#------------------------------------------------------------------------------ #$Date: 2016-05-11 06:37:04 +0300 (Wed, 11 May 2016) $ #$Revision: 182865 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/32/1543280.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1543280 loop_ _publ_author_name 'Elaatiaoui, Abdelmalik' 'Elkalai, Fouad' 'Benchat, Noureddine' 'Saadi, Mohamed' 'El Ammari, Lahcen' _publ_section_title ; (E)-2-Phenyl-N-(thiophen-2-ylmethylidene)imidazo[1,2-a]pyridin-3-amine ; _journal_coeditor_code BT4007 _journal_issue 5 _journal_name_full IUCrData _journal_page_first x160723 _journal_paper_doi 10.1107/S2414314616007239 _journal_volume 1 _journal_year 2016 _chemical_formula_iupac 'C18 H13 N3 S' _chemical_formula_moiety 'C18 H13 N3 S' _chemical_formula_sum 'C18 H13 N3 S' _chemical_formula_weight 303.37 _chemical_name_systematic (E)-2-Phenyl-N-(thiophen-2-ylmethylidene)imidazo[1,2-a]pyridin-3-amine _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 101.299(8) _cell_angle_beta 106.315(9) _cell_angle_gamma 95.628(8) _cell_formula_units_Z 4 _cell_length_a 9.6524(17) _cell_length_b 10.1168(17) _cell_length_c 16.655(3) _cell_measurement_reflns_used 8471 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 29.575 _cell_measurement_theta_min 2.081 _cell_volume 1510.2(5) _computing_cell_refinement ; SAINT (Bruker, 2009) ; _computing_data_collection ; APEX2 (Bruker, 2009) ; _computing_data_reduction ; SAINT (Bruker, 2009) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2009) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS2014 (Sheldrick, 2008) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker X8 APEX' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0424 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 66495 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.575 _diffrn_reflns_theta_min 2.081 _exptl_absorpt_coefficient_mu 0.213 _exptl_absorpt_correction_T_max 0.7462 _exptl_absorpt_correction_T_min 0.6410 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2009) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.332 _exptl_crystal_description parallelepiped _exptl_crystal_F_000 632 _exptl_crystal_size_max 0.44 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.292 _refine_diff_density_min -0.476 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 397 _refine_ls_number_reflns 8471 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.023 _refine_ls_R_factor_all 0.0742 _refine_ls_R_factor_gt 0.0436 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0559P)^2^+0.3505P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1068 _refine_ls_wR_factor_ref 0.1247 _reflns_number_gt 5839 _reflns_number_total 8471 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file bt4007sup1.cif _cod_data_source_block I _cod_original_cell_volume 1510.3(5) _cod_database_code 1543280 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; -2 0 0 5418.46 157.08 -2 0 0 5299.37 156.98 -2 0 0 5830.52 157.68 -2 0 0 5266.37 157.18 -2 0 0 5451.25 157.18 -2 0 0 5527.85 158.08 -2 0 0 5424.96 157.48 -2 0 0 5063.69 156.88 -2 0 0 5457.95 157.48 -2 0 0 5133.99 157.28 -2 0 0 5533.25 157.78 -2 0 0 5278.87 157.48 -2 0 0 5486.45 157.68 2 0 0 5621.64 157.78 2 0 0 5316.67 156.98 2 0 0 5681.73 157.58 2 0 0 5343.77 157.68 2 0 0 4964.30 157.48 2 0 0 5478.95 157.18 2 0 0 5261.67 156.98 2 0 0 5270.87 157.28 2 0 0 5381.36 157.28 2 0 0 5509.55 157.78 2 0 0 5563.54 157.78 2 0 0 5241.68 157.08 -3 0 0 198.38 6.20 -3 0 0 205.28 6.30 -3 0 0 197.88 6.20 -3 0 0 192.08 6.10 -3 0 0 192.78 6.20 -3 0 0 200.28 6.20 -3 0 0 195.78 6.10 -3 0 0 196.08 6.20 -3 0 0 196.28 6.20 -3 0 0 201.68 6.20 -3 0 0 201.78 6.10 3 0 0 196.88 6.30 3 0 0 203.08 6.10 3 0 0 188.58 6.10 3 0 0 190.38 6.20 3 0 0 195.98 6.20 3 0 0 202.08 6.20 3 0 0 208.28 6.20 3 0 0 196.08 6.10 3 0 0 199.78 6.20 3 0 0 208.48 6.30 -4 0 0 22.00 1.10 -4 0 0 19.70 1.00 -4 0 0 19.60 1.20 -4 0 0 19.90 1.10 -4 0 0 22.20 1.20 -4 0 0 22.30 1.20 -4 0 0 20.40 1.10 -4 0 0 20.80 1.10 -4 0 0 20.60 1.20 -4 0 0 21.40 1.20 4 0 0 21.40 1.10 4 0 0 21.20 1.10 4 0 0 21.00 1.20 4 0 0 19.30 1.20 4 0 0 21.60 1.20 4 0 0 23.80 1.20 4 0 0 19.30 1.10 4 0 0 20.90 1.00 -5 0 0 4.00 0.70 -5 0 0 3.60 0.70 -5 0 0 4.00 0.60 -5 0 0 3.80 0.70 -5 0 0 3.60 0.60 -5 0 0 4.50 0.60 -5 0 0 4.80 0.60 -5 0 0 4.60 0.70 -5 0 0 3.50 0.70 5 0 0 3.30 0.60 5 0 0 4.00 0.50 5 0 0 3.80 0.70 5 0 0 4.20 0.80 5 0 0 4.20 0.70 5 0 0 3.40 0.60 -6 0 0 41.50 1.90 -6 0 0 36.20 1.90 -6 0 0 42.20 2.10 -6 0 0 39.60 2.00 -6 0 0 40.60 1.90 -6 0 0 37.40 2.00 -6 0 0 41.40 2.00 -6 0 0 41.10 2.10 6 0 0 40.80 1.80 6 0 0 40.80 2.00 6 0 0 37.90 2.10 6 0 0 39.70 1.90 6 0 0 39.60 2.00 6 0 0 35.50 1.90 -7 0 0 1.90 0.80 -7 0 0 3.90 0.80 -7 0 0 1.10 0.50 -7 0 0 1.90 0.70 -7 0 0 3.00 0.70 -7 0 0 2.00 0.70 -7 0 0 1.70 0.80 7 0 0 1.50 0.60 7 0 0 3.00 0.90 7 0 0 2.00 0.70 7 0 0 3.10 0.90 7 0 0 1.90 0.70 7 0 0 2.90 0.30 -8 0 0 4.50 0.80 -8 0 0 3.30 1.00 -8 0 0 4.00 1.00 -8 0 0 4.40 0.90 -8 0 0 4.30 0.90 -8 0 0 4.60 1.00 -8 0 0 4.10 0.80 8 0 0 3.80 1.00 8 0 0 5.30 1.00 8 0 0 4.00 1.10 8 0 0 2.60 0.70 8 0 0 2.90 0.90 -9 0 0 6.90 1.20 -9 0 0 4.80 1.10 -9 0 0 4.30 0.90 -9 0 0 4.10 0.90 -9 0 0 4.80 1.30 -9 0 0 4.50 1.00 -9 0 0 4.70 0.90 9 0 0 5.70 1.10 9 0 0 5.80 1.20 9 0 0 4.10 0.80 9 0 0 6.00 1.20 9 0 0 5.20 1.20 -10 0 0 -0.30 0.80 -10 0 0 0.60 0.70 -10 0 0 -2.20 0.90 10 0 0 1.30 0.90 10 0 0 0.40 0.60 10 0 0 0.40 0.80 10 0 0 -0.80 1.20 10 0 0 0.30 0.80 -11 0 0 1.70 1.00 -11 0 0 1.00 1.30 -11 0 0 1.50 1.00 11 0 0 1.70 1.10 11 0 0 1.70 1.00 11 0 0 2.90 1.20 11 0 0 2.20 0.80 -12 0 0 3.60 1.20 -12 0 0 1.60 1.40 -12 0 0 2.10 1.20 12 0 0 2.90 0.90 12 0 0 3.20 1.30 12 0 0 4.20 1.30 12 0 0 2.50 1.30 -13 0 0 0.50 1.50 -13 0 0 0.80 1.10 -13 0 0 1.60 1.30 13 0 0 -1.30 1.00 13 0 0 1.10 1.10 13 -1 0 2.40 1.20 13 -1 0 2.10 1.30 13 -1 0 2.30 1.30 -13 1 0 -0.80 1.50 -13 1 0 1.30 1.20 12 -1 0 -0.50 0.60 12 -1 0 1.40 1.00 12 -1 0 2.30 1.20 12 -1 0 -0.50 1.00 -12 1 0 -0.40 0.80 -12 1 0 0.60 1.30 -12 1 0 1.00 1.00 11 -1 0 1.50 0.70 11 -1 0 2.90 1.10 11 -1 0 4.30 1.40 11 -1 0 2.20 1.00 -11 1 0 2.40 1.00 -11 1 0 2.20 1.40 -11 1 0 2.50 1.20 10 -1 0 34.00 2.30 10 -1 0 32.50 2.40 10 -1 0 33.50 2.40 10 -1 0 32.40 1.90 -10 1 0 32.00 2.30 -10 1 0 32.80 2.10 -10 1 0 30.40 2.20 -10 1 0 31.00 2.40 -10 1 0 32.80 2.60 -10 1 0 29.40 2.30 -10 1 0 32.10 2.40 9 -1 0 11.60 1.60 9 -1 0 10.70 1.20 9 -1 0 11.30 1.50 9 -1 0 11.60 1.60 9 -1 0 10.40 1.40 -9 1 0 12.10 1.50 -9 1 0 12.00 1.40 -9 1 0 9.80 1.50 -9 1 0 12.10 1.50 -9 1 0 13.00 1.40 -9 1 0 10.10 1.40 -9 1 0 10.80 1.40 8 -1 0 68.39 3.10 8 -1 0 61.09 2.70 8 -1 0 65.29 2.10 8 -1 0 63.69 3.20 8 -1 0 63.69 3.20 8 -1 0 61.39 3.00 -8 1 0 65.39 3.30 -8 1 0 66.19 3.10 -8 1 0 62.59 3.00 -8 1 0 63.79 3.10 -8 1 0 60.79 2.90 -8 1 0 68.49 3.20 -8 1 0 63.19 3.00 -8 1 0 64.79 2.80 7 -1 0 26.90 1.10 7 -1 0 28.60 1.90 7 -1 0 28.30 1.90 7 -1 0 28.70 1.80 7 -1 0 30.10 1.80 7 -1 0 26.00 1.40 -7 1 0 28.40 1.80 -7 1 0 24.90 1.90 -7 1 0 25.00 1.70 -7 1 0 27.30 1.70 -7 1 0 28.90 1.90 -7 1 0 26.40 1.50 -7 1 0 26.10 1.70 -7 1 0 27.30 1.70 6 -1 0 101.59 3.50 6 -1 0 96.49 3.90 6 -1 0 102.99 3.60 6 -1 0 99.49 3.80 6 -1 0 100.59 3.80 6 -1 0 98.39 3.90 -6 1 0 100.39 3.90 -6 1 0 96.49 3.70 -6 1 0 100.29 3.80 -6 1 0 98.39 3.50 -6 1 0 99.49 3.90 -6 1 0 98.29 3.70 -6 1 0 100.09 3.80 -6 1 0 98.39 3.80 5 -1 0 25.70 1.40 5 -1 0 24.90 1.30 5 -1 0 26.60 1.40 5 -1 0 23.40 1.40 5 -1 0 28.10 1.40 5 -1 0 24.80 1.50 5 -1 0 25.40 1.20 -5 1 0 22.30 1.40 -5 1 0 24.50 1.50 -5 1 0 24.30 1.30 -5 1 0 25.30 1.40 -5 1 0 23.70 1.50 -5 1 0 22.60 1.40 -5 1 0 23.80 1.20 -5 1 0 25.50 1.40 -5 1 0 25.40 1.40 4 -1 0 251.97 7.50 4 -1 0 244.98 7.70 4 -1 0 236.48 7.70 4 -1 0 242.58 7.80 4 -1 0 247.98 7.70 4 -1 0 258.27 7.90 -4 1 0 243.38 7.70 -4 1 0 243.78 7.50 -4 1 0 243.58 7.80 -4 1 0 240.78 7.60 -4 1 0 240.38 7.70 -4 1 0 249.28 7.80 -4 1 0 253.77 7.50 -4 1 0 246.78 7.60 -4 1 0 239.58 7.70 -4 1 0 234.18 7.70 3 -1 0 184.18 5.90 3 -1 0 196.28 6.10 3 -1 0 183.98 5.80 3 -1 0 187.08 5.70 3 -1 0 190.18 5.80 3 -1 0 192.28 5.80 3 -1 0 190.28 5.70 3 -1 0 180.98 5.80 3 -1 0 183.68 5.90 3 -1 0 177.58 5.90 3 -1 0 192.58 5.90 3 -1 0 184.88 5.70 -3 1 0 183.88 5.80 -3 1 0 184.38 6.00 -3 1 0 179.38 5.70 -3 1 0 191.08 6.10 -3 1 0 185.18 5.80 -3 1 0 179.98 5.70 -3 1 0 181.38 5.90 -3 1 0 186.68 5.90 -3 1 0 195.08 5.80 -3 1 0 191.58 5.70 -3 1 0 180.08 5.80 -3 1 0 179.68 5.80 2 -1 0 71.99 2.60 2 -1 0 77.09 2.40 2 -1 0 76.49 2.50 2 -1 0 76.79 2.50 2 -1 0 72.19 2.60 2 -1 0 82.19 2.60 2 -1 0 75.19 2.40 2 -1 0 76.99 2.50 2 -1 0 75.19 2.40 2 -1 0 72.99 2.50 2 -1 0 75.59 2.50 -2 1 0 79.29 2.50 -2 1 0 69.99 2.40 -2 1 0 73.69 2.50 -2 1 0 75.09 2.50 -2 1 0 75.89 2.50 -2 1 0 74.79 2.40 -2 1 0 73.89 2.50 -2 1 0 79.49 2.60 -2 1 0 74.29 2.60 -2 1 0 74.59 2.40 -2 1 0 75.19 2.60 -2 1 0 76.49 2.60 -2 1 0 72.69 2.50 1 -1 0 13.70 0.60 1 -1 0 17.10 0.60 1 -1 0 14.80 0.60 1 -1 0 13.90 0.70 1 -1 0 17.80 0.60 1 -1 0 15.60 0.60 1 -1 0 16.60 0.60 1 -1 0 17.00 0.60 1 -1 0 15.10 0.70 1 -1 0 16.50 0.60 -1 1 0 13.80 0.60 -1 1 0 15.30 0.60 -1 1 0 17.40 0.70 -1 1 0 18.00 0.70 -1 1 0 16.00 0.60 -1 1 0 15.10 0.60 -1 1 0 17.20 0.80 -1 1 0 17.30 0.60 -1 1 0 17.80 0.60 0 -1 0 -1.00 0.10 0 -1 0 -1.10 0.10 0 -1 0 -1.00 0.10 0 -1 0 -1.10 0.10 0 -1 0 -1.00 0.10 0 -1 0 -1.10 0.10 0 -1 0 -1.10 0.10 0 1 0 -1.00 0.10 0 1 0 -1.10 0.10 0 1 0 -1.00 0.10 0 1 0 -1.00 0.10 0 1 0 -1.00 0.10 0 1 0 -1.20 0.10 0 1 0 -1.10 0.10 -1 -1 0 18.40 0.80 -1 -1 0 19.80 0.80 -1 -1 0 19.20 0.80 -1 -1 0 19.20 0.80 -1 -1 0 19.60 0.80 -1 -1 0 19.60 0.80 -1 -1 0 21.70 0.90 -1 -1 0 20.70 0.80 -1 -1 0 19.60 0.80 1 1 0 19.50 0.80 1 1 0 18.70 0.80 1 1 0 19.50 0.80 1 1 0 21.90 0.80 1 1 0 20.30 0.80 1 1 0 20.70 0.80 1 1 0 17.80 0.90 1 1 0 19.30 0.80 1 1 0 18.40 0.80 -2 -1 0 3.30 0.40 -2 -1 0 3.30 0.40 -2 -1 0 4.20 0.50 -2 -1 0 4.60 0.50 -2 -1 0 4.90 0.30 -2 -1 0 3.40 0.40 -2 -1 0 4.30 0.50 -2 -1 0 5.00 0.60 -2 -1 0 4.70 0.50 -2 -1 0 4.60 0.50 -2 -1 0 4.80 0.30 -2 -1 0 5.10 0.50 2 1 0 4.30 0.40 2 1 0 4.90 0.50 2 1 0 4.00 0.40 2 1 0 5.20 0.50 2 1 0 5.10 0.50 2 1 0 4.40 0.50 2 1 0 4.30 0.40 2 1 0 4.60 0.30 2 1 0 4.40 0.50 2 1 0 4.50 0.50 2 1 0 4.30 0.60 2 1 0 3.60 0.40 -3 -1 0 820.12 24.80 -3 -1 0 854.01 24.60 -3 -1 0 856.71 24.80 -3 -1 0 838.32 24.80 -3 -1 0 839.22 24.80 -3 -1 0 835.52 24.80 -3 -1 0 814.42 24.70 -3 -1 0 821.82 24.80 -3 -1 0 815.62 24.70 3 1 0 844.32 24.90 3 1 0 853.31 24.70 3 1 0 798.92 24.80 3 1 0 848.82 24.80 3 1 0 865.81 24.80 3 1 0 860.11 24.80 3 1 0 843.32 24.80 3 1 0 853.21 24.70 3 1 0 888.51 24.50 -4 -1 0 0.90 0.40 -4 -1 0 1.00 0.40 -4 -1 0 0.70 0.20 -4 -1 0 0.50 0.40 -4 -1 0 0.50 0.40 -4 -1 0 0.40 0.40 -4 -1 0 0.90 0.30 -4 -1 0 0.40 0.40 4 1 0 1.00 0.40 4 1 0 0.80 0.40 4 1 0 0.40 0.40 4 1 0 0.60 0.20 4 1 0 0.80 0.40 4 1 0 0.50 0.40 4 1 0 0.50 0.30 4 1 0 1.10 0.40 -5 -1 0 113.79 4.00 -5 -1 0 111.29 4.00 -5 -1 0 103.79 3.90 -5 -1 0 111.39 3.70 -5 -1 0 106.49 4.00 -5 -1 0 107.69 4.00 -5 -1 0 111.39 3.70 -5 -1 0 124.69 4.10 5 1 0 106.79 3.90 5 1 0 105.09 3.80 5 1 0 113.79 3.50 5 1 0 110.89 4.00 5 1 0 115.09 3.90 5 1 0 104.39 3.90 5 1 0 102.19 4.10 5 1 0 115.09 4.10 -6 -1 0 0.00 0.50 -6 -1 0 -0.20 0.50 -6 -1 0 0.10 0.50 -6 -1 0 -0.30 0.40 -6 -1 0 0.20 0.50 -6 -1 0 -0.10 0.50 -6 -1 0 0.20 0.30 -6 -1 0 0.50 0.40 6 1 0 1.00 0.50 6 1 0 0.40 0.20 6 1 0 0.90 0.50 6 1 0 0.40 0.40 6 1 0 -0.10 0.60 6 1 0 0.50 0.50 6 1 0 0.00 0.40 -7 -1 0 1.80 0.80 -7 -1 0 -0.60 0.40 -7 -1 0 0.30 0.40 -7 -1 0 0.10 0.70 -7 -1 0 -0.50 0.70 -7 -1 0 0.50 0.60 -7 -1 0 0.20 0.60 7 1 0 -0.20 0.50 7 1 0 1.10 0.70 7 1 0 0.30 0.70 7 1 0 0.80 0.70 7 1 0 0.30 0.20 7 1 0 -0.10 0.60 -8 -1 0 33.20 2.10 -8 -1 0 34.90 2.20 -8 -1 0 31.20 2.30 -8 -1 0 33.70 1.90 -8 -1 0 31.80 1.70 -8 -1 0 32.70 2.00 8 1 0 33.10 2.10 8 1 0 29.20 1.80 8 1 0 30.80 2.20 8 1 0 34.10 2.20 8 1 0 33.10 2.10 -9 -1 0 25.30 1.90 -9 -1 0 25.90 1.90 -9 -1 0 25.50 2.20 -9 -1 0 27.30 2.00 9 1 0 28.60 2.10 9 1 0 25.10 2.00 9 1 0 27.70 2.00 9 1 0 26.20 2.10 9 1 0 25.00 1.70 -10 -1 0 1.30 1.10 -10 -1 0 2.00 0.90 -10 -1 0 2.40 0.90 10 1 0 3.40 1.20 10 1 0 0.70 0.70 10 1 0 1.80 1.00 10 1 0 3.60 1.00 10 1 0 2.10 0.90 -11 -1 0 0.20 1.20 -11 -1 0 0.10 0.80 -11 -1 0 0.20 1.00 11 1 0 2.10 1.10 11 1 0 1.50 0.80 11 1 0 1.10 1.00 11 1 0 -0.30 0.90 -12 -1 0 -1.40 1.20 -12 -1 0 0.10 1.00 -12 -1 0 0.60 1.00 12 1 0 -0.30 0.70 12 1 0 0.60 1.20 12 1 0 1.40 1.10 -13 -1 0 0.70 1.20 -13 -1 0 0.10 1.00 -13 -1 0 -0.70 1.40 13 1 0 -0.20 1.20 13 1 0 1.20 1.10 13 -2 0 1.60 1.20 13 -2 0 2.40 1.30 13 -2 0 -1.00 1.00 -13 2 0 0.40 1.10 -13 2 0 -2.50 1.40 12 -2 0 -0.20 0.90 12 -2 0 0.50 1.20 12 -2 0 1.10 1.10 -12 2 0 -0.40 0.90 -12 2 0 -0.80 1.20 -12 2 0 0.30 0.80 11 -2 0 0.00 0.50 11 -2 0 0.20 1.00 11 -2 0 0.40 0.90 11 -2 0 0.50 0.90 -11 2 0 -0.30 0.80 -11 2 0 0.10 0.70 -11 2 0 -1.20 0.80 -11 2 0 -1.70 0.90 10 -2 0 11.50 1.20 10 -2 0 12.30 1.60 10 -2 0 14.70 1.90 10 -2 0 12.10 1.80 -10 2 0 11.40 1.60 -10 2 0 12.90 1.70 -10 2 0 9.80 1.60 -10 2 0 13.60 1.60 -10 2 0 12.60 1.70 -10 2 0 7.50 1.30 -10 2 0 12.00 1.40 9 -2 0 5.60 0.90 9 -2 0 6.30 1.10 9 -2 0 7.20 1.30 9 -2 0 6.60 1.30 -9 2 0 4.50 1.10 -9 2 0 7.30 1.10 -9 2 0 6.50 1.10 -9 2 0 7.30 1.20 -9 2 0 5.00 1.00 -9 2 0 7.80 1.30 -9 2 0 6.40 1.30 -9 2 0 6.80 1.20 8 -2 0 64.99 3.00 8 -2 0 61.89 3.20 8 -2 0 62.09 3.10 8 -2 0 55.89 2.90 8 -2 0 56.99 2.50 8 -2 0 63.09 2.10 -8 2 0 61.99 2.80 -8 2 0 61.19 2.80 -8 2 0 62.49 3.10 -8 2 0 61.69 3.20 -8 2 0 61.09 3.20 -8 2 0 62.49 3.00 -8 2 0 64.09 3.10 -8 2 0 54.79 2.60 7 -2 0 14.50 1.60 7 -2 0 15.20 1.40 7 -2 0 15.90 1.40 7 -2 0 15.10 1.30 7 -2 0 15.30 0.80 7 -2 0 15.10 1.10 -7 2 0 17.90 1.60 -7 2 0 16.00 1.50 -7 2 0 17.50 1.30 -7 2 0 16.90 1.20 -7 2 0 15.10 1.50 -7 2 0 16.30 1.40 -7 2 0 15.90 1.30 -7 2 0 16.60 1.60 6 -2 0 23.10 1.60 6 -2 0 24.10 1.60 6 -2 0 22.40 1.40 6 -2 0 25.30 1.30 6 -2 0 24.30 1.30 6 -2 0 24.60 1.00 6 -2 0 23.90 1.50 -6 2 0 24.60 1.50 -6 2 0 25.50 1.70 -6 2 0 25.00 1.60 -6 2 0 22.60 1.20 -6 2 0 21.20 1.50 -6 2 0 23.40 1.40 -6 2 0 23.80 1.40 -6 2 0 22.30 1.60 -6 2 0 24.20 1.60 5 -2 0 12.50 1.10 5 -2 0 12.50 0.80 5 -2 0 12.50 1.00 5 -2 0 9.80 0.90 5 -2 0 11.70 1.10 5 -2 0 12.90 0.70 5 -2 0 12.00 0.90 5 -2 0 13.10 0.90 -5 2 0 11.40 0.90 -5 2 0 12.20 1.10 -5 2 0 13.70 1.20 -5 2 0 11.50 1.00 -5 2 0 11.50 1.00 -5 2 0 10.90 0.80 -5 2 0 9.70 1.00 -5 2 0 12.60 0.90 4 -2 0 19.90 0.90 4 -2 0 19.20 1.20 4 -2 0 18.50 1.10 4 -2 0 20.40 1.20 4 -2 0 17.20 1.20 4 -2 0 20.60 1.00 4 -2 0 20.00 1.10 4 -2 0 18.80 0.90 -4 2 0 21.70 0.90 -4 2 0 18.10 1.10 -4 2 0 17.30 1.10 -4 2 0 19.30 1.10 -4 2 0 18.00 1.00 -4 2 0 17.30 1.20 -4 2 0 19.40 1.00 -4 2 0 18.70 1.30 -4 2 0 18.50 1.20 3 -2 0 46.30 1.60 3 -2 0 40.40 1.80 3 -2 0 41.30 1.80 3 -2 0 43.60 1.60 3 -2 0 43.60 1.70 3 -2 0 41.60 1.50 3 -2 0 43.70 1.60 3 -2 0 44.60 1.70 3 -2 0 43.20 1.50 3 -2 0 44.30 1.90 -3 2 0 43.30 1.50 -3 2 0 41.80 1.70 -3 2 0 42.00 1.60 -3 2 0 44.60 1.70 -3 2 0 39.40 1.70 -3 2 0 41.70 1.60 -3 2 0 41.10 1.50 -3 2 0 39.10 1.80 -3 2 0 42.90 1.70 -3 2 0 43.60 1.90 2 -2 0 5.30 0.40 2 -2 0 4.30 0.50 2 -2 0 5.20 0.60 2 -2 0 4.60 0.40 2 -2 0 4.40 0.40 2 -2 0 5.80 0.40 2 -2 0 5.60 0.40 2 -2 0 4.70 0.40 2 -2 0 6.60 0.50 2 -2 0 5.10 0.40 2 -2 0 6.10 0.50 2 -2 0 5.20 0.40 -2 2 0 4.60 0.40 -2 2 0 4.90 0.40 -2 2 0 5.80 0.40 -2 2 0 4.90 0.50 -2 2 0 5.30 0.60 -2 2 0 5.20 0.40 -2 2 0 5.00 0.40 -2 2 0 4.70 0.60 -2 2 0 4.60 0.40 -2 2 0 4.90 0.40 -2 2 0 4.40 0.60 -2 2 0 6.20 0.60 1 -2 0 53.49 1.70 1 -2 0 54.29 1.70 1 -2 0 54.49 1.70 1 -2 0 57.19 1.90 1 -2 0 55.49 1.70 1 -2 0 52.69 1.90 1 -2 0 53.29 2.00 1 -2 0 55.59 1.90 -1 2 0 52.79 1.70 -1 2 0 50.29 1.70 -1 2 0 55.49 1.90 -1 2 0 55.79 1.80 -1 2 0 52.59 1.80 -1 2 0 51.09 1.90 -1 2 0 51.89 1.70 -1 2 0 51.19 2.00 -1 2 0 50.39 1.70 -1 2 0 55.99 1.70 -1 2 0 51.29 1.70 -1 2 0 54.09 2.00 0 -2 0 712.23 21.60 0 -2 0 751.02 21.60 0 -2 0 722.23 21.70 0 -2 0 750.12 21.60 0 -2 0 739.53 21.70 0 -2 0 743.73 21.70 0 -2 0 769.02 21.70 0 -2 0 745.33 21.70 0 2 0 757.92 21.70 0 2 0 721.93 21.60 0 2 0 765.92 21.70 0 2 0 797.92 21.70 0 2 0 712.13 21.70 0 2 0 694.03 21.70 0 2 0 744.53 21.50 0 2 0 717.63 21.60 0 2 0 776.72 21.70 -1 -2 0 1.80 0.30 -1 -2 0 1.90 0.50 -1 -2 0 2.70 0.30 -1 -2 0 2.40 0.30 -1 -2 0 2.80 0.30 -1 -2 0 1.60 0.40 -1 -2 0 2.10 0.30 -1 -2 0 2.20 0.40 -1 -2 0 2.20 0.30 -1 -2 0 2.80 0.30 1 2 0 2.80 0.30 1 2 0 2.40 0.40 1 2 0 2.00 0.30 1 2 0 2.80 0.30 1 2 0 2.40 0.30 1 2 0 2.40 0.40 1 2 0 2.70 0.40 1 2 0 1.40 0.20 1 2 0 2.50 0.30 1 2 0 1.70 0.30 1 2 0 3.20 0.60 1 2 0 2.20 0.30 1 2 0 2.80 0.30 -2 -2 0 1033.50 29.80 -2 -2 0 1082.19 29.60 -2 -2 0 983.50 29.60 -2 -2 0 1019.40 29.50 -2 -2 0 1026.60 29.70 -2 -2 0 984.60 29.60 -2 -2 0 1010.90 29.60 -2 -2 0 963.40 29.70 -2 -2 0 995.30 29.50 -2 -2 0 988.90 29.60 -2 -2 0 1078.39 29.60 2 2 0 1040.50 29.60 2 2 0 977.20 29.60 2 2 0 993.30 29.60 2 2 0 1009.70 29.60 2 2 0 953.70 29.80 2 2 0 1022.90 29.70 2 2 0 993.70 29.60 2 2 0 1074.99 29.60 2 2 0 1037.30 29.70 -3 -2 0 77.99 2.80 -3 -2 0 80.39 2.80 -3 -2 0 77.99 2.80 -3 -2 0 79.19 2.80 3 2 0 80.09 2.80 3 2 0 77.39 2.80 3 2 0 82.99 2.80 3 2 0 74.99 2.90 3 2 0 77.89 2.80 3 2 0 83.69 2.60 3 2 0 78.49 2.80 3 2 0 78.89 2.80 -4 -2 0 6.70 0.80 -4 -2 0 8.80 0.50 -4 -2 0 8.80 0.90 -4 -2 0 8.10 0.80 -4 -2 0 8.70 0.80 -4 -2 0 9.70 0.90 -4 -2 0 8.80 0.50 4 2 0 9.10 0.90 4 2 0 9.20 0.80 4 2 0 9.40 0.70 4 2 0 9.00 0.80 4 2 0 7.90 0.80 4 2 0 8.90 1.00 4 2 0 9.40 0.80 4 2 0 9.20 0.60 -5 -2 0 2.00 0.30 -5 -2 0 2.90 0.60 -5 -2 0 2.80 0.30 -5 -2 0 2.60 0.60 -5 -2 0 3.70 0.70 -5 -2 0 2.60 0.70 -5 -2 0 3.60 0.70 5 2 0 3.10 0.70 5 2 0 3.40 0.60 5 2 0 3.20 0.60 5 2 0 3.00 0.70 5 2 0 4.10 0.40 5 2 0 2.80 0.60 5 2 0 2.10 0.50 5 2 0 3.90 0.70 -6 -2 0 7.90 1.00 -6 -2 0 7.80 1.10 -6 -2 0 8.60 1.00 -6 -2 0 7.20 1.00 -6 -2 0 7.90 0.80 -6 -2 0 7.60 0.70 -6 -2 0 5.50 0.90 6 2 0 8.00 1.00 6 2 0 6.10 1.10 6 2 0 7.40 0.90 6 2 0 8.00 0.60 6 2 0 6.80 1.00 6 2 0 5.30 0.90 6 2 0 9.70 1.10 -7 -2 0 11.80 1.40 -7 -2 0 16.60 1.50 -7 -2 0 13.60 1.40 -7 -2 0 15.60 1.00 -7 -2 0 14.30 1.10 -7 -2 0 16.30 1.60 7 2 0 15.70 1.60 7 2 0 15.20 1.40 7 2 0 14.30 1.40 7 2 0 14.40 1.70 7 2 0 17.00 1.40 -8 -2 0 5.30 1.00 -8 -2 0 6.00 1.00 -8 -2 0 5.40 1.20 -8 -2 0 5.30 0.80 -8 -2 0 4.30 0.60 8 2 0 7.20 1.30 8 2 0 6.80 1.10 8 2 0 5.60 1.10 8 2 0 5.50 1.00 8 2 0 7.00 1.20 -9 -2 0 -0.30 0.60 -9 -2 0 0.00 0.70 -9 -2 0 0.30 0.90 9 2 0 0.80 0.80 9 2 0 0.60 0.90 9 2 0 -0.10 0.60 9 2 0 -0.20 0.60 9 2 0 0.40 0.80 -10 -2 0 0.10 1.00 -10 -2 0 0.10 0.80 -10 -2 0 -0.10 0.80 10 2 0 0.80 1.00 10 2 0 -0.90 0.80 10 2 0 -0.40 0.60 10 2 0 -0.70 0.70 10 2 0 0.50 0.80 -11 -2 0 1.20 1.00 -11 -2 0 2.20 1.10 -11 -2 0 0.90 1.30 11 2 0 1.80 1.10 11 2 0 1.40 1.10 11 2 0 1.80 0.80 -12 -2 0 2.40 1.10 -12 -2 0 0.70 1.00 -12 -2 0 -2.60 1.30 12 2 0 3.70 1.40 12 2 0 0.70 0.80 12 2 0 0.40 1.10 13 -3 0 0.60 1.10 13 -3 0 1.30 1.20 13 -3 0 1.50 1.30 -13 3 0 0.70 1.20 -13 3 0 -1.70 1.20 12 -3 0 1.20 1.10 12 -3 0 0.00 0.90 12 -3 0 0.40 1.00 -12 3 0 -1.70 1.00 -12 3 0 1.20 1.10 -12 3 0 -0.80 1.10 11 -3 0 2.50 1.20 11 -3 0 0.90 1.00 11 -3 0 1.10 1.00 11 -3 0 1.70 0.70 -11 3 0 0.10 0.90 -11 3 0 0.90 1.00 -11 3 0 1.10 1.20 -11 3 0 0.90 0.80 -11 3 0 1.70 1.00 -11 3 0 1.60 1.00 -11 3 0 0.90 0.90 10 -3 0 -1.00 0.80 10 -3 0 -0.30 0.40 10 -3 0 0.00 0.70 10 -3 0 0.00 0.70 -10 3 0 0.00 0.80 -10 3 0 -0.10 0.70 -10 3 0 -0.70 0.70 -10 3 0 -1.90 0.60 -10 3 0 0.30 0.80 -10 3 0 -0.30 0.70 -10 3 0 0.70 0.80 -10 3 0 0.00 0.90 9 -3 0 7.80 1.50 9 -3 0 6.20 1.10 9 -3 0 5.40 1.30 9 -3 0 8.50 1.00 -9 3 0 5.70 1.20 -9 3 0 7.00 1.10 -9 3 0 7.50 1.30 -9 3 0 7.80 1.30 -9 3 0 6.90 1.30 -9 3 0 8.60 1.10 -9 3 0 7.60 1.10 -9 3 0 6.20 1.20 8 -3 0 3.40 1.00 8 -3 0 3.00 0.50 8 -3 0 2.00 0.90 8 -3 0 2.40 0.80 8 -3 0 2.90 0.80 8 -3 0 2.80 0.60 -8 3 0 3.50 0.70 -8 3 0 3.00 0.70 -8 3 0 2.30 0.90 -8 3 0 2.20 0.90 -8 3 0 1.70 0.80 -8 3 0 2.40 0.90 -8 3 0 3.60 0.80 -8 3 0 4.20 1.00 7 -3 0 5.30 0.70 7 -3 0 4.30 0.50 7 -3 0 4.00 1.00 7 -3 0 4.20 0.80 7 -3 0 3.10 1.00 7 -3 0 4.30 0.80 -7 3 0 4.00 0.80 -7 3 0 4.10 0.90 -7 3 0 5.00 0.90 -7 3 0 4.90 0.80 -7 3 0 2.60 0.70 -7 3 0 3.00 0.80 -7 3 0 4.40 1.00 -7 3 0 3.60 0.90 -7 3 0 2.70 0.80 6 -3 0 52.79 2.00 6 -3 0 54.39 2.30 6 -3 0 52.69 2.70 6 -3 0 52.79 2.20 6 -3 0 51.39 2.00 6 -3 0 48.90 2.30 6 -3 0 52.09 2.50 -6 3 0 50.09 2.50 -6 3 0 51.49 2.40 -6 3 0 55.09 2.40 -6 3 0 51.09 2.20 -6 3 0 48.10 2.70 -6 3 0 52.99 2.50 -6 3 0 49.50 2.60 -6 3 0 52.39 2.20 5 -3 0 34.50 1.50 5 -3 0 35.30 1.40 5 -3 0 35.50 1.50 5 -3 0 34.40 1.90 5 -3 0 36.00 1.70 5 -3 0 36.30 1.90 -5 3 0 35.40 1.60 -5 3 0 31.50 1.80 -5 3 0 35.40 1.70 -5 3 0 35.10 2.00 -5 3 0 33.00 1.50 -5 3 0 34.20 1.70 -5 3 0 34.70 2.00 -5 3 0 35.30 1.70 4 -3 0 31.10 1.70 4 -3 0 32.10 1.40 4 -3 0 35.10 1.50 4 -3 0 30.70 1.30 4 -3 0 29.90 1.40 4 -3 0 32.10 1.30 4 -3 0 29.40 1.70 -4 3 0 32.00 1.40 -4 3 0 32.40 1.50 -4 3 0 30.90 1.50 -4 3 0 33.00 1.60 -4 3 0 32.20 1.50 -4 3 0 34.10 1.90 -4 3 0 30.10 1.70 -4 3 0 31.70 1.30 3 -3 0 3.90 0.40 3 -3 0 4.40 0.50 3 -3 0 3.70 0.40 3 -3 0 4.30 0.50 3 -3 0 3.00 0.40 3 -3 0 3.70 0.40 3 -3 0 4.00 0.70 3 -3 0 4.20 0.60 3 -3 0 4.80 0.40 -3 3 0 3.40 0.50 -3 3 0 3.60 0.40 -3 3 0 4.00 0.50 -3 3 0 4.60 0.50 -3 3 0 3.90 0.60 -3 3 0 3.40 0.60 -3 3 0 3.70 0.40 -3 3 0 3.90 0.50 -3 3 0 4.30 0.40 -3 3 0 4.20 0.50 2 -3 0 0.60 0.20 2 -3 0 0.90 0.20 2 -3 0 1.00 0.30 2 -3 0 0.90 0.30 2 -3 0 0.60 0.20 2 -3 0 1.10 0.20 2 -3 0 1.00 0.30 2 -3 0 0.50 0.40 2 -3 0 0.70 0.20 2 -3 0 0.80 0.30 -2 3 0 0.60 0.20 -2 3 0 0.60 0.20 -2 3 0 0.70 0.20 -2 3 0 0.50 0.20 -2 3 0 1.10 0.20 -2 3 0 1.00 0.40 -2 3 0 0.40 0.30 -2 3 0 1.30 0.20 -2 3 0 1.20 0.30 -2 3 0 0.80 0.30 1 -3 0 710.43 19.90 1 -3 0 660.93 20.10 1 -3 0 693.63 19.90 1 -3 0 706.13 20.10 1 -3 0 668.83 20.30 -1 3 0 659.73 19.80 -1 3 0 672.03 19.90 -1 3 0 654.53 20.30 -1 3 0 657.13 19.90 -1 3 0 700.43 20.20 -1 3 0 678.63 20.30 -1 3 0 701.73 19.80 -1 3 0 682.93 20.10 -1 3 0 704.73 20.00 0 -3 0 23.20 1.00 0 -3 0 23.60 0.80 0 -3 0 23.60 1.10 0 -3 0 22.30 0.80 0 -3 0 22.10 1.10 0 -3 0 22.70 1.00 0 -3 0 21.70 1.00 0 -3 0 22.10 0.80 0 3 0 23.50 0.80 0 3 0 22.10 0.80 0 3 0 22.00 0.80 0 3 0 21.90 1.10 0 3 0 22.10 0.80 0 3 0 23.40 1.00 0 3 0 22.00 1.10 0 3 0 24.00 1.10 0 3 0 24.70 1.00 0 3 0 23.00 0.80 -1 -3 0 880.41 24.60 -1 -3 0 839.22 24.70 -1 -3 0 857.81 24.50 -1 -3 0 863.81 24.60 -1 -3 0 811.72 24.70 -1 -3 0 833.02 24.60 -1 -3 0 850.71 24.80 1 3 0 793.02 24.90 1 3 0 817.52 24.70 1 3 0 871.21 24.50 1 3 0 828.02 24.60 1 3 0 841.12 24.60 1 3 0 846.82 24.60 1 3 0 809.62 24.60 1 3 0 821.82 24.60 1 3 0 850.01 24.60 1 3 0 874.71 24.70 1 3 0 867.91 24.60 -2 -3 0 11.70 0.70 -2 -3 0 11.90 0.80 -2 -3 0 11.90 0.70 -2 -3 0 12.30 0.70 -2 -3 0 12.40 0.80 -2 -3 0 13.60 0.70 -2 -3 0 12.70 0.70 -2 -3 0 12.00 0.70 2 3 0 11.60 0.70 2 3 0 12.40 0.50 2 3 0 11.40 1.00 2 3 0 12.00 0.50 2 3 0 11.50 0.80 2 3 0 13.00 0.70 2 3 0 11.40 0.70 2 3 0 12.70 0.80 -3 -3 0 15.00 0.90 -3 -3 0 14.90 0.80 -3 -3 0 13.80 1.00 -3 -3 0 13.90 0.80 -3 -3 0 13.90 0.90 -3 -3 0 15.10 0.90 -3 -3 0 14.00 0.90 3 3 0 13.60 0.90 3 3 0 13.30 1.10 3 3 0 14.60 1.00 3 3 0 13.80 0.90 3 3 0 14.00 0.90 3 3 0 13.80 0.90 3 3 0 15.20 1.00 -4 -3 0 47.40 2.00 -4 -3 0 46.20 2.00 -4 -3 0 44.60 1.80 -4 -3 0 45.40 2.00 -4 -3 0 45.70 2.10 -4 -3 0 41.90 1.90 4 3 0 50.09 2.10 4 3 0 47.10 1.80 4 3 0 43.90 2.00 4 3 0 46.20 2.00 4 3 0 46.50 2.00 4 3 0 46.70 2.00 4 3 0 44.90 2.20 -5 -3 0 0.80 0.50 -5 -3 0 1.00 0.60 -5 -3 0 0.30 0.50 -5 -3 0 1.30 0.60 -5 -3 0 0.20 0.20 5 3 0 0.00 0.50 5 3 0 0.70 0.50 5 3 0 0.30 0.50 5 3 0 0.70 0.50 5 3 0 1.30 0.40 5 3 0 0.30 0.80 5 3 0 0.10 0.50 -6 -3 0 11.50 1.30 -6 -3 0 11.60 1.30 -6 -3 0 13.60 1.40 -6 -3 0 13.10 1.30 -6 -3 0 11.20 1.20 6 3 0 12.90 1.10 6 3 0 16.00 1.40 6 3 0 14.20 1.60 6 3 0 11.40 1.30 6 3 0 11.50 1.20 6 3 0 14.60 1.30 -7 -3 0 0.00 0.70 -7 -3 0 0.40 0.60 -7 -3 0 0.80 0.60 -7 -3 0 0.60 0.90 7 3 0 0.40 0.70 7 3 0 0.70 0.70 7 3 0 0.30 0.60 7 3 0 0.10 0.60 7 3 0 0.00 0.90 -8 -3 0 15.90 1.70 -8 -3 0 19.30 1.80 -8 -3 0 23.20 1.80 8 3 0 16.40 1.70 8 3 0 19.00 2.10 8 3 0 20.90 1.50 8 3 0 21.80 1.70 8 3 0 19.10 1.70 -9 -3 0 0.90 0.80 -9 -3 0 1.20 1.10 -9 -3 0 0.80 0.80 9 3 0 1.20 0.70 9 3 0 0.40 0.70 9 3 0 1.10 0.80 9 3 0 0.10 0.80 9 3 0 0.90 1.00 -10 -3 0 2.10 1.00 -10 -3 0 2.60 1.10 -10 -3 0 2.30 1.30 10 3 0 1.70 1.10 10 3 0 3.30 1.20 10 3 0 2.50 0.90 10 3 0 4.00 1.30 -11 -3 0 0.10 1.00 -11 -3 0 -1.40 1.00 -11 -3 0 -0.60 0.80 11 3 0 0.50 1.10 11 3 0 0.60 1.10 11 3 0 0.30 0.70 11 3 0 1.60 1.20 -12 -3 0 1.60 1.20 -12 -3 0 2.20 1.20 -12 -3 0 -1.20 1.20 12 3 0 0.10 1.10 12 3 0 3.80 1.40 12 3 0 2.00 1.10 13 -4 0 10.00 2.10 13 -4 0 5.10 1.40 -13 4 0 6.00 1.60 -13 4 0 5.20 1.90 12 -4 0 1.50 1.20 12 -4 0 -0.80 0.90 -12 4 0 -0.50 1.00 -12 4 0 0.20 1.00 -12 4 0 0.50 1.40 11 -4 0 3.60 1.30 11 -4 0 1.60 1.00 -11 4 0 0.30 0.90 -11 4 0 1.40 1.10 -11 4 0 2.70 1.00 -11 4 0 1.10 1.10 -11 4 0 4.80 1.30 -11 4 0 0.50 1.20 -11 4 0 5.30 1.40 10 -4 0 14.00 1.70 10 -4 0 15.60 2.10 10 -4 0 14.50 1.40 -10 4 0 19.40 2.10 -10 4 0 18.10 1.90 -10 4 0 15.00 1.90 -10 4 0 19.10 1.80 -10 4 0 18.60 1.50 -10 4 0 20.60 2.20 -10 4 0 20.70 2.20 -10 4 0 20.40 1.90 9 -4 0 8.90 1.00 9 -4 0 9.40 0.80 9 -4 0 8.50 1.30 9 -4 0 8.40 1.50 -9 4 0 7.50 1.40 -9 4 0 8.00 1.10 -9 4 0 6.70 1.30 -9 4 0 7.70 1.20 -9 4 0 7.00 1.30 -9 4 0 7.90 1.30 -9 4 0 10.10 1.10 -9 4 0 8.30 1.30 8 -4 0 76.59 2.80 8 -4 0 70.69 3.70 8 -4 0 72.69 2.90 8 -4 0 80.79 3.40 -8 4 0 79.79 3.80 -8 4 0 73.69 3.50 -8 4 0 77.99 3.20 -8 4 0 71.09 3.30 -8 4 0 76.19 3.90 -8 4 0 68.59 3.60 -8 4 0 71.39 3.10 -8 4 0 73.59 2.90 7 -4 0 83.69 3.40 7 -4 0 82.99 3.10 7 -4 0 74.09 3.80 7 -4 0 84.19 3.00 -7 4 0 84.29 3.90 -7 4 0 87.59 3.40 -7 4 0 88.79 4.10 -7 4 0 83.49 3.80 -7 4 0 84.19 3.50 -7 4 0 90.49 3.30 -7 4 0 89.29 4.20 -7 4 0 86.19 3.60 6 -4 0 50.39 2.20 6 -4 0 45.30 2.50 6 -4 0 43.20 2.10 6 -4 0 47.20 2.00 6 -4 0 47.00 1.90 6 -4 0 42.50 1.90 -6 4 0 44.10 2.40 -6 4 0 49.40 2.70 -6 4 0 48.30 2.30 -6 4 0 44.10 2.20 -6 4 0 46.30 2.00 -6 4 0 48.90 2.70 -6 4 0 46.40 2.20 5 -4 0 325.67 9.90 5 -4 0 321.27 10.60 5 -4 0 325.27 9.90 5 -4 0 312.37 10.00 5 -4 0 326.87 10.00 5 -4 0 317.97 9.80 5 -4 0 333.47 10.60 -5 4 0 321.27 9.90 -5 4 0 325.97 10.10 -5 4 0 321.87 9.90 -5 4 0 319.17 10.10 -5 4 0 314.27 10.10 -5 4 0 313.77 10.70 -5 4 0 331.17 10.60 -5 4 0 319.07 10.40 4 -4 0 0.90 0.60 4 -4 0 0.90 0.40 4 -4 0 1.00 0.30 4 -4 0 0.50 0.30 4 -4 0 1.00 0.30 4 -4 0 1.10 0.40 -4 4 0 1.10 0.40 -4 4 0 0.90 0.30 -4 4 0 0.90 0.50 -4 4 0 0.70 0.40 -4 4 0 1.30 0.30 -4 4 0 1.20 0.50 -4 4 0 0.30 0.40 -4 4 0 0.60 0.40 3 -4 0 1050.99 30.70 3 -4 0 1058.29 30.60 3 -4 0 1095.79 30.70 3 -4 0 1011.00 31.10 3 -4 0 1093.99 30.70 3 -4 0 1050.09 30.60 3 -4 0 1060.99 30.70 3 -4 0 1034.50 31.30 3 -4 0 1018.30 30.80 -3 4 0 1012.90 31.00 -3 4 0 1055.99 30.70 -3 4 0 1008.80 30.70 -3 4 0 1042.80 30.70 -3 4 0 1057.19 30.80 -3 4 0 1056.69 30.60 -3 4 0 1028.90 31.40 -3 4 0 1090.39 30.70 -3 4 0 1047.30 31.30 2 -4 0 381.96 11.90 2 -4 0 386.36 11.70 2 -4 0 411.06 11.70 2 -4 0 384.66 12.10 2 -4 0 398.96 12.20 -2 4 0 387.86 12.00 -2 4 0 388.16 11.70 -2 4 0 406.56 11.90 -2 4 0 384.26 12.30 -2 4 0 398.56 12.30 -2 4 0 388.56 11.70 -2 4 0 391.16 11.70 -2 4 0 405.66 11.70 -2 4 0 379.66 11.70 -2 4 0 409.96 11.60 1 -4 0 19.00 1.10 1 -4 0 20.60 0.70 1 -4 0 19.90 0.70 1 -4 0 19.10 1.10 1 -4 0 17.90 1.00 1 -4 0 19.00 1.00 -1 4 0 20.00 1.00 -1 4 0 19.00 0.80 -1 4 0 17.20 0.70 -1 4 0 19.30 1.10 -1 4 0 20.10 0.70 -1 4 0 18.90 0.90 -1 4 0 18.30 0.80 -1 4 0 17.90 1.20 0 -4 0 350.16 10.70 0 -4 0 357.26 10.40 0 -4 0 344.77 10.70 0 -4 0 347.97 10.70 0 -4 0 369.36 10.40 0 -4 0 349.87 10.60 0 4 0 344.67 10.90 0 4 0 356.26 10.80 0 4 0 355.06 10.40 0 4 0 346.67 10.40 0 4 0 368.76 10.60 0 4 0 346.67 10.40 0 4 0 345.77 10.40 0 4 0 363.26 10.40 -1 -4 0 540.45 15.30 -1 -4 0 526.25 15.30 -1 -4 0 515.25 15.60 -1 -4 0 526.25 15.50 -1 -4 0 500.55 15.50 1 4 0 510.05 15.40 1 4 0 538.85 15.30 1 4 0 514.85 15.50 1 4 0 508.95 15.30 1 4 0 498.95 15.30 1 4 0 519.65 15.30 1 4 0 508.95 15.80 1 4 0 498.25 15.30 1 4 0 532.55 15.30 1 4 0 549.54 15.30 -2 -4 0 355.46 10.90 -2 -4 0 354.06 10.70 -2 -4 0 342.37 11.00 -2 -4 0 378.26 10.80 -2 -4 0 348.97 10.80 -2 -4 0 351.36 10.80 -2 -4 0 385.46 10.80 -2 -4 0 357.66 10.90 2 4 0 351.46 10.80 2 4 0 355.56 10.80 2 4 0 348.97 10.60 2 4 0 370.76 10.80 2 4 0 371.16 10.80 2 4 0 355.96 10.50 2 4 0 344.67 10.80 2 4 0 351.66 11.20 2 4 0 357.86 10.70 2 4 0 375.36 10.90 -3 -4 0 687.23 20.10 -3 -4 0 680.93 20.20 -3 -4 0 672.43 20.40 -3 -4 0 677.33 20.10 -3 -4 0 677.13 20.20 -3 -4 0 686.93 20.20 3 4 0 686.23 20.30 3 4 0 654.73 20.60 3 4 0 669.93 20.20 3 4 0 682.73 20.40 3 4 0 675.13 20.20 3 4 0 692.43 20.30 -4 -4 0 27.50 1.70 -4 -4 0 30.70 1.50 -4 -4 0 30.70 1.60 -4 -4 0 28.70 1.40 -4 -4 0 29.50 1.50 4 4 0 30.30 1.60 4 4 0 31.40 1.60 4 4 0 30.50 1.20 4 4 0 31.00 1.50 4 4 0 28.70 1.90 4 4 0 27.70 1.60 -5 -4 0 14.70 1.30 -5 -4 0 20.50 1.40 -5 -4 0 17.30 1.40 -5 -4 0 16.20 1.10 -5 -4 0 17.50 1.20 -5 -4 0 18.60 1.50 5 4 0 15.40 1.40 5 4 0 17.20 1.30 5 4 0 14.00 1.30 5 4 0 16.50 0.90 5 4 0 15.70 1.30 5 4 0 18.10 1.30 -6 -4 0 9.70 1.30 -6 -4 0 10.10 1.30 -6 -4 0 10.10 1.10 -6 -4 0 10.20 1.00 -6 -4 0 9.50 1.30 -6 -4 0 8.60 1.10 6 4 0 10.00 0.90 6 4 0 10.20 1.20 6 4 0 10.00 1.20 6 4 0 9.90 1.20 6 4 0 10.10 1.50 -7 -4 0 3.70 1.00 -7 -4 0 3.80 0.80 -7 -4 0 4.80 1.00 -7 -4 0 2.40 0.90 7 4 0 4.70 0.90 7 4 0 2.30 0.90 7 4 0 4.10 0.70 7 4 0 4.50 1.00 7 4 0 4.20 1.20 -8 -4 0 0.50 0.60 -8 -4 0 1.90 0.80 -8 -4 0 1.50 0.80 -8 -4 0 -0.90 0.70 8 4 0 0.60 0.90 8 4 0 0.50 0.70 8 4 0 0.60 0.80 8 4 0 1.00 1.00 -9 -4 0 -0.70 0.60 -9 -4 0 0.00 1.00 -9 -4 0 0.40 0.90 9 4 0 0.80 0.70 9 4 0 1.10 0.90 9 4 0 -0.60 0.90 9 4 0 1.30 0.90 -10 -4 0 -0.10 0.80 -10 -4 0 1.70 1.00 -10 -4 0 1.10 1.00 10 4 0 2.80 1.20 10 4 0 0.30 1.00 10 4 0 1.40 1.20 10 4 0 1.00 0.80 -11 -4 0 -2.40 1.00 -11 -4 0 0.10 1.00 -11 -4 0 1.80 1.00 11 4 0 0.60 1.10 11 4 0 -1.60 0.90 11 4 0 -0.80 0.80 11 4 0 0.40 1.10 -12 -4 0 1.20 1.10 -12 -4 0 -3.00 1.80 -12 -4 0 -0.70 1.00 12 4 0 0.60 0.80 12 4 0 -0.80 1.00 12 4 0 0.00 1.00 13 -5 0 12.10 2.30 13 -5 0 16.30 2.20 -13 5 0 12.60 2.10 -13 5 0 7.20 1.90 -13 5 0 8.30 2.20 12 -5 0 4.60 1.30 12 -5 0 4.90 1.50 -12 5 0 2.10 1.40 -12 5 0 1.30 1.30 -12 5 0 4.70 1.40 -12 5 0 3.60 1.40 11 -5 0 10.50 1.60 11 -5 0 9.40 1.90 -11 5 0 8.70 1.50 -11 5 0 6.40 1.60 -11 5 0 7.50 1.30 -11 5 0 7.00 1.60 -11 5 0 6.00 1.60 -11 5 0 7.20 1.30 -11 5 0 11.20 1.80 10 -5 0 7.20 1.30 10 -5 0 6.70 1.50 10 -5 0 5.90 0.90 -10 5 0 6.70 1.20 -10 5 0 6.40 1.10 -10 5 0 6.60 1.30 -10 5 0 4.40 1.30 -10 5 0 6.50 1.40 -10 5 0 5.80 1.40 -10 5 0 6.50 1.40 9 -5 0 -0.50 0.60 9 -5 0 -0.30 0.80 9 -5 0 0.50 0.40 9 -5 0 0.60 0.40 -9 5 0 0.10 0.70 -9 5 0 -0.40 0.80 -9 5 0 0.50 0.80 -9 5 0 0.40 0.70 -9 5 0 0.20 0.60 -9 5 0 -1.40 0.60 -9 5 0 0.10 0.80 -9 5 0 0.00 0.50 8 -5 0 51.59 2.60 8 -5 0 49.90 2.30 8 -5 0 55.09 3.10 8 -5 0 53.39 2.30 -8 5 0 53.59 2.80 -8 5 0 54.29 3.20 -8 5 0 57.09 2.60 -8 5 0 56.99 3.50 -8 5 0 54.29 2.70 -8 5 0 54.59 2.30 -8 5 0 51.39 2.40 -8 5 0 54.69 3.10 7 -5 0 18.00 1.90 7 -5 0 18.40 1.40 7 -5 0 19.10 1.20 7 -5 0 19.30 1.20 -7 5 0 18.90 1.80 -7 5 0 17.30 1.30 -7 5 0 19.10 1.60 -7 5 0 17.70 1.30 -7 5 0 13.50 1.70 -7 5 0 18.70 1.50 -7 5 0 18.60 1.70 6 -5 0 27.60 1.50 6 -5 0 27.90 1.60 6 -5 0 27.90 1.40 6 -5 0 23.80 1.90 6 -5 0 25.10 1.40 -6 5 0 27.30 1.50 -6 5 0 26.30 1.40 -6 5 0 28.20 1.60 -6 5 0 26.20 1.60 -6 5 0 26.30 1.70 -6 5 0 28.80 2.10 -6 5 0 25.80 1.80 -6 5 0 26.80 2.10 5 -5 0 0.70 0.40 5 -5 0 0.40 0.40 5 -5 0 0.70 0.40 5 -5 0 0.80 0.40 5 -5 0 1.30 0.70 5 -5 0 0.90 0.60 -5 5 0 0.70 0.60 -5 5 0 0.80 0.60 -5 5 0 -0.10 0.40 -5 5 0 0.50 0.30 -5 5 0 0.50 0.40 -5 5 0 1.00 0.40 -5 5 0 0.30 0.60 -5 5 0 0.30 0.50 4 -5 0 16.00 0.90 4 -5 0 15.10 0.90 4 -5 0 15.30 1.00 4 -5 0 13.80 1.30 4 -5 0 15.20 1.30 -4 5 0 15.00 1.20 -4 5 0 13.40 1.00 -4 5 0 14.20 0.90 -4 5 0 14.80 0.90 -4 5 0 16.20 1.50 -4 5 0 15.60 0.90 -4 5 0 13.90 0.90 -4 5 0 13.80 1.30 3 -5 0 4.40 0.50 3 -5 0 3.80 0.70 3 -5 0 3.80 0.50 3 -5 0 3.10 0.40 3 -5 0 3.80 0.70 3 -5 0 3.10 0.50 -3 5 0 3.70 0.40 -3 5 0 2.50 0.70 -3 5 0 3.50 0.50 -3 5 0 2.90 0.50 -3 5 0 3.00 0.40 -3 5 0 3.40 0.40 -3 5 0 2.60 0.50 -3 5 0 3.50 0.50 -3 5 0 3.10 0.70 2 -5 0 0.40 0.40 2 -5 0 0.70 0.40 2 -5 0 0.80 0.40 2 -5 0 1.40 0.30 2 -5 0 1.00 0.30 -2 5 0 0.80 0.30 -2 5 0 0.80 0.50 -2 5 0 0.90 0.30 -2 5 0 1.30 0.40 -2 5 0 1.30 0.20 -2 5 0 1.20 0.50 -2 5 0 0.70 0.30 -2 5 0 0.70 0.30 1 -5 0 2.10 0.20 1 -5 0 2.20 0.50 1 -5 0 2.10 0.20 1 -5 0 1.80 0.50 1 -5 0 1.30 0.40 -1 5 0 1.70 0.30 -1 5 0 1.30 0.40 -1 5 0 2.00 0.20 -1 5 0 1.40 0.50 -1 5 0 2.00 0.40 -1 5 0 1.10 0.40 -1 5 0 1.40 0.30 -1 5 0 1.80 0.20 0 -5 0 15.90 1.00 0 -5 0 15.90 0.70 0 -5 0 16.80 1.00 0 -5 0 16.30 0.90 0 -5 0 16.50 1.10 0 5 0 16.50 1.10 0 5 0 16.60 0.70 0 5 0 18.80 1.00 0 5 0 16.00 0.70 0 5 0 13.80 1.10 0 5 0 15.60 0.80 0 5 0 16.40 0.70 0 5 0 16.40 0.70 -1 -5 0 23.60 1.00 -1 -5 0 23.00 1.30 -1 -5 0 21.10 1.30 -1 -5 0 23.40 1.00 -1 -5 0 24.20 1.00 -1 -5 0 22.30 1.20 1 5 0 22.30 0.90 1 5 0 21.50 1.20 1 5 0 22.20 1.00 1 5 0 20.90 1.50 1 5 0 23.60 1.20 1 5 0 23.40 1.00 1 5 0 23.80 1.00 1 5 0 24.10 1.00 1 5 0 21.70 1.00 1 5 0 24.50 1.00 -2 -5 0 115.99 4.20 -2 -5 0 117.39 3.80 -2 -5 0 115.59 4.10 -2 -5 0 113.29 3.80 -2 -5 0 119.29 4.00 -2 -5 0 127.49 3.90 2 5 0 117.79 3.80 2 5 0 116.79 3.90 2 5 0 116.19 4.40 2 5 0 113.39 3.80 2 5 0 117.89 3.60 2 5 0 128.79 4.20 2 5 0 112.89 3.90 2 5 0 112.99 3.90 2 5 0 118.09 3.80 2 5 0 117.99 3.90 -3 -5 0 56.49 2.50 -3 -5 0 57.19 2.30 -3 -5 0 58.29 2.20 -3 -5 0 54.19 2.30 -3 -5 0 54.59 2.20 3 5 0 56.89 1.80 3 5 0 59.49 1.90 3 5 0 53.19 2.70 3 5 0 55.69 1.80 3 5 0 55.69 2.30 3 5 0 51.99 2.40 3 5 0 56.49 2.30 3 5 0 51.29 2.10 -4 -5 0 4.50 0.70 -4 -5 0 4.20 0.70 -4 -5 0 4.90 0.70 -4 -5 0 4.50 0.90 -4 -5 0 5.20 0.70 -4 -5 0 3.30 0.70 4 5 0 4.00 1.10 4 5 0 4.00 0.30 4 5 0 3.30 0.70 4 5 0 4.00 0.30 4 5 0 4.20 0.80 4 5 0 3.20 0.70 4 5 0 5.30 0.70 4 5 0 4.80 0.80 -5 -5 0 12.50 1.40 -5 -5 0 10.10 1.10 -5 -5 0 12.50 1.10 -5 -5 0 10.30 1.20 -5 -5 0 11.30 1.00 5 5 0 12.30 1.20 5 5 0 11.30 1.10 5 5 0 10.90 1.60 5 5 0 11.80 1.30 5 5 0 12.60 0.70 5 5 0 11.00 1.30 -6 -5 0 63.29 3.00 -6 -5 0 59.99 2.50 -6 -5 0 56.39 2.80 -6 -5 0 55.49 2.70 6 5 0 60.79 3.20 6 5 0 62.69 2.80 6 5 0 60.49 2.20 6 5 0 63.49 3.00 6 5 0 58.39 2.90 -7 -5 0 -0.50 0.60 -7 -5 0 0.40 0.50 -7 -5 0 -0.90 0.60 7 5 0 -0.10 0.70 7 5 0 0.60 0.70 7 5 0 0.60 0.80 7 5 0 1.50 1.10 -8 -5 0 2.40 1.00 -8 -5 0 3.00 1.10 -8 -5 0 3.50 1.00 8 5 0 1.80 1.00 8 5 0 4.20 1.10 8 5 0 2.30 0.90 8 5 0 3.90 1.30 -9 -5 0 0.20 0.70 -9 -5 0 1.30 1.10 -9 -5 0 0.80 0.90 9 5 0 3.40 1.10 9 5 0 0.10 0.80 9 5 0 0.30 0.80 9 5 0 0.90 1.10 -10 -5 0 1.50 1.00 -10 -5 0 0.20 0.90 10 5 0 -0.60 0.70 10 5 0 -1.40 0.90 10 5 0 1.60 1.10 10 5 0 0.10 1.30 -11 -5 0 2.30 1.20 -11 -5 0 2.20 1.10 11 5 0 0.90 1.10 11 5 0 0.00 1.00 11 5 0 1.70 1.30 11 5 0 0.40 1.20 12 -6 0 3.10 1.30 12 -6 0 3.10 1.50 -12 6 0 4.10 1.40 -12 6 0 1.30 1.50 -12 6 0 5.80 1.50 -12 6 0 4.20 1.60 11 -6 0 0.90 1.10 11 -6 0 0.70 0.90 -11 6 0 -0.20 0.90 -11 6 0 0.40 1.20 -11 6 0 0.50 0.90 -11 6 0 0.70 1.10 -11 6 0 3.10 1.20 10 -6 0 12.60 2.00 10 -6 0 16.40 1.80 -10 6 0 12.70 2.00 -10 6 0 14.50 1.80 -10 6 0 12.30 1.80 -10 6 0 19.00 2.10 -10 6 0 14.10 1.60 -10 6 0 14.00 1.50 -10 6 0 10.80 1.80 9 -6 0 7.10 0.90 9 -6 0 9.60 1.70 9 -6 0 8.30 1.20 -9 6 0 5.90 0.90 -9 6 0 6.70 1.30 -9 6 0 6.10 1.00 -9 6 0 5.80 1.00 -9 6 0 3.70 1.00 -9 6 0 6.10 1.30 -9 6 0 3.10 1.10 -9 6 0 5.10 1.40 8 -6 0 37.90 1.90 8 -6 0 32.50 2.50 8 -6 0 34.80 2.10 -8 6 0 36.40 2.70 -8 6 0 37.10 2.90 -8 6 0 37.10 2.00 -8 6 0 39.50 2.30 -8 6 0 38.00 2.40 -8 6 0 40.20 2.60 -8 6 0 39.20 2.10 7 -6 0 74.89 3.80 7 -6 0 77.39 3.10 7 -6 0 72.99 3.20 -7 6 0 77.19 3.70 -7 6 0 79.69 3.00 -7 6 0 80.49 3.50 -7 6 0 86.49 4.10 -7 6 0 78.99 3.10 -7 6 0 73.49 3.30 -7 6 0 76.99 4.20 6 -6 0 3.80 1.10 6 -6 0 5.40 0.80 6 -6 0 2.30 0.50 -6 6 0 2.60 0.80 -6 6 0 3.10 0.60 -6 6 0 1.40 0.80 -6 6 0 2.70 0.70 -6 6 0 2.50 0.70 -6 6 0 2.00 0.80 -6 6 0 3.40 0.60 -6 6 0 1.80 0.90 5 -6 0 102.89 3.60 5 -6 0 98.39 4.20 5 -6 0 99.69 3.80 -5 6 0 99.99 4.10 -5 6 0 100.39 3.70 -5 6 0 97.49 3.70 -5 6 0 105.29 3.50 -5 6 0 104.19 3.70 -5 6 0 97.69 4.50 -5 6 0 98.39 3.60 -5 6 0 102.39 4.40 4 -6 0 0.70 0.50 4 -6 0 1.70 0.40 4 -6 0 0.40 0.70 -4 6 0 1.20 0.40 -4 6 0 1.80 0.70 -4 6 0 1.50 0.40 -4 6 0 0.80 0.40 -4 6 0 0.30 0.60 -4 6 0 1.40 0.60 -4 6 0 0.50 0.40 -4 6 0 1.30 0.50 3 -6 0 26.20 1.20 3 -6 0 26.60 1.50 3 -6 0 26.30 1.10 3 -6 0 26.70 1.70 3 -6 0 24.70 1.10 -3 6 0 29.60 1.90 -3 6 0 24.30 1.50 -3 6 0 24.40 1.20 -3 6 0 25.20 1.20 -3 6 0 24.60 1.20 -3 6 0 24.80 1.20 -3 6 0 26.50 1.20 -3 6 0 25.50 1.90 -3 6 0 27.20 1.10 2 -6 0 61.89 2.10 2 -6 0 63.09 2.70 2 -6 0 66.29 2.10 2 -6 0 66.29 2.10 2 -6 0 62.99 2.70 -2 6 0 61.79 2.40 -2 6 0 63.09 2.20 -2 6 0 63.29 3.00 -2 6 0 62.99 2.20 -2 6 0 65.19 2.20 -2 6 0 65.99 2.10 -2 6 0 66.19 2.60 -2 6 0 64.39 2.30 -2 6 0 64.99 2.90 1 -6 0 4.80 0.30 1 -6 0 5.60 0.80 1 -6 0 4.30 0.70 1 -6 0 4.00 0.30 1 -6 0 4.60 0.30 -1 6 0 3.70 0.50 -1 6 0 5.00 0.80 -1 6 0 4.00 0.60 -1 6 0 4.00 0.40 -1 6 0 4.40 0.40 -1 6 0 5.30 0.30 -1 6 0 3.80 0.70 -1 6 0 4.10 0.40 0 -6 0 42.10 1.90 0 -6 0 38.70 1.90 0 -6 0 40.10 1.90 0 -6 0 41.30 1.40 0 -6 0 43.00 1.80 0 6 0 42.30 1.40 0 6 0 43.50 1.40 0 6 0 39.10 2.00 0 6 0 41.40 1.40 0 6 0 43.00 1.60 0 6 0 41.10 2.00 0 6 0 40.10 1.50 -1 -6 0 0.10 0.40 -1 -6 0 0.70 0.50 -1 -6 0 0.90 0.30 -1 -6 0 0.20 0.20 -1 -6 0 0.10 0.50 -1 -6 0 0.60 0.30 1 6 0 0.30 0.80 1 6 0 0.70 0.30 1 6 0 0.40 0.30 1 6 0 0.50 0.40 1 6 0 0.70 0.40 1 6 0 0.70 0.40 1 6 0 0.80 0.30 1 6 0 0.50 0.20 -2 -6 0 1.00 0.50 -2 -6 0 1.80 0.60 -2 -6 0 2.00 0.40 -2 -6 0 1.40 0.40 -2 -6 0 0.80 0.60 2 6 0 2.20 0.30 2 6 0 1.70 0.90 2 6 0 1.50 0.40 2 6 0 1.70 0.50 2 6 0 1.70 0.40 2 6 0 1.20 0.50 2 6 0 3.20 0.50 2 6 0 1.30 0.40 -3 -6 0 0.90 0.60 -3 -6 0 1.00 0.40 -3 -6 0 2.10 0.50 -3 -6 0 1.90 0.60 -3 -6 0 2.60 0.80 3 6 0 0.80 0.40 3 6 0 1.40 0.50 3 6 0 1.30 0.30 3 6 0 2.40 0.60 3 6 0 1.40 1.10 3 6 0 2.40 0.80 3 6 0 1.80 0.40 -4 -6 0 36.00 1.90 -4 -6 0 34.10 1.70 -4 -6 0 33.10 1.70 -4 -6 0 37.10 1.80 -4 -6 0 32.50 2.00 4 6 0 30.20 2.30 4 6 0 35.00 2.00 4 6 0 31.90 1.80 4 6 0 38.70 1.90 4 6 0 33.10 1.70 -5 -6 0 28.20 1.80 -5 -6 0 30.90 2.00 -5 -6 0 28.20 1.70 -5 -6 0 27.40 1.50 5 6 0 28.80 2.30 5 6 0 29.20 1.90 5 6 0 26.20 1.70 5 6 0 30.70 2.00 -6 -6 0 2.60 0.80 -6 -6 0 6.30 0.80 -6 -6 0 4.60 1.10 6 6 0 5.00 1.40 6 6 0 6.90 1.20 6 6 0 4.80 1.00 6 6 0 4.60 0.90 -7 -6 0 1.00 0.90 -7 -6 0 1.70 0.80 7 6 0 4.10 1.00 7 6 0 1.50 1.20 7 6 0 1.90 0.90 7 6 0 1.50 0.80 -8 -6 0 0.90 0.70 -8 -6 0 0.40 0.90 8 6 0 1.30 0.90 8 6 0 0.70 0.90 8 6 0 2.50 1.30 8 6 0 -0.40 0.70 -9 -6 0 1.10 0.90 -9 -6 0 0.10 0.90 9 6 0 0.90 1.20 9 6 0 -0.80 0.90 9 6 0 -0.40 0.80 9 6 0 0.70 0.80 -10 -6 0 0.70 1.10 -10 -6 0 -1.10 0.80 10 6 0 -0.70 1.00 10 6 0 2.10 1.40 10 6 0 -0.50 0.80 10 6 0 -0.40 1.00 -11 -6 0 0.60 0.90 -11 -6 0 -1.10 1.00 11 6 0 2.20 1.40 11 6 0 2.60 1.40 11 6 0 -1.20 0.90 11 6 0 0.50 1.00 12 -7 0 0.60 1.30 -12 7 0 2.50 1.20 -12 7 0 -1.80 1.20 -12 7 0 -0.50 1.00 -12 7 0 -1.40 1.10 11 -7 0 13.30 2.20 -11 7 0 10.40 2.10 -11 7 0 16.50 2.10 -11 7 0 10.80 1.90 -11 7 0 11.80 1.80 10 -7 0 1.60 1.10 -10 7 0 0.50 0.80 -10 7 0 0.00 0.80 -10 7 0 -0.10 0.90 -10 7 0 -0.90 0.90 -10 7 0 1.30 1.00 9 -7 0 19.60 2.40 9 -7 0 16.60 1.40 -9 7 0 17.30 1.60 -9 7 0 18.60 2.10 -9 7 0 18.70 1.80 -9 7 0 14.50 2.10 -9 7 0 20.50 1.80 -9 7 0 13.50 2.00 -9 7 0 23.40 2.10 8 -7 0 4.20 1.30 8 -7 0 4.20 0.80 -8 7 0 3.60 1.10 -8 7 0 2.40 1.10 -8 7 0 3.90 0.80 -8 7 0 2.60 0.90 -8 7 0 2.70 0.80 -8 7 0 3.50 1.00 -8 7 0 2.80 0.90 7 -7 0 -0.10 0.80 7 -7 0 1.10 0.60 -7 7 0 1.10 0.60 -7 7 0 0.40 0.50 -7 7 0 0.20 0.80 -7 7 0 1.40 0.80 -7 7 0 -0.70 0.70 -7 7 0 0.80 0.70 -7 7 0 1.10 0.50 6 -7 0 5.60 0.90 6 -7 0 6.00 0.80 6 -7 0 5.10 1.20 -6 7 0 6.70 0.80 -6 7 0 6.70 1.30 -6 7 0 3.70 1.10 -6 7 0 5.90 1.10 -6 7 0 5.00 0.90 -6 7 0 5.40 0.80 -6 7 0 5.20 0.80 5 -7 0 35.00 2.30 5 -7 0 35.30 1.60 5 -7 0 31.80 1.90 -5 7 0 33.10 1.70 -5 7 0 32.70 1.60 -5 7 0 38.90 2.50 -5 7 0 35.00 1.60 -5 7 0 30.50 2.40 -5 7 0 34.40 2.10 -5 7 0 32.70 1.80 -5 7 0 35.70 1.70 4 -7 0 16.00 1.70 4 -7 0 15.30 1.20 4 -7 0 14.90 1.00 4 -7 0 14.70 1.00 -4 7 0 15.80 1.00 -4 7 0 13.10 1.10 -4 7 0 15.70 1.00 -4 7 0 12.10 1.50 -4 7 0 15.00 1.30 -4 7 0 12.60 1.50 -4 7 0 14.00 0.90 -4 7 0 14.90 1.00 3 -7 0 0.30 0.30 3 -7 0 0.40 0.50 3 -7 0 0.50 0.30 3 -7 0 -0.40 0.60 3 -7 0 -0.10 0.30 -3 7 0 0.60 0.40 -3 7 0 0.30 0.50 -3 7 0 0.40 0.30 -3 7 0 0.00 0.30 -3 7 0 0.40 0.30 -3 7 0 -0.10 0.60 -3 7 0 -0.20 0.60 -3 7 0 -0.30 0.40 2 -7 0 23.10 1.50 2 -7 0 22.00 1.50 2 -7 0 23.40 0.90 2 -7 0 23.10 0.90 2 -7 0 22.50 0.90 -2 7 0 25.60 1.80 -2 7 0 21.10 1.20 -2 7 0 22.30 1.10 -2 7 0 23.50 1.80 -2 7 0 23.00 1.40 -2 7 0 22.40 0.90 -2 7 0 23.00 1.10 -2 7 0 23.30 0.90 -2 7 0 22.90 1.20 1 -7 0 30.00 1.70 1 -7 0 31.60 1.00 1 -7 0 31.10 1.70 1 -7 0 31.60 1.10 -1 7 0 30.60 1.30 -1 7 0 31.90 1.40 -1 7 0 33.00 1.70 -1 7 0 32.80 1.00 -1 7 0 31.60 1.50 -1 7 0 32.60 1.00 -1 7 0 33.70 2.10 -1 7 0 32.20 1.10 -1 7 0 31.40 1.90 0 -7 0 0.60 0.50 0 -7 0 0.40 0.20 0 -7 0 0.50 0.50 0 -7 0 -0.10 0.20 0 -7 0 0.40 0.20 0 -7 0 -0.10 0.60 0 -7 0 -0.10 0.50 0 7 0 0.10 0.50 0 7 0 0.50 0.30 0 7 0 0.10 0.40 0 7 0 0.20 0.40 0 7 0 0.20 0.20 0 7 0 -0.20 0.50 -1 -7 0 6.20 0.60 -1 -7 0 6.20 0.90 -1 -7 0 5.60 0.90 -1 -7 0 7.10 1.00 -1 -7 0 6.30 0.50 -1 -7 0 6.00 0.50 1 7 0 6.20 0.80 1 7 0 5.40 0.60 1 7 0 7.40 0.60 1 7 0 5.70 0.60 1 7 0 5.60 1.30 1 7 0 6.20 0.50 1 7 0 5.20 0.80 -2 -7 0 33.50 1.90 -2 -7 0 34.10 1.90 -2 -7 0 35.40 1.50 -2 -7 0 34.10 2.00 -2 -7 0 36.60 1.50 2 7 0 35.80 2.40 2 7 0 34.30 1.80 2 7 0 35.20 1.50 2 7 0 37.60 1.80 2 7 0 36.30 1.70 2 7 0 36.60 1.70 -3 -7 0 15.00 1.20 -3 -7 0 15.70 1.10 -3 -7 0 13.80 1.30 -3 -7 0 14.90 1.00 -3 -7 0 13.00 1.50 3 7 0 14.40 1.00 3 7 0 12.00 1.40 3 7 0 14.40 1.10 3 7 0 13.00 1.10 3 7 0 14.50 1.00 3 7 0 17.00 2.00 3 7 0 14.60 1.00 -4 -7 0 83.09 3.20 -4 -7 0 79.39 3.60 -4 -7 0 81.89 3.20 -4 -7 0 81.99 3.10 -4 -7 0 71.79 3.20 4 7 0 83.59 3.30 4 7 0 77.59 3.10 4 7 0 77.29 3.30 4 7 0 82.49 4.00 4 7 0 80.89 3.60 -5 -7 0 3.10 0.70 -5 -7 0 3.20 0.70 -5 -7 0 3.90 1.00 5 7 0 3.70 1.40 5 7 0 3.20 0.80 5 7 0 3.20 0.80 5 7 0 4.60 1.10 -6 -7 0 3.50 0.70 -6 -7 0 3.10 0.80 -6 -7 0 3.90 1.10 6 7 0 1.60 1.30 6 7 0 2.00 0.90 6 7 0 4.10 0.90 6 7 0 2.80 1.00 -7 -7 0 2.50 0.80 -7 -7 0 2.10 1.00 7 7 0 2.10 1.30 7 7 0 1.80 1.00 7 7 0 2.10 0.90 7 7 0 1.10 0.90 -8 -7 0 -0.10 1.00 -8 -7 0 -0.20 0.70 8 7 0 -0.40 0.80 8 7 0 0.00 0.80 8 7 0 1.20 1.30 8 7 0 0.70 0.90 -9 -7 0 0.30 1.00 -9 -7 0 0.20 0.70 9 7 0 0.50 0.90 9 7 0 -0.10 0.90 9 7 0 1.50 1.40 9 7 0 -0.10 0.80 -10 -7 0 0.70 1.10 -10 -7 0 0.30 0.90 10 7 0 1.30 1.40 10 7 0 -0.20 1.10 10 7 0 0.90 1.20 10 7 0 -2.20 0.90 12 -8 0 4.20 1.70 -12 8 0 5.90 1.80 -12 8 0 1.10 1.50 -12 8 0 8.30 1.60 -12 8 0 1.50 1.20 11 -8 0 5.40 1.60 -11 8 0 5.70 1.40 -11 8 0 5.40 1.50 -11 8 0 3.30 1.50 -11 8 0 2.90 1.70 10 -8 0 2.70 1.30 -10 8 0 0.30 1.10 -10 8 0 1.60 1.30 -10 8 0 1.70 1.00 -10 8 0 1.30 1.00 9 -8 0 1.10 1.00 9 -8 0 0.20 0.60 -9 8 0 0.60 0.80 -9 8 0 -1.10 0.90 -9 8 0 -1.50 0.60 -9 8 0 -0.60 0.80 8 -8 0 2.40 1.20 8 -8 0 0.70 0.60 -8 8 0 0.60 0.70 -8 8 0 -0.40 0.60 -8 8 0 1.80 0.90 -8 8 0 0.10 0.90 -8 8 0 -0.20 0.90 -8 8 0 0.60 0.90 7 -8 0 -0.90 0.70 7 -8 0 -0.50 0.50 -7 8 0 -0.10 0.80 -7 8 0 -0.70 0.80 -7 8 0 0.00 0.40 -7 8 0 0.60 0.80 -7 8 0 0.00 0.50 -7 8 0 -0.20 0.60 -7 8 0 0.30 0.50 6 -8 0 78.19 3.10 6 -8 0 76.49 3.40 6 -8 0 71.29 3.80 -6 8 0 83.29 4.20 -6 8 0 82.19 3.00 -6 8 0 78.89 3.70 -6 8 0 79.59 3.20 -6 8 0 77.39 3.30 -6 8 0 81.09 3.10 -6 8 0 78.39 4.40 5 -8 0 13.00 1.30 5 -8 0 13.00 1.10 5 -8 0 15.50 1.00 5 -8 0 16.00 1.80 -5 8 0 15.10 1.10 -5 8 0 11.00 1.60 -5 8 0 10.80 1.30 -5 8 0 13.40 1.10 -5 8 0 9.60 1.50 -5 8 0 13.40 1.00 -5 8 0 13.40 1.10 -5 8 0 13.80 1.20 4 -8 0 60.29 2.30 4 -8 0 64.39 3.20 4 -8 0 62.89 2.90 -4 8 0 65.49 3.00 -4 8 0 60.59 3.40 -4 8 0 59.49 2.50 -4 8 0 62.29 3.60 -4 8 0 63.09 2.60 -4 8 0 63.49 2.40 -4 8 0 64.29 2.50 3 -8 0 43.70 2.40 3 -8 0 46.00 1.60 3 -8 0 41.40 2.20 -3 8 0 43.10 2.30 -3 8 0 41.70 1.90 -3 8 0 46.60 2.80 -3 8 0 43.10 1.80 -3 8 0 41.60 1.90 -3 8 0 43.30 1.60 -3 8 0 41.30 2.80 -3 8 0 44.20 1.90 2 -8 0 177.38 6.40 2 -8 0 181.28 6.40 2 -8 0 184.68 5.50 2 -8 0 181.68 5.40 2 -8 0 181.18 5.40 2 -8 0 181.48 5.40 -2 8 0 187.58 6.00 -2 8 0 180.48 5.80 -2 8 0 181.98 5.80 -2 8 0 180.98 5.50 -2 8 0 181.18 5.90 -2 8 0 180.48 6.30 -2 8 0 182.68 5.40 -2 8 0 186.38 7.00 -2 8 0 189.88 6.80 1 -8 0 73.09 3.30 1 -8 0 73.09 3.10 -1 8 0 77.39 3.60 -1 8 0 79.89 3.10 -1 8 0 79.09 2.80 -1 8 0 73.99 2.70 -1 8 0 78.29 3.00 -1 8 0 87.19 3.70 0 -8 0 89.29 2.80 0 -8 0 90.49 3.40 0 -8 0 91.49 2.80 0 -8 0 84.79 3.60 0 8 0 87.79 3.90 0 8 0 96.89 3.80 0 8 0 86.19 3.10 0 8 0 87.89 2.70 0 8 0 93.19 3.50 0 8 0 88.69 3.10 0 8 0 92.79 3.40 0 8 0 91.69 4.10 -1 -8 0 3.50 0.40 -1 -8 0 4.20 1.00 -1 -8 0 3.40 0.80 -1 -8 0 3.40 0.90 1 8 0 2.70 1.30 1 8 0 3.40 0.40 1 8 0 2.80 0.50 1 8 0 2.80 0.70 1 8 0 2.70 0.60 1 8 0 3.60 0.70 -2 -8 0 6.20 0.60 -2 -8 0 6.20 1.00 -2 -8 0 7.70 1.20 -2 -8 0 7.00 1.00 2 8 0 5.60 0.80 2 8 0 6.00 0.80 2 8 0 5.80 0.80 2 8 0 6.00 1.40 2 8 0 6.80 0.60 2 8 0 5.30 0.80 -3 -8 0 17.60 1.10 -3 -8 0 19.20 1.40 -3 -8 0 18.60 1.50 -3 -8 0 15.20 1.60 3 8 0 16.50 1.30 3 8 0 15.70 1.60 3 8 0 17.90 1.10 3 8 0 16.80 1.30 3 8 0 17.90 2.10 3 8 0 18.00 1.20 -4 -8 0 1.40 0.70 -4 -8 0 0.50 0.60 -4 -8 0 1.70 0.80 -4 -8 0 0.50 0.50 4 8 0 0.80 0.60 4 8 0 0.60 0.80 4 8 0 0.80 1.20 4 8 0 0.70 0.50 -5 -8 0 0.50 0.60 -5 -8 0 -0.80 0.70 -5 -8 0 -0.50 0.50 5 8 0 0.10 0.60 5 8 0 -0.20 0.60 5 8 0 1.00 1.20 5 8 0 0.10 0.80 -6 -8 0 4.70 1.20 -6 -8 0 4.80 0.90 6 8 0 3.40 1.00 6 8 0 4.90 1.00 6 8 0 2.90 1.10 6 8 0 5.10 1.80 -7 -8 0 0.60 1.00 -7 -8 0 0.50 0.70 7 8 0 -1.50 1.20 7 8 0 0.60 0.80 7 8 0 -0.50 0.70 7 8 0 0.00 1.00 -8 -8 0 0.00 0.70 -8 -8 0 -0.80 0.90 8 8 0 -0.90 0.80 8 8 0 -0.10 0.80 8 8 0 -0.10 0.90 8 8 0 0.40 1.40 -9 -8 0 2.10 1.40 -9 -8 0 2.10 1.50 9 8 0 2.90 1.30 9 8 0 3.30 1.30 9 8 0 2.00 1.50 11 -9 0 19.70 2.90 -11 9 0 23.50 2.50 -11 9 0 19.00 2.90 -11 9 0 16.70 2.40 10 -9 0 27.00 3.10 -10 9 0 19.90 2.40 -10 9 0 17.50 2.70 -10 9 0 26.40 2.40 9 -9 0 1.40 0.80 9 -9 0 0.90 1.10 -9 9 0 3.60 1.10 -9 9 0 0.80 0.90 -9 9 0 1.30 1.10 -9 9 0 1.90 1.20 8 -9 0 5.30 1.00 8 -9 0 8.00 1.70 -8 9 0 7.10 1.30 -8 9 0 5.80 1.50 -8 9 0 5.90 1.10 -8 9 0 4.40 1.20 7 -9 0 0.50 0.90 7 -9 0 -0.90 0.50 -7 9 0 -0.70 0.60 -7 9 0 0.80 0.70 -7 9 0 -0.50 0.50 -7 9 0 0.10 0.90 -7 9 0 -1.20 0.80 6 -9 0 0.60 0.70 6 -9 0 1.30 0.90 6 -9 0 0.40 0.50 -6 9 0 -0.20 0.60 -6 9 0 0.10 0.80 -6 9 0 -0.40 0.60 -6 9 0 0.40 0.50 -6 9 0 1.30 1.00 -6 9 0 -0.20 0.40 5 -9 0 -0.20 0.60 5 -9 0 1.00 0.90 5 -9 0 0.10 0.40 -5 9 0 -0.70 0.50 -5 9 0 0.20 0.80 -5 9 0 -0.70 0.70 -5 9 0 -0.20 0.50 -5 9 0 0.20 0.40 -5 9 0 0.30 0.40 4 -9 0 7.00 1.30 4 -9 0 8.20 1.10 4 -9 0 5.70 1.00 -4 9 0 7.80 0.80 -4 9 0 5.60 1.30 -4 9 0 7.90 0.90 -4 9 0 7.10 0.80 -4 9 0 6.90 1.00 -4 9 0 6.40 1.30 -4 9 0 8.20 0.80 3 -9 0 5.40 1.00 3 -9 0 5.80 1.10 -3 9 0 5.00 0.70 -3 9 0 5.70 0.80 -3 9 0 5.60 0.90 -3 9 0 5.20 0.70 -3 9 0 5.50 0.80 -3 9 0 4.50 1.10 -3 9 0 3.70 1.10 2 -9 0 0.30 0.60 2 -9 0 0.30 0.70 -2 9 0 -0.30 0.70 -2 9 0 -0.90 0.70 -2 9 0 -0.30 0.40 -2 9 0 0.00 0.30 -2 9 0 -0.20 0.40 -2 9 0 0.30 0.40 -2 9 0 -0.40 0.40 1 -9 0 1.90 0.70 1 -9 0 1.30 0.70 -1 9 0 1.00 0.70 -1 9 0 2.20 0.60 -1 9 0 1.10 0.40 -1 9 0 1.10 0.50 -1 9 0 1.50 0.50 -1 9 0 1.00 0.80 0 -9 0 8.80 1.20 0 -9 0 7.40 1.00 0 9 0 9.40 1.00 0 9 0 11.20 1.80 0 9 0 7.50 0.90 0 9 0 8.30 1.20 0 9 0 7.70 0.70 0 9 0 7.30 1.10 0 9 0 9.60 0.90 -1 -9 0 31.10 1.90 -1 -9 0 30.60 2.00 1 9 0 29.70 1.50 1 9 0 29.70 2.40 1 9 0 31.80 2.00 1 9 0 33.00 1.80 1 9 0 32.80 1.60 1 9 0 29.70 2.00 -2 -9 0 1.60 0.80 -2 -9 0 1.20 0.70 -2 -9 0 0.90 0.70 2 9 0 0.10 0.50 2 9 0 1.30 0.50 2 9 0 0.20 1.10 2 9 0 0.90 0.60 2 9 0 0.50 0.50 -3 -9 0 9.80 1.30 -3 -9 0 9.50 1.20 -3 -9 0 8.10 1.30 3 9 0 9.00 1.40 3 9 0 6.80 1.70 3 9 0 7.80 1.00 -4 -9 0 2.80 0.80 -4 -9 0 1.70 0.80 -4 -9 0 1.40 0.90 4 9 0 0.90 0.70 4 9 0 1.70 1.00 4 9 0 2.40 1.50 -5 -9 0 0.20 0.80 5 9 0 0.80 0.70 5 9 0 0.30 0.90 5 9 0 1.60 1.30 -6 -9 0 0.60 1.00 6 9 0 -0.90 0.90 6 9 0 1.30 1.50 6 9 0 0.20 0.70 -7 -9 0 0.20 0.90 7 9 0 0.80 1.00 7 9 0 0.30 1.30 7 9 0 0.30 1.10 -8 -9 0 -0.20 0.90 8 9 0 1.30 1.60 8 9 0 0.30 1.00 8 9 0 1.90 1.20 11 -10 0 0.60 1.20 -11 10 0 1.50 1.10 -11 10 0 -0.60 1.40 -11 10 0 -1.80 1.10 10 -10 0 41.10 3.40 -10 10 0 42.00 3.40 -10 10 0 41.40 2.90 -10 10 0 30.30 3.60 9 -10 0 7.20 1.80 9 -10 0 8.80 1.30 -9 10 0 11.70 1.70 -9 10 0 8.60 2.10 -9 10 0 9.20 1.90 8 -10 0 13.00 2.10 8 -10 0 6.90 1.20 -8 10 0 8.40 1.40 -8 10 0 8.00 1.50 -8 10 0 6.20 1.70 7 -10 0 17.20 1.80 7 -10 0 16.80 2.20 -7 10 0 17.70 1.90 -7 10 0 16.80 2.30 -7 10 0 16.80 1.70 6 -10 0 2.80 0.90 6 -10 0 2.20 1.10 -6 10 0 2.00 0.80 -6 10 0 1.90 0.80 -6 10 0 2.00 1.10 -6 10 0 1.70 1.20 5 -10 0 19.80 2.10 5 -10 0 14.50 1.60 -5 10 0 15.20 1.30 -5 10 0 14.60 2.00 -5 10 0 19.20 1.70 -5 10 0 14.80 2.00 4 -10 0 12.60 1.50 4 -10 0 14.50 1.80 -4 10 0 13.70 1.10 -4 10 0 11.50 1.70 -4 10 0 12.40 1.20 -4 10 0 13.70 1.50 -4 10 0 13.50 1.90 3 -10 0 9.60 1.30 3 -10 0 9.40 1.40 -3 10 0 9.60 0.90 -3 10 0 8.00 0.90 -3 10 0 6.70 1.40 -3 10 0 8.60 1.50 -3 10 0 8.20 1.10 -3 10 0 8.90 1.00 -3 10 0 9.80 1.00 2 -10 0 6.60 1.20 2 -10 0 9.50 1.30 -2 10 0 6.20 1.00 -2 10 0 8.60 1.30 -2 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2.60 6 0 -23 -0.30 1.50 6 0 -23 1.00 1.60 -6 0 23 -0.60 1.30 -6 0 23 2.50 1.70 5 0 -23 4.40 1.70 5 0 -23 4.10 1.90 -5 0 23 3.10 1.80 4 0 -23 0.20 1.60 4 0 -23 -0.50 1.20 -4 0 23 0.40 1.30 3 0 -23 0.30 1.30 3 0 -23 0.10 1.60 -3 0 23 1.50 1.50 2 0 -23 -0.20 1.20 2 0 -23 0.30 1.50 -2 0 23 0.70 1.40 1 0 -23 2.30 1.70 1 0 -23 0.80 1.40 6 -1 -23 1.00 1.70 6 -1 -23 -0.20 1.70 -6 1 23 -1.30 1.50 5 -1 -23 3.90 2.00 5 -1 -23 3.70 1.70 -5 1 23 5.70 2.00 -5 1 23 0.70 1.50 4 -1 -23 -0.40 1.40 4 -1 -23 0.40 1.70 -4 1 23 -0.30 1.30 3 -1 -23 -0.20 1.50 3 -1 -23 -0.50 1.60 -3 1 23 1.60 1.40 5 4 -24 2.20 1.40 4 4 -24 -1.90 1.20 4 4 -24 1.50 1.10 4 4 -24 -0.20 1.20 -4 -4 24 1.80 1.30 -4 -4 24 0.90 1.30 3 4 -24 0.50 1.10 3 4 -24 0.10 1.50 3 4 -24 0.30 1.30 -3 -4 24 -0.40 1.30 5 3 -24 4.70 1.70 5 3 -24 3.80 1.80 -5 -3 24 1.70 1.50 4 3 -24 0.90 1.40 4 3 -24 -1.60 0.80 4 3 -24 -0.90 1.50 -4 -3 24 0.10 1.40 -4 -3 24 1.30 1.30 3 3 -24 4.30 1.60 3 3 -24 6.60 2.10 3 3 -24 1.90 1.10 -3 -3 24 4.50 1.60 5 2 -24 4.00 1.80 5 2 -24 7.50 2.10 -5 -2 24 1.20 1.70 4 2 -24 -3.10 1.30 4 2 -24 -0.50 1.30 -4 -2 24 -1.10 1.20 3 2 -24 7.00 1.80 3 2 -24 4.30 2.00 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 80207 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL EL16_D584_DRX4_1_a.res in P-1 CELL 0.71073 9.6524 10.1168 16.6554 101.299 106.315 95.628 ZERR 2.00 0.0017 0.0017 0.0031 0.008 0.009 0.008 LATT 1 SFAC C H N S UNIT 72 52 12 4 MERG 2 OMIT 0 1 1 OMIT 0 0 1 SHEL 50 0.72 EQIV $1 x-1, y, z HTAB C19 N3_$1 HTAB C14 N6_$2 EQIV $2 x, 1+y, z FMAP 2 PLAN 10 ACTA BOND BOND $H L.S. 10 TEMP 23.00 WGHT 0.055900 0.350500 FVAR 0.35633 C1 1 0.170584 1.074107 0.260576 11.00000 0.04488 0.06726 = 0.07289 0.02613 0.02835 0.02994 AFIX 43 H1 2 0.096377 1.104564 0.281129 11.00000 -1.20000 AFIX 0 C2 1 0.175706 1.070465 0.180526 11.00000 0.04162 0.06829 = 0.06368 0.02882 0.01345 0.02656 AFIX 43 H2 2 0.104904 1.097904 0.139242 11.00000 -1.20000 AFIX 0 C3 1 0.299933 1.020580 0.165620 11.00000 0.04614 0.05189 = 0.04402 0.01883 0.01618 0.01863 AFIX 43 H3 2 0.320156 1.012035 0.113611 11.00000 -1.20000 AFIX 0 C4 1 0.387535 0.986096 0.236208 11.00000 0.03650 0.03544 = 0.04105 0.01326 0.01498 0.01349 C5 1 0.514633 0.920900 0.240907 11.00000 0.04145 0.04364 = 0.04016 0.01286 0.01783 0.01864 AFIX 43 H5 2 0.550838 0.907651 0.194250 11.00000 -1.20000 AFIX 0 C6 1 0.686519 0.800009 0.311746 11.00000 0.03527 0.03880 = 0.03502 0.01121 0.01206 0.01446 C7 1 0.675715 0.766109 0.455239 11.00000 0.04415 0.05554 = 0.04066 0.01363 0.02076 0.02224 AFIX 43 H7 2 0.615675 0.830849 0.462999 11.00000 -1.20000 AFIX 0 C8 1 0.720084 0.692628 0.514582 11.00000 0.04920 0.06617 = 0.04032 0.01958 0.02018 0.02031 AFIX 43 H8 2 0.690562 0.707130 0.563727 11.00000 -1.20000 AFIX 0 C9 1 0.811079 0.593781 0.502649 11.00000 0.04433 0.05926 = 0.04415 0.02536 0.01428 0.01804 AFIX 43 H9 2 0.839826 0.543065 0.543631 11.00000 -1.20000 AFIX 0 C10 1 0.856621 0.572504 0.431932 11.00000 0.03751 0.04906 = 0.04500 0.01883 0.01214 0.01860 AFIX 43 H10 2 0.917068 0.508006 0.424539 11.00000 -1.20000 AFIX 0 C11 1 0.811715 0.648815 0.369708 11.00000 0.03129 0.04059 = 0.03875 0.01232 0.01217 0.01435 C12 1 0.762672 0.737253 0.259173 11.00000 0.03359 0.03815 = 0.03623 0.01084 0.01181 0.01384 C13 1 0.768975 0.752790 0.174234 11.00000 0.03607 0.04332 = 0.03756 0.01283 0.01485 0.01551 C14 1 0.784546 0.879312 0.153750 11.00000 0.04751 0.04362 = 0.04864 0.01380 0.02076 0.01324 AFIX 43 H14 2 0.789693 0.958380 0.194582 11.00000 -1.20000 AFIX 0 C15 1 0.792415 0.888673 0.073633 11.00000 0.05834 0.05942 = 0.06184 0.03205 0.02890 0.01835 AFIX 43 H15 2 0.802094 0.973766 0.060664 11.00000 -1.20000 AFIX 0 C16 1 0.786013 0.772695 0.012789 11.00000 0.07693 0.08186 = 0.04820 0.03157 0.03442 0.03499 AFIX 43 H16 2 0.789951 0.779084 -0.041499 11.00000 -1.20000 AFIX 0 C17 1 0.773752 0.647172 0.032667 11.00000 0.10872 0.06605 = 0.04736 0.01428 0.03640 0.03959 AFIX 43 H17 2 0.771295 0.568830 -0.008028 11.00000 -1.20000 AFIX 0 C18 1 0.765065 0.636671 0.112653 11.00000 0.08488 0.04583 = 0.04650 0.01585 0.02945 0.02788 AFIX 43 H18 2 0.756543 0.551301 0.125355 11.00000 -1.20000 AFIX 0 C19 1 0.153246 0.582624 0.248911 11.00000 0.04445 0.06087 = 0.06598 0.02031 0.02320 0.02705 AFIX 43 H19 2 0.067038 0.603626 0.258989 11.00000 -1.20000 AFIX 0 C20 1 0.212827 0.634926 0.196178 11.00000 0.05071 0.05058 = 0.05555 0.02183 0.01407 0.02279 AFIX 43 H20 2 0.172444 0.696448 0.165260 11.00000 -1.20000 AFIX 0 C21 1 0.343512 0.586595 0.192597 11.00000 0.04792 0.05201 = 0.05193 0.02450 0.02182 0.01636 AFIX 43 H21 2 0.398711 0.613115 0.159094 11.00000 -1.20000 AFIX 0 C22 1 0.380757 0.496751 0.243423 11.00000 0.03503 0.03932 = 0.03506 0.00916 0.01241 0.00981 C23 1 0.506606 0.428953 0.255372 11.00000 0.03454 0.04203 = 0.04329 0.01277 0.01461 0.01054 AFIX 43 H23 2 0.573201 0.445449 0.226132 11.00000 -1.20000 AFIX 0 C24 1 0.650153 0.280793 0.314982 11.00000 0.03239 0.03867 = 0.03706 0.01271 0.01010 0.00940 C25 1 0.648091 0.252570 0.460570 11.00000 0.04715 0.05292 = 0.04653 0.01695 0.02137 0.01302 AFIX 43 H25 2 0.566919 0.294868 0.461030 11.00000 -1.20000 AFIX 0 C26 1 0.717810 0.204100 0.528653 11.00000 0.06099 0.06077 = 0.04349 0.02072 0.02062 0.01045 AFIX 43 H26 2 0.682936 0.211104 0.575750 11.00000 -1.20000 AFIX 0 C27 1 0.843256 0.142930 0.528564 11.00000 0.05752 0.06118 = 0.04787 0.02814 0.00921 0.01020 AFIX 43 H27 2 0.890527 0.110329 0.575778 11.00000 -1.20000 AFIX 0 C28 1 0.895354 0.131287 0.460449 11.00000 0.04349 0.05553 = 0.05313 0.02534 0.01079 0.01615 AFIX 43 H28 2 0.978444 0.091599 0.461022 11.00000 -1.20000 AFIX 0 C29 1 0.822642 0.179828 0.388543 11.00000 0.03481 0.03837 = 0.04274 0.01297 0.00976 0.00984 C30 1 0.745350 0.241825 0.269317 11.00000 0.03274 0.03772 = 0.03853 0.01097 0.01079 0.01030 C31 1 0.743572 0.252912 0.182142 11.00000 0.04088 0.03751 = 0.04054 0.01290 0.01695 0.01457 C32 1 0.614483 0.229298 0.113945 11.00000 0.04613 0.06138 = 0.04207 0.01108 0.01445 0.00899 AFIX 43 H32 2 0.525119 0.208502 0.123270 11.00000 -1.20000 AFIX 0 C33 1 0.618094 0.236510 0.032597 11.00000 0.06853 0.07319 = 0.03871 0.01218 0.01252 0.01709 AFIX 43 H33 2 0.531170 0.220646 -0.012421 11.00000 -1.20000 AFIX 0 C34 1 0.749044 0.266920 0.017717 11.00000 0.09184 0.05949 = 0.04888 0.02206 0.03719 0.03053 AFIX 43 H34 2 0.750954 0.271857 -0.037144 11.00000 -1.20000 AFIX 0 C35 1 0.877080 0.289991 0.084191 11.00000 0.06667 0.06131 = 0.07095 0.03125 0.04484 0.02750 AFIX 43 H35 2 0.965862 0.311073 0.074256 11.00000 -1.20000 AFIX 0 C36 1 0.875266 0.282163 0.165899 11.00000 0.04457 0.05273 = 0.05740 0.02158 0.02272 0.01916 AFIX 43 H36 2 0.962885 0.296598 0.210259 11.00000 -1.20000 AFIX 0 N1 3 0.578774 0.880809 0.308117 11.00000 0.03727 0.03975 = 0.04259 0.01151 0.01379 0.01830 N2 3 0.720796 0.743502 0.383410 11.00000 0.03318 0.04192 = 0.03475 0.01239 0.01260 0.01647 N3 3 0.838215 0.644480 0.295499 11.00000 0.03732 0.04565 = 0.03976 0.01538 0.01515 0.01996 N4 3 0.529490 0.346087 0.305441 11.00000 0.03503 0.04542 = 0.04022 0.01265 0.01309 0.01484 N5 3 0.699193 0.238224 0.391003 11.00000 0.03474 0.03868 = 0.03662 0.01234 0.01160 0.00935 N6 3 0.851896 0.181422 0.315641 11.00000 0.03887 0.04709 = 0.04401 0.01617 0.01376 0.01705 S1 4 0.316550 1.016161 0.320358 11.00000 0.05354 0.06287 = 0.04728 0.02134 0.02553 0.02849 S2 4 0.254401 0.472516 0.295624 11.00000 0.05851 0.07984 = 0.07345 0.04584 0.04194 0.03677 HKLF 4 REM EL16_D584_DRX4_1_a.res in P-1 REM R1 = 0.0436 for 5839 Fo > 4sig(Fo) and 0.0742 for all 8471 data REM 397 parameters refined using 0 restraints END WGHT 0.0559 0.3505 REM Highest difference peak 0.292, deepest hole -0.476, 1-sigma level 0.042 Q1 1 0.3206 0.5386 0.3187 11.00000 0.05 0.29 Q2 1 0.7001 0.7777 0.3508 11.00000 0.05 0.27 Q3 1 0.8029 0.2154 0.2887 11.00000 0.05 0.24 Q4 1 0.7807 0.2229 0.3974 11.00000 0.05 0.23 Q5 1 0.7015 0.2861 0.2862 11.00000 0.05 0.22 Q6 1 0.8015 0.2913 0.1748 11.00000 0.05 0.22 Q7 1 0.4434 0.9574 0.2385 11.00000 0.05 0.22 Q8 1 0.8011 0.5525 0.4557 11.00000 0.05 0.22 Q9 1 0.2454 0.4369 0.2460 11.00000 0.05 0.21 Q10 1 0.2196 1.0452 0.2914 11.00000 0.05 0.21 ; _shelx_res_checksum 54875 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy C C1 0.17058(19) 1.07411(19) 0.26058(13) 0.0566(5) Uani d 1 H H1 0.0964 1.1046 0.2811 0.068 Uiso calc 1 C C2 0.17571(19) 1.07047(19) 0.18053(12) 0.0553(4) Uani d 1 H H2 0.1049 1.0979 0.1392 0.066 Uiso calc 1 C C3 0.29993(18) 1.02058(17) 0.16562(11) 0.0450(4) Uani d 1 H H3 0.3202 1.0120 0.1136 0.054 Uiso calc 1 C C4 0.38753(16) 0.98610(14) 0.23621(9) 0.0358(3) Uani d 1 C C5 0.51463(16) 0.92090(15) 0.24091(10) 0.0394(3) Uani d 1 H H5 0.5508 0.9077 0.1943 0.047 Uiso calc 1 C C6 0.68652(15) 0.80001(14) 0.31175(9) 0.0351(3) Uani d 1 C C7 0.67572(17) 0.76611(17) 0.45524(10) 0.0438(4) Uani d 1 H H7 0.6157 0.8308 0.4630 0.053 Uiso calc 1 C C8 0.72008(18) 0.69263(18) 0.51458(10) 0.0487(4) Uani d 1 H H8 0.6906 0.7071 0.5637 0.058 Uiso calc 1 C C9 0.81108(18) 0.59378(17) 0.50265(10) 0.0465(4) Uani d 1 H H9 0.8398 0.5431 0.5436 0.056 Uiso calc 1 C C10 0.85662(16) 0.57250(16) 0.43193(10) 0.0420(3) Uani d 1 H H10 0.9171 0.5080 0.4245 0.050 Uiso calc 1 C C11 0.81172(15) 0.64882(15) 0.36971(9) 0.0355(3) Uani d 1 C C12 0.76267(15) 0.73725(14) 0.25917(9) 0.0349(3) Uani d 1 C C13 0.76897(16) 0.75279(15) 0.17423(9) 0.0371(3) Uani d 1 C C14 0.78455(18) 0.87931(16) 0.15375(11) 0.0445(4) Uani d 1 H H14 0.7897 0.9584 0.1946 0.053 Uiso calc 1 C C15 0.7924(2) 0.88867(19) 0.07363(12) 0.0545(4) Uani d 1 H H15 0.8021 0.9738 0.0607 0.065 Uiso calc 1 C C16 0.7860(2) 0.7727(2) 0.01279(12) 0.0618(5) Uani d 1 H H16 0.7900 0.7791 -0.0415 0.074 Uiso calc 1 C C17 0.7738(3) 0.6472(2) 0.03267(12) 0.0695(6) Uani d 1 H H17 0.7713 0.5688 -0.0080 0.083 Uiso calc 1 C C18 0.7651(2) 0.63667(18) 0.11265(11) 0.0551(5) Uani d 1 H H18 0.7565 0.5513 0.1254 0.066 Uiso calc 1 C C19 0.15325(19) 0.58262(18) 0.24891(12) 0.0537(4) Uani d 1 H H19 0.0670 0.6036 0.2590 0.064 Uiso calc 1 C C20 0.21283(19) 0.63493(17) 0.19618(11) 0.0504(4) Uani d 1 H H20 0.1724 0.6964 0.1653 0.060 Uiso calc 1 C C21 0.34351(18) 0.58659(17) 0.19260(11) 0.0469(4) Uani d 1 H H21 0.3987 0.6131 0.1591 0.056 Uiso calc 1 C C22 0.38076(16) 0.49675(15) 0.24342(9) 0.0358(3) Uani d 1 C C23 0.50661(16) 0.42895(15) 0.25537(10) 0.0387(3) Uani d 1 H H23 0.5732 0.4454 0.2261 0.046 Uiso calc 1 C C24 0.65015(15) 0.28079(14) 0.31498(9) 0.0354(3) Uani d 1 C C25 0.64809(18) 0.25257(17) 0.46057(10) 0.0463(4) Uani d 1 H H25 0.5669 0.2949 0.4610 0.056 Uiso calc 1 C C26 0.7178(2) 0.20410(19) 0.52865(11) 0.0528(4) Uani d 1 H H26 0.6829 0.2111 0.5758 0.063 Uiso calc 1 C C27 0.8433(2) 0.14293(19) 0.52856(12) 0.0547(4) Uani d 1 H H27 0.8905 0.1103 0.5758 0.066 Uiso calc 1 C C28 0.89535(18) 0.13129(17) 0.46045(11) 0.0492(4) Uani d 1 H H28 0.9784 0.0916 0.4610 0.059 Uiso calc 1 C C29 0.82264(16) 0.17983(15) 0.38854(10) 0.0383(3) Uani d 1 C C30 0.74535(15) 0.24182(14) 0.26932(9) 0.0357(3) Uani d 1 C C31 0.74357(16) 0.25291(15) 0.18214(10) 0.0376(3) Uani d 1 C C32 0.61448(19) 0.22930(18) 0.11395(10) 0.0498(4) Uani d 1 H H32 0.5251 0.2085 0.1233 0.060 Uiso calc 1 C C33 0.6181(2) 0.2365(2) 0.03260(11) 0.0607(5) Uani d 1 H H33 0.5312 0.2206 -0.0124 0.073 Uiso calc 1 C C34 0.7490(2) 0.26692(19) 0.01772(12) 0.0608(5) Uani d 1 H H34 0.7510 0.2719 -0.0371 0.073 Uiso calc 1 C C35 0.8771(2) 0.28999(19) 0.08419(13) 0.0578(5) Uani d 1 H H35 0.9659 0.3111 0.0743 0.069 Uiso calc 1 C C36 0.87527(18) 0.28216(17) 0.16590(11) 0.0480(4) Uani d 1 H H36 0.9629 0.2966 0.2103 0.058 Uiso calc 1 N N1 0.57877(13) 0.88081(12) 0.30812(8) 0.0384(3) Uani d 1 N N2 0.72080(12) 0.74350(12) 0.38341(7) 0.0349(3) Uani d 1 N N3 0.83822(13) 0.64448(13) 0.29550(8) 0.0385(3) Uani d 1 N N4 0.52949(13) 0.34609(13) 0.30544(8) 0.0389(3) Uani d 1 N N5 0.69919(13) 0.23822(12) 0.39100(8) 0.0358(3) Uani d 1 N N6 0.85190(14) 0.18142(13) 0.31564(8) 0.0416(3) Uani d 1 S S1 0.31655(5) 1.01616(5) 0.32036(3) 0.04986(13) Uani d 1 S S2 0.25440(5) 0.47252(5) 0.29562(3) 0.06015(15) Uani d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0449(9) 0.0673(11) 0.0729(12) 0.0299(8) 0.0284(9) 0.0261(10) C2 0.0416(9) 0.0683(11) 0.0637(11) 0.0266(8) 0.0135(8) 0.0288(9) C3 0.0461(9) 0.0519(9) 0.0440(9) 0.0186(7) 0.0162(7) 0.0188(7) C4 0.0365(7) 0.0354(7) 0.0411(8) 0.0135(6) 0.0150(6) 0.0133(6) C5 0.0414(8) 0.0436(8) 0.0402(8) 0.0186(6) 0.0178(6) 0.0129(6) C6 0.0353(7) 0.0388(7) 0.0350(7) 0.0145(6) 0.0121(6) 0.0112(6) C7 0.0441(8) 0.0555(9) 0.0407(8) 0.0222(7) 0.0208(7) 0.0136(7) C8 0.0492(9) 0.0662(11) 0.0403(8) 0.0203(8) 0.0202(7) 0.0196(8) C9 0.0443(9) 0.0593(10) 0.0441(9) 0.0180(7) 0.0143(7) 0.0254(8) C10 0.0375(8) 0.0491(9) 0.0450(8) 0.0186(7) 0.0121(6) 0.0188(7) C11 0.0313(7) 0.0406(7) 0.0388(8) 0.0144(6) 0.0122(6) 0.0123(6) C12 0.0336(7) 0.0381(7) 0.0362(7) 0.0138(6) 0.0118(6) 0.0108(6) C13 0.0361(7) 0.0433(8) 0.0376(7) 0.0155(6) 0.0149(6) 0.0128(6) C14 0.0475(9) 0.0436(8) 0.0486(9) 0.0132(7) 0.0208(7) 0.0138(7) C15 0.0583(11) 0.0594(11) 0.0618(11) 0.0183(9) 0.0289(9) 0.0321(9) C16 0.0769(13) 0.0819(13) 0.0482(10) 0.0350(11) 0.0344(10) 0.0316(10) C17 0.1087(18) 0.0660(12) 0.0474(10) 0.0396(12) 0.0364(11) 0.0143(9) C18 0.0849(13) 0.0458(9) 0.0465(9) 0.0279(9) 0.0294(9) 0.0158(8) C19 0.0444(9) 0.0609(11) 0.0660(11) 0.0270(8) 0.0232(8) 0.0203(9) C20 0.0507(9) 0.0506(9) 0.0556(10) 0.0228(8) 0.0141(8) 0.0218(8) C21 0.0479(9) 0.0520(9) 0.0519(9) 0.0164(7) 0.0218(8) 0.0245(8) C22 0.0350(7) 0.0393(7) 0.0351(7) 0.0098(6) 0.0124(6) 0.0092(6) C23 0.0345(7) 0.0420(8) 0.0433(8) 0.0105(6) 0.0146(6) 0.0128(6) C24 0.0324(7) 0.0387(7) 0.0371(7) 0.0094(6) 0.0101(6) 0.0127(6) C25 0.0472(9) 0.0529(9) 0.0465(9) 0.0130(7) 0.0214(7) 0.0169(7) C26 0.0610(11) 0.0608(10) 0.0435(9) 0.0105(9) 0.0206(8) 0.0207(8) C27 0.0575(10) 0.0612(11) 0.0479(10) 0.0102(9) 0.0092(8) 0.0281(8) C28 0.0435(9) 0.0555(10) 0.0531(10) 0.0161(7) 0.0108(7) 0.0253(8) C29 0.0348(7) 0.0384(7) 0.0427(8) 0.0098(6) 0.0098(6) 0.0130(6) C30 0.0327(7) 0.0377(7) 0.0385(8) 0.0103(6) 0.0108(6) 0.0110(6) C31 0.0409(8) 0.0375(7) 0.0405(8) 0.0146(6) 0.0169(6) 0.0129(6) C32 0.0461(9) 0.0614(10) 0.0421(9) 0.0090(8) 0.0145(7) 0.0111(8) C33 0.0685(12) 0.0732(12) 0.0387(9) 0.0171(10) 0.0125(9) 0.0122(9) C34 0.0918(15) 0.0595(11) 0.0489(10) 0.0305(10) 0.0372(10) 0.0221(9) C35 0.0667(12) 0.0613(11) 0.0709(12) 0.0275(9) 0.0448(10) 0.0313(10) C36 0.0446(9) 0.0527(9) 0.0574(10) 0.0192(7) 0.0227(8) 0.0216(8) N1 0.0373(6) 0.0397(6) 0.0426(7) 0.0183(5) 0.0138(5) 0.0115(5) N2 0.0332(6) 0.0419(7) 0.0348(6) 0.0165(5) 0.0126(5) 0.0124(5) N3 0.0373(6) 0.0457(7) 0.0398(7) 0.0200(5) 0.0151(5) 0.0154(5) N4 0.0350(6) 0.0454(7) 0.0402(7) 0.0148(5) 0.0131(5) 0.0126(6) N5 0.0347(6) 0.0387(6) 0.0366(6) 0.0093(5) 0.0116(5) 0.0123(5) N6 0.0389(7) 0.0471(7) 0.0440(7) 0.0171(6) 0.0138(6) 0.0162(6) S1 0.0535(3) 0.0629(3) 0.0473(2) 0.0285(2) 0.02553(19) 0.0213(2) S2 0.0585(3) 0.0798(3) 0.0735(3) 0.0368(2) 0.0419(2) 0.0458(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 C1 S1 112.04(13) C2 C1 H1 124.0 S1 C1 H1 124.0 C1 C2 C3 112.84(15) C1 C2 H2 123.6 C3 C2 H2 123.6 C4 C3 C2 112.60(15) C4 C3 H3 123.7 C2 C3 H3 123.7 C3 C4 C5 127.09(14) C3 C4 S1 110.75(11) C5 C4 S1 121.90(11) N1 C5 C4 121.22(14) N1 C5 H5 119.4 C4 C5 H5 119.4 N1 C6 N2 114.96(12) N1 C6 C12 139.56(13) N2 C6 C12 104.65(11) C8 C7 N2 118.79(14) C8 C7 H7 120.6 N2 C7 H7 120.6 C7 C8 C9 120.61(15) C7 C8 H8 119.7 C9 C8 H8 119.7 C10 C9 C8 120.48(14) C10 C9 H9 119.8 C8 C9 H9 119.8 C9 C10 C11 119.51(14) C9 C10 H10 120.2 C11 C10 H10 120.2 N3 C11 N2 111.13(12) N3 C11 C10 130.72(13) N2 C11 C10 118.12(13) N3 C12 C6 110.91(13) N3 C12 C13 118.49(12) C6 C12 C13 130.57(12) C18 C13 C14 118.35(14) C18 C13 C12 118.66(14) C14 C13 C12 122.94(14) C15 C14 C13 120.75(16) C15 C14 H14 119.6 C13 C14 H14 119.6 C16 C15 C14 120.28(16) C16 C15 H15 119.9 C14 C15 H15 119.9 C15 C16 C17 119.66(17) C15 C16 H16 120.2 C17 C16 H16 120.2 C16 C17 C18 120.48(18) C16 C17 H17 119.8 C18 C17 H17 119.8 C17 C18 C13 120.45(16) C17 C18 H18 119.8 C13 C18 H18 119.8 C20 C19 S2 111.98(13) C20 C19 H19 124.0 S2 C19 H19 124.0 C19 C20 C21 112.60(15) C19 C20 H20 123.7 C21 C20 H20 123.7 C22 C21 C20 113.05(15) C22 C21 H21 123.5 C20 C21 H21 123.5 C21 C22 C23 127.71(14) C21 C22 S2 110.50(11) C23 C22 S2 121.79(11) N4 C23 C22 121.71(14) N4 C23 H23 119.1 C22 C23 H23 119.1 N4 C24 C30 138.57(13) N4 C24 N5 116.60(13) C30 C24 N5 104.83(12) C26 C25 N5 118.84(16) C26 C25 H25 120.6 N5 C25 H25 120.6 C25 C26 C27 120.38(17) C25 C26 H26 119.8 C27 C26 H26 119.8 C28 C27 C26 120.69(15) C28 C27 H27 119.7 C26 C27 H27 119.7 C27 C28 C29 119.54(16) C27 C28 H28 120.2 C29 C28 H28 120.2 N6 C29 N5 111.06(12) N6 C29 C28 131.03(15) N5 C29 C28 117.90(14) N6 C30 C24 110.99(13) N6 C30 C31 119.15(12) C24 C30 C31 129.83(13) C36 C31 C32 118.32(15) C36 C31 C30 119.20(14) C32 C31 C30 122.42(14) C33 C32 C31 120.55(17) C33 C32 H32 119.7 C31 C32 H32 119.7 C34 C33 C32 120.47(18) C34 C33 H33 119.8 C32 C33 H33 119.8 C35 C34 C33 119.64(17) C35 C34 H34 120.2 C33 C34 H34 120.2 C34 C35 C36 120.55(17) C34 C35 H35 119.7 C36 C35 H35 119.7 C35 C36 C31 120.47(16) C35 C36 H36 119.8 C31 C36 H36 119.8 C5 N1 C6 123.72(13) C7 N2 C11 122.48(12) C7 N2 C6 130.34(12) C11 N2 C6 107.15(11) C11 N3 C12 106.14(12) C23 N4 C24 120.64(13) C25 N5 C29 122.62(13) C25 N5 C24 130.14(13) C29 N5 C24 107.17(12) C29 N6 C30 105.92(12) C1 S1 C4 91.78(8) C22 S2 C19 91.88(8) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C1 C2 1.341(3) C1 S1 1.7096(17) C1 H1 0.9300 C2 C3 1.411(2) C2 H2 0.9300 C3 C4 1.371(2) C3 H3 0.9300 C4 C5 1.4392(19) C4 S1 1.7145(15) C5 N1 1.2801(18) C5 H5 0.9300 C6 N1 1.3799(17) C6 N2 1.3941(18) C6 C12 1.395(2) C7 C8 1.351(2) C7 N2 1.3703(19) C7 H7 0.9300 C8 C9 1.415(2) C8 H8 0.9300 C9 C10 1.355(2) C9 H9 0.9300 C10 C11 1.4088(19) C10 H10 0.9300 C11 N3 1.3242(18) C11 N2 1.3898(17) C12 N3 1.3739(17) C12 C13 1.471(2) C13 C18 1.390(2) C13 C14 1.393(2) C14 C15 1.379(2) C14 H14 0.9300 C15 C16 1.376(3) C15 H15 0.9300 C16 C17 1.376(3) C16 H16 0.9300 C17 C18 1.382(2) C17 H17 0.9300 C18 H18 0.9300 C19 C20 1.337(2) C19 S2 1.7105(17) C19 H19 0.9300 C20 C21 1.409(2) C20 H20 0.9300 C21 C22 1.366(2) C21 H21 0.9300 C22 C23 1.4376(19) C22 S2 1.7100(15) C23 N4 1.2860(18) C23 H23 0.9300 C24 N4 1.3806(18) C24 C30 1.387(2) C24 N5 1.3891(18) C25 C26 1.354(2) C25 N5 1.3697(19) C25 H25 0.9300 C26 C27 1.413(3) C26 H26 0.9300 C27 C28 1.354(2) C27 H27 0.9300 C28 C29 1.412(2) C28 H28 0.9300 C29 N6 1.324(2) C29 N5 1.3880(18) C30 N6 1.3743(18) C30 C31 1.473(2) C31 C36 1.388(2) C31 C32 1.393(2) C32 C33 1.381(2) C32 H32 0.9300 C33 C34 1.372(3) C33 H33 0.9300 C34 C35 1.372(3) C34 H34 0.9300 C35 C36 1.383(2) C35 H35 0.9300 C36 H36 0.9300 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA C19 H19 N3 1_455 0.93 2.50 3.428(2) 174.5 C14 H14 N6 1_565 0.93 2.61 3.526(2) 170.3 C15 H15 Cg1 1_565 0.93 2.97 3.778(2) 146 C18 H18 Cg1 1_555 0.93 2.88 3.761(2) 157 C33 H33 Cg2 2_665 0.93 2.95 3.814(2) 155 _cod_database_fobs_code 1543280