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Information card for entry 1519932
Preview
| Coordinates | 1519932.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | TripTpSnCpMe5 |
|---|---|
| Formula | C48.5 H70 Sn |
| Calculated formula | C48.5 H70 Sn |
| SMILES | [Sn]12([c]3([cH]1(C)[cH]2(c(c3C)C)C)C)c1c(c2c(cc(C(C)C)cc2C(C)C)C(C)C)cccc1c1c(cc(cc1C(C)C)C(C)C)C(C)C.CCCCC |
| Title of publication | A nitrogen-base catalyzed generation of organotin(ii) hydride from an organotin trihydride under reductive dihydrogen elimination |
| Authors of publication | Sindlinger, Christian P.; Stasch, Andreas; Bettinger, Holger F.; Wesemann, Lars |
| Journal of publication | Chem. Sci. |
| Year of publication | 2015 |
| Journal volume | 6 |
| Journal issue | 8 |
| Pages of publication | 4737 |
| a | 15.9849 ± 0.0004 Å |
| b | 15.9056 ± 0.0004 Å |
| c | 17.7408 ± 0.0004 Å |
| α | 90° |
| β | 100.754 ± 0.001° |
| γ | 90° |
| Cell volume | 4431.37 ± 0.19 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0448 |
| Residual factor for significantly intense reflections | 0.0303 |
| Weighted residual factors for significantly intense reflections | 0.0705 |
| Weighted residual factors for all reflections included in the refinement | 0.0767 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.011 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176429 (current) | 2016-02-13 | cif/ (antanas@kurmis) Replacing _cod_chemical_formula_sum_orig tag with _cod_original_formula_sum tag in multiple entries since the replaced tag is deprecated according to the COD CIF dictionary. |
1519932.cif |
| 153088 | 2015-08-08 | cif/ Updating files of 1519930, 1519931, 1519932 Original log message: Adding full bibliography for 1519930--1519932.cif. |
1519932.cif |
| 137271 | 2015-05-23 | cif/ Adding structures of 1519930, 1519931, 1519932 via cif-deposit CGI script. |
1519932.cif |
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Users of the data should acknowledge the original authors of the
structural data.