#------------------------------------------------------------------------------ #$Date: 2015-06-30 04:26:02 +0300 (Tue, 30 Jun 2015) $ #$Revision: 139788 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/52/06/1520694.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1520694 loop_ _publ_author_name 'Chen, Ji-Peng' 'He, Wei' 'Yang, Zhen-Yu' 'Yao, Zhu-Jun' _publ_section_title ; Synthesis of Tricyclo[4,3,1,01,5]decane Core of Plumisclerin A Using Pauson--Khand Annulation and SmI2-Mediated Radical Cyclization ; _journal_name_full 'Organic Letters' _journal_page_first 150629152933000 _journal_paper_doi 10.1021/acs.orglett.5b01563 _journal_year 2015 _chemical_formula_moiety 'C33 H27 N3 O13' _chemical_formula_sum 'C33 H27 N3 O13' _chemical_formula_weight 673.57 _chemical_name_systematic ; ? ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2015-05-29 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998) ; _cell_angle_alpha 86.284(4) _cell_angle_beta 86.306(4) _cell_angle_gamma 68.207(3) _cell_formula_units_Z 2 _cell_length_a 11.319(3) _cell_length_b 12.665(3) _cell_length_c 14.597(3) _cell_measurement_reflns_used 5517 _cell_measurement_temperature 133 _cell_measurement_theta_max 27.540 _cell_measurement_theta_min 2.410 _cell_volume 1937.1(8) _computing_cell_refinement 'SAINT v7.68A (Bruker, 2009)' _computing_data_reduction 'SAINT v7.68A (Bruker, 2009)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _diffrn_ambient_temperature 133 _diffrn_measured_fraction_theta_full 0.973 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0412 _diffrn_reflns_av_unetI/netI 0.0676 _diffrn_reflns_laue_measured_fraction_full 0.973 _diffrn_reflns_laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 11856 _diffrn_reflns_point_group_measured_fraction_full 0.973 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.099 _diffrn_reflns_theta_min 1.939 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.091 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.5039 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.0889 before and 0.0539 after correction. The Ratio of minimum to maximum transmission is 0.6758. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.155 _exptl_crystal_description block _exptl_crystal_F_000 700 _exptl_crystal_size_max 0.39 _exptl_crystal_size_mid 0.35 _exptl_crystal_size_min 0.25 _refine_diff_density_max 0.621 _refine_diff_density_min -0.526 _refine_diff_density_rms 0.076 _refine_ls_extinction_coef 0.009(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 470 _refine_ls_number_reflns 6820 _refine_ls_number_restraints 72 _refine_ls_restrained_S_all 1.079 _refine_ls_R_factor_all 0.0917 _refine_ls_R_factor_gt 0.0739 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1480P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2084 _refine_ls_wR_factor_ref 0.2246 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4773 _reflns_number_total 6820 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ol5b01563_si_002.cif _cod_data_source_block mo_dm12136_0m _cod_database_code 1520694 _shelxl_version_number 2014-3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.978 _shelx_estimated_absorpt_t_min 0.966 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints N1 \\sim O8 \\sim O9 \\sim N1' \\sim O8' \\sim O9': within 1.7A with sigma of 0.01 and sigma for terminal atoms of 0.02 N2 \\sim O11: within 1.7A with sigma of 0.001 and sigma for terminal atoms of 0.002 3. Others Fixed Sof: N1(0.5) O8(0.5) O9(0.5) N1'(0.5) O8'(0.5) O9'(0.5) 4.a Ternary CH refined with riding coordinates: C4(H4), C6(H6), C9(H9), C11(H11) 4.b Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C3(H3A,H3B), C7(H7A,H7B), C12(H12A,H12B) 4.c Me refined with riding coordinates: C10(H10A,H10B,H10C) 4.d Aromatic/amide H refined with riding coordinates: C15(H15), C16(H16), C18(H18), C19(H19), C22(H22), C23(H23), C25(H25), C26(H26), C29(H29), C30(H30), C32(H32), C33(H33) ; _shelx_res_file ; TITL mo_dm12136_0m in P-1 CELL 0.71073 11.3194 12.6649 14.5968 86.284 86.306 68.207 ZERR 2 0.0026 0.0029 0.0033 0.004 0.004 0.003 LATT 1 SFAC C H N O UNIT 66 54 6 26 SIMU 0.01 0.02 1.7 N1 > O9' SIMU 0.001 0.002 1.7 N2 O11 L.S. 12 PLAN 20 SIZE 0.25 0.35 0.39 TEMP -140.15 BOND $h conf wpdb -1 fmap 2 acta MORE -1 OMIT -3 50.2 OMIT 0 1 2 OMIT -1 5 3 OMIT -2 2 6 OMIT 0 3 2 OMIT -3 5 0 OMIT 0 2 1 OMIT -2 4 1 OMIT 0 8 1 OMIT 0 4 0 OMIT 4 2 2 OMIT 3 2 0 REM REM REM WGHT 0.148000 EXTI 0.008526 FVAR 2.11734 N2 3 -0.107589 1.116912 1.445470 11.00000 0.10253 0.06747 = 0.07029 -0.02006 0.03304 -0.00322 N3 3 0.016456 0.299010 0.795936 11.00000 0.04297 0.02763 = 0.05369 -0.01431 0.00348 -0.02003 O1 4 0.638673 0.592311 0.978242 11.00000 0.01405 0.03186 = 0.06931 -0.00124 -0.00361 -0.00234 O2 4 0.471637 1.169349 0.813928 11.00000 0.06235 0.04753 = 0.04255 0.00243 -0.01210 -0.04125 O3 4 0.380758 1.042500 0.798497 11.00000 0.02729 0.03491 = 0.03491 -0.00898 0.00440 -0.02082 O4 4 0.311517 1.066120 1.108558 11.00000 0.02073 0.02951 = 0.05270 -0.01550 0.00283 -0.01489 O5 4 0.237060 0.926845 1.090602 11.00000 0.01645 0.02273 = 0.03415 -0.01123 0.00224 -0.00924 O6 4 -0.042326 0.761853 0.982295 11.00000 0.01588 0.02551 = 0.05359 -0.01657 0.00632 -0.00937 O7 4 0.164846 0.697974 0.934871 11.00000 0.01332 0.01895 = 0.04096 -0.01024 -0.00107 -0.00813 PART 1 N1 3 0.458617 1.164121 0.373018 10.50000 0.08894 0.11493 = 0.04933 -0.00751 0.01675 -0.04756 O8 4 0.393164 1.132891 0.331470 10.50000 0.05874 0.09968 = 0.03772 -0.01214 -0.00472 -0.02315 O9 4 0.544359 1.193237 0.339894 10.50000 0.10673 0.11900 = 0.04776 -0.01226 0.02654 -0.07570 PART 0 PART 2 N1' 3 0.442065 1.196494 0.380117 10.50000 0.09613 0.13724 = 0.04349 -0.01798 0.00292 -0.08055 O8' 4 0.345624 1.202508 0.333774 10.50000 0.11354 0.20660 = 0.06548 -0.00345 -0.01886 -0.08785 O9' 4 0.511286 1.240806 0.343911 10.50000 0.13108 0.11653 = 0.05326 -0.00938 0.01585 -0.08020 PART 0 O10 4 -0.160100 1.051432 1.468934 11.00000 0.06719 0.11665 = 0.06149 -0.00083 0.02175 -0.02602 O11 4 -0.126227 1.204437 1.483358 11.00000 0.12816 0.08141 = 0.08104 -0.02130 0.04244 -0.00320 O12 4 -0.085968 0.287418 0.804101 11.00000 0.04444 0.03984 = 0.08735 -0.02205 0.00269 -0.02939 O13 4 0.113084 0.230274 0.759362 11.00000 0.05647 0.03473 = 0.07286 -0.02964 0.01972 -0.02394 C1 1 0.311547 0.942446 0.920105 11.00000 0.01218 0.02126 = 0.03163 -0.00904 0.00074 -0.00718 C2 1 0.168687 0.993116 0.900435 11.00000 0.01498 0.01918 = 0.03719 -0.00623 -0.00171 -0.00620 AFIX 23 H2A 2 0.157815 1.029889 0.837976 11.00000 -1.20000 H2B 2 0.123734 1.052410 0.944853 11.00000 -1.20000 AFIX 0 C3 1 0.108005 0.901500 0.907441 11.00000 0.01090 0.02223 = 0.04307 -0.00558 -0.00430 -0.00690 AFIX 23 H3A 2 0.018103 0.936980 0.929730 11.00000 -1.20000 H3B 2 0.108318 0.874573 0.845217 11.00000 -1.20000 AFIX 0 C4 1 0.175264 0.799257 0.970923 11.00000 0.01129 0.01623 = 0.03392 -0.01066 0.00211 -0.00580 AFIX 13 H4 2 0.135313 0.811708 1.034405 11.00000 -1.20000 AFIX 0 C5 1 0.316500 0.778965 0.972740 11.00000 0.01222 0.01722 = 0.03417 -0.00857 0.00083 -0.00629 C6 1 0.369744 0.820047 0.882156 11.00000 0.01484 0.02314 = 0.03040 -0.01035 0.00189 -0.00734 AFIX 13 H6 2 0.330316 0.810718 0.825359 11.00000 -1.20000 AFIX 0 C7 1 0.514582 0.754721 0.883893 11.00000 0.01305 0.02805 = 0.04152 -0.01230 0.00549 -0.00578 AFIX 23 H7A 2 0.548461 0.722244 0.823484 11.00000 -1.20000 H7B 2 0.558121 0.806080 0.898395 11.00000 -1.20000 AFIX 0 C8 1 0.535379 0.660751 0.957783 11.00000 0.01461 0.01996 = 0.04349 -0.01174 -0.00025 -0.00556 C9 1 0.409425 0.662133 1.003673 11.00000 0.01290 0.01872 = 0.03972 -0.00916 -0.00147 -0.00555 AFIX 13 H9 2 0.385976 0.603671 0.974595 11.00000 -1.20000 AFIX 0 C10 1 0.414310 0.634581 1.106111 11.00000 0.02407 0.02499 = 0.04423 -0.00535 -0.00290 -0.00741 AFIX 33 H10A 2 0.476941 0.557768 1.117870 11.00000 -1.50000 H10B 2 0.438951 0.689759 1.136272 11.00000 -1.50000 H10C 2 0.330203 0.638370 1.130541 11.00000 -1.50000 AFIX 0 C11 1 0.328823 0.883081 1.015235 11.00000 0.00929 0.01927 = 0.03466 -0.01049 -0.00041 -0.00563 AFIX 13 H11 2 0.417488 0.864450 1.035117 11.00000 -1.20000 AFIX 0 C12 1 0.374959 1.027894 0.897113 11.00000 0.01727 0.02321 = 0.03573 -0.00866 -0.00052 -0.01125 AFIX 23 H12A 2 0.324857 1.101314 0.925031 11.00000 -1.20000 H12B 2 0.461728 0.999310 0.920915 11.00000 -1.20000 AFIX 0 C13 1 0.433183 1.117148 0.765313 11.00000 0.02440 0.02742 = 0.04266 -0.00410 -0.00393 -0.01356 C14 1 0.435005 1.130824 0.663781 11.00000 0.03462 0.04079 = 0.04143 -0.00814 0.00408 -0.02107 C15 1 0.355127 1.100218 0.610432 11.00000 0.05551 0.09079 = 0.03793 -0.00811 0.00455 -0.05005 AFIX 43 H15 2 0.297594 1.068319 0.639271 11.00000 -1.20000 AFIX 0 C16 1 0.359858 1.116071 0.517752 11.00000 0.07517 0.13311 = 0.04516 -0.01720 -0.00003 -0.07310 AFIX 43 H16 2 0.307298 1.094216 0.480916 11.00000 -1.20000 AFIX 0 C17 1 0.443213 1.164969 0.477751 11.00000 0.07303 0.10671 = 0.04064 -0.00735 0.00997 -0.05615 C18 1 0.522267 1.195341 0.527821 11.00000 0.06342 0.08796 = 0.05231 -0.00102 0.00696 -0.05337 AFIX 43 H18 2 0.579869 1.226797 0.498438 11.00000 -1.20000 AFIX 0 C19 1 0.516717 1.179533 0.620898 11.00000 0.04956 0.06788 = 0.04597 -0.00494 -0.00069 -0.04086 AFIX 43 H19 2 0.569453 1.202131 0.656978 11.00000 -1.20000 AFIX 0 C20 1 0.244414 1.014134 1.134323 11.00000 0.01316 0.01881 = 0.03693 -0.00807 -0.00650 -0.00129 C21 1 0.157131 1.038236 1.217879 11.00000 0.02163 0.02521 = 0.03151 -0.00564 -0.00663 -0.00513 C22 1 0.128554 1.140976 1.259548 11.00000 0.04092 0.02875 = 0.04234 -0.01209 -0.00176 -0.00839 AFIX 43 H22 2 0.167677 1.192827 1.237309 11.00000 -1.20000 AFIX 0 C23 1 0.040516 1.166928 1.335381 11.00000 0.06570 0.03827 = 0.05415 -0.02481 0.00817 -0.00437 AFIX 43 H23 2 0.019044 1.236769 1.364835 11.00000 -1.20000 AFIX 0 C24 1 -0.013655 1.089870 1.365989 11.00000 0.04616 0.04513 = 0.03746 -0.00320 0.00821 -0.00119 C25 1 0.016648 0.987347 1.327420 11.00000 0.04167 0.04991 = 0.03471 0.00150 -0.00125 -0.01546 AFIX 43 H25 2 -0.020602 0.934749 1.351292 11.00000 -1.20000 AFIX 0 C26 1 0.102545 0.961497 1.252981 11.00000 0.02788 0.03724 = 0.03574 -0.00489 -0.00170 -0.01469 AFIX 43 H26 2 0.124574 0.890368 1.225444 11.00000 -1.20000 AFIX 0 C27 1 0.048440 0.692531 0.943975 11.00000 0.01434 0.01875 = 0.03142 -0.00485 -0.00265 -0.00712 C28 1 0.044305 0.589133 0.903422 11.00000 0.01541 0.01803 = 0.03433 -0.00259 -0.00275 -0.00945 C29 1 -0.075343 0.582323 0.896958 11.00000 0.01610 0.02131 = 0.03884 -0.00632 -0.00046 -0.00614 AFIX 43 H29 2 -0.150032 0.642978 0.916640 11.00000 -1.20000 AFIX 0 C30 1 -0.084633 0.486817 0.861752 11.00000 0.02251 0.02755 = 0.04410 -0.00877 -0.00073 -0.01581 AFIX 43 H30 2 -0.165082 0.480508 0.857212 11.00000 -1.20000 AFIX 0 C31 1 0.026677 0.400841 0.833377 11.00000 0.03005 0.02205 = 0.03864 -0.00723 0.00033 -0.01584 C32 1 0.145670 0.404687 0.840527 11.00000 0.02343 0.02476 = 0.04921 -0.01016 0.00335 -0.00797 AFIX 43 H32 2 0.220178 0.342920 0.822264 11.00000 -1.20000 AFIX 0 C33 1 0.153945 0.500277 0.874801 11.00000 0.01568 0.02237 = 0.04342 -0.00833 0.00009 -0.00658 AFIX 43 H33 2 0.234912 0.505670 0.878956 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_dm12136_0m in P-1 REM R1 = 0.0739 for 4773 Fo > 4sig(Fo) and 0.0917 for all 6820 data REM 470 parameters refined using 72 restraints END WGHT 0.1474 0.0000 REM Highest difference peak 0.621, deepest hole -0.526, 1-sigma level 0.076 Q1 1 -0.0431 1.2154 1.4991 11.00000 0.05 0.59 Q2 1 -0.1885 1.2333 1.4401 11.00000 0.05 0.34 Q3 1 0.3573 0.7176 0.9837 11.00000 0.05 0.34 Q4 1 0.0545 1.0984 1.3813 11.00000 0.05 0.32 Q5 1 -0.0737 0.7859 1.0480 11.00000 0.05 0.30 Q6 1 0.4441 0.9991 0.8293 11.00000 0.05 0.30 Q7 1 -0.0369 1.1479 1.4602 11.00000 0.05 0.29 Q8 1 0.1003 0.2208 0.8372 11.00000 0.05 0.29 Q9 1 0.4804 1.0854 0.8643 11.00000 0.05 0.29 Q10 1 0.1823 0.9390 1.1687 11.00000 0.05 0.29 Q11 1 0.5543 0.6533 0.9058 11.00000 0.05 0.29 Q12 1 0.3475 1.0610 1.0294 11.00000 0.05 0.29 Q13 1 0.1531 1.1783 0.9063 11.00000 0.05 0.29 Q14 1 0.2060 0.6975 0.8646 11.00000 0.05 0.27 Q15 1 -0.0185 0.7617 0.9101 11.00000 0.05 0.27 Q16 1 0.0664 0.2883 0.7238 11.00000 0.05 0.26 Q17 1 0.3187 1.1180 0.7722 11.00000 0.05 0.26 Q18 1 0.0003 1.0728 1.5035 11.00000 0.05 0.26 Q19 1 -0.1452 0.6345 0.9575 11.00000 0.05 0.25 Q20 1 0.5262 1.0858 0.7006 11.00000 0.05 0.25 ; _shelx_res_checksum 31602 _shelx_hkl_file ; -13 -8 1 538.86 60.50 -13 -8 2 92.27 48.50 -13 -7 1 247.25 44.50 -13 -7 2 50.44 41.00 -13 -7 3 11.23 25.04 -13 -6 1 465.03 67.00 -13 -6 2 301.93 49.00 -13 -6 3 66.46 37.00 -13 -5 1 7.91 34.00 -13 -5 2 40.34 36.00 -13 -5 3 42.87 33.00 -13 -4 1 454.82 63.00 -13 -4 2 3.23 30.00 -13 -4 3 292.92 52.00 -13 -3 1 223.40 47.00 -13 -3 2 9.05 32.00 -13 -2 1 544.95 68.00 -12 -11 1 20.60 30.01 -12 -10 1 370.34 58.00 -12 -10 2 444.00 101.00 -12 -10 3 31.09 32.50 -12 -9 1 5.51 25.91 -12 -9 2 20.78 26.17 -12 -9 3 0.01 25.23 -12 -9 4 1.40 24.99 -12 -9 5 17.71 25.91 -12 -8 1 100.66 47.00 -12 -8 2 7.59 23.92 -12 -8 3 10.26 31.00 -12 -8 4 114.21 27.33 -12 -8 5 74.89 28.47 -12 -7 1 165.29 26.76 -12 -7 2 33.98 25.50 -12 -7 3 194.08 62.50 -12 -7 4 667.13 56.58 -12 -7 5 1847.84 96.33 -12 -7 6 120.51 27.55 -12 -6 1 2798.88 133.64 -12 -6 2 116.57 26.16 -12 -6 3 9.25 22.91 -12 -6 4 37.92 24.01 -12 -6 5 120.65 26.87 -12 -6 6 0.99 22.27 -12 -5 1 286.67 46.00 -12 -5 2 13.58 22.63 -12 -5 3 39.04 23.68 -12 -5 4 14.50 21.56 -12 -5 5 0.15 21.92 -12 -5 6 37.79 22.97 -12 -4 1 284.44 41.00 -12 -4 2 311.74 45.00 -12 -4 3 19.39 30.00 -12 -4 4 50.00 33.00 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34.33 1 4 10 0.00 19.41 1 4 11 594.73 42.03 1 4 12 8147.64 284.32 1 4 13 5201.36 217.06 1 4 14 51.95 25.71 1 4 15 328.26 60.00 1 4 16 283.63 67.00 1 4 17 25.78 52.00 1 5 0 4286.88 274.00 1 5 1 679.94 22.33 1 5 2 2259.77 297.00 1 5 3 57.24 35.08 1 5 4 2266.25 102.94 1 5 5 8509.16 270.36 1 5 6 120.05 28.83 1 5 7 31.13 18.00 1 5 8 1.74 18.00 1 5 9 249.11 20.53 1 5 10 150.22 37.00 1 5 11 505.19 42.76 1 5 1211497.98 437.45 1 5 13 3728.39 130.65 1 5 14 124.42 31.93 1 5 15 380.90 59.00 1 5 16 624.84 98.00 1 6 0 8490.45 182.02 1 6 1 3315.13 99.98 1 6 2 2417.71 124.79 1 6 312253.42 831.78 1 6 415985.01 877.50 1 6 5 3016.34 121.30 1 6 6 512.80 38.58 1 6 7 639.27 54.00 1 6 8 261.38 43.00 1 6 9 30.06 22.00 1 6 10 122.10 42.50 1 6 11 3877.09 152.23 1 6 12 542.67 35.73 1 6 13 12.94 27.63 1 6 14 16.31 27.39 1 6 15 5.19 28.58 1 6 16 325.49 60.00 1 7 0 5052.39 123.71 1 7 1 530.83 34.35 1 7 2 583.40 45.22 1 7 3 3833.54 123.35 1 7 4 1711.06 69.91 1 7 5 334.46 57.00 1 7 6 3456.95 113.90 1 7 7 4806.84 198.74 1 7 8 2787.22 172.00 1 7 9 1549.24 78.00 1 7 10 11.70 32.00 1 7 11 68.87 26.90 1 7 12 310.77 42.50 1 7 13 23.44 26.43 1 7 14 0.82 26.43 1 7 15 68.03 31.18 1 8 0 2189.31 71.01 1 8 1 1454.97 59.22 1 8 2 1808.04 59.46 1 8 3 146.61 22.31 1 8 4 1959.43 81.58 1 8 5 136.40 22.00 1 8 6 1225.09 111.00 1 8 7 16.25 16.50 1 8 8 9.32 16.08 1 8 9 245.94 57.00 1 8 10 298.31 41.00 1 8 11 330.73 58.00 1 8 12 59.96 27.86 1 8 13 1205.27 71.04 1 8 14 312.92 36.44 1 8 15 99.52 31.32 1 9 0 2551.18 89.66 1 9 1 698.49 42.04 1 9 2 122.12 17.51 1 9 3 837.94 43.61 1 9 4 600.92 48.95 1 9 5 817.29 78.00 1 9 6 38.86 16.52 1 9 7 93.77 18.22 1 9 8 90.16 24.50 1 9 9 72.11 33.00 1 9 10 2.68 30.00 1 9 11 94.05 35.00 1 9 12 173.47 42.00 1 9 13 151.66 32.32 1 9 14 30.05 29.29 1 10 0 1068.32 51.70 1 10 1 1544.86 57.02 1 10 2 355.79 37.68 1 10 3 8.39 13.61 1 10 4 1.15 14.04 1 10 5 1.06 17.64 1 10 6 670.89 52.08 1 10 7 54.63 20.64 1 10 8 199.33 24.02 1 10 9 44.55 31.00 1 10 10 64.61 35.00 1 10 11 20.50 36.00 1 10 12 188.05 45.00 1 10 13 40.43 60.00 1 11 0 60.93 30.00 1 11 1 46.51 17.63 1 11 2 3.16 15.09 1 11 3 5.65 15.77 1 11 4 0.40 14.81 1 11 5 176.41 31.00 1 11 6 591.35 64.50 1 11 7 6.17 19.21 1 11 8 12.26 19.36 1 11 9 12.51 32.00 1 11 10 38.47 37.00 1 11 11 0.26 36.00 1 12 0 30.61 28.10 1 12 1 270.09 25.78 1 12 2 863.05 49.48 1 12 3 273.61 46.35 1 12 4 312.94 33.28 1 12 5 313.87 65.50 1 12 6 12.07 21.18 1 12 7 139.97 25.71 1 12 8 1065.90 65.20 1 12 9 640.29 78.00 1 12 10 48.72 40.00 1 13 0 0.31 20.30 1 13 1 15.54 20.55 1 13 2 175.97 23.25 1 13 3 45.14 20.01 1 13 4 310.89 41.72 1 13 5 632.20 56.22 1 13 6 17.71 22.78 1 13 7 48.91 24.02 1 13 8 916.72 68.20 1 14 0 84.17 24.41 1 14 1 37.27 26.54 1 14 2 1231.75 83.30 1 14 3 1761.55 73.98 1 14 4 525.75 48.20 1 14 5 41.01 26.17 2 -13 0 137.68 32.16 2 -12 0 56.06 27.14 2 -12 1 704.52 63.43 2 -12 2 883.14 64.63 2 -12 3 43.56 31.00 2 -12 4 148.93 32.00 2 -12 5 79.49 29.68 2 -12 6 794.19 108.00 2 -11 0 1455.55 69.76 2 -11 1 2047.94 105.72 2 -11 2 647.28 52.58 2 -11 3 100.21 25.88 2 -11 4 0.42 24.21 2 -11 5 567.82 51.98 2 -11 6 196.30 53.00 2 -11 7 305.07 59.00 2 -11 8 180.59 62.00 2 -10 0 8.34 15.51 2 -10 1 209.65 40.50 2 -10 2 255.45 28.05 2 -10 3 18.16 24.50 2 -10 4 230.43 29.53 2 -10 5 1504.65 93.00 2 -10 6 251.62 70.50 2 -10 7 7.03 47.00 2 -10 8 0.63 48.00 2 -10 9 221.25 60.00 2 -10 10 34.13 56.00 2 -9 0 639.36 45.53 2 -9 1 1622.36 55.53 2 -9 2 2339.82 88.71 2 -9 3 399.85 103.00 2 -9 4 96.05 21.46 2 -9 5 87.31 23.46 2 -9 6 70.64 22.38 2 -9 7 5.97 19.39 2 -9 8 106.79 46.00 2 -9 9 0.17 45.00 2 -9 10 0.12 49.00 2 -9 11 14.28 52.00 2 -8 0 20.04 13.04 2 -8 1 444.35 31.90 2 -8 2 10.65 12.76 2 -8 3 103.42 26.00 2 -8 4 1139.47 48.71 2 -8 5 2085.12 77.17 2 -8 6 2415.17 82.15 2 -8 7 638.39 38.05 2 -8 8 176.21 47.00 2 -8 9 13.48 41.00 2 -8 10 0.62 43.00 2 -8 11 0.55 46.00 2 -8 12 391.05 68.00 2 -7 0 273.01 53.00 2 -7 1 3584.15 98.44 2 -7 2 994.97 55.21 2 -7 3 18.25 14.98 2 -7 4 69.23 13.12 2 -7 5 0.89 11.72 2 -7 6 123.73 18.02 2 -7 7 86.28 19.64 2 -7 8 137.16 19.01 2 -7 9 532.91 73.00 2 -7 10 103.92 23.92 2 -7 11 334.40 60.00 2 -7 12 67.86 52.00 2 -7 13 0.51 53.00 2 -6 0 3480.12 184.08 2 -6 1 819.15 63.64 2 -6 2 248.25 23.62 2 -6 3 33.05 15.29 2 -6 4 0.56 7.79 2 -6 5 116.55 35.00 2 -6 6 714.38 37.27 2 -6 7 1510.74 50.05 2 -6 8 2190.24 113.39 2 -6 9 535.33 55.00 2 -6 10 179.59 48.00 2 -6 11 88.72 45.00 2 -6 12 1.28 46.00 2 -6 13 25.32 50.00 2 -6 14 0.05 55.00 2 -5 0 135.70 33.63 2 -5 1 1023.89 30.00 2 -5 2 51.05 12.56 2 -5 3 80.08 13.59 2 -5 4 2533.03 96.02 2 -5 5 2555.56 139.00 2 -5 6 150.60 14.91 2 -5 7 1136.44 104.00 2 -5 8 222.31 34.00 2 -5 9 75.46 38.00 2 -5 10 288.01 47.00 2 -5 11 66.51 41.00 2 -5 12 582.58 91.00 2 -5 13 1094.03 109.00 2 -5 14 76.31 56.00 2 -5 15 0.46 58.00 2 -4 014314.84 457.27 2 -4 1 4500.16 220.50 2 -4 2 29.17 17.23 2 -4 3 1288.37 44.45 2 -4 4 3905.44 161.87 2 -4 5 2511.96 67.15 2 -4 6 4338.59 231.00 2 -4 7 355.53 37.00 2 -4 8 841.47 38.00 2 -4 9 258.54 27.00 2 -4 10 195.37 40.00 2 -4 11 341.16 53.00 2 -4 12 45.28 42.00 2 -4 13 55.09 47.00 2 -4 14 112.16 55.00 2 -4 15 5.07 57.00 2 -4 16 190.53 63.00 2 -3 023670.25 948.00 2 -3 1 5879.17 160.00 2 -3 2 1573.48 123.00 2 -3 3 5489.49 328.00 2 -3 4 4679.57 137.00 2 -3 5 1393.22 109.00 2 -3 8 916.53 44.00 2 -3 9 1722.51 89.00 2 -3 11 395.84 47.00 2 -3 12 53.14 41.00 2 -3 13 27.01 45.00 2 -3 14 148.29 54.00 2 -3 15 0.00 51.00 2 -3 16 35.86 56.00 2 -2 074623.48 4814.00 2 -2 1 536.33 24.00 2 -2 2 3886.58 229.00 2 -2 327731.91 1032.00 2 -2 4 3658.62 301.00 2 -2 5 942.09 61.00 2 -2 6 2571.25 267.00 2 -2 7 2323.73 135.00 2 -2 8 101.88 26.00 2 -2 9 1091.96 65.00 2 -2 10 1327.41 66.00 2 -2 12 1059.28 106.00 2 -2 13 70.77 43.00 2 -2 14 490.91 64.00 2 -2 15 63.20 54.00 2 -2 16 0.03 51.00 2 -1 015434.99 184.00 2 -1 146997.13 2276.56 2 -1 251076.69 2936.00 2 -1 353459.15 3058.00 2 -1 411832.28 453.00 2 -1 5 1473.83 68.00 2 -1 6 1004.56 35.50 2 -1 7 1819.47 90.00 2 -1 8 639.91 42.04 2 -1 9 1096.18 96.50 2 -1 10 615.83 49.00 2 -1 11 55.87 18.00 2 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27.50 2 2 9 15.47 17.51 2 2 10 459.76 65.50 2 2 11 360.78 51.00 2 2 12 2485.79 256.00 2 2 13 532.87 48.94 2 2 14 333.38 55.00 2 2 15 906.76 110.00 2 2 16 328.87 73.00 2 2 17 287.29 73.00 2 3 0 3548.81 29.00 2 3 1 5499.07 425.00 2 3 3 7103.43 197.00 2 3 425828.60 843.22 2 3 5 54.62 20.16 2 3 6 5852.58 280.29 2 3 7 760.86 49.67 2 3 8 3046.03 111.94 2 3 9 5916.41 215.92 2 3 10 1055.07 59.37 2 3 11 1547.84 94.00 2 3 12 240.40 89.50 2 3 13 81.10 50.00 2 3 14 1904.61 146.00 2 3 15 561.87 93.00 2 3 16 385.48 62.00 2 3 17 293.61 70.00 2 4 0 9460.97 530.95 2 4 1 2406.80 115.00 2 4 4 0.27 15.00 2 4 5 382.92 70.00 2 4 611354.30 281.83 2 4 710639.24 380.69 2 4 8 6747.01 324.00 2 4 9 6.51 16.34 2 4 10 17.91 18.74 2 4 11 40.33 21.61 2 4 12 980.86 70.30 2 4 13 82.98 30.03 2 4 14 2223.64 96.96 2 4 15 55.29 51.00 2 4 16 20.06 52.00 2 4 17 1.27 47.00 2 5 0 9029.39 424.00 2 5 1 660.46 13.31 2 5 2 460.64 12.00 2 5 418533.26 1005.00 2 5 5 3178.69 141.00 2 5 6 75.97 20.00 2 5 7 1405.41 89.00 2 5 8 2993.02 91.14 2 5 9 4102.22 171.05 2 5 10 1641.66 81.17 2 5 11 3444.10 112.97 2 5 12 268.61 31.18 2 5 13 24.73 29.30 2 5 14 715.27 61.03 2 5 15 382.60 59.00 2 5 16 67.67 51.00 2 6 0 471.87 39.62 2 6 1 6807.94 139.46 2 6 2 46.94 13.24 2 6 3 9479.56 323.76 2 6 4 4975.15 787.50 2 6 5 1872.80 93.40 2 6 6 963.30 51.00 2 6 7 74.42 20.00 2 6 8 38.28 27.00 2 6 9 2.98 18.25 2 6 10 61.48 20.36 2 6 11 2354.55 115.48 2 6 12 96.51 56.50 2 6 13 137.62 30.46 2 6 14 180.30 33.03 2 6 15 74.92 30.25 2 6 16 20.37 46.00 2 7 0 8984.54 332.29 2 7 1 6206.79 154.56 2 7 2 116.56 10.87 2 7 3 339.70 29.07 2 7 4 231.15 56.00 2 7 5 270.64 65.00 2 7 6 290.62 36.52 2 7 7 140.38 23.00 2 7 8 432.95 58.00 2 7 9 377.95 50.00 2 7 10 7.58 21.14 2 7 11 941.44 54.67 2 7 12 208.67 30.31 2 7 13 722.73 57.50 2 7 14 20.02 27.76 2 7 15 159.25 32.87 2 8 0 1898.83 52.50 2 8 114032.08 419.06 2 8 2 4452.46 147.24 2 8 3 1064.89 45.25 2 8 4 16.92 19.00 2 8 5 1165.12 80.00 2 8 6 0.71 20.00 2 8 7 96.40 29.00 2 8 8 183.76 39.50 2 8 9 58.41 31.00 2 8 10 344.69 40.00 2 8 11 585.02 48.65 2 8 12 2253.25 103.76 2 8 13 56.61 28.89 2 8 14 18.83 28.18 2 8 15 47.85 31.32 2 9 0 566.92 36.47 2 9 1 224.51 22.14 2 9 2 3.79 11.56 2 9 3 187.74 27.95 2 9 4 318.21 27.00 2 9 5 1154.38 107.00 2 9 6 308.87 72.00 2 9 7 613.74 44.92 2 9 8 1155.28 63.93 2 9 9 3.45 17.64 2 9 10 22.17 28.00 2 9 11 647.82 68.00 2 9 12 115.61 29.60 2 9 13 17.17 27.05 2 9 14 0.09 27.76 2 10 0 5.18 14.77 2 10 1 21.69 17.25 2 10 2 156.06 18.24 2 10 3 322.46 25.01 2 10 4 23.39 15.50 2 10 5 169.18 34.00 2 10 6 115.37 23.50 2 10 7 1029.04 67.34 2 10 8 1654.59 79.86 2 10 9 12.40 18.94 2 10 10 16.33 30.00 2 10 11 218.48 45.00 2 10 12 4.94 27.47 2 10 13 41.67 29.29 2 11 0 1302.58 53.03 2 11 1 918.95 49.44 2 11 2 408.09 43.75 2 11 3 174.98 18.01 2 11 4 522.83 40.19 2 11 5 163.71 27.87 2 11 6 3.79 19.05 2 11 7 748.62 53.78 2 11 8 624.84 54.94 2 11 9 13.82 21.00 2 11 10 201.82 41.00 2 11 11 411.15 66.00 2 11 12 419.96 72.00 2 12 0 963.92 57.06 2 12 1 1133.97 57.76 2 12 2 369.87 43.53 2 12 3 9.09 18.21 2 12 4 157.94 22.10 2 12 5 372.42 45.50 2 12 6 62.15 24.33 2 12 7 189.56 28.76 2 12 8 49.60 22.06 2 12 9 91.22 26.17 2 12 10 2.77 36.00 2 13 0 3.54 20.02 2 13 1 301.12 26.72 2 13 2 196.01 32.39 2 13 3 178.19 32.83 2 13 4 204.43 25.61 2 13 5 6.38 23.33 2 13 6 123.00 28.58 2 13 7 378.81 62.50 2 13 8 68.56 26.34 2 13 9 224.64 30.73 2 14 0 514.46 64.35 2 14 1 26.82 22.12 2 14 2 492.22 85.50 2 14 3 8.94 20.84 2 14 4 64.45 27.47 2 14 5 5.41 24.39 2 14 6 103.92 28.18 3 -12 0 422.51 53.00 3 -12 1 531.08 56.43 3 -12 2 26.05 28.80 3 -12 3 1.32 27.54 3 -11 0 749.56 60.07 3 -11 1 2408.18 103.07 3 -11 2 1514.77 75.65 3 -11 3 87.28 30.98 3 -11 4 3.44 26.45 3 -11 5 77.94 29.60 3 -11 6 29.00 28.16 3 -11 7 14.32 57.00 3 -10 0 227.22 33.45 3 -10 1 37.46 23.76 3 -10 2 450.37 51.96 3 -10 3 7.82 23.78 3 -10 4 294.86 31.62 3 -10 5 1003.22 84.50 3 -10 6 65.49 27.11 3 -10 7 4.06 49.00 3 -10 8 769.65 108.00 3 -10 9 549.30 98.00 3 -9 0 0.58 19.46 3 -9 1 545.28 49.01 3 -9 2 525.99 31.44 3 -9 3 12.60 23.27 3 -9 4 116.18 24.79 3 -9 5 975.31 63.86 3 -9 6 531.19 93.50 3 -9 7 37.33 21.85 3 -9 8 15.18 47.00 3 -9 9 0.37 49.00 3 -9 10 61.60 54.00 3 -8 0 39.44 12.80 3 -8 1 591.12 33.96 3 -8 2 162.19 26.00 3 -8 3 556.51 50.91 3 -8 4 431.36 53.00 3 -8 5 538.81 43.45 3 -8 6 1367.70 70.61 3 -8 7 72.15 21.74 3 -8 8 20.78 43.00 3 -8 9 7.18 45.00 3 -8 10 62.36 51.00 3 -8 11 24.76 50.00 3 -8 12 86.42 56.00 3 -7 0 507.60 42.29 3 -7 1 1972.29 86.26 3 -7 2 73.32 20.18 3 -7 3 133.87 18.87 3 -7 4 54.43 18.63 3 -7 5 743.83 48.65 3 -7 6 406.09 43.00 3 -7 7 378.22 78.50 3 -7 8 17.11 16.90 3 -7 9 292.66 51.00 3 -7 10 142.89 47.00 3 -7 11 8.86 45.00 3 -7 12 167.36 57.00 3 -7 13 124.47 62.00 3 -6 0 2087.37 113.00 3 -6 1 773.68 55.00 3 -6 2 0.76 15.00 3 -6 3 97.20 21.00 3 -6 4 59.79 19.00 3 -6 5 595.89 53.00 3 -6 6 14.64 16.00 3 -6 7 13.73 12.24 3 -6 8 73.20 13.92 3 -6 9 82.76 40.00 3 -6 10 0.94 39.00 3 -6 11 0.17 42.00 3 -6 12 14.33 48.00 3 -6 13 1.26 51.00 3 -6 14 6.27 54.00 3 -5 1 7427.54 350.00 3 -5 2 8282.25 390.00 3 -5 3 8.02 11.65 3 -5 4 109.10 14.85 3 -5 5 268.39 36.00 3 -5 7 363.25 33.00 3 -5 8 1234.38 83.00 3 -5 9 2072.64 175.00 3 -5 10 193.04 44.00 3 -5 11 3.93 40.00 3 -5 12 9.81 44.00 3 -5 13 5.96 48.00 3 -5 14 7.71 54.00 3 -4 0 7175.42 264.10 3 -4 110242.80 462.00 3 -4 2 1286.02 66.00 3 -4 3 482.12 44.00 3 -4 4 1892.16 100.00 3 -4 5 96.56 9.60 3 -4 6 1765.71 105.00 3 -4 7 4033.79 189.00 3 -4 8 708.92 58.00 3 -4 9 3.16 15.00 3 -4 10 3.01 35.00 3 -4 11 149.93 48.00 3 -4 12 12.47 39.00 3 -4 13 37.11 47.00 3 -4 14 0.97 49.00 3 -4 15 3.61 56.00 3 -3 0 6097.36 322.00 3 -3 1 109.11 24.00 3 -3 2 3.66 9.06 3 -3 3 613.12 32.14 3 -3 4 1869.87 243.00 3 -3 5 738.99 47.33 3 -3 6 207.63 22.20 3 -3 7 3907.09 190.00 3 -3 8 445.06 35.00 3 -3 9 92.21 30.00 3 -3 10 56.27 16.99 3 -3 11 4.27 37.00 3 -3 12 4.96 43.00 3 -3 13 437.08 55.00 3 -3 14 60.92 52.00 3 -3 15 79.14 58.00 3 -3 16 7.75 55.00 3 -2 1 4322.31 231.00 3 -2 2 1097.30 43.00 3 -2 311377.23 876.00 3 -2 4 0.10 14.40 3 -2 5 3649.69 124.62 3 -2 6 356.40 31.44 3 -2 7 3672.09 139.35 3 -2 8 910.95 52.62 3 -2 9 722.16 40.50 3 -2 10 75.40 28.50 3 -2 11 403.00 47.00 3 -2 12 1216.63 126.00 3 -2 13 26.66 48.00 3 -2 14 43.91 48.00 3 -2 15 0.09 53.00 3 -2 16 0.75 54.00 3 -1 0 2958.41 160.00 3 -1 112859.34 406.84 3 -1 2 3063.01 289.50 3 -1 322918.82 765.00 3 -1 4 2494.68 169.00 3 -1 5 2171.50 126.00 3 -1 6 0.77 12.00 3 -1 7 793.48 44.56 3 -1 8 125.17 26.00 3 -1 9 11.06 17.39 3 -1 10 337.83 91.50 3 -1 11 28.97 19.97 3 -1 12 1093.27 86.00 3 -1 13 0.91 41.00 3 -1 14 35.72 47.00 3 -1 15 3.73 51.00 3 -1 16 1.39 55.00 3 0 0 1358.14 59.50 3 0 111423.82 619.00 3 0 210595.86 174.62 3 0 320873.77 1090.79 3 0 4 2614.81 197.00 3 0 5 1533.76 107.00 3 0 6 662.61 41.56 3 0 7 96.56 40.50 3 0 8 1624.82 176.00 3 0 9 44.00 16.52 3 0 10 748.38 59.00 3 0 11 18.69 21.27 3 0 12 90.70 44.00 3 0 13 241.19 54.00 3 0 14 6.59 47.00 3 0 15 0.25 48.00 3 0 16 46.49 58.00 3 0 17 279.08 74.00 3 1 0 2187.18 144.22 3 1 1 9274.05 300.54 3 1 235318.46 1375.91 3 1 3 8110.66 130.47 3 1 419223.28 536.01 3 1 5 1252.18 54.00 3 1 6 441.56 26.34 3 1 7 96.92 30.00 3 1 8 1525.25 108.00 3 1 9 132.75 17.77 3 1 10 354.96 31.50 3 1 11 396.17 56.00 3 1 12 56.88 24.60 3 1 13 595.94 60.00 3 1 14 7.04 46.00 3 1 15 378.38 68.00 3 1 16 357.94 75.00 3 1 17 0.86 56.00 3 2 1 2485.42 84.00 3 2 2 5063.87 96.67 3 2 3 4232.55 157.74 3 2 4 5897.77 214.72 3 2 5 4.09 6.79 3 2 6 451.61 39.95 3 2 7 365.08 36.04 3 2 8 0.13 14.48 3 2 9 375.17 44.40 3 2 10 221.93 21.89 3 2 11 3875.70 384.50 3 2 12 2.77 23.27 3 2 13 80.77 26.45 3 2 14 6.32 51.00 3 2 15 64.24 55.00 3 2 16 369.89 69.00 3 2 17 1.50 54.00 3 3 0 1427.60 68.48 3 3 1 2115.77 218.00 3 3 2 9643.91 442.00 3 3 3 609.00 40.88 3 3 4 2859.17 111.37 3 3 5 1506.03 51.00 3 3 6 69.46 11.88 3 3 7 5604.68 194.42 3 3 8 4656.41 134.33 3 3 9 1836.76 102.46 3 3 10 77.48 30.50 3 3 11 1677.18 71.25 3 3 12 1743.15 170.00 3 3 13 24.86 25.71 3 3 14 157.83 54.00 3 3 15 77.66 54.00 3 3 16 1316.62 129.00 3 3 17 0.57 53.00 3 4 0 24.37 42.00 3 4 2 1079.03 71.00 3 4 3 2109.19 95.50 3 4 4 2738.07 96.88 3 4 5 9520.47 388.23 3 4 6 4925.93 135.74 3 4 7 3159.98 82.69 3 4 8 2918.88 86.60 3 4 9 429.77 39.91 3 4 10 50.46 21.18 3 4 11 1568.21 74.40 3 4 12 115.72 31.02 3 4 13 49.40 29.30 3 4 14 1084.31 69.20 3 4 15 56.89 46.00 3 4 16 242.62 58.00 3 5 0 2945.92 39.00 3 5 1 484.58 20.00 3 5 420661.95 763.67 3 5 535589.70 1267.23 3 5 6 4.44 10.01 3 5 7 3192.11 131.53 3 5 8 2120.62 77.48 3 5 9 1190.50 68.49 3 5 10 1899.40 76.33 3 5 11 1544.62 112.50 3 5 12 50.24 27.55 3 5 13 2699.75 246.00 3 5 14 1901.55 92.34 3 5 15 0.56 28.11 3 5 16 20.58 49.00 3 6 018578.07 748.37 3 6 134940.74 846.53 3 6 2 9260.45 524.50 3 6 3 1240.94 72.00 3 6 4 760.06 53.00 3 6 518643.46 985.00 3 6 6 254.54 58.00 3 6 7 2531.80 81.32 3 6 8 840.38 44.50 3 6 9 763.29 59.38 3 6 10 27.92 20.14 3 6 11 257.66 63.00 3 6 12 1232.42 79.36 3 6 13 1270.11 106.00 3 6 14 604.48 55.81 3 6 15 34.81 28.83 3 6 16 54.62 47.00 3 7 0 2690.73 131.79 3 7 1 65.64 24.02 3 7 2 450.58 37.35 3 7 3 454.55 35.50 3 7 4 4915.43 265.00 3 7 6 6194.92 242.00 3 7 7 5585.86 289.00 3 7 8 5374.26 224.85 3 7 9 1868.53 68.94 3 7 10 21.95 21.50 3 7 11 1008.09 52.98 3 7 12 76.71 28.99 3 7 13 154.33 30.38 3 7 14 19.53 27.55 3 7 15 662.54 56.81 3 8 0 743.12 48.53 3 8 1 47.92 16.27 3 8 2 8.49 12.94 3 8 3 1.98 13.67 3 8 4 1317.74 126.00 3 8 7 55.27 23.00 3 8 8 857.68 84.00 3 8 9 881.18 41.41 3 8 10 678.65 44.90 3 8 11 935.20 61.84 3 8 12 566.41 50.47 3 8 13 137.84 29.34 3 8 14 0.26 27.16 3 8 15 10.42 29.29 3 9 0 471.91 40.00 3 9 1 1519.80 45.08 3 9 2 363.89 35.91 3 9 3 118.44 13.35 3 9 4 61.34 32.00 3 9 5 405.63 85.00 3 9 6 0.06 23.00 3 9 7 8.63 16.26 3 9 8 257.35 47.00 3 9 9 15.82 18.49 3 9 10 8.72 21.78 3 9 11 2.39 22.91 3 9 12 54.01 26.16 3 9 13 455.13 50.38 3 9 14 12.87 28.26 3 10 0 893.64 53.44 3 10 1 62.62 17.91 3 10 2 536.39 39.79 3 10 3 2476.55 86.35 3 10 4 1206.19 76.87 3 10 5 291.34 53.00 3 10 6 3.00 15.90 3 10 7 115.43 21.49 3 10 8 761.42 55.92 3 10 9 533.73 48.24 3 10 10 168.82 41.50 3 10 11 56.68 36.50 3 10 12 101.11 28.63 3 10 13 151.74 31.46 3 11 0 280.07 23.11 3 11 1 0.48 15.82 3 11 2 62.22 18.95 3 11 3 147.43 18.34 3 11 4 18.56 19.36 3 11 5 369.11 59.00 3 11 6 196.69 27.87 3 11 7 81.24 20.47 3 11 8 11.60 18.73 3 11 9 73.60 23.92 3 11 10 627.27 53.06 3 11 11 35.08 38.00 3 11 12 148.18 31.09 3 12 0 673.60 47.16 3 12 1 72.73 19.75 3 12 2 1329.47 55.28 3 12 3 2258.83 84.84 3 12 4 1449.25 80.46 3 12 5 65.84 23.68 3 12 6 26.04 20.85 3 12 7 151.32 43.00 3 12 8 104.02 31.00 3 12 9 37.47 24.20 3 12 10 40.82 25.19 3 12 11 279.01 52.00 3 13 0 94.33 20.90 3 13 1 11.63 19.20 3 13 2 361.76 53.50 3 13 3 1247.10 78.71 3 13 4 577.05 58.02 3 13 5 83.19 26.16 3 13 6 38.03 30.00 3 13 7 196.97 26.76 3 13 8 0.11 22.20 3 13 9 2.91 23.76 3 14 0 4.04 27.14 3 14 1 28.95 27.60 3 14 2 94.40 30.46 3 14 3 106.46 31.09 3 14 4 36.00 26.51 3 14 5 51.21 26.13 3 14 6 915.62 66.07 3 14 7 2021.89 114.02 4 -11 0 52.03 28.11 4 -11 1 28.99 28.58 4 -11 2 23.17 27.85 4 -11 3 3.20 27.55 4 -11 4 0.61 27.54 4 -11 5 32.87 29.21 4 -10 0 557.91 53.10 4 -10 1 368.29 57.00 4 -10 2 459.72 51.55 4 -10 3 150.05 30.51 4 -10 4 7.81 26.40 4 -10 5 57.26 32.00 4 -10 6 40.46 27.86 4 -10 7 75.99 56.00 4 -9 0 201.68 27.76 4 -9 1 951.48 57.41 4 -9 2 1662.95 85.71 4 -9 3 508.81 50.61 4 -9 4 21.74 23.86 4 -9 5 11.24 23.62 4 -9 6 69.97 25.44 4 -9 7 93.21 26.76 4 -9 8 172.90 56.00 4 -9 9 72.52 56.00 4 -8 0 241.51 42.00 4 -8 1 60.17 19.46 4 -8 2 486.81 96.50 4 -8 3 182.87 26.67 4 -8 4 126.50 24.41 4 -8 5 117.76 26.08 4 -8 6 224.02 26.63 4 -8 7 6.64 21.85 4 -8 8 68.00 47.00 4 -8 9 396.99 68.00 4 -8 10 426.57 66.00 4 -8 11 218.36 63.00 4 -7 0 0.44 16.58 4 -7 1 1227.91 71.46 4 -7 2 51.69 17.94 4 -7 3 262.30 26.43 4 -7 4 364.54 36.06 4 -7 5 30.78 19.53 4 -7 6 17.23 19.94 4 -7 7 119.65 26.63 4 -7 8 996.22 53.82 4 -7 9 806.92 99.00 4 -7 10 40.11 47.00 4 -7 11 174.82 54.00 4 -7 12 39.80 52.00 4 -6 0 734.70 57.00 4 -6 1 96.13 22.00 4 -6 2 177.26 30.00 4 -6 3 3.91 19.00 4 -6 4 585.78 54.00 4 -6 5 3125.63 127.10 4 -6 6 1568.50 77.59 4 -6 7 1.03 18.77 4 -6 8 1.21 18.26 4 -6 9 76.91 40.00 4 -6 10 20.44 41.00 4 -6 11 17.29 44.00 4 -6 12 22.21 48.00 4 -6 13 0.45 52.00 4 -5 0 756.48 48.00 4 -5 1 806.34 55.10 4 -5 2 2212.85 93.00 4 -5 3 908.70 55.00 4 -5 4 2295.68 108.00 4 -5 5 560.00 53.00 4 -5 6 45.70 19.00 4 -5 7 150.74 28.50 4 -5 8 18.01 18.14 4 -5 9 73.33 19.28 4 -5 10 55.88 40.00 4 -5 11 0.99 42.00 4 -5 12 3.84 45.00 4 -5 13 16.03 52.00 4 -5 14 216.82 62.00 4 -4 0 439.11 103.00 4 -4 1 22.58 15.54 4 -4 2 893.93 70.00 4 -4 3 1876.48 78.59 4 -4 4 1418.78 102.00 4 -4 5 796.50 45.00 4 -4 6 2486.97 131.00 4 -4 7 2769.41 128.00 4 -4 8 2042.84 99.51 4 -4 9 1545.14 76.00 4 -4 10 683.06 80.00 4 -4 11 286.33 56.00 4 -4 12 141.95 45.00 4 -4 13 0.01 48.00 4 -4 14 61.17 54.00 4 -4 15 2.12 55.00 4 -3 0 93.17 41.27 4 -3 1 10.36 33.88 4 -3 2 416.75 52.00 4 -3 3 3502.66 140.14 4 -3 4 2465.77 76.17 4 -3 5 7446.44 395.50 4 -3 6 1056.10 51.88 4 -3 7 2188.01 99.74 4 -3 8 976.63 93.00 4 -3 9 6.98 18.01 4 -3 10 46.30 19.53 4 -3 11 490.91 86.00 4 -3 12 485.38 51.00 4 -3 13 1367.03 134.00 4 -3 14 625.12 98.00 4 -3 15 4.12 56.00 4 -2 0 8694.06 258.00 4 -2 1 6638.86 367.23 4 -2 2 1565.42 45.99 4 -2 3 1017.06 47.50 4 -2 4 376.52 37.00 4 -2 5 2144.97 171.00 4 -2 6 6165.94 428.50 4 -2 7 1276.96 89.00 4 -2 8 25.29 17.74 4 -2 9 1749.97 88.56 4 -2 10 665.37 44.40 4 -2 11 885.45 52.50 4 -2 12 0.05 43.00 4 -2 13 23.18 44.00 4 -2 14 65.86 52.00 4 -2 15 289.03 63.00 4 -2 16 33.29 57.00 4 -1 0 463.51 84.00 4 -1 1 382.22 58.00 4 -1 2 3490.62 126.52 4 -1 3 7539.13 239.63 4 -1 4 3991.15 256.00 4 -1 5 1821.71 79.36 4 -1 6 3885.86 167.80 4 -1 7 186.25 17.51 4 -1 8 1919.63 76.52 4 -1 9 514.52 50.00 4 -1 10 11.17 19.61 4 -1 11 13.00 42.50 4 -1 12 177.02 42.00 4 -1 13 106.40 52.00 4 -1 14 335.07 63.00 4 -1 15 319.20 69.00 4 -1 16 5.24 60.00 4 0 017614.85 588.20 4 0 1 8460.30 385.00 4 0 2 1944.20 83.77 4 0 3 6352.51 277.00 4 0 410084.03 387.00 4 0 5 1251.36 122.50 4 0 6 2038.01 83.00 4 0 7 2012.26 60.70 4 0 8 1117.51 53.52 4 0 9 1014.10 70.50 4 0 10 2143.19 81.70 4 0 11 164.67 26.89 4 0 12 489.52 92.00 4 0 13 113.91 43.00 4 0 14 226.60 52.00 4 0 15 0.38 49.00 4 0 16 32.10 58.00 4 1 0 1076.18 42.00 4 1 1 816.55 87.00 4 1 2 160.85 19.52 4 1 3 2832.80 153.11 4 1 410231.96 435.60 4 1 5 558.39 27.00 4 1 6 574.41 72.41 4 1 7 353.32 16.26 4 1 8 47.49 15.51 4 1 9 1304.93 58.00 4 1 10 2199.28 186.00 4 1 11 5.22 21.35 4 1 12 461.07 84.50 4 1 13 198.98 49.00 4 1 14 73.83 50.00 4 1 15 9.98 49.00 4 1 16 622.83 102.00 4 2 0 308.69 39.84 4 2 1 330.65 31.00 4 2 3 1631.78 25.63 4 2 4 1748.80 73.59 4 2 5 14.70 11.65 4 2 6 18.06 28.26 4 2 7 1118.10 66.11 4 2 8 249.28 27.55 4 2 9 1617.96 96.00 4 2 10 389.12 37.00 4 2 11 511.69 59.50 4 2 12 2390.82 113.12 4 2 13 555.40 65.00 4 2 14 262.09 53.00 4 2 15 16.95 53.00 4 2 16 446.25 74.00 4 3 0 2019.93 156.00 4 3 1 2428.85 197.00 4 3 2 1337.71 43.00 4 3 3 3093.41 130.62 4 3 411491.78 373.95 4 3 5 670.18 68.61 4 3 6 411.00 35.71 4 3 7 2043.44 73.53 4 3 8 187.04 22.27 4 3 9 265.75 23.68 4 3 10 55.10 21.21 4 3 11 5237.97 176.71 4 3 12 2041.22 97.50 4 3 13 246.50 29.30 4 3 14 540.44 101.00 4 3 15 474.66 66.00 4 3 16 2.92 54.00 4 4 0 1629.79 116.00 4 4 1 3863.21 241.89 4 4 2 39.80 14.00 4 4 3 1037.14 135.00 4 4 4 3045.45 170.03 4 4 5 604.07 52.25 4 4 6 2442.50 95.50 4 4 7 189.49 20.39 4 4 8 687.93 49.82 4 4 9 0.35 16.93 4 4 10 22.09 19.05 4 4 11 3816.11 165.10 4 4 12 5.14 25.80 4 4 13 75.21 27.16 4 4 14 303.23 38.50 4 4 15 1247.71 124.00 4 4 16 19.75 50.00 4 5 0 625.84 66.19 4 5 111076.16 294.00 4 5 2 821.14 58.50 4 5 3 287.60 17.00 4 5 4 1986.05 66.44 4 5 5 282.67 30.92 4 5 6 21.78 11.48 4 5 7 86.19 11.16 4 5 8 502.86 47.57 4 5 9 134.62 24.33 4 5 10 19.01 21.18 4 5 11 18.45 24.33 4 5 12 478.82 48.54 4 5 13 196.50 30.41 4 5 14 953.79 78.50 4 5 15 2305.30 100.29 4 5 16 42.39 52.00 4 6 0 2996.77 94.00 4 6 113018.51 1246.00 4 6 2 7216.58 388.00 4 6 3 197.13 40.28 4 6 4 355.00 29.50 4 6 5 6152.84 198.61 4 6 6 0.46 10.51 4 6 7 186.34 28.57 4 6 8 263.73 33.66 4 6 9 315.92 43.28 4 6 10 123.71 21.18 4 6 11 389.37 92.50 4 6 12 917.52 100.00 4 6 13 478.74 52.39 4 6 14 198.51 38.00 4 6 15 288.38 38.53 4 6 16 75.82 47.00 4 7 0 29.34 11.52 4 7 1 68.65 17.00 4 7 2 6019.69 232.00 4 7 3 4491.74 251.00 4 7 6 163.11 18.49 4 7 7 27.12 18.94 4 7 8 35.76 15.40 4 7 9 405.38 34.89 4 7 10 86.42 20.85 4 7 11 10.29 21.92 4 7 12 1692.47 77.41 4 7 13 168.64 32.50 4 7 14 77.35 30.50 4 7 15 16.64 29.34 4 8 0 7.04 10.39 4 8 1 56.51 24.73 4 8 2 1135.71 91.00 4 8 3 782.36 68.00 4 8 7 342.10 39.43 4 8 8 347.44 46.63 4 8 9 731.65 37.80 4 8 10 282.00 35.02 4 8 11 0.21 22.91 4 8 12 6.84 25.46 4 8 13 5.94 26.16 4 8 14 0.13 27.22 4 8 15 9.03 29.34 4 9 0 1112.55 58.36 4 9 1 41.30 13.32 4 9 2 3574.70 119.05 4 9 3 1180.35 70.00 4 9 7 1062.85 54.29 4 9 8 843.75 58.51 4 9 9 237.37 27.40 4 9 10 816.20 44.17 4 9 11 3119.41 191.50 4 9 12 1485.33 78.48 4 9 13 1530.50 79.16 4 9 14 211.87 34.56 4 10 0 138.30 20.53 4 10 1 3455.59 117.22 4 10 211997.73 322.27 4 10 3 196.00 43.00 4 10 4 0.00 17.51 4 10 5 205.61 41.00 4 10 6 236.26 63.50 4 10 7 14.80 18.65 4 10 8 34.39 18.94 4 10 9 149.62 23.11 4 10 10 564.19 56.54 4 10 11 486.93 48.50 4 10 12 3.20 24.33 4 10 13 135.86 30.90 4 11 0 4231.47 148.98 4 11 1 51.45 16.58 4 11 2 3099.33 117.70 4 11 3 267.18 48.00 4 11 4 1247.82 102.00 4 11 5 688.16 82.00 4 11 6 29.20 20.51 4 11 7 189.66 37.00 4 11 8 968.05 64.76 4 11 9 2333.52 104.90 4 11 10 37.39 18.39 4 11 11 0.00 18.08 4 11 12 16.19 26.45 4 12 0 2148.90 106.15 4 12 1 74.26 17.69 4 12 2 1312.69 55.43 4 12 3 401.75 68.50 4 12 4 83.73 35.50 4 12 5 454.55 50.00 4 12 6 19.33 22.27 4 12 7 155.65 30.00 4 12 8 44.84 23.21 4 12 9 220.24 40.00 4 12 10 71.19 25.91 4 12 11 11.81 23.55 4 13 0 1744.36 95.78 4 13 1 981.85 69.17 4 13 2 25.37 25.46 4 13 3 2196.92 137.50 4 13 4 1035.37 79.00 4 13 5 84.70 25.46 4 13 6 79.76 24.75 4 13 7 172.03 28.89 4 13 8 195.02 29.75 4 13 9 356.71 76.00 4 14 0 41.03 35.00 4 14 1 29.09 28.76 4 14 2 57.83 29.03 4 14 3 274.76 34.16 4 14 4 58.40 27.87 4 14 5 284.44 42.00 4 14 6 426.91 53.50 4 14 7 456.46 51.24 4 15 0 47.31 31.50 4 15 1 2.29 29.07 4 15 2 51.32 31.61 5 -10 0 348.06 52.00 5 -10 1 5.46 26.67 5 -10 2 4.71 26.67 5 -10 3 22.57 27.63 5 -10 4 19.63 27.85 5 -10 5 70.82 31.26 5 -9 0 35.56 24.92 5 -9 1 27.91 24.74 5 -9 2 52.29 54.00 5 -9 3 23.26 24.99 5 -9 4 300.91 33.39 5 -9 5 97.07 28.86 5 -9 6 8.30 25.72 5 -9 7 27.60 27.86 5 -9 8 0.01 52.00 5 -8 0 262.74 29.75 5 -8 1 647.89 52.53 5 -8 2 318.12 47.50 5 -8 3 35.31 22.54 5 -8 4 479.23 52.36 5 -8 5 68.25 26.08 5 -8 6 1.11 24.38 5 -8 7 58.90 27.54 5 -8 8 50.25 50.00 5 -8 9 7.17 50.00 5 -8 10 5.78 53.00 5 -7 0 521.00 45.16 5 -7 1 684.61 51.90 5 -7 2 797.46 56.22 5 -7 3 155.15 38.50 5 -7 4 106.83 22.54 5 -7 5 40.98 22.75 5 -7 6 47.48 24.96 5 -7 7 110.69 23.77 5 -7 8 3.75 22.51 5 -7 9 69.44 49.00 5 -7 10 2.30 48.00 5 -7 11 14.27 53.00 5 -6 0 304.27 34.03 5 -6 1 67.94 17.51 5 -6 2 18.17 18.98 5 -6 3 1927.45 55.14 5 -6 4 1535.65 69.16 5 -6 5 21.09 15.08 5 -6 6 23.31 16.51 5 -6 7 265.32 20.72 5 -6 8 252.62 37.46 5 -6 9 66.31 23.92 5 -6 10 78.96 50.00 5 -6 11 239.53 56.00 5 -6 12 28.12 51.00 5 -5 0 199.38 28.45 5 -5 1 4.91 15.62 5 -5 2 304.72 34.41 5 -5 3 522.82 52.07 5 -5 4 336.98 20.71 5 -5 5 16.97 17.87 5 -5 6 57.13 24.50 5 -5 7 1358.85 128.00 5 -5 8 675.55 42.09 5 -5 9 28.43 20.71 5 -5 10 139.21 46.00 5 -5 11 127.15 50.00 5 -5 12 32.41 48.00 5 -5 13 18.52 53.00 5 -4 0 1942.31 54.04 5 -4 1 6592.34 286.58 5 -4 2 2320.77 95.18 5 -4 3 1025.32 40.49 5 -4 4 4.73 17.72 5 -4 5 26.99 19.00 5 -4 6 50.73 17.24 5 -4 7 53.75 18.01 5 -4 8 43.49 19.79 5 -4 9 193.97 33.45 5 -4 10 1299.69 68.94 5 -4 11 233.80 51.00 5 -4 12 323.04 62.00 5 -4 13 2.20 50.00 5 -4 14 0.03 52.00 5 -3 0 16.61 20.85 5 -3 1 8716.97 254.79 5 -3 2 7036.38 255.12 5 -3 3 2222.54 104.39 5 -3 4 64.97 26.00 5 -3 5 121.36 22.82 5 -3 6 698.18 44.35 5 -3 7 178.28 31.82 5 -3 8 651.76 35.36 5 -3 9 2652.80 123.36 5 -3 10 50.82 23.12 5 -3 11 571.39 82.00 5 -3 12 156.76 48.00 5 -3 13 48.86 51.00 5 -3 14 6.09 50.00 5 -3 15 143.46 60.00 5 -2 0 5403.15 233.97 5 -2 1 231.77 30.03 5 -2 2 1222.34 50.68 5 -2 3 525.02 33.38 5 -2 4 511.09 46.00 5 -2 5 1992.49 102.35 5 -2 611532.47 389.12 5 -2 7 842.43 44.43 5 -2 8 1201.52 73.88 5 -2 9 3788.50 237.00 5 -2 10 159.25 30.50 5 -2 11 486.35 49.45 5 -2 12 1.36 42.00 5 -2 13 2.12 46.00 5 -2 14 4.20 51.00 5 -2 15 33.44 57.00 5 -1 0 1393.41 87.00 5 -1 1 3.74 9.53 5 -1 2 1516.16 74.48 5 -1 3 7633.11 257.65 5 -1 4 1354.51 77.00 5 -1 5 55.59 15.80 5 -1 6 8440.46 328.32 5 -1 7 21.10 18.65 5 -1 8 275.13 21.50 5 -1 9 1143.26 135.50 5 -1 10 12.13 22.82 5 -1 11 2084.79 93.95 5 -1 12 1384.41 111.00 5 -1 13 1189.94 116.00 5 -1 14 60.25 51.00 5 -1 15 50.56 56.00 5 0 0 370.28 62.00 5 0 1 1966.05 100.00 5 0 2 3487.78 105.00 5 0 3 9254.65 337.92 5 0 4 351.15 43.50 5 0 5 505.36 56.05 5 0 6 8193.92 507.50 5 0 7 5.12 19.05 5 0 8 12.38 17.23 5 0 9 2.72 18.94 5 0 10 716.30 81.50 5 0 11 1913.04 247.00 5 0 12 32.90 24.50 5 0 13 15.58 44.00 5 0 14 78.01 52.00 5 0 15 0.26 52.00 5 0 16 2.69 59.00 5 1 0 4628.65 87.90 5 1 1 7584.94 266.48 5 1 2 3319.07 208.63 5 1 3 4042.41 157.92 5 1 4 2293.23 41.95 5 1 5 2153.51 111.33 5 1 6 369.55 41.00 5 1 7 2295.10 73.16 5 1 8 3.47 16.52 5 1 9 41.29 23.00 5 1 10 1162.14 66.59 5 1 11 1305.21 133.50 5 1 12 3.91 24.27 5 1 13 61.64 43.00 5 1 14 0.08 44.00 5 1 15 0.53 50.00 5 1 16 156.44 63.00 5 2 0 56.34 15.80 5 2 1 8574.87 362.47 5 2 2 5817.43 170.79 5 2 3 480.43 21.05 5 2 4 38.77 10.96 5 2 5 7126.70 215.59 5 2 6 111.79 22.91 5 2 7 2474.54 105.71 5 2 8 102.68 19.09 5 2 9 96.40 19.05 5 2 10 164.23 26.16 5 2 11 11.06 22.91 5 2 12 171.64 35.00 5 2 13 12.58 26.05 5 2 14 19.46 45.00 5 2 15 52.60 49.00 5 2 16 1.79 52.00 5 3 037811.91 2104.00 5 3 123462.92 1719.50 5 3 211683.41 391.85 5 3 3 1749.03 51.93 5 3 4 2359.82 71.03 5 3 5 3969.56 165.11 5 3 6 283.44 23.98 5 3 7 1470.12 60.11 5 3 8 99.47 16.52 5 3 9 7.17 17.94 5 3 10 1319.45 56.21 5 3 11 3572.97 321.00 5 3 12 531.37 51.97 5 3 13 35.43 26.17 5 3 14 98.82 30.50 5 3 15 0.00 46.00 5 3 16 82.18 56.00 5 4 0 576.78 36.04 5 4 1 165.88 18.00 5 4 2 9.29 12.50 5 4 3 65.67 8.14 5 4 4 2689.49 77.40 5 4 5 148.28 10.51 5 4 6 254.26 26.88 5 4 7 909.71 29.07 5 4 8 3978.21 182.18 5 4 9 1084.61 67.16 5 4 10 647.91 56.92 5 4 11 2161.46 131.00 5 4 12 911.35 66.80 5 4 13 201.82 31.41 5 4 14 85.13 32.50 5 4 15 31.90 48.00 5 4 16 28.78 54.00 5 5 0 6303.11 249.87 5 5 1 4715.14 186.00 5 5 2 139.93 19.00 5 5 3 257.83 47.00 5 5 4 965.62 63.45 5 5 5 2410.72 126.16 5 5 6 136.32 37.23 5 5 7 0.00 12.06 5 5 8 3455.67 135.17 5 5 9 1075.66 37.29 5 5 10 5.39 20.36 5 5 11 38.41 34.00 5 5 12 49.86 28.89 5 5 13 184.89 33.21 5 5 14 174.92 55.00 5 5 15 22.44 35.50 5 5 16 80.62 54.00 5 6 0 6887.87 205.17 5 6 1 4477.26 210.86 5 6 2 147.80 27.00 5 6 3 55.37 12.36 5 6 4 655.27 78.00 5 6 5 5303.99 178.54 5 6 6 88.77 36.42 5 6 7 202.81 20.10 5 6 8 111.13 23.48 5 6 9 944.29 37.68 5 6 10 189.01 26.34 5 6 11 12.43 22.06 5 6 12 1622.37 111.50 5 6 13 2.11 26.05 5 6 14 26.21 29.29 5 6 15 69.25 31.32 5 6 16 0.33 49.00 5 7 0 222.55 58.00 5 7 1 419.39 37.50 5 7 2 105.82 31.50 5 7 3 38.59 34.95 5 7 4 768.18 39.00 5 7 5 1053.68 81.00 5 7 6 1897.88 107.07 5 7 7 174.13 20.69 5 7 8 212.63 18.37 5 7 9 1579.83 70.00 5 7 10 57.65 21.92 5 7 11 1.94 21.49 5 7 12 730.57 50.19 5 7 13 183.43 31.41 5 7 14 321.41 59.00 5 7 15 123.38 32.03 5 8 0 85.46 21.00 5 8 1 993.06 86.00 5 8 2 330.18 30.00 5 8 3 26.55 21.00 5 8 6 98.88 21.00 5 8 7 17.67 12.92 5 8 8 183.38 17.82 5 8 9 55.07 15.42 5 8 10 23.26 15.17 5 8 11 172.26 30.73 5 8 12 35.39 25.50 5 8 13 0.92 26.45 5 8 14 26.63 29.29 5 8 15 173.22 34.50 5 9 0 52.17 21.00 5 9 1 39.18 23.00 5 9 2 3223.50 188.00 5 9 3 205.01 30.00 5 9 4 7.52 24.00 5 9 6 81.33 20.44 5 9 7 14.56 14.03 5 9 8 529.79 39.01 5 9 9 29.56 15.70 5 9 10 77.65 16.70 5 9 11 25.24 18.90 5 9 12 1.48 24.92 5 9 13 140.25 30.90 5 9 14 89.16 28.97 5 10 0 67.59 15.93 5 10 1 10.89 11.50 5 10 2 2014.70 130.50 5 10 3 432.07 99.00 5 10 4 51.93 39.00 5 10 5 47.07 37.00 5 10 6 280.02 66.00 5 10 7 887.83 48.56 5 10 8 0.51 15.31 5 10 9 265.71 32.53 5 10 10 33.82 16.70 5 10 11 53.12 18.58 5 10 12 289.27 33.03 5 10 13 119.70 29.19 5 11 0 61.55 30.00 5 11 1 685.13 67.00 5 11 2 456.57 111.00 5 11 3 1249.43 70.84 5 11 4 1631.99 124.00 5 11 5 693.97 113.50 5 11 6 3.41 18.73 5 11 7 1086.88 61.97 5 11 8 961.58 69.32 5 11 9 9.86 21.61 5 11 10 225.26 43.00 5 11 11 427.64 51.26 5 11 12 163.25 45.00 5 12 0 497.71 56.00 5 12 1 2695.56 133.01 5 12 2 46.16 26.45 5 12 3 180.32 28.99 5 12 4 95.50 32.50 5 12 5 838.96 63.41 5 12 6 634.04 54.76 5 12 7 252.86 59.50 5 12 8 0.08 21.18 5 12 9 470.75 56.09 5 12 10 233.32 57.00 5 12 11 17.77 24.73 5 13 0 14.63 26.43 5 13 1 478.42 105.50 5 13 2 191.23 66.00 5 13 3 293.14 48.00 5 13 4 328.93 42.00 5 13 5 142.93 52.50 5 13 6 28.17 24.04 5 13 7 32.12 32.50 5 13 8 2.37 23.21 5 13 9 362.66 60.50 5 14 0 156.87 49.00 5 14 1 797.30 65.47 5 14 2 225.60 34.95 5 14 3 608.08 60.50 5 14 4 23.26 32.00 5 14 5 375.54 87.00 5 14 6 735.06 67.28 5 14 7 47.99 27.47 5 15 0 337.70 95.00 5 15 1 126.56 33.31 5 15 2 47.52 30.73 5 15 3 460.63 68.50 6 -10 0 584.24 60.48 6 -10 1 87.73 31.47 6 -9 0 6.23 25.46 6 -9 1 132.98 33.31 6 -9 2 275.97 35.29 6 -9 3 43.17 28.35 6 -9 4 104.77 30.99 6 -9 5 159.40 35.55 6 -9 6 79.01 31.62 6 -8 0 22.70 23.76 6 -8 1 133.84 29.90 6 -8 2 193.15 28.76 6 -8 3 52.17 26.89 6 -8 4 1.75 24.94 6 -8 5 268.94 36.04 6 -8 6 34.83 27.01 6 -8 7 1.17 26.79 6 -8 8 18.10 54.00 6 -7 0 252.48 28.76 6 -7 1 30.42 20.90 6 -7 2 0.14 19.93 6 -7 3 0.06 21.60 6 -7 4 0.02 22.75 6 -7 5 192.13 29.30 6 -7 6 322.98 33.88 6 -7 7 421.62 48.00 6 -7 8 18.60 26.20 6 -7 9 0.96 51.00 6 -7 10 0.01 53.00 6 -6 0 59.84 20.90 6 -6 1 215.46 27.05 6 -6 2 401.15 38.31 6 -6 3 754.75 42.42 6 -6 4 1090.20 62.69 6 -6 5 1816.03 126.00 6 -6 6 70.60 26.81 6 -6 7 771.66 66.00 6 -6 8 135.89 39.00 6 -6 9 162.45 29.21 6 -6 10 312.21 64.00 6 -6 11 1197.06 123.00 6 -5 0 2364.59 100.14 6 -5 1 2590.94 93.95 6 -5 2 920.58 58.38 6 -5 3 702.24 48.82 6 -5 4 553.98 44.01 6 -5 5 1174.16 65.50 6 -5 6 0.01 20.58 6 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58.00 6 -1 0 907.48 70.00 6 -1 1 221.68 24.00 6 -1 2 8742.25 324.48 6 -1 3 1151.38 50.68 6 -1 4 794.07 95.00 6 -1 5 2299.12 141.50 6 -1 6 2989.91 109.54 6 -1 7 1065.23 181.00 6 -1 8 127.16 23.92 6 -1 9 2430.34 104.15 6 -1 10 3175.57 256.00 6 -1 11 1832.48 120.50 6 -1 12 200.68 49.00 6 -1 13 59.29 45.00 6 -1 14 0.69 48.00 6 -1 15 0.07 54.00 6 0 0 4661.85 160.10 6 0 1 1115.65 79.00 6 0 2 6783.27 230.00 6 0 3 1263.20 77.70 6 0 4 731.67 42.14 6 0 5 933.91 38.86 6 0 6 584.36 50.26 6 0 7 3342.24 133.22 6 0 8 201.45 27.16 6 0 9 185.98 25.74 6 0 10 321.67 35.33 6 0 11 789.87 89.00 6 0 12 431.54 62.50 6 0 13 309.81 56.00 6 0 14 475.67 69.00 6 0 15 417.67 70.00 6 1 0 1378.67 35.88 6 1 1 38.33 9.53 6 1 2 1618.43 66.52 6 1 3 2556.66 123.11 6 1 411612.51 353.22 6 1 5 2906.30 93.56 6 1 6 2994.79 148.50 6 1 7 1669.49 73.50 6 1 8 1223.92 172.50 6 1 9 459.43 41.79 6 1 10 0.50 22.20 6 1 11 1852.11 186.00 6 1 12 285.96 32.12 6 1 13 187.91 32.42 6 1 14 223.54 56.00 6 1 15 209.22 60.00 6 2 0 828.88 34.76 6 2 1 867.57 47.06 6 2 2 8592.65 583.50 6 2 3 3321.91 93.45 6 2 4 37.34 11.05 6 2 5 902.87 42.29 6 2 6 1298.72 58.87 6 2 7 633.06 45.57 6 2 8 910.97 80.50 6 2 9 207.39 25.43 6 2 10 297.71 45.50 6 2 11 978.78 66.68 6 2 12 359.85 34.65 6 2 13 151.63 32.50 6 2 14 0.49 44.00 6 2 15 7.94 50.00 6 2 16 204.31 62.00 6 3 0 479.40 35.76 6 3 1 1639.01 48.44 6 3 2 2448.86 149.35 6 3 3 129.13 17.01 6 3 4 289.37 37.90 6 3 5 4618.74 137.04 6 3 6 812.77 34.41 6 3 7 578.15 30.40 6 3 8 57.85 18.34 6 3 9 0.58 18.65 6 3 10 171.82 26.05 6 3 11 341.49 38.61 6 3 12 995.82 122.00 6 3 13 281.31 35.66 6 3 14 0.32 26.62 6 3 15 120.89 52.00 6 3 16 447.17 71.00 6 4 0 767.37 36.51 6 4 1 1154.02 35.78 6 4 2 2203.33 82.50 6 4 3 2285.00 114.00 6 4 4 319.47 25.07 6 4 510664.81 416.54 6 4 6 2.43 12.73 6 4 7 37.70 11.68 6 4 8 54.71 13.68 6 4 9 1941.53 82.72 6 4 10 1448.54 66.04 6 4 11 480.79 41.27 6 4 12 330.84 43.00 6 4 13 220.24 34.16 6 4 14 249.15 35.70 6 4 15 110.53 49.00 6 4 16 119.99 55.00 6 5 0 310.63 22.50 6 5 1 7728.89 373.00 6 5 2 940.60 105.00 6 5 3 7.06 13.44 6 5 4 326.36 72.50 6 5 5 2055.18 92.11 6 5 6 761.18 49.12 6 5 7 1538.28 63.19 6 5 8 524.43 35.75 6 5 9 14.57 13.77 6 5 10 62.13 33.00 6 5 11 305.22 41.08 6 5 12 409.48 45.50 6 5 13 74.67 29.90 6 5 14 0.00 28.58 6 5 15 857.96 69.58 6 6 0 964.31 60.50 6 6 1 219.96 34.20 6 6 2 293.21 30.50 6 6 3 722.64 77.00 6 6 4 329.61 71.00 6 6 5 37.57 11.47 6 6 6 1316.80 58.33 6 6 7 877.66 49.17 6 6 8 49.49 13.94 6 6 9 1097.31 59.69 6 6 10 146.23 28.80 6 6 11 237.04 28.58 6 6 12 828.59 59.38 6 6 13 399.73 38.58 6 6 14 107.05 32.74 6 6 15 443.53 48.05 6 7 0 57.46 15.19 6 7 1 2413.56 131.99 6 7 2 2538.98 95.23 6 7 3 16.98 13.77 6 7 4 358.51 79.00 6 7 5 461.95 58.50 6 7 6 148.42 21.00 6 7 7 31.22 11.73 6 7 8 548.15 36.76 6 7 9 352.92 36.75 6 7 10 42.14 17.69 6 7 11 198.01 26.43 6 7 12 209.96 31.44 6 7 13 179.42 31.89 6 7 14 0.25 28.89 6 7 15 12.04 31.41 6 8 0 1316.13 62.00 6 8 1 1059.60 91.00 6 8 2 1240.09 55.83 6 8 3 98.68 41.93 6 8 4 34.12 28.00 6 8 5 2990.94 226.00 6 8 6 90.28 23.00 6 8 7 653.43 80.23 6 8 8 673.14 60.71 6 8 9 9.36 14.19 6 8 10 54.39 16.40 6 8 11 24.51 18.05 6 8 12 447.29 47.63 6 8 13 260.01 38.50 6 8 14 4.92 28.05 6 9 0 448.50 68.00 6 9 1 7235.40 360.00 6 9 2 173.53 26.00 6 9 3 2600.89 111.00 6 9 4 4122.51 172.71 6 9 5 196.01 58.00 6 9 6 833.16 86.00 6 9 7 1380.53 80.40 6 9 8 594.15 41.84 6 9 9 543.12 39.23 6 9 10 549.64 38.26 6 9 11 409.82 40.33 6 9 12 26.49 25.46 6 9 13 188.01 32.42 6 9 14 232.57 55.50 6 10 0 50.05 24.39 6 10 1 57.94 40.50 6 10 2 484.50 42.00 6 10 3 9192.87 365.90 6 10 4 1709.39 100.50 6 10 5 59.04 36.00 6 10 6 117.11 33.00 6 10 7 62.45 28.00 6 10 8 126.80 46.00 6 10 9 1303.58 75.60 6 10 10 1646.10 89.39 6 10 11 33.26 23.50 6 10 12 417.67 56.00 6 10 13 348.47 57.00 6 11 0 2287.40 113.64 6 11 1 2135.21 108.33 6 11 2 1074.45 106.00 6 11 3 6717.24 260.27 6 11 4 438.16 51.00 6 11 5 9.11 21.21 6 11 6 93.44 25.00 6 11 7 50.57 22.50 6 11 8 137.80 29.00 6 11 9 521.05 54.67 6 11 10 21.35 22.33 6 11 11 48.68 23.55 6 11 12 116.85 28.11 6 12 0 79.17 57.50 6 12 1 84.53 25.74 6 12 2 966.01 134.00 6 12 3 2083.15 103.25 6 12 4 388.30 55.00 6 12 5 294.86 84.00 6 12 6 28.17 21.89 6 12 7 217.30 62.50 6 12 8 157.13 57.00 6 12 9 80.92 25.46 6 12 10 26.04 23.55 6 12 11 78.87 26.67 6 13 0 69.15 36.50 6 13 1 416.73 74.50 6 13 2 0.00 25.71 6 13 3 0.19 24.74 6 13 4 12.38 24.72 6 13 5 99.31 43.50 6 13 6 72.19 44.50 6 13 7 126.32 39.00 6 13 8 320.39 34.74 6 13 9 158.33 30.27 6 14 0 196.01 66.00 6 14 1 193.46 49.00 6 14 2 99.78 37.50 6 14 3 333.87 37.83 6 14 4 72.18 28.47 6 14 5 8.73 26.45 6 14 6 38.25 33.00 6 14 7 63.85 27.87 6 15 0 18.26 29.95 6 15 1 26.17 31.50 6 15 2 24.78 30.18 7 -9 0 151.95 32.32 7 -9 1 66.96 30.98 7 -8 0 69.32 27.60 7 -8 1 391.60 50.50 7 -8 2 1035.10 69.76 7 -8 3 525.82 57.18 7 -8 4 140.56 34.00 7 -8 5 9.19 28.28 7 -8 6 10.23 29.95 7 -7 0 365.74 102.50 7 -7 1 60.63 25.45 7 -7 2 29.96 28.50 7 -7 3 80.67 27.60 7 -7 4 95.85 30.01 7 -7 5 401.95 65.00 7 -7 6 119.08 32.87 7 -7 7 46.80 36.50 7 -7 8 75.68 32.19 7 -6 0 152.22 26.89 7 -6 1 1112.25 46.57 7 -6 2 992.06 51.63 7 -6 3 302.86 66.00 7 -6 4 5.01 22.75 7 -6 5 0.62 23.86 7 -6 6 27.40 27.01 7 -6 7 0.44 24.05 7 -6 8 2.84 25.33 7 -6 9 43.66 27.66 7 -6 10 348.09 68.00 7 -5 0 943.99 54.53 7 -5 1 26.77 17.74 7 -5 2 151.51 22.50 7 -5 3 81.06 22.54 7 -5 4 3.11 22.54 7 -5 5 2.38 23.48 7 -5 6 30.86 25.95 7 -5 7 26.60 24.68 7 -5 8 70.16 40.00 7 -5 9 278.21 37.50 7 -5 10 82.89 53.00 7 -5 11 125.26 57.00 7 -4 0 0.02 16.07 7 -4 1 909.18 50.45 7 -4 2 2963.51 128.09 7 -4 3 3923.20 156.04 7 -4 4 1231.50 100.00 7 -4 5 148.93 26.90 7 -4 6 330.12 36.75 7 -4 7 7.76 23.30 7 -4 8 65.15 26.81 7 -4 9 389.81 44.53 7 -4 10 622.75 52.69 7 -4 11 168.66 57.00 7 -4 12 52.52 52.00 7 -3 0 573.26 68.00 7 -3 1 719.50 53.32 7 -3 2 136.92 19.65 7 -3 3 522.90 57.50 7 -3 4 100.43 36.50 7 -3 5 5.28 20.87 7 -3 6 927.61 62.17 7 -3 7 1384.72 130.00 7 -3 8 786.95 62.95 7 -3 9 11.36 27.13 7 -3 10 732.41 112.00 7 -3 11 23.13 47.00 7 -3 12 4.38 48.00 7 -3 13 2.36 49.00 7 -2 0 81.78 27.00 7 -2 1 542.40 38.00 7 -2 2 173.00 25.91 7 -2 3 641.90 97.00 7 -2 4 1643.30 79.67 7 -2 5 1917.89 82.10 7 -2 6 3963.98 149.02 7 -2 7 2983.75 150.00 7 -2 8 62.85 34.00 7 -2 9 1389.70 73.99 7 -2 10 397.79 90.00 7 -2 11 159.84 35.02 7 -2 12 105.33 50.00 7 -2 13 162.28 55.00 7 -1 0 1228.60 77.00 7 -1 1 477.26 50.00 7 -1 2 2554.15 104.50 7 -1 3 333.12 60.50 7 -1 4 0.07 16.08 7 -1 5 697.67 50.00 7 -1 6 434.94 58.00 7 -1 7 5.03 20.78 7 -1 8 340.60 86.50 7 -1 9 1119.78 64.06 7 -1 10 962.72 132.50 7 -1 11 106.69 30.51 7 -1 12 31.42 27.63 7 -1 13 4.57 47.00 7 -1 14 0.37 50.00 7 0 0 117.72 23.00 7 0 1 1.91 17.00 7 0 2 433.14 51.00 7 0 3 422.78 34.50 7 0 4 1744.30 73.50 7 0 5 5.25 16.93 7 0 6 36.43 20.00 7 0 7 102.97 22.63 7 0 8 16.52 21.56 7 0 9 57.98 25.04 7 0 10 1766.19 91.52 7 0 11 993.71 78.00 7 0 12 96.14 30.27 7 0 13 291.31 55.00 7 0 14 42.45 50.00 7 1 0 16.24 9.42 7 1 1 644.16 50.47 7 1 2 398.15 49.00 7 1 3 2213.02 244.00 7 1 4 6230.41 221.29 7 1 5 324.93 36.16 7 1 6 997.22 49.05 7 1 7 890.31 50.38 7 1 8 114.73 22.59 7 1 9 106.91 25.50 7 1 10 162.75 27.87 7 1 11 1743.49 123.00 7 1 12 16.17 26.89 7 1 13 221.17 34.45 7 1 14 0.54 44.00 7 1 15 4.89 52.00 7 2 0 54.81 7.80 7 2 1 1437.48 46.00 7 2 2 1516.50 117.00 7 2 3 47.10 12.95 7 2 4 1349.39 47.70 7 2 5 385.15 32.10 7 2 6 66.13 10.89 7 2 7 313.33 40.23 7 2 8 32.20 21.89 7 2 9 672.30 49.11 7 2 10 19.60 24.01 7 2 11 2127.66 116.50 7 2 12 922.24 65.66 7 2 13 158.54 31.32 7 2 14 45.55 46.00 7 2 15 0.36 49.00 7 3 0 0.85 29.95 7 3 1 43.15 11.77 7 3 2 1267.01 99.00 7 3 3 998.70 79.00 7 3 4 16.80 13.38 7 3 5 1034.66 38.62 7 3 6 1087.60 40.57 7 3 7 5.48 12.47 7 3 8 15.82 18.34 7 3 9 634.56 47.73 7 3 10 324.97 39.55 7 3 11 62.66 27.16 7 3 12 247.09 34.95 7 3 13 62.00 31.02 7 3 14 687.21 59.79 7 3 15 266.74 60.00 7 4 0 1347.15 93.11 7 4 1 8153.13 328.00 7 4 2 118.16 25.00 7 4 3 2.53 9.80 7 4 4 531.08 70.00 7 4 5 188.17 26.00 7 4 6 156.44 29.15 7 4 7 4.74 11.57 7 4 8 1.85 12.60 7 4 9 3.45 19.92 7 4 10 0.09 22.06 7 4 11 68.48 26.43 7 4 12 683.97 51.97 7 4 13 175.07 36.29 7 4 14 29.95 31.09 7 4 15 254.61 56.00 7 5 0 132.08 38.00 7 5 1 5387.02 219.81 7 5 2 18.77 15.36 7 5 3 497.44 79.00 7 5 4 0.23 18.00 7 5 5 68.33 20.65 7 5 6 1.94 16.07 7 5 7 3.55 12.17 7 5 8 347.26 34.52 7 5 9 47.49 16.45 7 5 10 9.75 21.27 7 5 11 13.19 24.27 7 5 12 880.23 56.84 7 5 13 1692.77 209.50 7 5 14 220.99 34.45 7 5 15 0.80 31.46 7 6 0 3551.97 134.83 7 6 1 91.86 28.00 7 6 2 4963.01 156.04 7 6 3 0.18 22.00 7 6 4 101.16 26.00 7 6 5 9.26 26.00 7 6 6 281.48 35.50 7 6 7 173.35 20.07 7 6 8 1544.19 52.56 7 6 9 2626.60 94.96 7 6 10 2514.22 89.89 7 6 11 138.66 26.67 7 6 12 1.87 24.73 7 6 13 33.13 29.75 7 6 14 626.56 56.56 7 6 15 56.12 33.45 7 7 0 66.29 15.90 7 7 1 253.15 80.00 7 7 2 33.69 23.49 7 7 3 404.85 48.09 7 7 4 1067.40 112.00 7 7 5 402.50 29.00 7 7 6 21.57 20.36 7 7 7 159.19 48.00 7 7 8 1072.43 64.45 7 7 9 1165.42 53.33 7 7 10 737.30 64.09 7 7 11 72.20 25.95 7 7 12 0.32 25.19 7 7 13 0.49 27.60 7 7 14 356.74 48.00 7 8 0 844.30 86.00 7 8 1 1311.07 87.68 7 8 2 29.28 17.68 7 8 3 1586.43 87.89 7 8 4 3011.91 172.00 7 8 516201.99 987.00 7 8 610125.35 341.82 7 8 7 941.17 92.00 7 8 8 134.33 35.00 7 8 9 3340.16 141.90 7 8 10 981.61 59.79 7 8 11 657.18 60.21 7 8 12 0.56 41.00 7 8 13 43.23 46.00 7 8 14 177.21 52.00 7 9 0 59.46 21.18 7 9 1 615.55 79.00 7 9 212883.54 423.14 7 9 3 118.90 24.39 7 9 4 73.15 20.85 7 9 5 262.32 52.00 7 9 6 4.04 18.34 7 9 7 217.19 32.00 7 9 8 204.76 41.00 7 9 9 1611.46 78.73 7 9 10 1221.44 81.16 7 9 11 804.63 57.52 7 9 12 0.02 39.00 7 9 13 309.08 55.00 7 10 0 2979.39 120.57 7 10 1 9810.73 399.37 7 10 2 832.29 141.00 7 10 3 116.07 24.39 7 10 4 859.30 61.36 7 10 5 936.76 67.71 7 10 6 964.71 74.23 7 10 7 111.01 55.50 7 10 8 10.33 20.78 7 10 9 491.48 55.92 7 10 10 1000.54 59.76 7 10 11 173.17 42.50 7 10 12 11.09 24.50 7 11 0 1361.85 82.61 7 11 1 2984.49 119.59 7 11 2 5200.74 213.56 7 11 3 29.38 47.50 7 11 4 258.62 53.00 7 11 5 527.94 109.50 7 11 6 483.29 45.00 7 11 7 67.08 28.47 7 11 8 0.00 21.07 7 11 9 27.72 25.00 7 11 10 736.06 65.35 7 11 11 52.73 24.99 7 11 12 19.66 25.91 7 12 0 235.67 51.00 7 12 1 188.21 58.00 7 12 2 770.24 81.00 7 12 3 206.87 30.05 7 12 4 335.44 52.00 7 12 5 51.21 36.50 7 12 6 107.19 44.50 7 12 7 23.77 22.27 7 12 8 33.80 23.62 7 12 9 291.45 31.50 7 12 10 74.87 24.99 7 13 0 64.96 30.00 7 13 1 38.23 42.00 7 13 2 811.88 66.04 7 13 3 56.42 26.45 7 13 4 284.05 50.00 7 13 5 48.78 25.80 7 13 6 4.18 23.68 7 13 7 96.04 28.18 7 13 8 49.06 25.74 7 13 9 42.42 25.34 7 14 0 176.40 54.00 7 14 1 438.26 64.00 7 14 2 423.56 69.00 7 14 3 619.18 67.00 7 14 4 39.79 29.67 7 14 5 127.86 32.87 7 14 6 75.55 46.00 8 -7 0 16.64 24.50 8 -7 1 136.44 30.27 8 -7 2 9.18 26.62 8 -7 3 48.05 30.01 8 -7 4 70.42 30.75 8 -7 5 29.19 32.50 8 -6 0 60.67 56.00 8 -6 1 776.98 57.71 8 -6 2 274.45 26.68 8 -6 3 19.00 24.99 8 -6 4 15.68 26.67 8 -6 5 3.15 26.81 8 -6 6 171.79 35.32 8 -6 7 14.31 30.15 8 -6 8 118.24 32.36 8 -5 0 705.28 49.67 8 -5 1 30.65 20.34 8 -5 2 662.27 52.58 8 -5 3 37.64 23.05 8 -5 4 13.97 24.02 8 -5 5 2.39 26.18 8 -5 6 2.68 26.61 8 -5 7 66.04 31.47 8 -5 8 322.63 41.27 8 -5 9 41.55 39.00 8 -4 0 6.23 17.30 8 -4 1 16.58 20.18 8 -4 2 1962.70 90.52 8 -4 3 415.95 37.08 8 -4 4 293.93 36.77 8 -4 5 577.36 42.74 8 -4 6 1386.65 80.40 8 -4 7 576.69 55.93 8 -4 8 84.13 29.95 8 -4 9 1835.02 91.26 8 -4 10 551.67 113.00 8 -3 0 194.44 18.98 8 -3 1 317.26 46.50 8 -3 2 1359.30 65.35 8 -3 3 351.78 60.50 8 -3 4 338.39 79.00 8 -3 5 2647.21 108.65 8 -3 6 3384.43 145.15 8 -3 7 2201.47 101.56 8 -3 8 484.75 71.00 8 -3 9 352.52 39.83 8 -3 10 227.84 59.50 8 -3 11 648.93 93.00 8 -2 0 3873.60 167.85 8 -2 1 6262.23 221.27 8 -2 2 3723.11 139.21 8 -2 3 2812.29 110.14 8 -2 4 603.62 51.17 8 -2 5 203.85 33.50 8 -2 6 1169.16 70.47 8 -2 7 372.33 34.56 8 -2 8 39.33 27.00 8 -2 9 1145.18 73.46 8 -2 10 88.04 30.99 8 -2 11 111.17 32.16 8 -2 12 147.00 53.00 8 -1 0 229.42 33.00 8 -1 1 2718.83 166.00 8 -1 2 6544.56 282.50 8 -1 3 3827.06 158.50 8 -1 4 1064.06 67.71 8 -1 5 243.82 25.04 8 -1 6 872.77 53.06 8 -1 7 822.19 61.08 8 -1 8 25.94 24.92 8 -1 9 367.05 35.33 8 -1 10 83.30 28.05 8 -1 11 23.88 28.76 8 -1 12 61.43 29.07 8 -1 13 0.44 49.00 8 0 0 76.36 19.00 8 0 1 53.70 22.00 8 0 2 251.54 52.00 8 0 3 94.51 22.50 8 0 4 32.07 17.50 8 0 5 138.90 22.27 8 0 6 6.66 20.07 8 0 7 65.47 25.04 8 0 8 370.98 32.17 8 0 9 237.61 31.82 8 0 10 28.36 27.00 8 0 11 17.25 26.76 8 0 12 84.40 29.47 8 0 13 72.64 51.00 8 1 0 1315.09 73.69 8 1 1 2.23 10.81 8 1 2 23.77 17.00 8 1 3 4.93 15.90 8 1 4 287.45 36.29 8 1 5 2.85 17.31 8 1 6 169.74 22.27 8 1 7 193.66 26.51 8 1 8 9.59 21.21 8 1 9 47.21 25.09 8 1 10 267.56 33.94 8 1 11 69.67 28.18 8 1 12 34.21 28.89 8 1 13 2.07 28.05 8 1 14 1.09 46.00 8 2 0 178.98 24.83 8 2 1 593.28 44.66 8 2 2 9.68 12.02 8 2 3 6.90 12.36 8 2 4 1.15 10.17 8 2 5 1533.88 56.00 8 2 6 864.71 40.24 8 2 7 28.62 19.44 8 2 8 179.25 27.05 8 2 9 591.03 56.50 8 2 10 273.79 33.21 8 2 11 97.36 28.26 8 2 12 100.45 29.60 8 2 13 276.66 37.12 8 2 14 57.19 48.00 8 3 0 41.75 18.50 8 3 1 546.77 71.00 8 3 2 7251.84 399.00 8 3 3 3082.43 174.00 8 3 4 194.71 23.00 8 3 5 971.77 46.43 8 3 6 1073.91 42.12 8 3 7 22.04 12.56 8 3 8 394.90 28.05 8 3 9 1498.27 81.67 8 3 10 593.37 50.19 8 3 11 78.27 27.33 8 3 12 1.91 27.16 8 3 13 0.71 27.58 8 3 14 372.30 41.70 8 4 0 83.53 19.00 8 4 1 620.42 41.53 8 4 2 6401.31 339.00 8 4 3 2873.55 192.00 8 4 4 285.34 28.00 8 4 5 985.69 64.21 8 4 6 955.60 41.28 8 4 7 1162.46 44.52 8 4 8 886.08 50.60 8 4 9 1213.77 58.69 8 4 10 1084.37 65.01 8 4 11 357.94 53.00 8 4 12 11.52 27.76 8 4 13 22.07 31.18 8 4 14 810.29 69.83 8 5 0 122.62 18.34 8 5 1 106.29 16.61 8 5 2 4.90 15.51 8 5 3 586.48 77.00 8 5 4 21.04 23.00 8 5 5 103.86 16.79 8 5 6 623.37 47.32 8 5 7 393.93 36.68 8 5 8 123.61 15.24 8 5 9 5.74 15.24 8 5 10 1089.14 62.58 8 5 11 239.89 31.23 8 5 12 960.74 63.28 8 5 13 3276.86 137.88 8 5 14 1429.91 84.84 8 6 0 7.26 16.97 8 6 1 3623.60 172.56 8 6 2 111.07 21.78 8 6 3 30.41 22.00 8 6 4 115.05 33.00 8 6 5 1144.47 100.00 8 6 6 902.52 62.50 8 6 7 122.65 30.50 8 6 8 166.31 21.00 8 6 9 5707.40 179.32 8 6 10 2106.04 76.70 8 6 11 309.18 34.36 8 6 12 22.57 26.90 8 6 13 182.98 35.08 8 6 14 0.00 30.01 8 7 0 596.13 56.43 8 7 112539.57 419.00 8 7 2 6564.28 236.91 8 7 3 1871.10 113.18 8 7 4 1247.51 102.00 8 7 5 3674.11 140.53 8 7 610802.42 433.35 8 7 7 2348.87 104.36 8 7 8 2194.10 104.60 8 7 9 2275.09 105.41 8 7 10 549.08 51.39 8 7 11 129.74 45.00 8 7 12 677.68 80.00 8 7 13 62.61 48.00 8 7 14 154.87 53.00 8 8 0 2.73 20.47 8 8 1 689.04 120.00 8 8 2 6465.56 282.61 8 8 3 42.26 38.00 8 8 4 4240.82 160.75 8 8 515713.95 552.81 8 8 6 4325.38 182.51 8 8 7 508.46 53.58 8 8 8 779.95 58.51 8 8 9 845.18 60.50 8 8 10 0.50 22.01 8 8 11 24.76 23.48 8 8 12 150.39 50.00 8 8 13 38.87 48.00 8 9 0 335.60 35.00 8 9 1 9235.72 350.67 8 9 2 2029.73 156.50 8 9 3 9838.46 350.81 8 9 4 2668.88 115.42 8 9 5 1646.10 87.17 8 9 6 23.75 20.47 8 9 7 129.38 32.00 8 9 8 0.03 20.64 8 9 9 74.01 25.23 8 9 10 498.16 85.00 8 9 11 231.48 76.00 8 9 12 261.48 57.00 8 9 13 0.40 45.00 8 10 0 207.60 30.50 8 10 1 1144.91 68.08 8 10 2 7668.26 299.28 8 10 3 69.66 26.84 8 10 4 1107.38 92.00 8 10 5 608.64 59.16 8 10 6 609.53 60.94 8 10 7 395.93 87.00 8 10 8 124.07 51.50 8 10 9 41.10 24.74 8 10 10 352.20 37.50 8 10 11 300.77 65.50 8 10 12 221.21 37.50 8 11 0 156.25 40.00 8 11 1 827.01 60.83 8 11 2 1.16 23.62 8 11 3 151.95 25.80 8 11 4 1832.93 91.27 8 11 5 1158.20 67.83 8 11 6 78.80 35.50 8 11 7 46.25 23.62 8 11 8 42.24 24.20 8 11 9 7.29 23.21 8 11 10 35.44 24.50 8 11 11 11.01 23.55 8 12 0 347.09 58.00 8 12 1 0.69 23.76 8 12 2 288.08 41.00 8 12 3 583.07 63.98 8 12 4 113.76 28.28 8 12 5 277.32 62.00 8 12 6 9.29 23.33 8 12 7 0.25 22.97 8 12 8 68.47 24.39 8 12 9 54.87 25.19 8 12 10 96.34 26.62 8 13 0 28.70 26.76 8 13 1 60.01 28.05 8 13 2 1656.54 86.73 8 13 3 97.99 30.00 8 13 4 64.98 40.00 8 13 5 83.35 27.92 8 13 6 9.37 25.43 8 13 7 30.22 26.45 8 13 8 176.73 30.18 8 14 0 265.20 51.50 8 14 1 62.43 45.00 8 14 2 345.37 68.00 8 14 3 222.17 51.00 8 14 4 64.60 30.38 8 14 5 172.87 54.00 9 -6 0 14.90 24.99 9 -6 1 12.59 19.50 9 -6 2 267.81 30.77 9 -6 3 290.23 36.52 9 -6 4 371.98 47.02 9 -5 0 429.97 45.29 9 -5 1 245.76 38.00 9 -5 2 7.57 23.48 9 -5 3 3.52 24.21 9 -5 4 27.57 27.39 9 -5 5 14.99 29.30 9 -5 6 2.64 30.27 9 -5 7 16.86 33.14 9 -4 0 645.27 49.98 9 -4 1 356.24 39.24 9 -4 2 397.88 38.50 9 -4 3 305.11 38.42 9 -4 4 0.08 23.27 9 -4 5 11.39 26.17 9 -4 6 41.81 30.27 9 -4 7 71.83 31.20 9 -4 8 29.29 31.95 9 -4 9 14.45 33.38 9 -3 0 518.83 44.87 9 -3 1 10.57 19.70 9 -3 2 72.81 24.02 9 -3 3 1.44 21.78 9 -3 4 4.36 23.92 9 -3 5 563.27 54.00 9 -3 6 1247.81 74.46 9 -3 7 695.29 59.57 9 -3 8 20.81 30.46 9 -3 9 599.93 61.03 9 -3 10 869.72 71.56 9 -2 0 320.16 33.59 9 -2 1 54.65 20.07 9 -2 2 958.20 63.22 9 -2 3 4374.41 158.69 9 -2 4 188.74 27.16 9 -2 5 112.27 26.05 9 -2 6 797.15 57.80 9 -2 7 344.67 35.98 9 -2 8 53.21 30.31 9 -2 9 270.37 38.49 9 -2 10 749.31 140.00 9 -2 11 40.85 31.70 9 -1 0 4769.19 191.93 9 -1 1 106.25 20.47 9 -1 2 649.75 52.96 9 -1 3 26.48 20.51 9 -1 4 83.57 22.97 9 -1 5 250.91 30.05 9 -1 6 247.49 33.00 9 -1 7 473.49 51.10 9 -1 8 454.20 65.50 9 -1 9 0.07 27.16 9 -1 10 254.42 72.50 9 -1 11 632.23 59.50 9 -1 12 770.23 63.78 9 0 0 180.68 51.50 9 0 1 53.36 17.64 9 0 2 123.62 22.97 9 0 3 173.35 20.85 9 0 4 648.84 45.11 9 0 5 746.57 52.51 9 0 6 598.46 50.11 9 0 7 206.72 29.70 9 0 8 14.87 26.13 9 0 9 511.58 52.34 9 0 10 785.25 63.45 9 0 11 135.00 38.50 9 0 12 572.88 75.00 9 1 0 104.84 16.52 9 1 1 735.53 43.28 9 1 2 0.84 15.09 9 1 3 18.28 17.06 9 1 4 399.14 41.32 9 1 5 581.16 43.38 9 1 6 70.24 22.27 9 1 7 30.41 22.59 9 1 8 405.79 48.02 9 1 9 62.81 26.45 9 1 10 11.96 26.13 9 1 11 141.62 31.80 9 1 12 399.38 40.94 9 1 13 196.34 37.00 9 2 0 1105.29 46.44 9 2 1 1494.73 56.58 9 2 2 635.48 45.38 9 2 3 978.10 60.50 9 2 4 1.88 16.08 9 2 5 64.65 26.50 9 2 6 23.08 19.05 9 2 7 340.52 52.50 9 2 8 947.52 54.39 9 2 9 1575.93 80.60 9 2 10 187.75 30.18 9 2 11 69.09 28.58 9 2 12 133.68 32.50 9 2 13 580.11 60.50 9 3 0 1041.68 61.42 9 3 1 0.57 10.73 9 3 2 2839.58 109.49 9 3 3 261.48 41.50 9 3 4 483.57 36.29 9 3 5 3.77 11.85 9 3 6 149.85 24.48 9 3 7 23.00 20.07 9 3 8 32.29 21.61 9 3 9 540.88 48.79 9 3 10 8.93 25.46 9 3 11 0.17 26.34 9 3 12 0.17 43.00 9 3 13 4.14 30.31 9 4 0 4177.34 172.56 9 4 1 83.70 32.50 9 4 2 1564.21 76.88 9 4 3 13.00 22.00 9 4 4 5.00 16.58 9 4 5 1407.35 55.91 9 4 6 2579.86 76.49 9 4 7 568.09 40.71 9 4 8 361.47 32.45 9 4 9 570.59 51.56 9 4 10 2282.47 97.93 9 4 11 1328.45 76.99 9 4 12 129.58 33.03 9 4 13 529.38 59.50 9 5 0 1716.70 72.52 9 5 1 688.73 85.50 9 5 2 289.84 58.50 9 5 3 38.27 19.21 9 5 4 18.57 16.50 9 5 5 5.91 16.22 9 5 6 264.64 32.50 9 5 7 1338.67 76.28 9 5 8 1599.62 79.20 9 5 9 2597.59 116.28 9 5 10 2808.37 169.00 9 5 11 1169.61 100.00 9 5 12 290.34 58.00 9 5 13 303.19 62.00 9 6 0 1185.05 77.59 9 6 1 6810.03 253.00 9 6 2 190.25 61.00 9 6 3 1321.04 77.59 9 6 4 0.34 16.93 9 6 5 872.52 63.15 9 6 6 50.95 18.74 9 6 7 66.51 20.14 9 6 8 29.31 25.50 9 6 9 47.35 20.14 9 6 10 411.96 75.00 9 6 11 69.50 44.00 9 6 12 93.81 49.00 9 6 13 0.00 46.00 9 7 0 90.20 19.76 9 7 1 2385.89 124.50 9 7 2 2378.66 94.60 9 7 3 62.72 22.20 9 7 4 838.21 60.51 9 7 5 5219.15 204.72 9 7 6 7086.92 269.19 9 7 7 6193.78 234.14 9 7 8 793.66 63.35 9 7 9 1789.84 95.26 9 7 10 1164.38 85.50 9 7 11 881.66 86.00 9 7 12 247.46 58.00 9 7 13 10.66 47.00 9 8 0 14.73 20.07 9 8 1 127.07 27.55 9 8 2 1426.17 114.50 9 8 3 8132.10 306.53 9 8 4 2993.14 132.27 9 8 5 103.87 22.20 9 8 6 91.65 22.78 9 8 7 44.28 22.82 9 8 8 1.20 22.33 9 8 9 45.36 22.94 9 8 10 1132.03 68.81 9 8 11 1638.52 95.26 9 8 12 463.07 63.00 9 9 0 140.89 27.55 9 9 1 4189.01 162.30 9 9 215402.79 561.80 9 9 3 31.49 22.63 9 9 4 1395.98 75.41 9 9 5 3220.81 148.78 9 9 6 1121.64 71.84 9 9 7 546.53 59.57 9 9 8 2320.74 101.94 9 9 9 8.40 23.05 9 9 10 1027.30 71.04 9 9 11 1359.92 77.54 9 9 12 166.71 31.20 9 10 0 490.72 52.00 9 10 1 23.91 24.33 9 10 2 1555.61 88.66 9 10 3 127.21 48.00 9 10 4 6.08 22.27 9 10 5 1064.15 67.98 9 10 6 1675.05 86.91 9 10 7 349.26 59.00 9 10 8 1318.18 82.71 9 10 9 486.37 56.81 9 10 10 136.69 29.00 9 10 11 24.94 24.79 9 11 0 0.39 23.49 9 11 1 0.03 23.92 9 11 2 96.64 28.99 9 11 3 35.50 26.13 9 11 4 653.33 57.89 9 11 5 2371.26 113.01 9 11 6 3069.88 137.38 9 11 7 108.80 27.05 9 11 8 197.30 30.01 9 11 9 7.01 24.02 9 11 10 112.57 27.63 9 12 0 0.01 25.46 9 12 1 256.34 44.00 9 12 2 46.35 28.05 9 12 3 534.12 85.50 9 12 4 8.45 25.74 9 12 5 0.18 24.39 9 12 6 15.51 24.75 9 12 7 107.04 41.00 9 12 8 65.20 26.76 9 12 9 186.13 32.00 9 13 0 32.93 37.50 9 13 1 361.32 77.50 9 13 2 803.43 69.19 9 13 3 814.85 67.70 9 13 4 18.49 26.84 9 13 5 5.39 25.74 9 13 6 102.80 29.70 9 13 7 335.24 50.00 9 14 0 26.66 30.01 9 14 1 141.86 49.50 9 14 2 41.44 31.61 9 14 3 39.31 29.90 10 -5 0 586.31 52.36 10 -5 1 394.34 66.00 10 -5 2 301.32 38.67 10 -5 3 1328.37 76.56 10 -4 0 210.24 30.46 10 -4 1 313.07 33.59 10 -4 2 156.77 30.90 10 -4 3 31.40 26.67 10 -4 4 98.94 30.90 10 -4 5 7.14 29.19 10 -4 6 137.67 35.29 10 -3 0 903.13 55.01 10 -3 1 614.73 52.62 10 -3 2 430.70 40.94 10 -3 3 28.22 24.48 10 -3 4 4.20 24.92 10 -3 5 48.94 44.50 10 -3 6 1118.42 73.88 10 -3 7 1142.37 72.00 10 -3 8 598.56 60.54 10 -2 0 0.94 19.05 10 -2 1 3.78 20.07 10 -2 2 875.86 57.80 10 -2 3 3669.10 149.15 10 -2 4 1854.91 89.67 10 -2 5 11.43 25.34 10 -2 6 0.76 26.13 10 -2 7 0.37 28.89 10 -2 8 45.65 31.41 10 -2 9 14.87 31.89 10 -1 0 207.27 26.13 10 -1 1 936.01 91.50 10 -1 2 2877.33 112.03 10 -1 3 488.22 48.41 10 -1 4 150.37 26.16 10 -1 5 212.77 30.05 10 -1 6 219.56 32.17 10 -1 7 292.18 37.12 10 -1 8 252.26 35.36 10 -1 9 340.15 42.74 10 -1 10 697.74 65.06 10 0 0 952.30 55.42 10 0 1 258.27 24.63 10 0 2 1133.17 68.55 10 0 3 206.05 24.92 10 0 4 247.51 26.76 10 0 5 1.82 20.85 10 0 6 27.08 24.01 10 0 7 98.31 28.28 10 0 8 33.85 27.58 10 0 9 238.03 45.00 10 0 10 29.64 31.46 10 0 11 5.07 29.47 10 1 0 39.08 17.77 10 1 1 211.70 19.92 10 1 2 35.58 20.50 10 1 3 1.06 17.06 10 1 4 17.42 21.07 10 1 5 180.97 30.00 10 1 6 451.00 45.41 10 1 7 220.77 28.58 10 1 8 13.75 24.33 10 1 9 42.81 30.00 10 1 10 20.06 29.29 10 1 11 3.81 30.31 10 2 0 46.86 18.47 10 2 1 975.30 47.36 10 2 2 720.40 47.73 10 2 3 719.33 51.94 10 2 4 280.41 22.82 10 2 5 3.16 19.92 10 2 6 10.93 20.36 10 2 7 31.90 22.50 10 2 8 85.17 27.76 10 2 9 101.83 32.50 10 2 10 96.35 29.90 10 2 11 48.21 30.70 10 2 12 0.06 30.31 10 3 0 2978.49 116.95 10 3 1 245.73 31.00 10 3 2 1.76 14.23 10 3 3 664.13 38.53 10 3 4 58.89 20.42 10 3 5 305.92 39.24 10 3 6 169.97 25.19 10 3 7 25.06 21.61 10 3 8 1653.10 81.67 10 3 9 1976.67 93.69 10 3 10 3002.81 123.39 10 3 11 1899.32 94.38 10 3 12 498.40 46.54 10 4 0 1380.00 60.31 10 4 1 529.65 47.91 10 4 2 0.05 16.79 10 4 3 1126.59 74.50 10 4 4 586.11 61.50 10 4 5 466.02 45.99 10 4 6 379.12 61.00 10 4 7 170.32 40.00 10 4 8 1456.05 107.00 10 4 9 13.49 39.00 10 4 10 0.16 41.00 10 4 11 0.00 44.00 10 4 12 41.88 48.00 10 5 0 7.73 17.68 10 5 1 953.30 60.42 10 5 2 1009.03 68.47 10 5 3 181.59 55.50 10 5 4 312.93 54.50 10 5 5 1.20 17.30 10 5 6 775.19 58.18 10 5 7 386.97 49.00 10 5 8 236.03 75.50 10 5 9 40.76 39.00 10 5 10 126.55 48.00 10 5 11 354.47 58.00 10 5 12 291.03 60.00 10 6 0 111.57 24.33 10 6 1 39.27 20.14 10 6 2 6127.64 240.17 10 6 3 240.51 33.00 10 6 4 18.44 18.34 10 6 5 1164.05 67.34 10 6 6 16.58 19.92 10 6 7 162.25 24.73 10 6 8 170.30 46.00 10 6 9 1076.26 69.30 10 6 10 975.50 66.11 10 6 11 278.26 56.00 10 6 12 0.01 46.00 10 7 0 1983.25 108.53 10 7 1 519.87 55.49 10 7 2 2246.61 95.31 10 7 3 13.77 19.09 10 7 4 38.61 29.00 10 7 5 783.22 62.22 10 7 6 544.94 51.66 10 7 7 182.67 27.63 10 7 8 3693.16 151.13 10 7 9 82.11 23.86 10 7 10 32.46 22.75 10 7 11 101.82 49.00 10 7 12 8.95 46.00 10 8 0 126.03 54.00 10 8 1 1255.53 70.76 10 8 2 203.27 41.50 10 8 3 133.88 28.00 10 8 4 5.10 20.14 10 8 5 33.59 22.50 10 8 6 100.95 25.19 10 8 7 857.25 62.43 10 8 8 2146.98 101.65 10 8 9 14.86 23.48 10 8 10 9.47 24.04 10 8 11 14.32 24.60 10 9 0 292.91 44.00 10 9 1 673.71 74.50 10 9 2 788.25 62.34 10 9 3 403.67 53.50 10 9 4 43.42 24.72 10 9 5 217.30 43.50 10 9 6 2.56 22.91 10 9 7 656.28 61.97 10 9 8 469.80 56.22 10 9 9 216.65 37.00 10 9 10 550.16 57.95 10 9 11 22.32 25.88 10 10 0 98.54 28.50 10 10 1 382.98 81.50 10 10 2 1911.55 105.95 10 10 3 56.99 27.55 10 10 4 22.10 24.04 10 10 5 537.18 60.94 10 10 6 705.46 60.50 10 10 7 17.53 23.76 10 10 8 98.21 27.13 10 10 9 23.28 24.74 10 10 10 92.03 27.85 10 11 0 234.01 59.50 10 11 1 21.99 25.74 10 11 2 272.67 42.50 10 11 3 110.63 34.00 10 11 4 7.73 24.33 10 11 5 38.09 26.84 10 11 6 141.56 31.50 10 11 7 7.16 23.62 10 11 8 15.50 24.63 10 11 9 33.68 24.99 10 12 0 16.51 27.60 10 12 1 51.88 33.50 10 12 2 6.25 28.05 10 12 3 797.70 69.74 10 12 4 415.47 82.50 10 12 5 102.98 28.26 10 12 6 31.48 26.84 10 12 7 41.99 27.05 10 13 0 144.03 62.00 10 13 1 65.22 52.50 10 13 2 301.07 64.50 10 13 3 7.52 28.76 10 13 4 142.15 33.58 10 13 5 27.97 27.92 11 -3 0 670.46 53.06 11 -3 1 47.42 24.92 11 -3 2 7.09 23.76 11 -3 3 20.31 26.62 11 -3 4 14.28 28.05 11 -2 0 13.43 21.50 11 -2 1 56.35 23.62 11 -2 2 545.86 51.37 11 -2 3 1165.53 68.32 11 -2 4 468.33 58.00 11 -2 5 120.77 31.11 11 -2 6 401.44 79.50 11 -1 0 180.60 26.13 11 -1 1 103.17 23.30 11 -1 2 281.05 32.17 11 -1 3 156.30 27.16 11 -1 4 0.38 22.97 11 -1 5 2.54 24.72 11 -1 6 0.00 25.43 11 -1 7 31.71 29.70 11 0 0 123.39 27.00 11 0 1 245.19 26.76 11 0 2 45.12 20.47 11 0 3 174.09 26.05 11 0 4 434.22 47.12 11 0 5 4.75 22.97 11 0 6 0.16 24.04 11 0 7 190.13 32.03 11 0 8 205.12 34.95 11 0 9 584.62 61.21 11 1 0 320.38 35.08 11 1 1 895.61 60.50 11 1 2 52.28 20.36 11 1 3 44.58 20.36 11 1 4 410.65 44.99 11 1 5 6.50 21.49 11 1 6 7.79 23.62 11 1 7 11.94 25.80 11 1 8 69.52 29.60 11 1 9 29.27 29.60 11 2 0 613.48 55.50 11 2 1 242.04 70.50 11 2 2 868.62 51.60 11 2 3 1470.40 73.87 11 2 4 396.85 43.77 11 2 5 281.20 28.58 11 2 6 59.02 25.63 11 2 7 0.43 23.21 11 2 8 266.59 32.74 11 2 9 6.31 43.00 11 2 10 121.29 51.00 11 3 0 450.28 60.00 11 3 1 424.46 58.00 11 3 2 708.05 67.00 11 3 3 7.25 29.00 11 3 4 25.19 31.00 11 3 5 102.91 36.00 11 3 6 1187.75 98.00 11 3 7 2350.61 141.00 11 3 8 876.82 81.00 11 3 9 8.07 41.00 11 3 10 38.91 42.00 11 4 0 240.41 64.00 11 4 1 523.43 64.00 11 4 2 2119.59 139.00 11 4 3 1030.07 77.00 11 4 4 452.93 61.00 11 4 5 10.34 30.00 11 4 6 247.96 49.00 11 4 7 159.58 41.00 11 4 8 0.01 36.00 11 4 9 228.40 55.00 11 4 10 10.75 43.00 11 5 0 35.21 21.89 11 5 1 3301.11 137.97 11 5 2 2941.37 138.82 11 5 3 2908.26 113.33 11 5 4 728.63 74.00 11 5 5 2.56 29.00 11 5 6 32.80 35.00 11 5 7 11.67 35.00 11 5 8 5.88 38.00 11 5 9 377.39 58.00 11 5 10 320.20 61.00 11 5 11 261.53 56.00 11 6 0 829.97 96.00 11 6 1 178.82 35.00 11 6 2 285.98 40.00 11 6 3 385.97 41.00 11 6 4 917.21 64.00 11 6 5 515.11 52.50 11 6 6 214.11 28.50 11 6 7 25.06 36.00 11 6 8 10.44 39.00 11 6 9 0.47 39.00 11 6 10 4.44 40.00 11 7 0 226.38 51.50 11 7 1 145.53 50.50 11 7 2 1829.31 96.08 11 7 3 53.71 22.91 11 7 4 705.40 100.00 11 7 5 292.69 40.00 11 7 6 61.51 23.05 11 7 7 258.36 40.00 11 7 8 1665.72 84.71 11 7 9 862.83 93.00 11 7 10 835.21 96.00 11 8 0 108.09 25.74 11 8 1 47.72 38.50 11 8 2 130.71 42.00 11 8 3 26.62 22.63 11 8 4 2.65 21.21 11 8 5 89.16 24.92 11 8 6 136.51 25.46 11 8 7 0.58 20.90 11 8 8 187.04 30.47 11 8 9 14.53 23.48 11 8 10 581.66 59.20 11 9 0 134.25 29.60 11 9 1 40.68 24.92 11 9 2 257.72 49.50 11 9 3 68.15 36.50 11 9 4 1.98 23.33 11 9 5 1121.38 75.21 11 9 6 2298.40 113.48 11 9 7 2210.12 104.93 11 9 8 138.01 28.11 11 9 9 308.60 56.00 11 10 0 1469.81 87.24 11 10 1 630.21 115.00 11 10 2 16.07 25.34 11 10 3 42.18 29.50 11 10 4 17.31 24.33 11 10 5 109.52 28.26 11 10 6 171.39 36.50 11 10 7 223.06 43.00 11 10 8 39.55 25.19 11 11 0 1079.75 71.56 11 11 1 142.09 38.50 11 11 2 24.45 27.05 11 11 3 14.38 26.62 11 11 4 21.44 26.45 11 11 5 71.25 27.58 11 11 6 191.29 41.00 11 11 7 5.02 25.04 11 12 0 327.84 40.85 11 12 1 174.25 48.00 11 12 2 445.07 91.00 11 12 3 431.48 76.50 11 12 4 520.29 92.00 11 12 5 174.99 33.94 12 -1 0 118.50 25.43 12 -1 1 78.40 24.04 12 -1 2 478.35 50.54 12 -1 3 1013.45 66.29 12 0 0 166.29 29.00 12 0 1 885.75 57.55 12 0 2 120.29 24.63 12 0 3 45.87 23.21 12 0 4 74.46 25.91 12 0 5 94.37 27.33 12 1 0 106.29 37.00 12 1 1 778.56 75.00 12 1 2 245.61 46.00 12 1 3 509.57 66.00 12 1 4 39.49 36.00 12 1 5 37.45 37.00 12 1 6 41.35 41.00 12 1 7 44.13 39.00 12 2 0 274.72 48.00 12 2 1 124.59 39.00 12 2 2 76.86 37.00 12 2 3 26.03 30.00 12 2 4 22.70 34.00 12 2 5 49.01 39.00 12 2 6 3.85 37.00 12 2 7 112.46 44.00 12 3 0 206.81 38.00 12 3 1 165.73 44.00 12 3 2 0.16 31.00 12 3 3 12.81 31.00 12 3 4 0.19 30.00 12 3 5 45.94 34.00 12 3 6 314.98 55.00 12 3 7 72.37 43.00 12 3 8 127.62 48.00 12 4 0 535.80 67.00 12 4 1 1033.79 79.00 12 4 2 40.19 34.00 12 4 3 767.18 74.00 12 4 4 487.42 53.00 12 4 5 25.49 36.00 12 4 6 65.93 38.00 12 4 7 251.35 51.00 12 4 8 783.09 84.00 12 5 0 95.34 34.00 12 5 1 3133.08 194.00 12 5 2 224.29 41.00 12 5 3 101.23 35.00 12 5 4 150.09 42.00 12 5 5 355.29 49.00 12 5 6 106.86 41.00 12 5 7 13.70 38.00 12 5 8 1130.80 98.00 12 6 0 405.18 46.00 12 6 1 444.86 47.00 12 6 2 1104.02 88.00 12 6 3 6.75 31.00 12 6 4 566.13 70.00 12 6 5 253.68 48.00 12 6 6 242.61 46.00 12 6 7 334.69 54.00 12 6 8 1327.61 109.00 12 7 0 78.91 27.58 12 7 1 1.21 22.27 12 7 2 1761.57 95.62 12 7 3 196.38 39.50 12 7 4 296.88 67.50 12 7 5 35.87 34.00 12 7 6 4.02 34.00 12 7 7 13.85 36.00 12 7 8 24.31 40.00 12 8 0 480.23 91.50 12 8 1 4.61 24.01 12 8 2 2196.22 108.33 12 8 3 2058.07 104.74 12 8 4 250.16 43.00 12 8 5 21.18 22.78 12 8 6 199.90 37.50 12 8 7 596.72 56.94 12 8 8 490.69 76.00 12 9 0 481.45 96.50 12 9 1 214.26 49.00 12 9 2 2.46 24.72 12 9 3 3.93 24.01 12 9 4 71.25 32.50 12 9 5 674.50 63.90 12 9 6 124.50 34.00 12 9 7 233.62 43.50 12 10 0 265.75 55.50 12 10 1 6.66 25.91 12 10 2 880.61 117.50 12 10 3 502.49 44.70 12 10 4 267.28 39.00 12 10 5 402.63 69.50 12 10 6 338.41 66.00 12 11 0 4.87 28.35 12 11 1 254.03 55.00 12 11 2 16.31 28.11 12 11 3 333.89 70.50 12 11 4 0.23 26.05 13 2 0 2139.81 138.00 13 2 1 3.23 33.00 13 2 2 0.55 32.00 13 2 3 19.35 33.00 13 3 0 1567.10 109.00 13 3 1 31.82 34.00 13 3 2 26.03 33.00 13 3 3 55.09 35.00 13 3 4 0.43 32.00 13 4 0 1166.81 95.00 13 4 1 77.30 36.00 13 4 2 304.93 50.00 13 4 3 414.92 64.00 13 4 4 368.20 52.00 13 4 5 224.80 49.00 13 5 0 0.13 32.00 13 5 1 6.90 33.00 13 5 2 8.35 36.00 13 5 3 40.43 35.00 13 5 4 141.05 40.00 13 5 5 147.45 42.00 13 6 0 383.97 63.00 13 6 1 11.28 33.00 13 6 2 0.66 33.00 13 6 3 43.05 34.00 13 6 4 0.70 32.00 13 6 5 44.75 37.00 13 7 0 284.33 52.00 13 7 1 106.90 37.00 13 7 2 96.75 38.00 13 7 3 253.48 50.00 13 7 4 426.92 54.00 13 7 5 33.91 38.00 13 8 0 1856.98 96.79 13 8 1 330.44 55.00 13 8 2 107.15 42.00 13 8 3 0.01 33.00 13 8 4 63.90 39.00 13 9 0 1182.87 79.55 13 9 1 137.77 53.00 13 9 2 8.20 26.05 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 34518 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N2 N -0.1076(4) 1.1169(3) 1.4455(3) 0.0891(11) Uani 1 1 d . U . . . N3 N 0.0165(2) 0.29901(19) 0.79594(19) 0.0391(6) Uani 1 1 d . . . . . O1 O 0.63867(16) 0.59231(16) 0.97824(16) 0.0401(5) Uani 1 1 d . . . . . O2 O 0.4716(2) 1.16935(18) 0.81393(15) 0.0445(6) Uani 1 1 d . . . . . O3 O 0.38076(16) 1.04250(15) 0.79850(13) 0.0296(4) Uani 1 1 d . . . . . O4 O 0.31152(16) 1.06612(15) 1.10856(14) 0.0323(5) Uani 1 1 d . . . . . O5 O 0.23706(14) 0.92685(13) 1.09060(12) 0.0236(4) Uani 1 1 d . . . . . O6 O -0.04233(15) 0.76185(14) 0.98229(14) 0.0308(5) Uani 1 1 d . . . . . O7 O 0.16485(14) 0.69797(13) 0.93487(12) 0.0234(4) Uani 1 1 d . . . . . N1 N 0.459(3) 1.1641(16) 0.3730(19) 0.082(4) Uani 0.5 1 d . U P A 1 O8 O 0.3932(7) 1.1329(7) 0.3315(5) 0.0666(19) Uani 0.5 1 d . U P A 1 O9 O 0.5444(15) 1.1932(11) 0.3399(12) 0.082(3) Uani 0.5 1 d . U P A 1 N1' N 0.442(2) 1.1965(18) 0.3801(17) 0.081(3) Uani 0.5 1 d . U P A 2 O8' O 0.3456(11) 1.2025(12) 0.3338(7) 0.120(3) Uani 0.5 1 d . U P A 2 O9' O 0.5113(18) 1.2408(11) 0.3439(13) 0.091(4) Uani 0.5 1 d . U P A 2 O10 O -0.1601(3) 1.0514(3) 1.4689(2) 0.0853(10) Uani 1 1 d . . . . . O11 O -0.1262(4) 1.2044(3) 1.4834(3) 0.1084(11) Uani 1 1 d . U . . . O12 O -0.0860(2) 0.28742(18) 0.80410(18) 0.0526(6) Uani 1 1 d . . . . . O13 O 0.1131(2) 0.23027(17) 0.75936(17) 0.0524(6) Uani 1 1 d . . . . . C1 C 0.3115(2) 0.94245(19) 0.92010(17) 0.0211(5) Uani 1 1 d . . . . . C2 C 0.1687(2) 0.99312(19) 0.90044(19) 0.0236(6) Uani 1 1 d . . . . . H2A H 0.1578 1.0299 0.8380 0.028 Uiso 1 1 calc R . . . . H2B H 0.1237 1.0524 0.9449 0.028 Uiso 1 1 calc R . . . . C3 C 0.1080(2) 0.90150(19) 0.90744(19) 0.0248(6) Uani 1 1 d . . . . . H3A H 0.0181 0.9370 0.9297 0.030 Uiso 1 1 calc R . . . . H3B H 0.1083 0.8746 0.8452 0.030 Uiso 1 1 calc R . . . . C4 C 0.1753(2) 0.79926(18) 0.97092(18) 0.0200(5) Uani 1 1 d . . . . . H4 H 0.1353 0.8117 1.0344 0.024 Uiso 1 1 calc R . . . . C5 C 0.3165(2) 0.77896(18) 0.97274(18) 0.0207(5) Uani 1 1 d . . . . . C6 C 0.3697(2) 0.82005(19) 0.88216(18) 0.0224(5) Uani 1 1 d . . . . . H6 H 0.3303 0.8107 0.8254 0.027 Uiso 1 1 calc R . . . . C7 C 0.5146(2) 0.7547(2) 0.8839(2) 0.0279(6) Uani 1 1 d . . . . . H7A H 0.5485 0.7222 0.8235 0.033 Uiso 1 1 calc R . . . . H7B H 0.5581 0.8061 0.8984 0.033 Uiso 1 1 calc R . . . . C8 C 0.5354(2) 0.66075(19) 0.95778(19) 0.0258(6) Uani 1 1 d . . . . . C9 C 0.4094(2) 0.66213(19) 1.00367(18) 0.0235(6) Uani 1 1 d . . . . . H9 H 0.3860 0.6037 0.9746 0.028 Uiso 1 1 calc R . . . . C10 C 0.4143(2) 0.6346(2) 1.1061(2) 0.0313(6) Uani 1 1 d . . . . . H10A H 0.4769 0.5578 1.1179 0.047 Uiso 1 1 calc R . . . . H10B H 0.4390 0.6898 1.1363 0.047 Uiso 1 1 calc R . . . . H10C H 0.3302 0.6384 1.1305 0.047 Uiso 1 1 calc R . . . . C11 C 0.3288(2) 0.88308(18) 1.01524(17) 0.0206(5) Uani 1 1 d . . . . . H11 H 0.4175 0.8645 1.0351 0.025 Uiso 1 1 calc R . . . . C12 C 0.3750(2) 1.02789(19) 0.89711(18) 0.0240(6) Uani 1 1 d . . . . . H12A H 0.3249 1.1013 0.9250 0.029 Uiso 1 1 calc R . . . . H12B H 0.4617 0.9993 0.9209 0.029 Uiso 1 1 calc R . . . . C13 C 0.4332(2) 1.1171(2) 0.7653(2) 0.0301(6) Uani 1 1 d . . . . . C14 C 0.4350(3) 1.1308(2) 0.6638(2) 0.0369(7) Uani 1 1 d . . . . . C15 C 0.3551(3) 1.1002(4) 0.6104(2) 0.0548(9) Uani 1 1 d . . . . . H15 H 0.2976 1.0683 0.6393 0.066 Uiso 1 1 calc R . . . . C16 C 0.3599(4) 1.1161(4) 0.5178(3) 0.0740(13) Uani 1 1 d . . . . . H16 H 0.3073 1.0942 0.4809 0.089 Uiso 1 1 calc R . . . . C17 C 0.4432(4) 1.1650(4) 0.4778(3) 0.0672(11) Uani 1 1 d . . . . . C18 C 0.5223(4) 1.1953(4) 0.5278(3) 0.0611(10) Uani 1 1 d . . . . . H18 H 0.5799 1.2268 0.4984 0.073 Uiso 1 1 calc R . . . . C19 C 0.5167(3) 1.1795(3) 0.6209(2) 0.0489(8) Uani 1 1 d . . . . . H19 H 0.5695 1.2021 0.6570 0.059 Uiso 1 1 calc R . . . . C20 C 0.2444(2) 1.01413(19) 1.13432(18) 0.0237(6) Uani 1 1 d . . . . . C21 C 0.1571(2) 1.0382(2) 1.21788(18) 0.0267(6) Uani 1 1 d . . . . . C22 C 0.1286(3) 1.1410(2) 1.2595(2) 0.0381(7) Uani 1 1 d . . . . . H22 H 0.1677 1.1928 1.2373 0.046 Uiso 1 1 calc R . . . . C23 C 0.0405(4) 1.1669(3) 1.3354(3) 0.0564(9) Uani 1 1 d . . . . . H23 H 0.0190 1.2368 1.3648 0.068 Uiso 1 1 calc R . . . . C24 C -0.0137(3) 1.0899(3) 1.3660(2) 0.0478(8) Uani 1 1 d . . . . . C25 C 0.0166(3) 0.9873(3) 1.3274(2) 0.0427(7) Uani 1 1 d . . . . . H25 H -0.0206 0.9347 1.3513 0.051 Uiso 1 1 calc R . . . . C26 C 0.1025(2) 0.9615(2) 1.2530(2) 0.0327(6) Uani 1 1 d . . . . . H26 H 0.1246 0.8904 1.2254 0.039 Uiso 1 1 calc R . . . . C27 C 0.0484(2) 0.69253(19) 0.94398(17) 0.0210(5) Uani 1 1 d . . . . . C28 C 0.0443(2) 0.58913(18) 0.90342(18) 0.0215(5) Uani 1 1 d . . . . . C29 C -0.0753(2) 0.5823(2) 0.89696(19) 0.0254(6) Uani 1 1 d . . . . . H29 H -0.1500 0.6430 0.9166 0.031 Uiso 1 1 calc R . . . . C30 C -0.0846(2) 0.4868(2) 0.8618(2) 0.0292(6) Uani 1 1 d . . . . . H30 H -0.1651 0.4805 0.8572 0.035 Uiso 1 1 calc R . . . . C31 C 0.0267(2) 0.4008(2) 0.83338(19) 0.0283(6) Uani 1 1 d . . . . . C32 C 0.1457(2) 0.4047(2) 0.8405(2) 0.0326(6) Uani 1 1 d . . . . . H32 H 0.2202 0.3429 0.8223 0.039 Uiso 1 1 calc R . . . . C33 C 0.1539(2) 0.5003(2) 0.87480(19) 0.0270(6) Uani 1 1 d . . . . . H33 H 0.2349 0.5057 0.8790 0.032 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N2 0.103(2) 0.0675(18) 0.070(2) -0.0201(16) 0.0330(19) -0.0032(18) N3 0.0430(14) 0.0276(11) 0.0537(17) -0.0143(11) 0.0035(12) -0.0200(11) O1 0.0141(9) 0.0319(10) 0.0693(15) -0.0012(9) -0.0036(9) -0.0023(8) O2 0.0624(14) 0.0475(12) 0.0425(13) 0.0024(10) -0.0121(10) -0.0413(11) O3 0.0273(9) 0.0349(9) 0.0349(11) -0.0090(8) 0.0044(8) -0.0208(8) O4 0.0207(9) 0.0295(9) 0.0527(13) -0.0155(8) 0.0028(8) -0.0149(8) O5 0.0164(8) 0.0227(8) 0.0342(11) -0.0112(7) 0.0022(7) -0.0092(7) O6 0.0159(8) 0.0255(9) 0.0536(13) -0.0166(8) 0.0063(8) -0.0094(7) O7 0.0133(8) 0.0189(8) 0.0410(11) -0.0102(7) -0.0011(7) -0.0081(6) N1 0.089(6) 0.115(8) 0.049(5) -0.008(6) 0.017(4) -0.048(6) O8 0.059(4) 0.100(5) 0.038(3) -0.012(4) -0.005(3) -0.023(4) O9 0.107(7) 0.119(9) 0.048(4) -0.012(7) 0.027(5) -0.076(7) N1' 0.096(7) 0.137(9) 0.043(5) -0.018(6) 0.003(5) -0.081(6) O8' 0.114(7) 0.207(9) 0.065(5) -0.003(7) -0.019(5) -0.088(7) O9' 0.131(9) 0.117(9) 0.053(5) -0.009(7) 0.016(6) -0.080(7) O10 0.0672(19) 0.117(3) 0.061(2) -0.0008(18) 0.0218(15) -0.0260(19) O11 0.128(2) 0.0814(18) 0.081(2) -0.0213(15) 0.0424(18) -0.0032(18) O12 0.0444(12) 0.0398(11) 0.0873(19) -0.0220(11) 0.0027(11) -0.0294(10) O13 0.0565(14) 0.0347(11) 0.0729(17) -0.0296(11) 0.0197(12) -0.0239(10) C1 0.0122(10) 0.0213(11) 0.0316(15) -0.0090(10) 0.0007(9) -0.0072(9) C2 0.0150(11) 0.0192(11) 0.0372(16) -0.0062(10) -0.0017(10) -0.0062(9) C3 0.0109(10) 0.0222(11) 0.0431(17) -0.0056(11) -0.0043(10) -0.0069(9) C4 0.0113(10) 0.0162(10) 0.0339(15) -0.0107(10) 0.0021(9) -0.0058(8) C5 0.0122(11) 0.0172(11) 0.0342(15) -0.0086(10) 0.0008(9) -0.0063(9) C6 0.0148(11) 0.0231(12) 0.0304(14) -0.0104(10) 0.0019(9) -0.0073(9) C7 0.0131(11) 0.0281(12) 0.0415(17) -0.0123(11) 0.0055(10) -0.0058(10) C8 0.0146(11) 0.0200(11) 0.0435(17) -0.0117(11) -0.0002(10) -0.0056(9) C9 0.0129(11) 0.0187(11) 0.0397(16) -0.0092(10) -0.0015(10) -0.0055(9) C10 0.0241(12) 0.0250(12) 0.0442(18) -0.0054(11) -0.0029(11) -0.0074(10) C11 0.0093(10) 0.0193(11) 0.0347(15) -0.0105(10) -0.0004(9) -0.0056(8) C12 0.0173(11) 0.0232(12) 0.0357(16) -0.0087(10) -0.0005(10) -0.0112(9) C13 0.0244(13) 0.0274(12) 0.0427(17) -0.0041(11) -0.0039(11) -0.0136(11) C14 0.0346(15) 0.0408(15) 0.0414(18) -0.0081(13) 0.0041(12) -0.0211(12) C15 0.056(2) 0.091(3) 0.038(2) -0.0081(18) 0.0046(15) -0.050(2) C16 0.075(3) 0.133(4) 0.045(2) -0.017(2) 0.0000(19) -0.073(3) C17 0.073(3) 0.107(3) 0.041(2) -0.007(2) 0.0100(18) -0.056(2) C18 0.063(2) 0.088(3) 0.052(2) -0.001(2) 0.0070(18) -0.053(2) C19 0.0496(18) 0.068(2) 0.046(2) -0.0049(16) -0.0007(15) -0.0409(17) C20 0.0132(10) 0.0188(11) 0.0369(15) -0.0081(10) -0.0065(10) -0.0013(9) C21 0.0216(12) 0.0252(12) 0.0315(15) -0.0056(11) -0.0066(10) -0.0051(10) C22 0.0409(16) 0.0287(13) 0.0423(18) -0.0121(12) -0.0018(13) -0.0084(12) C23 0.066(2) 0.0383(17) 0.054(2) -0.0248(16) 0.0082(18) -0.0044(16) C24 0.0462(18) 0.0451(17) 0.0375(19) -0.0032(14) 0.0082(14) -0.0012(14) C25 0.0417(16) 0.0499(17) 0.0347(18) 0.0015(14) -0.0012(13) -0.0155(14) C26 0.0279(13) 0.0372(14) 0.0357(17) -0.0049(12) -0.0017(11) -0.0147(12) C27 0.0143(11) 0.0187(11) 0.0314(15) -0.0049(10) -0.0026(10) -0.0071(9) C28 0.0154(11) 0.0180(11) 0.0343(15) -0.0026(10) -0.0027(10) -0.0094(9) C29 0.0161(11) 0.0213(11) 0.0388(16) -0.0063(10) -0.0005(10) -0.0061(9) C30 0.0225(12) 0.0276(13) 0.0441(17) -0.0088(11) -0.0007(11) -0.0158(10) C31 0.0301(13) 0.0220(12) 0.0386(16) -0.0072(11) 0.0003(11) -0.0158(11) C32 0.0234(13) 0.0248(12) 0.0492(19) -0.0102(12) 0.0034(12) -0.0080(10) C33 0.0157(11) 0.0224(12) 0.0434(17) -0.0083(11) 0.0001(11) -0.0066(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O10 N2 O11 123.8(4) O10 N2 C24 119.1(4) O11 N2 C24 117.1(4) O12 N3 O13 124.1(2) O12 N3 C31 118.3(2) O13 N3 C31 117.6(2) C13 O3 C12 115.24(19) C20 O5 C11 117.02(17) C27 O7 C4 115.28(17) O8 N1 O9 125(2) O8 N1 C17 120(2) O9 N1 C17 115(2) O8' N1' C17 119.3(19) O9' N1' O8' 116(2) O9' N1' C17 122.7(17) C2 C1 C6 108.42(17) C11 C1 C2 109.30(19) C11 C1 C6 85.96(17) C12 C1 C2 111.63(19) C12 C1 C6 120.73(19) C12 C1 C11 118.08(19) C1 C2 H2A 109.2 C1 C2 H2B 109.2 C1 C2 C3 112.11(18) H2A C2 H2B 107.9 C3 C2 H2A 109.2 C3 C2 H2B 109.2 C2 C3 H3A 108.7 C2 C3 H3B 108.7 H3A C3 H3B 107.6 C4 C3 C2 114.10(18) C4 C3 H3A 108.7 C4 C3 H3B 108.7 O7 C4 C3 108.62(18) O7 C4 H4 110.1 O7 C4 C5 107.49(16) C3 C4 H4 110.1 C3 C4 C5 110.50(19) C5 C4 H4 110.1 C4 C5 C6 113.2(2) C4 C5 C11 107.92(17) C9 C5 C4 119.24(19) C9 C5 C6 109.49(18) C9 C5 C11 116.74(19) C11 C5 C6 85.43(17) C1 C6 H6 114.3 C5 C6 C1 86.71(17) C5 C6 H6 114.3 C7 C6 C1 119.12(19) C7 C6 C5 104.23(19) C7 C6 H6 114.3 C6 C7 H7A 110.5 C6 C7 H7B 110.5 H7A C7 H7B 108.7 C8 C7 C6 106.3(2) C8 C7 H7A 110.5 C8 C7 H7B 110.5 O1 C8 C7 124.5(2) O1 C8 C9 123.8(2) C7 C8 C9 111.73(19) C5 C9 C8 102.21(19) C5 C9 H9 107.7 C8 C9 H9 107.7 C10 C9 C5 116.6(2) C10 C9 C8 114.3(2) C10 C9 H9 107.7 C9 C10 H10A 109.5 C9 C10 H10B 109.5 C9 C10 H10C 109.5 H10A C10 H10B 109.5 H10A C10 H10C 109.5 H10B C10 H10C 109.5 O5 C11 C1 121.53(18) O5 C11 C5 112.90(17) O5 C11 H11 110.7 C1 C11 C5 88.48(17) C1 C11 H11 110.7 C5 C11 H11 110.7 O3 C12 C1 106.86(18) O3 C12 H12A 110.3 O3 C12 H12B 110.3 C1 C12 H12A 110.3 C1 C12 H12B 110.3 H12A C12 H12B 108.6 O2 C13 O3 122.8(3) O2 C13 C14 123.9(2) O3 C13 C14 113.3(2) C15 C14 C13 122.7(3) C19 C14 C13 117.9(3) C19 C14 C15 119.3(3) C14 C15 H15 120.0 C16 C15 C14 120.1(3) C16 C15 H15 120.0 C15 C16 H16 120.7 C15 C16 C17 118.6(3) C17 C16 H16 120.7 C16 C17 N1 115.9(11) C16 C17 N1' 121.2(10) C18 C17 N1 120.7(12) C18 C17 N1' 116.0(10) C18 C17 C16 122.6(4) C17 C18 H18 120.8 C19 C18 C17 118.4(3) C19 C18 H18 120.8 C14 C19 H19 119.6 C18 C19 C14 120.9(3) C18 C19 H19 119.6 O4 C20 O5 124.3(2) O4 C20 C21 125.1(2) O5 C20 C21 110.6(2) C22 C21 C20 118.7(2) C26 C21 C20 121.3(2) C26 C21 C22 120.0(3) C21 C22 H22 120.6 C21 C22 C23 118.9(3) C23 C22 H22 120.6 C22 C23 H23 120.5 C24 C23 C22 119.0(3) C24 C23 H23 120.5 C23 C24 N2 119.4(3) C25 C24 N2 118.0(3) C25 C24 C23 122.6(3) C24 C25 H25 120.7 C24 C25 C26 118.7(3) C26 C25 H25 120.7 C21 C26 H26 119.6 C25 C26 C21 120.8(3) C25 C26 H26 119.6 O6 C27 O7 124.3(2) O6 C27 C28 123.5(2) O7 C27 C28 112.23(19) C29 C28 C27 117.3(2) C33 C28 C27 122.4(2) C33 C28 C29 120.2(2) C28 C29 H29 120.1 C30 C29 C28 119.8(2) C30 C29 H29 120.1 C29 C30 H30 120.9 C31 C30 C29 118.1(2) C31 C30 H30 120.9 C30 C31 N3 118.0(2) C32 C31 N3 118.8(2) C32 C31 C30 123.2(2) C31 C32 H32 120.8 C33 C32 C31 118.3(2) C33 C32 H32 120.8 C28 C33 H33 119.8 C32 C33 C28 120.4(2) C32 C33 H33 119.8 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance N2 O10 1.209(5) N2 O11 1.212(5) N2 C24 1.489(5) N3 O12 1.219(3) N3 O13 1.232(3) N3 C31 1.478(3) O1 C8 1.211(3) O2 C13 1.202(3) O3 C12 1.440(3) O3 C13 1.342(3) O4 C20 1.206(3) O5 C11 1.449(3) O5 C20 1.343(3) O6 C27 1.208(3) O7 C4 1.464(2) O7 C27 1.342(3) N1 O8 1.17(3) N1 O9 1.22(3) N1 C17 1.53(3) N1' O8' 1.30(3) N1' O9' 1.20(3) N1' C17 1.45(3) C1 C2 1.541(3) C1 C6 1.565(3) C1 C11 1.524(4) C1 C12 1.516(3) C2 H2A 0.9900 C2 H2B 0.9900 C2 C3 1.548(3) C3 H3A 0.9900 C3 H3B 0.9900 C3 C4 1.523(3) C4 H4 1.0000 C4 C5 1.524(3) C5 C6 1.557(4) C5 C9 1.523(3) C5 C11 1.548(3) C6 H6 1.0000 C6 C7 1.539(3) C7 H7A 0.9900 C7 H7B 0.9900 C7 C8 1.514(4) C8 C9 1.530(3) C9 H9 1.0000 C9 C10 1.513(4) C10 H10A 0.9800 C10 H10B 0.9800 C10 H10C 0.9800 C11 H11 1.0000 C12 H12A 0.9900 C12 H12B 0.9900 C13 C14 1.481(4) C14 C15 1.402(4) C14 C19 1.388(4) C15 H15 0.9500 C15 C16 1.355(5) C16 H16 0.9500 C16 C17 1.389(5) C17 C18 1.364(5) C18 H18 0.9500 C18 C19 1.361(5) C19 H19 0.9500 C20 C21 1.492(4) C21 C22 1.390(4) C21 C26 1.389(4) C22 H22 0.9500 C22 C23 1.410(5) C23 H23 0.9500 C23 C24 1.371(5) C24 C25 1.364(5) C25 H25 0.9500 C25 C26 1.381(4) C26 H26 0.9500 C27 C28 1.489(3) C28 C29 1.398(3) C28 C33 1.392(3) C29 H29 0.9500 C29 C30 1.386(3) C30 H30 0.9500 C30 C31 1.385(4) C31 C32 1.377(4) C32 H32 0.9500 C32 C33 1.376(3) C33 H33 0.9500 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion N2 C24 C25 C26 179.3(3) N3 C31 C32 C33 179.5(2) O1 C8 C9 C5 165.4(2) O1 C8 C9 C10 38.5(3) O2 C13 C14 C15 -158.4(3) O2 C13 C14 C19 19.4(4) O3 C13 C14 C15 19.8(4) O3 C13 C14 C19 -162.3(3) O4 C20 C21 C22 14.4(4) O4 C20 C21 C26 -167.0(2) O5 C20 C21 C22 -164.8(2) O5 C20 C21 C26 13.7(3) O6 C27 C28 C29 10.4(4) O6 C27 C28 C33 -167.9(3) O7 C4 C5 C6 90.0(2) O7 C4 C5 C9 -40.9(3) O7 C4 C5 C11 -177.26(18) O7 C27 C28 C29 -171.1(2) O7 C27 C28 C33 10.6(3) N1 C17 C18 C19 -170.9(9) O8 N1 C17 N1' -107(8) O8 N1 C17 C16 6.7(19) O8 N1 C17 C18 176.7(12) O9 N1 C17 N1' 75(8) O9 N1 C17 C16 -170.6(11) O9 N1 C17 C18 -0.7(17) N1' C17 C18 C19 172.7(10) O8' N1' C17 N1 89(8) O8' N1' C17 C16 15(2) O8' N1' C17 C18 -159.3(14) O9' N1' C17 N1 -108(9) O9' N1' C17 C16 178.6(13) O9' N1' C17 C18 4(2) O10 N2 C24 C23 176.0(4) O10 N2 C24 C25 -5.1(6) O11 N2 C24 C23 -4.3(6) O11 N2 C24 C25 174.5(4) O12 N3 C31 C30 -10.7(4) O12 N3 C31 C32 167.8(3) O13 N3 C31 C30 170.3(3) O13 N3 C31 C32 -11.3(4) C1 C2 C3 C4 26.4(3) C1 C6 C7 C8 108.3(2) C2 C1 C6 C5 -81.8(2) C2 C1 C6 C7 173.7(2) C2 C1 C11 O5 -35.4(2) C2 C1 C11 C5 80.77(18) C2 C1 C12 O3 -70.7(2) C2 C3 C4 O7 -147.39(19) C2 C3 C4 C5 -29.7(3) C3 C4 C5 C6 -28.4(3) C3 C4 C5 C9 -159.3(2) C3 C4 C5 C11 64.4(3) C4 O7 C27 O6 -3.2(4) C4 O7 C27 C28 178.34(18) C4 C5 C6 C1 80.78(19) C4 C5 C6 C7 -159.99(18) C4 C5 C9 C8 156.5(2) C4 C5 C9 C10 -78.1(3) C4 C5 C11 O5 38.4(3) C4 C5 C11 C1 -85.4(2) C5 C6 C7 C8 14.1(2) C6 C1 C2 C3 34.8(3) C6 C1 C11 O5 -143.47(19) C6 C1 C11 C5 -27.34(15) C6 C1 C12 O3 58.5(3) C6 C5 C9 C8 23.9(2) C6 C5 C9 C10 149.3(2) C6 C5 C11 O5 151.35(19) C6 C5 C11 C1 27.52(15) C6 C7 C8 O1 -179.9(2) C6 C7 C8 C9 0.4(3) C7 C8 C9 C5 -14.8(3) C7 C8 C9 C10 -141.8(2) C9 C5 C6 C1 -143.55(18) C9 C5 C6 C7 -24.3(2) C9 C5 C11 O5 -99.1(2) C9 C5 C11 C1 137.1(2) C11 O5 C20 O4 9.0(3) C11 O5 C20 C21 -171.77(19) C11 C1 C2 C3 -57.4(3) C11 C1 C6 C5 27.21(15) C11 C1 C6 C7 -77.3(2) C11 C1 C12 O3 161.41(18) C11 C5 C6 C1 -26.77(15) C11 C5 C6 C7 92.46(18) C11 C5 C9 C8 -70.9(3) C11 C5 C9 C10 54.5(3) C12 O3 C13 O2 -0.7(3) C12 O3 C13 C14 -179.0(2) C12 C1 C2 C3 170.1(2) C12 C1 C6 C5 147.7(2) C12 C1 C6 C7 43.2(3) C12 C1 C11 O5 93.7(2) C12 C1 C11 C5 -150.22(19) C13 O3 C12 C1 179.19(18) C13 C14 C15 C16 179.1(4) C13 C14 C19 C18 -179.5(3) C14 C15 C16 C17 -1.2(7) C15 C14 C19 C18 -1.6(5) C15 C16 C17 N1 171.1(9) C15 C16 C17 N1' -172.7(10) C15 C16 C17 C18 1.4(8) C16 C17 C18 C19 -1.7(7) C17 C18 C19 C14 1.7(6) C19 C14 C15 C16 1.3(6) C20 O5 C11 C1 -79.8(2) C20 O5 C11 C5 177.13(19) C20 C21 C22 C23 176.4(3) C20 C21 C26 C25 -176.5(2) C21 C22 C23 C24 0.3(5) C22 C21 C26 C25 2.0(4) C22 C23 C24 N2 -179.5(3) C22 C23 C24 C25 1.7(5) C23 C24 C25 C26 -1.9(5) C24 C25 C26 C21 0.0(4) C26 C21 C22 C23 -2.2(4) C27 O7 C4 C3 -71.9(2) C27 O7 C4 C5 168.5(2) C27 C28 C29 C30 -178.5(2) C27 C28 C33 C32 177.8(2) C28 C29 C30 C31 -0.4(4) C29 C28 C33 C32 -0.5(4) C29 C30 C31 N3 179.9(2) C29 C30 C31 C32 1.6(4) C30 C31 C32 C33 -2.2(4) C31 C32 C33 C28 1.6(4) C33 C28 C29 C30 -0.1(4) loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons 1 -0.465 0.500 0.500 504.9 8.7