#------------------------------------------------------------------------------ #$Date: 2016-05-10 05:42:01 +0300 (Tue, 10 May 2016) $ #$Revision: 182844 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/32/1543273.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1543273 loop_ _publ_author_name 'Arz, Marius I.' 'Schnakenburg, Gregor' 'Meyer, Andreas' 'Schiemann, Olav' 'Filippou, Alexander' _publ_section_title ; The Si2H radical supported by two N-heterocyclic carbenes ; _journal_name_full 'Chem. Sci.' _journal_paper_doi 10.1039/C6SC01569G _journal_year 2016 _chemical_formula_moiety 'C54 H73 N4 Si2' _chemical_formula_sum 'C54 H73 N4 Si2' _chemical_formula_weight 834.34 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2016-03-29 deposited with the CCDC. 2016-05-09 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 126.432(5) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 12.9588(11) _cell_length_b 13.5352(9) _cell_length_c 18.2226(15) _cell_measurement_reflns_used 3919 _cell_measurement_temperature 123(2) _cell_measurement_theta_max 26.97 _cell_measurement_theta_min 2.71 _cell_volume 2571.6(4) _computing_cell_refinement 'STOE X-AREA, STOE&CIE, 2011' _computing_data_collection 'STOE X-AREA, STOE&CIE, 2011' _computing_data_reduction 'STOE X-RED, STOE&CIE, 2011' _computing_molecular_graphics 'DIAMOND (Brandenburg, 1999)' _computing_publication_material 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 123(2) _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_detector_type STOE _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ' 171 frames, detector distance = 100 mm, exposure time = 4min' _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'STOE IPDS 2T' _diffrn_measurement_method 'rotation method' _diffrn_radiation_collimation '0.5 mm diameter, monocapillary' _diffrn_radiation_monochromator 'plane graphite' _diffrn_radiation_polarisn_norm 0 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1649 _diffrn_reflns_av_unetI/netI 0.2106 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 20621 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.997 _diffrn_reflns_theta_min 2.712 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _diffrn_source_current 40 _diffrn_source_power 2.00 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.106 _exptl_absorpt_correction_T_max 0.9185 _exptl_absorpt_correction_T_min 0.6417 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'XRed, STOE & CIE, 2011' _exptl_crystal_colour 'clear dark blue' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary blue _exptl_crystal_density_diffrn 1.078 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 906 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.461 _refine_diff_density_min -0.272 _refine_diff_density_rms 0.073 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.754 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 279 _refine_ls_number_reflns 6197 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.754 _refine_ls_R_factor_all 0.1885 _refine_ls_R_factor_gt 0.0755 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0929P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1721 _refine_ls_wR_factor_ref 0.2042 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2130 _reflns_number_total 6197 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c6sc01569g2.cif _cod_data_source_block 3756 _cod_database_code 1543273 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; 3756.res created by SHELXL-2014/7 TITL 3756 P 1 21/n 1 R = New: P21/c CELL 0.71073 12.9588 13.5352 18.2226 90 126.432 90 ZERR 2 0.0011 0.0009 0.0015 0 0.005 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N Si UNIT 108 146 8 4 L.S. 5 PLAN -5 BOND $H CONF TEMP -150 fmap 2 acta MORE -1 OMIT -2 56 REM S:/3756/XShape/3756.hkl WGHT 0.092900 FVAR 0.53092 SI 4 0.570854 -0.460100 -0.007432 11.00000 0.07647 0.04865 = 0.05495 0.01844 0.04239 0.01191 AFIX 3 H 2 0.574044 -0.431900 0.041138 10.50000 -1.20000 AFIX 0 N1 3 0.354505 -0.366417 -0.179490 11.00000 0.02928 0.03518 = 0.03625 0.00497 0.01860 -0.00154 N2 3 0.542641 -0.329150 -0.141316 11.00000 0.03330 0.03320 = 0.03594 0.00409 0.02195 0.00260 C1 1 0.482605 -0.383529 -0.110900 11.00000 0.03325 0.02603 = 0.03614 -0.00651 0.02223 -0.00300 C2 1 0.337896 -0.306511 -0.246520 11.00000 0.03124 0.04140 = 0.03966 0.00781 0.01681 0.00760 AFIX 43 H2 2 0.258141 -0.285386 -0.299934 11.00000 -1.20000 AFIX 0 C3 1 0.454308 -0.283193 -0.223101 11.00000 0.04111 0.03601 = 0.04204 0.00695 0.02724 0.00590 AFIX 43 H3 2 0.472474 -0.242563 -0.256649 11.00000 -1.20000 AFIX 0 C4 1 0.248488 -0.396726 -0.176753 11.00000 0.02363 0.04737 = 0.03325 0.00304 0.01351 0.00104 C5 1 0.180851 -0.480704 -0.226771 11.00000 0.02691 0.05329 = 0.03637 -0.00172 0.01131 -0.00605 C6 1 0.075634 -0.505637 -0.224871 11.00000 0.03824 0.09666 = 0.05080 -0.02242 0.02311 -0.03247 AFIX 43 H6 2 0.023959 -0.561249 -0.258418 11.00000 -1.20000 AFIX 0 C7 1 0.048098 -0.451718 -0.176316 11.00000 0.03302 0.11977 = 0.05705 -0.01454 0.02823 -0.01826 AFIX 43 H7 2 -0.021637 -0.471103 -0.175459 11.00000 -1.20000 AFIX 0 C8 1 0.117626 -0.370103 -0.128397 11.00000 0.03480 0.08383 = 0.05140 -0.00556 0.02605 0.00376 AFIX 43 H8 2 0.094344 -0.332595 -0.096226 11.00000 -1.20000 AFIX 0 C9 1 0.222891 -0.341298 -0.126316 11.00000 0.02746 0.04506 = 0.03846 0.00656 0.01661 0.00850 C10 1 0.208053 -0.539276 -0.283054 11.00000 0.03873 0.05103 = 0.04526 -0.00490 0.02148 -0.00668 AFIX 13 H10 2 0.289736 -0.513012 -0.269693 11.00000 -1.20000 AFIX 0 C11 1 0.104696 -0.524136 -0.384157 11.00000 0.05231 0.07793 = 0.05116 -0.00748 0.02406 0.00852 AFIX 137 H11A 2 0.021896 -0.545958 -0.399499 11.00000 -1.50000 H11B 2 0.125620 -0.562732 -0.419218 11.00000 -1.50000 H11C 2 0.099773 -0.453935 -0.399095 11.00000 -1.50000 AFIX 0 C12 1 0.229107 -0.648443 -0.259369 11.00000 0.10766 0.05244 = 0.07181 -0.00687 0.05307 -0.00843 AFIX 137 H12A 2 0.299069 -0.656533 -0.194414 11.00000 -1.50000 H12B 2 0.251478 -0.681955 -0.295843 11.00000 -1.50000 H12C 2 0.150366 -0.677319 -0.272560 11.00000 -1.50000 AFIX 0 C13 1 0.300732 -0.250274 -0.072438 11.00000 0.05296 0.04114 = 0.05799 0.00066 0.03727 0.00869 AFIX 13 H13 2 0.385538 -0.256364 -0.061853 11.00000 -1.20000 AFIX 0 C14 1 0.328037 -0.242343 0.019895 11.00000 0.07495 0.05282 = 0.07030 -0.00942 0.04636 -0.00503 AFIX 137 H14A 2 0.247288 -0.233715 0.012563 11.00000 -1.50000 H14B 2 0.383916 -0.185410 0.052534 11.00000 -1.50000 H14C 2 0.370702 -0.302735 0.054769 11.00000 -1.50000 AFIX 0 C15 1 0.238002 -0.156078 -0.127877 11.00000 0.12149 0.05590 = 0.08045 0.01057 0.05629 0.01430 AFIX 137 H15A 2 0.220278 -0.163437 -0.187893 11.00000 -1.50000 H15B 2 0.295983 -0.100020 -0.095774 11.00000 -1.50000 H15C 2 0.157485 -0.144320 -0.135544 11.00000 -1.50000 AFIX 0 C16 1 0.679399 -0.312923 -0.086933 11.00000 0.03353 0.02888 = 0.03512 0.00368 0.02247 -0.00187 C17 1 0.753403 -0.379506 -0.095841 11.00000 0.03894 0.03249 = 0.04507 -0.00075 0.02898 -0.00123 C18 1 0.884921 -0.362463 -0.042519 11.00000 0.03174 0.03855 = 0.06350 -0.00002 0.02835 0.00230 AFIX 43 H18 2 0.938795 -0.406213 -0.046444 11.00000 -1.20000 AFIX 0 C19 1 0.937762 -0.283100 0.015735 11.00000 0.03594 0.04685 = 0.06880 -0.00676 0.02838 -0.00838 AFIX 43 H19 2 1.027738 -0.272603 0.051112 11.00000 -1.20000 AFIX 0 C20 1 0.863029 -0.218295 0.023995 11.00000 0.04321 0.03586 = 0.05411 -0.00813 0.02405 -0.00725 AFIX 43 H20 2 0.901928 -0.164898 0.065909 11.00000 -1.20000 AFIX 0 C21 1 0.728498 -0.231311 -0.029916 11.00000 0.04448 0.03506 = 0.04537 0.00011 0.03072 -0.00221 C22 1 0.694008 -0.464607 -0.161757 11.00000 0.03142 0.04014 = 0.04967 -0.00371 0.02663 -0.00260 AFIX 13 H22 2 0.609149 -0.478615 -0.174231 11.00000 -1.20000 AFIX 0 C23 1 0.774630 -0.559850 -0.122717 11.00000 0.05085 0.03832 = 0.06758 -0.00489 0.03578 -0.00338 AFIX 137 H23A 2 0.853945 -0.551552 -0.117413 11.00000 -1.50000 H23B 2 0.725465 -0.615315 -0.163571 11.00000 -1.50000 H23C 2 0.795731 -0.573225 -0.062349 11.00000 -1.50000 AFIX 0 C24 1 0.668985 -0.437992 -0.251219 11.00000 0.05272 0.06375 = 0.05650 -0.00698 0.03266 0.00302 AFIX 137 H24A 2 0.612525 -0.380178 -0.277206 11.00000 -1.50000 H24B 2 0.627749 -0.493782 -0.293501 11.00000 -1.50000 H24C 2 0.750387 -0.422684 -0.241209 11.00000 -1.50000 AFIX 0 C25 1 0.647574 -0.157692 -0.022445 11.00000 0.04739 0.04017 = 0.06684 -0.01780 0.04074 -0.01068 AFIX 13 H25 2 0.557050 -0.181845 -0.063325 11.00000 -1.20000 AFIX 0 C26 1 0.680451 -0.149665 0.070965 11.00000 0.11138 0.07016 = 0.09305 0.00941 0.07814 0.02180 AFIX 137 H26A 2 0.679313 -0.215549 0.092777 11.00000 -1.50000 H26B 2 0.617463 -0.107385 0.069003 11.00000 -1.50000 H26C 2 0.766157 -0.120793 0.112423 11.00000 -1.50000 AFIX 0 C27 1 0.650306 -0.056762 -0.059268 11.00000 0.07318 0.04957 = 0.08556 0.00316 0.05596 0.01269 AFIX 137 H27A 2 0.737315 -0.029543 -0.020240 11.00000 -1.50000 H27B 2 0.590768 -0.011808 -0.059576 11.00000 -1.50000 H27C 2 0.624584 -0.064357 -0.121549 11.00000 -1.50000 AFIX 0 HKLF 4 1 1 0 0 0 -1 0 -1 0 -1 REM 3756 P 1 21/n 1 R = New: P21/c REM R1 = 0.0755 for 2130 Fo > 4sig(Fo) and 0.1885 for all 6197 data REM 279 parameters refined using 0 restraints END WGHT 0.0924 0.0000 REM Highest difference peak 0.461, deepest hole -0.272, 1-sigma level 0.073 Q1 1 0.5452 -0.4107 -0.0504 11.00000 0.05 0.46 Q2 1 0.4966 -0.4385 -0.0756 11.00000 0.05 0.46 Q3 1 0.6784 -0.1120 0.0209 11.00000 0.05 0.32 Q4 1 0.6880 -0.3231 -0.1427 11.00000 0.05 0.31 Q5 1 0.6921 -0.3998 -0.1624 11.00000 0.05 0.30 ; _shelx_res_checksum 62786 _shelx_hkl_file ; -2 0 0 5.38 19.90 0 2 0 0 6.97 19.21 0 4 0 0 847.94 25.65 0 -4 0 0 914.21 27.77 0 6 0 0 521.70 23.82 0 -6 0 0 554.65 25.25 0 -8 0 0 70.07 15.36 0 8 0 0 61.69 13.75 0 -10 0 0 4.80 21.51 0 10 0 0 20.66 18.29 0 -12 0 0 446.59 26.19 0 12 0 0 402.09 20.83 0 14 0 0 5.44 19.98 0 -14 0 0 30.38 18.02 0 16 0 0 34.54 23.57 0 -16 0 0 -16.09 30.10 0 -2 -1 0 256.88 21.94 0 2 1 0 265.91 22.06 0 -2 1 0 289.13 20.83 0 2 -1 0 349.51 26.89 0 -3 1 0 4353.56 51.74 0 3 1 0 4966.05 49.29 0 3 -1 0 4838.97 54.93 0 -3 -1 0 4803.13 48.60 0 4 1 0 48.29 13.37 0 4 -1 0 59.67 14.65 0 -4 1 0 78.73 22.08 0 -4 -1 0 77.61 19.51 0 -5 1 0 46.34 22.44 0 5 1 0 33.79 18.77 0 5 -1 0 38.08 14.55 0 -5 -1 0 28.77 19.59 0 6 -1 0 223.80 17.31 0 6 1 0 163.15 14.77 0 -6 1 0 325.75 23.93 0 -6 -1 0 232.31 21.43 0 -7 -1 0 74.78 14.48 0 7 -1 0 114.32 19.71 0 7 1 0 75.04 18.88 0 -7 1 0 138.97 22.05 0 8 1 0 7.88 12.60 0 -8 -1 0 4.69 13.85 0 8 -1 0 6.64 17.80 0 -8 1 0 8.00 14.46 0 -9 -1 0 6.94 13.68 0 9 -1 0 35.03 18.53 0 -9 1 0 28.67 21.96 0 9 1 0 13.08 17.50 0 -10 1 0 24.18 21.20 0 -10 -1 0 3.03 14.96 0 10 1 0 10.99 19.32 0 10 -1 0 26.68 18.52 0 -11 1 0 324.73 22.15 0 11 -1 0 277.43 20.43 0 -11 -1 0 217.91 23.50 0 11 1 0 184.27 20.67 0 12 -1 0 235.33 14.99 0 -12 1 0 273.83 22.41 0 12 1 0 240.36 21.56 0 -12 -1 0 274.56 24.75 0 -13 -1 0 13.71 16.58 0 13 1 0 12.90 19.50 0 13 -1 0 8.64 20.72 0 -13 1 0 15.95 22.02 0 -14 -1 0 10.81 25.24 0 14 -1 0 -5.37 16.10 0 14 1 0 -8.83 20.27 0 -14 1 0 10.36 23.15 0 -15 -1 0 8.04 20.92 0 15 1 0 4.12 22.57 0 -15 1 0 44.92 24.28 0 16 1 0 4.16 24.36 0 -16 1 0 18.37 26.91 0 -16 -1 0 10.73 30.69 0 -17 1 0 25.19 28.38 0 17 1 0 8.44 26.56 0 -17 -1 0 10.76 31.35 0 0 2 0 40.20 17.13 0 1 -2 0 58.81 17.77 0 -1 2 0 55.77 18.26 0 1 2 0 37.00 12.92 0 -1 -2 0 56.00 17.75 0 2 2 0 2966.81 40.52 0 -2 2 0 2972.58 42.55 0 -2 -2 0 2913.02 40.35 0 -3 -2 0 2170.97 30.24 0 -3 2 0 2801.82 39.54 0 3 2 0 2718.23 36.04 0 4 2 0 69.67 13.97 0 -4 2 0 120.03 21.03 0 -4 -2 0 83.86 19.06 0 5 2 0 262.53 19.93 0 -5 2 0 318.89 23.81 0 -5 -2 0 222.44 20.14 0 -6 2 0 358.04 23.51 0 -6 -2 0 250.52 21.88 0 6 2 0 259.14 21.29 0 6 -2 0 273.13 22.25 0 7 2 0 136.55 19.08 0 -7 -2 0 123.67 14.43 0 -7 2 0 122.35 15.80 0 7 -2 0 122.05 14.67 0 -8 -2 0 4.81 13.09 0 -8 2 0 -2.19 18.98 0 8 2 0 12.15 17.26 0 8 -2 0 8.41 12.10 0 9 2 0 41.33 17.17 0 9 -2 0 40.27 17.33 0 -9 -2 0 32.40 17.99 0 -9 2 0 45.44 20.57 0 10 2 0 93.00 14.40 0 -10 -2 0 89.97 15.78 0 -10 2 0 127.63 15.65 0 10 -2 0 154.33 18.43 0 11 2 0 -18.98 18.79 0 -11 -2 0 6.87 20.92 0 11 -2 0 17.20 18.52 0 -11 2 0 0.84 21.15 0 -12 2 0 8.33 15.32 0 -12 -2 0 13.52 21.85 0 12 2 0 2.87 13.96 0 -13 -2 0 -17.06 23.73 0 -13 2 0 -5.24 22.96 0 13 2 0 13.09 19.81 0 14 2 0 48.75 22.54 0 -14 -2 0 57.63 18.17 0 -14 2 0 103.60 25.94 0 -15 2 0 2.77 18.90 0 -15 -2 0 10.06 25.79 0 15 2 0 12.00 24.68 0 16 2 0 32.41 25.23 0 -16 -2 0 19.16 31.95 0 -16 2 0 6.02 21.11 0 -17 2 0 21.59 28.55 0 -17 -2 0 -6.31 25.29 0 17 2 0 3.72 22.26 0 -1 3 0 298.02 21.57 0 1 -3 0 286.61 21.35 0 1 3 0 177.83 15.59 0 -1 -3 0 255.12 21.09 0 2 -3 0 1003.32 23.53 0 2 3 0 922.18 21.95 0 -2 3 0 1120.67 27.35 0 -2 -3 0 1089.15 26.82 0 -3 3 0 29.99 12.25 0 3 3 0 33.99 17.09 0 -3 -3 0 23.94 12.17 0 4 3 0 12.56 12.52 0 -4 3 0 6.42 18.99 0 -4 3 0 10.17 18.27 0 -4 -3 0 9.07 12.56 0 -5 -3 0 279.99 14.61 0 -5 3 0 270.49 17.07 0 5 3 0 322.70 19.73 0 6 3 0 205.29 19.95 0 -6 3 0 252.03 21.92 0 -6 -3 0 176.30 19.17 0 -7 -3 0 89.56 18.33 0 7 3 0 103.85 18.17 0 -7 3 0 107.76 18.66 0 -8 -3 0 84.18 18.43 0 8 3 0 96.74 17.63 0 -8 3 0 119.59 18.95 0 -9 3 0 51.44 19.54 0 -9 -3 0 31.02 17.86 0 9 3 0 21.54 16.85 0 10 3 0 84.00 17.62 0 -10 -3 0 72.69 20.36 0 -10 3 0 112.81 15.31 0 -11 -3 0 13.80 14.57 0 11 3 0 5.85 18.48 0 -11 3 0 10.95 18.97 0 12 3 0 15.02 19.64 0 -12 -3 0 12.27 21.70 0 -12 3 0 23.96 21.48 0 -13 -3 0 20.78 22.96 0 -13 3 0 18.95 21.84 0 13 3 0 17.52 15.43 0 -14 -3 0 -10.89 24.73 0 14 3 0 -7.61 22.02 0 -14 3 0 12.61 25.65 0 15 3 0 16.22 22.63 0 -15 3 0 13.36 18.96 0 -15 -3 0 7.13 27.30 0 -16 3 0 8.27 28.47 0 -16 -3 0 23.24 32.44 0 16 3 0 9.89 20.56 0 -17 -3 0 15.21 27.27 0 17 3 0 -16.73 31.83 0 -17 3 0 20.49 27.99 0 0 4 0 33.71 12.74 0 0 -4 0 61.16 17.47 0 -1 -4 0 282.79 19.32 0 -1 4 0 342.69 19.91 0 1 -4 0 330.87 19.77 0 1 4 0 221.54 14.36 0 2 4 0 410.73 19.60 0 -2 -4 0 312.99 14.81 0 2 -4 0 376.08 19.76 0 -2 4 0 365.15 19.56 0 3 -4 0 313.31 15.88 0 -3 4 0 348.62 19.84 0 -3 -4 0 339.18 19.84 0 3 4 0 350.12 19.77 0 -4 -4 0 72.19 12.87 0 -4 4 0 68.68 18.73 0 4 4 0 92.80 17.33 0 -5 -4 0 219.13 19.49 0 -5 4 0 238.97 15.22 0 -5 4 0 269.69 19.98 0 5 4 0 267.90 19.61 0 -6 4 0 13.92 18.28 0 -6 4 0 17.96 17.56 0 -6 -4 0 8.99 17.60 0 6 4 0 18.82 16.56 0 7 4 0 2.91 12.38 0 -7 4 0 21.74 17.60 0 -7 -4 0 14.90 17.31 0 -7 4 0 10.85 13.20 0 -8 -4 0 10.61 16.67 0 -8 4 0 0.22 18.67 0 8 4 0 15.95 11.74 0 -9 -4 0 57.88 18.20 0 9 4 0 35.83 17.89 0 -9 4 0 67.16 19.41 0 10 4 0 32.04 14.16 0 -10 -4 0 62.26 20.02 0 -10 4 0 57.71 14.72 0 11 4 0 20.14 16.99 0 -11 4 0 70.19 19.21 0 -11 -4 0 36.47 19.32 0 12 4 0 -3.26 14.17 0 -12 -4 0 1.65 19.73 0 -12 4 0 1.08 19.82 0 13 4 0 8.42 18.96 0 -13 4 0 12.84 17.06 0 -13 -4 0 1.38 22.80 0 -14 -4 0 6.54 18.22 0 -14 4 0 26.53 22.58 0 14 4 0 11.08 22.63 0 -15 4 0 18.46 26.82 0 15 4 0 8.87 17.89 0 -15 -4 0 -3.22 25.22 0 -16 -4 0 -12.18 29.59 0 -16 4 0 8.95 20.58 0 16 4 0 34.17 28.78 0 -16 4 0 -4.76 25.66 0 -17 -4 0 -0.62 26.75 0 -17 4 0 -8.06 28.58 0 17 4 0 12.95 23.36 0 -17 4 0 -13.41 31.85 0 -1 5 0 585.22 21.48 0 -1 -5 0 515.63 21.51 0 1 -5 0 407.92 16.51 0 1 5 0 587.29 21.03 0 -2 -5 0 8.21 16.98 0 2 5 0 9.66 17.23 0 2 -5 0 9.74 17.20 0 -2 5 0 16.67 17.03 0 3 5 0 261.10 14.74 0 3 -5 0 267.06 19.11 0 -3 -5 0 277.32 19.29 0 -3 5 0 298.34 19.60 0 -4 5 0 30.14 17.39 0 4 5 0 32.33 16.91 0 -4 -5 0 22.00 16.86 0 -5 -5 0 98.57 17.76 0 -5 5 0 81.65 12.70 0 5 5 0 96.16 12.76 0 -6 5 0 15.80 16.88 0 -6 -5 0 11.62 12.22 0 -6 5 0 11.76 17.24 0 6 5 0 11.79 12.05 0 7 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104.86 16.03 0 -3 4 3 137.84 17.13 0 2 -4 -3 338.69 15.19 0 2 4 -3 449.68 21.36 0 -2 4 3 477.23 20.26 0 1 -4 -3 1320.50 22.39 0 -1 4 3 1775.97 28.69 0 1 4 -3 1513.01 32.45 0 0 -4 3 742.17 28.34 0 0 -4 -3 1100.13 24.36 0 0 4 -3 732.41 26.57 0 0 4 3 802.34 19.09 0 -1 4 -3 690.27 27.39 0 1 -4 3 890.65 28.23 0 1 4 3 1150.64 24.71 0 -1 -4 -3 866.20 19.13 0 -2 4 -3 1311.19 32.09 0 2 4 3 1425.69 24.78 0 -2 -4 -3 959.18 19.71 0 -3 4 -3 501.49 22.49 0 3 4 3 691.91 21.66 0 -3 -4 -3 525.02 20.59 0 -3 4 -3 585.34 24.80 0 -4 -4 -3 162.76 18.80 0 -4 4 -3 165.82 19.69 0 4 4 3 182.33 17.61 0 -4 4 -3 172.39 22.62 0 5 4 3 108.32 17.81 0 -5 -4 -3 115.25 17.46 0 -5 4 -3 88.28 20.96 0 -5 4 -3 102.52 19.29 0 6 4 3 78.39 17.22 0 -6 -4 -3 79.94 12.27 0 -6 4 -3 118.90 19.66 0 -7 -4 -3 2.62 16.25 0 -7 4 -3 4.57 19.68 0 7 4 3 15.46 11.49 0 -8 -4 -3 16.03 16.37 0 8 4 3 -6.13 17.33 0 -8 4 -3 -11.54 18.89 0 -9 -4 -3 -0.53 17.71 0 -9 4 -3 10.76 20.31 0 9 4 3 3.65 16.40 0 -10 -4 -3 110.04 13.94 0 10 4 3 91.77 19.04 0 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23.04 23.16 0 -14 5 -3 33.72 20.05 0 -14 -5 -3 31.33 27.03 0 -14 5 -3 41.50 19.92 0 -15 -5 -3 9.29 27.40 0 15 5 3 0.85 25.35 0 -15 5 -3 -8.82 21.12 0 -15 5 -3 22.72 29.26 0 -16 -5 -3 27.81 34.40 0 -16 5 -3 18.01 27.85 0 16 5 3 10.56 31.70 0 -16 5 -3 30.13 27.88 0 -16 -6 3 2.42 23.83 0 -16 6 3 2.99 21.44 0 16 6 -3 -1.23 21.89 0 -16 6 3 24.17 30.80 0 -15 6 3 6.89 20.51 0 -15 6 3 16.01 28.58 0 -15 -6 3 -10.70 29.22 0 15 6 -3 1.25 27.63 0 -14 -6 3 7.46 23.51 0 -14 6 3 33.90 23.35 0 -14 6 3 10.46 23.04 0 14 6 -3 16.87 17.57 0 -13 6 3 28.46 22.60 0 -13 6 3 31.25 23.09 0 13 6 -3 30.27 22.24 0 -13 -6 3 13.80 23.55 0 12 6 -3 10.45 14.70 0 -12 -6 3 18.85 15.12 0 -12 6 3 14.32 15.29 0 -12 6 3 25.80 21.17 0 -11 -6 3 5.54 13.81 0 11 6 -3 18.96 18.02 0 -11 6 3 -2.48 20.05 0 -11 6 3 -17.86 20.60 0 -10 -6 3 22.18 18.42 0 -10 6 3 4.18 20.12 0 10 6 -3 22.27 18.43 0 -10 6 3 14.71 20.23 0 -9 6 3 15.53 13.31 0 9 6 -3 17.11 17.33 0 -9 6 3 1.81 13.48 0 -9 -6 3 21.79 17.46 0 -8 -6 3 4.11 17.85 0 -8 6 3 11.25 17.46 0 -8 6 3 27.19 12.86 0 8 6 -3 7.70 18.05 0 -7 -6 3 18.60 16.96 0 -7 6 3 5.58 12.23 0 7 6 -3 21.26 12.21 0 -6 -6 3 84.94 12.68 0 -6 6 3 88.14 16.86 0 6 6 -3 131.76 18.33 0 5 6 -3 11.73 16.77 0 5 -6 -3 -3.92 11.89 0 -5 6 3 -0.65 11.79 0 -5 -6 3 10.49 16.42 0 4 6 -3 7.38 16.54 0 4 -6 -3 -7.37 12.13 0 -4 6 3 5.98 16.85 0 -4 -6 3 7.61 11.29 0 3 6 -3 96.14 18.36 0 -3 6 3 86.74 13.00 0 3 -6 -3 74.12 13.15 0 -3 -6 3 92.69 17.69 0 2 -6 -3 447.25 15.91 0 -2 6 3 552.26 20.88 0 2 6 -3 554.51 22.21 0 -1 6 3 -1.03 12.26 0 1 6 -3 -2.42 16.62 0 1 -6 -3 4.85 12.17 0 0 6 -3 1197.96 26.43 0 0 6 3 1246.58 20.31 0 0 -6 -3 1223.16 20.22 0 -1 -6 -3 57.41 17.82 0 -1 6 -3 51.46 16.97 0 1 6 3 57.34 16.72 0 2 6 3 228.95 14.08 0 -2 6 -3 154.34 18.60 0 -2 -6 -3 235.28 19.44 0 -3 6 -3 73.28 16.92 0 3 6 3 74.95 12.25 0 -3 -6 -3 90.79 17.07 0 4 6 3 597.94 20.14 0 -4 6 -3 514.58 22.92 0 -4 -6 -3 563.41 15.36 0 -5 6 -3 39.19 18.81 0 -5 6 -3 44.06 17.00 0 -5 -6 -3 33.92 16.60 0 5 6 3 39.56 11.78 0 -6 6 -3 85.70 18.63 0 6 6 3 88.64 11.77 0 -6 6 -3 93.65 20.66 0 -6 -6 -3 89.27 15.57 0 7 6 3 11.88 16.95 0 -7 -6 -3 7.10 12.32 0 -7 6 -3 -3.20 20.36 0 -7 6 -3 21.54 17.09 0 8 6 3 13.69 16.63 0 -8 6 -3 7.71 19.03 0 -8 6 -3 10.29 20.21 0 -8 -6 -3 12.84 17.73 0 -9 -6 -3 -1.89 12.62 0 -9 6 -3 5.89 19.54 0 -9 6 -3 4.48 18.28 0 9 6 3 -0.80 17.83 0 -10 6 -3 25.20 18.71 0 10 6 3 -10.61 18.67 0 -10 6 -3 30.67 21.11 0 -10 -6 -3 19.32 13.19 0 -11 -6 -3 4.16 14.10 0 -11 6 -3 13.89 20.65 0 11 6 3 7.82 19.13 0 -11 6 -3 13.34 21.27 0 12 6 3 31.95 14.71 0 -12 -6 -3 22.86 21.95 0 -12 6 -3 21.50 16.23 0 -12 6 -3 29.25 21.35 0 -13 6 -3 34.98 22.44 0 -13 -6 -3 50.29 24.26 0 13 6 3 35.18 21.10 0 -13 6 -3 26.77 23.35 0 -14 -6 -3 -10.14 27.53 0 14 6 3 12.83 25.31 0 -14 6 -3 12.01 28.32 0 -14 6 -3 13.92 28.25 0 -15 6 -3 -12.95 27.39 0 -15 6 -3 32.95 27.35 0 15 6 3 7.55 28.14 0 -15 -6 -3 -21.93 28.40 0 -16 6 -3 -17.31 29.05 0 -16 6 -3 13.33 29.19 0 -16 -6 -3 33.80 35.47 0 16 6 3 29.72 31.97 0 -16 -7 3 -4.27 32.88 0 16 7 -3 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15.52 0 -4 7 3 44.37 15.73 0 -4 -7 3 35.37 16.36 0 3 7 -3 284.26 18.31 0 -3 7 3 315.74 18.65 0 -3 -7 3 301.25 18.05 0 3 -7 -3 330.69 18.92 0 2 7 -3 0.62 15.24 0 2 -7 -3 21.72 16.37 0 -2 7 3 0.81 16.34 0 -2 -7 3 12.61 15.21 0 -1 7 3 24.34 11.65 0 1 -7 -3 28.30 16.40 0 1 7 -3 23.34 15.97 0 0 7 -3 22.72 15.55 0 0 -7 -3 19.05 16.45 0 0 7 3 23.65 16.61 0 -1 -7 -3 119.58 17.36 0 1 7 3 134.21 17.53 0 -1 7 -3 114.42 15.68 0 -2 -7 -3 356.01 18.04 0 2 7 3 331.97 18.59 0 -2 7 -3 268.03 18.64 0 3 7 3 112.75 12.61 0 -3 -7 -3 123.34 17.19 0 -3 7 -3 108.37 17.33 0 4 7 3 52.21 16.51 0 -4 -7 -3 38.65 11.71 0 -4 7 -3 19.09 17.47 0 -5 7 -3 183.09 20.75 0 5 7 3 246.05 12.86 0 -5 -7 -3 264.50 16.83 0 -5 7 -3 195.16 19.73 0 6 7 3 7.78 16.52 0 -6 -7 -3 4.21 11.98 0 -6 7 -3 4.42 17.09 0 -6 7 -3 -9.28 17.77 0 -7 -7 -3 8.96 12.20 0 -7 7 -3 15.54 20.50 0 -7 7 -3 -10.10 17.32 0 7 7 3 5.43 12.48 0 8 7 3 60.69 16.77 0 -8 7 -3 70.07 20.91 0 -8 7 -3 65.53 13.97 0 -8 -7 -3 77.74 17.08 0 9 7 3 84.24 17.67 0 -9 7 -3 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4 68.51 20.23 0 -9 3 4 111.74 15.03 0 -9 3 4 97.16 19.51 0 9 3 -4 89.79 20.72 0 -9 -3 4 103.69 20.88 0 -8 -3 4 377.82 17.16 0 -8 3 4 496.44 21.46 0 8 3 -4 392.01 17.26 0 -8 3 4 490.71 21.65 0 -7 -3 4 15.50 16.67 0 7 3 -4 5.53 12.25 0 -7 3 4 3.93 13.29 0 -7 3 4 16.36 18.51 0 -6 3 4 16.26 18.19 0 6 3 -4 23.24 12.13 0 -6 3 4 20.22 18.10 0 -6 -3 4 21.79 12.34 0 -5 3 4 21.36 18.84 0 5 3 -4 35.85 18.15 0 -5 -3 4 24.50 17.64 0 -4 -3 4 16.77 18.35 0 -4 3 4 10.89 17.87 0 4 3 -4 20.28 19.00 0 -3 3 4 333.49 15.20 0 3 3 -4 449.84 22.75 0 3 -3 -4 370.02 15.77 0 -2 3 4 105.63 13.19 0 2 -3 -4 108.65 13.75 0 2 3 -4 109.79 19.69 0 -1 3 4 200.89 14.52 0 1 3 -4 222.70 27.97 0 1 -3 -4 225.51 18.88 0 -1 -3 4 173.96 24.56 0 0 3 -4 91.95 31.20 0 0 -3 4 65.09 29.15 0 0 -3 -4 86.79 13.60 0 0 3 4 89.14 16.78 0 -1 -3 -4 190.52 14.28 0 -1 3 -4 391.35 40.71 0 -1 3 -4 166.02 28.29 0 1 3 4 277.70 19.26 0 2 3 4 -3.93 12.34 0 -2 -3 -4 6.92 12.35 0 -2 3 -4 5.91 21.55 0 -2 3 -4 2.90 21.40 0 3 3 4 202.68 19.48 0 -3 3 -4 152.47 21.84 0 -3 -3 -4 194.13 19.12 0 -4 -3 -4 196.58 14.44 0 -4 3 -4 341.26 24.15 0 4 3 4 288.84 18.87 0 5 -3 4 117.34 20.16 0 5 3 4 133.99 17.42 0 -5 -3 -4 97.16 12.53 0 -5 3 -4 129.52 21.22 0 -6 -3 -4 117.28 16.86 0 6 -3 4 69.89 19.66 0 6 3 4 123.85 17.02 0 -6 3 -4 138.47 21.74 0 -7 -3 -4 356.16 14.14 0 7 -3 4 318.75 20.65 0 7 3 4 414.16 18.89 0 -7 3 -4 373.37 18.04 0 8 -3 4 15.93 13.44 0 -8 -3 -4 29.96 17.52 0 8 3 4 21.37 17.42 0 -8 3 -4 26.24 15.15 0 -9 -3 -4 15.89 18.82 0 -9 3 -4 26.60 21.49 0 9 -3 4 3.62 19.43 0 9 3 4 23.75 18.66 0 10 -3 4 -16.59 20.11 0 -10 3 -4 4.21 21.28 0 10 3 4 -15.10 12.77 0 -10 -3 -4 -0.84 18.58 0 -11 -3 -4 9.75 19.83 0 11 3 4 2.81 18.86 0 -11 3 -4 42.98 22.31 0 12 3 4 19.32 20.92 0 -12 -3 -4 -11.87 22.86 0 -12 3 -4 2.03 23.05 0 -13 3 -4 3.09 25.51 0 -13 -3 -4 9.36 22.31 0 13 3 4 16.35 22.48 0 14 3 4 3.37 25.67 0 -14 -3 -4 -4.48 28.08 0 -14 3 -4 14.16 28.34 0 -15 3 -4 21.72 27.02 0 -15 -3 -4 18.20 20.91 0 15 3 4 18.88 27.23 0 -16 3 -4 5.69 23.20 0 16 3 4 3.35 21.27 0 -16 -3 -4 9.07 29.59 0 -17 -4 4 -3.59 35.53 0 -17 4 4 15.06 29.23 0 17 4 -4 -18.91 28.03 0 -17 4 4 -3.06 29.00 0 16 4 -4 -4.02 26.17 0 -16 4 4 -16.53 21.20 0 -16 4 4 1.73 21.05 0 -16 -4 4 7.41 24.08 0 -15 -4 4 5.78 27.50 0 15 4 -4 6.30 18.82 0 -15 4 4 21.54 24.67 0 -15 4 4 26.51 22.64 0 -14 -4 4 9.22 24.05 0 -14 4 4 12.08 16.56 0 14 4 -4 15.80 16.97 0 -14 4 4 9.14 22.80 0 -13 -4 4 3.91 21.75 0 -13 4 4 15.43 19.91 0 -13 4 4 0.07 15.34 0 13 4 -4 1.76 15.35 0 -12 4 4 53.17 15.36 0 12 4 -4 63.23 15.44 0 -12 4 4 50.37 15.07 0 -12 -4 4 48.51 16.04 0 -11 -4 4 5.63 19.11 0 -11 4 4 -0.86 19.16 0 11 4 -4 11.46 14.32 0 -11 4 4 18.61 19.09 0 -10 -4 4 2.27 19.88 0 -10 4 4 9.99 14.15 0 10 4 -4 -9.95 19.18 0 -10 4 4 0.96 14.39 0 -9 4 4 5.92 18.74 0 -9 -4 4 -0.17 18.80 0 -9 4 4 5.64 14.00 0 9 4 -4 0.31 18.37 0 -8 -4 4 -11.57 18.09 0 8 4 -4 1.54 12.51 0 -8 4 4 16.36 17.50 0 -8 4 4 12.27 12.54 0 -7 4 4 6.41 17.95 0 -7 4 4 6.95 18.09 0 7 4 -4 -13.80 17.52 0 -7 -4 4 8.14 12.44 0 -6 -4 4 87.18 17.82 0 -6 4 4 78.26 17.80 0 6 4 -4 77.35 18.29 0 -5 -4 4 6.73 17.37 0 5 4 -4 4.95 17.86 0 -5 4 4 2.54 12.32 0 -4 -4 4 81.06 17.77 0 -4 4 4 78.80 17.96 0 4 -4 -4 49.40 12.96 0 4 4 -4 92.92 19.21 0 3 4 -4 306.80 20.24 0 3 -4 -4 327.91 19.34 0 -3 4 4 215.71 14.11 0 -2 4 4 41.22 12.14 0 2 -4 -4 55.48 17.09 0 2 4 -4 55.31 17.69 0 1 4 -4 225.46 21.19 0 -1 4 4 283.39 18.51 0 -1 -4 4 159.90 19.26 0 1 -4 -4 274.32 18.51 0 0 -4 -4 3940.37 36.62 0 0 4 -4 2721.54 51.45 0 0 -4 4 2299.37 49.57 0 0 4 4 2827.77 28.98 0 -1 -4 -4 404.79 19.75 0 -1 4 -4 229.16 25.18 0 1 -4 4 317.97 26.55 0 1 4 4 402.94 19.66 0 -2 -4 -4 885.70 19.63 0 2 4 4 914.34 19.43 0 -2 4 -4 958.80 29.92 0 -2 4 -4 1123.63 33.73 0 -3 4 -4 117.24 20.91 0 3 4 4 138.24 18.61 0 -3 4 -4 154.51 25.90 0 -3 -4 -4 92.42 17.72 0 -4 -4 -4 188.97 13.39 0 4 4 4 207.41 13.49 0 -4 4 -4 228.21 20.40 0 -4 4 -4 258.30 23.06 0 -5 -4 -4 164.23 17.10 0 -5 4 -4 172.30 21.46 0 5 4 4 149.48 12.69 0 6 4 4 352.05 17.50 0 -6 -4 -4 349.20 17.97 0 -6 4 -4 279.14 17.70 0 -7 4 -4 5.14 20.20 0 -7 -4 -4 4.21 11.93 0 7 4 4 -2.90 16.60 0 -8 -4 -4 81.99 13.16 0 -8 4 -4 116.42 20.89 0 8 4 4 109.63 17.70 0 -9 -4 -4 87.08 19.04 0 -9 4 -4 111.34 23.51 0 9 4 4 63.13 18.55 0 -10 -4 -4 -3.67 18.94 0 10 4 4 10.08 18.84 0 -10 4 -4 15.54 21.49 0 -11 -4 -4 18.51 18.41 0 11 4 4 8.23 18.45 0 -11 4 -4 35.23 21.73 0 12 4 4 24.63 21.54 0 -12 -4 -4 32.82 15.74 0 -12 4 -4 50.50 24.81 0 -13 4 -4 -7.24 26.27 0 -13 -4 -4 0.04 16.70 0 13 4 4 -13.94 22.99 0 -14 -4 -4 25.73 26.70 0 -14 4 -4 8.13 27.32 0 14 4 4 -4.33 24.66 0 -15 4 -4 4.26 29.55 0 15 4 4 18.57 28.11 0 -15 -4 -4 10.00 22.25 0 -16 4 -4 -1.17 28.99 0 -16 -4 -4 -0.20 33.38 0 16 4 4 34.55 31.04 0 17 5 -4 26.55 23.14 0 -17 5 4 16.24 24.70 0 -17 -5 4 6.53 37.23 0 -17 5 4 21.81 33.50 0 -16 -5 4 -4.58 34.99 0 16 5 -4 5.71 26.20 0 -16 5 4 -20.09 27.03 0 -16 5 4 3.18 30.27 0 -15 -5 4 18.79 29.63 0 -15 5 4 -6.98 19.53 0 15 5 -4 26.74 26.95 0 -15 5 4 6.83 24.03 0 -14 5 4 23.48 21.55 0 14 5 -4 -8.56 24.96 0 -14 5 4 4.28 22.72 0 -14 -5 4 -2.08 25.90 0 -13 5 4 3.96 19.99 0 -13 -5 4 8.58 16.76 0 13 5 -4 26.08 20.97 0 -13 5 4 34.17 21.40 0 -12 5 4 53.71 14.79 0 -12 -5 4 50.37 21.98 0 -12 5 4 45.97 15.00 0 12 5 -4 55.90 15.75 0 -11 5 4 99.77 20.53 0 -11 -5 4 63.19 14.37 0 -11 5 4 73.27 20.75 0 11 5 -4 72.79 19.43 0 -10 -5 4 1.50 13.66 0 -10 5 4 18.36 20.19 0 10 5 -4 2.78 17.31 0 -10 5 4 32.44 19.83 0 -9 -5 4 10.97 18.09 0 -9 5 4 27.25 19.48 0 -9 5 4 16.81 14.07 0 9 5 -4 11.89 18.81 0 -8 -5 4 30.84 12.77 0 -8 5 4 35.41 17.26 0 8 5 -4 12.39 16.92 0 -8 5 4 23.21 12.24 0 -7 5 4 139.93 17.68 0 -7 -5 4 188.81 17.97 0 7 5 -4 157.21 18.26 0 -7 5 4 163.54 17.25 0 -6 -5 4 135.65 17.01 0 -6 5 4 93.17 17.96 0 6 5 -4 102.60 18.71 0 5 -5 -4 1.77 17.17 0 -5 -5 4 7.58 16.91 0 -5 5 4 20.36 17.09 0 5 5 -4 20.71 17.24 0 -4 5 4 46.88 17.73 0 4 5 -4 33.66 17.86 0 -4 -5 4 27.55 16.86 0 4 -5 -4 65.76 17.73 0 3 5 -4 129.87 19.49 0 -3 5 4 119.58 13.47 0 3 -5 -4 193.28 18.65 0 2 -5 -4 221.73 17.85 0 -2 5 4 209.67 18.15 0 2 5 -4 224.63 21.53 0 -1 5 4 112.54 17.49 0 1 5 -4 124.20 21.40 0 1 -5 -4 130.16 17.46 0 -1 -5 4 74.08 16.67 0 0 -5 -4 4.93 11.64 0 0 5 -4 -0.05 18.73 0 0 -5 4 1.89 18.98 0 0 5 4 5.43 11.81 0 -1 -5 -4 556.87 21.11 0 1 5 4 444.94 15.59 0 1 -5 4 495.42 25.10 0 -1 5 -4 316.83 24.55 0 2 5 4 4.87 16.72 0 -2 5 -4 6.43 15.38 0 -2 -5 -4 4.92 16.91 0 -3 5 -4 9.71 16.18 0 3 5 4 0.33 12.05 0 -3 5 -4 24.83 18.48 0 -3 -5 -4 10.50 16.83 0 4 5 4 158.69 17.68 0 -4 5 -4 139.41 20.51 0 -4 -5 -4 141.11 17.38 0 -4 5 -4 131.45 19.88 0 5 5 4 230.32 17.38 0 -5 5 -4 284.51 22.84 0 -5 5 -4 220.16 19.81 0 -5 -5 -4 173.52 12.60 0 6 5 4 1.98 16.05 0 -6 5 -4 11.22 18.20 0 -6 -5 -4 -3.84 11.28 0 -6 5 -4 -1.50 20.43 0 -7 -5 -4 125.73 17.57 0 7 5 4 111.07 12.59 0 -7 5 -4 92.20 20.37 0 -7 5 -4 111.18 21.47 0 8 5 4 2.07 12.32 0 -8 5 -4 6.78 13.99 0 -8 -5 -4 18.31 16.14 0 -8 5 -4 27.19 20.23 0 -9 5 -4 -4.21 13.54 0 -9 -5 -4 14.55 17.67 0 -9 5 -4 2.16 20.93 0 9 5 4 8.45 17.82 0 -10 -5 -4 -6.89 18.82 0 10 5 4 16.70 18.26 0 -10 5 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6 -4 43.38 19.73 0 -10 6 4 81.29 19.56 0 -10 -6 4 68.49 13.36 0 -10 6 4 80.72 20.48 0 10 6 -4 38.96 13.31 0 9 6 -4 79.60 18.64 0 -9 -6 4 81.82 18.01 0 -9 6 4 120.57 18.25 0 -9 6 4 77.51 13.99 0 -8 -6 4 -3.14 12.72 0 -8 6 4 10.27 17.72 0 -8 6 4 -3.80 13.04 0 8 6 -4 -1.70 12.64 0 -7 6 4 2.15 11.50 0 7 6 -4 14.99 17.20 0 -7 -6 4 7.25 16.71 0 6 6 -4 224.03 19.25 0 -6 6 4 232.58 17.61 0 -6 -6 4 225.08 18.46 0 -5 -6 4 78.31 16.70 0 -5 6 4 66.18 12.43 0 5 -6 -4 46.86 16.61 0 5 6 -4 72.65 17.53 0 4 6 -4 78.43 13.00 0 -4 6 4 122.60 17.17 0 -4 -6 4 102.85 16.46 0 4 -6 -4 84.56 16.47 0 3 6 -4 660.02 25.31 0 -3 6 4 942.56 22.14 0 3 -6 -4 649.23 17.46 0 2 -6 -4 375.21 15.49 0 -2 6 4 410.19 15.42 0 2 6 -4 454.49 21.09 0 -1 6 4 27.58 12.38 0 1 6 -4 35.97 18.49 0 1 -6 -4 46.67 17.40 0 0 -6 -4 107.36 13.18 0 0 6 -4 98.55 16.20 0 0 6 4 153.65 17.94 0 0 -6 4 104.55 19.07 0 -1 6 -4 300.23 19.24 0 -1 -6 -4 327.25 14.79 0 1 -6 4 487.39 23.64 0 1 6 4 369.36 15.05 0 2 6 4 155.30 17.50 0 -2 6 -4 90.49 16.96 0 2 -6 4 146.98 20.84 0 -2 -6 -4 128.42 17.37 0 -3 -6 -4 983.40 17.92 0 -3 6 -4 850.68 26.02 0 3 6 4 1122.19 22.74 0 4 6 4 -1.06 16.07 0 -4 6 -4 8.87 19.05 0 -4 -6 -4 -6.08 16.08 0 -4 6 -4 -2.99 17.18 0 -5 6 -4 2.08 20.43 0 5 6 4 -0.80 11.12 0 -5 -6 -4 -3.53 11.06 0 -5 6 -4 4.53 17.64 0 6 6 4 -4.02 11.60 0 -6 6 -4 -1.44 16.73 0 -6 -6 -4 5.39 16.39 0 -6 6 -4 3.91 18.90 0 -7 6 -4 21.89 20.22 0 7 6 4 19.04 16.65 0 -7 -6 -4 3.71 17.21 0 -7 6 -4 3.70 18.96 0 -8 -6 -4 21.71 16.07 0 8 6 4 19.44 12.14 0 -8 6 -4 18.07 20.19 0 -8 6 -4 18.83 18.08 0 9 6 4 405.67 21.07 0 -9 -6 -4 489.13 21.06 0 -9 6 -4 483.53 24.45 0 -9 6 -4 533.35 22.99 0 -10 6 -4 -12.25 22.30 0 -10 6 -4 7.82 20.53 0 -10 -6 -4 1.44 18.47 0 10 6 4 11.58 18.42 0 11 6 4 13.43 20.63 0 -11 -6 -4 41.70 20.18 0 -11 6 -4 27.12 20.66 0 -11 6 -4 27.52 23.92 0 -12 6 -4 -8.41 22.16 0 -12 -6 -4 12.85 15.46 0 12 6 4 7.90 20.35 0 -12 6 -4 26.44 25.28 0 -13 -6 -4 11.17 24.80 0 13 6 4 11.18 24.32 0 -13 6 -4 23.38 23.13 0 -13 6 -4 6.50 23.27 0 14 6 4 3.93 23.86 0 -14 -6 -4 16.41 27.65 0 -14 6 -4 -27.15 27.61 0 -14 6 -4 16.07 28.42 0 15 6 4 27.85 25.56 0 -15 -6 -4 20.58 27.91 0 -15 6 -4 -2.65 28.61 0 -15 6 -4 29.23 27.92 0 -16 -7 4 -19.89 32.53 0 16 7 -4 -4.83 30.73 0 -16 7 4 -5.65 31.31 0 -16 7 4 -7.77 28.25 0 -15 -7 4 28.05 20.25 0 15 7 -4 36.70 25.24 0 -15 7 4 40.70 28.88 0 -15 7 4 17.10 21.15 0 -14 -7 4 30.25 25.92 0 -14 7 4 6.64 19.11 0 -14 7 4 24.06 24.31 0 14 7 -4 34.06 23.57 0 -13 -7 4 18.35 22.40 0 13 7 -4 0.48 23.36 0 -13 7 4 -2.43 23.30 0 -13 7 4 -6.94 23.76 0 12 7 -4 12.31 20.59 0 -12 -7 4 11.29 20.96 0 -12 7 4 7.74 16.45 0 -12 7 4 18.61 20.97 0 11 7 -4 20.52 15.03 0 -11 7 4 15.74 19.83 0 -11 7 4 2.06 19.63 0 -11 -7 4 23.68 20.51 0 -10 7 4 19.82 14.05 0 -10 -7 4 3.74 17.85 0 -10 7 4 5.46 19.62 0 10 7 -4 1.12 18.29 0 -9 -7 4 -5.95 17.80 0 -9 7 4 19.77 18.85 0 9 7 -4 2.93 13.81 0 -9 7 4 3.43 18.69 0 -8 -7 4 13.95 18.62 0 -8 7 4 26.31 17.82 0 8 7 -4 23.55 19.36 0 -7 7 4 46.45 17.22 0 -7 -7 4 41.96 12.28 0 7 7 -4 48.79 12.75 0 -6 7 4 29.43 16.39 0 -6 -7 4 38.41 11.85 0 6 7 -4 24.64 12.30 0 5 -7 -4 -1.48 15.60 0 -5 -7 4 4.82 16.58 0 -5 7 4 4.72 15.35 0 5 7 -4 11.56 16.92 0 4 7 -4 13.64 16.37 0 4 -7 -4 11.69 11.48 0 -4 7 4 10.21 16.31 0 -4 -7 4 4.83 11.12 0 3 -7 -4 115.25 17.18 0 -3 7 4 141.72 17.17 0 3 7 -4 125.26 16.87 0 -2 7 4 249.26 17.85 0 2 7 -4 207.16 17.88 0 2 -7 -4 292.18 17.46 0 -1 7 4 17.09 16.10 0 1 7 -4 12.01 15.79 0 1 -7 -4 20.82 16.21 0 0 -7 -4 49.60 11.72 0 0 7 -4 51.21 18.17 0 0 7 4 42.98 11.75 0 1 -7 4 117.11 17.25 0 1 7 4 129.51 16.92 0 -1 -7 -4 94.07 12.04 0 -1 7 -4 98.07 16.77 0 -2 -7 -4 224.19 17.06 0 -2 7 -4 177.82 18.35 0 2 7 4 215.74 13.35 0 3 7 4 26.31 15.48 0 -3 7 -4 12.25 17.44 0 -3 -7 -4 16.58 16.15 0 -4 -7 -4 237.80 16.11 0 4 7 4 222.85 12.46 0 -4 7 -4 137.80 19.99 0 -5 7 -4 12.54 19.03 0 5 7 4 -1.19 11.15 0 -5 -7 -4 4.76 11.13 0 -5 7 -4 8.59 19.14 0 6 7 4 9.70 16.27 0 -6 7 -4 12.05 17.69 0 -6 -7 -4 27.27 16.68 0 -6 7 -4 18.14 20.15 0 7 7 4 18.64 12.00 0 -7 7 -4 8.14 19.80 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51.43 11.56 0 -4 -4 -5 73.76 16.15 0 -4 4 -5 63.03 19.88 0 -4 4 -5 58.83 20.76 0 5 4 5 156.03 12.67 0 -5 -4 -5 228.08 16.69 0 -5 4 -5 210.81 23.06 0 6 4 5 41.41 15.84 0 -6 -4 -5 25.94 11.78 0 -6 4 -5 30.03 21.74 0 7 4 5 126.40 17.80 0 -7 -4 -5 115.98 17.28 0 -7 4 -5 117.45 20.77 0 -8 -4 -5 18.02 13.03 0 -8 4 -5 30.85 20.37 0 8 4 5 39.84 18.18 0 -9 -4 -5 24.70 18.33 0 9 4 5 12.22 16.95 0 -9 4 -5 21.50 20.92 0 10 4 5 27.95 17.62 0 -10 -4 -5 21.04 18.58 0 -10 4 -5 34.84 21.83 0 -11 -4 -5 19.92 15.19 0 11 4 5 14.23 20.79 0 -11 4 -5 13.31 17.43 0 -12 4 -5 12.31 19.08 0 12 4 5 18.10 20.42 0 -12 -4 -5 -2.89 22.90 0 -13 4 -5 26.71 24.94 0 -13 -4 -5 26.29 24.67 0 13 4 5 22.01 21.92 0 -14 4 -5 45.13 25.74 0 14 4 5 32.66 23.95 0 -14 -4 -5 24.30 24.70 0 -15 4 -5 -14.29 28.02 0 -15 -4 -5 -7.88 26.46 0 15 4 5 15.37 25.43 0 -16 -4 -5 2.18 31.45 0 -16 -5 5 16.26 33.68 0 -16 5 5 -12.14 26.99 0 16 5 -5 20.54 28.51 0 -16 5 5 -12.22 29.46 0 -15 -5 5 -0.75 29.06 0 15 5 -5 1.21 26.31 0 -15 5 5 14.46 25.65 0 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5 366.47 19.14 0 -3 6 -5 28.21 16.66 0 3 6 5 29.51 11.53 0 -3 -6 -5 36.93 15.71 0 -3 6 -5 34.39 23.01 0 -4 6 -5 7.04 17.60 0 4 6 5 6.59 11.04 0 -4 6 -5 4.74 20.99 0 -4 -6 -5 5.25 10.74 0 5 6 5 72.18 17.00 0 -5 6 -5 51.16 21.73 0 -5 -6 -5 81.17 16.88 0 -5 6 -5 61.19 21.53 0 6 6 5 13.92 16.16 0 -6 6 -5 7.31 16.34 0 -6 6 -5 10.27 19.48 0 -6 -6 -5 2.84 12.23 0 -7 6 -5 1.88 18.07 0 -7 6 -5 1.48 20.14 0 -7 -6 -5 13.54 15.77 0 7 6 5 2.29 16.96 0 8 6 5 227.91 19.12 0 -8 6 -5 200.82 20.23 0 -8 -6 -5 202.26 13.87 0 -8 6 -5 198.75 22.10 0 -9 6 -5 15.33 19.99 0 -9 6 -5 -5.66 21.43 0 -9 -6 -5 9.50 12.90 0 9 6 5 -0.16 12.74 0 -10 6 -5 35.13 22.25 0 -10 -6 -5 19.10 18.59 0 -10 6 -5 36.34 22.84 0 10 6 5 20.42 14.58 0 -11 -6 -5 3.55 19.32 0 -11 6 -5 -7.62 20.30 0 11 6 5 12.71 15.07 0 -11 6 -5 20.44 23.89 0 -12 6 -5 9.34 24.56 0 12 6 5 11.51 22.80 0 -12 -6 -5 21.92 21.05 0 -12 6 -5 18.39 24.04 0 -13 -6 -5 8.95 18.04 0 -13 6 -5 -0.96 23.80 0 13 6 5 -0.89 17.61 0 -13 6 -5 -7.66 26.87 0 -14 6 -5 6.52 28.19 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20.62 0 -6 -7 -5 22.08 17.02 0 -6 7 -5 23.78 16.55 0 7 7 5 8.51 17.32 0 -7 7 -5 12.02 17.44 0 -7 7 -5 9.87 19.43 0 -7 -7 -5 25.06 16.30 0 8 7 5 22.77 12.78 0 -8 -7 -5 22.04 17.86 0 -8 7 -5 34.00 19.07 0 -8 7 -5 22.64 20.31 0 -9 7 -5 79.29 22.64 0 -9 7 -5 97.76 24.06 0 -9 -7 -5 102.31 19.00 0 9 7 5 73.61 19.16 0 -10 7 -5 12.71 22.13 0 -10 -7 -5 9.77 18.33 0 -10 7 -5 9.65 23.72 0 10 7 5 -0.44 18.06 0 -11 -7 -5 31.84 19.86 0 -11 7 -5 13.09 22.85 0 11 7 5 29.87 22.03 0 -11 7 -5 43.41 25.27 0 12 7 5 7.24 23.27 0 -12 7 -5 -7.09 26.83 0 -12 7 -5 7.73 17.82 0 -12 -7 -5 8.56 23.06 0 -13 -7 -5 1.32 19.47 0 13 7 5 15.83 19.28 0 -13 7 -5 2.18 25.59 0 -13 7 -5 21.00 24.70 0 14 7 5 15.72 25.12 0 -14 -7 -5 4.07 25.91 0 -14 7 -5 -6.69 27.28 0 -14 7 -5 -3.23 30.60 0 -15 -7 -5 6.01 28.70 0 -15 7 -5 -2.53 34.20 0 -15 7 -5 15.36 33.63 0 -15 -8 5 -7.69 26.50 0 15 8 -5 3.10 29.33 0 -15 8 5 4.99 27.46 0 -15 8 5 -2.41 29.50 0 -14 8 5 -18.04 19.32 0 -14 8 5 9.34 24.03 0 -14 -8 5 13.18 26.99 0 14 8 -5 7.36 19.24 0 -13 -8 5 0.45 25.14 0 13 8 -5 9.98 24.63 0 -13 8 5 -10.25 25.83 0 -13 8 5 10.62 24.78 0 -12 -8 5 -9.45 23.44 0 -12 8 5 22.08 22.87 0 -12 8 5 22.04 21.88 0 12 8 -5 18.81 16.68 0 -11 -8 5 30.17 20.01 0 -11 8 5 58.85 22.23 0 -11 8 5 34.04 20.15 0 11 8 -5 37.66 21.29 0 -10 8 5 45.52 19.09 0 -10 -8 5 35.60 18.14 0 10 8 -5 22.30 20.08 0 -10 8 5 13.30 19.67 0 -9 8 5 2.36 17.57 0 9 8 -5 36.20 19.63 0 -9 -8 5 9.73 19.20 0 -9 8 5 10.74 17.52 0 -8 8 5 95.95 18.64 0 -8 -8 5 72.45 19.46 0 8 8 -5 58.05 20.35 0 -7 -8 5 30.28 13.13 0 7 8 -5 26.17 18.41 0 -7 8 5 26.74 17.90 0 6 -8 -5 409.02 19.12 0 -6 -8 5 420.80 20.40 0 -6 8 5 395.99 18.96 0 6 8 -5 411.68 16.57 0 -5 8 5 115.79 17.74 0 5 -8 -5 84.14 13.26 0 5 8 -5 122.88 18.84 0 -5 -8 5 126.73 17.02 0 -4 8 5 349.01 14.57 0 4 8 -5 397.97 21.14 0 4 -8 -5 306.11 14.29 0 3 8 -5 35.55 18.16 0 -3 8 5 29.30 15.79 0 3 -8 -5 25.67 15.62 0 2 -8 -5 20.83 14.60 0 2 8 -5 17.78 18.06 0 -2 8 5 16.81 14.61 0 1 8 -5 15.65 18.09 0 -1 -8 5 13.07 17.04 0 -1 8 5 28.25 15.48 0 1 -8 -5 27.20 15.30 0 0 -8 -5 51.33 14.82 0 0 8 -5 40.73 17.77 0 0 8 5 36.55 11.20 0 0 -8 5 60.55 20.27 0 -1 -8 -5 4.78 10.63 0 1 8 5 8.25 14.80 0 -1 8 -5 -0.66 17.15 0 1 -8 5 -1.33 17.04 0 2 -8 5 112.19 19.59 0 2 8 5 134.66 11.96 0 -2 8 -5 114.15 18.30 0 -2 -8 -5 148.80 16.31 0 -3 -8 -5 40.15 11.40 0 -3 8 -5 21.95 20.37 0 3 8 5 42.36 16.28 0 -4 8 -5 147.72 21.22 0 -4 8 -5 150.55 19.07 0 4 8 5 260.08 18.39 0 -4 -8 -5 260.84 17.60 0 -5 8 -5 148.54 18.34 0 5 8 5 183.37 17.04 0 -5 8 -5 134.77 21.25 0 -5 -8 -5 199.87 18.04 0 -6 8 -5 185.60 23.08 0 -6 -8 -5 265.81 13.48 0 6 8 5 246.64 18.17 0 -6 8 -5 183.69 19.49 0 -7 8 -5 8.07 20.41 0 7 8 5 6.78 18.06 0 -7 8 -5 20.62 23.37 0 -7 -8 -5 5.47 17.27 0 8 8 5 46.96 17.99 0 -8 8 -5 34.15 20.03 0 -8 -8 -5 70.68 17.01 0 -8 8 -5 51.03 21.94 0 9 8 5 19.26 17.59 0 -9 8 -5 22.78 19.33 0 -9 -8 -5 10.15 13.43 0 -9 8 -5 33.42 22.78 0 -10 8 -5 18.99 24.28 0 -10 -8 -5 13.69 19.90 0 -10 8 -5 19.55 22.83 0 10 8 5 -8.48 14.55 0 11 8 5 -1.11 20.24 0 -11 -8 -5 2.69 21.95 0 -11 8 -5 1.23 22.83 0 -11 8 -5 8.67 21.76 0 -12 -8 -5 -10.95 25.24 0 -12 8 -5 14.45 25.30 0 12 8 5 34.26 24.73 0 -12 8 -5 21.72 24.21 0 -13 8 -5 -4.39 25.05 0 -13 -8 -5 -2.77 19.22 0 -13 8 -5 12.61 26.07 0 13 8 5 0.04 20.08 0 -14 -8 -5 -9.80 26.93 0 -14 8 -5 -14.76 30.31 0 14 8 5 6.53 29.35 0 -14 8 -5 -12.10 30.49 0 -15 9 5 2.59 27.77 0 -15 -9 5 15.23 31.12 0 -15 9 5 -20.34 27.69 0 15 9 -5 -3.86 28.31 0 -14 9 5 -9.83 26.89 0 -14 9 5 -15.20 29.49 0 14 9 -5 0.66 25.90 0 -14 -9 5 -1.73 28.65 0 -13 9 5 -8.21 25.21 0 -13 9 5 8.57 27.43 0 -13 -9 5 25.62 25.69 0 13 9 -5 6.81 24.66 0 12 9 -5 3.44 16.81 0 -12 9 5 -11.82 23.02 0 -12 -9 5 -20.07 21.53 0 -12 9 5 -5.93 17.67 0 -11 9 5 9.18 22.48 0 -11 -9 5 -2.50 20.09 0 -11 9 5 3.19 16.00 0 11 9 -5 12.46 22.35 0 -10 9 5 -6.02 19.26 0 -10 9 5 2.69 14.91 0 -10 -9 5 6.64 14.38 0 10 9 -5 9.04 20.59 0 -9 9 5 17.83 18.87 0 -9 -9 5 7.53 19.21 0 9 9 -5 15.30 19.09 0 -8 -9 5 16.04 17.83 0 8 9 -5 43.56 18.96 0 -8 9 5 36.67 17.19 0 7 9 -5 -3.28 19.33 0 -7 -9 5 13.79 18.14 0 -7 9 5 -5.49 17.74 0 6 -9 -5 137.44 18.05 0 -6 9 5 126.73 13.18 0 -6 -9 5 172.68 18.32 0 6 9 -5 151.53 19.32 0 -5 9 5 71.85 12.77 0 -5 -9 5 78.07 12.54 0 5 -9 -5 80.67 12.89 0 5 9 -5 106.32 17.49 0 -4 9 5 0.28 17.18 0 4 9 -5 1.55 17.35 0 -4 -9 5 24.17 15.14 0 4 -9 -5 -4.41 17.19 0 3 9 -5 55.97 16.46 0 -3 9 5 48.48 17.62 0 3 -9 -5 43.86 17.20 0 -2 9 5 8.44 12.07 0 2 -9 -5 16.07 16.25 0 2 9 -5 29.74 16.96 0 1 9 -5 113.02 17.69 0 -1 9 5 102.97 16.97 0 1 -9 -5 79.59 16.80 0 0 9 -5 8.33 17.05 0 0 -9 -5 -5.26 16.05 0 0 9 5 6.85 15.31 0 0 -9 5 3.89 19.03 0 -1 9 -5 6.71 17.04 0 -1 -9 -5 14.83 15.72 0 1 -9 5 17.66 17.01 0 1 9 5 10.34 15.94 0 -2 -9 -5 -9.85 16.45 0 2 9 5 -6.19 17.23 0 -2 9 -5 0.63 18.92 0 2 -9 5 2.19 20.20 0 -3 9 -5 -4.02 19.52 0 -3 -9 -5 -3.08 16.96 0 3 9 5 10.88 17.07 0 -4 -9 -5 55.73 17.38 0 -4 9 -5 39.82 20.61 0 4 9 5 36.31 12.86 0 5 9 5 41.60 17.45 0 -5 9 -5 42.42 19.96 0 -5 9 -5 47.19 19.61 0 -5 -9 -5 28.26 17.36 0 -6 9 -5 9.60 21.26 0 6 9 5 7.52 17.20 0 -6 9 -5 4.82 18.64 0 -6 -9 -5 1.30 17.41 0 -7 9 -5 1.68 20.16 0 7 9 5 4.85 17.72 0 -7 9 -5 10.13 22.87 0 -7 -9 -5 8.72 17.54 0 8 9 5 9.12 13.41 0 -8 9 -5 -5.89 22.37 0 -8 9 -5 11.42 22.61 0 -8 -9 -5 -6.47 13.37 0 9 9 5 13.21 18.45 0 -9 9 -5 8.82 19.12 0 -9 9 -5 2.80 22.88 0 -9 -9 -5 19.97 17.82 0 10 9 5 10.45 20.45 0 -10 9 -5 9.42 25.33 0 -10 9 -5 32.09 22.59 0 -10 -9 -5 20.17 20.66 0 11 9 5 32.77 21.14 0 -11 9 -5 23.25 24.94 0 -11 -9 -5 0.04 23.67 0 -11 9 -5 23.00 26.71 0 -12 9 -5 3.12 26.26 0 -12 -9 -5 0.12 25.36 0 12 9 5 -0.26 18.34 0 -12 9 -5 -5.32 27.73 0 -13 9 -5 -10.10 28.80 0 13 9 5 2.08 28.32 0 -13 -9 -5 -9.17 20.57 0 -13 9 -5 -6.65 27.46 0 14 9 5 3.43 23.14 0 -14 9 -5 -3.51 31.73 0 -14 -9 -5 -1.53 32.09 0 -14 9 -5 2.13 29.24 0 -14 10 5 -4.61 27.31 0 14 10 -5 19.66 25.96 0 -14 -10 5 -11.55 29.68 0 -14 10 5 14.96 28.24 0 -13 10 5 30.62 21.89 0 -13 -10 5 -9.15 24.80 0 -13 10 5 37.16 26.73 0 13 10 -5 22.85 24.53 0 -12 10 5 23.99 19.05 0 -12 10 5 -16.50 26.89 0 -12 -10 5 13.33 24.56 0 12 10 -5 10.36 24.68 0 -11 10 5 9.46 23.90 0 -11 -10 5 18.58 22.33 0 -11 10 5 -2.23 24.26 0 11 10 -5 16.30 23.17 0 10 10 -5 -1.26 21.93 0 -10 -10 5 24.76 21.10 0 -10 10 5 10.25 21.13 0 -10 10 5 20.62 15.90 0 -9 -10 5 41.42 20.37 0 -9 10 5 40.78 14.58 0 9 10 -5 30.38 21.62 0 8 10 -5 186.52 20.34 0 -8 -10 5 179.43 19.20 0 -8 10 5 190.55 19.27 0 -7 10 5 -6.94 17.95 0 -7 -10 5 -4.68 17.67 0 7 10 -5 11.18 19.79 0 6 -10 -5 32.95 18.48 0 -6 10 5 19.75 17.13 0 -6 -10 5 24.92 17.73 0 6 10 -5 17.37 19.25 0 5 10 -5 16.79 17.67 0 -5 10 5 17.53 17.25 0 5 -10 -5 21.87 16.44 0 -5 -10 5 28.97 16.80 0 -4 10 5 -2.55 16.45 0 -4 -10 5 7.12 15.45 0 4 10 -5 2.16 17.05 0 4 -10 -5 -10.66 11.74 0 -3 10 5 18.65 16.80 0 3 10 -5 4.67 18.09 0 3 -10 -5 21.69 16.66 0 2 -10 -5 54.12 16.21 0 2 10 -5 85.97 20.00 0 -2 10 5 68.30 17.26 0 1 10 -5 41.60 19.53 0 -1 10 5 28.27 16.98 0 1 -10 -5 23.67 15.86 0 0 -10 -5 2.77 15.65 0 0 10 -5 3.00 17.31 0 0 10 5 -8.64 11.93 0 1 -10 5 16.72 19.90 0 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0 -12 10 -5 19.87 26.01 0 12 10 5 1.28 27.87 0 -13 10 -5 0.97 30.19 0 13 10 5 9.31 27.06 0 -13 -10 -5 -1.07 22.39 0 -13 10 -5 -7.69 29.13 0 -14 11 5 7.45 32.81 0 -14 -11 5 -12.97 27.95 0 14 11 -5 18.54 30.60 0 -14 11 5 -30.76 32.24 0 -13 11 5 0.52 21.82 0 -13 -11 5 -11.41 25.24 0 13 11 -5 -10.33 25.25 0 -13 11 5 5.26 30.76 0 -12 -11 5 0.66 26.10 0 -12 11 5 13.63 25.66 0 12 11 -5 6.96 19.79 0 -12 11 5 19.14 28.66 0 -11 11 5 -8.66 17.60 0 -11 11 5 -6.74 25.56 0 -11 -11 5 10.64 24.35 0 11 11 -5 4.05 18.16 0 10 11 -5 23.86 16.73 0 -10 11 5 16.20 21.10 0 -10 -11 5 -3.23 20.64 0 -10 11 5 6.19 22.44 0 9 11 -5 13.14 22.42 0 -9 -11 5 -5.06 19.75 0 -9 11 5 6.82 19.43 0 -8 -11 5 10.72 20.44 0 8 11 -5 12.27 21.42 0 -8 11 5 11.05 18.27 0 7 11 -5 25.24 20.96 0 -7 11 5 29.41 14.01 0 7 -11 -5 42.02 20.09 0 -7 -11 5 29.21 19.85 0 6 11 -5 60.99 20.41 0 6 -11 -5 67.24 14.34 0 -6 11 5 62.02 16.96 0 -6 -11 5 62.95 19.69 0 5 11 -5 30.42 19.82 0 -5 11 5 36.82 16.67 0 5 -11 -5 29.94 12.57 0 -5 -11 5 39.94 17.58 0 -4 -11 5 35.60 18.67 0 4 11 -5 45.10 19.49 0 -4 11 5 36.68 17.42 0 4 -11 -5 49.96 16.67 0 -3 11 5 6.65 12.45 0 3 11 -5 4.61 17.59 0 3 -11 -5 0.12 17.68 0 2 -11 -5 26.33 17.41 0 2 11 -5 13.62 17.89 0 -2 11 5 22.86 16.24 0 1 -11 -5 115.10 16.83 0 1 11 -5 135.10 17.89 0 -1 11 5 111.73 18.28 0 0 -11 -5 51.52 16.53 0 0 11 -5 55.45 18.20 0 0 11 5 42.71 17.63 0 -1 11 -5 39.77 18.06 0 -1 -11 -5 30.61 17.19 0 1 11 5 33.34 17.38 0 -2 11 -5 13.04 18.68 0 -2 -11 -5 8.49 16.20 0 2 -11 5 25.44 18.69 0 2 11 5 -2.66 16.22 0 -3 -11 -5 59.01 17.39 0 -3 11 -5 43.67 18.95 0 3 11 5 60.34 12.44 0 -4 11 -5 18.72 18.86 0 -4 -11 -5 21.01 16.21 0 4 11 5 10.26 16.50 0 -5 -11 -5 0.28 18.11 0 -5 11 -5 -6.57 19.51 0 5 11 5 2.45 18.27 0 -6 -11 -5 10.37 19.42 0 6 11 5 2.09 19.41 0 -6 11 -5 12.11 20.03 0 -6 11 -5 0.88 24.60 0 7 11 5 23.28 17.94 0 -7 11 -5 3.52 19.11 0 -7 11 -5 15.87 23.41 0 -7 -11 -5 30.91 19.16 0 8 11 5 23.74 14.99 0 -8 11 -5 22.37 21.66 0 -8 11 -5 17.59 24.48 0 -8 -11 -5 33.23 20.50 0 9 11 5 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19.81 0 -5 8 -10 13.39 36.25 0 -5 8 -10 14.62 34.00 0 -6 -8 -10 42.80 14.53 0 6 8 10 52.75 20.78 0 -6 8 -10 63.29 28.98 0 -6 8 -10 54.98 28.64 0 -7 -8 -10 4.19 21.15 0 7 8 10 -2.73 15.37 0 -7 8 -10 0.94 29.50 0 -7 8 -10 -0.38 27.20 0 8 8 10 -2.64 22.05 0 -8 8 -10 3.03 26.90 0 -8 -8 -10 10.08 15.86 0 -8 8 -10 0.91 29.24 0 9 8 10 23.59 21.94 0 -9 8 -10 10.09 30.31 0 -9 8 -10 0.58 28.65 0 -9 -8 -10 -7.32 21.36 0 -10 8 -10 -4.22 32.68 0 -10 8 -10 -4.34 30.96 0 -10 -8 -10 16.25 25.57 0 10 8 10 23.61 23.78 0 -11 8 -10 9.63 32.36 0 -11 8 -10 -1.91 28.78 0 -11 -8 -10 -5.33 25.02 0 11 8 10 2.09 25.26 0 -12 8 -10 2.06 32.42 0 -13 9 10 22.36 31.19 0 -13 -9 10 15.09 28.38 0 13 9 -10 4.53 26.86 0 -13 9 10 15.77 28.78 0 -12 -9 10 33.42 26.61 0 -12 9 10 55.13 26.21 0 12 9 -10 70.16 27.74 0 -12 9 10 78.12 21.12 0 -11 -9 10 0.13 26.21 0 -11 9 10 -7.37 19.01 0 11 9 -10 21.75 25.42 0 -11 9 10 14.52 25.98 0 -10 9 10 17.63 21.90 0 -10 -9 10 13.67 22.14 0 10 9 -10 3.41 26.19 0 -10 9 10 1.39 24.04 0 -9 9 10 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14.91 0 -1 -12 10 9.60 30.99 0 -1 12 10 30.90 20.48 0 1 12 -10 10.61 36.64 0 0 12 10 43.78 20.51 0 0 12 -10 49.09 43.77 0 0 -12 -10 75.45 19.64 0 1 12 10 1.93 19.48 0 -1 12 -10 18.89 56.39 0 -1 -12 -10 9.63 21.41 0 -1 12 -10 5.87 46.74 0 2 12 10 10.87 15.69 0 -2 -12 -10 -0.02 15.71 0 -3 12 -10 2.81 56.10 0 3 12 10 26.32 22.16 0 -3 -12 -10 -1.25 21.86 0 -4 12 -10 4.98 44.73 0 4 12 10 2.82 22.95 0 -4 -12 -10 19.97 23.58 0 -4 12 -10 8.37 52.08 0 5 12 10 12.61 21.87 0 -5 -12 -10 -2.89 17.71 0 -5 12 -10 2.89 39.68 0 -5 12 -10 1.79 39.81 0 6 12 10 -0.41 23.11 0 -6 -12 -10 6.11 25.58 0 -6 12 -10 6.60 33.77 0 -6 12 -10 3.12 42.64 0 -7 12 -10 4.78 41.67 0 7 12 10 5.44 19.31 0 -7 -12 -10 -0.49 18.87 0 -7 12 -10 6.17 33.75 0 -8 12 -10 16.32 44.80 0 8 12 10 6.30 20.08 0 -8 -12 -10 15.77 19.95 0 -8 12 -10 1.50 36.23 0 -10 13 10 -0.79 26.39 0 10 13 -10 8.26 33.27 0 -9 13 10 -16.68 25.31 0 9 13 -10 8.60 26.78 0 -8 13 10 8.82 26.56 0 8 13 -10 5.35 29.87 0 -8 -13 10 15.97 26.69 0 -7 -13 10 3.83 24.63 0 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27.78 0 -2 9 17 15.77 28.06 0 1 -9 -17 11.97 25.06 0 -1 9 17 16.51 27.26 0 0 9 17 -2.17 25.08 0 0 -9 -17 17.76 27.98 0 1 9 17 17.44 29.31 0 -1 -9 -17 -18.08 26.10 0 3 -10 -17 2.12 29.77 0 2 -10 -17 4.42 26.70 0 1 -10 -17 23.57 25.97 0 -10 0 18 22.73 30.58 0 -10 0 18 -12.32 35.89 0 -8 0 18 8.69 27.15 0 -8 0 18 -1.76 33.15 0 -6 0 18 24.55 28.18 0 -6 0 18 12.11 34.45 0 -4 0 18 1.71 28.76 0 -4 0 18 -2.55 33.99 0 -2 0 18 56.57 31.24 0 -2 0 18 64.54 39.64 0 0 0 18 8.58 36.86 0 0 0 18 7.29 46.55 0 2 0 18 5.84 45.74 0 -4 0 -18 5.30 41.31 0 4 0 18 2.85 45.25 0 -10 1 18 17.18 29.92 0 -10 -1 18 33.49 34.58 0 -10 -1 18 -2.13 35.27 0 -9 1 18 0.55 28.04 0 -9 -1 18 10.64 33.24 0 -9 -1 18 13.43 34.11 0 -8 1 18 5.37 27.47 0 -8 -1 18 2.83 29.89 0 -8 1 18 -5.48 32.08 0 -8 -1 18 -0.34 32.87 0 -7 1 18 3.96 26.91 0 -7 -1 18 4.86 28.83 0 -7 1 18 13.08 30.32 0 -7 -1 18 3.42 30.05 0 -6 -1 18 1.60 29.30 0 -6 1 18 10.76 28.65 0 -6 1 18 -2.56 31.59 0 -6 -1 18 6.72 38.09 0 -5 1 18 7.41 31.97 0 -5 -1 18 6.24 31.29 0 -5 -1 18 1.86 37.23 0 -5 1 18 12.72 27.52 0 -4 -1 18 5.17 31.75 0 -4 1 18 -1.32 33.50 0 -4 1 18 -0.00 26.92 0 -4 -1 18 -4.46 37.00 0 -3 -1 18 20.90 35.38 0 -3 1 18 10.61 27.67 0 -3 1 18 21.78 33.79 0 -3 -1 18 18.88 42.30 0 -2 1 18 4.39 30.34 0 -2 1 18 1.11 35.56 0 -1 1 18 7.56 31.11 0 -1 1 18 16.12 32.51 0 0 1 18 10.43 31.56 0 1 1 18 53.00 32.26 0 -2 -1 -18 7.95 34.77 0 2 1 18 11.81 34.54 0 -3 -1 -18 3.22 35.38 0 3 1 18 9.52 36.98 0 4 1 18 7.07 37.03 0 -4 -1 -18 6.56 36.15 0 -5 -1 -18 4.40 34.41 0 5 1 18 8.06 35.65 0 -10 2 18 -7.20 30.10 0 -10 -2 18 16.20 30.29 0 -10 2 18 9.39 29.79 0 -10 -2 18 6.36 33.67 0 -9 2 18 23.76 28.30 0 -9 -2 18 9.13 32.46 0 -9 -2 18 10.32 36.83 0 -8 2 18 14.09 26.88 0 -8 -2 18 19.39 30.82 0 -8 -2 18 8.92 35.21 0 -7 2 18 3.83 26.97 0 -7 -2 18 6.26 29.97 0 -7 2 18 6.70 32.14 0 -7 -2 18 0.23 35.16 0 -6 2 18 3.52 26.06 0 -6 2 18 12.68 35.04 0 -6 -2 18 -0.50 32.63 0 -6 -2 18 17.85 34.39 0 -5 -2 18 4.91 38.74 0 -5 2 18 0.79 29.35 0 -5 -2 18 1.07 30.66 0 -5 2 18 1.02 24.22 0 -4 -2 18 1.85 54.47 0 -4 -2 18 -0.40 50.24 0 -4 2 18 -0.54 29.97 0 -4 2 18 6.55 27.36 0 -3 2 18 4.35 30.97 0 -3 2 18 -12.32 27.84 0 -2 2 18 3.14 27.18 0 -1 2 18 44.46 27.91 0 0 2 18 100.11 28.78 0 1 2 18 24.47 29.73 0 -1 -2 -18 40.81 26.95 0 2 2 18 2.48 29.94 0 -2 -2 -18 15.05 30.02 0 -3 -2 -18 12.25 30.57 0 3 2 18 5.29 32.41 0 -4 -2 -18 4.65 31.89 0 4 2 18 7.69 33.32 0 -5 -2 -18 15.73 34.15 0 5 2 18 11.72 34.11 0 -9 -3 18 10.91 33.19 0 -9 3 18 13.31 25.10 0 -9 -3 18 4.30 31.30 0 -9 3 18 -7.39 29.64 0 -8 -3 18 9.29 34.80 0 -8 3 18 -5.58 26.93 0 -8 -3 18 7.04 30.93 0 -8 3 18 -5.19 33.74 0 -7 -3 18 5.74 37.17 0 -7 3 18 17.43 26.64 0 -7 -3 18 4.36 33.84 0 -6 3 18 21.07 25.45 0 -6 -3 18 2.46 39.53 0 -6 -3 18 7.04 34.07 0 -5 3 18 0.64 28.80 0 -5 3 18 -7.38 28.82 0 -4 3 18 8.70 28.92 0 -4 3 18 19.50 25.79 0 -3 3 18 -0.77 27.96 0 -2 3 18 10.68 24.69 0 -1 3 18 24.41 25.27 0 1 -3 -18 36.55 26.49 0 0 3 18 4.42 28.79 0 0 -3 -18 14.73 25.84 0 1 3 18 9.58 29.32 0 -1 -3 -18 8.12 28.01 0 -2 -3 -18 -2.21 30.04 0 2 3 18 6.59 29.61 0 3 3 18 6.82 31.39 0 -3 -3 -18 6.20 29.95 0 -4 -3 -18 43.97 30.23 0 4 3 18 33.87 33.73 0 -5 -3 -18 10.89 33.46 0 5 3 18 11.29 32.63 0 -9 -4 18 8.17 36.45 0 -9 4 18 6.61 28.28 0 -9 -4 18 -2.88 33.71 0 -9 4 18 7.33 33.19 0 -8 4 18 15.78 24.83 0 -8 -4 18 3.94 38.53 0 -8 -4 18 2.96 36.08 0 -8 4 18 4.94 31.70 0 -7 4 18 1.88 28.30 0 -7 -4 18 6.03 38.17 0 -7 -4 18 0.49 39.64 0 -7 4 18 14.67 27.39 0 -6 4 18 -9.43 27.28 0 -6 4 18 12.75 25.68 0 -5 4 18 9.22 25.02 0 -4 4 18 2.19 25.07 0 -3 4 18 0.37 25.65 0 -2 4 18 13.41 28.99 0 -1 4 18 0.32 28.93 0 1 -4 -18 3.72 26.26 0 0 4 18 12.00 26.17 0 0 -4 -18 21.61 26.38 0 -1 -4 -18 4.74 30.93 0 1 4 18 0.40 27.71 0 2 4 18 10.02 27.98 0 -2 -4 -18 -10.35 28.53 0 3 4 18 2.62 30.47 0 -3 -4 -18 2.78 30.13 0 4 4 18 -14.85 29.77 0 -4 -4 -18 9.03 33.21 0 -8 5 18 -9.16 27.88 0 -8 -5 18 9.10 39.28 0 -8 -5 18 12.47 43.34 0 -8 5 18 -10.73 28.89 0 -7 5 18 -3.15 24.49 0 -7 5 18 7.89 29.79 0 -6 5 18 21.10 26.84 0 -6 5 18 30.64 26.68 0 -5 5 18 33.69 23.37 0 -4 5 18 -2.66 25.39 0 -3 5 18 8.54 25.13 0 2 -5 -18 11.20 28.27 0 -2 5 18 26.33 22.83 0 -1 5 18 -7.81 25.09 0 1 -5 -18 11.08 23.79 0 0 -5 -18 2.13 26.16 0 0 5 18 13.15 26.42 0 1 5 18 6.10 28.85 0 -1 -5 -18 -3.99 27.11 0 2 5 18 15.90 28.48 0 -2 -5 -18 25.52 28.06 0 3 5 18 16.76 29.43 0 -3 -5 -18 -10.80 28.70 0 4 5 18 7.19 31.72 0 -4 -5 -18 3.03 31.16 0 -8 6 18 6.47 26.50 0 -7 6 18 21.91 27.38 0 -7 6 18 21.94 32.35 0 -6 6 18 12.32 27.58 0 -5 6 18 4.58 26.96 0 -4 6 18 16.35 27.79 0 3 -6 -18 -4.30 27.54 0 -3 6 18 21.05 26.54 0 2 -6 -18 2.55 27.41 0 -2 6 18 26.48 26.21 0 -1 6 18 21.97 25.58 0 1 -6 -18 7.64 23.99 0 0 -6 -18 14.86 24.69 0 0 6 18 21.05 28.28 0 1 6 18 0.71 25.31 0 -1 -6 -18 4.09 25.07 0 2 6 18 16.55 28.27 0 -2 -6 -18 5.00 25.49 0 3 6 18 -4.32 30.17 0 -3 -6 -18 15.58 29.07 0 -6 7 18 5.89 29.14 0 -5 7 18 9.38 27.20 0 -4 7 18 12.62 27.55 0 -3 7 18 6.37 24.51 0 3 -7 -18 2.20 28.82 0 2 -7 -18 6.72 25.53 0 -2 7 18 19.83 26.88 0 1 -7 -18 23.76 27.67 0 -1 7 18 12.35 24.23 0 0 -7 -18 8.26 27.16 0 0 7 18 -2.33 29.03 0 1 7 18 -6.88 25.05 0 -1 -7 -18 11.32 25.59 0 2 7 18 23.27 28.89 0 -2 -7 -18 10.54 29.57 0 4 -8 -18 7.61 26.64 0 -4 8 18 5.91 26.56 0 -3 8 18 7.81 28.94 0 3 -8 -18 11.97 29.78 0 -2 8 18 15.97 27.78 0 2 -8 -18 10.64 25.42 0 1 -8 -18 6.60 25.23 0 -1 8 18 3.53 25.00 0 0 8 18 20.44 28.28 0 0 -8 -18 19.81 28.31 0 -7 0 19 16.83 32.63 0 -7 0 19 5.13 38.88 0 -5 0 19 2.35 30.81 0 -5 0 19 3.15 35.67 0 -3 0 19 0.70 32.68 0 -3 0 19 2.53 43.40 0 -1 0 19 34.24 44.52 0 -1 0 19 27.57 49.07 0 -8 1 19 7.06 29.95 0 -8 -1 19 12.19 34.53 0 -8 1 19 10.01 35.01 0 -8 -1 19 4.17 35.16 0 -7 1 19 1.39 28.61 0 -7 -1 19 -2.20 35.80 0 -7 1 19 -3.68 37.18 0 -7 -1 19 5.41 37.77 0 -6 1 19 0.72 36.14 0 -6 -1 19 2.89 31.35 0 -6 1 19 -0.90 31.51 0 -6 -1 19 9.40 36.67 0 -5 -1 19 3.35 33.98 0 -5 1 19 6.55 36.84 0 -5 1 19 -8.20 26.38 0 -5 -1 19 3.73 38.91 0 -4 -1 19 5.36 41.75 0 -4 1 19 2.72 33.62 0 -4 1 19 -9.70 37.80 0 -4 -1 19 11.33 43.38 0 -3 1 19 16.68 30.61 0 -3 1 19 13.59 38.33 0 -2 1 19 0.97 33.41 0 -2 1 19 8.55 40.53 0 -1 1 19 9.75 37.62 0 -1 1 19 -2.48 39.65 0 0 1 19 0.67 34.53 0 0 1 19 8.16 40.95 0 1 1 19 13.56 41.54 0 2 1 19 -3.34 41.76 0 -3 -1 -19 0.82 45.69 0 3 1 19 5.95 43.61 0 -8 -2 19 10.97 39.00 0 -8 2 19 23.36 31.14 0 -8 -2 19 14.60 34.17 0 -8 2 19 7.66 34.44 0 -7 -2 19 13.17 40.67 0 -7 2 19 4.77 33.36 0 -7 2 19 1.83 34.84 0 -7 -2 19 21.90 36.32 0 -6 -2 19 -5.77 40.63 0 -6 2 19 9.01 34.78 0 -6 -2 19 -4.56 39.57 0 -6 2 19 8.19 32.14 0 -5 -2 19 4.74 54.81 0 -5 -2 19 1.13 49.67 0 -5 2 19 5.87 32.38 0 -5 2 19 7.90 30.69 0 -4 2 19 -0.93 35.99 0 -4 2 19 10.31 25.90 0 -3 2 19 2.40 29.53 0 -3 2 19 -5.04 34.90 0 -2 2 19 3.01 31.50 0 -2 2 19 9.21 34.56 0 -1 2 19 0.59 30.92 0 0 2 19 -6.52 31.62 0 1 2 19 -4.69 31.97 0 2 2 19 -0.01 36.90 0 -2 -2 -19 8.27 33.85 0 -3 -2 -19 15.93 35.48 0 3 2 19 13.98 35.80 0 -7 3 19 -0.65 29.59 0 -7 -3 19 -3.61 43.59 0 -7 -3 19 9.51 41.40 0 -6 3 19 7.19 33.73 0 -6 3 19 11.11 31.50 0 -5 3 19 11.47 32.96 0 -5 3 19 34.91 27.80 0 -4 3 19 -10.67 35.04 0 -4 3 19 14.19 27.44 0 -3 3 19 0.17 26.24 0 -2 3 19 1.15 27.83 0 -1 3 19 -1.23 27.59 0 0 3 19 3.41 32.04 0 0 -3 -19 -5.09 36.19 0 1 3 19 23.48 34.24 0 -1 -3 -19 30.32 30.33 0 2 3 19 -0.27 31.68 0 -2 -3 -19 10.07 32.19 0 -3 -3 -19 -1.22 34.81 0 -7 4 19 4.04 31.24 0 -6 4 19 16.87 29.09 0 -5 4 19 -9.58 27.56 0 -4 4 19 -5.76 28.16 0 -3 4 19 16.87 31.41 0 -2 4 19 13.44 29.18 0 -1 4 19 15.10 29.77 0 1 -4 -19 2.29 33.80 0 0 4 19 9.99 30.40 0 0 -4 -19 15.05 31.28 0 1 4 19 19.35 30.45 0 -1 -4 -19 -1.56 33.69 0 2 4 19 7.37 34.00 0 -2 -4 -19 4.26 30.14 0 -6 5 19 12.61 29.27 0 -5 5 19 12.65 28.72 0 -4 5 19 15.30 29.11 0 -3 5 19 32.61 28.29 0 -2 5 19 22.15 28.23 0 1 -5 -19 7.17 30.61 0 -1 5 19 6.35 32.92 0 0 5 19 18.55 29.50 0 0 -5 -19 -9.31 31.27 0 1 5 19 -9.41 31.48 0 -1 -5 -19 3.18 30.72 0 -4 6 19 23.35 29.43 0 -3 6 19 7.16 30.36 0 2 -6 -19 6.66 30.65 0 -2 6 19 1.69 26.66 0 1 -6 -19 19.11 29.97 0 -1 6 19 31.11 30.91 0 0 -6 -19 -0.56 31.68 0 -4 0 20 5.63 42.42 0 -4 0 20 -0.57 46.57 0 -5 -1 20 2.39 44.63 0 -5 1 20 11.72 33.59 0 -4 1 20 10.93 33.75 0 -4 1 20 13.32 42.95 0 -3 1 20 4.04 33.62 0 -3 1 20 -2.07 44.15 0 -2 1 20 -2.61 43.42 0 -2 1 20 5.98 46.02 0 -1 1 20 5.26 39.03 0 -1 1 20 -0.29 51.42 0 -4 2 20 -0.38 34.10 0 -4 2 20 6.20 41.97 0 -3 2 20 5.13 33.49 0 -3 2 20 4.83 40.26 0 -2 2 20 -0.04 37.85 0 -2 2 20 7.15 39.34 0 -1 2 20 17.00 34.45 0 ; _shelx_hkl_checksum 23943 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy Si Si 0.57085(13) -0.46010(9) -0.00743(9) 0.0580(4) Uani 1 1 d . . . H H 0.5740 -0.4319 0.0411 0.070 Uiso 0.5 1 d R U P N1 N 0.3545(3) -0.3664(2) -0.17949(19) 0.0341(7) Uani 1 1 d . . . N2 N 0.5426(3) -0.32915(19) -0.14132(19) 0.0333(7) Uani 1 1 d . . . C1 C 0.4826(3) -0.3835(2) -0.1109(2) 0.0308(8) Uani 1 1 d . . . C2 C 0.3379(4) -0.3065(2) -0.2465(3) 0.0400(9) Uani 1 1 d . . . H2 H 0.2581 -0.2854 -0.2999 0.048 Uiso 1 1 calc R U . C3 C 0.4543(3) -0.2832(2) -0.2231(2) 0.0382(9) Uani 1 1 d . . . H3 H 0.4725 -0.2426 -0.2566 0.046 Uiso 1 1 calc R U . C4 C 0.2485(3) -0.3967(3) -0.1768(2) 0.0368(8) Uani 1 1 d . . . C5 C 0.1809(3) -0.4807(3) -0.2268(2) 0.0434(9) Uani 1 1 d . . . C6 C 0.0756(4) -0.5056(4) -0.2249(3) 0.0639(13) Uani 1 1 d . . . H6 H 0.0240 -0.5612 -0.2584 0.077 Uiso 1 1 calc R U . C7 C 0.0481(4) -0.4517(4) -0.1763(3) 0.0690(13) Uani 1 1 d . . . H7 H -0.0216 -0.4711 -0.1755 0.083 Uiso 1 1 calc R U . C8 C 0.1176(4) -0.3701(3) -0.1284(3) 0.0564(11) Uani 1 1 d . . . H8 H 0.0943 -0.3326 -0.0962 0.068 Uiso 1 1 calc R U . C9 C 0.2229(3) -0.3413(3) -0.1263(2) 0.0388(9) Uani 1 1 d . . . C10 C 0.2081(4) -0.5393(3) -0.2831(3) 0.0471(9) Uani 1 1 d . . . H10 H 0.2897 -0.5130 -0.2697 0.057 Uiso 1 1 calc R U . C11 C 0.1047(4) -0.5241(4) -0.3842(3) 0.0645(12) Uani 1 1 d . . . H11A H 0.0219 -0.5460 -0.3995 0.097 Uiso 1 1 calc R U . H11B H 0.1256 -0.5627 -0.4192 0.097 Uiso 1 1 calc R U . H11C H 0.0998 -0.4539 -0.3991 0.097 Uiso 1 1 calc R U . C12 C 0.2291(6) -0.6484(3) -0.2594(4) 0.0774(15) Uani 1 1 d . . . H12A H 0.2991 -0.6565 -0.1944 0.116 Uiso 1 1 calc R U . H12B H 0.2515 -0.6820 -0.2958 0.116 Uiso 1 1 calc R U . H12C H 0.1504 -0.6773 -0.2726 0.116 Uiso 1 1 calc R U . C13 C 0.3007(4) -0.2503(3) -0.0724(3) 0.0481(10) Uani 1 1 d . . . H13 H 0.3855 -0.2564 -0.0619 0.058 Uiso 1 1 calc R U . C14 C 0.3280(5) -0.2423(3) 0.0199(3) 0.0640(12) Uani 1 1 d . . . H14A H 0.2473 -0.2337 0.0126 0.096 Uiso 1 1 calc R U . H14B H 0.3839 -0.1854 0.0525 0.096 Uiso 1 1 calc R U . H14C H 0.3707 -0.3027 0.0548 0.096 Uiso 1 1 calc R U . C15 C 0.2380(6) -0.1561(3) -0.1279(4) 0.0882(17) Uani 1 1 d . . . H15A H 0.2203 -0.1634 -0.1879 0.132 Uiso 1 1 calc R U . H15B H 0.2960 -0.1000 -0.0958 0.132 Uiso 1 1 calc R U . H15C H 0.1575 -0.1443 -0.1355 0.132 Uiso 1 1 calc R U . C16 C 0.6794(3) -0.3129(2) -0.0869(2) 0.0312(8) Uani 1 1 d . . . C17 C 0.7534(3) -0.3795(2) -0.0958(2) 0.0364(8) Uani 1 1 d . . . C18 C 0.8849(3) -0.3625(3) -0.0425(3) 0.0446(9) Uani 1 1 d . . . H18 H 0.9388 -0.4062 -0.0464 0.053 Uiso 1 1 calc R U . C19 C 0.9378(4) -0.2831(3) 0.0157(3) 0.0522(11) Uani 1 1 d . . . H19 H 1.0277 -0.2726 0.0511 0.063 Uiso 1 1 calc R U . C20 C 0.8630(4) -0.2183(3) 0.0240(3) 0.0474(10) Uani 1 1 d . . . H20 H 0.9019 -0.1649 0.0659 0.057 Uiso 1 1 calc R U . C21 C 0.7285(4) -0.2313(2) -0.0299(3) 0.0392(9) Uani 1 1 d . . . C22 C 0.6940(3) -0.4646(3) -0.1618(2) 0.0388(8) Uani 1 1 d . . . H22 H 0.6091 -0.4786 -0.1742 0.047 Uiso 1 1 calc R U . C23 C 0.7746(4) -0.5598(3) -0.1227(3) 0.0519(11) Uani 1 1 d . . . H23A H 0.8539 -0.5516 -0.1174 0.078 Uiso 1 1 calc R U . H23B H 0.7255 -0.6153 -0.1636 0.078 Uiso 1 1 calc R U . H23C H 0.7957 -0.5732 -0.0623 0.078 Uiso 1 1 calc R U . C24 C 0.6690(4) -0.4380(3) -0.2512(3) 0.0575(11) Uani 1 1 d . . . H24A H 0.6125 -0.3802 -0.2772 0.086 Uiso 1 1 calc R U . H24B H 0.6277 -0.4938 -0.2935 0.086 Uiso 1 1 calc R U . H24C H 0.7504 -0.4227 -0.2412 0.086 Uiso 1 1 calc R U . C25 C 0.6476(4) -0.1577(3) -0.0224(3) 0.0473(10) Uani 1 1 d . . . H25 H 0.5571 -0.1818 -0.0633 0.057 Uiso 1 1 calc R U . C26 C 0.6805(6) -0.1497(4) 0.0710(4) 0.0809(16) Uani 1 1 d . . . H26A H 0.6793 -0.2155 0.0928 0.121 Uiso 1 1 calc R U . H26B H 0.6175 -0.1074 0.0690 0.121 Uiso 1 1 calc R U . H26C H 0.7662 -0.1208 0.1124 0.121 Uiso 1 1 calc R U . C27 C 0.6503(5) -0.0568(3) -0.0593(3) 0.0640(12) Uani 1 1 d . . . H27A H 0.7373 -0.0295 -0.0202 0.096 Uiso 1 1 calc R U . H27B H 0.5908 -0.0118 -0.0596 0.096 Uiso 1 1 calc R U . H27C H 0.6246 -0.0644 -0.1215 0.096 Uiso 1 1 calc R U . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si 0.0765(9) 0.0487(7) 0.0549(8) 0.0184(6) 0.0424(7) 0.0119(6) N1 0.0293(16) 0.0352(15) 0.0362(17) 0.0050(13) 0.0186(14) -0.0015(12) N2 0.0333(17) 0.0332(15) 0.0359(17) 0.0041(13) 0.0219(15) 0.0026(13) C1 0.033(2) 0.0260(16) 0.036(2) -0.0065(15) 0.0222(18) -0.0030(14) C2 0.031(2) 0.041(2) 0.040(2) 0.0078(18) 0.0168(18) 0.0076(16) C3 0.041(2) 0.0360(18) 0.042(2) 0.0070(17) 0.027(2) 0.0059(16) C4 0.0236(18) 0.047(2) 0.033(2) 0.0030(17) 0.0135(17) 0.0010(16) C5 0.0269(19) 0.053(2) 0.036(2) -0.0017(18) 0.0113(18) -0.0060(17) C6 0.038(2) 0.097(3) 0.051(3) -0.022(3) 0.023(2) -0.032(2) C7 0.033(2) 0.120(4) 0.057(3) -0.015(3) 0.028(2) -0.018(3) C8 0.035(2) 0.084(3) 0.051(3) -0.006(2) 0.026(2) 0.004(2) C9 0.0275(19) 0.045(2) 0.038(2) 0.0066(17) 0.0166(18) 0.0085(16) C10 0.039(2) 0.051(2) 0.045(2) -0.005(2) 0.021(2) -0.0067(18) C11 0.052(3) 0.078(3) 0.051(3) -0.007(2) 0.024(2) 0.009(2) C12 0.108(4) 0.052(3) 0.072(3) -0.007(2) 0.053(3) -0.008(3) C13 0.053(3) 0.041(2) 0.058(3) 0.0007(19) 0.037(2) 0.0087(18) C14 0.075(3) 0.053(2) 0.070(3) -0.009(2) 0.046(3) -0.005(2) C15 0.121(5) 0.056(3) 0.080(4) 0.011(3) 0.056(4) 0.014(3) C16 0.0335(19) 0.0289(17) 0.035(2) 0.0037(15) 0.0225(17) -0.0019(14) C17 0.039(2) 0.0325(18) 0.045(2) -0.0007(16) 0.0290(19) -0.0012(16) C18 0.032(2) 0.039(2) 0.064(3) 0.0000(19) 0.028(2) 0.0023(16) C19 0.036(2) 0.047(2) 0.069(3) -0.007(2) 0.028(2) -0.0084(18) C20 0.043(2) 0.036(2) 0.054(3) -0.0081(18) 0.024(2) -0.0073(17) C21 0.044(2) 0.0351(19) 0.045(2) 0.0001(17) 0.031(2) -0.0022(16) C22 0.0314(19) 0.0401(19) 0.050(2) -0.0037(18) 0.0266(19) -0.0026(16) C23 0.051(3) 0.038(2) 0.068(3) -0.0049(19) 0.036(2) -0.0034(18) C24 0.053(3) 0.064(3) 0.056(3) -0.007(2) 0.033(2) 0.003(2) C25 0.047(2) 0.040(2) 0.067(3) -0.0178(19) 0.041(2) -0.0107(17) C26 0.111(5) 0.070(3) 0.093(4) 0.009(3) 0.078(4) 0.022(3) C27 0.073(3) 0.050(2) 0.086(3) 0.003(2) 0.056(3) 0.013(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 Si Si 109.55(13) . 3_645 C1 Si H 112.9 . . Si Si H 70.7 3_645 . C2 N1 C1 111.9(3) . . C2 N1 C4 122.8(3) . . C1 N1 C4 124.8(3) . . C3 N2 C1 111.4(3) . . C3 N2 C16 124.6(3) . . C1 N2 C16 123.5(3) . . N1 C1 N2 101.8(3) . . N1 C1 Si 134.8(2) . . N2 C1 Si 123.3(2) . . C3 C2 N1 107.7(3) . . C3 C2 H2 126.1 . . N1 C2 H2 126.1 . . C2 C3 N2 107.1(3) . . C2 C3 H3 126.5 . . N2 C3 H3 126.5 . . C9 C4 C5 125.2(3) . . C9 C4 N1 118.4(3) . . C5 C4 N1 116.4(3) . . C4 C5 C6 114.6(4) . . C4 C5 C10 124.6(3) . . C6 C5 C10 120.7(3) . . C7 C6 C5 121.2(4) . . C7 C6 H6 119.4 . . C5 C6 H6 119.4 . . C6 C7 C8 121.8(4) . . C6 C7 H7 119.1 . . C8 C7 H7 119.1 . . C7 C8 C9 120.4(4) . . C7 C8 H8 119.8 . . C9 C8 H8 119.8 . . C4 C9 C8 116.7(3) . . C4 C9 C13 122.9(3) . . C8 C9 C13 120.3(3) . . C5 C10 C11 111.3(3) . . C5 C10 C12 113.4(3) . . C11 C10 C12 110.9(4) . . C5 C10 H10 106.9 . . C11 C10 H10 106.9 . . C12 C10 H10 106.9 . . C10 C11 H11A 109.5 . . C10 C11 H11B 109.5 . . H11A C11 H11B 109.5 . . C10 C11 H11C 109.5 . . H11A C11 H11C 109.5 . . H11B C11 H11C 109.5 . . C10 C12 H12A 109.5 . . C10 C12 H12B 109.5 . . H12A C12 H12B 109.5 . . C10 C12 H12C 109.5 . . H12A C12 H12C 109.5 . . H12B C12 H12C 109.5 . . C14 C13 C9 113.9(3) . . C14 C13 C15 111.1(4) . . C9 C13 C15 111.1(4) . . C14 C13 H13 106.8 . . C9 C13 H13 106.8 . . C15 C13 H13 106.8 . . C13 C14 H14A 109.5 . . C13 C14 H14B 109.5 . . H14A C14 H14B 109.5 . . C13 C14 H14C 109.5 . . H14A C14 H14C 109.5 . . H14B C14 H14C 109.5 . . C13 C15 H15A 109.5 . . C13 C15 H15B 109.5 . . H15A C15 H15B 109.5 . . C13 C15 H15C 109.5 . . H15A C15 H15C 109.5 . . H15B C15 H15C 109.5 . . C21 C16 C17 124.2(3) . . C21 C16 N2 117.8(3) . . C17 C16 N2 118.1(3) . . C18 C17 C16 117.0(3) . . C18 C17 C22 121.2(3) . . C16 C17 C22 121.8(3) . . C19 C18 C17 120.7(3) . . C19 C18 H18 119.6 . . C17 C18 H18 119.6 . . C18 C19 C20 121.4(4) . . C18 C19 H19 119.3 . . C20 C19 H19 119.3 . . C19 C20 C21 120.0(4) . . C19 C20 H20 120.0 . . C21 C20 H20 120.0 . . C16 C21 C20 116.6(3) . . C16 C21 C25 124.0(3) . . C20 C21 C25 119.4(3) . . C24 C22 C17 111.1(3) . . C24 C22 C23 110.6(3) . . C17 C22 C23 112.7(3) . . C24 C22 H22 107.4 . . C17 C22 H22 107.4 . . C23 C22 H22 107.4 . . C22 C23 H23A 109.5 . . C22 C23 H23B 109.5 . . H23A C23 H23B 109.5 . . C22 C23 H23C 109.5 . . H23A C23 H23C 109.5 . . H23B C23 H23C 109.5 . . C22 C24 H24A 109.5 . . C22 C24 H24B 109.5 . . H24A C24 H24B 109.5 . . C22 C24 H24C 109.5 . . H24A C24 H24C 109.5 . . H24B C24 H24C 109.5 . . C26 C25 C21 114.0(4) . . C26 C25 C27 111.7(3) . . C21 C25 C27 110.6(3) . . C26 C25 H25 106.7 . . C21 C25 H25 106.7 . . C27 C25 H25 106.7 . . C25 C26 H26A 109.5 . . C25 C26 H26B 109.5 . . H26A C26 H26B 109.5 . . C25 C26 H26C 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . C25 C27 H27A 109.5 . . C25 C27 H27B 109.5 . . H27A C27 H27B 109.5 . . C25 C27 H27C 109.5 . . H27A C27 H27C 109.5 . . H27B C27 H27C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si C1 1.837(4) . Si Si 2.281(3) 3_645 Si H 0.9420 . N1 C2 1.372(4) . N1 C1 1.381(4) . N1 C4 1.463(4) . N2 C3 1.376(4) . N2 C1 1.402(4) . N2 C16 1.444(4) . C2 C3 1.339(5) . C2 H2 0.9500 . C3 H3 0.9500 . C4 C9 1.371(5) . C4 C5 1.394(5) . C5 C6 1.425(5) . C5 C10 1.495(5) . C6 C7 1.348(6) . C6 H6 0.9500 . C7 C8 1.364(6) . C7 H7 0.9500 . C8 C9 1.397(5) . C8 H8 0.9500 . C9 C13 1.524(5) . C10 C11 1.516(6) . C10 C12 1.518(6) . C10 H10 1.0000 . C11 H11A 0.9800 . C11 H11B 0.9800 . C11 H11C 0.9800 . C12 H12A 0.9800 . C12 H12B 0.9800 . C12 H12C 0.9800 . C13 C14 1.504(5) . C13 C15 1.527(6) . C13 H13 1.0000 . C14 H14A 0.9800 . C14 H14B 0.9800 . C14 H14C 0.9800 . C15 H15A 0.9800 . C15 H15B 0.9800 . C15 H15C 0.9800 . C16 C21 1.385(5) . C16 C17 1.394(5) . C17 C18 1.391(5) . C17 C22 1.505(5) . C18 C19 1.373(5) . C18 H18 0.9500 . C19 C20 1.380(5) . C19 H19 0.9500 . C20 C21 1.415(5) . C20 H20 0.9500 . C21 C25 1.510(5) . C22 C24 1.505(5) . C22 C23 1.542(5) . C22 H22 1.0000 . C23 H23A 0.9800 . C23 H23B 0.9800 . C23 H23C 0.9800 . C24 H24A 0.9800 . C24 H24B 0.9800 . C24 H24C 0.9800 . C25 C26 1.493(6) . C25 C27 1.532(5) . C25 H25 1.0000 . C26 H26A 0.9800 . C26 H26B 0.9800 . C26 H26C 0.9800 . C27 H27A 0.9800 . C27 H27B 0.9800 . C27 H27C 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 C2 N1 C1 N2 0.1(3) . C4 N1 C1 N2 -172.3(3) . C2 N1 C1 Si -175.7(3) . C4 N1 C1 Si 11.9(5) . C3 N2 C1 N1 -0.1(3) . C16 N2 C1 N1 171.9(3) . C3 N2 C1 Si 176.3(2) . C16 N2 C1 Si -11.7(4) . Si Si C1 N1 -1.6(4) 3_645 Si Si C1 N2 -176.7(2) 3_645 C1 N1 C2 C3 -0.1(4) . C4 N1 C2 C3 172.5(3) . N1 C2 C3 N2 0.0(4) . C1 N2 C3 C2 0.0(4) . C16 N2 C3 C2 -171.8(3) . C2 N1 C4 C9 -93.3(4) . C1 N1 C4 C9 78.3(4) . C2 N1 C4 C5 86.4(4) . C1 N1 C4 C5 -101.9(4) . C9 C4 C5 C6 1.9(6) . N1 C4 C5 C6 -177.9(3) . C9 C4 C5 C10 178.7(4) . N1 C4 C5 C10 -1.1(5) . C4 C5 C6 C7 -1.3(6) . C10 C5 C6 C7 -178.2(4) . C5 C6 C7 C8 1.3(7) . C6 C7 C8 C9 -1.8(7) . C5 C4 C9 C8 -2.4(5) . N1 C4 C9 C8 177.4(3) . C5 C4 C9 C13 179.7(3) . N1 C4 C9 C13 -0.6(5) . C7 C8 C9 C4 2.2(6) . C7 C8 C9 C13 -179.8(4) . C4 C5 C10 C11 -108.0(4) . C6 C5 C10 C11 68.7(5) . C4 C5 C10 C12 126.1(4) . C6 C5 C10 C12 -57.3(5) . C4 C9 C13 C14 -139.0(4) . C8 C9 C13 C14 43.1(5) . C4 C9 C13 C15 94.6(4) . C8 C9 C13 C15 -83.3(5) . C3 N2 C16 C21 82.4(4) . C1 N2 C16 C21 -88.5(4) . C3 N2 C16 C17 -96.8(4) . C1 N2 C16 C17 92.2(4) . C21 C16 C17 C18 1.0(5) . N2 C16 C17 C18 -179.8(3) . C21 C16 C17 C22 -177.5(3) . N2 C16 C17 C22 1.7(5) . C16 C17 C18 C19 -0.2(5) . C22 C17 C18 C19 178.3(3) . C17 C18 C19 C20 0.5(6) . C18 C19 C20 C21 -1.7(6) . C17 C16 C21 C20 -2.1(5) . N2 C16 C21 C20 178.7(3) . C17 C16 C21 C25 178.2(3) . N2 C16 C21 C25 -1.0(5) . C19 C20 C21 C16 2.3(5) . C19 C20 C21 C25 -177.9(4) . C18 C17 C22 C24 -84.0(4) . C16 C17 C22 C24 94.4(4) . C18 C17 C22 C23 40.8(5) . C16 C17 C22 C23 -140.8(3) . C16 C21 C25 C26 120.0(4) . C20 C21 C25 C26 -59.8(5) . C16 C21 C25 C27 -113.2(4) . C20 C21 C25 C27 67.0(5) .