042811 11.00000 0.06816 0.07868 = 0.04333 0.01101 0.00256 0.04159 AFIX 137 H14A 2 0.411335 1.011866 -0.033717 11.00000 -1.50000 H14B 2 0.554962 1.055777 -0.089144 11.00000 -1.50000 H14C 2 0.556115 1.196568 -0.041981 11.00000 -1.50000 AFIX 0 C7 1 0.857107 1.044016 0.288186 11.00000 0.05302 0.09066 = 0.05581 0.00182 -0.02228 0.02500 AFIX 137 H7A 2 0.794314 0.953796 0.320921 11.00000 -1.50000 H7B 2 0.850437 1.139790 0.302915 11.00000 -1.50000 H7C 2 0.971440 1.070780 0.288337 11.00000 -1.50000 AFIX 0 HKLF 4 REM mp-17a in P3(1) REM R1 = 0.0240 for 2573 Fo > 4sig(Fo) and 0.0241 for all 2582 data REM 242 parameters refined using 1 restraints END WGHT 0.0395 0.1344 REM Highest difference peak 0.126, deepest hole -0.114, 1-sigma level 0.022 Q1 1 0.5951 1.0147 0.1139 11.00000 0.05 0.13 Q2 1 0.4778 0.8654 0.1282 11.00000 0.05 0.12 Q3 1 -0.0602 0.3371 0.1629 11.00000 0.05 0.11 Q4 1 0.4996 1.0774 0.0969 11.00000 0.05 0.11 Q5 1 0.6076 1.0719 0.0542 11.00000 0.05 0.10 Q6 1 0.0811 0.6263 0.1648 11.00000 0.05 0.09 Q7 1 0.3743 1.0086 0.1417 11.00000 0.05 0.09 Q8 1 0.3631 0.9969 0.0873 11.00000 0.05 0.09 Q9 1 0.1979 0.5970 0.1553 11.00000 0.05 0.08 Q10 1 0.6653 1.2967 0.1351 11.00000 0.05 0.08 Q11 1 0.3455 0.8361 0.1161 11.00000 0.05 0.08 Q12 1 0.3789 0.7648 0.0803 11.00000 0.05 0.07 Q13 1 0.0684 0.5854 0.1157 11.00000 0.05 0.07 Q14 1 0.0859 0.9121 0.1489 11.00000 0.05 0.07 Q15 1 0.5956 0.9458 0.1676 11.00000 0.05 0.07 Q16 1 0.5965 0.9649 0.0149 11.00000 0.05 0.07 Q17 1 0.9808 0.9826 0.2649 11.00000 0.05 0.07 Q18 1 0.1841 0.8960 0.1650 11.00000 0.05 0.06 Q19 1 0.7019 1.1057 0.0059 11.00000 0.05 0.06 Q20 1 0.4236 0.6125 0.0587 11.00000 0.05 0.06 Q21 1 0.6791 1.3037 0.1906 11.00000 0.05 0.06 Q22 1 0.4993 0.6379 0.1103 11.00000 0.05 0.06 Q23 1 0.7626 1.0012 0.3261 11.00000 0.05 0.06 Q24 1 0.3034 0.8415 0.2139 11.00000 0.05 0.06 Q25 1 0.5042 1.4396 0.0344 11.00000 0.05 0.06 ; _shelx_res_checksum 73432 _shelx_hkl_file ; 0 0 2 25.5134 15.4543 9 0 0 2 69.9154 20.2489 7 0 0 2 78.2792 38.0159 5 0 0 4 78.6169 32.2733 7 0 0 4 27.9121 17.4668 5 0 0 4 55.0494 29.7079 8 0 0 5 30.9234 29.5942 5 0 0 5 30.5110 16.6503 7 0 0 7 96.9672 43.6368 5 0 0 7 140.699 61.0908 9 0 0 7 70.2649 48.5938 7 0 0 8 676.287 147.603 5 0 0 8 434.494 120.156 9 0 0 8 858.375 159.964 7 0 0 9 658440. 4535.81 8 0 0 9 664686. 4828.64 9 0 0 9 654489. 4740.51 5 0 0 9 661887. 4630.10 7 0 0 10-22.2901 62.2504 5 0 0 10 98.8369 76.4645 9 0 0 11 195.401 91.5469 8 0 0 12 351907. 3977.02 8 0 0 12 361183. 2998.56 32 0 0 12 360711. 2809.17 17 0 0 12 360789. 2981.71 19 0 0 13 191.445 82.7500 19 0 0 13 162.589 74.8364 17 0 0 14 201.479 114.155 8 0 0 14 325.874 100.915 32 0 0 14 180.923 67.8369 17 0 0 14 41.0772 41.1459 19 0 0 15 22963.9 880.304 19 0 0 15 22062.3 805.019 17 0 0 15 22539.9 863.888 32 0 0 16 33.8270 52.5343 32 0 0 16 37.8595 10.8363 17 0 0 17 104.071 30.4045 32 0 0 17-51.4936 23.8529 17 0 0 17 109.371 80.6104 19 0 0 18 1638.30 225.701 13 0 0 18 1552.83 229.037 32 0 0 19 25.9673 16.0580 32 0 0 20 369.302 98.1908 32 0 0 21 15231.7 583.565 32 -1 0 -18 1473.83 223.261 25 0 1 -17 5860.93 439.172 25 0 1 -16 112254. 1913.52 25 0 1 -6 367065. 1907.81 22 1 -1 3 37664.5 563.659 23 0 1 3 39638.7 535.492 7 0 1 3 39257.9 488.009 8 -1 0 3 37230.5 663.005 8 0 1 3 40466.9 510.193 22 -1 0 3 37724.5 677.824 6 0 1 4 262549. 1655.50 7 0 1 4 264685. 1558.37 8 -1 0 4 247715. 1915.56 8 -1 0 4 250701. 1942.38 6 1 -1 4 241285. 1571.80 23 0 1 4 262709. 1229.23 22 1 -1 4 249941. 1990.35 8 0 1 5 66579.0 962.920 7 0 1 5 69348.5 927.696 8 1 -1 5 67184.1 1137.70 8 0 1 6 104666. 1506.88 5 0 1 6 98912.6 1248.77 8 -1 0 6 101083. 1540.96 1 0 1 6 107634. 1367.51 7 0 1 6 103325. 1543.70 9 1 -1 6 102350. 1491.71 9 1 -1 6 102706. 1487.96 5 -1 0 6 102210. 1478.54 8 1 -1 6 102612. 1536.90 8 0 1 7 576962. 3886.68 5 0 1 7 603287. 3412.22 8 1 -1 7 572421. 3927.61 7 1 -1 7 577865. 3859.07 5 0 1 7 595487. 3558.75 7 1 -1 7 580144. 3933.19 8 1 -1 7 579700. 3867.98 9 -1 0 7 568051. 3759.07 8 0 1 7 580070. 3976.96 9 1 -1 8 861085. 5131.94 8 1 -1 8 854013. 5130.00 7 1 -1 8 865142. 5101.00 9 0 1 8 830632. 5032.74 5 1 -1 8 866971. 5083.45 5 0 1 8 842843. 5194.82 9 -1 0 8 827919. 4897.36 8 1 -1 9 173032. 2453.72 8 1 -1 9 170198. 2445.26 7 1 -1 9 164851. 2384.51 5 1 -1 9 171596. 2447.32 9 -1 0 9 170428. 2399.57 8 0 1 9 165566. 2466.75 9 0 1 9 174568. 2168.45 8 0 1 9 165291. 2390.79 5 1 -1 10 135094. 2326.55 9 -1 0 10 130703. 2253.81 8 0 1 10 133091. 2370.37 9 0 1 10 129299. 2278.47 5 1 -1 10 129801. 2279.13 8 1 -1 10 133284. 2328.47 7 0 1 10 139079. 2070.84 8 1 -1 10 132834. 2284.21 5 -1 0 11 377970. 2850.63 19 1 -1 11 374115. 4138.00 7 0 1 11 377402. 3660.80 8 0 1 11 371058. 4218.71 9 0 1 11 387917. 2944.63 19 1 -1 11 376339. 4132.15 5 1 -1 11 376278. 4138.08 9 1 -1 11 378526. 4143.43 8 0 1 11 372627. 4128.07 5 -1 0 11 379913. 2965.50 32 -1 0 11 368294. 4001.32 8 -1 0 12 7343.32 436.674 32 1 -1 12 5887.77 546.205 7 1 -1 12 6670.20 399.976 17 1 -1 12 6705.56 401.887 32 1 -1 12 6574.92 399.327 19 0 1 12 5878.23 539.817 5 -1 0 12 6553.70 402.950 19 0 1 12 6433.63 395.581 32 1 -1 12 6734.84 411.417 14 0 1 12 6367.91 494.759 8 0 1 12 5880.35 558.785 9 -1 0 12 6831.91 568.932 8 0 1 12 6818.52 411.583 14 -1 0 12 6610.65 390.531 17 1 -1 12 6187.22 554.738 9 0 1 12 6676.47 414.077 19 1 -1 12 6030.45 545.115 8 1 -1 12 6558.92 577.407 5 -1 0 12 6059.19 348.498 31 1 -1 13 76302.5 2049.58 8 -1 0 13 80913.8 2065.43 8 0 1 13 78338.4 1496.41 19 1 -1 13 77103.8 1458.63 19 0 1 13 79708.7 1478.09 32 1 -1 13 77899.5 1456.83 17 1 -1 13 79699.6 1483.20 32 -1 0 13 78101.9 1461.03 19 -1 0 13 77796.6 1507.83 32 -1 0 13 75424.9 1315.89 31 -1 0 13 79046.4 1443.55 17 0 1 14 2226.59 262.633 19 1 -1 14 1925.75 232.870 17 -1 0 14 2034.49 239.416 17 1 -1 14 1687.88 224.906 19 0 1 14 2410.28 269.895 32 1 -1 14 1961.88 241.923 32 -1 0 14 2119.87 258.877 32 -1 0 14 2581.88 280.897 19 -1 0 14 2028.65 222.107 31 0 1 15 10853.1 612.155 19 -1 0 15 11517.9 596.161 17 1 -1 15 11360.2 610.963 32 1 -1 15 11478.9 609.167 19 1 -1 15 11408.1 602.582 17 -1 0 15 10920.2 613.515 32 -1 0 15 11727.0 620.882 13 0 1 15 11110.0 601.036 32 -1 0 16 12358.3 671.484 32 1 -1 16 12915.4 668.732 32 0 1 16 13152.4 692.117 19 1 -1 16 12881.9 660.244 19 0 1 16 12586.0 656.484 32 -1 0 16 12681.4 643.131 17 1 -1 16 12824.4 649.667 17 -1 0 16 12364.6 648.955 13 -1 0 17 5582.26 433.363 12 -1 0 17 5425.31 442.408 32 0 1 17 5009.35 380.771 13 0 1 17 5190.15 421.987 32 -1 0 17 5668.61 437.911 13 0 1 17 4946.46 396.189 31 1 -1 17 5635.69 440.287 19 1 -1 17 5606.04 430.611 32 0 1 17 5499.86 446.068 19 -1 0 17 5611.97 427.941 11 1 -1 17 5194.66 413.340 17 0 1 18 188.973 90.3033 19 1 -1 18 151.318 80.3018 32 -1 0 18 131.732 56.3911 32 -1 0 18 120.621 69.1391 11 1 -1 18 187.938 76.3144 17 0 1 18 328.448 103.656 32 -1 0 18 301.046 82.9670 12 0 1 18 144.654 70.3185 31 1 -1 18 190.897 64.7083 19 -1 0 18 182.838 90.0944 13 -1 0 19 13111.9 650.561 32 1 -1 19 13238.1 624.227 17 1 -1 19 13280.3 627.887 32 0 1 19 13118.0 629.661 32 0 1 20 5646.55 382.755 32 1 -1 20 5780.12 381.513 32 -1 0 20 6006.33 412.156 32 -1 0 21 6368.56 381.542 32 -1 1 -18 151.155 67.5603 25 -1 1 -17 5348.08 436.270 25 -1 1 -16 12391.0 665.652 25 0 -1 3 562687. 2536.62 8 0 -1 3 554856. 2448.62 1 1 0 3 556996. 2563.42 23 1 0 6 353854. 2615.86 8 0 -1 6 344840. 2763.61 8 0 -1 6 344744. 2764.41 7 -1 1 6 344394. 2532.47 8 -1 1 7 60199.7 1149.24 8 1 0 7 58500.5 1190.09 7 0 -1 7 58627.8 1248.76 8 1 0 7 61756.6 1191.74 8 1 0 8 505824. 3793.77 7 0 -1 8 507917. 3937.88 7 -1 1 8 516750. 3659.69 8 0 -1 8 505775. 3958.11 8 1 0 8 496079. 4024.08 5 1 0 8 518857. 3726.83 8 1 0 8 510007. 4149.50 9 0 -1 9 217870. 2774.29 7 -1 1 9 218391. 2551.92 8 1 0 9 216926. 2651.66 7 1 0 9 216826. 2874.61 9 0 -1 9 216943. 2764.82 8 1 0 9 214644. 2577.42 8 1 0 9 210719. 2798.70 5 1 0 10 85066.7 1920.80 9 1 0 10 88073.5 1918.77 5 1 0 10 88619.5 1826.55 7 0 -1 10 88323.3 1875.06 8 1 0 10 88253.3 1768.33 8 -1 1 10 90795.3 1760.60 8 1 0 11 16773.6 817.352 8 1 0 11 16611.2 882.345 5 1 0 11 20309.6 682.391 14 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13 554.976 176.037 8 -1 1 14 178976. 2358.49 19 -1 1 14 176028. 2357.73 32 0 -1 14 178631. 2408.32 32 -1 1 14 181802. 2170.82 17 -1 1 14 182799. 2277.62 31 0 -1 14 180756. 2345.35 17 1 0 14 181422. 2308.42 32 1 0 14 179737. 2421.17 19 0 -1 14 179632. 2303.68 19 1 0 14 183470. 2188.70 17 0 -1 15 12394.8 624.364 19 -1 1 15 12724.2 621.321 13 -1 1 15 12735.7 654.566 32 0 -1 15 12836.1 648.133 17 0 -1 15 13417.4 684.316 32 1 0 15 12980.4 636.166 32 1 0 15 13421.4 682.076 19 1 0 15 13539.5 612.977 17 -1 1 15 12580.9 646.463 19 -1 1 15 12492.4 611.105 31 0 -1 16 116270. 1970.27 19 1 0 16 117227. 1833.28 17 -1 1 16 113782. 2023.25 19 -1 1 16 116201. 1904.30 13 1 0 16 116866. 1958.50 32 0 -1 16 115906. 2000.06 17 -1 1 16 116751. 1906.58 31 -1 1 16 114261. 2031.12 32 0 -1 16 114727. 2041.16 32 1 0 16 113091. 2039.43 19 -1 1 17 5968.98 427.005 31 -1 1 17 6319.31 438.546 13 0 -1 17 5797.42 444.785 17 0 -1 17 6171.28 470.808 32 1 0 17 6147.16 478.929 19 1 0 17 6492.86 461.570 32 -1 1 17 5977.70 463.776 32 -1 1 18 1470.71 206.788 12 1 0 18 1520.64 237.283 19 0 -1 18 1765.90 243.947 13 0 -1 18 1652.49 220.203 11 -1 1 18 1465.30 216.427 32 1 0 18 1315.24 192.584 32 -1 1 18 1707.98 237.405 11 -1 1 18 1628.28 217.917 13 0 -1 18 1683.92 242.197 32 0 -1 18 1591.80 234.989 17 0 -1 18 1664.62 228.945 12 -1 1 18 1620.21 211.578 31 1 0 19 620.476 133.535 19 0 -1 19 559.768 121.076 32 -1 1 19 623.447 130.363 32 1 0 19 654.334 137.716 32 1 0 20 2506.93 245.548 32 -1 1 20 2362.78 253.851 32 0 -1 20 2703.60 273.030 32 -1 1 21 13518.2 553.731 32 0 -1 21 13890.0 560.551 32 -2 1 -17 79724.6 1727.82 25 -2 1 -16 9617.73 594.792 25 1 1 -7 117519. 1426.36 22 1 1 -6 29186.3 712.098 22 1 1 -5 35947.1 775.086 22 1 1 -5 36754.0 469.331 23 1 1 -4 368898. 1385.02 23 1 1 -4 365298. 2407.93 22 1 1 -3 95303.1 690.390 23 1 1 -3 91590.7 1177.03 22 1 1 -2 325358. 2157.83 22 1 1 -2 342427. 1426.05 23 1 1 -1 57310.9 883.823 22 1 -2 -1 57558.0 948.504 24 1 1 1 199718. 1578.65 22 -2 1 1 199648. 1594.54 3 1 -2 1 198035. 1673.61 24 1 1 1 200846. 1524.33 23 1 1 2 553661. 2551.67 22 1 1 2 543300. 2745.77 23 -2 1 2 523906. 2908.50 4 -2 1 2 533002. 2892.63 2 -2 1 2 545953. 2678.54 3 1 -2 3 111220. 936.284 9 1 1 3 108695. 1109.97 22 1 -2 3 107749. 988.283 5 -2 1 3 105532. 1344.99 2 1 -2 3 106397. 1266.13 8 -2 1 3 106850. 1296.82 6 -2 1 3 106879. 1342.30 4 1 -2 3 111411. 820.116 23 -2 1 4 792.442 120.269 6 1 -2 4 1468.18 163.926 8 -2 1 4 909.900 134.238 1 1 -2 4 635.646 63.1625 23 1 1 4 1186.73 111.515 8 1 -2 4 981.285 104.262 9 1 1 5 171363. 1492.49 8 -2 1 5 163012. 1896.12 6 1 1 5 167133. 1244.92 22 -2 1 5 171188. 1312.58 13 -2 1 5 162998. 1898.14 1 1 -2 5 161143. 1628.03 5 1 -2 5 162235. 1572.26 9 1 -2 5 161364. 1893.89 8 -2 1 5 168308. 1350.56 10 -2 1 5 167066. 1905.24 8 1 1 6 99410.8 1272.63 8 -2 1 6 97239.0 1066.19 13 1 1 6 100956. 1330.15 7 -2 1 6 92484.8 1554.06 1 1 -2 6 93814.2 1556.27 8 1 -2 6 96562.2 1556.53 7 1 -2 6 94184.0 1388.73 5 -2 1 6 99412.0 1554.55 8 1 -2 6 94379.7 1349.18 9 1 1 6 98916.5 860.250 22 1 1 7 448921. 3080.88 7 1 -2 7 432275. 3617.80 8 1 -2 7 428541. 3544.90 7 1 -2 7 431795. 3186.98 9 -2 1 7 432439. 3592.61 1 1 1 7 454521. 2941.15 8 -2 1 7 446898. 3509.54 8 -2 1 7 445806. 2458.89 13 1 -2 7 434966. 3269.94 5 1 -2 8 943.605 159.205 5 1 -2 8 1037.25 181.832 7 1 -2 8 1271.62 208.243 8 1 -2 8 1212.93 178.255 9 -2 1 8 1082.16 183.882 8 1 1 8 1449.49 181.903 8 -2 1 8 1177.21 133.539 13 1 1 9 4984.54 378.231 7 -2 1 9 5373.35 306.400 13 1 1 9 4618.72 423.429 5 1 -2 9 4264.41 369.536 9 -2 1 9 4997.40 416.470 8 1 1 9 4502.14 425.272 9 1 1 9 5155.38 368.321 8 1 -2 9 5182.98 445.463 7 1 -2 9 4662.88 421.240 8 1 1 10 144761. 2543.55 5 -2 1 10 145616. 1723.96 13 1 1 10 142226. 2578.07 9 1 -2 10 150125. 2581.65 8 1 1 10 154280. 2277.11 7 1 1 10 154414. 2177.82 8 1 -2 10 149844. 2568.31 7 -2 1 10 147140. 2409.37 8 -2 1 11 41354.9 982.836 32 1 1 11 40846.2 1000.59 14 1 1 11 41831.0 930.098 32 1 -2 11 41689.5 1002.85 17 1 -2 11 40695.1 1414.87 7 1 1 11 40524.4 1003.72 19 -2 1 11 41402.6 1356.32 8 1 -2 11 41452.9 995.385 32 -2 1 11 39468.2 948.709 13 -2 1 11 40688.4 937.640 31 1 -2 11 38602.4 1396.19 8 1 1 11 39198.0 1429.62 9 1 -2 11 41453.0 911.715 33 -2 1 11 40286.4 967.441 19 1 1 11 38128.0 1376.97 5 1 -2 12 121508. 2589.47 7 -2 1 12 117579. 1740.85 13 1 1 12 120089. 1815.11 14 1 1 12 118747. 2604.05 9 -2 1 12 121007. 2426.71 8 1 -2 12 119671. 2563.33 8 1 -2 12 121930. 1810.45 17 -2 1 12 120877. 1780.96 32 1 1 12 119145. 1817.35 19 -2 1 12 121507. 1716.84 31 1 1 12 114593. 2494.44 5 1 -2 12 117771. 1631.41 34 1 -2 12 121545. 1671.55 19 1 1 12 122731. 1703.28 32 1 -2 12 123026. 1823.94 32 -2 1 13 123324. 1812.55 31 1 1 13 120884. 1931.50 19 -2 1 13 123455. 2569.17 8 1 -2 13 122532. 1761.37 19 1 1 13 124458. 2739.43 5 -2 1 13 121397. 1886.74 32 1 1 13 122141. 2777.18 9 -2 1 13 119220. 1823.11 13 1 -2 13 121291. 1912.29 32 1 -2 13 121948. 1916.71 17 1 1 13 122840. 1942.20 14 1 1 13 123227. 1793.73 32 1 -2 13 127229. 2750.43 8 -2 1 14 29740.2 945.044 13 1 1 14 29664.2 1004.17 14 1 1 14 29944.8 1005.10 19 -2 1 14 29760.0 920.128 31 -2 1 14 28729.9 942.953 11 1 -2 14 30377.3 921.579 19 1 -2 14 29531.5 988.751 17 -2 1 14 28979.1 965.382 32 1 1 14 29985.6 925.738 32 1 -2 14 30325.3 997.025 32 1 1 15 9834.60 544.219 32 -2 1 15 10134.8 586.193 32 -2 1 15 9645.53 533.426 31 -2 1 15 9215.89 537.914 12 1 1 15 9767.90 590.117 19 -2 1 15 10118.2 566.109 13 -2 1 15 9439.36 556.630 11 1 -2 15 9766.90 583.992 32 1 -2 15 9424.36 575.836 17 1 -2 15 10035.0 545.495 19 -2 1 16 61301.8 1428.97 12 1 -2 16 61450.3 1379.35 19 1 -2 16 61639.3 1502.27 17 -2 1 16 60109.7 1473.11 32 -2 1 16 61219.7 1436.74 11 -2 1 16 62416.2 1431.13 13 1 -2 16 61056.2 1479.62 32 1 1 16 62919.6 1406.71 32 1 1 16 60064.7 1503.13 19 -2 1 16 61768.0 1379.45 31 -2 1 17 50469.7 1283.56 13 -2 1 17 48119.5 1270.27 11 1 -2 17 48877.7 1338.10 17 1 -2 17 48391.8 1311.09 32 1 1 17 49229.9 1244.66 32 -2 1 17 47537.6 1307.17 32 -2 1 17 50934.2 1298.92 12 -2 1 17 47572.8 1194.09 31 1 1 17 48427.4 1341.50 19 -2 1 18 6971.88 482.640 32 1 -2 18 6517.65 472.881 17 1 1 18 7004.60 498.146 19 -2 1 18 7718.70 461.017 31 1 1 18 7736.20 480.017 32 1 -2 18 7151.50 487.975 32 -2 1 19 13175.7 642.286 32 1 -2 19 13349.2 632.576 32 1 1 19 13208.3 656.226 19 1 -2 19 12740.5 631.987 17 1 1 19 13257.6 592.468 32 1 1 19 12214.6 568.720 31 -2 1 20 4095.80 332.603 32 1 -2 20 3886.32 313.635 32 -3 1 -17 5226.29 438.632 25 -3 1 -16 9469.26 598.975 25 -3 1 -15 39156.2 1203.48 25 -3 1 -14 62881.0 1496.46 25 1 2 -7 4937.34 359.341 22 1 2 -6 167520. 2080.16 22 -3 1 -5 141854. 1318.84 25 1 2 -5 142329. 1883.55 22 1 2 -4 17552.2 647.799 22 -3 1 -4 14793.8 392.147 25 2 -3 -3 178454. 2158.70 24 1 2 -3 179585. 2040.40 22 1 2 -2 846888. 4342.96 22 2 -3 -2 824120. 4521.89 24 1 2 -1 107990. 1530.65 22 2 -3 -1 110291. 1596.76 24 1 2 0 369878. 2777.43 22 2 -3 0 368852. 2859.63 24 1 2 1 165811. 1839.62 22 2 -3 1 166734. 1908.84 24 -3 1 2 253358. 2411.24 3 -3 1 2 256328. 2479.12 2 -3 1 2 257987. 2523.94 4 1 2 2 252900. 2241.03 22 2 -3 2 254490. 1131.24 5 2 -3 2 249721. 1024.19 9 2 -3 3 602681. 2260.65 5 -3 1 3 562929. 3766.48 2 2 -3 3 588737. 2859.63 23 -3 1 3 571030. 3657.14 3 -3 1 3 567640. 3796.17 4 1 2 3 570456. 3287.43 22 -3 1 4 170872. 2111.65 6 2 -3 4 179885. 1467.00 5 2 -3 4 179644. 1397.30 9 2 -3 4 172776. 1533.21 23 -3 1 4 169134. 2153.05 2 -3 1 4 173126. 1417.50 11 1 2 4 176574. 1814.30 22 -3 1 4 176982. 1405.43 12 -3 1 4 174181. 1508.88 10 -3 1 4 171985. 2196.76 4 -3 1 5 268480. 1832.32 12 1 2 5 265273. 2222.60 22 2 -3 5 272745. 2070.27 5 2 -3 5 271554. 2750.54 8 -3 1 5 266190. 1989.82 10 2 -3 5 270152. 1982.22 9 -3 1 5 270535. 1853.17 11 -3 1 5 271684. 1914.10 13 2 -3 5 270167. 1907.98 23 -3 1 6 11405.1 606.108 8 -3 1 6 11172.7 430.736 10 2 -3 6 11405.2 453.146 9 -3 1 6 11162.4 595.368 6 -3 1 6 12764.0 427.722 11 2 -3 6 11714.5 611.512 8 2 -3 6 11422.1 478.859 5 -3 1 6 12063.9 407.666 12 1 2 6 12112.5 450.249 22 -3 1 6 11414.2 418.200 13 -3 1 6 11412.6 613.326 1 -3 1 7 121977. 1380.16 12 -3 1 7 119135. 2069.33 6 -3 1 7 121309. 1425.49 13 -3 1 7 122658. 2080.72 8 2 -3 7 117359. 2059.10 8 2 -3 7 123630. 1653.58 9 -3 1 7 118555. 2097.51 1 2 -3 7 120800. 1716.54 5 -3 1 7 120291. 1397.35 11 2 -3 8 31623.1 1131.30 8 -3 1 8 31561.0 769.885 13 -3 1 8 31629.9 1123.61 1 2 -3 8 32207.7 920.463 9 2 -3 8 31954.6 1122.04 7 -3 1 8 31737.6 759.132 11 2 -3 8 31744.4 945.848 5 -3 1 8 31318.6 745.554 12 -3 1 8 31520.4 1118.09 8 2 -3 9 103656. 1775.82 9 -3 1 9 100125. 1429.13 11 2 -3 9 100210. 2119.67 8 -3 1 9 101554. 1438.02 12 -3 1 9 100446. 1457.43 13 2 -3 9 103238. 1828.05 5 2 -3 9 100532. 2113.52 7 1 2 9 99046.4 2095.92 9 -3 1 9 102532. 2108.76 8 -3 1 10 5229.84 330.132 32 2 -3 10 5136.71 350.760 34 2 -3 10 5297.77 355.007 20 2 -3 10 5069.20 508.327 8 2 -3 10 5149.39 338.893 32 2 -3 10 5260.48 357.387 17 1 2 10 4894.29 478.971 5 -3 1 10 5448.98 340.897 31 1 2 10 5126.42 504.175 9 2 -3 10 5808.24 533.748 7 -3 1 10 6741.38 387.989 12 -3 1 10 5463.04 356.057 15 1 2 10 5208.28 338.388 14 -3 1 10 5036.21 345.593 13 -3 1 10 5247.41 499.735 8 -3 1 10 4882.46 331.379 11 1 2 10 5560.66 354.347 19 2 -3 11 137038. 1949.55 17 -3 1 11 138425. 1824.55 32 -3 1 11 136334. 1885.03 13 2 -3 11 140139. 1962.43 20 -3 1 11 138493. 1900.38 15 1 2 11 143028. 1926.57 19 -3 1 11 135911. 1856.43 11 -3 1 11 140848. 1836.45 31 1 2 11 136838. 2654.03 5 2 -3 11 139317. 1925.91 34 1 2 11 133652. 2686.72 9 2 -3 11 137307. 2739.99 7 -3 1 11 135429. 1849.25 12 -3 1 11 145179. 2757.00 8 1 2 11 140620. 1890.03 14 1 2 11 138678. 1781.54 32 2 -3 11 141755. 1896.60 32 2 -3 11 139300. 2765.41 8 -3 1 12 32585.2 959.667 13 -3 1 12 32560.0 950.629 11 1 2 12 32787.0 1390.24 9 2 -3 12 33530.4 1428.94 8 1 2 12 33762.3 984.129 19 2 -3 12 33575.2 973.755 32 1 2 12 37816.3 970.090 32 1 2 12 33063.0 970.965 14 -3 1 12 32867.1 928.124 31 2 -3 12 33702.5 1012.45 17 -3 1 12 33316.3 946.577 32 2 -3 12 32738.0 1000.96 20 2 -3 12 34907.9 1446.88 7 1 2 12 30928.1 1313.57 5 -3 1 12 34063.0 965.752 12 -3 1 12 33402.2 1367.21 8 2 -3 12 32578.8 968.132 34 -3 1 13 19791.3 755.178 12 -3 1 13 19028.7 755.455 11 1 2 13 20471.4 747.050 32 -3 1 13 19176.5 766.563 13 -3 1 13 19246.5 738.583 31 -3 1 13 19262.9 753.748 32 1 2 13 19534.6 782.886 19 2 -3 13 19516.0 768.066 34 2 -3 13 18490.6 789.318 17 1 2 13 19430.1 773.150 14 2 -3 13 20629.6 795.618 32 1 2 14 54272.3 1262.38 32 1 2 14 53209.0 1341.79 19 2 -3 14 53732.1 1386.28 17 -3 1 14 53188.0 1300.15 11 -3 1 14 53255.8 1326.02 13 -3 1 14 54246.7 1266.91 31 -3 1 14 53982.0 1311.86 32 2 -3 14 54386.9 1179.84 19 2 -3 14 54961.6 1346.73 32 -3 1 14 54662.0 1309.19 12 1 2 14 56077.3 1359.82 14 -3 1 15 32670.6 1032.48 12 -3 1 15 33569.5 1051.87 11 -3 1 15 32832.0 1056.87 32 2 -3 15 34523.5 957.776 19 -3 1 15 33700.5 1013.22 31 2 -3 15 33386.9 1122.98 17 1 2 15 34526.4 1021.41 32 -3 1 15 33313.4 1067.13 13 2 -3 15 34940.0 1087.09 32 1 2 15 33422.9 1083.76 19 2 -3 16 35432.9 1164.55 17 1 2 16 37331.4 1018.57 28 -3 1 16 38788.6 1125.46 12 -3 1 16 37101.9 1126.79 13 -3 1 16 35070.2 1095.80 32 -3 1 16 37326.4 1120.24 11 2 -3 16 37145.2 1126.08 32 -3 1 16 36483.3 1057.75 31 1 2 16 35881.0 1132.20 19 -3 1 17 11506.1 604.229 12 2 -3 17 11209.6 600.083 32 -3 1 17 11660.6 609.624 11 2 -3 17 11080.7 638.388 17 -3 1 17 10465.5 593.361 32 -3 1 17 11059.3 559.668 31 -3 1 17 12241.9 627.198 13 1 2 17 11125.5 616.446 19 2 -3 18 2601.79 274.971 32 2 -3 18 2772.52 304.245 17 1 2 18 2681.63 293.776 19 -3 1 18 2782.28 292.387 32 2 -3 19 305.953 79.7866 32 2 -3 19 275.425 85.0455 17 -3 1 19 193.152 70.8520 32 1 2 19 121.326 31.1713 19 1 2 19 401.328 105.679 31 2 -3 20 2456.99 243.376 17 1 2 20 2371.94 228.523 31 -3 1 20 2323.34 230.359 32 0 2 -14 173516. 2226.39 25 0 2 -13 94290.0 1573.59 25 0 2 -12 3838.28 297.185 25 0 2 -11 28019.4 764.350 25 0 2 -10 23992.9 674.343 25 0 2 -9 59528.4 987.862 25 0 2 -8 40993.8 758.975 25 0 2 -7 114788. 1506.05 22 0 2 -7 108752. 1149.21 25 0 2 -6 175487. 1342.53 25 0 2 -6 182446. 1890.89 22 0 2 -5 242391. 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716.696 1 2 -4 8 11140.2 666.841 7 -4 2 8 11277.1 514.974 16 -4 2 8 10858.1 471.963 11 -4 2 8 11457.8 470.155 12 2 -4 8 11673.4 526.068 34 2 -4 8 10384.8 667.176 8 -4 2 8 11341.4 500.183 31 2 -4 9 28378.7 1128.24 7 2 -4 9 30293.0 825.874 20 2 -4 9 30812.2 848.986 17 2 2 9 30353.3 858.132 19 -4 2 9 28673.5 837.870 31 -4 2 9 29230.5 835.339 15 -4 2 9 28688.0 856.811 16 -4 2 9 28130.2 780.272 12 -4 2 9 29153.8 1186.40 1 2 -4 9 29577.4 868.083 34 -4 2 9 28188.6 804.630 11 -4 2 10 21504.5 776.209 16 2 2 10 21232.1 757.658 19 -4 2 10 24646.1 811.203 31 -4 2 10 20027.8 650.198 32 2 -4 10 21099.7 764.924 34 2 -4 10 21396.6 736.716 20 -4 2 10 20770.2 712.117 11 2 -4 10 21173.6 1055.97 8 -4 2 10 21696.2 747.021 15 2 -4 10 20859.6 1023.86 7 2 -4 10 20298.5 735.346 17 2 -4 10 20906.3 761.399 32 -4 2 10 21687.7 712.077 12 2 -4 11 49997.6 1228.55 32 2 2 11 48820.8 1202.29 19 2 -4 11 49528.1 1704.58 8 -4 2 11 49138.4 1184.11 31 -4 2 11 48327.2 1174.66 15 -4 2 11 49721.0 1086.73 32 2 2 11 50149.9 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13386.4 795.181 22 -5 2 -8 14025.6 594.062 25 3 -5 -8 14971.9 942.077 24 2 3 -7 1596.26 269.580 22 -5 2 -7 1335.65 174.368 25 3 -5 -7 724.563 189.909 24 -5 2 -7 884.328 140.578 29 -5 2 -6 34049.9 833.165 25 3 -5 -6 32561.7 1310.62 24 2 3 -6 34952.7 1247.09 22 3 -5 -5 115893. 2407.98 24 -5 2 -5 119309. 1502.22 25 2 3 -5 120413. 2292.55 22 3 -5 -4 217592. 3220.34 24 2 3 -4 215492. 3057.73 22 3 -5 -3 37531.2 1300.19 24 2 3 -3 37484.5 1254.05 22 3 -5 -2 122205. 2264.47 24 2 3 -2 121606. 2230.16 22 2 3 -1 22379.9 941.646 22 3 -5 -1 23266.3 974.511 24 3 -5 0 187644. 2759.87 24 -5 2 0 190212. 2744.94 3 2 3 0 189826. 2709.45 22 3 -5 0 194443. 2418.87 23 3 -5 1 71243.0 1402.86 23 2 3 1 70260.7 1630.72 22 -5 2 1 67577.3 1751.76 4 -5 2 1 68199.2 1632.58 3 -5 2 2 92858.6 2068.10 4 -5 2 2 97329.1 1935.51 3 -5 2 2 95284.7 2060.31 2 2 3 2 93883.5 1862.71 22 2 3 3 127495. 2157.22 22 -5 2 3 123164. 2372.01 4 -5 2 3 127457. 2405.09 2 3 -5 3 131679. 1972.11 8 -5 2 3 132800. 2279.75 3 -5 2 4 12196.3 508.743 10 -5 2 4 12000.8 758.285 4 -5 2 4 12404.4 767.141 2 2 3 4 12125.2 659.681 22 -5 2 4 11488.9 702.454 6 3 -5 4 11316.8 609.209 8 3 -5 5 110418. 1997.82 8 -5 2 5 110940. 1589.95 31 2 3 5 109277. 1959.31 22 -5 2 5 109625. 1585.36 10 -5 2 5 112208. 1648.15 16 3 -5 5 114148. 1654.13 34 -5 2 5 110636. 2240.86 6 -5 2 6 272102. 2496.48 15 -5 2 6 270950. 2420.45 18 -5 2 6 264837. 2533.23 31 -5 2 6 269022. 3593.47 6 -5 2 6 263056. 2547.71 10 3 -5 6 264156. 3284.26 8 -5 2 6 269808. 3637.54 1 3 -5 6 271233. 2651.02 34 -5 2 6 264431. 2623.66 16 -5 2 7 23765.7 778.271 31 3 -5 7 22696.6 707.802 17 -5 2 7 22545.9 764.763 10 3 -5 7 24904.4 1023.87 7 3 -5 7 23602.0 1028.51 8 -5 2 7 24443.0 1127.33 1 -5 2 7 23577.9 1097.45 6 -5 2 7 24133.6 776.469 15 -5 2 7 23149.8 796.294 16 3 -5 7 23206.6 690.752 20 -5 2 7 24609.8 753.617 18 3 -5 7 23095.1 800.807 34 3 -5 8 102041. 2227.89 8 3 -5 8 103705. 1549.89 20 3 -5 8 104371. 1593.63 17 2 3 8 101581. 1538.08 19 -5 2 8 100695. 1733.91 16 -5 2 8 107335. 2426.24 1 -5 2 8 104253. 1653.88 15 3 -5 8 103685. 2176.70 7 -5 2 8 105325. 1691.64 31 3 -5 8 103441. 1754.48 34 2 3 9 135919. 1857.28 19 3 -5 9 135563. 1910.59 17 3 -5 9 134174. 2667.56 8 -5 2 9 135301. 1960.66 15 -5 2 9 133107. 1970.99 31 3 -5 9 132916. 1850.03 20 3 -5 9 131537. 2576.65 7 3 -5 9 133282. 2059.39 34 -5 2 9 132349. 2053.89 16 -5 2 9 137425. 2809.83 1 3 -5 10 30593.5 928.808 20 3 -5 10 29126.8 993.206 34 2 3 10 30342.9 916.322 19 3 -5 10 30124.1 941.726 17 -5 2 10 29358.2 955.110 31 3 -5 10 29972.7 950.752 32 -5 2 10 28970.5 985.209 16 -5 2 10 29845.6 957.946 15 2 3 11 55890.5 1260.47 14 -5 2 11 55303.7 1345.87 31 2 3 11 56689.4 1281.51 19 3 -5 11 55551.8 1326.68 17 -5 2 11 55232.7 1342.05 15 3 -5 11 56145.4 1307.01 20 3 -5 11 56957.3 1344.86 32 3 -5 11 56150.0 1413.57 34 3 -5 12 43755.4 1207.57 17 3 -5 12 45720.6 1221.16 32 -5 2 12 43387.5 1207.22 31 3 -5 12 43896.3 1273.23 34 -5 2 12 43996.8 1230.74 15 2 3 12 44762.7 1163.50 14 2 3 12 46068.2 1190.50 19 3 -5 13 36407.6 1168.51 34 3 -5 13 38189.7 1126.06 32 3 -5 13 36358.1 1127.03 17 2 3 13 37452.5 1073.24 14 2 3 13 36692.4 1074.76 19 -5 2 13 36807.5 1119.35 31 3 -5 14 604.379 149.560 34 2 3 14 464.796 112.612 19 2 3 14 746.615 160.150 28 -5 2 14 642.634 152.852 31 3 -5 14 933.803 184.364 17 3 -5 14 645.214 141.123 32 2 3 14 754.878 156.164 14 -5 2 14 634.560 141.477 37 -5 2 15 62792.0 1437.80 31 2 3 15 61847.3 1376.10 19 2 3 15 59478.5 1387.04 28 2 3 15 63257.0 1371.14 14 3 -5 15 60393.3 1453.34 17 3 -5 15 64742.7 1424.17 32 3 -5 16 2646.76 295.473 17 2 3 16 2685.24 273.452 19 -5 2 16 2392.77 267.097 31 2 3 16 2304.29 262.440 28 2 3 17 4884.95 354.874 19 -5 2 17 5050.16 364.915 31 2 3 17 4461.79 341.532 28 3 -5 17 4737.96 374.218 17 -5 2 18 4281.20 305.837 31 2 3 18 4290.47 303.694 19 2 3 18 4622.41 313.552 28 3 -5 18 4988.75 360.832 17 -4 1 -16 46451.8 1282.49 25 -4 1 -15 4588.23 404.407 25 -4 1 -14 9965.48 593.262 25 -4 1 -13 23332.3 887.751 25 -4 1 -12 14269.7 668.314 25 -4 1 -11 44076.9 1127.81 25 -4 1 -10 55322.7 1201.17 25 -4 1 -9 53598.2 1127.27 25 3 -4 -8 140388. 2606.31 24 -4 1 -8 136669. 1685.82 25 3 -4 -7 788.361 180.423 24 -4 1 -7 405.113 81.7412 25 3 -4 -6 84904.3 1882.93 24 1 3 -6 84455.2 1770.43 22 -4 1 -6 83241.0 1177.11 25 3 -4 -5 394258. 3936.23 24 1 3 -5 400337. 3751.16 22 -4 1 -5 389054. 2349.14 25 3 -4 -4 22352.6 908.873 24 -4 1 -4 22591.4 527.048 25 1 3 -4 23199.4 886.038 22 3 -4 -3 382882. 3652.18 24 1 3 -3 384968. 3556.49 22 3 -4 -2 946941. 5521.44 24 1 3 -2 962764. 5540.67 22 1 3 -1 16491.9 716.446 22 3 -4 -1 15767.5 695.166 24 1 3 0 731925. 4719.40 22 3 -4 0 741948. 4445.05 23 3 -4 0 748092. 4764.58 24 -4 1 1 499304. 4042.06 2 -4 1 1 497356. 4152.84 3 3 -4 1 509647. 3937.87 24 -4 1 1 504408. 4103.34 4 1 3 1 497384. 3865.56 22 1 3 2 85817.7 1583.65 22 3 -4 2 87969.7 1448.37 23 -4 1 2 88483.5 1698.74 2 -4 1 2 84923.2 1702.48 3 -4 1 2 84380.4 1700.66 4 -4 1 3 307038. 3251.47 3 -4 1 3 311344. 3240.70 2 3 -4 3 323361. 2703.25 23 -4 1 3 300776. 3228.20 4 1 3 3 316490. 3037.09 22 -4 1 4 451128. 4168.21 4 1 3 4 458627. 3628.24 22 -4 1 4 461641. 4108.60 2 -4 1 4 455361. 4041.61 3 -4 1 5 1200.11 212.283 6 1 3 5 1445.42 200.933 22 3 -4 5 1391.39 223.428 8 3 -4 6 39283.3 1238.34 8 -4 1 6 39240.8 1287.12 6 -4 1 6 38313.1 919.260 10 -4 1 6 38910.8 1302.97 1 -4 1 7 71518.4 1806.01 6 -4 1 7 71586.5 1847.56 1 -4 1 7 69834.3 1295.91 10 3 -4 7 71455.5 1762.63 8 3 -4 8 195209. 2217.86 34 3 -4 8 195634. 3065.70 8 3 -4 8 198375. 2126.07 17 -4 1 8 191064. 3096.00 6 -4 1 8 192313. 2052.98 12 3 -4 8 198630. 2111.40 20 -4 1 8 190731. 2063.35 11 -4 1 8 195821. 2173.85 16 -4 1 8 192200. 2111.84 15 -4 1 8 197051. 2080.80 31 -4 1 8 187741. 3096.95 1 1 3 9 1051.11 149.194 19 -4 1 9 1071.30 221.160 1 1 3 9 952.936 210.426 9 -4 1 9 744.550 133.707 12 3 -4 9 842.088 146.509 17 -4 1 9 861.865 144.704 31 1 3 9 598.793 162.201 5 3 -4 9 1054.51 231.353 7 -4 1 9 928.721 151.382 11 3 -4 9 693.324 125.407 34 -4 1 9 879.351 146.881 15 -4 1 9 928.136 158.345 16 3 -4 9 1069.90 162.902 20 -4 1 10 208790. 3526.81 1 1 3 10 199033. 3158.78 9 -4 1 10 207253. 2407.52 15 3 -4 10 211725. 2451.30 17 -4 1 10 212146. 2427.30 13 3 -4 10 207854. 3392.26 7 3 -4 10 210450. 3448.12 8 3 -4 10 210551. 2519.84 34 -4 1 10 207365. 2356.43 11 1 3 10 207124. 2225.08 19 -4 1 10 206226. 2334.58 12 3 -4 10 210213. 2433.15 20 -4 1 10 211021. 2330.19 31 1 3 10 205799. 3118.93 5 1 3 11 73899.7 1999.38 9 1 3 11 75881.3 1410.62 19 -4 1 11 71254.3 1484.94 15 -4 1 11 72871.0 1445.11 11 1 3 11 74108.7 1372.78 14 3 -4 11 71810.0 2075.94 7 3 -4 11 74629.2 1553.89 34 -4 1 11 73585.7 1484.55 13 -4 1 11 74176.8 1448.34 12 3 -4 11 75135.1 2142.59 8 3 -4 11 73467.8 1509.34 17 -4 1 11 74489.7 1435.39 31 3 -4 11 71760.8 1494.98 20 -4 1 11 75758.4 1351.35 32 1 3 12 43171.2 1107.60 19 3 -4 12 40641.8 1165.98 20 -4 1 12 42346.0 1161.95 13 -4 1 12 42730.2 1139.58 11 3 -4 12 41336.2 1181.69 17 -4 1 12 41774.1 1122.67 12 -4 1 12 42264.5 1110.49 31 -4 1 12 41606.7 1160.63 15 -4 1 12 42280.1 1062.08 32 3 -4 12 42552.7 1202.84 34 1 3 12 42648.9 1081.02 14 -4 1 13 59226.7 1370.80 12 -4 1 13 56619.0 1270.79 37 -4 1 13 55103.0 1224.91 33 -4 1 13 57198.0 1316.47 31 1 3 13 58029.5 1301.35 14 -4 1 13 56482.6 1273.61 32 3 -4 13 56205.3 1413.16 34 1 3 13 56182.2 1298.45 19 3 -4 13 54929.1 1407.63 17 3 -4 13 57185.5 1433.00 20 -4 1 13 56857.5 1354.68 11 3 -4 14 10837.8 639.896 17 -4 1 14 10321.8 588.338 11 1 3 14 9765.93 555.059 28 1 3 14 10162.5 552.197 14 1 3 14 10369.4 567.839 19 -4 1 14 10429.2 566.586 31 -4 1 14 10610.9 585.270 12 3 -4 14 10188.4 603.838 34 -4 1 14 10147.4 550.564 32 -4 1 15 965.810 172.816 31 -4 1 15 1154.03 195.721 12 3 -4 15 967.543 194.650 17 1 3 15 1382.27 207.379 19 -4 1 15 1072.00 188.373 11 1 3 15 1017.57 183.408 28 -4 1 15 983.981 179.803 32 1 3 16 22242.3 812.470 28 3 -4 16 22202.3 907.019 17 -4 1 16 24295.6 881.361 12 -4 1 16 22232.5 798.101 31 1 3 16 22868.3 839.088 19 -4 1 16 21421.9 811.089 32 -4 1 17 3237.42 290.171 31 3 -4 17 3670.64 355.072 17 -4 1 17 3321.03 308.957 32 1 3 17 3239.80 293.600 28 1 3 17 3671.62 325.754 19 3 -4 18 4878.89 390.948 17 -4 1 18 5092.14 361.865 32 1 3 18 5048.55 359.302 19 1 3 19 2571.67 257.537 31 3 -4 19 2751.13 266.243 17 -4 1 19 2602.64 235.325 32 1 3 19 2777.89 243.347 19 -3 0 -16 19077.9 835.038 25 0 3 -7 22988.0 831.882 22 0 3 -6 519309. 3927.13 22 0 3 -5 34546.0 630.786 25 0 3 -5 35251.4 1014.49 22 3 -3 -5 36054.5 1021.42 24 3 -3 -4 244169. 2567.51 24 0 3 -4 241676. 2608.55 22 3 -3 -3 900372. 4724.15 24 0 3 -3 931509. 5074.80 22 3 -3 -2 132387. 1745.76 24 0 3 -2 135539. 1901.98 22 3 -3 -1 29387.8 788.053 24 0 3 -1 29518.1 879.535 22 3 -3 -1 27980.4 831.920 23 3 -3 0 64321.9 1168.85 24 0 3 0 63486.4 1276.47 22 3 -3 0 63991.6 1220.10 23 -3 0 0 63874.3 1202.91 4 0 3 1 3048.36 271.612 22 -3 0 1 4268.28 317.016 4 3 -3 1 3059.10 260.146 23 -3 0 1 4348.71 308.895 2 0 3 2 173955. 2062.06 22 -3 0 2 171076. 2042.07 4 -3 0 2 176963. 2007.08 2 3 -3 2 175785. 1959.56 23 -3 0 2 169176. 2210.53 3 0 3 3 80462.4 1397.61 22 -3 0 3 78534.9 1513.36 3 3 -3 3 78748.1 1311.24 23 -3 0 3 81598.0 1474.33 4 -3 0 3 78891.9 1410.43 2 3 -3 4 1368.64 172.487 23 0 3 4 1264.30 173.466 22 -3 0 5 248068. 1877.74 13 -3 0 5 251469. 1915.65 12 0 3 5 254177. 2475.47 22 -3 0 5 247476. 2085.93 10 3 -3 5 247538. 2406.42 23 -3 0 5 242088. 2817.34 6 -3 0 6 151581. 1553.28 11 -3 0 6 147774. 1694.29 10 3 -3 6 152608. 1926.64 23 -3 0 6 152959. 1572.24 12 0 3 6 155036. 1887.30 22 -3 0 6 149822. 2307.52 8 -3 0 6 152990. 1565.80 13 -3 0 6 147203. 2294.74 6 0 3 6 153743. 2030.52 9 -3 0 6 148009. 2396.51 1 -3 0 7 286962. 2464.66 10 0 3 7 297553. 3036.13 9 3 -3 7 303918. 2915.48 5 3 -3 7 292205. 2721.32 23 -3 0 7 292915. 3405.78 6 -3 0 7 288901. 2285.20 12 -3 0 7 300723. 3440.08 8 -3 0 7 287575. 3481.03 1 -3 0 7 291995. 2296.62 13 0 3 7 301724. 2931.37 5 -3 0 7 295454. 2281.96 11 3 -3 7 292148. 3454.12 8 -3 0 8 109568. 1486.76 13 -3 0 8 108036. 1460.90 12 -3 0 8 107941. 1451.81 11 -3 0 8 105286. 2216.14 1 0 3 8 110070. 1965.97 9 0 3 8 111069. 1901.01 5 3 -3 8 108506. 2213.08 8 -3 0 8 109504. 2172.91 8 3 -3 8 109776. 1852.91 9 3 -3 8 112910. 1906.66 5 -3 0 9 16553.8 611.357 13 3 -3 9 15543.6 882.432 8 -3 0 9 16252.5 600.394 15 -3 0 9 15284.6 580.560 12 -3 0 9 14688.2 852.027 1 -3 0 9 15745.5 576.008 11 0 3 9 16885.9 817.306 9 3 -3 9 15807.3 755.385 5 3 -3 9 16791.5 637.977 34 0 3 9 16382.5 771.290 5 -3 0 9 16287.1 879.460 8 3 -3 9 16604.5 626.314 17 3 -3 9 16284.6 751.949 9 3 -3 9 17995.8 653.645 20 0 3 9 16874.7 598.502 32 -3 0 10 19377.6 633.479 31 0 3 10 18036.9 897.197 9 0 3 10 22248.8 947.813 5 -3 0 10 18953.8 683.205 13 3 -3 10 19861.7 733.030 34 -3 0 10 19665.1 1008.27 8 -3 0 10 18506.2 668.223 12 3 -3 10 19564.1 721.647 17 3 -3 10 19397.8 1040.40 8 3 -3 10 19194.6 863.615 9 3 -3 10 19140.8 713.848 20 -3 0 10 19510.1 671.793 11 -3 0 10 19130.2 654.803 32 3 -3 10 19253.3 624.515 14 -3 0 10 18994.6 682.482 15 0 3 10 20124.9 682.796 32 3 -3 10 19483.1 878.978 5 3 -3 10 18792.5 1012.31 7 0 3 10 18911.8 629.794 19 -3 0 11 80442.0 1492.43 15 3 -3 11 80542.9 1906.09 5 -3 0 11 79546.9 1480.02 13 3 -3 11 80311.2 1533.50 17 -3 0 11 79109.6 1457.74 12 -3 0 11 83813.5 2192.48 8 -3 0 11 82172.6 1365.60 31 -3 0 11 80206.0 1441.77 11 0 3 11 83691.1 1466.10 32 3 -3 11 83795.2 1569.73 34 0 3 11 79471.3 1913.08 5 3 -3 11 82713.7 1386.16 14 0 3 11 78889.2 1987.86 9 3 -3 11 85018.8 2256.49 8 3 -3 11 81098.9 1564.51 20 0 3 11 81482.5 1390.67 19 -3 0 11 83056.8 1403.40 37 -3 0 11 82627.6 1457.81 32 3 -3 11 82799.7 2202.96 7 3 -3 12 10072.3 571.376 20 -3 0 12 9536.21 536.449 13 3 -3 12 9939.45 562.285 34 -3 0 12 9956.76 533.561 12 3 -3 12 9836.45 564.883 17 -3 0 12 10036.9 544.788 15 3 -3 12 9778.77 499.712 14 -3 0 12 9547.66 513.756 11 -3 0 12 9823.73 502.426 33 -3 0 12 10196.3 499.121 37 0 3 12 10036.7 512.266 19 0 3 12 9364.35 703.448 9 3 -3 12 9204.77 663.865 5 0 3 12 9832.84 512.012 28 -3 0 12 9539.99 481.243 31 0 3 12 9751.28 522.997 32 -3 0 12 9778.94 525.675 32 0 3 12 9277.47 480.164 14 3 -3 12 9317.86 470.633 19 3 -3 13 4336.20 383.036 17 -3 0 13 4165.86 363.879 13 0 3 13 4336.84 344.708 28 -3 0 13 4087.20 346.205 11 -3 0 13 4626.53 350.793 33 -3 0 13 4454.86 334.563 31 3 -3 13 4423.59 332.531 19 3 -3 13 3856.32 367.871 20 0 3 13 4119.13 355.061 32 -3 0 13 3942.44 351.050 12 0 3 13 4081.51 341.245 19 -3 0 13 4301.26 362.362 32 0 3 14 58861.2 1303.14 28 -3 0 14 57510.5 1258.73 33 -3 0 14 59352.7 1378.35 11 0 3 14 58755.3 1337.35 19 -3 0 14 58633.8 1387.98 12 -3 0 14 58115.6 1408.96 13 3 -3 14 59942.9 1270.38 19 3 -3 14 57196.6 1461.11 17 -3 0 14 58454.7 1392.33 32 -3 0 15 48238.6 1251.96 11 3 -3 15 45645.0 1312.69 17 -3 0 15 46141.1 1272.71 13 0 3 15 46535.0 1158.28 28 -3 0 15 45984.4 1235.50 12 3 -3 15 46540.2 1136.63 19 -3 0 15 43856.0 1221.48 32 0 3 15 45582.3 1200.81 19 -3 0 16 17932.2 759.158 11 -3 0 16 18850.6 797.004 12 -3 0 16 17772.7 782.933 13 3 -3 16 17766.7 690.652 19 3 -3 16 16735.8 794.783 17 0 3 16 17328.8 692.268 28 -3 0 16 16843.6 757.515 32 0 3 16 16843.4 731.020 19 -3 0 17 18862.5 791.854 32 0 3 17 19396.8 767.528 19 3 -3 17 19914.7 846.200 17 0 3 18 833.599 153.702 31 3 -3 18 880.094 163.481 17 0 3 18 755.513 138.278 19 -3 0 18 881.044 159.696 32 0 3 19 6031.94 411.851 31 -3 0 19 5967.81 401.688 32 3 -3 19 6008.38 409.671 17 0 3 20 7299.64 404.157 31 3 -3 20 6789.78 394.220 17 -3 0 20 7103.62 393.905 32 -1 3 -15 9914.18 566.848 25 -1 3 -14 10311.9 565.173 25 -1 3 -13 78219.2 1520.42 25 -1 3 -12 87248.3 1549.17 25 -1 3 -11 14473.1 598.648 25 -1 3 -10 27355.9 785.967 25 -1 3 -9 9784.60 441.290 25 -1 3 -8 368833. 2545.75 25 -1 3 -7 75593.3 1093.84 25 -1 3 -7 75338.7 1403.34 22 -1 3 -6 4187.23 245.033 25 -1 3 -6 5557.82 377.109 22 -1 3 -5 131131. 1316.45 25 -1 3 -5 136082. 1872.01 22 -1 3 -4 24288.9 774.252 22 -1 3 -4 24127.9 540.305 25 -1 3 -3 173758. 1413.55 25 -1 3 -3 178097. 2073.86 22 3 -2 -3 173065. 2066.58 23 3 -2 -3 179508. 1673.70 24 3 -2 -2 633692. 2983.88 24 3 -2 -2 636693. 3836.33 23 -1 3 -1 219070. 2264.61 22 3 -2 -1 226666. 1691.40 24 3 -2 -1 217746. 2200.01 23 -2 -1 -1 227403. 1768.99 4 -1 3 0 1399.00 176.183 22 3 -2 0 1385.56 119.967 26 -2 -1 0 1353.59 128.442 2 -2 -1 0 1380.87 138.007 4 -2 -1 0 1392.60 106.479 24 3 -2 1 206656. 1497.78 26 -1 3 1 193491. 2101.09 22 -2 -1 1 201808. 1672.68 2 -2 -1 1 201710. 1798.98 4 -1 3 1 206316. 1153.71 2 3 -2 1 196074. 2034.44 23 -1 3 2 651640. 3819.44 22 3 -2 2 648534. 3717.59 23 -1 3 2 651331. 2640.49 25 -2 -1 2 640902. 3830.31 3 -1 3 3 453905. 2003.73 5 3 -2 3 469657. 2391.97 26 -1 3 3 434957. 3107.61 22 -2 -1 3 421112. 3170.15 3 -1 3 3 459574. 2245.11 9 -2 -1 3 427532. 2992.67 8 3 -2 3 423286. 3037.63 23 -2 -1 4 60803.8 899.727 10 -1 3 4 61301.8 866.682 5 -2 -1 4 58074.5 1180.85 8 -1 3 4 59551.7 947.487 9 3 -2 4 60761.4 877.362 26 -2 -1 4 58694.2 814.937 12 -2 -1 4 60036.5 1208.30 6 -2 -1 4 58541.8 770.440 13 -1 3 4 58566.4 1141.98 22 3 -2 4 57874.0 1158.15 23 -2 -1 5 100097. 1641.98 6 -1 3 5 100472. 1279.28 5 -2 -1 5 99613.7 1724.61 1 3 -2 5 104621. 1611.58 23 -2 -1 5 101703. 1237.23 10 -2 -1 5 100563. 1136.54 12 3 -2 5 102564. 1167.65 26 -2 -1 5 101324. 1096.32 11 -2 -1 5 100050. 1661.09 8 -1 3 5 103190. 1391.91 9 -2 -1 5 99332.3 1080.28 13 -2 -1 6 1335.48 131.380 13 3 -2 6 908.084 155.227 23 -2 -1 6 1171.37 137.855 10 -2 -1 6 1076.65 122.042 12 -2 -1 6 1146.40 184.581 8 -2 -1 6 950.949 179.164 1 3 -2 6 1301.46 135.336 26 -1 3 6 1157.73 159.628 9 -2 -1 6 1002.78 115.772 11 -1 3 6 1274.79 160.626 5 -2 -1 6 1102.89 181.612 6 -1 3 7 53397.0 1146.10 5 -2 -1 7 50474.3 1319.14 8 -2 -1 7 50676.7 1370.63 1 -2 -1 7 51760.7 873.390 11 -2 -1 7 54239.2 927.580 13 3 -2 7 51307.8 1222.43 23 -1 3 7 51787.7 1193.95 9 -2 -1 7 50586.1 898.507 12 -2 -1 8 162597. 1695.65 12 3 -2 8 157081. 2591.89 8 -2 -1 8 163767. 2502.71 8 -2 -1 8 159211. 1638.33 11 -2 -1 8 160084. 1698.71 13 3 -2 8 159060. 2263.54 23 -1 3 8 167373. 2197.30 5 -1 3 8 161876. 2293.61 9 -2 -1 8 156912. 2513.39 1 -2 -1 9 108553. 1480.25 12 -2 -1 9 107981. 2149.22 8 3 -2 9 109205. 2108.56 5 -2 -1 9 108444. 1498.43 13 3 -2 9 108007. 2247.61 8 -1 3 9 111732. 2036.41 9 -2 -1 9 106834. 1417.34 11 -1 3 9 112654. 1924.41 5 3 -2 10 46842.2 1022.93 14 -2 -1 10 45357.8 1477.57 8 -2 -1 10 45967.1 1042.17 17 3 -2 10 46957.2 1084.63 20 -1 3 10 45834.4 962.922 28 -2 -1 10 45753.8 1012.20 12 3 -2 10 46616.9 1065.46 17 3 -2 10 44628.4 1431.86 9 -2 -1 10 46201.5 994.873 33 -2 -1 10 45727.2 1008.43 15 -2 -1 10 44107.6 1017.19 13 -2 -1 10 44293.0 962.816 11 3 -2 10 44883.9 1521.76 8 3 -2 10 44950.5 996.344 19 3 -2 10 46992.0 1083.21 34 -2 -1 10 45150.1 1037.15 32 3 -2 10 43723.1 1413.44 5 -1 3 10 45914.4 1029.34 32 3 -2 11 115117. 1772.47 17 -2 -1 11 116514. 1741.26 13 -1 3 11 112067. 1577.74 28 3 -2 11 110321. 2494.74 8 3 -2 11 110291. 2353.09 5 -2 -1 11 114837. 1690.27 12 3 -2 11 111668. 1770.66 20 -2 -1 11 112663. 1618.08 11 -2 -1 11 112353. 1639.26 33 -2 -1 11 112387. 1652.43 15 3 -2 11 112376. 1672.12 19 -2 -1 11 115196. 2489.37 8 3 -2 11 112404. 2385.26 9 -1 3 11 110261. 1690.76 32 -2 -1 11 110302. 1494.27 37 3 -2 11 115974. 1712.46 14 3 -2 11 109599. 2497.71 7 -1 3 11 111830. 1578.82 19 -2 -1 11 114900. 1748.66 32 -2 -1 11 111494. 1708.89 17 3 -2 12 49093.2 1722.66 7 -2 -1 12 49586.6 1705.24 8 3 -2 12 47327.9 1159.07 14 3 -2 12 46416.1 1583.62 9 3 -2 12 45684.7 1568.48 5 -2 -1 12 47117.5 1177.17 17 -1 3 12 47954.0 1092.03 19 -2 -1 12 47734.0 1102.07 33 3 -2 12 48507.7 1198.05 17 -2 -1 12 47625.0 1138.51 12 3 -2 12 48691.2 1225.31 20 3 -2 12 47989.9 1686.78 8 -2 -1 12 49697.2 1126.81 11 -2 -1 12 46592.3 1173.47 32 -1 3 12 47885.2 1154.82 32 3 -2 12 46918.2 1130.62 19 -1 3 12 47333.5 1057.52 28 -2 -1 12 46908.0 1159.79 13 -2 -1 13 22720.9 839.605 13 -1 3 13 23555.5 772.106 28 -2 -1 13 23328.8 825.743 12 -2 -1 13 23343.7 796.625 33 -2 -1 13 23355.2 873.406 32 -2 -1 13 24333.2 818.139 11 3 -2 13 22589.1 819.698 19 -1 3 13 23377.6 846.612 32 -1 3 13 24259.6 814.968 19 3 -2 13 23158.4 865.302 17 3 -2 13 22466.5 867.590 20 3 -2 13 22255.3 830.052 14 3 -2 14 10353.2 565.950 19 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6255.42 435.761 17 3 -2 18 6703.67 441.716 19 -1 3 19 2059.97 246.119 31 -2 -1 19 2295.95 262.027 32 3 -2 19 2284.43 238.617 19 3 -2 19 2250.33 243.762 17 -2 -1 20 16002.4 635.358 32 -1 3 20 15278.1 600.720 31 -2 3 -17 11196.0 621.361 25 -2 3 -16 36772.9 1150.12 25 -2 3 -15 33929.2 1099.85 25 -2 3 -14 55389.6 1375.96 25 -2 3 -13 19283.1 786.958 25 -2 3 -12 34370.7 1001.71 25 -2 3 -11 139692. 1933.35 25 -2 3 -10 5337.48 356.982 25 -2 3 -9 100206. 1475.49 25 3 -1 -8 32640.3 981.181 23 -2 3 -8 30821.7 772.542 25 -2 3 -7 119730. 1454.63 25 3 -1 -7 119792. 1805.70 23 -2 3 -6 11619.7 427.530 25 3 -1 -6 11842.4 545.466 23 3 -1 -5 272567. 2543.52 23 -2 3 -5 270401. 1980.94 25 -2 3 -4 177401. 1542.82 25 3 -1 -4 172705. 1987.15 23 -2 3 -3 578457. 2729.10 25 3 -1 -3 581151. 3560.04 23 3 -1 -2 255684. 2327.29 23 -2 3 -2 266551. 1805.73 25 -2 3 -1 176124. 1424.50 25 -1 -2 -1 172262. 1739.54 24 -2 3 0 380921. 2041.67 25 -1 -2 0 380536. 2484.98 24 3 -1 0 374654. 2789.01 23 -1 -2 1 112297. 1365.05 3 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305080. 3314.83 2 -4 3 3 324342. 2834.71 6 1 -4 3 313083. 2410.53 8 -4 3 4 25537.6 965.061 2 -4 3 4 23406.5 907.226 4 1 -4 4 27124.9 787.287 8 -4 3 4 25898.3 812.957 1 3 1 4 24679.4 918.324 23 1 -4 4 26204.5 707.310 7 3 1 4 25498.5 831.290 22 -4 3 4 25936.1 839.110 6 1 -4 5 70981.3 1297.05 7 -4 3 5 74830.0 1451.72 1 3 1 5 73525.1 1385.68 22 1 -4 5 70431.9 1387.22 8 -4 3 5 70400.8 1659.69 2 -4 3 5 74064.2 1494.78 6 -4 3 5 70737.7 997.614 10 -4 3 5 70309.0 1616.02 4 -4 3 6 244618. 1932.86 11 1 -4 6 245280. 2630.98 7 -4 3 6 249556. 2793.03 1 1 -4 6 241385. 2766.74 8 1 -4 7 396.673 117.660 7 -4 3 7 364.394 76.0579 12 1 -4 7 356.826 116.278 8 -4 3 7 341.144 69.5300 11 -4 3 7 278.510 102.613 1 1 -4 8 241342. 2345.21 34 3 1 8 235732. 2434.97 19 -4 3 8 236401. 2337.16 31 1 -4 8 231647. 3075.13 8 1 -4 8 236128. 2958.62 7 -4 3 8 232460. 1994.85 12 -4 3 8 236712. 2323.78 16 -4 3 8 229594. 2088.74 11 1 -4 8 238450. 2284.53 33 3 1 9 85715.4 1548.79 19 -4 3 9 87123.4 1391.47 15 1 -4 9 85326.5 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14 12936.6 642.031 31 2 4 14 12342.8 633.342 28 4 -6 14 12721.3 678.068 34 -6 2 14 12492.3 620.963 37 4 -6 14 12914.1 641.350 17 2 4 15 28396.4 915.818 28 -6 2 15 28499.6 883.294 37 4 -6 15 27173.2 898.180 17 -6 2 15 28696.2 909.291 31 -6 2 16 1340.95 183.301 31 4 -6 16 1319.68 183.010 17 2 4 16 1038.71 163.112 28 2 4 17 7200.46 393.639 28 4 -6 17 7639.88 415.627 17 -5 1 -14 3001.24 310.139 25 -5 1 -13 26122.1 921.183 25 -5 1 -12 12949.9 632.569 25 -5 1 -11 32374.8 971.577 25 -5 1 -10 42755.0 1072.94 25 4 -5 -9 15042.2 930.302 24 4 -5 -8 153237. 2911.40 24 1 4 -7 53788.5 1638.79 22 4 -5 -7 55206.3 1700.41 24 1 4 -6 150031. 2696.60 22 4 -5 -6 148737. 2718.84 24 4 -5 -5 268192. 3547.42 24 1 4 -5 261958. 3565.44 22 4 -5 -4 66218.6 1702.71 24 1 4 -4 68979.4 1789.76 22 1 4 -3 3160.21 380.489 22 4 -5 -3 3263.82 363.770 24 4 -5 -2 201016. 2853.63 24 1 4 -2 197411. 2959.71 22 4 -5 -2 197462. 2847.06 23 1 4 -1 261047. 3384.14 22 4 -5 -1 260471. 3203.44 24 4 -5 -1 257723. 3162.41 23 1 4 0 10880.3 682.443 22 4 -5 0 10395.6 618.730 23 -5 1 0 10198.6 669.898 4 -5 1 0 11228.8 683.605 2 -5 1 1 30909.0 1203.51 3 1 4 1 33599.0 1189.65 22 -5 1 1 30204.6 1152.49 4 4 -5 1 31317.7 1042.22 23 -5 1 1 31369.6 1142.58 2 -5 1 2 99287.6 2159.41 3 -5 1 2 96871.5 2057.64 4 -5 1 2 104267. 2090.98 2 4 -5 2 103460. 1840.48 23 1 4 2 98534.2 2016.44 22 -5 1 3 40631.1 1365.78 4 -5 1 3 40352.7 1334.98 2 1 4 3 41002.6 1293.38 22 -5 1 3 41085.9 1399.51 3 1 4 4 94678.9 1941.01 22 -5 1 4 92538.8 1565.21 10 -5 1 4 94821.3 2162.50 3 -5 1 4 98341.0 1489.92 31 -5 1 4 97188.9 1525.31 15 -5 1 5 78614.3 1389.03 18 4 -5 5 78209.5 1831.75 8 1 4 5 79133.7 1274.76 28 -5 1 5 72875.5 1416.68 10 -5 1 5 78753.1 1371.47 16 -5 1 5 79126.2 1372.43 31 4 -5 5 81523.0 1426.83 34 1 4 5 78584.6 1755.10 22 -5 1 5 78427.2 1397.34 15 -5 1 5 76098.1 1985.53 6 -5 1 6 18604.3 679.112 31 4 -5 6 18501.6 705.150 34 -5 1 6 18611.2 697.219 15 -5 1 6 19922.9 1061.72 1 -5 1 6 18817.9 737.780 10 4 -5 6 19264.5 662.175 17 -5 1 6 19279.5 1016.10 6 -5 1 6 19801.0 708.410 16 -5 1 6 18736.2 694.731 18 1 4 6 19646.1 659.187 28 4 -5 6 17772.4 910.631 8 -5 1 7 40105.6 1117.73 10 -5 1 7 40389.7 1062.36 15 -5 1 7 42720.0 1570.53 6 4 -5 7 42650.3 1029.37 17 4 -5 7 41978.1 1463.61 8 -5 1 7 42202.5 1079.85 16 -5 1 7 43400.8 1052.10 31 -5 1 7 42765.9 1613.13 1 4 -5 7 40600.1 1097.16 34 -5 1 7 41771.4 1067.91 18 -5 1 8 107141. 1762.77 18 -5 1 8 112942. 2668.84 1 -5 1 8 110493. 1813.65 15 1 4 8 108494. 1680.40 28 4 -5 8 107196. 2428.67 8 -5 1 8 114601. 2636.24 6 -5 1 8 108526. 1792.76 16 4 -5 8 108473. 1851.03 34 -5 1 8 110101. 1721.93 31 4 -5 8 109079. 1706.79 20 -5 1 8 102854. 1834.62 10 4 -5 8 108981. 1714.69 17 1 4 9 21022.7 769.454 28 4 -5 9 20951.0 784.665 17 4 -5 9 20901.5 1108.56 8 -5 1 9 20877.8 811.018 16 4 -5 9 21032.5 837.588 34 -5 1 9 20377.7 804.792 15 4 -5 9 21229.9 787.043 20 -5 1 9 20421.9 760.329 31 1 4 10 70680.4 1460.73 28 4 -5 10 69564.4 1484.75 17 -5 1 10 71535.1 1547.75 16 -5 1 10 69187.2 1523.99 15 4 -5 10 71045.1 1591.14 34 -5 1 10 71249.6 1449.72 31 4 -5 10 69741.9 1479.14 20 -5 1 11 52056.0 1262.44 31 1 4 11 50492.8 1263.76 28 4 -5 11 49822.7 1299.97 17 4 -5 11 50204.8 1373.72 34 -5 1 11 49895.9 1287.58 37 -5 1 11 48812.4 1321.24 15 4 -5 11 50130.9 1293.99 20 -5 1 12 103711. 1813.31 31 4 -5 12 103945. 1909.19 20 1 4 12 100974. 1827.87 28 4 -5 12 100109. 1897.58 17 -5 1 12 101478. 1938.11 15 -5 1 12 102229. 1849.86 37 4 -5 12 101767. 1990.66 34 -5 1 13 36745.6 1080.88 31 1 4 13 36141.4 1105.14 28 4 -5 13 37238.8 1155.43 20 4 -5 13 37366.2 1170.91 17 -5 1 13 36489.3 1166.63 15 4 -5 13 36462.8 1197.91 34 -5 1 13 35571.1 1077.65 37 -5 1 14 18390.4 752.007 31 1 4 14 18165.3 770.775 28 -5 1 14 18461.7 747.285 37 4 -5 14 17976.0 810.475 17 -5 1 14 18885.9 747.634 33 1 4 15 39132.8 1114.44 28 -5 1 15 39229.0 1039.03 37 4 -5 15 38228.8 1170.17 17 -5 1 15 39584.2 1067.09 31 4 -5 16 13543.1 670.366 17 1 4 16 13576.8 622.765 28 -5 1 16 13864.8 593.958 31 4 -5 17 1575.27 215.110 17 1 4 17 1475.93 188.388 28 4 -5 18 12035.7 548.283 17 1 4 18 11607.3 479.932 28 -4 0 -15 8554.44 534.297 25 -4 0 -14 85.7727 20.7376 25 -4 0 -13 41487.2 1157.38 25 -4 0 -12 11712.5 600.524 25 -4 0 -11 7898.75 471.506 25 0 4 -7 23302.2 994.936 22 4 -4 -7 24012.4 1003.90 24 0 4 -6 338525. 3788.85 22 4 -4 -6 343083. 3702.37 24 4 -4 -5 49238.3 1332.92 24 0 4 -5 46378.8 1381.83 22 0 4 -4 147344. 2412.06 22 4 -4 -4 153946. 2271.70 24 4 -4 -3 443811. 4158.86 23 4 -4 -3 447831. 3731.39 24 4 -4 -2 413050. 3873.72 23 4 -4 -2 418737. 3548.12 24 0 4 -2 420955. 3987.81 22 4 -4 -1 298613. 3224.37 23 -4 0 -1 292275. 3038.23 4 4 -4 -1 300416. 2960.27 24 0 4 -1 297040. 3336.06 22 4 -4 0 323591. 3265.11 23 -4 0 0 326289. 3240.64 4 0 4 0 320890. 3422.43 22 -4 0 0 325883. 3122.80 2 -4 0 1 215838. 2974.73 3 4 -4 1 224055. 2682.72 23 -4 0 1 216327. 2636.23 4 0 4 1 217995. 2798.49 22 -4 0 1 219416. 2591.45 2 0 4 2 97418.2 1867.24 22 -4 0 2 97394.5 1810.58 4 4 -4 2 98657.2 1747.79 23 -4 0 2 99762.1 1768.25 2 -4 0 2 98617.6 2019.13 3 4 -4 3 191602. 2426.18 23 0 4 3 187619. 2573.31 22 -4 0 3 188680. 2794.60 3 -4 0 4 247804. 3252.38 3 4 -4 4 255072. 2802.13 23 0 4 4 254645. 2978.77 22 4 -4 5 4704.00 379.787 23 -4 0 5 4415.22 325.994 10 -4 0 5 4605.72 449.995 6 0 4 5 4241.74 384.905 22 -4 0 6 13495.1 795.065 6 -4 0 6 13360.5 591.422 10 -4 0 7 19390.8 628.457 31 -4 0 7 19201.4 679.625 18 -4 0 7 18144.4 959.144 6 4 -4 7 19227.4 699.731 34 0 4 7 19449.2 651.154 28 4 -4 7 19245.2 681.793 17 -4 0 7 20349.8 674.071 16 4 -4 7 19478.6 982.074 8 -4 0 7 18282.0 712.623 10 -4 0 7 18284.8 660.032 15 -4 0 7 18586.4 1002.31 1 -4 0 8 12681.4 524.091 31 -4 0 8 12002.9 828.187 1 -4 0 8 11996.4 554.444 15 -4 0 8 12062.5 559.642 18 0 4 8 12004.9 532.981 28 -4 0 8 13366.9 629.525 10 4 -4 8 12930.8 830.315 8 4 -4 8 11720.2 555.792 17 -4 0 8 11393.0 787.642 6 4 -4 8 12030.6 580.102 34 -4 0 8 12499.5 549.889 16 -4 0 9 7010.83 400.958 31 -4 0 9 6559.92 424.305 15 0 4 9 6714.39 413.832 28 4 -4 9 6893.43 446.592 17 4 -4 9 6854.62 620.739 8 -4 0 9 6627.40 425.061 37 4 -4 9 7052.05 459.564 34 -4 0 9 6658.02 643.850 1 4 -4 9 6015.90 416.499 20 -4 0 10 9083.12 768.936 1 4 -4 10 8878.59 544.946 34 4 -4 10 9503.58 771.862 8 4 -4 10 8981.69 530.267 17 -4 0 10 9777.33 538.277 15 -4 0 10 9457.69 521.984 37 0 4 10 9509.96 511.781 28 -4 0 10 9744.71 491.031 31 4 -4 10 8961.44 531.656 20 -4 0 11 26778.6 832.367 31 -4 0 11 26172.9 919.615 15 0 4 11 25757.0 872.220 28 4 -4 11 25793.6 931.539 17 -4 0 11 26142.1 885.608 37 4 -4 11 25134.2 926.155 20 4 -4 11 25264.5 947.182 34 -4 0 12 20994.4 745.930 31 -4 0 12 20479.0 782.503 37 0 4 12 20318.6 793.115 28 4 -4 12 19803.0 856.714 34 4 -4 12 19478.1 838.404 17 4 -4 12 20766.4 866.203 20 -4 0 12 20488.4 845.028 15 -4 0 12 21053.0 756.523 32 -4 0 13 5415.17 411.181 33 -4 0 13 5987.01 398.409 31 4 -4 13 5834.24 463.741 17 -4 0 13 6021.36 417.347 37 0 4 13 5963.69 436.923 28 -4 0 13 5628.63 442.968 15 4 -4 13 5668.03 463.661 20 -4 0 13 5968.74 415.803 32 -4 0 14 44400.0 1121.16 37 4 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312122. 3281.60 23 -1 4 -3 318883. 3368.77 22 4 -3 -2 249427. 2902.17 23 4 -3 -2 254400. 1922.82 26 -1 4 -2 247875. 1842.96 25 4 -3 -2 253672. 2281.72 24 -1 4 -2 255285. 2964.73 22 4 -3 -1 82510.1 1618.53 23 4 -3 -1 83350.3 1121.43 26 -1 4 -1 82017.5 1031.21 25 -3 -1 -1 86508.4 1368.11 4 -1 4 -1 82573.3 1673.40 22 -3 -1 -1 86494.3 1277.93 2 -3 -1 0 388745. 2725.77 2 -3 -1 0 386452. 2908.81 4 4 -3 0 379813. 2451.06 26 -1 4 0 367521. 2193.08 25 -1 4 0 374831. 3540.14 22 4 -3 0 369596. 3408.23 23 -3 -1 1 86511.3 1709.49 3 -3 -1 1 90006.9 1461.87 4 -3 -1 1 91810.4 1384.97 2 4 -3 1 87501.8 1198.78 26 -1 4 1 87857.7 1103.54 25 -1 4 1 87811.6 1706.17 22 4 -3 1 88201.2 1640.86 23 -3 -1 2 426897. 3811.90 3 4 -3 2 427427. 3580.54 23 4 -3 2 438426. 2727.37 26 -1 4 2 425599. 3703.41 22 4 -3 3 35919.6 798.435 26 4 -3 3 34611.9 1020.59 23 -1 4 3 34939.3 1055.09 22 -3 -1 3 34812.7 1094.50 3 -3 -1 4 15591.4 747.840 3 -1 4 4 21000.9 819.112 22 4 -3 4 15738.1 539.302 26 -3 -1 4 23948.3 674.904 10 4 -3 4 14625.9 675.261 23 4 -3 5 245229. 2827.64 23 -1 4 5 242592. 2781.10 22 -3 -1 5 239724. 1908.80 13 -3 -1 5 241083. 2229.10 10 -3 -1 5 245497. 3019.44 6 -3 -1 6 62183.0 1033.54 13 -3 -1 6 62750.0 1579.54 6 -3 -1 6 60836.7 1631.99 1 4 -3 6 62853.5 1471.39 23 -3 -1 6 62830.4 1559.89 8 -3 -1 6 59838.3 1164.62 10 -3 -1 7 4547.74 296.985 13 -3 -1 7 4524.13 461.765 1 -3 -1 7 4909.97 459.056 8 4 -3 7 4723.43 410.344 23 -3 -1 7 4502.41 330.615 10 -3 -1 7 5029.30 459.755 6 -3 -1 8 10142.5 462.237 13 -1 4 8 10060.6 466.441 28 4 -3 8 10848.1 522.676 17 -3 -1 8 9319.56 453.420 12 -3 -1 8 10378.3 731.997 1 4 -3 8 9658.73 709.692 8 4 -3 8 10447.0 625.365 23 -3 -1 8 9459.59 451.706 15 4 -3 8 9881.18 501.272 34 -3 -1 8 9589.04 461.679 27 -3 -1 8 10354.4 703.058 8 -3 -1 8 9716.99 468.341 37 4 -3 9 21781.7 668.833 19 -3 -1 9 21807.1 1100.84 1 -3 -1 9 23074.8 737.144 13 -1 4 9 23373.8 741.990 28 -3 -1 9 22823.6 755.612 27 4 -3 9 23909.4 807.258 17 -3 -1 9 22491.5 735.237 12 4 -3 9 23635.4 1160.64 8 4 -3 9 21943.6 963.615 5 -3 -1 9 23850.8 736.699 11 -3 -1 9 23621.2 748.964 15 -3 -1 9 24309.8 759.537 37 4 -3 9 23369.0 809.330 34 -3 -1 9 22347.5 709.637 32 -3 -1 9 23310.1 1096.18 8 4 -3 9 22161.5 679.922 14 4 -3 10 93098.2 1468.50 14 -3 -1 10 96441.9 2341.63 8 -3 -1 10 92392.5 1559.29 15 -3 -1 10 95118.9 2388.60 1 -3 -1 10 91973.2 1550.73 13 4 -3 10 91810.9 2050.20 5 -1 4 10 94377.3 1549.70 28 -3 -1 10 94272.2 1548.08 37 4 -3 10 91995.9 1654.08 17 4 -3 10 91640.6 1441.46 19 -3 -1 10 91227.5 1537.71 12 4 -3 10 94233.8 2398.06 8 -3 -1 10 92669.2 1506.70 11 4 -3 10 90558.2 1670.86 34 4 -3 10 91879.4 2050.47 9 4 -3 10 91827.6 1669.24 20 -3 -1 10 90277.6 1511.02 32 4 -3 11 38149.5 996.348 14 4 -3 11 35762.4 1322.39 5 -3 -1 11 39517.4 1063.66 13 -3 -1 11 40709.4 1568.93 8 -1 4 11 37975.3 1023.82 28 4 -3 11 38237.7 1119.02 17 -3 -1 11 38624.0 1049.32 15 -3 -1 11 38781.6 1009.91 11 -3 -1 11 39238.7 1044.52 12 -3 -1 11 39189.6 1015.18 37 4 -3 11 38784.1 981.906 19 4 -3 11 36979.9 1108.39 20 -3 -1 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30 -7 4 2 17742.1 777.444 29 -7 4 2 18280.1 797.231 38 -7 4 2 17515.7 783.715 21 3 -7 3 198852. 2544.49 30 -7 4 3 200610. 2622.20 38 -7 4 3 199008. 2686.71 16 -7 4 3 200589. 2425.90 31 -7 4 3 197411. 2652.02 21 -7 4 4 89889.6 1658.39 31 3 -7 4 91658.1 1759.37 30 -7 4 4 89945.1 1498.88 15 -7 4 4 89408.6 1794.01 21 3 -7 4 91350.0 1771.47 34 -7 4 4 87287.6 1796.73 16 -7 4 4 93160.8 1768.30 38 -7 4 5 21680.2 833.429 31 -7 4 5 20235.3 871.598 16 -7 4 5 21445.1 839.604 38 -7 4 5 20864.7 731.608 15 3 -7 5 19687.3 843.206 34 -7 4 6 87875.3 1714.40 31 4 3 6 91024.4 1606.20 19 -7 4 6 90229.8 1860.96 16 3 -7 6 89976.6 1826.15 34 -7 4 6 90505.8 1564.95 15 -7 4 7 38530.9 1146.33 31 4 3 7 38301.7 1065.64 19 -7 4 7 37724.5 1017.83 15 -7 4 7 37553.2 1206.15 16 3 -7 7 37683.3 1198.17 34 -7 4 8 98618.6 1879.46 31 4 3 8 98688.2 1727.93 19 -7 4 8 97808.8 1690.49 15 -7 4 8 99259.6 1978.94 16 3 -7 8 96405.8 1942.96 34 -7 4 9 12945.4 686.120 31 4 3 9 13157.3 638.962 19 -7 4 9 13152.3 716.080 16 -7 4 9 13274.8 622.180 15 3 -7 9 12957.3 708.550 34 4 3 10 5790.97 422.385 19 -7 4 10 4991.39 440.148 16 3 -7 10 5158.02 445.291 34 -7 4 10 5299.78 394.871 15 -7 4 10 5685.20 453.307 31 3 -7 10 5519.20 454.043 32 -7 4 11 9560.82 586.512 31 4 3 11 10199.5 556.641 14 4 3 11 10086.2 558.219 19 -7 4 11 10007.9 535.475 15 3 -7 11 9750.47 613.811 34 3 -7 11 10754.9 625.191 32 4 3 12 23915.4 835.588 19 -7 4 12 24543.9 924.100 31 4 3 12 24122.4 838.026 14 3 -7 12 23594.8 928.116 34 3 -7 12 25236.9 936.458 32 -7 4 13 2067.94 257.678 31 4 3 13 1961.08 227.734 14 4 3 13 1957.22 237.742 28 4 3 13 2028.18 226.844 19 3 -7 13 1708.32 235.211 34 3 -7 13 1746.91 240.158 32 -7 4 14 27449.4 900.852 31 4 3 14 26196.8 859.554 28 -7 4 14 25392.6 856.834 37 3 -7 14 26327.0 888.663 34 3 -7 14 26664.6 875.766 32 4 3 14 25653.8 796.060 19 -7 4 15 6699.69 417.779 31 4 3 15 6914.60 411.472 28 -7 4 15 6088.96 376.611 37 3 -7 15 6288.99 393.160 32 4 3 15 6423.05 367.469 19 3 -7 15 6060.53 390.808 34 -7 4 16 1808.68 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28734.9 907.837 15 4 -8 4 28049.3 1020.18 34 -8 4 4 29100.2 1002.00 31 -8 4 5 8316.61 582.511 16 -8 4 5 8335.00 539.591 31 4 -8 5 8487.40 566.630 34 -8 4 5 8437.78 493.128 15 -8 4 6 103082. 1923.88 31 -8 4 6 100449. 1706.80 15 -8 4 6 101482. 2036.49 16 4 -8 6 100821. 1975.21 34 -8 4 7 44923.4 1269.37 31 -8 4 7 45989.7 1156.49 15 4 -8 7 45002.9 1324.39 34 -8 4 7 43933.0 1338.23 16 -8 4 8 12142.0 657.853 31 4 -8 8 12156.2 685.397 34 4 4 8 12402.3 592.750 28 -8 4 8 12799.7 714.830 16 -8 4 8 11727.6 584.495 15 4 4 9 39498.7 1067.44 28 -8 4 9 37889.9 1033.63 15 -8 4 9 36914.6 1190.45 16 4 -8 9 38262.2 1202.84 34 -8 4 9 38193.3 1159.06 31 4 -8 9 39202.8 1125.29 32 -8 4 10 441.904 129.261 31 4 4 10 513.063 117.554 28 4 -8 10 397.826 106.912 34 -8 4 10 401.917 123.541 16 -8 4 10 564.776 129.238 15 4 -8 10 509.321 120.320 32 -8 4 11 14796.2 690.907 31 4 4 11 15747.0 660.112 28 4 -8 11 14904.6 714.714 34 -8 4 12 8217.56 499.343 37 4 4 12 8136.73 461.302 28 -8 4 12 8217.33 487.979 31 4 -8 12 8236.76 507.953 34 -8 4 13 2637.69 264.789 31 4 4 13 2569.54 245.827 28 -8 4 13 2733.46 268.036 37 4 -8 13 2694.65 271.347 34 -8 4 14 1369.44 169.734 31 4 4 14 1247.22 157.396 28 -9 4 -10 3797.52 309.875 21 -9 4 -9 7589.04 463.416 21 -9 4 -8 4469.93 371.160 21 -9 4 -7 15415.5 707.456 21 -9 4 -6 13417.8 677.155 21 5 -9 -5 26182.9 932.816 30 -9 4 -5 26070.8 964.501 21 5 -9 -4 17224.5 762.937 30 -9 4 -4 17549.1 800.271 21 -9 4 -3 21074.0 884.201 21 5 -9 -3 21766.3 851.792 30 5 -9 -2 48055.3 1272.10 30 -9 4 -2 48417.6 1144.85 15 -9 4 -2 48213.0 1357.53 21 5 -9 -1 21783.8 859.280 30 -9 4 -1 21261.5 898.269 16 -9 4 -1 21824.3 772.135 15 -9 4 -1 21461.0 910.628 21 -9 4 0 15146.5 762.537 21 -9 4 0 15297.3 760.244 16 5 -9 0 16457.6 743.165 30 -9 4 0 15937.3 662.813 15 5 -9 1 2291.05 275.979 30 -9 4 1 2266.27 294.049 21 -9 4 1 2638.28 269.465 15 -9 4 1 1967.08 271.680 16 5 -9 2 22734.5 871.893 30 -9 4 2 22124.5 918.342 16 -9 4 2 22794.6 794.539 15 5 -9 2 24177.5 876.604 34 5 -9 3 29846.6 988.567 30 5 -9 3 28883.5 977.114 34 -9 4 3 28658.7 888.381 15 -9 4 3 29040.6 1044.30 16 -9 4 4 8586.52 570.492 16 -9 4 4 8130.91 471.639 15 5 -9 4 8381.92 527.454 34 -9 4 5 16303.0 776.127 16 -9 4 5 17028.0 681.476 15 5 -9 5 16977.3 756.161 34 -9 4 6 58906.4 1253.61 15 -9 4 6 58592.9 1459.40 16 5 -9 6 59617.8 1418.63 34 5 -9 7 43040.0 1195.80 34 -9 4 7 42282.6 1218.44 16 -9 4 7 42887.9 1049.33 15 -9 4 7 41186.7 1134.55 37 -9 4 7 43225.5 1167.87 31 -9 4 8 6042.61 384.472 15 -9 4 8 6008.17 444.708 16 -9 4 8 5869.22 421.679 37 5 -9 8 5865.77 430.917 34 -9 4 8 6393.47 437.884 31 -9 4 9 1672.73 211.430 31 -9 4 9 1548.14 185.075 15 -9 4 9 1559.47 218.740 16 -9 4 9 1657.45 219.944 37 5 -9 9 1650.88 217.234 34 -9 4 10 2821.40 241.456 15 -9 4 10 3278.42 297.544 37 5 -9 10 3234.42 299.571 34 -9 4 10 3166.36 285.714 31 5 -9 11 7064.52 421.778 34 -9 4 11 6854.45 406.543 37 -9 4 11 7842.63 425.451 31 -8 3 -13 1888.96 209.451 15 -8 3 -12 402.639 95.9707 15 -8 3 -11 33572.8 989.161 15 -8 3 -10 1667.72 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34 -6 5 11 5756.24 447.792 31 5 1 11 5652.75 467.022 19 1 -6 11 5525.93 438.848 34 1 -6 11 5339.25 479.643 32 -6 5 12 1884.85 253.848 31 5 1 12 1517.68 232.851 19 1 -6 12 1403.39 219.172 34 1 -6 12 1763.39 257.956 32 5 1 13 80148.2 1726.98 19 -6 5 13 78551.4 1641.41 31 5 1 13 78688.0 1709.27 14 1 -6 13 79878.2 1810.89 32 5 1 14 2533.65 294.539 19 -6 5 14 2379.50 273.700 31 5 1 14 2102.15 262.305 14 1 -6 14 2238.63 293.786 32 -6 5 15 23001.8 831.884 31 5 1 15 22795.0 847.423 14 1 -6 15 23496.7 905.486 32 5 1 15 23482.7 853.867 19 5 1 16 6424.73 417.386 14 -6 5 16 6714.80 418.721 31 1 -6 16 6739.32 448.935 32 5 1 16 6642.84 424.899 19 -6 5 17 2175.24 215.737 31 -7 5 -10 48449.8 1330.28 29 -7 5 -10 49363.5 1324.27 25 -7 5 -9 90689.4 1875.86 29 -7 5 -9 90081.2 1785.12 25 -7 5 -8 66842.2 1631.00 29 -7 5 -8 69112.6 1545.06 25 -7 5 -7 51277.4 1437.79 29 -7 5 -7 52462.1 1322.98 25 -7 5 -6 103227. 2043.03 29 -7 5 -6 104158. 1833.57 25 -7 5 -5 21358.2 925.152 29 -7 5 -5 20674.2 795.072 25 -7 5 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3464.11 361.528 29 -6 6 -4 3227.48 323.766 25 -6 6 -4 3187.81 330.478 38 0 -6 -4 2799.56 306.111 35 0 -6 -3 53199.7 1161.40 30 -6 6 -3 53308.2 1408.69 29 -6 6 -3 54277.7 1308.40 25 0 -6 -3 57742.3 1383.23 35 -6 6 -3 53295.9 1369.78 38 0 -6 -2 58534.1 1225.14 30 -6 6 -2 58877.1 1446.19 29 -6 6 -2 57602.0 1328.50 25 0 -6 -2 57374.4 1724.18 24 -6 6 -2 59049.9 1454.60 38 0 -6 -2 57922.8 1362.53 35 0 -6 -1 5171.20 365.919 30 -6 6 -1 5653.08 437.891 29 -6 6 -1 5419.40 404.622 25 -6 6 -1 5405.10 440.859 38 0 -6 -1 5422.78 404.540 35 0 -6 0 7180.77 437.533 30 -6 6 0 7442.02 627.732 2 -6 6 0 8184.45 519.022 29 -6 6 0 7689.53 480.643 25 6 0 0 7388.80 615.689 23 -6 6 0 7274.67 512.339 38 0 -6 0 7457.29 474.196 35 0 -6 1 84676.8 1546.16 30 -6 6 1 87704.7 1688.29 29 -6 6 1 90073.6 1667.32 25 6 0 1 89662.1 2202.35 23 -6 6 1 86974.9 1776.49 38 0 -6 1 90643.5 1675.89 35 -6 6 1 87482.2 2150.59 2 -6 6 2 16009.2 711.276 29 6 0 2 16505.6 755.809 26 -6 6 2 16179.6 712.613 25 0 -6 2 17443.6 733.498 35 -6 6 3 9872.79 539.283 29 6 0 3 9456.58 568.494 26 -6 6 3 9563.46 497.111 16 -6 6 3 9939.75 596.906 38 0 -6 3 9904.77 558.502 35 6 0 4 58618.8 1415.22 26 -6 6 4 64082.8 1289.23 16 -6 6 4 60187.7 1488.64 38 0 -6 4 62950.0 1447.84 35 0 -6 5 25950.8 917.740 27 6 0 5 25698.4 930.848 26 -6 6 5 25187.7 964.044 38 0 -6 5 26275.9 953.997 35 0 -6 6 5378.84 419.072 27 6 0 6 4509.20 385.963 26 -6 6 6 4561.53 407.187 38 0 -6 6 4876.90 421.714 35 0 -6 7 24451.1 916.339 27 6 0 7 24618.7 884.081 26 -6 6 7 25334.5 957.853 38 0 -6 7 25019.0 972.851 35 0 -6 7 24576.6 923.312 34 0 -6 7 23396.5 793.706 33 -6 6 8 10423.3 548.486 31 6 0 8 9590.30 608.148 19 0 -6 8 9614.46 578.832 27 -6 6 8 10231.9 598.231 38 0 -6 8 9833.68 586.929 34 0 -6 8 9662.86 525.356 33 -6 6 9 64268.1 1404.84 31 6 0 9 62080.3 1563.69 19 0 -6 9 65536.4 1532.00 27 -6 6 9 66145.0 1491.25 38 0 -6 9 64135.9 1483.77 34 -6 6 10 1061.68 180.576 31 6 0 10 1128.55 208.073 19 0 -6 10 871.952 168.879 34 0 -6 10 1409.07 240.203 32 -6 6 11 15750.2 710.256 31 6 0 11 16253.1 795.659 19 0 -6 11 15422.0 809.477 32 6 0 12 23308.0 940.668 19 -6 6 12 26576.4 913.829 31 0 -6 12 23923.2 995.382 32 6 0 13 31102.3 1053.13 19 -6 6 13 31770.5 981.273 31 6 0 13 31075.3 1052.69 14 0 -6 13 30169.5 1085.22 32 6 0 14 7301.28 483.967 19 -6 6 14 6997.32 443.300 31 6 0 14 7021.48 478.722 14 0 -6 14 7201.15 508.681 32 -6 6 15 16514.0 643.553 31 6 0 15 16523.2 691.605 14 0 -6 15 16427.6 724.359 32 6 0 15 16721.6 689.539 19 6 0 16 4359.94 324.336 14 -6 6 16 4197.71 300.726 31 0 -6 16 4116.02 331.002 32 6 0 16 3922.89 303.790 19 -7 6 -11 65358.8 1496.22 29 -7 6 -10 153.865 47.6373 29 -7 6 -10 711.282 152.395 25 -7 6 -9 11962.8 691.392 29 -7 6 -9 12133.4 657.674 25 -7 6 -8 61503.4 1608.66 29 -7 6 -8 62554.0 1495.45 25 -7 6 -7 42571.4 1348.50 29 -7 6 -7 42848.6 1232.31 25 -7 6 -6 2108.30 299.829 29 -7 6 -6 1112.78 194.058 25 1 -7 -5 46480.8 1168.50 30 -7 6 -5 46286.2 1404.30 29 -7 6 -5 46356.0 1243.52 25 1 -7 -5 45762.9 1304.66 35 1 -7 -4 46200.8 1168.24 30 -7 6 -4 46095.5 1386.74 29 -7 6 -4 47082.0 1232.23 25 -7 6 -4 44504.9 1330.34 38 1 -7 -4 46540.4 1295.67 35 1 -7 -3 44917.3 1167.20 30 -7 6 -3 44031.2 1349.37 29 1 -7 -3 46500.9 1261.64 35 -7 6 -3 45013.1 1188.93 25 -7 6 -3 44444.6 1341.56 38 1 -7 -2 117320. 1888.11 30 -7 6 -2 117752. 2180.34 29 -7 6 -2 120525. 1938.93 25 -7 6 -2 115932. 2186.83 38 1 -7 -2 116402. 1981.18 35 1 -7 -1 58930.5 1344.15 30 -7 6 -1 59793.5 1530.19 29 -7 6 -1 60098.6 1359.62 25 -7 6 -1 58059.1 1550.56 38 1 -7 -1 59224.2 1390.94 35 -7 6 -1 56975.1 1375.01 21 1 -7 0 672.802 147.965 30 -7 6 0 875.286 178.915 29 -7 6 0 501.983 124.679 25 -7 6 0 593.095 157.095 38 1 -7 0 545.622 131.527 35 -7 6 0 646.833 145.585 21 1 -7 1 180016. 2423.89 30 -7 6 1 181275. 2604.16 29 -7 6 1 186838. 2406.50 25 -7 6 1 180516. 2735.42 38 1 -7 1 180295. 2400.45 35 -7 6 1 184314. 2396.67 21 1 -7 2 70759.1 1539.61 30 -7 6 2 72376.1 1615.28 29 -7 6 2 72516.4 1538.61 16 -7 6 2 70288.2 1694.59 38 1 -7 2 72647.7 1519.88 35 -7 6 2 75699.6 1519.27 21 -7 6 3 7154.84 490.319 29 -7 6 3 7484.51 489.386 16 -7 6 3 6983.44 535.329 38 1 -7 3 7408.00 490.290 35 -7 6 3 7851.43 480.524 21 6 1 4 89424.6 1799.92 26 -7 6 4 94372.9 1745.90 16 -7 6 4 91128.2 1913.52 38 1 -7 4 94739.2 1774.23 35 -7 6 4 94634.7 1661.79 21 6 1 5 6729.46 483.121 26 -7 6 5 6072.80 440.449 16 -7 6 5 6272.97 491.892 38 1 -7 5 6557.04 474.080 35 6 1 6 9774.06 574.475 26 -7 6 6 9953.52 560.639 16 -7 6 6 9517.49 605.130 38 1 -7 6 11411.8 627.841 35 1 -7 6 9534.98 601.499 34 -7 6 7 105384. 1771.91 31 6 1 7 104906. 1982.07 19 -7 6 7 109043. 1860.65 16 -7 6 7 109707. 1999.73 38 1 -7 7 109657. 1954.39 35 1 -7 7 106070. 2003.73 34 -7 6 8 673.052 129.889 31 6 1 8 866.347 174.480 19 -7 6 8 855.088 160.278 16 -7 6 8 910.222 176.047 38 1 -7 8 1029.01 184.301 34 -7 6 9 10561.9 571.500 31 6 1 9 10359.5 618.396 19 -7 6 9 10302.0 549.899 16 1 -7 9 9665.81 589.327 34 -7 6 10 117881. 1919.28 31 6 1 10 113758. 2038.42 19 1 -7 10 112630. 2000.48 34 1 -7 10 116132. 2193.53 32 -7 6 11 10306.2 557.864 31 6 1 11 10559.6 608.774 19 1 -7 11 10180.7 572.318 34 1 -7 11 10314.7 640.696 32 -7 6 12 1725.05 224.376 31 6 1 12 1893.62 245.952 19 1 -7 12 1862.87 231.886 34 1 -7 12 1841.33 257.345 32 6 1 13 4011.14 340.555 19 -7 6 13 4041.19 328.130 31 1 -7 13 4263.46 379.949 32 6 1 14 6882.08 423.008 19 -7 6 14 7497.55 426.256 31 6 1 14 7496.02 442.480 14 1 -7 14 7673.10 477.656 32 1 -7 15 3686.98 301.949 32 2 -8 -13 11803.4 530.795 35 -8 6 -10 14727.5 689.882 29 -8 6 -9 5412.46 442.417 29 2 -8 -8 9145.28 509.919 30 -8 6 -8 9228.71 599.995 29 2 -8 -8 9719.00 586.721 35 2 -8 -7 71145.4 1470.63 30 -8 6 -7 69598.4 1692.60 29 2 -8 -7 71614.5 1600.94 35 2 -8 -6 16184.9 709.882 30 -8 6 -6 14740.5 793.645 29 2 -8 -6 15914.5 748.834 35 2 -8 -5 12456.7 631.407 30 -8 6 -5 12957.0 751.239 29 2 -8 -5 12670.5 657.562 35 2 -8 -4 130555. 2078.69 30 -8 6 -4 131745. 2401.37 29 2 -8 -4 137515. 2159.01 35 2 -8 -3 82994.1 1659.37 30 -8 6 -3 82087.2 1885.94 29 2 -8 -3 84522.1 1681.85 35 -8 6 -3 81928.4 1769.16 21 2 -8 -2 12875.4 655.563 30 -8 6 -2 13255.7 750.222 29 2 -8 -2 12933.6 645.970 35 -8 6 -2 12219.5 675.868 21 2 -8 -1 98664.0 1848.46 30 -8 6 -1 101461. 2068.52 29 2 -8 -1 101371. 1790.72 35 -8 6 -1 99421.6 1914.40 21 2 -8 0 103041. 1896.74 30 -8 6 0 100795. 2027.55 29 -8 6 0 100787. 2113.44 38 2 -8 0 103903. 1796.23 35 -8 6 0 101924. 1917.04 21 2 -8 1 5148.98 429.168 30 -8 6 1 6966.01 521.737 29 -8 6 1 5275.83 438.707 16 -8 6 1 5703.20 497.413 38 2 -8 1 5870.62 420.044 35 -8 6 1 5231.46 428.893 21 2 -8 2 56089.9 1417.19 30 -8 6 2 54719.1 1442.69 29 -8 6 2 56005.8 1435.14 16 -8 6 2 56044.8 1556.17 38 2 -8 2 56065.9 1304.13 35 -8 6 2 57119.9 1405.43 21 -8 6 3 149433. 2340.92 29 -8 6 3 151935. 2531.67 38 2 -8 3 155365. 2180.05 35 -8 6 3 150720. 2273.04 21 6 2 4 17601.4 803.718 26 -8 6 4 16671.7 769.415 16 -8 6 4 17615.1 846.764 38 2 -8 4 17428.6 724.014 35 2 -8 4 16794.3 810.476 34 6 2 5 120608. 2043.13 26 -8 6 5 122725. 2084.27 16 -8 6 5 121777. 2199.25 38 2 -8 5 118826. 2157.94 34 6 2 6 5768.71 441.232 19 -8 6 6 5831.40 445.565 16 -8 6 6 6053.24 467.882 38 2 -8 6 6251.89 485.790 34 6 2 7 1427.22 210.279 19 -8 6 7 1479.70 218.204 16 -8 6 7 1548.81 223.382 38 2 -8 7 1478.81 240.844 34 -8 6 8 109647. 1795.77 31 6 2 8 103757. 1845.50 19 -8 6 8 104647. 1838.14 16 2 -8 8 103631. 1952.05 34 -8 6 9 16352.6 685.333 31 6 2 9 15783.8 708.160 19 -8 6 9 16312.6 697.820 16 2 -8 9 16183.0 749.639 34 -8 6 10 10935.1 552.067 31 6 2 10 9872.12 541.150 19 2 -8 10 9740.66 564.172 34 2 -8 10 10461.5 608.475 32 -8 6 11 7976.99 455.607 31 6 2 11 7647.05 452.627 19 2 -8 11 6993.27 450.569 34 2 -8 11 7653.50 495.718 32 6 2 12 5320.09 357.476 19 -8 6 12 5382.75 360.254 31 6 2 12 5205.22 356.232 14 2 -8 12 5413.23 370.877 34 2 -8 12 5682.26 408.341 32 -8 6 13 8075.27 411.126 31 6 2 13 8490.34 419.359 28 2 -8 13 8235.75 452.423 32 3 -9 -10 2088.60 202.177 30 3 -9 -10 2182.97 215.697 35 3 -9 -9 18729.3 652.083 30 3 -9 -9 18996.4 667.829 35 3 -9 -8 15068.4 620.711 30 -9 6 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654.414 34 -9 6 3 683.196 150.061 16 3 -9 3 484.867 130.819 34 -9 6 4 41995.7 1205.90 16 3 -9 4 42126.6 1222.47 34 -9 6 5 2228.45 271.755 16 3 -9 5 2328.74 278.892 34 -9 6 6 133.369 73.9114 16 3 -9 6 341.562 116.884 34 -9 6 7 5376.99 401.727 16 3 -9 7 5196.60 416.567 34 -9 6 7 4888.19 349.369 31 -9 6 8 20107.3 755.796 16 3 -9 8 19362.7 777.365 34 -9 6 8 19139.5 687.009 31 -9 6 9 3225.18 289.378 16 3 -9 9 2983.23 293.674 34 3 -9 9 3238.47 299.784 32 -9 6 9 3097.72 267.819 31 -9 6 10 6659.07 374.849 31 3 -9 10 6931.37 423.535 34 3 -9 10 6668.84 406.578 32 4 -10 -6 2440.19 231.782 30 -10 6 -6 2040.63 221.287 21 4 -10 -5 5842.33 377.806 30 -10 6 -5 5635.03 383.516 21 4 -10 -4 6470.43 407.469 30 -10 6 -4 6357.71 421.749 16 -10 6 -4 5857.17 401.424 21 4 -10 -3 969.010 161.121 30 -10 6 -3 850.902 157.729 16 -10 6 -3 722.280 144.636 21 4 -10 -2 207.088 72.9084 30 -10 6 -2 133.969 48.8417 16 -10 6 -2 175.985 61.3181 21 4 -10 -1 1808.93 228.832 30 -10 6 -1 1640.39 217.923 16 -10 6 -1 1700.55 222.969 21 -10 6 0 2274.66 256.741 16 4 -10 0 2353.23 239.612 34 -10 6 1 421.033 107.147 16 4 -10 1 189.627 56.6847 34 -10 6 2 826.450 155.169 16 4 -10 2 749.191 141.339 34 -10 6 3 7563.97 463.851 16 4 -10 3 8065.24 464.810 34 -10 6 4 11230.8 556.042 16 4 -10 4 10155.2 519.685 34 -10 6 5 419.962 109.534 16 4 -10 5 423.229 104.215 34 -10 6 6 26653.0 805.508 16 4 -10 6 25882.3 803.554 34 7 -10 -4 7476.79 390.658 30 -10 3 -4 6821.05 375.969 15 7 -10 -3 4430.57 304.754 30 -10 3 -3 4003.89 281.424 18 -10 3 -3 4154.75 301.835 15 7 -10 -2 2780.64 239.422 30 -10 3 -2 2653.80 232.504 18 -10 3 -2 2719.91 249.635 15 7 -10 -1 2711.98 237.191 30 -10 3 -1 2745.50 239.935 18 -10 3 -1 2807.74 253.612 15 -10 3 0 1830.00 196.662 18 -10 3 0 1802.28 201.483 16 -10 3 0 2020.11 215.628 15 -10 3 1 3120.82 256.474 18 -10 3 1 3139.74 267.409 16 -10 3 1 3130.63 266.684 15 -10 3 2 3489.76 264.328 18 -10 3 2 3472.06 281.849 16 -10 3 2 3392.03 279.478 15 -10 3 3 5014.26 313.238 18 -10 3 3 5346.02 349.372 16 -10 3 3 5369.05 351.037 15 -10 3 4 2329.32 227.161 16 -10 3 4 2063.99 215.241 15 -9 2 -9 3338.32 280.921 15 -9 2 -8 15531.6 632.407 15 -9 2 -7 10039.9 523.678 15 -9 2 -6 2733.38 278.075 15 7 -9 -5 8284.43 467.503 30 -9 2 -5 8373.02 498.259 15 7 -9 -4 8568.95 474.038 30 -9 2 -4 8487.12 509.536 15 7 -9 -3 141.575 74.6675 30 -9 2 -3 13.5763 51.9334 15 7 -9 -2 11041.2 534.378 30 -9 2 -2 10494.7 582.047 15 -9 2 -1 4079.58 357.693 18 -9 2 -1 4007.35 363.244 15 -9 2 0 8447.08 517.205 18 -9 2 0 7932.89 510.026 15 -9 2 1 15315.0 695.898 18 -9 2 1 14335.1 689.342 15 -9 2 2 24208.9 872.618 18 -9 2 2 25048.3 838.908 16 -9 2 2 24019.1 888.881 15 -9 2 3 8933.62 521.826 18 -9 2 3 9117.61 505.855 16 -9 2 3 9039.42 540.250 15 -9 2 4 24710.2 868.615 18 -9 2 4 24437.9 831.306 16 -9 2 4 25408.0 899.469 15 -9 2 5 20703.6 780.790 18 -9 2 5 20311.3 747.184 16 -9 2 5 20180.9 714.349 37 -9 2 5 20671.1 803.775 15 -9 2 6 4416.51 343.870 16 -9 2 6 4452.71 333.365 37 -9 2 6 4635.56 372.607 15 -9 2 7 13540.5 582.091 37 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6354.03 464.849 27 9 -3 6 6886.86 442.978 17 -6 9 6 6527.71 485.345 38 9 -3 7 2478.30 260.443 19 -3 -6 7 3165.49 322.026 27 9 -3 7 2730.60 268.585 17 -6 9 7 2922.71 313.204 38 9 -3 8 8396.36 461.971 19 -3 -6 8 8705.49 523.874 27 9 -3 8 7844.96 432.978 17 -6 9 8 8249.69 506.952 38 9 -3 9 5315.42 353.108 19 -6 9 9 6063.20 414.300 38 -6 9 10 5295.37 352.796 38 -7 9 -9 3227.97 301.426 29 -2 -7 -9 3145.09 257.686 35 -7 9 -8 3270.28 320.836 29 -2 -7 -8 3498.84 284.681 35 -7 9 -7 13645.9 670.426 29 -2 -7 -7 13196.7 580.489 35 -7 9 -6 4017.61 368.812 29 -2 -7 -6 4466.17 345.714 35 -7 9 -5 20399.6 846.750 29 -2 -7 -5 20510.5 769.721 35 -7 9 -4 24584.1 930.502 29 -2 -7 -4 25525.5 877.157 35 -7 9 -3 9196.91 562.325 29 -7 9 -3 9793.88 563.225 38 -2 -7 -3 9036.16 526.982 35 -7 9 -2 23127.7 889.726 29 -7 9 -2 22960.9 895.014 38 -2 -7 -2 23739.3 873.931 35 -7 9 -1 15031.0 694.421 29 -7 9 -1 15537.9 748.414 38 -2 -7 -1 14991.9 707.045 35 -7 9 0 8147.43 493.562 29 -7 9 0 8208.21 549.406 38 -2 -7 0 8236.61 524.836 35 -7 9 1 4013.90 392.866 38 -2 -7 1 3829.74 358.391 35 -7 9 2 10792.0 641.068 38 -2 -7 2 10671.7 606.011 35 -2 -7 3 180.572 87.7582 27 -7 9 3 134.564 68.3034 38 -2 -7 4 8373.96 520.162 27 -7 9 4 8664.09 569.623 38 -2 -7 4 8357.07 533.754 35 9 -2 5 8373.02 508.807 19 -2 -7 5 8566.95 523.692 27 -7 9 5 8480.27 550.517 38 -2 -7 5 8454.00 467.473 34 9 -2 6 2473.17 270.018 19 -2 -7 6 2676.59 288.454 27 -7 9 6 2524.53 288.568 38 9 -2 7 10327.8 533.468 19 -2 -7 7 10251.5 544.904 27 -7 9 7 10407.6 572.454 38 9 -2 8 14776.3 619.621 19 -2 -7 8 15210.6 642.778 27 -7 9 8 15205.0 656.307 38 9 -2 9 3529.13 286.951 19 -7 9 9 3469.70 289.288 38 -8 9 -8 191.286 70.5556 29 -8 9 -7 14516.6 640.513 29 -1 -8 -7 14338.8 573.251 35 -8 9 -6 44194.6 1156.58 29 -1 -8 -6 42970.4 1037.93 35 -8 9 -5 1902.99 236.581 29 -1 -8 -5 2058.20 234.451 35 -8 9 -4 12195.0 619.507 29 -1 -8 -4 11964.6 579.669 35 -8 9 -3 24818.0 885.428 29 -1 -8 -3 24336.7 837.150 35 -8 9 -2 5153.44 395.892 29 -8 9 -2 4905.60 394.486 38 -1 -8 -2 5021.44 384.740 35 -8 9 -1 1597.09 217.130 29 -8 9 -1 1655.72 239.254 38 -1 -8 -1 1520.07 215.818 35 -8 9 0 3024.03 287.144 29 -8 9 0 3464.92 347.630 38 -1 -8 0 3042.36 300.417 35 -1 -8 1 11636.0 575.571 27 -8 9 1 11509.1 636.773 38 -1 -8 1 11487.1 602.211 35 -1 -8 2 5123.32 376.501 27 -8 9 2 5273.91 428.819 38 -1 -8 2 4721.65 382.192 35 -1 -8 3 8244.21 474.108 27 -8 9 3 8557.06 541.620 38 -1 -8 3 8466.41 509.849 35 9 -1 4 17947.5 732.412 19 -1 -8 4 17375.5 680.700 27 -8 9 4 17235.1 756.119 38 -1 -8 4 17489.9 720.117 35 -1 -8 4 17195.0 680.719 34 9 -1 5 6307.11 419.528 19 -1 -8 5 6340.18 400.400 27 -8 9 5 6636.82 454.827 38 -1 -8 5 6722.70 409.763 34 9 -1 6 143.710 56.3729 19 -1 -8 6 110.758 47.1254 27 -8 9 6 149.312 58.9746 38 -1 -8 6 157.213 46.0559 34 9 -1 7 1764.90 208.825 19 -1 -8 7 1217.54 161.872 27 -8 9 7 1411.50 188.035 38 -1 -8 7 1356.05 179.912 32 -9 9 -4 5833.89 382.909 29 0 -9 -4 6464.43 382.612 35 -9 9 -3 1978.62 226.727 29 0 -9 -3 1550.90 187.775 35 -9 9 -2 4160.97 318.930 29 0 -9 -2 4233.94 322.062 35 -9 9 -1 12006.0 535.934 29 0 -9 -1 13047.6 573.267 35 0 -9 0 640.327 129.608 35 0 -9 1 1070.06 160.075 35 0 -9 2 6144.94 384.269 35 0 -9 2 6124.86 394.159 34 9 0 3 4108.11 317.434 19 0 -9 3 4069.42 308.267 35 0 -9 3 4282.86 326.096 34 9 0 4 9320.16 465.672 19 0 -9 4 8965.60 453.805 34 -8 -2 -1 7460.09 402.567 36 -7 -3 -5 16580.4 606.539 36 -7 -3 -4 2583.86 247.153 36 -7 -3 -3 5614.08 376.773 36 -7 -3 -2 2698.37 260.319 36 -7 -3 -1 11313.0 541.709 36 10 -7 0 10590.4 501.157 17 -7 -3 0 11698.8 544.595 36 10 -7 1 10990.5 510.994 17 -7 -3 1 12037.3 541.826 36 10 -7 2 11204.6 517.687 17 -3 10 2 10657.7 505.476 38 -7 -3 2 11206.7 505.649 36 10 -7 3 14689.2 585.926 17 -3 10 3 14500.6 595.248 38 -7 -3 3 14209.2 540.643 36 10 -7 4 12082.7 522.936 17 -3 10 4 11858.5 536.473 38 10 -7 5 25357.0 746.840 17 -3 10 5 26212.4 792.840 38 -4 10 -6 27207.6 823.478 29 -6 -4 -6 26790.7 769.063 36 -4 10 -5 546.784 121.119 29 -6 -4 -5 609.095 121.531 36 -4 10 -4 10109.3 505.759 29 -6 -4 -4 10256.3 516.132 36 -4 10 -3 7994.57 443.015 29 -6 -4 -3 8367.06 476.241 36 -6 -4 -2 860.056 155.771 36 -6 -4 -1 293.337 78.8518 27 -6 -4 -1 173.507 47.1283 36 -6 -4 0 2323.17 236.860 27 -6 -4 0 2371.95 258.036 36 -6 -4 1 1581.71 195.971 27 -4 10 1 1281.07 181.678 38 -6 -4 1 1715.32 213.978 36 -6 -4 2 358.750 97.4146 27 10 -6 2 139.051 40.9896 17 -4 10 2 302.516 102.424 38 -6 -4 3 746.087 130.632 27 10 -6 3 714.983 144.266 17 -4 10 3 745.109 140.407 38 -6 -4 4 5494.58 352.166 27 10 -6 4 6126.15 404.168 17 -4 10 4 5799.35 401.084 38 10 -6 5 5641.36 377.512 17 -4 10 5 6038.84 403.017 38 10 -6 6 2375.51 235.028 17 -4 10 6 2206.79 235.092 38 -5 10 -7 2414.69 245.437 29 -5 10 -6 1639.41 205.150 29 -5 10 -5 2874.28 275.891 29 -5 10 -4 7494.67 448.999 29 -5 10 -3 2774.49 268.386 29 -5 10 0 1339.16 192.962 38 -5 -5 1 4847.66 371.559 27 -5 10 1 3933.78 339.752 38 -5 -5 2 1324.76 190.685 27 -5 10 2 1452.07 210.550 38 -5 -5 3 8668.76 486.567 27 10 -5 3 8197.22 482.938 17 -5 10 3 8173.08 490.115 38 -5 -5 4 10470.7 530.094 27 10 -5 4 10292.1 526.121 17 -5 10 4 10745.6 560.326 38 -5 -5 5 127.713 36.5294 27 10 -5 5 140.791 62.8609 17 -5 10 5 246.369 80.7541 38 -5 -5 6 821.444 135.566 27 10 -5 6 829.645 140.288 17 -5 10 6 959.381 158.501 38 10 -5 7 2336.13 223.558 17 -5 10 7 2703.12 259.968 38 -6 10 -6 8509.45 467.483 29 -6 10 -5 21666.3 760.381 29 -6 10 -4 3494.15 304.981 29 -6 10 -3 2752.12 270.184 29 -6 10 -2 180.814 54.0143 29 -4 -6 -2 421.230 81.9398 35 -6 10 -1 11390.1 555.435 38 -4 -6 -1 10833.2 520.580 35 -6 10 0 3329.59 309.296 38 -4 -6 0 3626.07 305.010 35 -4 -6 1 3332.33 312.585 27 -6 10 1 3809.05 337.423 38 -4 -6 1 3140.06 283.606 35 -4 -6 2 3293.49 306.458 27 -6 10 2 3318.05 315.473 38 -4 -6 3 13651.0 623.914 27 10 -4 3 12687.9 576.944 17 -6 10 3 13420.4 634.675 38 -4 -6 4 168.097 85.2372 27 10 -4 4 276.819 87.0048 17 -6 10 4 55.9211 19.2110 38 -4 -6 5 7546.52 445.124 27 10 -4 5 7193.60 411.488 17 -6 10 5 8172.80 480.707 38 -4 -6 6 2100.84 228.348 27 10 -4 6 1731.84 189.190 17 -6 10 6 1619.79 207.875 38 -7 10 -5 3177.03 279.208 29 -7 10 -4 2349.50 240.211 29 -3 -7 -4 2272.87 224.044 35 -7 10 -3 5374.80 363.383 29 -3 -7 -3 5333.94 353.269 35 -7 10 -2 3195.01 272.571 29 -3 -7 -2 3777.56 304.204 35 -7 10 -1 3432.92 305.851 38 -3 -7 -1 3460.95 295.774 35 -7 10 0 1869.92 227.062 38 -3 -7 0 1827.34 220.738 35 -3 -7 1 2793.99 274.353 27 -7 10 1 2800.47 282.722 38 -3 -7 1 2599.27 261.482 35 -3 -7 2 2870.07 278.179 27 -7 10 2 2871.17 287.524 38 -3 -7 2 2666.08 263.183 35 10 -3 3 4196.53 308.652 19 -3 -7 3 4486.59 341.807 27 10 -3 3 3848.52 287.293 17 -7 10 3 4634.81 366.586 38 10 -3 4 6944.12 385.570 19 -3 -7 4 7662.14 439.518 27 -7 10 4 8011.31 474.444 38 -3 -7 5 1964.76 215.513 27 -7 10 5 2354.46 245.430 38 -2 -8 -1 405.062 95.9086 27 -2 -8 -1 380.575 82.3060 35 -2 -8 0 4458.93 314.585 27 -2 -8 0 4782.67 336.166 35 -2 -8 1 5880.98 362.752 27 -8 10 1 6424.73 406.048 38 -2 -8 1 6069.51 381.060 35 -8 10 2 10466.3 517.688 38 -2 -8 2 10026.3 483.422 35 0 0 0 0.00 0.00 0 TITL mp-17a in P3(1) REM P3(1) (#144 in standard setting) CELL 1.54184 9.268342 9.268342 18.590143 90.0000 90.0000 120.0000 ZERR 3.00 0.000120 0.000120 0.000262 0.0000 0.0000 0.0000 LATT -1 SYMM -y, x-y, z+1/3 SYMM -x+y,-x, z+2/3 SFAC C H O UNIT 63.00 66.00 21.00 TREF HKLF 4 END ; _shelx_hkl_checksum 44787 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z+2/3' '-x+y, -x, z+1/3' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp O3 O 0.66703(18) 0.87305(19) 0.08856(8) 0.0436(4) Uani 1 1 d . . O2 O 0.14411(16) 0.83557(17) 0.12648(9) 0.0412(4) Uani 1 1 d . . O5 O 0.78966(19) 0.9954(2) 0.21662(10) 0.0546(5) Uani 1 1 d . . O1 O 0.71400(18) 1.23170(19) 0.12570(9) 0.0484(4) Uani 1 1 d . . H1 H 0.7131 1.3114 0.1070 0.073 Uiso 1 1 calc R U O7 O 0.0304(2) 0.41728(19) 0.19719(10) 0.0549(5) Uani 1 1 d . . H7 H -0.0705 0.3723 0.1910 0.082 Uiso 1 1 calc R U O6 O 0.5030(2) 1.3417(2) 0.08758(13) 0.0702(6) Uani 1 1 d . . O4 O 0.5464(2) 0.9566(2) 0.25780(10) 0.0546(4) Uani 1 1 d . . C15 C 0.2986(3) 0.6421(3) 0.16670(13) 0.0403(5) Uani 1 1 d . . H15A H 0.3352 0.5632 0.1556 0.048 Uiso 1 1 calc R U H15B H 0.3239 0.6746 0.2167 0.048 Uiso 1 1 calc R U C3 C 0.3079(2) 0.9012(2) 0.11943(11) 0.0323(4) Uani 1 1 d . . C4 C 0.3877(2) 0.7945(2) 0.11839(11) 0.0333(5) Uani 1 1 d . . C2 C 0.4169(2) 1.0621(2) 0.10527(12) 0.0354(5) Uani 1 1 d . . C16 C 0.1122(3) 0.5627(2) 0.15372(13) 0.0398(5) Uani 1 1 d . . H16 H 0.0887 0.5304 0.1030 0.048 Uiso 1 1 calc R U C6 C 0.6325(3) 0.9580(2) 0.20905(13) 0.0393(5) Uani 1 1 d . . C5 C 0.5754(2) 0.9243(2) 0.13230(12) 0.0355(5) Uani 1 1 d . . C10 C 0.4032(3) 0.7474(3) 0.03935(13) 0.0444(5) Uani 1 1 d . . H10A H 0.3791 0.6330 0.0361 0.053 Uiso 1 1 calc R U H10B H 0.3289 0.7626 0.0075 0.053 Uiso 1 1 calc R U C8 C 0.3862(3) 1.2016(3) 0.09942(13) 0.0432(5) Uani 1 1 d . . C12 C 0.6274(3) 1.0528(3) 0.01489(13) 0.0464(5) Uani 1 1 d . . C1 C 0.5878(2) 1.0819(2) 0.09433(12) 0.0367(5) Uani 1 1 d . . C17 C 0.0508(3) 0.6850(3) 0.17162(13) 0.0405(5) Uani 1 1 d . . C11 C 0.5861(3) 0.8700(3) 0.02144(13) 0.0468(6) Uani 1 1 d . . H11 H 0.6271 0.8339 -0.0194 0.056 Uiso 1 1 calc R U C19 C -0.1273(3) 0.6207(3) 0.14813(16) 0.0528(6) Uani 1 1 d . . H19A H -0.1402 0.5846 0.0990 0.079 Uiso 1 1 calc R U H19B H -0.1539 0.7081 0.1524 0.079 Uiso 1 1 calc R U H19C H -0.2010 0.5287 0.1781 0.079 Uiso 1 1 calc R U C9 C 0.2148(3) 1.1762(3) 0.10793(16) 0.0563(7) Uani 1 1 d . . H9A H 0.2181 1.2807 0.1017 0.084 Uiso 1 1 calc R U H9B H 0.1736 1.1333 0.1551 0.084 Uiso 1 1 calc R U H9C H 0.1425 1.0984 0.0724 0.084 Uiso 1 1 calc R U C18 C 0.0781(4) 0.7397(3) 0.24933(16) 0.0600(7) Uani 1 1 d . . H18A H 0.0328 0.8113 0.2579 0.090 Uiso 1 1 calc R U H18B H 0.1953 0.7989 0.2596 0.090 Uiso 1 1 calc R U H18C H 0.0236 0.6436 0.2799 0.090 Uiso 1 1 calc R U C13 C 0.8145(3) 1.1623(4) -0.00171(18) 0.0659(8) Uani 1 1 d . . H13A H 0.8432 1.2772 -0.0031 0.099 Uiso 1 1 calc R U H13B H 0.8385 1.1310 -0.0474 0.099 Uiso 1 1 calc R U H13C H 0.8782 1.1470 0.0351 0.099 Uiso 1 1 calc R U C14 C 0.5283(4) 1.0819(4) -0.04281(15) 0.0612(7) Uani 1 1 d . . H14A H 0.4113 1.0119 -0.0337 0.092 Uiso 1 1 calc R U H14B H 0.5550 1.0558 -0.0891 0.092 Uiso 1 1 calc R U H14C H 0.5561 1.1966 -0.0420 0.092 Uiso 1 1 calc R U C7 C 0.8571(4) 1.0440(4) 0.28819(17) 0.0713(8) Uani 1 1 d . . H7A H 0.7943 0.9538 0.3209 0.107 Uiso 1 1 calc R U H7B H 0.8504 1.1398 0.3029 0.107 Uiso 1 1 calc R U H7C H 0.9714 1.0708 0.2883 0.107 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O3 0.0381(8) 0.0497(9) 0.0481(9) -0.0025(7) -0.0013(6) 0.0257(7) O2 0.0300(7) 0.0331(7) 0.0573(10) 0.0052(7) 0.0015(6) 0.0134(6) O5 0.0359(8) 0.0689(11) 0.0526(10) -0.0001(8) -0.0122(7) 0.0214(8) O1 0.0347(7) 0.0310(7) 0.0664(11) 0.0014(7) -0.0109(7) 0.0066(6) O7 0.0415(9) 0.0354(8) 0.0722(12) 0.0144(8) -0.0045(8) 0.0075(7) O6 0.0519(10) 0.0317(9) 0.1185(18) 0.0075(9) -0.0126(10) 0.0144(8) O4 0.0468(9) 0.0655(11) 0.0442(9) -0.0072(8) -0.0037(8) 0.0227(8) C15 0.0367(11) 0.0312(10) 0.0492(13) -0.0002(9) -0.0072(9) 0.0141(9) C3 0.0312(10) 0.0314(10) 0.0327(10) -0.0025(8) -0.0026(8) 0.0143(8) C4 0.0306(10) 0.0295(10) 0.0387(11) -0.0032(8) -0.0042(8) 0.0141(8) C2 0.0345(10) 0.0330(11) 0.0372(11) -0.0023(8) -0.0044(9) 0.0157(9) C16 0.0363(11) 0.0301(10) 0.0449(12) 0.0026(9) -0.0036(9) 0.0104(9) C6 0.0330(11) 0.0313(10) 0.0461(13) 0.0026(9) -0.0054(10) 0.0106(8) C5 0.0306(10) 0.0334(10) 0.0413(12) 0.0000(8) -0.0019(8) 0.0151(8) C10 0.0454(12) 0.0448(12) 0.0433(13) -0.0109(10) -0.0057(10) 0.0227(10) C8 0.0451(12) 0.0339(12) 0.0495(13) -0.0038(9) -0.0095(10) 0.0188(10) C12 0.0382(12) 0.0552(13) 0.0436(13) 0.0073(10) 0.0051(10) 0.0218(11) C1 0.0295(10) 0.0318(10) 0.0428(12) 0.0023(9) -0.0033(9) 0.0108(8) C17 0.0314(10) 0.0321(10) 0.0476(13) 0.0027(9) 0.0035(9) 0.0081(8) C11 0.0438(12) 0.0612(14) 0.0405(13) -0.0063(11) 0.0014(10) 0.0300(12) C19 0.0338(12) 0.0441(12) 0.0742(18) 0.0033(12) 0.0065(11) 0.0147(10) C9 0.0562(14) 0.0458(13) 0.076(2) -0.0033(12) -0.0033(13) 0.0326(11) C18 0.0624(16) 0.0570(15) 0.0542(15) -0.0061(13) 0.0067(12) 0.0250(13) C13 0.0472(15) 0.0741(17) 0.0719(19) 0.0181(14) 0.0205(13) 0.0269(13) C14 0.0682(17) 0.0787(18) 0.0433(14) 0.0110(13) 0.0026(12) 0.0416(15) C7 0.0530(15) 0.091(2) 0.0558(16) 0.0018(15) -0.0223(13) 0.0250(15) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C5 O3 C11 96.29(15) C3 O2 C17 118.83(15) C6 O5 C7 115.3(2) C1 O1 H1 109.5 C16 O7 H7 109.5 C16 C15 C4 108.27(17) C16 C15 H15A 110.0 C4 C15 H15A 110.0 C16 C15 H15B 110.0 C4 C15 H15B 110.0 H15A C15 H15B 108.4 O2 C3 C2 125.40(18) O2 C3 C4 121.71(17) C2 C3 C4 112.55(17) C3 C4 C15 112.71(17) C3 C4 C10 109.95(17) C15 C4 C10 112.27(17) C3 C4 C5 102.50(15) C15 C4 C5 119.64(17) C10 C4 C5 98.51(16) C3 C2 C8 128.74(19) C3 C2 C1 108.71(17) C8 C2 C1 122.54(18) O7 C16 C15 107.84(17) O7 C16 C17 110.95(18) C15 C16 C17 111.00(17) O7 C16 H16 109.0 C15 C16 H16 109.0 C17 C16 H16 109.0 O4 C6 O5 124.0(2) O4 C6 C5 123.49(19) O5 C6 C5 112.5(2) O3 C5 C6 114.06(17) O3 C5 C4 105.67(16) C6 C5 C4 117.28(17) O3 C5 C1 106.00(17) C6 C5 C1 112.25(17) C4 C5 C1 100.15(15) C11 C10 C4 102.69(17) C11 C10 H10A 111.2 C4 C10 H10A 111.2 C11 C10 H10B 111.2 C4 C10 H10B 111.2 H10A C10 H10B 109.1 O6 C8 C2 119.5(2) O6 C8 C9 119.5(2) C2 C8 C9 121.0(2) C14 C12 C13 108.8(2) C14 C12 C11 114.2(2) C13 C12 C11 108.6(2) C14 C12 C1 114.7(2) C13 C12 C1 110.9(2) C11 C12 C1 99.38(18) O1 C1 C2 111.35(17) O1 C1 C5 111.47(17) C2 C1 C5 103.93(16) O1 C1 C12 113.83(18) C2 C1 C12 115.07(18) C5 C1 C12 100.14(17) O2 C17 C18 107.76(18) O2 C17 C19 102.46(18) C18 C17 C19 112.0(2) O2 C17 C16 108.36(17) C18 C17 C16 113.1(2) C19 C17 C16 112.36(19) O3 C11 C10 101.36(18) O3 C11 C12 101.83(18) C10 C11 C12 113.95(19) O3 C11 H11 112.9 C10 C11 H11 112.9 C12 C11 H11 112.9 C17 C19 H19A 109.5 C17 C19 H19B 109.5 H19A C19 H19B 109.5 C17 C19 H19C 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 C8 C9 H9A 109.5 C8 C9 H9B 109.5 H9A C9 H9B 109.5 C8 C9 H9C 109.5 H9A C9 H9C 109.5 H9B C9 H9C 109.5 C17 C18 H18A 109.5 C17 C18 H18B 109.5 H18A C18 H18B 109.5 C17 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 C12 C13 H13A 109.5 C12 C13 H13B 109.5 H13A C13 H13B 109.5 C12 C13 H13C 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 C12 C14 H14A 109.5 C12 C14 H14B 109.5 H14A C14 H14B 109.5 C12 C14 H14C 109.5 H14A C14 H14C 109.5 H14B C14 H14C 109.5 O5 C7 H7A 109.5 O5 C7 H7B 109.5 H7A C7 H7B 109.5 O5 C7 H7C 109.5 H7A C7 H7C 109.5 H7B C7 H7C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O3 C5 1.418(3) O3 C11 1.449(3) O2 C3 1.330(2) O2 C17 1.481(3) O5 C6 1.326(3) O5 C7 1.443(3) O1 C1 1.418(3) O1 H1 0.8200 O7 C16 1.422(3) O7 H7 0.8200 O6 C8 1.225(3) O4 C6 1.203(3) C15 C16 1.521(3) C15 C4 1.523(3) C15 H15A 0.9700 C15 H15B 0.9700 C3 C2 1.345(3) C3 C4 1.502(3) C4 C10 1.560(3) C4 C5 1.564(3) C2 C8 1.460(3) C2 C1 1.515(3) C16 C17 1.538(3) C16 H16 0.9800 C6 C5 1.499(3) C5 C1 1.574(3) C10 C11 1.533(3) C10 H10A 0.9700 C10 H10B 0.9700 C8 C9 1.493(3) C12 C14 1.522(4) C12 C13 1.540(3) C12 C11 1.543(3) C12 C1 1.577(3) C17 C18 1.510(4) C17 C19 1.512(3) C11 H11 0.9800 C19 H19A 0.9600 C19 H19B 0.9600 C19 H19C 0.9600 C9 H9A 0.9600 C9 H9B 0.9600 C9 H9C 0.9600 C18 H18A 0.9600 C18 H18B 0.9600 C18 H18C 0.9600 C13 H13A 0.9600 C13 H13B 0.9600 C13 H13C 0.9600 C14 H14A 0.9600 C14 H14B 0.9600 C14 H14C 0.9600 C7 H7A 0.9600 C7 H7B 0.9600 C7 H7C 0.9600 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1 O6 0.82 2.13 2.714(2) 127.7 . O7 H7 O1 0.82 2.13 2.878(2) 150.7 1_445 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C17 O2 C3 C2 -153.3(2) C17 O2 C3 C4 33.9(3) O2 C3 C4 C15 -34.0(3) C2 C3 C4 C15 152.40(19) O2 C3 C4 C10 92.1(2) C2 C3 C4 C10 -81.5(2) O2 C3 C4 C5 -163.89(19) C2 C3 C4 C5 22.5(2) C16 C15 C4 C3 45.4(2) C16 C15 C4 C10 -79.4(2) C16 C15 C4 C5 165.99(18) O2 C3 C2 C8 4.7(4) C4 C3 C2 C8 178.0(2) O2 C3 C2 C1 -174.52(19) C4 C3 C2 C1 -1.2(3) C4 C15 C16 O7 178.02(18) C4 C15 C16 C17 -60.2(2) C7 O5 C6 O4 -3.0(3) C7 O5 C6 C5 174.6(2) C11 O3 C5 C6 -174.99(18) C11 O3 C5 C4 54.73(18) C11 O3 C5 C1 -50.98(19) O4 C6 C5 O3 -158.4(2) O5 C6 C5 O3 23.9(3) O4 C6 C5 C4 -34.2(3) O5 C6 C5 C4 148.18(18) O4 C6 C5 C1 81.0(3) O5 C6 C5 C1 -96.7(2) C3 C4 C5 O3 -142.30(16) C15 C4 C5 O3 92.2(2) C10 C4 C5 O3 -29.56(19) C3 C4 C5 C6 89.3(2) C15 C4 C5 C6 -36.2(3) C10 C4 C5 C6 -157.94(18) C3 C4 C5 C1 -32.35(19) C15 C4 C5 C1 -157.88(19) C10 C4 C5 C1 80.39(18) C3 C4 C10 C11 100.4(2) C15 C4 C10 C11 -133.25(19) C5 C4 C10 C11 -6.3(2) C3 C2 C8 O6 178.4(2) C1 C2 C8 O6 -2.5(4) C3 C2 C8 C9 -1.3(4) C1 C2 C8 C9 177.8(2) C3 C2 C1 O1 -140.74(18) C8 C2 C1 O1 40.0(3) C3 C2 C1 C5 -20.6(2) C8 C2 C1 C5 160.1(2) C3 C2 C1 C12 87.8(2) C8 C2 C1 C12 -91.4(3) O3 C5 C1 O1 -97.95(19) C6 C5 C1 O1 27.2(2) C4 C5 C1 O1 152.38(17) O3 C5 C1 C2 142.01(17) C6 C5 C1 C2 -92.9(2) C4 C5 C1 C2 32.3(2) O3 C5 C1 C12 22.81(19) C6 C5 C1 C12 147.94(17) C4 C5 C1 C12 -86.86(17) C14 C12 C1 O1 -105.6(2) C13 C12 C1 O1 18.1(3) C11 C12 C1 O1 132.21(18) C14 C12 C1 C2 24.7(3) C13 C12 C1 C2 148.3(2) C11 C12 C1 C2 -97.5(2) C14 C12 C1 C5 135.4(2) C13 C12 C1 C5 -100.9(2) C11 C12 C1 C5 13.17(19) C3 O2 C17 C18 78.4(2) C3 O2 C17 C19 -163.28(19) C3 O2 C17 C16 -44.3(2) O7 C16 C17 O2 178.16(17) C15 C16 C17 O2 58.3(2) O7 C16 C17 C18 58.7(2) C15 C16 C17 C18 -61.2(2) O7 C16 C17 C19 -69.4(3) C15 C16 C17 C19 170.7(2) C5 O3 C11 C10 -57.52(18) C5 O3 C11 C12 60.20(18) C4 C10 C11 O3 39.3(2) C4 C10 C11 C12 -69.3(2) C14 C12 C11 O3 -167.71(19) C13 C12 C11 O3 70.7(2) C1 C12 C11 O3 -45.17(19) C14 C12 C11 C10 -59.5(3) C13 C12 C11 C10 179.0(2) C1 C12 C11 C10 63.1(2)