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Information card for entry 1543257
Preview
| Coordinates | 1543257.cif |
|---|---|
| Structure factors | 1543257.hkl |
| Original IUCr paper | HTML |
| External links | PubChem |
| Chemical name | Bis[μ-2-(trimethylsilylamido)-6-(trimethylsilylamino)pyridine-κ^3^<i>N</i>^1^,<i>N</i>^2^:<i>N</i>^2^]bis[(diethyl ether-κ<i>O</i>)lithium(I)] |
|---|---|
| Formula | C30 H64 Li2 N6 O2 Si4 |
| Calculated formula | C30 H64 Li2 N6 O2 Si4 |
| Title of publication | Bis[μ-2-(trimethylsilylamido)-6-(trimethylsilylamino)pyridine-κ^3^<i>N</i>^1^,<i>N</i>^2^:<i>N</i>^2^]bis[(diethyl ether-κ<i>O</i>)lithium(I)] |
| Authors of publication | Rave, Justin A.; Garcia, Diego A.; Hillesheim, Patrick C.; Guillet, Gary L. |
| Journal of publication | IUCrData |
| Year of publication | 2016 |
| Journal volume | 1 |
| Journal issue | 5 |
| Pages of publication | x160707 |
| a | 9.87 ± 0.007 Å |
| b | 10.624 ± 0.008 Å |
| c | 11.319 ± 0.007 Å |
| α | 74.34 ± 0.02° |
| β | 81.35 ± 0.02° |
| γ | 68.246 ± 0.019° |
| Cell volume | 1059.8 ± 1.3 Å3 |
| Cell temperature | 173 K |
| Ambient diffraction temperature | 173 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1087 |
| Residual factor for significantly intense reflections | 0.0592 |
| Weighted residual factors for significantly intense reflections | 0.1249 |
| Weighted residual factors for all reflections included in the refinement | 0.1575 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301779 (current) | 2025-08-18 | Add cross-references to PubChem compounds in COD range 1/54 Each referenced PubChem compound corresponds to the full crystal structure. |
1543257.cif 1543257.hkl |
| 183649 | 2016-06-17 | cif/ Updating files of 1543257 Original log message: Adding full bibliography for 1543257.cif. |
1543257.cif 1543257.hkl |
| 182574 | 2016-05-05 | cif/ hkl/ Adding structures of 1543257 via cif-deposit CGI script. |
1543257.cif 1543257.hkl |
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Users of the data should acknowledge the original authors of the
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