#------------------------------------------------------------------------------ #$Date: 2016-09-10 02:12:59 +0300 (Sat, 10 Sep 2016) $ #$Revision: 186333 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/32/1543286.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1543286 loop_ _publ_author_name 'Andrez, Julie' 'P\'ecaut, Jacques' 'Scopelliti, Rosario' 'Kefalidis, Christos E.' 'Maron, Laurent' 'Rosenzweig, Michael W.' 'Meyer, Karsten' 'Mazzanti, Marinella' _publ_section_title ; Synthesis and reactivity of a terminal uranium(iv) sulfide supported by siloxide ligands ; _journal_issue 9 _journal_name_full 'Chem. Sci.' _journal_page_first 5846 _journal_paper_doi 10.1039/C6SC00675B _journal_volume 7 _journal_year 2016 _chemical_formula_moiety 'C48 H108 K O16 S Si4 U, C18 H36 K N2 O6, C6 H14' _chemical_formula_sum 'C72 H158 K2 N2 O22 S Si4 U' _chemical_formula_weight 1864.65 _space_group_IT_number 2 _symmetry_cell_setting triclinic _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _audit_update_record ; 2016-01-18 deposited with the CCDC. 2016-04-11 downloaded from the CCDC. ; _cell_angle_alpha 84.563(10) _cell_angle_beta 84.218(9) _cell_angle_gamma 83.002(12) _cell_formula_units_Z 2 _cell_length_a 14.610(2) _cell_length_b 17.221(3) _cell_length_c 19.8684(19) _cell_measurement_reflns_used 744 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 22 _cell_measurement_theta_min 3 _cell_volume 4919.1(12) _computing_cell_refinement 'Dirax/lsq (Duisenberg & Schreurs, 1989-2000)' _computing_data_collection 'Collect (Bruker AXS BV, 1997-2004)' _computing_data_reduction 'EvalCCD (Duisenberg & Schreurs, 1990-2000)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_device_type 'Bruker APEX II CCD' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0677 _diffrn_reflns_av_sigmaI/netI 0.0893 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 75038 _diffrn_reflns_theta_full 25.25 _diffrn_reflns_theta_max 30.00 _diffrn_reflns_theta_min 1.03 _exptl_absorpt_coefficient_mu 1.864 _exptl_absorpt_correction_T_max 0.7460 _exptl_absorpt_correction_T_min 0.4965 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS 2008, Bruker AXS, 2008' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.259 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1964 _exptl_crystal_size_max 0.39 _exptl_crystal_size_mid 0.26 _exptl_crystal_size_min 0.21 _refine_diff_density_max 3.508 _refine_diff_density_min -1.868 _refine_diff_density_rms 0.168 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.181 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1167 _refine_ls_number_reflns 27810 _refine_ls_number_restraints 619 _refine_ls_restrained_S_all 1.172 _refine_ls_R_factor_all 0.1037 _refine_ls_R_factor_gt 0.0677 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0277P)^2^+28.2718P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1388 _refine_ls_wR_factor_ref 0.1574 _reflns_number_gt 21309 _reflns_number_total 27810 _reflns_threshold_expression >2sigma(I) _iucr_refine_instructions_details ; TITL JA566 in P-1 CELL 0.71073 14.6100 17.2213 19.8684 84.5625 84.2176 83.0023 ZERR 2.00 0.0023 0.0033 0.0019 0.0100 0.0090 0.0120 LATT 1 SFAC C H N O SI S K U UNIT 144 316 4 44 8 2 4 2 REM -------------------------------------------------------------- REM Data collection: Bruker Nonius APEX II CCD REM Absorption correction: SADABS REM Crystal habit: prism; Crystal colour: colourless REM -------------------------------------------------------------- L.S. 10 FMAP 2 PLAN 20 ACTA 50.5 OMIT 0 1 1 OMIT -1 0 1 OMIT 0 2 0 OMIT 1 1 0 OMIT 0 -1 1 OMIT 0 0 2 OMIT 1 1 1 OMIT 1 0 0 OMIT 0 1 0 OMIT 3 3 1 OMIT 1 1 2 TEMP -173 BOND $H SIZE 0.387 0.263 0.208 WPDB -2 CONF SIMU 0.02 K2 > C96B SADI C95 C96A C95 C96B WGHT 0.027700 28.271799 FVAR 0.25480 0.55862 0.55115 MOLE 1 U1 8 0.776708 0.277701 0.229688 11.00000 0.01221 0.02099 = 0.01591 -0.00248 -0.00140 -0.00313 K1 7 0.549627 0.224628 0.217776 11.00000 0.01669 0.02621 = 0.02052 -0.00291 -0.00321 -0.00514 S1 6 0.837445 0.328400 0.329575 11.00000 0.02149 0.04209 = 0.02074 -0.01003 -0.00187 -0.01223 SI1 5 0.668020 0.118561 0.346551 11.00000 0.01857 0.02279 = 0.01655 0.00111 -0.00234 -0.00754 SI2 5 0.558317 0.423431 0.231733 11.00000 0.01456 0.02268 = 0.01973 -0.00467 -0.00263 -0.00063 SI3 5 0.696546 0.194535 0.074983 11.00000 0.01745 0.02413 = 0.01576 -0.00434 -0.00110 -0.00202 SI4 5 1.013366 0.290576 0.141244 11.00000 0.01342 0.02223 = 0.01724 -0.00136 -0.00130 -0.00290 O1 4 0.710869 0.176892 0.289161 11.00000 0.01896 0.02416 = 0.03017 -0.00301 -0.01113 -0.00305 O2 4 0.712034 0.026655 0.342459 11.00000 0.03272 0.02402 = 0.01800 -0.00273 -0.00313 -0.00496 O3 4 0.673206 0.137292 0.424384 11.00000 0.01972 0.03255 = 0.01976 -0.00169 -0.00332 -0.00132 O4 4 0.555994 0.128677 0.335433 11.00000 0.01981 0.02919 = 0.02484 0.00480 -0.00579 -0.00825 O21 4 0.647621 0.360879 0.225444 11.00000 0.02130 0.02326 = 0.02071 -0.00569 -0.00144 0.00080 O22 4 0.539263 0.462203 0.304282 11.00000 0.03038 0.02569 = 0.01978 -0.00625 -0.00042 -0.00066 O23 4 0.471503 0.374556 0.219092 11.00000 0.01552 0.02875 = 0.03188 -0.00319 -0.00659 -0.00109 O24 4 0.554234 0.497150 0.173617 11.00000 0.01695 0.02653 = 0.02468 -0.00015 -0.00479 -0.00366 O41 4 0.722044 0.226017 0.142484 11.00000 0.01557 0.02380 = 0.01918 -0.00349 -0.00427 -0.00289 O42 4 0.584390 0.184019 0.088703 11.00000 0.02009 0.02969 = 0.02515 -0.01213 -0.00464 -0.00395 O43 4 0.719666 0.251677 0.006249 11.00000 0.03007 0.02477 = 0.02013 -0.00206 0.00018 0.00150 O44 4 0.744601 0.107180 0.057686 11.00000 0.02211 0.02503 = 0.02371 -0.00513 0.00029 -0.00055 O61 4 0.907267 0.283667 0.165018 11.00000 0.01713 0.03384 = 0.01966 -0.00568 -0.00105 -0.00556 O62 4 1.024555 0.312962 0.059672 11.00000 0.02254 0.07624 = 0.02024 -0.00177 0.00012 -0.01041 O63 4 1.077508 0.207144 0.152011 11.00000 0.03126 0.03755 = 0.03625 0.00386 -0.00326 -0.00042 O64 4 1.060201 0.353320 0.180576 11.00000 0.02932 0.03436 = 0.03972 -0.00464 -0.00739 -0.00136 C1 1 0.741599 -0.015680 0.283871 11.00000 0.04901 0.02099 = 0.02391 -0.00704 -0.00727 0.00117 C2 1 0.674164 0.004799 0.229350 11.00000 0.04146 0.04645 = 0.03335 -0.01350 -0.01095 -0.00490 AFIX 137 H2A 2 0.673279 0.060536 0.213587 11.00000 -1.50000 H2B 2 0.611950 -0.005827 0.248343 11.00000 -1.50000 H2C 2 0.693936 -0.027153 0.191089 11.00000 -1.50000 AFIX 0 C3 1 0.837294 0.003970 0.256413 11.00000 0.04639 0.04967 = 0.03239 -0.01009 -0.00555 0.00307 AFIX 137 H3A 2 0.834217 0.059784 0.240524 11.00000 -1.50000 H3B 2 0.860240 -0.027776 0.218527 11.00000 -1.50000 H3C 2 0.879351 -0.007382 0.292422 11.00000 -1.50000 AFIX 0 C4 1 0.744953 -0.102670 0.308922 11.00000 0.08658 0.02690 = 0.04819 -0.00558 -0.01926 -0.00446 AFIX 137 H4A 2 0.790751 -0.115394 0.342255 11.00000 -1.50000 H4B 2 0.762403 -0.134692 0.270429 11.00000 -1.50000 H4C 2 0.683854 -0.113654 0.330130 11.00000 -1.50000 AFIX 0 C5 1 0.749862 0.131454 0.465886 11.00000 0.02876 0.03255 = 0.01512 -0.00155 -0.00857 -0.01034 C6 1 0.842565 0.120885 0.423691 11.00000 0.02076 0.04591 = 0.02485 0.00120 -0.00421 -0.00844 AFIX 137 H6A 2 0.848220 0.166607 0.390840 11.00000 -1.50000 H6B 2 0.846480 0.073443 0.399449 11.00000 -1.50000 H6C 2 0.892764 0.115791 0.453578 11.00000 -1.50000 AFIX 0 C7 1 0.735649 0.062667 0.518614 11.00000 0.03491 0.05575 = 0.02982 0.01577 -0.01221 -0.01896 AFIX 137 H7A 2 0.674405 0.071759 0.543464 11.00000 -1.50000 H7B 2 0.783471 0.057874 0.550459 11.00000 -1.50000 H7C 2 0.739936 0.014156 0.495810 11.00000 -1.50000 AFIX 0 C8 1 0.740309 0.208275 0.499069 11.00000 0.04806 0.04908 = 0.04012 -0.01868 0.00059 -0.01788 AFIX 137 H8A 2 0.679002 0.216483 0.523986 11.00000 -1.50000 H8B 2 0.747598 0.251684 0.464041 11.00000 -1.50000 H8C 2 0.788162 0.206233 0.530594 11.00000 -1.50000 AFIX 0 C9 1 0.480620 0.095641 0.377218 11.00000 0.01734 0.04232 = 0.03584 0.00874 -0.00007 -0.01364 C10 1 0.509961 0.011211 0.404069 11.00000 0.03730 0.03612 = 0.04147 0.01044 0.00155 -0.01746 AFIX 137 H10A 2 0.531429 -0.020421 0.365853 11.00000 -1.50000 H10B 2 0.457069 -0.010553 0.430223 11.00000 -1.50000 H10C 2 0.560222 0.010397 0.433369 11.00000 -1.50000 AFIX 0 C11 1 0.449458 0.146592 0.435752 11.00000 0.03056 0.04851 = 0.05011 0.00111 0.00900 -0.00551 AFIX 137 H11A 2 0.429715 0.200290 0.417667 11.00000 -1.50000 H11B 2 0.501011 0.147008 0.463635 11.00000 -1.50000 H11C 2 0.397593 0.125265 0.463622 11.00000 -1.50000 AFIX 0 C12 1 0.402756 0.098535 0.330434 11.00000 0.02782 0.07678 = 0.06203 0.02409 -0.01742 -0.03234 AFIX 137 H12A 2 0.424800 0.068100 0.291561 11.00000 -1.50000 H12B 2 0.384155 0.153167 0.314246 11.00000 -1.50000 H12C 2 0.349548 0.076189 0.355593 11.00000 -1.50000 AFIX 0 C21 1 0.541089 0.428922 0.374113 11.00000 0.02653 0.03058 = 0.01848 -0.00756 -0.00005 -0.00372 C22 1 0.547488 0.340046 0.379741 11.00000 0.06224 0.03197 = 0.02414 -0.00433 0.00292 -0.00746 AFIX 137 H22A 2 0.606614 0.318678 0.357049 11.00000 -1.50000 H22B 2 0.496386 0.323725 0.358082 11.00000 -1.50000 H22C 2 0.543600 0.320288 0.427730 11.00000 -1.50000 AFIX 0 C23 1 0.623411 0.456296 0.402131 11.00000 0.02920 0.04499 = 0.03483 -0.01251 -0.00896 -0.00429 AFIX 137 H23A 2 0.680820 0.433511 0.378080 11.00000 -1.50000 H23B 2 0.623137 0.439362 0.450645 11.00000 -1.50000 H23C 2 0.619455 0.513698 0.395767 11.00000 -1.50000 AFIX 0 C24 1 0.451001 0.464087 0.411011 11.00000 0.02829 0.07065 = 0.02145 -0.00625 0.00226 -0.00358 AFIX 137 H24A 2 0.398481 0.443516 0.394528 11.00000 -1.50000 H24B 2 0.444831 0.521368 0.402272 11.00000 -1.50000 H24C 2 0.451880 0.449944 0.459913 11.00000 -1.50000 AFIX 0 C25 1 0.380435 0.403019 0.198223 11.00000 0.01571 0.03224 = 0.03039 -0.00480 -0.00630 -0.00343 C26 1 0.339735 0.476342 0.232718 11.00000 0.02116 0.04770 = 0.03240 -0.01263 -0.00603 0.00127 AFIX 137 H26A 2 0.335926 0.464575 0.282088 11.00000 -1.50000 H26B 2 0.277607 0.493434 0.218554 11.00000 -1.50000 H26C 2 0.379465 0.518226 0.219723 11.00000 -1.50000 AFIX 0 C27 1 0.387791 0.419656 0.120729 11.00000 0.01698 0.03588 = 0.02745 -0.00859 -0.00519 -0.00023 AFIX 137 H27A 2 0.412852 0.371517 0.099501 11.00000 -1.50000 H27B 2 0.429001 0.460369 0.107283 11.00000 -1.50000 H27C 2 0.326218 0.437706 0.105914 11.00000 -1.50000 AFIX 0 C28 1 0.321390 0.335883 0.218746 11.00000 0.01921 0.04239 = 0.05033 0.00308 -0.00673 -0.01197 AFIX 137 H28A 2 0.315191 0.326224 0.268313 11.00000 -1.50000 H28B 2 0.351150 0.288313 0.198615 11.00000 -1.50000 H28C 2 0.259921 0.350009 0.202486 11.00000 -1.50000 AFIX 0 C29 1 0.605955 0.563484 0.161388 11.00000 0.02519 0.03049 = 0.02932 -0.00236 -0.00097 -0.01189 C30 1 0.708203 0.536991 0.168135 11.00000 0.03178 0.05364 = 0.07636 0.01517 -0.02668 -0.01813 AFIX 137 H30A 2 0.717689 0.522117 0.215985 11.00000 -1.50000 H30B 2 0.744654 0.580062 0.151132 11.00000 -1.50000 H30C 2 0.728048 0.491749 0.141628 11.00000 -1.50000 AFIX 0 C31 1 0.569709 0.623547 0.209890 11.00000 0.10533 0.03017 = 0.06749 -0.01179 0.02610 -0.01644 AFIX 137 H31A 2 0.503722 0.639177 0.205243 11.00000 -1.50000 H31B 2 0.603641 0.669596 0.199826 11.00000 -1.50000 H31C 2 0.577985 0.601271 0.256418 11.00000 -1.50000 AFIX 0 C32 1 0.592929 0.596681 0.089015 11.00000 0.05194 0.04504 = 0.03753 0.01432 -0.01095 -0.02511 AFIX 137 H32A 2 0.526659 0.608683 0.083508 11.00000 -1.50000 H32B 2 0.620560 0.558005 0.057532 11.00000 -1.50000 H32C 2 0.623156 0.644788 0.079274 11.00000 -1.50000 AFIX 0 C41 1 0.525564 0.143386 0.052440 11.00000 0.02649 0.03218 = 0.03383 -0.01459 -0.01161 -0.00309 C42 1 0.427815 0.180074 0.070583 11.00000 0.02667 0.06524 = 0.07857 -0.03598 -0.01697 -0.00434 AFIX 137 H42A 2 0.412704 0.172254 0.119760 11.00000 -1.50000 H42B 2 0.384491 0.155317 0.047217 11.00000 -1.50000 H42C 2 0.422922 0.236418 0.056526 11.00000 -1.50000 AFIX 0 C43 1 0.550910 0.155730 -0.024183 11.00000 0.05619 0.05728 = 0.03221 -0.01073 -0.02062 -0.01088 AFIX 137 H43A 2 0.543541 0.212014 -0.038488 11.00000 -1.50000 H43B 2 0.510057 0.129001 -0.048140 11.00000 -1.50000 H43C 2 0.615355 0.134075 -0.034965 11.00000 -1.50000 AFIX 0 C44 1 0.537500 0.057083 0.076900 11.00000 0.04534 0.04050 = 0.04536 -0.01012 -0.01517 -0.01528 AFIX 137 H44A 2 0.520678 0.050886 0.125962 11.00000 -1.50000 H44B 2 0.602194 0.035559 0.067005 11.00000 -1.50000 H44C 2 0.497355 0.028945 0.053565 11.00000 -1.50000 AFIX 0 C45 1 0.709488 0.336068 -0.006155 11.00000 0.02727 0.03287 = 0.01879 0.00053 0.00003 0.00039 C46 1 0.793746 0.367223 0.016388 11.00000 0.03357 0.04278 = 0.06047 0.01767 -0.01448 -0.01018 AFIX 137 H46A 2 0.850240 0.340916 -0.006183 11.00000 -1.50000 H46B 2 0.794636 0.356884 0.065692 11.00000 -1.50000 H46C 2 0.790558 0.423907 0.004156 11.00000 -1.50000 AFIX 0 C47 1 0.619497 0.371340 0.029641 11.00000 0.03503 0.03052 = 0.02498 -0.00244 -0.00228 0.00554 AFIX 137 H47A 2 0.567748 0.347069 0.015945 11.00000 -1.50000 H47B 2 0.610699 0.428022 0.017225 11.00000 -1.50000 H47C 2 0.621922 0.361710 0.078874 11.00000 -1.50000 AFIX 0 C48 1 0.707403 0.352066 -0.082907 11.00000 0.05453 0.04054 = 0.02054 0.00279 -0.00027 0.00771 AFIX 137 H48A 2 0.655085 0.329288 -0.097434 11.00000 -1.50000 H48B 2 0.765305 0.328321 -0.105629 11.00000 -1.50000 H48C 2 0.700479 0.408859 -0.094935 11.00000 -1.50000 AFIX 0 C49 1 0.838237 0.080875 0.032083 11.00000 0.02796 0.02815 = 0.02397 -0.00431 -0.00061 0.00456 C50 1 0.851546 0.103845 -0.043584 11.00000 0.05059 0.05299 = 0.02850 -0.00526 0.00815 0.01000 AFIX 137 H50A 2 0.843061 0.161181 -0.051712 11.00000 -1.50000 H50B 2 0.806014 0.081377 -0.066667 11.00000 -1.50000 H50C 2 0.914160 0.083814 -0.061250 11.00000 -1.50000 AFIX 0 C51 1 0.848153 -0.008419 0.045558 11.00000 0.04049 0.03021 = 0.04427 -0.00736 0.00315 0.00551 AFIX 137 H51A 2 0.838417 -0.022557 0.094490 11.00000 -1.50000 H51B 2 0.910400 -0.030143 0.028545 11.00000 -1.50000 H51C 2 0.802005 -0.029850 0.022285 11.00000 -1.50000 AFIX 0 C52 1 0.907224 0.116204 0.069758 11.00000 0.02211 0.04371 = 0.04296 -0.01121 -0.00035 -0.00338 AFIX 137 H52A 2 0.894438 0.104027 0.118745 11.00000 -1.50000 H52B 2 0.901165 0.173277 0.059396 11.00000 -1.50000 H52C 2 0.970320 0.093969 0.055300 11.00000 -1.50000 AFIX 0 C61 1 1.101977 0.302206 0.009596 11.00000 0.02090 0.04982 = 0.02061 -0.00550 0.00197 -0.00722 C62 1 1.083901 0.371512 -0.043056 11.00000 0.03923 0.05375 = 0.03839 -0.00448 -0.00649 0.00239 AFIX 137 H62A 2 1.026362 0.367427 -0.063253 11.00000 -1.50000 H62B 2 1.135498 0.370918 -0.078643 11.00000 -1.50000 H62C 2 1.078240 0.420680 -0.021067 11.00000 -1.50000 AFIX 0 C63 1 1.102616 0.225895 -0.021053 11.00000 0.05468 0.04258 = 0.05018 -0.00564 -0.00305 -0.01717 AFIX 137 H63A 2 1.112147 0.182338 0.013930 11.00000 -1.50000 H63B 2 1.152863 0.221050 -0.057528 11.00000 -1.50000 H63C 2 1.043255 0.224390 -0.039606 11.00000 -1.50000 AFIX 0 C64 1 1.194400 0.306639 0.038574 11.00000 0.01758 0.06250 = 0.02812 -0.00050 0.00629 -0.00751 AFIX 137 H64A 2 1.205173 0.263201 0.073483 11.00000 -1.50000 H64B 2 1.192407 0.356684 0.058702 11.00000 -1.50000 H64C 2 1.244696 0.302865 0.002059 11.00000 -1.50000 AFIX 0 C65 1 1.100794 0.156942 0.212288 11.00000 0.02258 0.02631 = 0.03100 0.00887 -0.00583 -0.00384 C66 1 1.132362 0.077957 0.181788 11.00000 0.06793 0.04453 = 0.06205 -0.00742 0.00814 -0.00682 AFIX 137 H66A 2 1.178120 0.085844 0.142904 11.00000 -1.50000 H66B 2 1.078815 0.057387 0.166816 11.00000 -1.50000 H66C 2 1.160217 0.040436 0.216258 11.00000 -1.50000 AFIX 0 C67 1 1.181777 0.183154 0.240919 11.00000 0.03579 0.08448 = 0.05605 -0.00770 -0.01070 -0.02525 AFIX 137 H67A 2 1.163790 0.234723 0.258327 11.00000 -1.50000 H67B 2 1.232865 0.186778 0.205219 11.00000 -1.50000 H67C 2 1.201683 0.145118 0.277953 11.00000 -1.50000 AFIX 0 C68 1 1.019341 0.150163 0.264043 11.00000 0.03033 0.03880 = 0.04206 0.01021 0.00090 -0.00565 AFIX 137 H68A 2 1.003113 0.199986 0.284807 11.00000 -1.50000 H68B 2 1.035231 0.108203 0.299211 11.00000 -1.50000 H68C 2 0.966483 0.137873 0.241912 11.00000 -1.50000 AFIX 0 C69 1 1.034656 0.436498 0.187397 11.00000 0.01521 0.01789 = 0.02819 -0.00265 -0.00108 -0.00364 C70 1 1.098810 0.483410 0.138410 11.00000 0.02705 0.04282 = 0.03118 0.00250 -0.00655 -0.00960 AFIX 137 H70A 2 1.163380 0.464475 0.145643 11.00000 -1.50000 H70B 2 1.086566 0.539121 0.146551 11.00000 -1.50000 H70C 2 1.087672 0.476751 0.091586 11.00000 -1.50000 AFIX 0 C71 1 1.051164 0.444804 0.260269 11.00000 0.03182 0.06232 = 0.03182 0.00275 -0.00481 -0.00575 AFIX 137 H71A 2 1.012219 0.411714 0.290801 11.00000 -1.50000 H71B 2 1.035499 0.499744 0.270239 11.00000 -1.50000 H71C 2 1.116458 0.428331 0.266931 11.00000 -1.50000 AFIX 0 C72 1 0.934439 0.463774 0.176876 11.00000 0.02136 0.04737 = 0.03467 0.00554 -0.00058 -0.00166 AFIX 137 H72A 2 0.894501 0.431253 0.207121 11.00000 -1.50000 H72B 2 0.923760 0.459023 0.129603 11.00000 -1.50000 H72C 2 0.920063 0.518733 0.187082 11.00000 -1.50000 AFIX 0 MOLE 2 K2 7 -0.010237 0.715760 0.394792 11.00000 0.08401 0.02467 = 0.03467 -0.00368 -0.03260 -0.00533 PART 1 O65A 4 0.167703 0.663636 0.381806 21.00000 0.03611 0.02568 = 0.02852 -0.00510 -0.00483 -0.00157 O66A 4 0.053204 0.600391 0.494971 21.00000 0.04967 0.03917 = 0.03287 0.00426 -0.02413 -0.02334 O67A 4 -0.200816 0.666790 0.399938 21.00000 0.03839 0.04119 = 0.03914 0.00095 0.00115 -0.01223 O68A 4 -0.065855 0.832691 0.490740 21.00000 0.05111 0.03626 = 0.02478 -0.00289 0.00034 -0.01669 N1A 3 0.087900 0.752563 0.265951 21.00000 0.03099 0.03937 = 0.02248 -0.00723 -0.00282 -0.00103 N2A 3 -0.131899 0.682479 0.529639 21.00000 0.07215 0.03692 = 0.01982 -0.00338 0.00638 -0.02019 C73A 1 0.187454 0.730752 0.270974 21.00000 0.02812 0.03903 = 0.02875 -0.00338 0.00164 -0.00333 AFIX 23 H73A 2 0.212938 0.773098 0.291018 21.00000 -1.20000 H73B 2 0.218915 0.725963 0.224793 21.00000 -1.20000 AFIX 0 C74A 1 0.208031 0.654942 0.313355 21.00000 0.03440 0.03538 = 0.03670 -0.00925 0.00485 0.00818 AFIX 23 H74A 2 0.181922 0.612235 0.294293 21.00000 -1.20000 H74B 2 0.275839 0.641100 0.313149 21.00000 -1.20000 AFIX 0 C75A 1 0.200764 0.602682 0.426841 21.00000 0.04774 0.03370 = 0.04883 0.01103 -0.01697 -0.00995 AFIX 23 H75A 2 0.268085 0.603320 0.428917 21.00000 -1.20000 H75B 2 0.190837 0.551825 0.410967 21.00000 -1.20000 AFIX 0 C76A 1 0.150322 0.611508 0.497379 21.00000 0.05992 0.04282 = 0.04662 0.01508 -0.02603 -0.02629 AFIX 23 H76A 2 0.178970 0.571969 0.530779 21.00000 -1.20000 H76B 2 0.154985 0.664368 0.511548 21.00000 -1.20000 AFIX 0 C77A 1 0.009817 0.595128 0.560192 21.00000 0.06227 0.04073 = 0.02264 0.00582 -0.02750 -0.03065 AFIX 23 H77A 2 0.026763 0.637124 0.585723 21.00000 -1.20000 H77B 2 0.030735 0.543872 0.583972 21.00000 -1.20000 AFIX 0 C78A 1 -0.095643 0.603313 0.557856 21.00000 0.06778 0.03839 = 0.02415 0.00495 -0.01095 -0.02622 AFIX 23 H78A 2 -0.111777 0.563484 0.529605 21.00000 -1.20000 H78B 2 -0.125466 0.593119 0.604330 21.00000 -1.20000 AFIX 0 C79A 1 0.057181 0.707604 0.213614 21.00000 0.04258 0.05196 = 0.02255 -0.01427 -0.00415 -0.00403 AFIX 23 H79A 2 0.085572 0.652465 0.219478 21.00000 -1.20000 H79B 2 0.079954 0.729841 0.168093 21.00000 -1.20000 AFIX 0 C80A 1 -0.045322 0.708692 0.216780 21.00000 0.04829 0.05516 = 0.02351 -0.00889 -0.00688 -0.00699 AFIX 23 H80A 2 -0.074228 0.763656 0.210711 21.00000 -1.20000 H80B 2 -0.061344 0.680281 0.179322 21.00000 -1.20000 AFIX 0 C81A 1 -0.209754 0.621592 0.344777 21.00000 0.04141 0.04636 = 0.04569 -0.00399 -0.00905 -0.02065 AFIX 23 H81A 2 -0.175125 0.568779 0.351656 21.00000 -1.20000 H81B 2 -0.275704 0.615334 0.342015 21.00000 -1.20000 AFIX 0 C82A 1 -0.246297 0.634998 0.461225 21.00000 0.04436 0.05913 = 0.05377 -0.00266 0.00255 -0.01671 AFIX 23 H82A 2 -0.221027 0.579571 0.471265 21.00000 -1.20000 H82B 2 -0.313451 0.636911 0.456836 21.00000 -1.20000 AFIX 0 C83A 1 -0.230102 0.684011 0.518393 21.00000 0.06520 0.05053 = 0.03533 0.00220 0.02484 -0.00802 AFIX 23 H83A 2 -0.256083 0.739076 0.507503 21.00000 -1.20000 H83B 2 -0.264071 0.664223 0.560972 21.00000 -1.20000 AFIX 0 C84A 1 0.070187 0.837194 0.245916 21.00000 0.03448 0.04264 = 0.02165 0.00383 -0.00515 -0.00421 AFIX 23 H84A 2 0.009081 0.846745 0.227300 21.00000 -1.20000 H84B 2 0.117114 0.850253 0.208360 21.00000 -1.20000 AFIX 0 C85A 1 -0.137329 0.824434 0.543462 21.00000 0.08593 0.04662 = 0.04396 -0.00899 0.02367 -0.01570 AFIX 23 H85A 2 -0.198266 0.834838 0.524639 21.00000 -1.20000 H85B 2 -0.134912 0.862918 0.577050 21.00000 -1.20000 AFIX 0 C86A 1 -0.125964 0.743360 0.577124 21.00000 0.08858 0.04583 = 0.03370 -0.01184 0.01696 -0.01871 AFIX 23 H86A 2 -0.174606 0.738601 0.615272 21.00000 -1.20000 H86B 2 -0.065129 0.733780 0.596142 21.00000 -1.20000 AFIX 0 PART 2 O65B 4 0.190924 0.668451 0.335006 -21.00000 0.03088 0.02682 = 0.03702 -0.00427 -0.00508 0.00586 O66B 4 0.115233 0.595297 0.458806 -21.00000 0.05521 0.02902 = 0.03224 -0.00064 -0.02565 0.00388 O67B 4 -0.160647 0.644770 0.408196 -21.00000 0.04376 0.04267 = 0.03426 -0.00585 -0.00065 -0.01217 O68B 4 -0.037260 0.828198 0.488702 -21.00000 0.03360 0.02478 = 0.01797 -0.00757 -0.00414 -0.00017 N1B 3 0.076699 0.773730 0.245359 -21.00000 0.03393 0.03077 = 0.01584 -0.00532 -0.00154 0.00302 N2B 3 -0.066693 0.663437 0.528659 -21.00000 0.05930 0.04305 = 0.01263 -0.00518 0.00201 -0.00465 C73B 1 0.177774 0.757849 0.235965 -21.00000 0.03525 0.02875 = 0.03760 -0.00635 0.00157 0.00182 AFIX 23 H73C 2 0.205502 0.796359 0.259283 -21.00000 -1.20000 H73D 2 0.198210 0.764992 0.186956 -21.00000 -1.20000 AFIX 0 C74B 1 0.212279 0.677111 0.262780 -21.00000 0.03362 0.02676 = 0.03808 -0.00431 0.00381 0.00393 AFIX 23 H74C 2 0.182822 0.638147 0.241260 -21.00000 -1.20000 H74D 2 0.280088 0.667492 0.251750 -21.00000 -1.20000 AFIX 0 C75B 1 0.229702 0.594114 0.363013 -21.00000 0.03473 0.02594 = 0.04431 -0.00223 -0.01086 -0.00141 AFIX 23 H75C 2 0.297358 0.586676 0.350629 -21.00000 -1.20000 H75D 2 0.201565 0.551446 0.345544 -21.00000 -1.20000 AFIX 0 C76B 1 0.209084 0.592959 0.440743 -21.00000 0.05222 0.02756 = 0.03813 0.01292 -0.02819 -0.00454 AFIX 23 H76C 2 0.241523 0.544698 0.462540 -21.00000 -1.20000 H76D 2 0.232534 0.638722 0.457056 -21.00000 -1.20000 AFIX 0 C77B 1 0.097261 0.596900 0.529263 -21.00000 0.06642 0.04118 = 0.03750 -0.00357 -0.01217 0.00770 AFIX 23 H77C 2 0.111395 0.647396 0.543442 -21.00000 -1.20000 H77D 2 0.136606 0.553831 0.552594 -21.00000 -1.20000 AFIX 0 C78B 1 -0.009932 0.586708 0.549150 -21.00000 0.06982 0.04657 = 0.02831 -0.00260 -0.01064 -0.01627 AFIX 23 H78C 2 -0.027873 0.543753 0.525260 -21.00000 -1.20000 H78D 2 -0.021069 0.573401 0.598644 -21.00000 -1.20000 AFIX 0 C79B 1 0.032904 0.733028 0.195093 -21.00000 0.03915 0.04496 = 0.01898 -0.00448 -0.00200 -0.00590 AFIX 23 H79C 2 0.065257 0.679332 0.192158 -21.00000 -1.20000 H79D 2 0.041441 0.761731 0.149732 -21.00000 -1.20000 AFIX 0 C80B 1 -0.069277 0.727753 0.213394 -21.00000 0.03561 0.04910 = 0.01747 -0.00293 -0.01102 0.00214 AFIX 23 H80C 2 -0.102036 0.780534 0.220529 -21.00000 -1.20000 H80D 2 -0.096261 0.706474 0.176229 -21.00000 -1.20000 AFIX 0 C81B 1 -0.177616 0.603397 0.351163 -21.00000 0.04334 0.03788 = 0.03980 -0.00372 -0.00144 -0.01356 AFIX 23 H81C 2 -0.239223 0.584101 0.359309 -21.00000 -1.20000 H81D 2 -0.130236 0.557604 0.345887 -21.00000 -1.20000 AFIX 0 C82B 1 -0.178516 0.598180 0.471078 -21.00000 0.05565 0.04634 = 0.04916 0.00218 0.00453 -0.01662 AFIX 23 H82C 2 -0.137710 0.547865 0.471477 -21.00000 -1.20000 H82D 2 -0.243684 0.586531 0.476565 -21.00000 -1.20000 AFIX 0 C83B 1 -0.159206 0.646063 0.529934 -21.00000 0.06738 0.04331 = 0.02690 -0.00126 0.01665 -0.01333 AFIX 23 H83C 2 -0.200615 0.696058 0.528286 -21.00000 -1.20000 H83D 2 -0.175444 0.616151 0.573669 -21.00000 -1.20000 AFIX 0 C84B 1 0.048127 0.858901 0.234430 -21.00000 0.03718 0.02934 = 0.02463 0.00181 -0.00063 0.00545 AFIX 23 H84C 2 -0.018894 0.869121 0.228611 -21.00000 -1.20000 H84D 2 0.082978 0.881775 0.193514 -21.00000 -1.20000 AFIX 0 C85B 1 -0.094576 0.806219 0.549568 -21.00000 0.03726 0.04008 = 0.02245 -0.00042 -0.00581 -0.00049 AFIX 23 H85C 2 -0.159926 0.809733 0.539266 -21.00000 -1.20000 H85D 2 -0.090783 0.842821 0.584461 -21.00000 -1.20000 AFIX 0 C86B 1 -0.063187 0.725096 0.575852 -21.00000 0.05618 0.03472 = 0.00951 -0.00340 -0.00234 -0.01144 AFIX 23 H86C 2 -0.101906 0.712143 0.618303 -21.00000 -1.20000 H86D 2 0.001358 0.723300 0.587565 -21.00000 -1.20000 AFIX 0 PART 0 O69 4 -0.079603 0.674552 0.277269 11.00000 0.03885 0.05131 = 0.02724 -0.00949 -0.00827 -0.01038 O70 4 0.004659 0.875967 0.353586 11.00000 0.02766 0.03012 = 0.02367 -0.00475 -0.00428 -0.00649 C87 1 -0.173576 0.661652 0.284029 11.00000 0.04672 0.05053 = 0.04589 -0.01801 -0.00799 -0.01929 PART 1 AFIX 23 H87A 2 -0.183939 0.631885 0.245751 21.00000 -1.20000 H87B 2 -0.210864 0.713453 0.278387 21.00000 -1.20000 AFIX 23 PART 2 H87C 2 -0.190011 0.636943 0.244549 -21.00000 -1.20000 H87D 2 -0.214853 0.711031 0.289901 -21.00000 -1.20000 AFIX 0 PART 0 C88 1 0.070610 0.894900 0.299513 11.00000 0.04385 0.04079 = 0.03776 -0.00734 0.00770 -0.01653 PART 1 AFIX 23 H88A 2 0.132859 0.890950 0.316020 21.00000 -1.20000 H88B 2 0.054638 0.949300 0.279880 21.00000 -1.20000 AFIX 23 PART 2 H88C 2 0.133529 0.873513 0.311304 -21.00000 -1.20000 H88D 2 0.068675 0.952627 0.290957 -21.00000 -1.20000 AFIX 0 PART 0 C89 1 0.007381 0.924430 0.408113 11.00000 0.03587 0.02716 = 0.02840 -0.00554 -0.01365 -0.00416 AFIX 23 H89A 2 -0.000469 0.980453 0.390829 11.00000 -1.20000 H89B 2 0.068151 0.913141 0.427111 11.00000 -1.20000 AFIX 0 C90 1 -0.067380 0.908766 0.461751 11.00000 0.04155 0.03507 = 0.02751 -0.00939 -0.00912 -0.00603 PART 1 AFIX 23 H90A 2 -0.064910 0.943622 0.498236 21.00000 -1.20000 H90B 2 -0.127448 0.923580 0.442277 21.00000 -1.20000 AFIX 23 PART 2 H90C 2 -0.071954 0.946016 0.497278 -21.00000 -1.20000 H90D 2 -0.127906 0.911987 0.442684 -21.00000 -1.20000 AFIX 0 PART 0 MOLE 3 C91 1 0.655760 0.077098 -0.196587 11.00000 0.06872 0.20221 = 0.10839 -0.06809 -0.00227 -0.01119 AFIX 137 H91A 2 0.695955 0.054483 -0.234004 11.00000 -1.50000 H91B 2 0.638265 0.034928 -0.162853 11.00000 -1.50000 H91C 2 0.688908 0.113046 -0.175311 11.00000 -1.50000 AFIX 0 C92 1 0.574913 0.118843 -0.222054 11.00000 0.08581 0.16854 = 0.11980 -0.04266 -0.01917 -0.01016 AFIX 23 H92A 2 0.546313 0.154244 -0.187391 11.00000 -1.20000 H92B 2 0.531046 0.080083 -0.225156 11.00000 -1.20000 AFIX 0 C93 1 0.580876 0.165832 -0.286956 11.00000 0.08335 0.20694 = 0.09805 -0.06005 0.00893 -0.00791 AFIX 23 H93A 2 0.615190 0.131950 -0.320836 11.00000 -1.20000 H93B 2 0.619362 0.208221 -0.282390 11.00000 -1.20000 AFIX 0 C94 1 0.494490 0.203074 -0.316080 11.00000 0.14733 0.15415 = 0.12209 -0.06984 -0.01908 0.01685 AFIX 23 H94A 2 0.451699 0.162087 -0.310509 11.00000 -1.20000 H94B 2 0.467407 0.243574 -0.285368 11.00000 -1.20000 AFIX 0 C95 1 0.487750 0.237531 -0.380030 11.00000 0.16578 0.18237 = 0.13231 -0.04597 0.03458 0.02241 PART 1 AFIX 23 H95A 2 0.521964 0.201922 -0.412603 31.00000 -1.20000 H95B 2 0.421856 0.244464 -0.389447 31.00000 -1.20000 AFIX 23 PART 2 H95C 2 0.548632 0.257734 -0.390557 -31.00000 -1.20000 H95D 2 0.491526 0.191489 -0.406889 -31.00000 -1.20000 AFIX 0 PART 1 C96A 1 0.519833 0.305545 -0.390366 31.00000 0.12420 0.06121 = 0.08634 -0.04010 0.00879 0.02037 AFIX 137 H96A 2 0.473150 0.346168 -0.372659 31.00000 -1.50000 H96B 2 0.534311 0.317822 -0.439170 31.00000 -1.50000 H96C 2 0.576136 0.303727 -0.367031 31.00000 -1.50000 AFIX 0 PART 2 C96B 1 0.431839 0.291485 -0.415223 -31.00000 0.17708 0.04443 = 0.09359 -0.00314 0.05695 0.03501 AFIX 137 H96D 2 0.464990 0.336877 -0.431167 -31.00000 -1.50000 H96E 2 0.376532 0.308387 -0.385741 -31.00000 -1.50000 H96F 2 0.413453 0.268314 -0.454282 -31.00000 -1.50000 PART 0 MOLE 0 HKLF 4 REM JA566 in P-1 REM R1 = 0.0677 for 21309 Fo > 4sig(Fo) and 0.1037 for all 27810 data REM 1167 parameters refined using 619 restraints END WGHT 0.0277 28.2636 REM Highest difference peak 3.508, deepest hole -1.868, 1-sigma level 0.168 Q1 1 0.7216 0.2681 0.2475 11.00000 0.05 3.51 Q2 1 0.7710 0.3320 0.2256 11.00000 0.05 3.12 Q3 1 0.7872 0.2211 0.2332 11.00000 0.05 3.10 Q4 1 0.8375 0.2822 0.2096 11.00000 0.05 2.68 Q5 1 0.8206 0.3028 0.2004 11.00000 0.05 2.37 Q6 1 1.0951 0.2422 0.1911 11.00000 0.05 2.28 Q7 1 1.0385 0.3807 0.1352 11.00000 0.05 2.12 Q8 1 1.0402 0.2561 0.0659 11.00000 0.05 2.10 Q9 1 0.6624 0.1660 0.3143 11.00000 0.05 1.88 Q10 1 0.7605 0.2749 0.2091 11.00000 0.05 1.25 Q11 1 0.4809 0.0948 -0.3209 11.00000 0.05 1.15 Q12 1 0.7009 0.2240 0.2995 11.00000 0.05 1.14 Q13 1 0.7169 0.1231 0.3205 11.00000 0.05 1.09 Q14 1 0.9301 0.5393 0.2181 11.00000 0.05 1.04 Q15 1 0.8009 0.1790 0.2274 11.00000 0.05 1.02 Q16 1 0.0224 0.7257 0.3768 11.00000 0.05 0.91 Q17 1 0.6230 0.1136 -0.2684 11.00000 0.05 0.90 Q18 1 -0.0455 0.7207 0.3912 11.00000 0.05 0.90 Q19 1 0.6328 0.2059 0.3314 11.00000 0.05 0.89 Q20 1 0.6830 0.2809 0.2810 11.00000 0.05 0.89 ; _cod_data_source_file c6sc00675b2.cif _cod_data_source_block 3 _cod_depositor_comments 'Adding full bibliography for 1543284--1543292.cif.' _cod_original_cell_volume 4919.2(13) _cod_database_code 1543286 _publcif_datablock.id {ccf01662-334d-4da6-bf0d-aa6de768a695} _iucr_refine_reflections_details ; -1 0 0 0.40368 1.51534 1 -1 0 0 0.38685 0.94272 5 -2 0 0 73.8471 6.3568 1 -2 0 0 83.8851 6.3855 1 -2 0 0 75.9806 5.5750 5 2 0 0 88.6580 6.7329 1 2 0 0 83.8140 5.7957 3 -3 0 0 651.987 37.882 1 -3 0 0 664.303 37.886 1 -3 0 0 699.028 36.510 5 3 0 0 671.296 37.990 1 3 0 0 678.489 37.570 3 3 0 0 784.824 36.891 5 3 0 0 702.361 38.284 1 -4 0 0 1598.85 85.60 1 -4 0 0 1596.74 85.51 1 -4 0 0 1588.30 85.12 5 4 0 0 1633.71 85.76 1 4 0 0 1607.31 86.20 3 4 0 0 1655.37 83.37 5 4 0 0 1663.74 85.66 1 -5 0 0 298.519 20.405 1 -5 0 0 325.315 21.274 1 -5 0 0 307.988 18.488 5 5 0 0 282.706 20.727 1 5 0 0 297.326 19.027 3 5 0 0 313.517 18.862 5 5 0 0 309.433 20.774 1 -6 0 0 428.892 27.511 1 -6 0 0 379.796 23.958 5 6 0 0 414.197 27.439 1 6 0 0 379.499 24.730 3 6 0 0 438.891 27.571 1 6 0 0 417.590 24.940 5 -7 0 0 83.2234 15.4224 1 -7 0 0 62.8332 7.6190 5 7 0 0 81.2208 8.4592 3 7 0 0 86.2496 11.6686 5 -8 0 0 356.065 26.433 1 -8 0 0 306.841 21.574 5 8 0 0 354.883 22.880 3 8 0 0 346.663 26.188 1 8 0 0 338.568 23.304 5 -9 0 0 1045.94 61.39 1 9 0 0 1015.21 57.96 3 9 0 0 921.177 60.109 1 9 0 0 1059.23 58.23 5 -10 0 0 -10.183 10.286 1 10 0 0 -0.8800 5.3903 3 10 0 0 3.98581 7.59594 1 -11 0 0 66.0502 14.9972 1 11 0 0 37.4830 9.9338 5 11 0 0 41.5979 11.4914 1 12 0 0 46.0599 11.7191 5 12 0 0 37.0687 8.8204 3 -13 0 0 789.723 55.407 1 13 0 0 766.412 50.399 5 13 0 0 739.665 53.551 1 13 0 0 784.843 48.118 3 14 0 0 160.578 19.065 5 14 0 0 153.232 16.019 3 14 0 0 199.041 23.037 1 -15 0 0 133.277 22.850 1 15 0 0 97.9720 18.6144 1 -16 0 0 324.145 33.975 1 16 0 0 274.079 30.780 1 -17 0 0 108.975 24.740 1 17 0 0 70.3847 18.4787 1 -18 0 0 475.781 45.262 1 18 0 0 416.520 41.508 1 19 0 0 56.6208 18.8482 1 20 -1 0 50.6943 23.1997 1 -20 1 0 13.6678 20.1205 1 19 -1 0 32.0488 19.7330 1 -19 1 0 77.6192 24.3787 1 18 -1 0 14.7294 18.5032 1 -18 1 0 10.5029 18.3130 1 17 -1 0 454.885 42.988 1 -17 1 0 476.202 44.875 1 16 -1 0 105.104 22.301 1 -16 1 0 77.2457 20.8447 1 15 -1 0 59.7529 13.6553 5 15 -1 0 36.9702 14.5195 1 -15 1 0 97.4562 21.4326 1 14 -1 0 342.811 25.133 3 14 -1 0 347.242 30.206 5 14 -1 0 316.455 31.841 1 -14 1 0 407.648 35.420 1 13 -1 0 315.980 31.168 1 13 -1 0 242.243 20.632 3 13 -1 0 293.234 26.694 5 -13 1 0 309.254 30.963 1 12 -1 0 980.818 61.633 1 12 -1 0 921.499 57.954 5 12 -1 0 861.952 53.570 3 -12 1 0 935.482 60.594 1 11 -1 0 -3.1682 4.9931 3 11 -1 0 -19.223 12.479 1 11 -1 0 4.77673 9.01919 5 -11 1 0 15.4697 12.5386 1 10 -1 0 334.489 22.948 3 10 -1 0 351.195 26.469 5 10 -1 0 324.621 27.344 1 -10 1 0 363.395 29.302 1 9 -1 0 -19.847 10.267 1 9 -1 0 7.88008 4.60303 3 9 -1 0 -0.6357 6.6981 5 -9 1 0 1.09395 6.58993 1 8 -1 0 1229.07 67.31 5 8 -1 0 1241.20 69.67 1 8 -1 0 1105.21 65.67 3 -8 1 0 1220.61 69.88 1 7 -1 0 352.668 21.629 3 7 -1 0 339.981 23.227 5 7 -1 0 372.204 25.783 1 -7 1 0 312.619 24.349 1 -7 1 0 321.360 22.047 5 6 -1 0 285.618 18.610 3 6 -1 0 309.987 20.327 5 6 -1 0 277.411 21.372 1 -6 1 0 325.537 22.810 1 -6 1 0 311.626 19.904 5 5 -1 0 2015.74 116.42 1 5 -1 0 2164.52 129.99 1 5 -1 0 2279.76 118.61 3 5 -1 0 2254.61 114.89 5 -5 1 0 2353.80 118.83 1 -5 1 0 2254.16 121.01 5 4 -1 0 1393.98 73.81 1 4 -1 0 1362.24 73.79 1 4 -1 0 1523.04 72.76 5 4 -1 0 1294.10 72.70 3 -4 1 0 1438.16 72.22 5 -4 1 0 1326.21 73.74 1 -4 1 0 1324.25 73.65 1 3 -1 0 4380.18 213.52 1 3 -1 0 4153.65 223.79 1 -3 1 0 4173.28 219.22 1 -3 1 0 4051.09 215.91 1 2 -1 0 315.582 18.181 1 2 -1 0 257.416 15.971 3 2 -1 0 287.398 17.595 1 -2 1 0 295.536 17.573 1 -2 1 0 281.173 16.081 3 -2 1 0 298.096 17.142 5 -2 1 0 301.710 18.166 1 0 -1 0 -0.7462 2.3800 5 0 1 0 -2.0576 1.6030 1 0 1 0 -3.6867 1.8734 1 -1 -1 0 -1.7753 1.8024 1 1 1 0 -0.0012 1.8114 1 -2 -1 0 1512.84 73.54 1 -2 -1 0 1421.21 74.03 1 2 1 0 1211.84 73.64 1 2 1 0 1527.37 73.50 1 -3 -1 0 2481.29 146.55 5 -3 -1 0 3058.41 146.85 1 -3 -1 0 2916.03 147.55 1 3 1 0 2962.49 146.95 1 3 1 0 2856.49 146.17 1 -4 -1 0 827.295 45.350 1 -4 -1 0 757.627 42.325 5 -4 -1 0 847.439 45.521 1 4 1 0 873.380 45.532 1 4 1 0 855.196 45.590 1 4 1 0 741.288 42.314 5 -5 -1 0 30.1080 4.0024 5 -5 -1 0 50.1964 10.6712 1 -5 -1 0 39.5167 6.8315 1 5 1 0 28.7921 4.2540 5 5 1 0 36.7972 11.2844 1 5 1 0 30.8957 7.2287 1 5 1 0 36.2421 5.9914 3 -6 -1 0 20.5959 2.8854 4 -6 -1 0 21.0957 7.3425 1 6 1 0 31.2756 5.8278 3 6 1 0 30.5217 6.2536 5 -7 -1 0 201.498 13.978 5 -7 -1 0 244.433 21.527 1 -7 -1 0 176.481 12.568 4 7 1 0 208.803 14.735 5 7 1 0 219.947 16.260 3 7 1 0 198.652 17.148 1 -8 -1 0 441.796 32.200 1 -8 -1 0 464.501 28.325 5 8 1 0 495.061 33.371 1 8 1 0 489.430 31.007 3 8 1 0 508.007 29.512 5 -9 -1 0 73.6840 8.2573 5 -9 -1 0 97.5732 14.0133 1 9 1 0 89.3512 10.2514 5 9 1 0 64.1757 13.0470 1 9 1 0 63.4069 9.9169 3 -10 -1 0 319.121 26.635 1 -10 -1 0 271.108 19.811 5 10 1 0 296.140 22.481 3 10 1 0 321.323 22.392 5 10 1 0 268.815 24.545 1 11 1 0 44.5653 9.2748 3 11 1 0 26.5693 12.9216 1 11 1 0 39.6597 9.0820 5 -12 -1 0 41.8427 11.2892 1 12 1 0 33.9212 9.4601 3 12 1 0 57.5995 10.1845 5 12 1 0 12.0100 12.3418 1 -13 -1 0 884.916 57.548 1 13 1 0 849.545 56.711 1 13 1 0 701.294 49.438 5 13 1 0 808.475 51.186 3 -14 -1 0 300.968 30.754 1 14 1 0 280.145 23.753 3 14 1 0 313.619 30.529 1 14 1 0 227.725 22.676 5 -15 -1 0 307.448 32.202 1 15 1 0 277.846 24.399 3 15 1 0 292.932 30.434 1 -16 -1 0 96.3027 21.8819 1 16 1 0 79.3907 19.5070 1 -17 -1 0 494.792 46.323 1 17 1 0 531.133 46.986 1 -18 -1 0 91.0714 22.4599 1 18 1 0 131.641 26.351 1 -19 -1 0 175.830 27.856 1 19 1 0 197.011 30.659 1 20 -2 0 92.7236 26.5786 1 18 -2 0 60.3514 22.0009 1 17 -2 0 110.691 24.293 1 -17 2 0 118.613 21.965 1 16 -2 0 65.5824 20.3664 1 -16 2 0 85.4248 22.1635 1 15 -2 0 274.084 27.778 5 15 -2 0 259.975 29.178 1 -15 2 0 317.540 33.286 1 14 -2 0 85.4910 17.0570 5 14 -2 0 63.0201 18.6027 1 -14 2 0 118.546 20.758 1 13 -2 0 865.644 56.119 5 13 -2 0 724.721 47.838 3 13 -2 0 895.616 58.802 1 -13 2 0 872.277 58.385 1 12 -2 0 1.99803 4.62035 3 12 -2 0 -6.9065 11.6978 5 12 -2 0 1.95298 9.50454 1 11 -2 0 257.896 19.654 3 11 -2 0 320.329 28.570 1 11 -2 0 319.991 26.680 5 -11 2 0 313.166 27.490 1 10 -2 0 109.628 14.609 5 10 -2 0 79.8489 8.8002 3 10 -2 0 106.034 14.568 1 -10 2 0 109.327 16.426 1 9 -2 0 732.557 46.367 1 9 -2 0 758.736 45.160 5 9 -2 0 622.183 39.532 3 -9 2 0 697.768 45.686 1 8 -2 0 195.043 18.295 5 8 -2 0 215.324 20.063 1 8 -2 0 180.929 13.689 3 -8 2 0 240.011 19.783 1 7 -2 0 84.4509 11.8542 5 7 -2 0 73.0034 6.7470 3 7 -2 0 60.1273 17.6586 1 -7 2 0 49.9795 9.7073 1 6 -2 0 872.113 48.974 3 6 -2 0 931.194 53.091 1 6 -2 0 907.929 51.623 5 -6 2 0 910.789 53.147 1 -6 2 0 919.688 50.919 5 5 -2 0 810.035 44.389 5 5 -2 0 759.591 44.889 1 5 -2 0 740.753 44.369 1 -5 2 0 748.691 44.540 1 -5 2 0 791.062 43.711 5 4 -2 0 4928.80 240.20 1 4 -2 0 4871.10 237.90 5 4 -2 0 4191.24 243.93 3 4 -2 0 4492.71 266.46 1 -4 2 0 4734.10 257.47 1 -4 2 0 5039.28 245.97 5 -4 2 0 4586.97 248.57 1 3 -2 0 43.6154 6.9921 5 3 -2 0 42.1413 6.7592 1 3 -2 0 38.1640 6.4428 1 -3 2 0 40.1710 5.6342 1 -3 2 0 32.2689 6.0516 1 -3 2 0 44.6884 6.6289 5 2 -2 0 2283.11 117.66 1 2 -2 0 1970.83 117.19 1 2 -2 0 2482.53 117.27 5 -2 2 0 2639.08 117.33 5 -2 2 0 2067.24 120.75 1 -2 2 0 2252.95 117.72 1 1 -2 0 3639.17 184.06 1 1 -2 0 3272.29 186.22 1 1 -2 0 3631.55 194.72 1 -1 2 0 3979.05 194.01 1 0 2 0 -20.458 9.510 1 -1 -2 0 430.582 25.064 1 1 2 0 530.392 24.727 5 1 2 0 427.980 25.027 1 -2 -2 0 31.3784 5.2837 1 -2 -2 0 32.0259 4.6730 1 2 2 0 44.5940 5.9432 1 2 2 0 30.5555 5.0700 1 -3 -2 0 1229.12 68.78 1 -3 -2 0 1323.28 68.89 1 3 2 0 1335.99 68.88 1 3 2 0 1322.02 68.70 1 -4 -2 0 207.263 14.632 1 -4 -2 0 210.640 15.241 1 4 2 0 184.128 11.801 5 4 2 0 201.002 15.005 1 4 2 0 233.891 15.256 1 -5 -2 0 474.234 28.502 1 5 2 0 442.963 28.377 1 5 2 0 432.750 24.344 5 5 2 0 447.032 27.792 1 6 2 0 12.3734 9.9704 1 6 2 0 7.18226 6.98737 5 -7 -2 0 1022.35 60.46 1 -7 -2 0 950.027 58.670 4 7 2 0 1128.90 61.18 3 7 2 0 1068.65 56.05 5 7 2 0 1113.03 61.21 1 -8 -2 0 214.698 19.804 1 8 2 0 200.121 14.936 5 8 2 0 249.779 20.634 1 -9 -2 0 745.891 47.140 1 -9 -2 0 640.564 42.043 4 9 2 0 787.112 42.739 5 9 2 0 793.764 48.260 1 9 2 0 779.503 46.500 3 -10 -2 0 364.309 29.121 1 10 2 0 330.085 25.847 3 10 2 0 349.312 23.558 5 10 2 0 335.455 27.609 1 -11 -2 0 130.514 17.758 1 11 2 0 150.540 16.262 3 11 2 0 153.807 19.699 1 11 2 0 139.844 13.841 5 -12 -2 0 98.8850 17.8249 1 12 2 0 104.344 15.912 1 12 2 0 90.4011 13.6125 3 12 2 0 90.9422 11.7691 5 -13 -2 0 70.9246 16.2931 1 13 2 0 58.0925 10.7882 5 13 2 0 72.7093 13.1889 3 -14 -2 0 517.346 41.837 1 14 2 0 485.114 36.400 3 14 2 0 494.625 41.439 1 -15 -2 0 82.7686 19.6541 1 15 2 0 91.1469 14.5905 3 15 2 0 59.4727 15.5533 1 -16 -2 0 552.834 46.816 1 16 2 0 549.497 46.287 1 16 2 0 539.154 39.797 3 -17 -2 0 112.353 21.371 1 17 2 0 153.237 27.054 1 -18 -2 0 120.699 24.897 1 18 2 0 120.466 25.231 1 -19 -2 0 92.6248 24.5892 1 19 2 0 67.3180 19.8877 1 19 -3 0 142.554 27.286 1 -19 3 0 120.239 28.245 1 -18 3 0 47.3027 22.4733 1 17 -3 0 156.570 27.563 1 -17 3 0 118.150 25.532 1 16 -3 0 397.126 38.945 1 -16 3 0 354.690 37.205 1 15 -3 0 30.0508 14.9468 5 15 -3 0 -3.3934 14.2685 1 -15 3 0 22.2323 17.6862 1 14 -3 0 375.928 35.131 1 14 -3 0 320.766 30.884 5 -14 3 0 303.456 32.975 1 13 -3 0 8.7816 12.2486 5 13 -3 0 54.7345 17.1799 1 12 -3 0 548.281 39.887 5 12 -3 0 517.696 40.364 1 12 -3 0 439.111 29.606 3 -12 3 0 544.281 40.940 1 11 -3 0 -12.746 9.814 1 11 -3 0 7.4256 10.3820 5 -11 3 0 22.5644 13.4578 1 10 -3 0 272.471 25.205 5 10 -3 0 281.380 26.016 1 -10 3 0 311.347 27.127 1 9 -3 0 26.8451 11.7425 1 9 -3 0 35.8008 10.9757 5 -9 3 0 40.9758 11.9548 1 8 -3 0 7.02987 7.06571 5 8 -3 0 -23.749 11.092 1 -8 3 0 -5.6290 13.7285 1 7 -3 0 1610.93 85.54 5 7 -3 0 1412.97 85.14 1 -7 3 0 1593.23 86.53 1 6 -3 0 1206.40 67.47 5 6 -3 0 1232.70 68.19 1 -6 3 0 1155.60 68.00 1 5 -3 0 2780.23 142.03 5 5 -3 0 2568.65 142.51 1 -5 3 0 2901.03 147.52 5 -5 3 0 2892.40 143.52 1 -5 3 0 2455.54 153.51 3 4 -3 0 16.4746 6.2620 1 4 -3 0 33.3996 10.6815 5 4 -3 0 21.2344 5.6720 1 -4 3 0 4.82774 9.32946 1 -4 3 0 14.6799 6.6700 1 -4 3 0 30.2259 6.8290 5 -4 3 0 16.7654 2.4460 3 3 -3 0 3286.20 162.77 5 3 -3 0 2984.96 163.35 1 3 -3 0 3119.71 166.08 1 -3 3 0 3285.72 162.50 5 -3 3 0 3482.55 164.28 1 -3 3 0 2866.17 163.05 1 2 -3 0 1995.66 96.53 5 2 -3 0 1777.19 96.44 1 2 -3 0 1740.98 96.35 1 -2 3 0 1730.73 96.24 1 -2 3 0 1939.33 96.26 5 -2 3 0 1877.88 96.64 1 1 -3 0 5329.22 249.46 5 1 -3 0 4448.43 253.05 1 1 -3 0 4763.02 254.79 1 -1 3 0 4723.89 256.63 1 -1 3 0 5450.64 249.56 5 0 -3 0 646.320 36.018 1 0 -3 0 621.169 35.667 1 0 -3 0 737.434 36.120 5 0 -3 0 617.818 36.493 2 0 3 0 692.089 36.023 1 0 3 0 604.825 35.715 1 0 3 0 609.100 36.404 2 -1 -3 0 283.992 16.650 5 -1 -3 0 256.954 16.980 2 -1 -3 0 291.709 17.850 1 -1 -3 0 281.538 17.401 1 1 3 0 295.895 17.744 1 1 3 0 291.014 17.391 1 -2 -3 0 1695.34 91.08 1 -2 -3 0 1591.70 100.75 1 2 3 0 1705.60 92.57 1 2 3 0 1620.25 89.06 1 2 3 0 1834.33 85.94 5 -3 -3 0 73.3439 7.4190 1 -3 -3 0 70.3019 8.8474 1 3 3 0 66.6555 6.7843 1 3 3 0 76.6147 8.7839 1 -4 -3 0 1422.69 78.26 1 -4 -3 0 1477.46 78.87 1 4 3 0 1533.16 78.96 1 4 3 0 1469.21 78.51 1 -5 -3 0 25.2005 6.1865 1 5 3 0 28.1844 3.3620 5 5 3 0 37.2905 6.8664 1 5 3 0 35.7821 7.7232 1 6 3 0 19.9170 3.5160 5 6 3 0 36.3727 8.8106 1 -7 -3 0 6.32483 7.81189 1 7 3 0 7.90693 8.50854 5 7 3 0 -10.540 19.444 1 -8 -3 0 728.747 45.253 4 -8 -3 0 813.724 48.713 1 8 3 0 746.398 47.755 1 8 3 0 822.384 48.709 3 8 3 0 796.660 42.454 5 -9 -3 0 40.4317 11.8220 1 -9 -3 0 43.4751 5.9922 4 9 3 0 53.8672 6.4945 5 9 3 0 55.6321 11.4155 1 9 3 0 56.2213 10.6065 3 -10 -3 0 17.4885 10.8233 1 -10 -3 0 20.9555 4.1787 4 10 3 0 37.6597 10.5478 3 10 3 0 25.7493 9.1222 1 10 3 0 31.1815 5.9515 5 -11 -3 0 534.629 39.408 1 11 3 0 525.706 32.720 5 11 3 0 535.421 37.873 3 11 3 0 553.038 39.669 1 -12 -3 0 541.104 40.941 1 12 3 0 610.111 40.476 3 12 3 0 515.082 34.153 5 12 3 0 570.178 42.311 1 -13 -3 0 527.731 40.844 1 13 3 0 438.859 31.262 5 13 3 0 500.763 39.896 1 13 3 0 512.054 37.121 3 -14 -3 0 61.9828 16.6126 1 14 3 0 77.3002 19.2279 1 14 3 0 42.6309 12.1110 3 -15 -3 0 322.009 32.420 1 15 3 0 268.413 29.372 1 15 3 0 287.873 27.206 3 -16 -3 0 103.611 20.809 1 16 3 0 58.8680 19.3320 1 16 3 0 67.0420 15.3800 3 -17 -3 0 391.158 40.577 1 17 3 0 450.416 42.178 1 -18 -3 0 20.9523 19.1074 1 18 3 0 20.1044 17.3458 1 -19 -3 0 10.0548 16.5984 1 19 3 0 42.5774 21.3903 1 19 -4 0 88.4140 25.0673 1 -19 4 0 122.437 25.058 1 18 -4 0 153.780 29.274 1 -18 4 0 125.162 27.424 1 17 -4 0 303.115 34.146 1 -17 4 0 300.723 36.780 1 16 -4 0 5.6549 12.6269 5 16 -4 0 2.3623 17.5256 1 15 -4 0 411.801 39.229 1 15 -4 0 354.074 35.859 5 -15 4 0 438.374 40.756 1 14 -4 0 61.8368 19.0548 1 -14 4 0 30.4328 16.1005 1 13 -4 0 185.426 22.068 5 13 -4 0 148.914 21.329 1 -13 4 0 169.798 24.607 1 12 -4 0 42.2983 14.8134 5 -12 4 0 -7.4371 13.8456 1 11 -4 0 63.2574 16.1765 1 11 -4 0 83.9251 16.7241 5 -11 4 0 77.7856 14.5732 1 10 -4 0 15.5140 11.5587 5 10 -4 0 9.0798 11.4463 1 -10 4 0 -1.1615 8.0249 1 9 -4 0 260.669 24.385 5 9 -4 0 274.946 25.227 1 -9 4 0 249.225 23.484 1 8 -4 0 402.603 24.452 4 8 -4 0 432.312 31.260 5 8 -4 0 377.791 29.813 1 -8 4 0 413.674 31.355 1 7 -4 0 -18.167 10.528 5 7 -4 0 10.2850 12.1989 1 -7 4 0 -7.9847 7.3088 1 6 -4 0 1744.91 93.59 1 6 -4 0 1703.67 93.07 5 -6 4 0 1631.78 93.12 1 5 -4 0 144.655 14.187 5 5 -4 0 134.567 14.369 1 -5 4 0 120.511 8.560 3 -5 4 0 149.044 15.370 1 4 -4 0 2216.90 117.00 1 4 -4 0 2274.77 116.87 5 -4 4 0 2091.38 116.68 1 -4 4 0 2237.90 123.52 5 3 -4 0 195.220 15.032 1 3 -4 0 226.155 16.855 5 3 -4 0 181.687 14.841 1 -3 4 0 200.863 15.299 5 -3 4 0 171.791 15.190 1 -3 4 0 187.845 15.264 1 2 -4 0 1318.56 70.01 5 2 -4 0 1281.40 69.81 1 2 -4 0 1172.00 69.27 1 -2 4 0 1303.40 69.91 1 -2 4 0 1329.07 69.92 1 -2 4 0 1346.51 70.03 5 1 -4 0 263.333 18.212 1 1 -4 0 272.641 18.575 1 1 -4 0 297.665 20.296 5 -1 4 0 273.210 18.556 1 -1 4 0 270.675 19.139 1 -1 4 0 292.555 19.279 5 0 -4 0 338.870 20.776 2 0 -4 0 375.130 21.553 5 0 -4 0 324.595 21.496 1 0 -4 0 326.634 21.727 1 0 4 0 316.247 21.014 1 0 4 0 380.628 21.964 5 0 4 0 362.273 22.219 1 0 4 0 316.071 20.513 2 -1 -4 0 871.574 50.365 1 -1 -4 0 898.478 52.161 2 -1 -4 0 962.692 49.924 5 -1 -4 0 916.217 50.696 1 1 4 0 865.372 52.210 2 1 4 0 1016.42 51.42 1 1 4 0 991.688 50.337 5 1 4 0 937.965 50.618 1 -2 -4 0 10.5912 3.8904 2 -2 -4 0 16.0891 4.8932 5 -2 -4 0 6.14253 6.63069 1 -2 -4 0 15.1880 4.6696 1 2 4 0 12.2113 3.7619 5 2 4 0 6.32526 3.93148 1 -3 -4 0 867.772 46.441 1 -3 -4 0 867.196 46.736 1 3 4 0 815.304 43.734 5 3 4 0 822.839 46.130 1 3 4 0 803.350 46.183 1 -4 -4 0 369.426 31.599 1 -4 -4 0 346.145 23.512 1 4 4 0 399.979 31.969 1 4 4 0 352.541 20.320 5 4 4 0 393.029 23.963 1 -5 -4 0 66.3539 8.6074 1 5 4 0 52.7391 8.2029 1 5 4 0 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890.563 51.025 1 1 7 -3 586.878 34.889 1 1 7 -3 488.436 32.799 5 1 7 -3 516.729 35.400 2 1 7 -3 532.890 33.681 1 -1 -7 3 583.099 33.817 5 -1 -7 3 509.642 33.594 1 -1 -7 3 555.945 36.100 2 0 7 -3 103.826 13.000 1 0 7 -3 119.603 12.455 1 0 7 -3 126.243 13.564 2 0 -7 3 115.416 12.505 2 0 -7 3 128.259 13.838 5 0 -7 3 142.041 14.112 1 -1 7 -3 3503.89 192.76 1 -1 7 -3 3786.61 206.23 2 -1 7 -3 3697.71 199.58 1 1 -7 3 3898.21 193.51 1 1 -7 3 3604.27 191.12 5 -2 7 -3 -12.041 8.727 2 -2 7 -3 -9.3006 5.6644 3 -2 7 -3 0.37282 8.34235 1 -2 7 -3 -12.376 8.246 1 2 -7 3 -25.500 12.260 1 2 -7 3 -8.9992 16.4498 5 -3 7 -3 698.380 42.700 3 -3 7 -3 729.559 46.014 1 3 -7 3 808.818 46.652 1 3 -7 3 749.883 46.379 5 -4 7 -3 730.966 42.699 3 -4 7 -3 737.967 47.028 1 4 -7 3 746.606 47.801 5 4 -7 3 827.433 47.767 1 -5 7 -3 675.462 39.436 3 -5 7 -3 765.644 46.807 1 5 -7 3 734.666 46.061 1 5 -7 3 704.760 46.651 5 -6 7 -3 331.592 26.418 1 -6 7 -3 317.945 26.023 1 6 -7 3 322.864 26.667 5 6 -7 3 335.074 27.028 1 -7 7 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1560.55 80.56 1 4 6 -3 1571.65 86.05 3 4 6 -3 1292.79 76.90 5 4 6 -3 1471.63 79.86 1 -4 -6 3 1483.69 80.15 1 -4 -6 3 1512.90 76.91 5 3 6 -3 140.559 11.045 5 3 6 -3 140.833 15.236 3 3 6 -3 135.333 12.039 1 3 6 -3 159.018 13.255 1 -3 -6 3 156.890 15.017 2 -3 -6 3 152.114 12.811 1 -3 -6 3 155.261 11.823 5 2 6 -3 123.211 10.931 5 2 6 -3 119.596 11.272 1 2 6 -3 113.469 13.217 2 2 6 -3 127.315 11.652 1 2 6 -3 163.377 15.278 3 -2 -6 3 132.479 11.676 5 -2 -6 3 137.122 12.980 2 -2 -6 3 126.735 11.790 1 1 6 -3 -2.9315 6.1436 2 1 6 -3 3.5140 26.0289 5 1 6 -3 -3.5847 5.8122 1 1 6 -3 -5.8988 21.6578 1 1 6 -3 -11.195 25.848 3 -1 -6 3 -1.0715 8.4012 5 -1 -6 3 -8.7306 5.2789 2 -1 -6 3 -1.8019 3.9560 1 0 6 -3 860.067 51.986 2 0 6 -3 806.959 49.188 3 0 6 -3 795.606 47.745 1 0 6 -3 888.281 49.185 1 0 6 -3 783.159 47.575 5 0 -6 3 792.771 48.030 1 0 -6 3 917.844 52.560 2 0 -6 3 889.654 48.252 5 -1 6 -3 210.906 16.623 1 -1 6 -3 184.340 17.550 2 -1 6 -3 209.378 17.566 1 -1 6 -3 169.561 14.999 3 1 -6 3 215.703 17.157 1 1 -6 3 215.740 17.598 5 -2 6 -3 1996.55 106.15 1 -2 6 -3 2014.73 106.40 1 -2 6 -3 1835.49 105.98 3 -2 6 -3 1943.30 113.38 2 2 -6 3 1930.53 105.43 5 2 -6 3 2159.32 106.47 1 -3 6 -3 268.374 17.944 3 -3 6 -3 293.030 21.713 1 -3 6 -3 290.792 21.311 1 3 -6 3 248.537 20.784 1 3 -6 3 267.398 21.070 5 -4 6 -3 105.976 12.495 1 -4 6 -3 89.2757 9.0655 3 4 -6 3 115.939 27.760 5 4 -6 3 133.288 19.183 1 -5 6 -3 1266.54 68.33 1 5 -6 3 1102.32 67.05 5 5 -6 3 1118.09 66.89 1 -6 6 -3 238.631 21.514 1 6 -6 3 246.419 22.625 5 6 -6 3 266.240 22.541 1 -7 6 -3 10.9385 12.8616 1 7 -6 3 25.0577 11.2785 1 7 -6 3 -2.7624 10.0634 5 8 -6 3 28.9368 12.5984 1 8 -6 3 37.3698 13.3128 5 -9 6 -3 470.618 36.881 1 9 -6 3 417.722 28.178 4 9 -6 3 457.555 36.356 5 9 -6 3 494.774 36.618 1 -10 6 -3 550.688 42.708 1 10 -6 3 586.221 43.990 1 10 -6 3 617.467 44.742 5 -11 6 -3 355.594 33.927 1 11 -6 3 351.126 33.668 5 11 -6 3 358.006 33.253 1 -12 6 -3 86.3412 20.5276 1 12 -6 3 69.6581 19.1651 1 12 -6 3 123.710 21.550 5 -13 6 -3 174.577 23.922 1 13 -6 3 173.347 26.018 1 13 -6 3 201.643 26.048 5 -14 6 -3 338.295 36.056 1 14 -6 3 340.530 35.643 1 14 -6 3 295.230 34.068 5 -15 6 -3 168.541 28.843 1 15 -6 3 153.473 23.597 1 15 -6 3 180.395 28.714 5 -16 6 -3 60.9674 20.3385 1 16 -6 3 93.8948 23.0459 5 16 -6 3 40.1962 20.7926 1 -17 6 -3 7.2601 20.5727 1 17 -6 3 24.0214 18.5857 1 17 -6 3 -14.363 18.089 5 -18 6 -3 193.359 29.966 1 18 -6 3 145.559 29.974 1 -19 6 -3 23.4363 23.0690 1 18 5 -3 102.202 24.731 1 17 5 -3 243.675 29.620 3 17 5 -3 230.642 30.165 1 -17 -5 3 261.709 31.385 1 16 5 -3 225.919 26.842 3 16 5 -3 258.632 30.838 1 -16 -5 3 175.768 25.613 1 15 5 -3 217.558 27.403 1 15 5 -3 228.321 26.886 3 -15 -5 3 187.382 25.476 1 14 5 -3 201.635 24.549 3 14 5 -3 177.177 24.074 1 -14 -5 3 151.004 22.402 1 13 5 -3 64.8050 17.7679 3 -13 -5 3 73.6725 14.5872 1 12 5 -3 463.244 38.122 3 12 5 -3 472.090 37.312 1 -12 -5 3 451.993 36.326 1 11 5 -3 -6.8534 12.2411 3 11 5 -3 8.6516 12.2587 1 -11 -5 3 -9.4819 10.5154 1 10 5 -3 76.9908 15.3142 3 10 5 -3 84.0540 14.7258 1 9 5 -3 157.618 16.998 1 9 5 -3 180.688 19.366 3 -9 -5 3 181.249 18.532 1 8 5 -3 934.268 55.689 1 8 5 -3 919.390 59.181 3 -8 -5 3 921.753 55.166 1 7 5 -3 11.6067 5.7403 1 7 5 -3 3.54317 8.32792 1 -7 -5 3 -8.6740 7.6913 1 6 5 -3 192.196 16.932 1 6 5 -3 221.449 21.186 3 6 5 -3 225.193 17.273 1 -6 -5 3 240.687 18.386 1 5 5 -3 2070.05 108.89 3 5 5 -3 1992.92 104.37 1 5 5 -3 1684.11 101.80 1 -5 -5 3 1972.34 102.70 1 4 5 -3 243.315 16.727 1 4 5 -3 235.520 16.981 1 4 5 -3 201.640 13.420 5 4 5 -3 228.156 19.303 3 -4 -5 3 239.236 14.095 5 -4 -5 3 262.345 17.283 1 3 5 -3 835.114 45.118 1 3 5 -3 753.796 42.611 5 3 5 -3 828.434 48.914 3 3 5 -3 782.971 44.572 1 -3 -5 3 838.622 43.250 5 -3 -5 3 794.699 44.837 1 -3 -5 3 802.183 44.805 1 -3 -5 3 790.526 49.494 2 2 5 -3 705.352 43.015 3 2 5 -3 752.915 44.751 2 2 5 -3 684.638 39.701 1 2 5 -3 733.397 40.399 1 2 5 -3 699.701 38.970 5 -2 -5 3 715.828 39.149 5 -2 -5 3 710.839 43.948 2 -2 -5 3 661.207 39.674 1 -2 -5 3 727.106 40.204 1 1 5 -3 1112.55 66.10 3 1 5 -3 1184.20 63.76 1 1 5 -3 1134.80 62.80 5 1 5 -3 1182.48 69.23 2 1 5 -3 1206.08 64.06 1 -1 -5 3 1107.95 63.45 1 -1 -5 3 1301.56 63.39 5 -1 -5 3 1173.10 63.74 1 -1 -5 3 1201.02 69.19 2 0 5 -3 1661.53 89.62 5 0 5 -3 1617.63 91.04 3 0 5 -3 1585.79 89.06 1 0 5 -3 1664.59 96.13 2 0 5 -3 1776.14 89.14 1 0 -5 3 1630.86 87.96 5 0 -5 3 1689.07 96.28 2 0 -5 3 1728.10 88.99 1 0 -5 3 1734.16 89.39 1 -1 5 -3 2259.10 125.95 2 -1 5 -3 2190.32 118.49 3 -1 5 -3 2043.86 119.74 5 -1 5 -3 1980.78 116.17 1 -1 5 -3 2253.97 116.82 1 1 -5 3 2524.67 117.24 1 1 -5 3 2240.90 116.70 1 1 -5 3 2273.89 116.13 5 -2 5 -3 242.505 16.508 3 -2 5 -3 234.349 19.171 2 -2 5 -3 255.820 18.272 1 -2 5 -3 259.264 21.810 1 2 -5 3 248.321 18.939 5 2 -5 3 261.652 18.539 1 -3 5 -3 144.494 10.007 3 -3 5 -3 144.563 13.098 1 -3 5 -3 150.158 13.798 1 3 -5 3 119.310 13.764 5 3 -5 3 109.719 11.818 1 -4 5 -3 795.945 47.567 1 4 -5 3 771.722 48.627 5 4 -5 3 833.845 47.671 1 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21.6268 5 17 -5 3 37.8357 18.6025 1 -18 5 -3 5.0142 21.1574 1 18 -5 3 24.6107 21.2684 1 -19 5 -3 150.207 27.898 1 19 -5 3 221.901 34.223 1 18 4 -3 135.819 25.284 1 17 4 -3 163.454 26.595 1 17 4 -3 122.694 21.310 3 -17 -4 3 150.152 24.207 1 16 4 -3 320.106 34.516 1 16 4 -3 346.323 33.529 3 -16 -4 3 388.704 36.841 1 15 4 -3 148.803 21.477 3 15 4 -3 163.180 23.827 1 -15 -4 3 142.209 22.399 1 14 4 -3 3.4104 12.4237 3 -14 -4 3 16.0434 12.9311 1 13 4 -3 679.770 49.161 1 13 4 -3 666.172 48.786 3 -13 -4 3 657.367 47.815 1 12 4 -3 139.834 18.470 1 12 4 -3 127.864 20.037 3 11 4 -3 145.821 18.945 3 11 4 -3 141.685 19.011 1 -11 -4 3 158.230 18.678 1 10 4 -3 22.7557 10.6588 1 10 4 -3 23.9834 8.7664 3 -10 -4 3 11.9180 9.0286 1 9 4 -3 491.739 35.218 1 9 4 -3 492.696 37.004 3 -9 -4 3 548.082 35.791 1 8 4 -3 110.356 16.037 3 8 4 -3 134.306 14.243 1 8 4 -3 124.065 14.711 1 -8 -4 3 144.686 15.207 1 7 4 -3 380.692 25.839 1 7 4 -3 328.963 25.292 1 7 4 -3 403.706 29.357 3 -7 -4 3 397.882 26.875 1 6 4 -3 141.458 12.764 1 6 4 -3 146.299 14.299 1 6 4 -3 158.268 16.964 3 -6 -4 3 135.679 12.726 1 -6 -4 3 127.970 12.756 4 5 4 -3 131.029 11.371 1 5 4 -3 142.866 14.813 3 5 4 -3 122.981 11.658 1 -5 -4 3 122.311 11.592 1 -5 -4 3 117.003 11.833 4 4 4 -3 1147.52 60.61 1 4 4 -3 1132.03 60.83 1 4 4 -3 1201.32 65.30 3 -4 -4 3 1221.34 61.24 1 -4 -4 3 976.084 59.987 1 -4 -4 3 1063.58 65.13 4 3 4 -3 139.665 13.907 3 3 4 -3 138.999 10.467 1 3 4 -3 130.274 10.357 1 3 4 -3 123.004 8.641 5 -3 -4 3 137.474 10.326 1 -3 -4 3 111.289 8.498 5 -3 -4 3 142.122 12.988 2 -3 -4 3 126.705 10.392 1 2 4 -3 2807.14 163.56 5 2 4 -3 3246.81 166.07 2 2 4 -3 2577.45 153.63 1 2 4 -3 2894.00 152.44 1 2 4 -3 2985.82 158.73 3 -2 -4 3 3057.96 170.64 2 -2 -4 3 3007.80 157.72 1 -2 -4 3 3287.06 151.19 5 -2 -4 3 2935.48 165.27 1 1 4 -3 1007.27 52.89 1 1 4 -3 1036.13 58.31 2 1 4 -3 977.695 52.165 5 1 4 -3 1026.62 55.71 3 1 4 -3 826.424 52.102 1 -1 -4 3 967.863 52.636 1 -1 -4 3 1082.86 52.53 5 -1 -4 3 972.152 57.762 2 -1 -4 3 918.858 52.367 1 0 4 -3 2179.27 129.26 1 0 4 -3 2625.71 133.42 3 0 4 -3 2536.69 140.35 2 0 4 -3 2678.75 129.74 1 0 4 -3 2373.40 134.03 5 0 -4 3 2537.86 140.49 2 0 -4 3 2490.90 134.74 1 0 -4 3 2560.76 129.79 1 0 -4 3 2615.79 128.83 5 -1 4 -3 657.267 44.764 2 -1 4 -3 667.574 41.032 5 -1 4 -3 805.571 41.520 1 -1 4 -3 720.268 41.502 3 -1 4 -3 703.101 41.233 1 1 -4 3 763.913 41.651 5 1 -4 3 779.993 41.387 1 1 -4 3 800.315 44.991 1 -2 4 -3 234.462 17.529 5 -2 4 -3 250.080 17.368 1 -2 4 -3 271.459 18.015 1 -2 4 -3 248.272 15.809 3 2 -4 3 260.460 18.327 5 2 -4 3 227.034 16.695 1 -3 4 -3 127.960 12.393 1 -3 4 -3 154.707 12.751 1 -3 4 -3 117.329 8.865 3 3 -4 3 121.922 12.282 5 3 -4 3 155.338 13.017 1 -4 4 -3 49.2545 8.7082 1 4 -4 3 48.5906 11.0885 1 -5 4 -3 1427.11 84.05 1 5 -4 3 1636.63 84.70 1 5 -4 3 1523.95 83.84 5 -6 4 -3 0.46273 6.92585 1 6 -4 3 -2.4943 8.3099 1 6 -4 3 -11.406 10.153 5 -7 4 -3 69.0110 12.8990 1 7 -4 3 55.8348 5.8323 4 7 -4 3 55.2164 12.1070 1 -8 4 -3 86.9983 13.2105 1 8 -4 3 75.1460 14.0981 1 8 -4 3 96.7500 13.0852 5 8 -4 3 74.4099 6.5591 4 -9 4 -3 1162.40 69.06 1 9 -4 3 1062.91 67.72 1 9 -4 3 1136.67 67.36 5 -10 4 -3 491.244 37.056 1 10 -4 3 417.517 35.047 1 10 -4 3 460.404 35.554 5 -11 4 -3 570.954 43.358 1 11 -4 3 604.839 44.367 1 11 -4 3 613.044 44.045 5 -12 4 -3 87.2484 19.2944 1 12 -4 3 57.7774 17.8587 1 12 -4 3 112.847 19.064 5 -13 4 -3 317.885 32.950 1 13 -4 3 255.776 28.086 1 13 -4 3 308.076 31.442 5 -14 4 -3 433.100 39.423 1 14 -4 3 503.183 40.462 5 14 -4 3 413.870 40.044 1 -15 4 -3 -3.4713 18.0993 1 15 -4 3 -28.197 16.437 1 -16 4 -3 112.193 24.429 1 16 -4 3 113.644 22.993 5 16 -4 3 101.057 24.431 1 -17 4 -3 34.5995 20.1137 1 17 -4 3 20.9505 20.0970 1 -18 4 -3 97.7744 27.1787 1 18 -4 3 156.702 26.537 1 -19 4 -3 116.131 27.099 1 19 -4 3 115.643 27.120 1 18 3 -3 88.9716 23.8674 1 17 3 -3 229.623 26.196 3 17 3 -3 247.908 30.995 1 -17 -3 3 300.489 32.634 1 16 3 -3 333.160 31.608 3 16 3 -3 361.188 34.119 1 -16 -3 3 324.240 33.801 1 15 3 -3 48.9519 17.6454 1 15 3 -3 30.7645 12.9263 3 -15 -3 3 51.9091 16.6996 1 14 3 -3 223.622 25.954 1 14 3 -3 215.469 24.101 3 -14 -3 3 230.536 25.475 1 13 3 -3 130.271 18.532 1 13 3 -3 133.526 19.171 3 12 3 -3 499.585 37.066 1 12 3 -3 438.918 35.146 3 -12 -3 3 410.479 34.128 1 11 3 -3 25.0544 9.9023 1 11 3 -3 28.3543 11.8756 3 -11 -3 3 17.3403 8.2460 4 10 3 -3 401.088 30.594 3 10 3 -3 440.709 31.265 1 -10 -3 3 318.295 25.489 4 -10 -3 3 387.621 29.630 1 9 3 -3 62.2453 10.5998 3 -9 -3 3 59.7754 11.1461 1 -9 -3 3 51.5218 7.4406 4 8 3 -3 178.920 18.003 3 8 3 -3 171.927 16.380 1 8 3 -3 189.379 17.636 1 -8 -3 3 172.691 16.676 1 -8 -3 3 164.392 14.469 4 7 3 -3 309.034 22.596 1 7 3 -3 373.477 24.622 1 7 3 -3 295.017 24.521 3 -7 -3 3 290.709 22.464 4 -7 -3 3 382.248 24.344 1 6 3 -3 217.910 18.661 3 6 3 -3 221.996 17.494 1 6 3 -3 217.253 16.835 1 -6 -3 3 244.247 17.766 1 -6 -3 3 223.667 17.244 4 5 3 -3 516.856 33.250 1 5 3 -3 594.848 33.525 1 5 3 -3 560.576 36.397 3 -5 -3 3 555.889 35.234 4 -5 -3 3 620.375 34.129 1 4 3 -3 353.650 21.794 1 4 3 -3 391.555 44.507 3 4 3 -3 351.211 22.097 1 -4 -3 3 372.479 21.862 1 -4 -3 3 323.212 23.511 4 -4 -3 3 377.386 22.327 1 3 3 -3 2136.28 111.51 3 3 3 -3 1963.40 105.93 1 3 3 -3 2043.65 107.98 1 -3 -3 3 2017.93 118.77 4 -3 -3 3 2022.92 105.95 1 -3 -3 3 2118.61 116.64 2 -3 -3 3 2099.61 107.90 1 2 3 -3 346.046 19.983 1 2 3 -3 386.815 23.501 3 2 3 -3 346.140 23.887 2 2 3 -3 349.604 19.959 1 2 3 -3 347.243 19.541 5 -2 -3 3 341.287 19.346 5 -2 -3 3 382.409 24.358 2 -2 -3 3 342.050 19.887 1 -2 -3 3 305.937 19.690 1 -2 -3 3 389.099 23.043 3 -2 -3 3 312.240 22.382 4 1 3 -3 4446.97 203.50 3 1 3 -3 3998.11 213.41 2 1 3 -3 3662.66 212.44 5 -1 -3 3 3816.14 209.00 1 -1 -3 3 3711.90 204.91 1 -1 -3 3 3826.51 220.20 2 -1 -3 3 3579.18 206.95 5 0 3 -3 1211.86 63.68 3 0 3 -3 1077.32 61.10 1 0 3 -3 1083.50 67.32 2 0 3 -3 1145.69 61.02 1 0 3 -3 1016.97 60.70 5 0 -3 3 1272.41 61.26 1 0 -3 3 1188.68 61.26 1 0 -3 3 1272.76 61.57 5 0 -3 3 1135.17 67.42 2 0 -3 3 1248.31 63.47 3 -1 3 -3 4849.03 235.36 1 -1 3 -3 4429.61 235.17 1 -1 3 -3 4431.35 236.56 5 -1 3 -3 5132.49 241.10 3 -1 3 -3 4540.66 259.85 2 1 -3 3 4416.34 242.06 1 1 -3 3 4603.39 235.90 1 1 -3 3 4681.66 233.90 5 -2 3 -3 1910.22 100.09 1 -2 3 -3 2054.74 100.24 1 -2 3 -3 1662.00 104.97 3 -2 3 -3 1867.12 99.55 5 2 -3 3 1975.26 100.05 1 2 -3 3 1983.82 100.09 1 2 -3 3 1986.35 99.95 5 2 -3 3 1874.30 101.28 3 -3 3 -3 245.296 17.319 5 -3 3 -3 270.141 18.078 1 -3 3 -3 248.462 17.458 1 3 -3 3 240.990 16.513 4 3 -3 3 268.404 18.723 5 3 -3 3 249.665 17.576 1 3 -3 3 220.163 18.711 3 -4 3 -3 256.945 19.330 1 -4 3 -3 298.807 20.580 1 4 -3 3 305.769 20.990 5 4 -3 3 260.187 17.950 4 4 -3 3 298.757 20.125 1 -5 3 -3 61.8879 9.3194 1 5 -3 3 52.7418 5.7847 4 5 -3 3 54.9723 10.1484 5 5 -3 3 66.8488 10.3560 1 -6 3 -3 1316.26 77.02 1 6 -3 3 1389.44 76.32 5 6 -3 3 1423.51 77.38 1 -7 3 -3 65.0681 12.9729 1 7 -3 3 55.4252 5.1040 4 7 -3 3 87.8849 14.0766 5 -8 3 -3 564.375 37.796 1 8 -3 3 542.321 36.088 5 8 -3 3 503.936 36.395 1 -9 3 -3 91.2762 19.9811 1 9 -3 3 97.2243 15.3578 5 9 -3 3 77.3702 14.9945 1 -10 3 -3 412.615 32.904 1 10 -3 3 396.167 32.147 5 10 -3 3 452.747 34.201 1 -11 3 -3 105.939 24.176 1 11 -3 3 149.836 19.794 1 11 -3 3 103.433 18.092 5 -12 3 -3 114.102 20.093 1 12 -3 3 134.762 20.666 1 12 -3 3 128.677 18.465 5 -13 3 -3 280.352 30.351 1 13 -3 3 270.513 28.122 5 13 -3 3 232.855 27.424 1 -14 3 -3 37.7232 15.0078 1 14 -3 3 57.3704 18.1387 1 -15 3 -3 343.199 36.466 1 15 -3 3 332.281 33.480 5 15 -3 3 322.786 34.445 1 -16 3 -3 -8.9054 18.7514 1 16 -3 3 51.6550 19.7143 1 16 -3 3 50.6535 18.0704 5 -17 3 -3 109.146 24.609 1 17 -3 3 133.569 26.211 1 -18 3 -3 64.3994 21.5717 1 18 -3 3 102.758 25.959 1 -19 3 -3 48.1453 24.9004 1 19 2 -3 97.9545 24.4856 1 18 2 -3 25.4782 18.1353 1 17 2 -3 257.744 30.222 1 -17 -2 3 274.335 32.204 1 16 2 -3 97.8967 21.5439 1 16 2 -3 95.1761 16.6158 3 -16 -2 3 96.6412 20.8879 1 15 2 -3 265.141 25.046 3 15 2 -3 226.136 27.850 1 -15 -2 3 213.713 26.757 1 14 2 -3 48.4397 13.2186 3 -14 -2 3 52.3731 13.4527 1 13 2 -3 418.926 36.696 1 13 2 -3 467.974 35.598 3 -13 -2 3 497.905 38.630 1 12 2 -3 296.043 26.579 3 12 2 -3 265.481 25.979 1 -12 -2 3 337.279 28.749 1 11 2 -3 567.257 35.214 5 11 2 -3 652.827 44.499 1 11 2 -3 672.205 43.969 3 -11 -2 3 720.664 45.151 1 -11 -2 3 599.782 38.857 4 10 2 -3 418.334 29.752 1 10 2 -3 341.487 27.628 3 10 2 -3 329.664 20.697 5 -10 -2 3 379.247 27.870 1 -10 -2 3 331.345 23.477 4 -10 -2 3 318.367 20.386 5 9 2 -3 24.6420 7.8843 1 9 2 -3 30.0198 10.3109 3 -9 -2 3 23.9861 5.3154 4 -9 -2 3 31.2694 10.0746 1 -9 -2 3 16.7456 3.3942 5 8 2 -3 180.159 17.088 3 -8 -2 3 185.400 16.141 1 -8 -2 3 131.026 9.541 5 -8 -2 3 135.785 12.504 4 7 2 -3 94.6501 12.3087 3 7 2 -3 93.8496 10.6961 1 -7 -2 3 71.6599 5.6170 5 -7 -2 3 77.7349 10.6835 1 -7 -2 3 72.3353 8.3701 4 6 2 -3 2100.73 110.65 3 6 2 -3 2116.06 106.85 1 6 2 -3 1773.50 105.95 1 -6 -2 3 2063.33 106.75 1 -6 -2 3 2000.81 115.53 4 5 2 -3 302.914 19.456 1 5 2 -3 331.885 38.506 3 5 2 -3 305.567 19.801 1 -5 -2 3 300.415 19.652 1 -5 -2 3 252.325 19.458 4 -5 -2 3 282.421 29.678 3 4 2 -3 3150.64 162.04 1 4 2 -3 3178.09 164.77 1 4 2 -3 3307.33 170.16 3 -4 -2 3 3167.86 160.36 1 -4 -2 3 2772.66 173.07 4 -4 -2 3 3078.71 158.72 1 -4 -2 3 3021.09 165.99 3 3 2 -3 416.119 23.604 1 3 2 -3 455.111 26.981 3 3 2 -3 421.141 23.467 1 -3 -2 3 376.143 23.146 1 -3 -2 3 396.994 25.871 3 -3 -2 3 409.732 26.079 4 -3 -2 3 435.334 28.092 2 -3 -2 3 397.062 23.480 1 2 2 -3 372.656 21.328 1 2 2 -3 456.692 25.195 3 2 2 -3 357.620 24.457 4 2 2 -3 454.045 26.469 2 -2 -2 3 374.178 21.296 1 -2 -2 3 378.946 24.116 3 -2 -2 3 363.612 21.320 1 -2 -2 3 422.326 24.880 4 -2 -2 3 350.784 20.950 5 1 2 -3 3001.01 142.68 2 1 2 -3 2648.80 140.07 4 1 2 -3 2722.86 135.66 3 1 2 -3 2407.19 143.26 5 -1 -2 3 2419.04 142.27 5 -1 -2 3 2432.07 132.87 1 -1 -2 3 2263.53 142.39 1 -1 -2 3 2790.73 140.01 4 -1 -2 3 2353.75 141.43 2 0 2 -3 3020.79 164.50 4 0 2 -3 3425.87 159.21 3 0 2 -3 3029.79 155.49 1 0 2 -3 2753.64 163.06 1 0 2 -3 3069.04 153.34 5 0 2 -3 2736.39 166.83 2 0 -2 3 3001.31 164.24 4 0 -2 3 3071.34 153.24 5 0 -2 3 2599.44 166.58 2 0 -2 3 3183.97 153.48 1 0 -2 3 3471.75 159.09 3 -1 2 -3 110.383 8.792 3 -1 2 -3 122.778 8.899 1 -1 2 -3 127.604 9.854 5 -1 2 -3 103.082 10.446 2 -1 2 -3 106.346 8.082 1 1 -2 3 141.950 10.173 5 1 -2 3 134.611 9.843 4 1 -2 3 127.690 8.520 1 1 -2 3 101.349 7.999 1 1 -2 3 123.952 8.839 3 -2 2 -3 1675.76 89.84 1 -2 2 -3 1681.02 89.96 1 -2 2 -3 1525.25 90.37 3 -2 2 -3 1751.99 89.91 5 2 -2 3 1735.01 94.70 4 2 -2 3 1864.62 90.13 1 2 -2 3 1812.03 90.11 5 2 -2 3 1676.28 90.53 3 2 -2 3 1845.28 90.11 1 -3 2 -3 1738.27 88.49 1 -3 2 -3 1631.31 87.59 5 -3 2 -3 1574.94 88.12 1 3 -2 3 1790.60 88.24 5 3 -2 3 1619.44 88.02 1 3 -2 3 1691.42 88.19 1 -4 2 -3 106.959 10.966 1 -4 2 -3 106.980 10.355 5 -4 2 -3 109.110 10.686 1 4 -2 3 102.529 10.935 5 4 -2 3 95.5568 10.5082 1 4 -2 3 106.462 10.856 1 4 -2 3 87.6618 7.6494 4 -5 2 -3 343.181 25.719 1 -5 2 -3 386.064 26.230 1 5 -2 3 452.004 27.095 1 -6 2 -3 130.393 13.716 1 6 -2 3 121.733 14.553 1 6 -2 3 151.890 14.309 5 -7 2 -3 836.922 52.453 1 7 -2 3 905.575 53.131 1 7 -2 3 886.751 51.394 5 -8 2 -3 115.581 16.351 1 8 -2 3 139.350 15.905 1 8 -2 3 145.152 15.699 5 -9 2 -3 1616.93 87.54 1 9 -2 3 1503.62 84.28 5 9 -2 3 1365.13 85.26 1 10 -2 3 45.4699 13.3420 1 10 -2 3 16.5342 9.0812 5 -11 2 -3 101.940 17.907 1 11 -2 3 87.8800 14.9656 5 11 -2 3 82.5386 15.8129 1 -12 2 -3 354.016 33.446 1 12 -2 3 359.180 32.592 1 12 -2 3 379.356 31.239 5 13 -2 3 4.0398 14.8352 1 -14 2 -3 371.598 35.120 1 14 -2 3 331.199 31.388 5 14 -2 3 358.282 35.028 1 -15 2 -3 60.4383 20.3647 1 15 -2 3 68.1273 17.4554 5 15 -2 3 48.8554 18.2355 1 -16 2 -3 254.897 32.311 1 16 -2 3 176.969 25.841 1 16 -2 3 264.442 28.978 5 -17 2 -3 116.271 25.234 1 17 -2 3 63.8114 21.9731 1 -18 2 -3 90.8486 25.9915 1 18 -2 3 85.5008 23.7289 1 -19 2 -3 159.948 29.849 1 19 -2 3 184.855 30.182 1 -20 2 -3 27.2712 20.9273 1 20 -2 3 20.7763 23.7514 1 19 1 -3 73.6699 22.0687 1 18 1 -3 188.692 28.026 1 -18 -1 3 136.718 25.821 1 17 1 -3 70.3790 20.2177 1 -17 -1 3 63.0710 19.9439 1 16 1 -3 341.755 35.093 1 16 1 -3 316.980 28.509 3 -16 -1 3 338.051 34.061 1 15 1 -3 53.2831 12.5606 3 14 1 -3 315.222 27.096 3 14 1 -3 294.891 30.327 1 -14 -1 3 341.716 31.136 1 13 1 -3 57.0892 8.1507 5 13 1 -3 82.2855 13.9771 3 12 1 -3 239.426 24.730 1 12 1 -3 199.072 16.762 5 12 1 -3 263.650 22.548 3 -12 -1 3 246.299 23.813 1 11 1 -3 131.159 18.139 1 11 1 -3 154.718 16.377 3 11 1 -3 119.314 11.265 5 -11 -1 3 115.197 10.662 5 -11 -1 3 135.453 11.217 4 -11 -1 3 113.424 15.714 1 10 1 -3 165.522 13.061 5 10 1 -3 156.747 16.223 3 -10 -1 3 164.425 17.351 1 -10 -1 3 169.085 13.173 4 -10 -1 3 160.628 12.365 5 9 1 -3 477.729 33.234 1 9 1 -3 493.801 28.246 5 9 1 -3 446.146 32.005 3 -9 -1 3 480.158 32.613 1 -9 -1 3 439.763 29.356 4 -9 -1 3 475.467 27.390 5 8 1 -3 185.882 17.062 3 8 1 -3 194.981 13.265 5 8 1 -3 182.687 17.535 1 -8 -1 3 173.622 13.897 4 -8 -1 3 173.134 16.115 1 -8 -1 3 184.383 12.581 5 7 1 -3 1667.65 89.59 1 7 1 -3 1658.47 87.96 1 7 1 -3 1619.84 83.14 5 7 1 -3 1688.06 90.02 3 -7 -1 3 1520.81 82.51 5 -7 -1 3 1578.96 89.64 4 -7 -1 3 1494.35 87.08 1 6 1 -3 43.2545 8.3789 1 6 1 -3 39.0956 6.0980 4 6 1 -3 39.1212 7.1229 1 6 1 -3 35.7553 7.0861 3 -6 -1 3 39.1377 10.0204 4 -6 -1 3 26.2770 6.9360 1 -6 -1 3 35.1820 4.5044 5 -6 -1 3 38.9378 72.0211 3 5 1 -3 2644.51 140.99 1 5 1 -3 2377.19 145.22 4 5 1 -3 2637.94 137.81 1 5 1 -3 2775.45 141.88 3 -5 -1 3 2666.81 137.44 1 -5 -1 3 2767.61 153.29 5 -5 -1 3 2776.19 154.98 3 -5 -1 3 2539.03 144.36 4 4 1 -3 351.310 23.152 3 4 1 -3 311.057 20.951 1 4 1 -3 341.679 22.507 4 4 1 -3 340.959 21.383 1 -4 -1 3 370.567 21.588 1 -4 -1 3 376.891 23.599 3 -4 -1 3 357.721 19.632 5 -4 -1 3 353.953 22.595 4 -4 -1 3 359.437 21.579 1 3 1 -3 1622.80 83.47 1 3 1 -3 1615.49 83.45 1 3 1 -3 1428.40 88.94 4 -3 -1 3 1782.64 88.96 3 -3 -1 3 1682.82 83.58 1 -3 -1 3 1545.46 83.33 1 -3 -1 3 1635.36 89.77 4 2 1 -3 604.688 34.459 1 2 1 -3 666.407 38.676 4 2 1 -3 793.454 38.705 3 -2 -1 3 674.162 38.482 4 -2 -1 3 625.683 34.520 1 -2 -1 3 610.969 34.504 1 1 1 -3 345.789 22.321 4 1 1 -3 360.620 21.810 3 1 1 -3 369.680 23.168 2 -1 -1 3 373.440 21.729 3 -1 -1 3 317.268 21.767 4 0 1 -3 722.268 39.333 2 0 1 -3 668.849 34.027 1 0 1 -3 649.182 37.737 4 0 1 -3 619.178 36.019 3 0 -1 3 567.011 34.697 1 0 -1 3 689.666 39.015 2 0 -1 3 699.779 36.300 3 0 -1 3 652.740 37.519 4 0 -1 3 588.188 34.735 5 -1 1 -3 55.2194 5.2708 1 -1 1 -3 45.2386 5.7252 4 -1 1 -3 44.3403 4.4758 1 -1 1 -3 47.8890 5.8077 3 -1 1 -3 60.7046 6.6336 5 1 -1 3 52.9670 5.2766 3 1 -1 3 52.7918 4.8898 1 1 -1 3 59.2785 6.1183 4 1 -1 3 52.7626 4.7374 1 -2 1 -3 3925.16 196.20 5 -2 1 -3 3788.51 197.30 1 -2 1 -3 3727.91 197.71 1 2 -1 3 3904.59 208.49 4 2 -1 3 4209.23 196.41 5 2 -1 3 4139.52 197.50 1 2 -1 3 3300.82 211.63 3 2 -1 3 4040.08 197.30 1 -3 1 -3 258.819 16.815 4 -3 1 -3 308.309 18.224 1 -3 1 -3 293.420 18.362 1 3 -1 3 278.034 17.884 1 3 -1 3 239.516 16.645 4 3 -1 3 292.986 18.253 5 3 -1 3 251.916 17.452 1 -4 1 -3 2239.62 110.48 1 -4 1 -3 2306.26 109.16 5 -4 1 -3 2203.86 110.53 1 -4 1 -3 1852.28 115.26 4 4 -1 3 1979.32 109.80 1 4 -1 3 2387.42 109.49 5 4 -1 3 1767.94 115.69 4 4 -1 3 2026.92 109.87 1 -5 1 -3 95.5773 9.7653 5 -5 1 -3 128.291 14.522 1 -5 1 -3 122.016 12.279 1 5 -1 3 132.226 12.794 5 5 -1 3 99.7324 7.6458 4 5 -1 3 115.813 12.434 1 -6 1 -3 18.7766 8.9609 1 6 -1 3 22.3702 7.8800 1 6 -1 3 15.3005 7.6977 5 -7 1 -3 84.2155 11.5449 1 7 -1 3 100.372 10.971 5 7 -1 3 82.4314 13.3300 1 -8 1 -3 1335.90 74.13 1 8 -1 3 1255.29 71.16 5 8 -1 3 1237.16 73.52 1 8 -1 3 1267.06 68.64 3 -9 1 -3 1070.43 62.24 1 9 -1 3 962.539 55.139 3 9 -1 3 1067.16 59.39 5 9 -1 3 916.008 60.256 1 -10 1 -3 362.233 30.706 1 10 -1 3 372.229 28.023 5 10 -1 3 344.174 22.790 3 10 -1 3 389.920 30.697 1 -11 1 -3 143.458 18.503 1 11 -1 3 156.572 17.503 5 11 -1 3 136.379 11.880 3 11 -1 3 183.368 21.087 1 -12 1 -3 132.621 18.832 1 12 -1 3 130.175 11.831 3 12 -1 3 118.626 16.483 5 12 -1 3 167.747 22.517 1 -13 1 -3 513.161 40.348 1 13 -1 3 431.495 38.356 1 13 -1 3 416.500 28.137 3 13 -1 3 487.763 35.776 5 -14 1 -3 15.0152 17.3236 1 14 -1 3 0.2449 10.5166 5 14 -1 3 20.0868 15.2689 1 -15 1 -3 192.549 27.714 1 15 -1 3 145.488 24.088 1 15 -1 3 206.694 23.731 5 16 -1 3 91.2764 18.0921 5 -17 1 -3 132.486 27.053 1 17 -1 3 158.355 24.833 1 -18 1 -3 177.972 29.636 1 18 -1 3 197.692 28.016 1 19 -1 3 36.2504 17.5409 1 -20 1 -3 67.9219 25.2216 1 20 -1 3 51.8230 19.4902 1 19 0 -3 323.718 38.359 1 18 0 -3 112.699 24.998 1 -18 0 3 96.4869 22.6993 1 17 0 -3 261.490 32.379 1 -17 0 3 251.465 29.844 1 16 0 -3 56.1828 19.9388 1 -16 0 3 68.1261 16.4312 1 15 0 -3 226.831 27.383 1 15 0 -3 200.193 20.336 3 -15 0 3 189.512 25.228 1 14 0 -3 205.411 20.701 3 14 0 -3 252.966 27.314 1 -14 0 3 213.069 25.784 1 13 0 -3 499.884 36.115 5 13 0 -3 640.204 45.028 1 13 0 -3 538.498 39.138 3 -13 0 3 664.414 45.337 1 12 0 -3 10.3938 8.4205 3 12 0 -3 10.4476 9.3919 1 11 0 -3 113.328 17.261 1 11 0 -3 115.354 14.045 3 11 0 -3 113.362 12.417 5 -11 0 3 151.705 18.477 1 10 0 -3 873.285 54.577 3 10 0 -3 932.980 56.696 1 10 0 -3 917.358 51.965 5 -10 0 3 892.752 50.480 5 -10 0 3 892.261 55.877 1 9 0 -3 88.6378 16.0472 3 9 0 -3 70.6805 10.2276 5 -9 0 3 57.5748 7.4420 5 8 0 -3 989.674 54.276 5 8 0 -3 980.275 57.433 3 8 0 -3 964.300 57.600 1 -8 0 3 982.716 53.432 5 -8 0 3 1017.34 57.95 1 -8 0 3 933.351 56.043 4 7 0 -3 133.712 10.787 5 7 0 -3 102.071 9.821 4 7 0 -3 123.363 13.369 1 7 0 -3 96.8806 11.8708 1 7 0 -3 114.200 12.067 3 -7 0 3 111.244 12.971 1 -7 0 3 126.021 10.199 5 -7 0 3 102.925 9.708 4 6 0 -3 1981.96 105.11 1 6 0 -3 2008.95 105.00 1 6 0 -3 1828.31 108.36 4 6 0 -3 2015.14 103.38 5 6 0 -3 1995.98 107.18 3 -6 0 3 2003.64 116.07 3 -6 0 3 2034.46 110.57 5 -6 0 3 1980.54 108.75 4 -6 0 3 1916.54 104.96 1 5 0 -3 869.327 48.826 1 5 0 -3 825.751 50.137 4 5 0 -3 810.480 49.784 3 5 0 -3 939.205 47.140 5 5 0 -3 866.367 48.926 1 -5 0 3 920.198 50.465 3 -5 0 3 855.953 48.930 1 -5 0 3 891.816 50.352 4 -5 0 3 896.275 47.445 5 4 0 -3 1566.52 79.60 3 4 0 -3 1473.21 76.74 1 4 0 -3 1309.67 80.28 4 4 0 -3 1300.83 76.17 1 -4 0 3 1475.05 77.15 1 -4 0 3 1485.85 80.81 4 -4 0 3 1409.62 77.71 5 -4 0 3 1573.72 79.58 3 -4 0 3 1471.40 76.75 1 3 0 -3 2181.93 114.48 3 3 0 -3 2033.30 110.37 1 3 0 -3 2082.76 117.42 4 3 0 -3 2090.10 110.40 1 -3 0 3 2231.72 117.81 4 -3 0 3 2107.98 112.49 1 -3 0 3 2281.97 117.70 3 -3 0 3 2216.55 115.73 1 2 0 -3 45.3138 6.4720 3 2 0 -3 41.6615 5.9270 4 2 0 -3 43.4167 4.1639 1 2 0 -3 36.6227 5.3819 1 -2 0 3 51.8983 11.5930 3 -2 0 3 42.2188 8.6826 1 -2 0 3 49.8317 5.4378 4 -2 0 3 45.9560 4.9775 1 1 0 -3 59.4941 7.4374 4 1 0 -3 68.9783 4.5622 1 1 0 -3 71.7337 7.5675 3 1 0 -3 79.2945 8.3343 2 -1 0 3 79.1462 7.0336 2 -1 0 3 61.3718 6.1446 3 -1 0 3 64.7146 4.3924 1 -1 0 3 55.0635 6.0982 4 0 0 -3 107.005 7.112 1 0 0 -3 132.843 9.718 4 0 0 -3 130.971 9.425 3 0 0 3 117.918 9.292 4 0 0 3 125.270 7.192 1 0 0 3 151.169 10.624 2 0 0 3 129.476 9.178 3 0 0 3 115.341 7.146 1 -1 0 -3 2557.45 132.24 2 -1 0 -3 2555.11 129.67 4 -1 0 -3 2509.31 121.59 1 -1 0 -3 2448.27 121.55 1 1 0 3 2233.92 129.30 4 1 0 3 2376.44 121.45 1 1 0 3 2069.90 121.25 1 -2 0 -3 428.338 24.433 1 -2 0 -3 421.364 24.486 1 -2 0 -3 412.618 25.145 4 2 0 3 433.105 24.412 1 2 0 3 414.196 24.335 1 2 0 3 448.606 25.189 5 2 0 3 425.741 25.230 4 -3 0 -3 180.403 13.478 1 -3 0 -3 228.941 14.372 1 -3 0 -3 168.456 12.220 4 3 0 3 196.724 13.885 1 3 0 3 224.708 14.270 5 3 0 3 203.028 13.962 1 3 0 3 166.422 12.322 4 -4 0 -3 1826.17 90.39 5 -4 0 -3 1808.14 91.85 1 -4 0 -3 1626.66 91.26 1 4 0 3 1755.50 90.01 5 4 0 3 1786.68 91.67 1 4 0 3 1543.93 90.85 1 -5 0 -3 818.065 44.857 5 -5 0 -3 753.297 45.996 1 -5 0 -3 779.593 46.153 1 5 0 3 855.717 46.635 1 5 0 3 792.468 44.769 5 -6 0 -3 445.306 28.702 1 -6 0 -3 403.351 26.294 5 6 0 3 409.613 28.072 1 6 0 3 423.969 26.749 5 -7 0 -3 856.590 54.594 1 7 0 3 961.423 55.795 1 7 0 3 978.537 53.158 5 -8 0 -3 708.741 46.609 1 8 0 3 792.584 47.819 1 8 0 3 743.067 44.434 5 -9 0 -3 309.096 26.918 1 9 0 3 327.730 26.989 1 9 0 3 304.104 20.930 3 9 0 3 317.468 23.909 5 -10 0 -3 372.926 31.406 1 10 0 3 370.225 27.281 5 10 0 3 382.811 31.010 1 10 0 3 376.798 24.732 3 -11 0 -3 56.6454 14.7484 1 11 0 3 57.7203 14.2655 1 11 0 3 65.2535 8.6572 3 11 0 3 68.2739 12.0682 5 -12 0 -3 207.956 24.472 1 12 0 3 198.404 22.283 1 12 0 3 220.803 21.408 5 12 0 3 212.238 17.089 3 -13 0 -3 260.100 29.019 1 13 0 3 223.109 24.601 1 13 0 3 211.850 22.800 5 13 0 3 229.930 18.777 3 -14 0 -3 656.183 48.095 1 14 0 3 535.702 35.354 3 14 0 3 551.152 40.746 5 14 0 3 491.348 42.585 1 -15 0 -3 89.0130 21.0576 1 15 0 3 101.980 20.286 1 15 0 3 55.6569 14.5042 5 -16 0 -3 23.4436 17.9161 1 16 0 3 19.1531 17.9507 1 -17 0 -3 277.015 35.388 1 17 0 3 260.914 33.390 1 -18 0 -3 185.912 30.023 1 18 0 3 183.036 31.236 1 -19 0 -3 172.415 29.276 1 19 0 3 222.960 33.258 1 20 0 3 86.7661 25.7133 1 19 -1 -3 84.2432 23.0261 1 18 -1 -3 301.146 34.656 1 -18 1 3 341.819 37.809 1 17 -1 -3 40.7456 18.3502 1 16 -1 -3 195.866 28.013 1 -16 1 3 252.699 29.631 1 15 -1 -3 103.984 21.114 1 -15 1 3 119.821 19.939 1 14 -1 -3 117.195 19.917 1 14 -1 -3 110.694 14.288 5 14 -1 -3 117.462 14.564 3 -14 1 3 121.093 20.122 1 13 -1 -3 142.221 16.373 3 13 -1 -3 174.647 21.900 1 13 -1 -3 180.425 17.860 5 -13 1 3 212.701 24.088 1 12 -1 -3 170.025 16.687 3 12 -1 -3 143.121 20.654 1 12 -1 -3 178.481 17.458 5 -12 1 3 179.672 20.622 1 11 -1 -3 124.401 13.872 3 11 -1 -3 125.849 14.468 5 11 -1 -3 138.835 17.503 1 -11 1 3 134.917 19.018 1 10 -1 -3 8.00799 6.73869 3 10 -1 -3 -7.3259 7.0284 5 10 -1 -3 -9.6216 11.7291 1 -10 1 3 7.71814 8.14843 1 9 -1 -3 1277.42 71.27 5 9 -1 -3 1302.06 72.94 3 9 -1 -3 1291.80 74.30 1 9 -1 -3 1188.97 71.53 4 -9 1 3 1339.70 74.52 1 8 -1 -3 19.0597 5.2655 4 8 -1 -3 46.3423 13.7272 1 8 -1 -3 41.7563 14.7520 5 -8 1 3 -3.8008 21.3883 1 7 -1 -3 1032.85 59.51 1 7 -1 -3 1043.92 57.41 5 7 -1 -3 940.569 58.528 1 7 -1 -3 1021.52 58.73 3 7 -1 -3 957.476 58.343 4 -7 1 3 1078.37 59.56 1 -7 1 3 1105.45 57.19 5 -7 1 3 1047.11 59.16 3 6 -1 -3 52.2592 6.6605 4 6 -1 -3 41.2739 10.5044 1 6 -1 -3 70.2279 8.3926 5 6 -1 -3 54.1621 8.5781 1 6 -1 -3 46.7004 8.1917 3 -6 1 3 50.9085 8.5329 1 -6 1 3 65.2133 7.6998 5 -6 1 3 50.4950 7.7890 3 5 -1 -3 689.606 43.977 4 5 -1 -3 754.551 43.880 3 5 -1 -3 727.342 43.426 1 5 -1 -3 796.250 42.694 5 5 -1 -3 769.598 43.649 1 -5 1 3 786.678 44.341 4 -5 1 3 777.896 44.092 3 -5 1 3 783.745 44.046 1 -5 1 3 775.729 42.760 5 4 -1 -3 1301.30 68.71 1 4 -1 -3 1233.80 68.44 1 4 -1 -3 1385.48 67.95 5 4 -1 -3 1151.71 69.68 3 4 -1 -3 1245.42 71.73 4 -4 1 3 1322.16 68.11 5 -4 1 3 1377.01 72.05 4 -4 1 3 1331.38 70.39 3 -4 1 3 1308.72 68.77 1 -4 1 3 1180.92 68.24 1 3 -1 -3 820.957 44.959 1 3 -1 -3 824.157 46.470 3 3 -1 -3 853.973 47.803 4 3 -1 -3 774.487 44.846 1 -3 1 3 880.540 44.723 5 -3 1 3 836.536 47.651 4 -3 1 3 831.088 45.092 1 -3 1 3 814.679 44.941 1 -3 1 3 844.941 46.555 3 2 -1 -3 420.557 25.328 3 2 -1 -3 416.428 23.870 1 2 -1 -3 448.597 26.315 4 2 -1 -3 419.080 23.998 1 -2 1 3 431.730 25.410 3 -2 1 3 421.737 24.005 1 -2 1 3 409.325 25.868 4 -2 1 3 404.345 23.806 1 -2 1 3 472.526 24.295 5 1 -1 -3 843.823 43.667 2 1 -1 -3 699.185 39.477 1 1 -1 -3 756.450 43.293 4 1 -1 -3 699.617 39.670 1 -1 1 3 851.671 40.126 1 -1 1 3 682.054 39.404 1 -1 1 3 765.371 43.238 4 -1 1 3 832.973 43.742 2 -1 1 3 646.105 41.269 3 0 -1 -3 3215.63 176.39 2 0 -1 -3 3445.58 163.96 1 0 -1 -3 3126.45 174.78 4 0 1 3 3045.14 176.32 2 0 1 3 3359.95 163.82 1 -1 -1 -3 564.116 31.042 4 -1 -1 -3 541.454 31.702 2 -1 -1 -3 527.329 28.459 1 -1 -1 -3 537.190 28.577 1 1 1 3 485.939 28.342 1 1 1 3 469.245 28.168 1 -2 -1 -3 197.790 13.115 1 -2 -1 -3 212.393 13.726 4 -2 -1 -3 219.067 13.641 1 2 1 3 179.880 12.765 1 2 1 3 189.356 13.041 1 -3 -1 -3 617.823 80.617 1 -3 -1 -3 710.399 36.187 1 3 1 3 591.948 35.554 1 3 1 3 584.324 41.511 1 -4 -1 -3 1450.71 82.79 1 -4 -1 -3 1675.28 83.58 1 4 1 3 1474.28 82.84 1 4 1 3 1577.98 83.28 1 4 1 3 1617.79 81.64 5 -5 -1 -3 633.557 39.627 1 -5 -1 -3 658.248 38.104 4 -5 -1 -3 739.149 40.790 1 5 1 3 644.889 39.720 1 5 1 3 712.728 38.582 5 -6 -1 -3 366.236 23.501 4 -6 -1 -3 461.065 28.352 1 6 1 3 433.138 28.213 1 6 1 3 389.943 25.137 5 7 1 3 56.0903 8.6290 5 7 1 3 42.9824 15.1472 1 -8 -1 -3 592.838 39.100 1 8 1 3 597.621 35.924 5 8 1 3 560.144 38.135 1 -9 -1 -3 754.207 49.722 1 9 1 3 830.206 47.215 5 9 1 3 796.941 51.055 1 -10 -1 -3 108.769 17.841 1 10 1 3 84.4803 12.2840 5 10 1 3 74.1312 15.2536 1 10 1 3 69.0430 9.8145 3 -11 -1 -3 574.942 41.585 1 11 1 3 544.138 40.623 1 11 1 3 546.492 36.689 5 11 1 3 545.400 35.542 3 -12 -1 -3 116.542 17.577 1 12 1 3 120.750 15.244 5 12 1 3 128.429 19.541 1 12 1 3 121.656 13.458 3 -13 -1 -3 415.743 37.432 1 13 1 3 446.138 33.013 5 13 1 3 417.761 30.335 3 13 1 3 459.740 38.302 1 -14 -1 -3 396.391 36.220 1 14 1 3 300.604 31.031 1 14 1 3 323.359 25.867 3 14 1 3 367.855 29.651 5 -15 -1 -3 110.942 22.085 1 15 1 3 112.977 17.133 5 15 1 3 108.729 20.800 1 16 1 3 82.2594 21.9382 1 17 1 3 175.265 28.771 1 -18 -1 -3 518.354 48.728 1 18 1 3 514.431 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47.713 1 8 4 -4 798.479 51.252 3 8 4 -4 799.899 46.783 1 -8 -4 4 721.274 46.619 1 7 4 -4 126.650 16.329 3 7 4 -4 112.060 11.986 1 7 4 -4 96.9372 12.5559 1 -7 -4 4 139.842 13.377 1 6 4 -4 1123.32 66.96 3 6 4 -4 1009.08 61.29 1 6 4 -4 1202.77 62.82 1 -6 -4 4 1144.15 62.48 1 5 4 -4 2065.47 106.88 1 5 4 -4 2146.38 113.61 3 5 4 -4 1856.29 106.68 1 -5 -4 4 2075.90 107.22 1 4 4 -4 63.1129 9.6370 3 4 4 -4 57.0313 6.7340 1 4 4 -4 59.2172 7.3282 1 -4 -4 4 66.5985 7.2220 1 -4 -4 4 66.6190 5.0532 5 -4 -4 4 56.4529 11.1138 1 3 4 -4 1594.30 80.91 1 3 4 -4 1605.32 80.90 1 3 4 -4 1505.10 86.13 3 -3 -4 4 1413.88 84.44 5 -3 -4 4 1474.15 80.67 1 -3 -4 4 1496.99 85.62 1 -3 -4 4 1655.79 88.52 4 -3 -4 4 1601.52 90.36 2 2 4 -4 2.50098 6.57364 3 2 4 -4 -12.063 10.434 2 2 4 -4 -2.1537 6.5059 1 2 4 -4 1.23326 3.91167 1 2 4 -4 -4.5766 3.9175 5 -2 -4 4 5.55026 4.42517 2 -2 -4 4 -14.837 16.056 4 -2 -4 4 -0.3970 8.4882 5 -2 -4 4 4.73040 2.76628 1 -2 -4 4 -0.8894 2.8997 1 1 4 -4 782.901 43.198 1 1 4 -4 779.199 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63.01 1 1 3 -4 1390.18 68.20 3 1 3 -4 1149.87 65.07 5 -1 -3 4 1114.92 63.60 1 -1 -3 4 1323.78 67.52 3 -1 -3 4 1042.69 64.23 1 -1 -3 4 1335.90 71.34 2 -1 -3 4 1134.94 63.28 5 -1 -3 4 1211.40 69.27 4 0 3 -4 1150.10 63.81 3 0 3 -4 1059.42 67.88 2 0 3 -4 1077.21 60.60 1 0 3 -4 1153.65 60.52 1 0 3 -4 1150.66 61.43 5 0 -3 4 1288.91 64.10 3 0 -3 4 1172.22 60.52 1 0 -3 4 1150.82 60.65 1 0 -3 4 1139.59 66.14 4 0 -3 4 1160.41 68.25 2 0 -3 4 1246.81 61.73 5 -1 3 -4 18.9295 7.3331 2 -1 3 -4 27.1246 4.9046 1 -1 3 -4 21.3889 4.2242 1 -1 3 -4 15.9397 4.9300 3 -1 3 -4 21.6763 4.8697 5 1 -3 4 22.5182 5.6478 4 1 -3 4 25.8873 4.8079 3 1 -3 4 30.7926 7.8452 2 1 -3 4 32.5283 7.1316 5 1 -3 4 22.8637 7.5774 1 -2 3 -4 1273.87 66.49 1 -2 3 -4 1178.26 67.44 3 -2 3 -4 1354.22 66.65 1 -2 3 -4 1158.44 66.40 5 -2 3 -4 1224.08 73.09 2 2 -3 4 1339.01 67.34 5 2 -3 4 1214.47 70.64 3 2 -3 4 1295.75 66.34 1 2 -3 4 1139.20 65.82 1 -3 3 -4 1032.10 55.30 1 -3 3 -4 970.430 55.397 5 -3 3 -4 1051.67 55.51 1 3 -3 4 992.502 54.957 1 3 -3 4 1018.05 53.70 3 3 -3 4 912.120 54.562 1 3 -3 4 966.912 56.921 4 3 -3 4 1053.49 56.00 5 -4 3 -4 -4.0084 12.3282 1 -4 3 -4 -1.5943 4.3462 1 4 -3 4 -9.5851 7.7122 5 4 -3 4 0.08823 3.07146 4 4 -3 4 -3.0493 8.9307 1 4 -3 4 -0.0204 2.5934 3 -5 3 -4 346.743 25.148 1 5 -3 4 386.545 26.113 5 5 -3 4 339.411 22.764 4 5 -3 4 392.161 25.833 1 -6 3 -4 67.7151 16.9720 1 6 -3 4 50.4927 12.9912 5 6 -3 4 51.4031 11.7243 1 6 -3 4 59.8355 6.0557 4 -7 3 -4 612.754 40.238 1 7 -3 4 663.015 40.477 5 7 -3 4 559.820 35.647 4 7 -3 4 670.025 41.259 1 8 -3 4 147.244 18.789 1 8 -3 4 135.988 17.103 5 -9 3 -4 1322.49 83.16 1 9 -3 4 1444.42 82.24 5 9 -3 4 1522.89 84.33 1 -10 3 -4 123.921 19.764 1 10 -3 4 183.954 21.092 5 10 -3 4 178.566 19.399 1 -11 3 -4 503.515 38.572 1 11 -3 4 420.528 34.408 5 11 -3 4 491.767 37.876 1 -12 3 -4 230.110 28.445 1 12 -3 4 305.969 28.583 5 12 -3 4 313.419 29.883 1 -13 3 -4 59.4803 16.8959 1 13 -3 4 79.3487 19.3918 1 13 -3 4 48.8188 16.1826 5 -14 3 -4 328.062 35.609 1 14 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5 5 -5 889.128 49.828 1 5 5 -5 927.398 50.477 1 -5 -5 5 800.805 49.530 1 4 5 -5 776.742 55.420 3 4 5 -5 803.065 43.120 1 4 5 -5 749.264 42.641 1 -4 -5 5 780.589 42.933 1 -4 -5 5 715.246 40.666 5 3 5 -5 3309.22 167.95 3 3 5 -5 3324.22 175.60 2 3 5 -5 3103.96 158.92 1 3 5 -5 3180.39 162.25 5 3 5 -5 2869.20 169.85 1 -3 -5 5 3144.12 159.02 1 -3 -5 5 3034.87 199.17 1 -3 -5 5 2718.96 183.22 5 2 5 -5 559.513 30.888 5 2 5 -5 520.772 30.303 1 2 5 -5 556.839 36.783 2 2 5 -5 540.318 34.983 3 2 5 -5 468.092 30.015 1 -2 -5 5 536.227 30.571 5 -2 -5 5 489.801 30.193 1 -2 -5 5 532.548 30.166 1 1 5 -5 47.2147 6.2971 1 1 5 -5 53.1366 7.3371 5 1 5 -5 58.3104 9.9239 3 1 5 -5 45.1698 6.6176 1 1 5 -5 47.0513 10.5535 2 -1 -5 5 51.4734 7.2656 5 -1 -5 5 55.0011 6.5978 1 -1 -5 5 55.3638 6.3101 1 0 5 -5 424.483 25.084 1 0 5 -5 376.975 26.978 3 0 5 -5 375.616 25.717 5 0 5 -5 424.883 30.491 2 0 5 -5 398.632 25.501 1 0 -5 5 433.893 26.320 5 0 -5 5 431.858 26.648 3 0 -5 5 395.903 25.136 1 0 -5 5 409.901 24.791 1 0 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53.134 1 4 3 6 980.942 53.750 1 -5 -3 -6 843.771 52.167 1 5 3 6 954.857 52.975 1 -6 -3 -6 329.025 26.009 1 6 3 6 381.076 26.866 1 -7 -3 -6 46.9517 11.0640 1 7 3 6 70.4925 10.8706 5 7 3 6 76.6055 12.9817 1 -8 -3 -6 1667.80 90.41 1 -8 -3 -6 1557.18 88.76 4 8 3 6 1520.79 88.88 1 8 3 6 1536.17 86.15 5 -9 -3 -6 36.5422 6.9179 4 -9 -3 -6 63.5499 14.2004 1 9 3 6 45.5704 8.5307 5 9 3 6 52.4516 12.7410 1 -10 -3 -6 1381.16 74.42 1 -10 -3 -6 1050.06 67.39 4 10 3 6 1103.03 71.43 1 10 3 6 1247.57 68.99 5 -11 -3 -6 33.8851 16.2595 1 11 3 6 6.9706 11.1654 1 -12 -3 -6 514.372 42.046 1 12 3 6 625.979 40.351 5 12 3 6 600.456 44.658 1 -13 -3 -6 29.6996 16.0911 1 -14 -3 -6 173.112 26.226 1 14 3 6 210.957 22.196 5 14 3 6 204.043 27.734 1 -15 -3 -6 108.741 23.184 1 15 3 6 70.1157 14.9863 5 15 3 6 122.743 22.251 1 15 3 6 95.3563 14.5949 3 -16 -3 -6 130.755 22.132 1 16 3 6 121.977 25.135 1 -17 -3 -6 170.406 28.714 1 17 3 6 117.859 22.591 1 18 3 6 44.6626 21.4859 1 20 3 6 80.1529 22.6549 1 18 -4 -6 114.351 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9 -5 -6 2.3615 10.6707 1 -9 5 6 10.3372 9.7396 1 8 -5 -6 40.1436 9.5422 4 8 -5 -6 51.6955 12.8144 1 7 -5 -6 882.807 55.502 1 7 -5 -6 878.887 55.981 4 -7 5 6 942.229 55.852 1 6 -5 -6 717.473 46.764 1 6 -5 -6 736.001 47.753 4 -6 5 6 786.373 47.234 1 5 -5 -6 294.476 24.391 4 5 -5 -6 350.485 25.631 1 -5 5 6 330.027 25.011 1 4 -5 -6 395.148 28.543 1 4 -5 -6 391.105 28.211 1 -4 5 6 448.081 29.399 1 3 -5 -6 394.595 28.834 1 3 -5 -6 436.216 28.708 1 -3 5 6 462.807 30.029 1 -3 5 6 413.113 28.582 2 2 -5 -6 142.667 13.353 1 2 -5 -6 124.572 13.455 1 -2 5 6 110.221 11.061 2 -2 5 6 132.943 14.156 1 1 -5 -6 1680.12 94.71 1 1 -5 -6 1842.82 95.55 1 -1 5 6 1852.82 95.62 1 -1 5 6 1656.67 101.56 2 0 -5 -6 203.205 14.218 2 0 -5 -6 198.399 17.053 1 0 -5 -6 224.474 17.356 1 0 5 6 228.167 17.687 1 0 5 6 193.044 14.552 2 -1 -5 -6 30.7119 6.2644 2 -1 -5 -6 31.6224 7.2770 1 -1 -5 -6 29.2978 8.5746 1 1 5 6 29.9942 9.1906 1 -2 -5 -6 129.212 11.952 2 -2 -5 -6 147.751 13.740 1 -2 -5 -6 128.194 12.319 1 2 5 6 157.671 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39.6949 16.9179 1 15 -6 -6 302.531 35.350 1 -15 6 6 371.317 37.038 1 14 -6 -6 105.570 22.728 1 -14 6 6 111.351 22.788 1 13 -6 -6 133.546 23.128 1 -13 6 6 150.018 22.805 1 12 -6 -6 -2.2302 10.1229 1 -12 6 6 -23.813 14.620 1 11 -6 -6 562.568 38.803 4 11 -6 -6 558.083 43.538 1 11 -6 -6 553.684 43.321 5 -11 6 6 591.662 43.863 1 10 -6 -6 56.0445 13.0504 1 10 -6 -6 52.4021 14.4211 5 10 -6 -6 56.3351 11.1367 4 -10 6 6 48.2430 14.9593 1 9 -6 -6 147.529 15.946 4 9 -6 -6 164.653 20.357 5 9 -6 -6 126.578 19.341 1 8 -6 -6 5.9637 10.9728 5 8 -6 -6 -3.8199 7.3601 4 -8 6 6 28.4231 11.4975 1 7 -6 -6 106.086 13.994 4 7 -6 -6 120.038 15.636 5 7 -6 -6 111.263 17.031 1 -7 6 6 108.286 14.681 1 6 -6 -6 1247.17 72.34 1 6 -6 -6 1057.21 71.99 4 -6 6 6 1363.16 72.89 1 5 -6 -6 481.340 35.441 1 -5 6 6 446.945 32.668 1 4 -6 -6 581.017 39.499 1 -4 6 6 591.483 39.264 1 -3 6 6 62.2905 10.5235 1 2 -6 -6 994.901 62.049 1 2 -6 -6 1063.01 62.87 1 -2 6 6 1193.96 64.28 1 1 -6 -6 204.271 17.403 1 1 -6 -6 191.664 17.149 1 -1 6 6 177.254 13.734 2 -1 6 6 235.560 18.907 1 0 -6 -6 115.263 13.233 1 0 -6 -6 89.9496 11.7011 1 0 6 6 112.060 12.368 1 0 6 6 103.849 8.542 2 -1 -6 -6 273.832 20.662 1 -1 -6 -6 248.446 19.547 1 -1 -6 -6 227.068 15.861 2 1 6 6 278.700 20.643 1 -2 -6 -6 775.319 43.546 1 -2 -6 -6 686.986 41.559 2 2 6 6 654.508 42.308 1 -3 -6 -6 3453.60 171.17 1 3 6 6 3051.39 170.23 1 -4 -6 -6 9.6371 20.4683 1 -5 -6 -6 53.6482 19.8917 1 5 6 6 40.2322 10.6177 1 -6 -6 -6 175.114 18.568 1 6 6 6 160.743 16.742 1 -7 -6 -6 2278.90 129.93 1 7 6 6 2496.15 130.94 1 -8 -6 -6 81.0507 14.7805 1 8 6 6 87.9376 16.1736 1 -9 -6 -6 887.927 55.097 1 9 6 6 762.755 53.539 1 -10 -6 -6 -3.5254 11.9356 1 10 6 6 2.26586 7.99360 5 10 6 6 -18.626 13.782 1 -11 -6 -6 44.1961 16.8405 1 11 6 6 58.0586 11.0466 5 11 6 6 41.7807 13.0182 1 -12 -6 -6 255.778 28.257 1 12 6 6 225.859 25.660 1 12 6 6 254.126 22.031 5 -13 -6 -6 163.371 24.310 1 13 6 6 118.203 15.737 5 13 6 6 157.280 21.541 1 -14 -6 -6 159.281 25.098 1 14 6 6 179.350 18.810 5 14 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279.310 27.095 5 -7 8 -7 165.230 21.443 1 7 -8 7 152.384 20.134 5 7 -8 7 171.650 20.250 1 -8 8 -7 217.509 24.572 1 8 -8 7 220.401 23.182 1 8 -8 7 190.889 25.517 5 -9 8 -7 69.9725 17.4548 1 9 -8 7 93.5774 17.9789 1 9 -8 7 102.413 21.320 5 -10 8 -7 416.845 38.156 1 10 -8 7 463.595 37.758 1 10 -8 7 411.667 38.772 5 -11 8 -7 353.756 34.089 1 11 -8 7 362.088 37.160 5 11 -8 7 394.713 35.881 1 -12 8 -7 -18.039 18.831 1 12 -8 7 -6.8750 19.1988 5 -13 8 -7 327.863 36.181 1 13 -8 7 310.768 35.886 5 13 -8 7 322.896 34.677 1 -14 8 -7 -24.923 17.868 1 14 -8 7 1.7355 16.7010 1 14 -8 7 10.7364 14.1998 5 -15 8 -7 98.7043 22.1871 1 15 -8 7 143.824 27.752 1 15 -8 7 146.515 29.317 5 -16 8 -7 101.822 26.935 1 16 -8 7 93.7531 26.7596 5 -17 8 -7 -13.620 22.070 1 17 -8 7 14.0336 18.9294 1 17 -8 7 57.0214 22.4680 5 18 7 -7 68.6938 19.8485 1 18 7 -7 80.2124 24.3965 3 17 7 -7 178.046 26.547 1 17 7 -7 198.203 30.687 3 16 7 -7 -11.996 13.966 3 15 7 -7 170.116 26.601 3 15 7 -7 114.995 21.133 1 14 7 -7 72.3088 21.7441 3 13 7 -7 114.641 24.922 3 13 7 -7 96.7286 18.0390 1 12 7 -7 -2.0891 18.7188 3 12 7 -7 59.7364 14.6219 1 11 7 -7 170.744 25.955 3 11 7 -7 170.161 19.927 1 -11 -7 7 180.100 18.539 1 10 7 -7 437.326 34.238 1 10 7 -7 534.495 42.173 3 -10 -7 7 494.245 34.650 1 9 7 -7 11.0995 16.5186 3 -9 -7 7 2.18645 7.14167 1 8 7 -7 672.752 42.075 1 8 7 -7 635.752 40.773 1 8 7 -7 655.825 49.561 3 -8 -7 7 671.165 41.504 1 7 7 -7 186.903 15.693 1 7 7 -7 187.672 16.868 1 7 7 -7 167.181 21.507 3 -7 -7 7 170.131 15.868 1 6 7 -7 1064.40 66.91 3 6 7 -7 1017.72 58.16 1 6 7 -7 1170.03 59.74 1 -6 -7 7 866.318 56.000 5 -6 -7 7 1051.19 58.61 1 5 7 -7 38.4704 6.7482 1 5 7 -7 43.2315 14.2862 3 5 7 -7 38.0415 8.7457 1 -5 -7 7 29.9303 5.8354 5 -5 -7 7 52.5948 7.9471 1 4 7 -7 575.824 42.246 2 4 7 -7 519.035 33.039 1 4 7 -7 542.782 40.115 3 4 7 -7 582.513 33.679 1 -4 -7 7 538.730 33.129 1 -4 -7 7 560.014 32.778 5 3 7 -7 275.783 19.267 1 3 7 -7 288.812 19.983 5 3 7 -7 258.798 24.881 3 3 7 -7 254.958 18.761 1 3 7 -7 266.454 25.842 2 -3 -7 7 273.946 19.467 5 -3 -7 7 267.582 18.827 1 2 7 -7 333.281 28.801 2 2 7 -7 362.954 27.628 3 2 7 -7 283.152 20.938 1 2 7 -7 315.161 21.647 1 -2 -7 7 329.787 22.659 5 -2 -7 7 317.034 21.454 1 1 7 -7 299.594 24.778 3 1 7 -7 356.014 28.728 2 1 7 -7 294.742 21.687 1 1 7 -7 311.348 21.196 1 -1 -7 7 328.677 23.159 5 -1 -7 7 291.172 21.126 1 0 7 -7 4.93610 7.94707 3 0 7 -7 8.21778 6.54471 1 0 7 -7 5.44360 7.27980 2 0 7 -7 2.88695 4.70993 1 0 -7 7 5.24793 5.33274 1 -1 7 -7 334.141 28.149 2 -1 7 -7 294.595 22.502 1 -1 7 -7 313.303 24.232 3 -1 7 -7 295.208 21.619 1 1 -7 7 286.273 21.850 1 1 -7 7 304.717 24.021 5 -2 7 -7 128.373 13.855 1 -2 7 -7 108.513 12.176 1 -2 7 -7 108.937 12.740 3 -2 7 -7 125.667 17.328 2 2 -7 7 122.066 15.485 5 2 -7 7 121.250 13.051 1 -3 7 -7 155.747 15.487 1 -3 7 -7 160.160 16.665 1 -3 7 -7 177.836 15.458 3 -3 7 -7 166.526 20.306 2 3 -7 7 181.435 16.610 1 3 -7 7 173.103 17.330 5 -4 7 -7 98.4618 13.8508 1 -4 7 -7 92.6113 14.6344 2 -4 7 -7 87.1688 10.1908 3 4 -7 7 102.164 13.339 1 4 -7 7 102.413 15.456 5 -5 7 -7 717.809 51.400 2 -5 7 -7 730.533 42.767 3 -5 7 -7 702.107 46.486 1 -5 7 -7 700.790 46.416 1 5 -7 7 758.227 49.078 5 5 -7 7 828.382 48.108 1 -6 7 -7 13.2688 11.8208 1 6 -7 7 -11.010 9.861 5 6 -7 7 8.63153 9.83143 1 -7 7 -7 167.071 19.121 1 7 -7 7 208.156 21.242 1 7 -7 7 188.061 21.145 5 -8 7 -7 349.207 30.481 1 8 -7 7 386.730 33.707 5 8 -7 7 372.918 31.482 1 -9 7 -7 365.963 32.920 1 9 -7 7 355.103 31.248 1 9 -7 7 327.371 32.146 5 -10 7 -7 793.357 55.677 1 10 -7 7 751.219 54.987 5 10 -7 7 858.614 56.787 1 -11 7 -7 117.526 22.879 1 11 -7 7 131.786 21.045 5 11 -7 7 135.221 21.905 1 -12 7 -7 131.427 23.676 1 12 -7 7 121.779 21.095 1 12 -7 7 109.144 23.775 5 -13 7 -7 -21.678 19.913 1 13 -7 7 13.4920 19.1437 5 13 -7 7 40.3418 17.1320 1 -14 7 -7 293.485 35.549 1 14 -7 7 336.243 37.430 5 14 -7 7 350.925 36.801 1 -15 7 -7 -24.901 19.963 1 15 -7 7 -17.256 16.942 5 15 -7 7 -11.928 18.754 1 -16 7 -7 44.0675 23.5285 1 16 -7 7 78.6220 19.3413 1 16 -7 7 65.2965 23.1965 5 -17 7 -7 150.168 26.709 1 17 -7 7 143.753 28.286 5 17 -7 7 154.034 29.576 1 18 -7 7 54.6759 24.7013 5 18 -7 7 48.4466 19.3574 1 18 6 -7 232.282 30.956 3 17 6 -7 -2.2055 17.2680 3 17 6 -7 19.1824 14.2588 1 16 6 -7 111.106 23.194 3 16 6 -7 114.728 21.888 1 15 6 -7 -8.6003 12.2658 1 14 6 -7 87.9953 18.8883 3 13 6 -7 336.262 35.320 3 13 6 -7 400.656 32.634 1 12 6 -7 297.619 27.574 1 12 6 -7 282.574 31.994 3 -12 -6 7 340.966 28.028 1 11 6 -7 69.1452 16.8726 3 11 6 -7 33.8737 11.5943 1 -11 -6 7 52.7462 12.0294 1 10 6 -7 59.2046 12.1541 1 9 6 -7 410.325 36.167 3 9 6 -7 408.317 29.313 1 -9 -6 7 389.037 28.791 1 8 6 -7 63.6092 9.3055 1 8 6 -7 73.3404 11.5099 1 8 6 -7 92.8263 15.9556 3 -8 -6 7 62.4852 18.9894 1 7 6 -7 850.853 56.001 3 7 6 -7 734.692 46.433 1 7 6 -7 843.445 47.769 1 -7 -6 7 788.770 47.061 1 6 6 -7 1.27554 6.06791 1 6 6 -7 -1.9457 4.1949 1 -6 -6 7 -1.1507 2.4166 5 -6 -6 7 10.5515 5.5571 1 5 6 -7 510.880 31.476 1 5 6 -7 495.415 37.701 3 5 6 -7 507.380 31.142 1 -5 -6 7 558.048 31.625 1 -5 -6 7 527.487 29.638 5 4 6 -7 87.8196 8.9161 1 4 6 -7 93.9605 9.3623 1 4 6 -7 85.5737 17.0953 2 4 6 -7 92.4340 14.1052 3 -4 -6 7 105.002 9.230 5 -4 -6 7 104.377 9.373 1 3 6 -7 879.686 50.191 1 3 6 -7 940.105 58.364 3 3 6 -7 951.565 61.047 2 3 6 -7 888.866 50.420 1 -3 -6 7 899.510 50.073 1 -3 -6 7 943.465 50.923 5 2 6 -7 241.930 16.172 1 2 6 -7 222.035 20.412 3 2 6 -7 202.405 15.352 1 2 6 -7 225.071 23.030 2 -2 -6 7 231.783 17.248 5 -2 -6 7 239.671 15.874 1 1 6 -7 3.19851 4.52474 1 1 6 -7 1.82319 3.83557 1 1 6 -7 10.1364 8.1116 3 1 6 -7 1.2626 12.3904 2 -1 -6 7 4.04119 6.57300 5 -1 -6 7 5.61432 4.13209 1 0 6 -7 228.109 22.815 2 0 6 -7 212.767 16.208 1 0 6 -7 232.501 20.322 3 0 6 -7 226.677 17.381 1 0 -6 7 236.115 17.081 1 0 -6 7 231.533 18.758 5 -1 6 -7 321.973 28.192 2 -1 6 -7 286.425 20.610 1 -1 6 -7 311.692 26.544 3 -1 6 -7 313.477 21.672 1 1 -6 7 301.539 21.220 1 1 -6 7 297.311 22.751 5 -2 6 -7 1022.27 61.22 3 -2 6 -7 1023.42 59.54 1 -2 6 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135.905 21.488 5 13 -6 7 123.704 19.728 1 14 -6 7 123.809 25.217 5 14 -6 7 122.514 23.844 1 -15 6 -7 279.765 35.092 1 15 -6 7 282.774 33.660 1 15 -6 7 245.459 32.906 5 -16 6 -7 76.2900 23.6433 1 16 -6 7 86.1199 22.8608 1 16 -6 7 137.167 27.182 5 -17 6 -7 9.3719 20.0132 1 17 -6 7 18.3629 20.8559 1 17 -6 7 -12.313 18.465 5 -18 6 -7 179.599 32.759 1 18 -6 7 169.720 31.334 1 18 -6 7 183.404 31.698 5 18 5 -7 20.8524 15.8493 1 18 5 -7 13.6272 17.1804 3 17 5 -7 182.344 27.009 3 17 5 -7 179.299 25.876 1 16 5 -7 20.6706 16.8237 3 16 5 -7 14.9094 15.3066 1 15 5 -7 50.0020 17.6483 3 15 5 -7 39.4414 14.5673 1 14 5 -7 82.4555 17.1560 1 14 5 -7 107.043 21.299 3 13 5 -7 100.864 21.147 3 13 5 -7 149.004 19.034 1 12 5 -7 426.602 33.382 1 12 5 -7 427.184 37.913 3 -12 -5 7 386.993 31.237 1 11 5 -7 571.530 46.036 3 11 5 -7 587.401 40.382 1 -11 -5 7 568.291 39.623 1 10 5 -7 383.375 35.523 3 10 5 -7 389.011 29.805 1 -10 -5 7 411.879 29.609 1 9 5 -7 25.0785 11.0534 1 9 5 -7 5.06684 5.65202 1 9 5 -7 6.6820 11.5166 3 -9 -5 7 -1.3611 6.6018 1 8 5 -7 891.424 54.475 1 8 5 -7 993.774 63.458 3 8 5 -7 962.038 55.440 1 -8 -5 7 975.670 55.295 1 7 5 -7 5.62213 5.14477 1 7 5 -7 -5.6220 11.8310 3 -7 -5 7 5.9703 28.7906 1 6 5 -7 565.647 41.659 3 6 5 -7 624.791 35.988 1 6 5 -7 628.593 35.537 1 -6 -5 7 646.635 35.973 1 -6 -5 7 536.995 31.936 5 5 5 -7 278.931 25.546 3 5 5 -7 288.281 19.275 1 5 5 -7 311.949 19.005 1 -5 -5 7 287.246 18.824 1 -5 -5 7 266.112 17.401 5 4 5 -7 741.292 40.765 1 4 5 -7 723.193 40.874 1 4 5 -7 739.315 48.042 3 -4 -5 7 719.133 40.621 5 -4 -5 7 767.536 41.005 1 3 5 -7 1229.45 73.61 2 3 5 -7 1214.86 61.49 1 3 5 -7 1224.04 70.16 3 -3 -5 7 1082.90 61.04 1 -3 -5 7 1115.63 62.11 5 -3 -5 7 1098.79 61.47 1 2 5 -7 414.404 32.361 2 2 5 -7 417.398 29.467 3 2 5 -7 377.906 23.243 1 -2 -5 7 434.241 25.732 5 -2 -5 7 387.998 23.171 1 -2 -5 7 381.969 23.218 1 1 5 -7 176.355 12.458 1 1 5 -7 196.745 18.372 3 1 5 -7 180.979 19.929 2 1 5 -7 166.517 12.693 1 -1 -5 7 166.736 12.454 1 -1 -5 7 198.440 12.630 1 -1 -5 7 183.633 15.007 5 0 5 -7 318.240 27.365 2 0 5 -7 366.847 26.023 3 0 5 -7 328.705 21.967 1 0 5 -7 337.414 21.390 1 0 -5 7 372.655 24.426 5 0 -5 7 360.643 22.033 1 -1 5 -7 1502.93 85.06 2 -1 5 -7 1301.09 76.87 3 -1 5 -7 1297.82 72.91 1 -1 5 -7 1338.65 73.48 1 1 -5 7 1335.22 75.20 5 1 -5 7 1419.76 73.45 1 -2 5 -7 20.6933 6.9480 1 -2 5 -7 26.6899 6.6422 3 -2 5 -7 -3.6613 11.2983 2 -2 5 -7 15.5148 5.1108 1 2 -5 7 18.8054 5.8904 3 2 -5 7 4.49728 6.53368 5 2 -5 7 27.5477 6.3154 1 -3 5 -7 360.832 29.897 2 -3 5 -7 309.841 22.839 1 -3 5 -7 327.276 23.578 1 -3 5 -7 355.483 23.330 3 3 -5 7 342.835 22.776 3 3 -5 7 356.949 25.870 5 3 -5 7 353.996 23.772 1 -4 5 -7 17.4763 5.3225 3 -4 5 -7 17.8723 15.3282 2 -4 5 -7 13.1356 6.7604 1 -4 5 -7 18.8505 6.9404 1 4 -5 7 10.1806 7.4573 1 4 -5 7 24.4235 8.4798 5 -5 5 -7 651.262 43.223 1 5 -5 7 773.106 44.378 1 5 -5 7 664.322 40.325 3 5 -5 7 731.375 45.312 5 -6 5 -7 805.342 47.214 1 6 -5 7 742.422 47.453 5 6 -5 7 642.736 42.744 3 6 -5 7 697.483 45.437 1 -7 5 -7 587.489 40.265 1 7 -5 7 589.132 41.542 5 7 -5 7 560.523 39.329 1 -8 5 -7 75.9610 15.2032 1 8 -5 7 64.7264 13.3449 1 8 -5 7 59.3781 15.8654 5 8 -5 7 82.7842 9.3624 4 -9 5 -7 -2.1632 9.5483 1 9 -5 7 -0.1784 11.2070 1 9 -5 7 -0.5949 10.0755 5 -10 5 -7 857.857 58.318 1 10 -5 7 849.873 57.411 1 10 -5 7 890.932 58.812 5 -11 5 -7 62.2954 15.6859 1 11 -5 7 67.3137 17.6481 1 11 -5 7 47.2366 27.7687 5 -12 5 -7 163.842 23.399 1 12 -5 7 179.655 24.331 5 12 -5 7 144.690 22.871 1 -13 5 -7 226.973 29.801 1 13 -5 7 252.550 30.167 5 13 -5 7 248.416 28.163 1 -14 5 -7 193.762 29.291 1 14 -5 7 223.514 29.746 1 14 -5 7 273.110 30.452 5 -15 5 -7 164.534 28.298 1 15 -5 7 209.776 29.507 1 15 -5 7 199.952 29.666 5 -16 5 -7 49.0371 21.4182 1 16 -5 7 75.9639 22.5040 5 16 -5 7 77.8052 22.3818 1 -17 5 -7 148.777 28.674 1 17 -5 7 94.3783 23.0167 1 17 -5 7 145.202 27.711 5 18 -5 7 -15.083 21.046 5 18 -5 7 2.6736 18.9611 1 -19 5 -7 111.464 29.231 1 19 -5 7 84.0209 25.6739 1 18 4 -7 169.046 27.277 1 17 4 -7 1.8501 14.6721 1 16 4 -7 110.496 21.755 3 16 4 -7 118.610 20.414 1 15 4 -7 9.2940 14.7732 3 15 4 -7 30.9655 14.1747 1 14 4 -7 108.831 20.028 3 14 4 -7 150.040 20.459 1 13 4 -7 265.277 25.796 1 13 4 -7 249.271 28.175 3 -13 -4 7 249.830 24.720 1 12 4 -7 117.394 20.407 3 12 4 -7 144.692 17.297 1 -12 -4 7 153.680 18.008 1 11 4 -7 669.292 44.488 1 11 4 -7 653.258 48.915 3 -11 -4 7 669.652 43.899 1 10 4 -7 60.0451 15.8812 3 -10 -4 7 62.6561 13.8077 1 9 4 -7 398.004 27.399 1 9 4 -7 376.093 32.145 3 9 4 -7 404.479 28.454 1 -9 -4 7 382.825 27.504 1 8 4 -7 47.2263 7.7180 1 8 4 -7 53.8647 9.1544 1 -8 -4 7 56.0409 8.8572 1 7 4 -7 1152.18 71.34 1 7 4 -7 1246.68 70.04 1 7 4 -7 1324.97 77.78 3 -7 -4 7 1383.12 70.39 1 6 4 -7 223.723 21.780 3 6 4 -7 203.291 16.005 1 6 4 -7 231.413 15.887 1 -6 -4 7 229.470 16.044 1 5 4 -7 61.1983 6.4001 1 5 4 -7 51.5620 11.2331 3 5 4 -7 49.4846 6.6155 1 -5 -4 7 50.5055 5.5244 5 -5 -4 7 53.0068 6.3501 1 4 4 -7 773.711 45.621 3 4 4 -7 620.989 36.719 1 -4 -4 7 670.856 37.195 5 -4 -4 7 707.021 37.015 1 -4 -4 7 616.997 36.668 1 3 4 -7 132.309 9.066 1 3 4 -7 154.424 20.313 3 3 4 -7 137.076 15.697 2 -3 -4 7 117.274 8.615 1 -3 -4 7 124.378 8.881 1 -3 -4 7 133.125 10.786 5 2 4 -7 872.207 54.081 2 2 4 -7 821.371 50.551 3 -2 -4 7 782.967 42.889 1 -2 -4 7 801.677 45.596 5 -2 -4 7 817.898 43.154 1 1 4 -7 12.3101 6.6201 3 1 4 -7 4.53890 9.78179 2 1 4 -7 16.1905 3.1626 1 -1 -4 7 16.0017 2.8374 1 -1 -4 7 10.6031 2.9954 1 0 4 -7 501.161 34.464 2 0 4 -7 403.855 25.007 1 0 4 -7 452.405 30.202 3 0 4 -7 442.977 25.857 1 0 -4 7 437.117 25.572 1 0 -4 7 467.720 28.660 5 0 -4 7 412.002 24.842 1 -1 4 -7 52.1156 10.9032 2 -1 4 -7 62.5547 12.9478 1 -1 4 -7 42.3535 5.7890 1 1 -4 7 43.7161 6.9384 3 1 -4 7 39.4456 5.8817 1 -2 4 -7 2216.00 118.88 1 -2 4 -7 2123.46 123.62 1 -2 4 -7 2223.00 122.48 3 2 -4 7 2248.21 120.28 5 2 -4 7 2391.75 122.61 3 2 -4 7 2443.73 119.11 1 -3 4 -7 324.520 22.702 1 -3 4 -7 352.040 22.668 3 -3 4 -7 286.669 22.069 1 -3 4 -7 317.216 27.333 2 3 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24.194 3 4 13 -9 152.239 18.629 1 -4 -13 9 157.694 18.124 5 -4 -13 9 131.070 17.024 1 3 13 -9 70.4017 19.1160 2 3 13 -9 37.8889 18.0874 3 2 13 -9 155.277 22.391 3 2 13 -9 189.558 25.833 2 2 13 -9 196.797 20.677 1 -2 -13 9 156.243 20.340 5 -2 -13 9 159.984 18.705 1 1 13 -9 164.062 23.635 3 1 13 -9 172.759 24.698 2 1 13 -9 173.594 20.732 1 -1 -13 9 163.565 21.610 5 -1 -13 9 167.102 19.212 1 0 13 -9 478.260 36.943 1 0 13 -9 447.827 39.431 3 0 13 -9 478.858 40.858 2 0 -13 9 462.614 38.126 5 0 -13 9 457.319 35.583 1 -1 13 -9 11.9057 13.2464 1 -1 13 -9 -2.1152 11.5459 3 -1 13 -9 -19.897 15.255 2 1 -13 9 2.69229 9.93846 1 -2 13 -9 276.794 27.834 3 -2 13 -9 293.974 31.546 2 -2 13 -9 333.904 30.622 1 2 -13 9 303.006 28.384 1 2 -13 9 290.798 30.519 5 -3 13 -9 16.1102 10.2634 3 -3 13 -9 3.5389 14.9205 2 -3 13 -9 -30.807 16.446 1 3 -13 9 -7.1667 11.3634 1 3 -13 9 -7.6019 15.5571 5 -4 13 -9 160.191 19.236 3 -4 13 -9 186.875 26.189 2 -4 13 -9 197.154 25.749 1 4 -13 9 204.247 24.841 1 4 -13 9 213.332 27.332 5 -5 13 -9 332.271 34.794 2 -5 13 -9 334.026 33.376 1 5 -13 9 309.950 33.785 5 5 -13 9 253.699 29.047 1 -6 13 -9 59.6584 19.8533 1 6 -13 9 62.7015 18.1009 1 6 -13 9 55.5598 16.7158 5 -7 13 -9 58.7503 19.8078 2 -7 13 -9 59.1311 19.6420 1 7 -13 9 34.0577 21.3933 5 7 -13 9 62.1795 19.2885 1 -8 13 -9 59.9535 20.4692 2 -8 13 -9 42.0916 18.9380 1 8 -13 9 76.2766 19.4194 1 8 -13 9 104.481 25.154 5 -9 13 -9 139.760 26.345 2 -9 13 -9 192.858 28.407 1 9 -13 9 145.823 24.823 1 -10 13 -9 17.1976 18.1600 2 -10 13 -9 -4.3690 16.2819 1 10 -13 9 4.0763 17.5385 5 10 -13 9 21.4819 18.0781 1 -11 13 -9 185.345 29.884 1 -11 13 -9 168.362 30.556 2 11 -13 9 187.830 30.098 1 11 -13 9 240.617 34.700 5 -12 13 -9 -27.072 21.915 1 -12 13 -9 31.4159 20.9506 2 12 -13 9 12.2862 23.4261 5 12 -13 9 -19.315 18.175 1 -13 13 -9 187.155 31.907 1 13 -13 9 124.521 29.380 5 13 -13 9 161.031 28.259 1 -14 13 -9 33.2205 21.0338 1 -14 13 -9 37.0854 23.9112 2 14 -13 9 27.0231 21.8132 1 14 -13 9 -5.2154 18.0250 5 16 12 -9 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29.217 2 7 -12 9 206.551 28.973 5 7 -12 9 223.601 26.895 1 -8 12 -9 400.989 37.982 1 -8 12 -9 388.027 38.939 2 8 -12 9 374.997 39.134 5 8 -12 9 339.128 35.224 1 -9 12 -9 -4.1105 16.4825 2 -9 12 -9 -38.921 19.922 1 -10 12 -9 159.316 28.207 2 -10 12 -9 190.057 25.832 1 10 -12 9 137.844 24.868 1 10 -12 9 170.351 29.739 5 -11 12 -9 -5.2888 18.7549 1 11 -12 9 -19.615 22.188 5 11 -12 9 -4.8859 16.2884 1 -12 12 -9 205.814 29.686 1 -12 12 -9 218.743 32.989 2 12 -12 9 184.432 28.429 1 12 -12 9 177.838 28.541 5 -13 12 -9 46.8890 22.3893 1 13 -12 9 68.3572 18.2742 1 13 -12 9 113.299 27.929 5 -14 12 -9 11.7920 20.2818 1 14 -12 9 6.2243 23.5798 5 -15 12 -9 3.1015 19.5306 1 15 -12 9 77.8126 28.5724 5 16 11 -9 147.936 24.220 1 16 11 -9 153.076 30.839 3 15 11 -9 -38.263 22.401 3 15 11 -9 30.4068 14.6895 1 14 11 -9 19.4286 17.5236 3 14 11 -9 32.3822 14.6875 1 13 11 -9 54.2760 22.5282 3 13 11 -9 60.2594 16.2613 1 12 11 -9 12.1363 23.7965 3 12 11 -9 28.6264 13.1798 1 11 11 -9 231.890 24.233 1 11 11 -9 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295.760 31.485 1 10 -8 9 360.107 32.623 1 10 -8 9 295.364 31.547 5 -11 8 -9 83.2189 20.2613 1 11 -8 9 69.8008 17.8634 5 11 -8 9 49.3797 17.1000 1 -12 8 -9 0.2938 16.4381 1 12 -8 9 -4.9426 17.9936 5 -13 8 -9 242.598 32.265 1 13 -8 9 249.425 33.427 5 13 -8 9 221.044 27.460 1 -14 8 -9 -0.4574 19.2929 1 14 -8 9 -30.511 16.542 1 14 -8 9 16.9756 21.3473 5 -15 8 -9 82.8103 23.5074 1 15 -8 9 60.9753 22.7258 1 -16 8 -9 2.8882 18.4100 1 16 -8 9 39.3540 21.8255 5 16 -8 9 -6.4771 20.2292 1 -17 8 -9 96.9765 27.5869 1 17 -8 9 69.0242 26.9070 5 17 -8 9 78.6322 20.5533 1 18 7 -9 125.733 26.511 3 17 7 -9 150.075 28.666 3 17 7 -9 197.094 25.980 1 16 7 -9 34.9074 14.3580 1 16 7 -9 42.4384 21.0378 3 15 7 -9 61.8376 22.2335 3 15 7 -9 83.5735 17.2764 1 14 7 -9 34.7172 12.4347 1 14 7 -9 39.4844 19.9219 3 13 7 -9 397.977 41.103 3 13 7 -9 426.215 34.050 1 12 7 -9 38.4068 15.1907 3 11 7 -9 100.385 15.076 1 11 7 -9 145.691 24.026 3 10 7 -9 210.730 20.304 1 10 7 -9 221.688 28.733 3 9 7 -9 313.951 32.120 3 9 7 -9 342.106 25.386 1 -9 -7 9 328.962 25.706 1 8 7 -9 764.847 45.517 1 8 7 -9 751.003 56.032 3 -8 -7 9 746.688 44.983 1 7 7 -9 189.989 15.896 1 7 7 -9 189.983 15.264 1 7 7 -9 158.797 23.528 3 -7 -7 9 182.189 14.986 1 -7 -7 9 167.400 12.078 5 6 7 -9 107.618 11.247 1 6 7 -9 110.608 10.658 1 6 7 -9 113.741 19.658 3 -6 -7 9 111.620 9.830 5 -6 -7 9 118.218 10.941 1 5 7 -9 -4.3955 3.7105 1 5 7 -9 9.3840 13.4587 3 5 7 -9 -5.2417 5.5182 1 -5 -7 9 -8.3516 4.5049 1 -5 -7 9 -0.5290 4.4618 5 4 7 -9 405.086 24.476 1 4 7 -9 383.181 33.696 2 4 7 -9 398.006 33.588 3 -4 -7 9 361.920 23.817 1 -4 -7 9 404.944 25.759 5 3 7 -9 14.7631 15.0150 2 3 7 -9 -1.2818 5.5719 1 3 7 -9 10.5674 10.4492 3 -3 -7 9 1.56636 7.30684 5 -3 -7 9 2.85212 3.43213 1 2 7 -9 155.935 12.542 1 2 7 -9 151.846 21.091 2 2 7 -9 164.569 12.846 1 2 7 -9 160.152 19.567 3 -2 -7 9 167.993 15.337 5 -2 -7 9 139.080 11.990 1 1 7 -9 8.78997 9.68540 3 1 7 -9 13.2087 4.1002 1 1 7 -9 19.3324 5.2259 1 1 7 -9 -0.8844 10.9067 2 -1 -7 9 12.4814 4.4819 1 0 7 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42.927 1 8 -7 9 538.862 43.724 5 -9 7 -9 153.210 22.045 1 9 -7 9 166.177 24.709 5 9 -7 9 153.795 21.065 1 -10 7 -9 222.953 27.378 1 10 -7 9 221.901 24.998 1 10 -7 9 188.123 28.489 5 -11 7 -9 139.787 23.631 1 11 -7 9 131.743 24.464 5 11 -7 9 130.059 19.729 1 -12 7 -9 137.200 24.105 1 12 -7 9 197.652 27.307 5 12 -7 9 158.574 23.040 1 -13 7 -9 -9.1078 17.0612 1 13 -7 9 -13.212 12.471 1 13 -7 9 -32.148 17.241 5 -14 7 -9 274.268 34.265 1 14 -7 9 239.108 30.631 1 14 -7 9 236.996 33.069 5 -15 7 -9 43.6855 17.9554 1 15 -7 9 74.5591 24.0693 5 -16 7 -9 75.5440 25.3073 1 16 -7 9 45.7578 21.7609 1 -17 7 -9 124.904 29.773 1 17 -7 9 139.817 30.495 5 17 -7 9 124.354 26.858 1 -18 7 -9 99.8266 29.1897 1 18 -7 9 117.710 28.510 5 18 -7 9 168.143 30.468 1 18 6 -9 69.8281 22.8058 3 17 6 -9 47.5376 17.5257 1 17 6 -9 42.2525 20.5011 3 16 6 -9 90.8045 18.0383 1 16 6 -9 85.5986 20.4620 3 15 6 -9 -5.9582 14.1875 3 15 6 -9 18.2483 13.1213 1 14 6 -9 151.266 20.655 1 14 6 -9 220.543 27.338 3 13 6 -9 116.598 17.087 1 13 6 -9 113.271 21.275 3 12 6 -9 411.101 40.056 3 12 6 -9 392.693 31.193 1 11 6 -9 89.7364 14.0225 1 11 6 -9 69.6476 20.2490 3 10 6 -9 441.478 31.079 1 10 6 -9 432.039 38.693 3 -10 -6 9 415.262 29.927 1 9 6 -9 903.522 53.346 1 9 6 -9 900.645 62.957 3 -9 -6 9 889.198 52.770 1 8 6 -9 80.7598 16.6255 3 8 6 -9 70.9026 10.2954 1 -8 -6 9 82.2321 10.0689 1 7 6 -9 235.543 17.374 1 7 6 -9 243.023 17.669 1 7 6 -9 251.851 26.487 3 -7 -6 9 245.016 17.554 1 -7 -6 9 213.433 14.529 5 6 6 -9 2.16267 5.37514 1 6 6 -9 -0.7921 12.6642 3 6 6 -9 5.30182 4.10221 1 -6 -6 9 -3.0570 3.9095 1 -6 -6 9 2.64871 3.62453 5 5 6 -9 569.400 33.473 1 5 6 -9 569.130 43.122 3 -5 -6 9 614.817 33.538 1 -5 -6 9 574.332 33.933 5 4 6 -9 254.012 17.346 1 4 6 -9 273.752 25.468 3 4 6 -9 272.047 27.650 2 -4 -6 9 282.302 19.617 5 -4 -6 9 299.666 17.643 1 3 6 -9 630.534 43.405 3 3 6 -9 532.086 33.384 1 3 6 -9 648.453 46.524 2 -3 -6 9 618.171 33.783 1 -3 -6 9 618.247 36.698 5 2 6 -9 132.905 10.103 1 2 6 -9 107.054 16.536 3 2 6 -9 118.306 17.557 2 -2 -6 9 130.137 13.010 5 -2 -6 9 115.596 9.341 1 1 6 -9 76.8828 14.0212 3 1 6 -9 73.5325 7.7365 1 1 6 -9 85.6921 15.5519 2 -1 -6 9 64.5870 7.0578 1 -1 -6 9 68.6919 10.5133 5 0 6 -9 1481.57 84.54 2 0 6 -9 1292.70 76.84 3 0 6 -9 1201.12 70.32 1 0 -6 9 1261.09 72.82 5 0 -6 9 1290.76 70.46 1 -1 6 -9 33.8652 10.5362 3 -1 6 -9 37.8832 6.4740 1 -1 6 -9 46.8587 14.7677 2 -1 6 -9 40.8136 7.7576 1 1 -6 9 45.5340 7.2211 1 1 -6 9 38.0155 11.0351 5 -2 6 -9 141.143 14.645 3 -2 6 -9 111.300 11.934 1 -2 6 -9 100.177 10.734 1 -2 6 -9 97.1003 17.6442 2 2 -6 9 119.617 11.987 1 2 -6 9 118.020 15.196 5 -3 6 -9 236.091 24.653 2 -3 6 -9 193.533 16.722 1 -3 6 -9 188.423 17.639 3 -3 6 -9 220.554 18.205 1 3 -6 9 226.286 17.734 1 3 -6 9 170.409 18.426 5 -4 6 -9 1127.93 62.06 1 -4 6 -9 1014.52 60.77 3 -4 6 -9 962.317 60.553 1 -4 6 -9 1087.98 71.08 2 4 -6 9 1049.30 61.08 1 4 -6 9 1074.01 64.06 5 -5 6 -9 33.0642 7.2411 3 -5 6 -9 42.3546 12.1241 1 -5 6 -9 53.6652 16.6831 2 5 -6 9 37.4961 6.5555 3 5 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17.9277 3 17 5 -9 218.025 26.502 1 17 5 -9 196.839 29.486 3 16 5 -9 85.4730 18.1447 1 15 5 -9 61.0733 15.9953 1 15 5 -9 99.4586 22.5035 3 14 5 -9 52.6889 13.9372 1 13 5 -9 403.436 32.080 1 13 5 -9 383.249 38.330 3 12 5 -9 377.738 37.138 3 12 5 -9 331.115 28.243 1 11 5 -9 473.251 33.985 1 11 5 -9 474.704 40.369 3 10 5 -9 466.240 32.301 1 10 5 -9 484.052 40.838 3 -10 -5 9 454.146 31.617 1 9 5 -9 25.0314 14.2179 3 9 5 -9 31.6086 9.8292 1 8 5 -9 469.996 38.013 3 8 5 -9 462.248 29.233 1 8 5 -9 445.709 29.326 1 -8 -5 9 447.275 28.930 1 7 5 -9 57.1242 14.7422 3 7 5 -9 56.6319 8.1535 1 7 5 -9 49.2423 6.9989 1 -7 -5 9 47.1238 6.8698 1 -7 -5 9 43.9638 5.3101 5 6 5 -9 44.1600 13.7472 3 6 5 -9 48.9508 6.3223 1 -6 -5 9 47.7184 6.0467 5 -6 -5 9 59.3092 6.5157 1 5 5 -9 413.449 32.766 3 5 5 -9 400.247 23.160 1 -5 -5 9 343.864 22.552 1 -5 -5 9 420.825 24.439 5 4 5 -9 165.995 10.784 1 4 5 -9 129.919 18.420 3 4 5 -9 142.368 19.956 2 4 5 -9 135.510 9.658 1 -4 -5 9 115.421 9.164 1 -4 -5 9 156.590 12.472 5 3 5 -9 210.137 23.394 3 3 5 -9 201.555 23.387 2 -3 -5 9 206.155 15.904 5 2 5 -9 320.462 26.841 3 2 5 -9 299.777 28.382 2 -2 -5 9 295.556 21.589 5 1 5 -9 444.782 34.644 2 1 5 -9 399.360 30.230 3 1 5 -9 406.140 23.208 1 -1 -5 9 371.540 22.721 1 -1 -5 9 376.310 22.329 1 0 5 -9 1.74082 7.59071 3 0 5 -9 -0.5984 4.4923 1 0 5 -9 24.7404 13.4277 2 0 -5 9 6.17251 5.91997 5 -1 5 -9 271.329 25.675 2 -1 5 -9 204.793 15.688 1 -1 5 -9 234.123 20.406 3 -1 5 -9 224.654 16.566 1 1 -5 9 237.954 16.275 1 1 -5 9 240.044 20.023 5 -2 5 -9 910.996 54.464 1 -2 5 -9 991.271 55.233 1 -2 5 -9 963.508 58.280 3 2 -5 9 1012.71 55.02 1 2 -5 9 1032.31 58.59 5 -3 5 -9 866.956 53.667 1 -3 5 -9 963.751 54.500 1 -3 5 -9 979.159 56.264 3 3 -5 9 893.001 53.630 1 3 -5 9 1031.89 58.03 5 -4 5 -9 223.374 19.345 1 -4 5 -9 228.557 25.259 2 -4 5 -9 210.383 17.981 3 -4 5 -9 186.247 17.371 1 4 -5 9 254.790 19.193 1 4 -5 9 228.385 20.888 5 -5 5 -9 665.915 40.875 1 -5 5 -9 580.933 46.283 2 5 -5 9 626.092 37.358 3 5 -5 9 625.299 39.695 1 5 -5 9 579.177 41.277 5 -6 5 -9 5.03401 9.90929 1 6 -5 9 -24.474 18.245 5 6 -5 9 12.1802 7.6344 1 -7 5 -9 703.707 45.295 1 7 -5 9 664.273 43.706 1 7 -5 9 714.824 47.056 5 7 -5 9 597.104 42.612 3 -8 5 -9 275.531 25.834 1 8 -5 9 328.489 28.930 5 8 -5 9 327.163 27.422 1 8 -5 9 304.811 18.990 3 -9 5 -9 18.8087 14.4583 1 9 -5 9 -1.1884 15.1699 5 -10 5 -9 282.123 28.833 1 10 -5 9 281.416 30.137 5 10 -5 9 250.660 25.883 1 -11 5 -9 121.011 22.134 1 11 -5 9 135.998 20.579 1 -12 5 -9 527.140 43.178 1 12 -5 9 493.760 42.517 5 12 -5 9 496.017 41.572 1 -13 5 -9 52.5923 19.1205 1 13 -5 9 76.4237 18.7528 1 13 -5 9 81.2130 20.1537 5 -14 5 -9 131.406 24.591 1 14 -5 9 153.606 25.704 5 14 -5 9 98.3352 19.2124 1 -15 5 -9 -0.7462 12.6858 1 15 -5 9 3.4920 14.7620 5 15 -5 9 -29.908 17.378 1 -16 5 -9 179.104 30.997 1 16 -5 9 204.822 31.157 5 16 -5 9 187.436 26.461 1 -17 5 -9 104.380 25.143 1 17 -5 9 92.3521 24.1151 5 -18 5 -9 63.5272 25.0688 1 18 -5 9 102.022 27.418 5 18 -5 9 79.8416 24.3176 1 18 4 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314.514 28.718 2 3 4 -9 305.164 26.060 3 3 4 -9 339.211 27.361 4 -3 -4 9 256.392 20.075 5 2 4 -9 456.062 33.899 4 2 4 -9 413.904 34.904 2 2 4 -9 437.649 33.010 3 -2 -4 9 446.906 28.321 5 1 4 -9 776.800 54.151 4 1 4 -9 895.218 58.446 2 1 4 -9 808.191 75.852 3 -1 -4 9 918.242 50.047 5 0 4 -9 845.232 48.412 1 0 4 -9 967.108 55.910 3 0 4 -9 839.273 56.858 4 0 4 -9 874.491 59.809 2 0 -4 9 995.479 53.204 5 0 -4 9 914.821 48.485 1 -1 4 -9 64.7418 6.9511 1 -1 4 -9 86.1212 8.2793 1 -1 4 -9 81.3335 10.8441 3 -1 4 -9 70.0951 15.1216 2 -1 4 -9 84.4605 13.3105 4 1 -4 9 85.1765 7.8405 1 -2 4 -9 891.642 54.782 3 -2 4 -9 858.806 61.095 2 -2 4 -9 969.086 51.795 1 -2 4 -9 825.559 50.784 1 -2 4 -9 980.215 58.870 4 2 -4 9 966.584 51.519 1 2 -4 9 983.315 55.250 5 -3 4 -9 -0.7803 7.0934 1 -3 4 -9 -0.7254 4.8768 1 -3 4 -9 4.8667 10.9779 3 -3 4 -9 6.8894 15.2590 4 3 -4 9 10.8205 5.9241 1 3 -4 9 0.0925 10.2900 5 -4 4 -9 537.720 40.074 2 -4 4 -9 446.884 31.050 1 -4 4 -9 494.546 31.952 1 4 -4 9 536.752 32.011 1 4 -4 9 446.391 30.533 3 4 -4 9 487.491 34.355 5 -5 4 -9 175.180 22.057 2 -5 4 -9 186.303 16.884 1 -5 4 -9 183.296 17.220 1 5 -4 9 178.879 14.283 3 5 -4 9 163.481 15.852 1 5 -4 9 163.885 19.024 5 -6 4 -9 758.486 46.238 1 6 -4 9 696.432 45.061 1 6 -4 9 706.670 47.547 5 6 -4 9 725.962 42.075 3 -7 4 -9 416.457 32.172 1 7 -4 9 459.924 32.175 1 7 -4 9 453.409 34.129 5 7 -4 9 394.892 26.026 3 -8 4 -9 177.575 19.829 1 8 -4 9 172.216 19.024 1 8 -4 9 143.838 11.576 3 8 -4 9 169.907 21.857 5 -9 4 -9 343.843 29.947 1 9 -4 9 296.759 28.692 5 9 -4 9 324.239 28.532 1 -10 4 -9 5.8567 10.0749 1 10 -4 9 24.2736 12.7642 1 10 -4 9 -25.173 16.032 5 -11 4 -9 600.005 46.683 1 11 -4 9 608.776 45.799 1 11 -4 9 627.720 47.034 5 12 -4 9 38.3834 12.5899 1 12 -4 9 41.9103 18.7949 5 -13 4 -9 230.549 27.072 1 13 -4 9 265.462 29.176 1 13 -4 9 242.980 29.460 5 -14 4 -9 13.5179 18.3961 1 14 -4 9 17.1621 15.1587 5 14 -4 9 47.4423 16.4767 1 -15 4 -9 233.277 29.811 1 15 -4 9 269.354 31.938 1 15 -4 9 309.112 33.556 5 -16 4 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1 -2 3 -9 312.810 24.186 4 -2 3 -9 271.338 26.678 2 2 -3 9 271.192 18.245 1 2 -3 9 303.838 23.027 5 -3 3 -9 375.247 26.696 1 -3 3 -9 460.067 35.764 2 -3 3 -9 446.539 27.716 1 -3 3 -9 452.199 31.706 4 3 -3 9 429.161 29.992 5 3 -3 9 448.253 27.297 1 -4 3 -9 599.187 42.347 2 -4 3 -9 520.579 33.672 1 -4 3 -9 473.765 32.920 1 -4 3 -9 569.312 37.085 4 4 -3 9 504.810 33.194 3 4 -3 9 564.932 33.730 1 4 -3 9 538.926 36.558 5 -5 3 -9 281.306 23.503 1 -5 3 -9 398.137 26.789 4 -5 3 -9 387.596 31.952 2 -5 3 -9 359.589 25.617 1 5 -3 9 340.490 27.417 5 5 -3 9 340.263 24.507 1 5 -3 9 318.185 22.669 3 -6 3 -9 344.048 23.910 4 -6 3 -9 313.073 23.914 1 6 -3 9 252.731 24.328 5 6 -3 9 274.361 22.688 1 6 -3 9 261.744 19.318 3 -7 3 -9 87.3667 14.1054 1 7 -3 9 53.7612 10.9566 1 7 -3 9 73.0737 7.5494 3 7 -3 9 49.0932 14.3119 5 -8 3 -9 929.799 54.273 1 8 -3 9 704.409 47.920 3 8 -3 9 828.175 53.852 5 8 -3 9 835.702 52.300 1 9 -3 9 -5.8127 13.7496 1 9 -3 9 2.9966 11.8306 5 9 -3 9 -0.8177 4.8030 4 -10 3 -9 141.278 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2 -5 8 -10 622.122 40.358 3 -5 8 -10 633.059 43.017 1 5 -8 10 643.418 43.163 1 5 -8 10 658.838 46.809 5 -6 8 -10 38.5231 15.0350 2 -6 8 -10 37.4020 11.9615 1 6 -8 10 49.7176 12.9620 1 -7 8 -10 403.303 36.807 2 -7 8 -10 319.131 30.108 1 7 -8 10 320.177 28.792 1 7 -8 10 329.102 31.073 5 -8 8 -10 27.4062 13.8090 2 8 -8 10 17.4545 13.1204 5 8 -8 10 24.6432 10.2707 1 -9 8 -10 67.5042 18.1802 1 -10 8 -10 101.969 21.499 1 10 -8 10 128.570 21.153 1 10 -8 10 146.088 22.371 5 11 -8 10 7.0794 12.8883 5 11 -8 10 18.2275 14.4358 1 -12 8 -10 219.843 29.784 1 12 -8 10 251.854 31.985 5 12 -8 10 241.550 28.295 1 -13 8 -10 -36.943 19.447 1 13 -8 10 15.4530 12.5833 1 13 -8 10 -5.4062 19.6086 5 -14 8 -10 273.902 36.300 1 14 -8 10 376.155 41.262 5 14 -8 10 317.049 35.255 1 -15 8 -10 -28.684 20.646 1 15 -8 10 -5.1361 18.3490 1 -16 8 -10 27.5695 19.0234 1 16 -8 10 12.0103 20.4917 1 -17 8 -10 -29.040 23.104 1 17 -8 10 -3.2732 16.4041 1 17 -8 10 -33.808 25.677 5 17 7 -10 44.1007 16.5645 1 17 7 -10 57.2049 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248.278 24.630 3 -4 -5 10 249.142 18.287 5 3 5 -10 590.866 42.020 3 3 5 -10 577.947 44.928 2 -3 -5 10 592.220 35.998 5 2 5 -10 210.470 24.250 2 2 5 -10 202.399 22.315 3 -2 -5 10 236.098 18.639 5 1 5 -10 85.9773 14.5610 2 1 5 -10 72.3349 14.0608 3 1 5 -10 89.9721 6.9179 1 1 5 -10 77.5313 6.5126 1 -1 -5 10 82.5644 6.4785 1 -1 -5 10 89.7110 11.2992 5 -1 -5 10 67.6232 5.7984 1 0 5 -10 782.862 56.966 2 0 5 -10 813.926 45.885 1 0 5 -10 869.341 53.406 3 0 -5 10 809.268 45.618 1 0 -5 10 892.831 50.451 5 -1 5 -10 625.447 39.564 1 -1 5 -10 723.946 40.563 1 -1 5 -10 782.615 46.999 3 1 -5 10 674.303 39.963 1 1 -5 10 751.226 44.963 5 -2 5 -10 380.589 26.284 1 -2 5 -10 439.911 30.957 3 -2 5 -10 426.633 27.321 1 -2 5 -10 409.994 35.332 2 2 -5 10 446.756 31.553 5 2 -5 10 464.093 27.401 1 -3 5 -10 150.795 21.099 2 -3 5 -10 140.016 13.152 1 -3 5 -10 156.616 14.622 1 -3 5 -10 163.793 15.657 3 3 -5 10 127.970 17.079 5 3 -5 10 143.577 13.460 1 -4 5 -10 1102.88 76.69 2 -4 5 -10 1128.51 67.87 3 -4 5 -10 1289.37 68.09 1 -4 5 -10 1050.25 67.08 1 4 -5 10 1253.70 67.39 1 4 -5 10 1259.82 70.90 5 -5 5 -10 367.191 33.942 2 -5 5 -10 445.833 29.908 1 5 -5 10 389.844 28.468 1 5 -5 10 386.137 30.887 5 -6 5 -10 840.624 51.654 1 -6 5 -10 873.867 60.132 2 6 -5 10 820.531 53.838 5 6 -5 10 784.895 47.502 3 6 -5 10 763.065 49.845 1 -7 5 -10 84.5908 15.3162 1 7 -5 10 104.412 13.760 1 7 -5 10 111.592 19.017 5 7 -5 10 103.586 9.825 3 -8 5 -10 147.685 17.861 1 8 -5 10 143.332 11.398 3 8 -5 10 139.582 21.233 5 -9 5 -10 229.309 25.596 1 9 -5 10 244.453 24.240 1 9 -5 10 243.296 25.796 5 -10 5 -10 1.8054 16.2213 1 10 -5 10 78.2977 25.7661 5 10 -5 10 22.5824 12.0912 1 -11 5 -10 366.894 33.920 1 11 -5 10 323.964 31.101 1 11 -5 10 329.983 33.504 5 -12 5 -10 127.061 22.439 1 12 -5 10 126.184 20.962 1 12 -5 10 90.0145 21.8120 5 -13 5 -10 48.5625 17.7299 1 13 -5 10 19.3880 15.2756 1 -14 5 -10 26.0202 19.0075 1 14 -5 10 17.5993 12.6175 1 -15 5 -10 107.072 21.043 1 15 -5 10 140.675 24.830 1 15 -5 10 90.7179 23.2520 5 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66.4128 13.0517 3 -6 -4 10 48.2783 6.8389 5 -6 -4 10 40.5720 5.1046 1 5 4 -10 160.878 20.829 3 -5 -4 10 162.160 13.494 5 4 4 -10 1204.51 79.57 2 4 4 -10 1240.22 77.09 4 4 4 -10 1249.53 75.74 3 -4 -4 10 1220.55 67.25 5 3 4 -10 602.465 42.049 3 3 4 -10 597.084 42.072 4 3 4 -10 589.723 44.894 2 -3 -4 10 568.066 35.681 5 2 4 -10 543.315 38.923 4 2 4 -10 487.381 37.355 3 2 4 -10 502.238 40.633 2 -2 -4 10 534.676 33.082 5 1 4 -10 477.115 35.728 4 1 4 -10 434.247 36.548 2 1 4 -10 442.608 33.238 3 -1 -4 10 509.641 31.673 5 0 4 -10 651.994 41.795 3 0 4 -10 699.740 46.923 2 0 4 -10 650.635 43.453 4 0 4 -10 530.525 33.172 1 0 -4 10 579.159 33.250 1 0 -4 10 664.647 39.290 5 0 -4 10 532.982 34.528 1 -1 4 -10 1373.22 79.56 3 -1 4 -10 1394.37 83.16 4 -1 4 -10 1314.43 72.42 1 1 -4 10 1399.10 72.53 1 1 -4 10 1362.20 76.65 5 -2 4 -10 13.1359 7.7402 4 -2 4 -10 13.7566 5.6771 1 -2 4 -10 18.2033 4.7939 1 -2 4 -10 1.5955 12.4731 2 -2 4 -10 7.1794 10.5873 3 2 -4 10 12.0875 9.0636 5 2 -4 10 16.7681 5.1869 1 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24.102 1 12 -4 10 128.729 19.382 1 12 -4 10 146.352 23.393 5 -13 4 -10 3.9877 11.9955 1 13 -4 10 -14.614 15.872 5 13 -4 10 16.6779 13.7656 1 -14 4 -10 131.934 25.090 1 14 -4 10 116.472 24.072 5 14 -4 10 131.081 21.919 1 -15 4 -10 6.4044 12.9723 1 15 -4 10 27.3232 17.7585 1 15 -4 10 12.8422 18.1541 5 16 -4 10 82.1554 19.2473 1 16 -4 10 51.8497 18.3648 5 -17 4 -10 146.288 28.696 1 17 -4 10 163.764 29.486 5 17 -4 10 102.206 24.670 1 -18 4 -10 -2.2762 14.7087 1 18 -4 10 2.9426 19.4400 1 18 -4 10 63.8118 23.4909 5 17 3 -10 88.7193 18.8099 1 17 3 -10 94.6686 22.3877 3 16 3 -10 248.795 26.994 1 16 3 -10 256.004 30.814 3 15 3 -10 86.0969 16.5207 1 15 3 -10 91.3796 19.5820 3 14 3 -10 385.048 36.468 3 14 3 -10 320.738 29.968 1 13 3 -10 159.822 24.708 3 13 3 -10 168.785 19.760 1 12 3 -10 290.635 31.026 3 12 3 -10 256.035 23.358 1 11 3 -10 235.340 26.452 3 11 3 -10 253.271 21.586 1 10 3 -10 70.3693 10.8449 1 -10 -3 10 50.1486 9.2285 1 9 3 -10 527.093 40.255 3 9 3 -10 448.799 30.321 1 -9 -3 10 448.243 29.966 1 8 3 -10 138.675 12.600 1 8 3 -10 140.082 18.600 3 -8 -3 10 140.903 12.168 1 -8 -3 10 138.345 11.057 5 7 3 -10 237.095 16.516 1 7 3 -10 246.479 24.358 4 7 3 -10 235.075 23.509 3 -7 -3 10 215.513 15.791 1 6 3 -10 173.810 11.785 1 6 3 -10 157.075 19.429 3 -6 -3 10 151.032 11.129 1 5 3 -10 563.640 40.687 4 5 3 -10 514.899 39.907 3 4 3 -10 493.927 38.686 2 4 3 -10 509.409 37.737 4 4 3 -10 459.999 35.831 3 -4 -3 10 501.422 30.961 5 3 3 -10 673.674 46.987 3 3 3 -10 728.768 48.628 4 3 3 -10 698.877 50.080 2 -3 -3 10 737.548 42.359 5 2 3 -10 625.888 42.408 3 2 3 -10 688.862 47.174 2 2 3 -10 566.124 42.657 4 -2 -3 10 650.840 38.746 5 1 3 -10 1208.92 74.39 4 1 3 -10 1322.55 78.52 2 1 3 -10 1184.15 71.86 3 -1 -3 10 1106.05 66.86 5 0 3 -10 260.832 24.233 4 0 3 -10 269.639 23.417 3 0 3 -10 251.457 25.906 2 0 -3 10 300.078 22.250 5 -1 3 -10 212.721 19.299 3 -1 3 -10 194.497 22.306 2 -1 3 -10 209.075 20.326 4 -1 3 -10 189.464 13.257 1 1 -3 10 185.112 17.429 5 1 -3 10 200.745 13.200 1 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420.437 33.012 1 10 -3 10 31.3499 12.1414 1 10 -3 10 16.5573 14.4293 5 -11 3 -10 110.161 20.812 1 11 -3 10 132.614 20.544 5 11 -3 10 139.944 18.578 1 -12 3 -10 63.8404 17.6536 1 -13 3 -10 400.559 36.162 1 13 -3 10 306.779 32.590 1 13 -3 10 309.242 33.530 5 14 -3 10 31.8365 16.5068 1 14 -3 10 4.2986 15.3970 5 -15 3 -10 121.629 21.599 1 15 -3 10 114.415 21.595 5 15 -3 10 68.9164 21.0219 1 -16 3 -10 78.0717 23.4229 1 16 -3 10 101.535 22.961 5 16 -3 10 102.295 22.680 1 17 -3 10 85.5680 20.7928 1 -18 3 -10 37.9252 23.2121 1 18 -3 10 91.4765 25.2046 1 -19 3 -10 -11.439 18.431 1 19 -3 10 14.1417 21.7940 1 17 2 -10 329.282 36.149 3 17 2 -10 394.505 36.133 1 16 2 -10 33.6361 14.7991 3 15 2 -10 256.412 29.383 3 15 2 -10 217.972 24.422 1 14 2 -10 202.545 25.303 3 14 2 -10 204.107 22.796 1 13 2 -10 268.293 25.056 1 13 2 -10 260.492 29.803 3 12 2 -10 187.768 24.659 3 12 2 -10 173.166 19.041 1 11 2 -10 3.42034 8.24583 1 11 2 -10 12.2336 10.5266 3 10 2 -10 190.882 23.814 3 10 2 -10 143.318 16.101 1 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-10 323.399 26.081 1 -5 -3 -10 409.163 29.319 4 5 3 10 383.780 27.268 1 -6 -3 -10 303.099 25.185 4 -6 -3 -10 337.944 25.789 1 6 3 10 282.688 23.899 1 -7 -3 -10 951.896 62.075 1 -7 -3 -10 1071.97 64.49 4 7 3 10 1100.06 63.56 1 -8 -3 -10 -2.3544 8.3156 1 -8 -3 -10 12.4289 7.6331 4 8 3 10 4.2788 11.2739 5 8 3 10 5.5953 11.0149 1 -9 -3 -10 190.288 21.116 1 -9 -3 -10 215.875 19.437 4 9 3 10 210.149 22.611 1 9 3 10 236.320 22.521 5 -10 -3 -10 73.3619 10.9031 4 -10 -3 -10 82.1787 17.4437 1 10 3 10 53.0724 14.6650 1 10 3 10 88.2707 15.3292 5 -11 -3 -10 39.4489 7.9891 4 11 3 10 53.2349 14.4306 5 -12 -3 -10 500.399 40.513 1 -12 -3 -10 446.002 32.937 4 12 3 10 534.210 39.724 5 12 3 10 620.486 44.086 1 -13 -3 -10 72.7204 20.7690 1 -14 -3 -10 411.130 37.873 1 14 3 10 337.803 32.388 5 14 3 10 328.165 35.137 1 -15 -3 -10 216.314 29.787 1 15 3 10 160.234 22.870 5 15 3 10 192.650 27.667 1 -16 -3 -10 476.279 45.603 1 16 3 10 473.839 40.644 5 16 3 10 440.841 42.213 1 -17 -3 -10 143.645 26.670 1 17 3 10 192.403 30.655 1 -18 -3 -10 111.377 27.321 1 18 3 10 130.352 27.261 1 19 3 10 57.4982 19.3450 1 17 -4 -10 -29.499 17.575 1 16 -4 -10 208.329 27.266 1 14 -4 -10 266.348 28.930 1 12 -4 -10 73.1490 13.9882 4 12 -4 -10 76.1902 16.6426 1 -12 4 10 72.9914 14.4415 1 11 -4 -10 66.9303 13.8514 1 11 -4 -10 68.7242 14.7062 4 -11 4 10 61.0279 14.0126 1 10 -4 -10 431.778 34.597 1 10 -4 -10 476.023 36.439 4 -10 4 10 448.480 34.347 1 9 -4 -10 39.1467 10.9714 1 9 -4 -10 30.9576 10.8052 4 -9 4 10 31.9220 10.4643 1 8 -4 -10 175.006 19.898 4 8 -4 -10 148.684 18.197 1 -8 4 10 142.898 16.458 1 7 -4 -10 496.977 34.101 1 7 -4 -10 444.439 31.918 1 7 -4 -10 443.209 35.962 4 -7 4 10 466.766 32.529 1 6 -4 -10 28.0935 13.0081 4 6 -4 -10 50.0854 9.0700 1 6 -4 -10 58.3622 12.1698 1 -6 4 10 41.1770 10.2800 1 5 -4 -10 1048.23 61.95 1 5 -4 -10 1091.67 64.01 1 5 -4 -10 1100.07 69.33 4 -5 4 10 1116.12 63.76 1 4 -4 -10 3.84518 5.61580 1 4 -4 -10 7.75416 8.34890 4 -4 4 10 -4.2673 6.3147 1 3 -4 -10 430.432 29.989 1 3 -4 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83.7376 16.3981 1 5 4 10 118.055 14.145 1 -6 -4 -10 407.973 30.962 4 -6 -4 -10 361.764 29.711 1 6 4 10 432.451 30.693 1 -7 -4 -10 77.1613 12.5967 4 -7 -4 -10 94.4187 15.4254 1 7 4 10 85.4914 14.4177 1 -8 -4 -10 257.181 22.727 4 -8 -4 -10 218.536 23.433 1 8 4 10 282.052 25.363 1 -9 -4 -10 -2.7889 14.5068 1 9 4 10 12.1961 11.9655 5 -10 -4 -10 -15.962 13.799 1 -10 -4 -10 -2.1114 7.1371 4 10 4 10 7.4235 11.6327 1 -11 -4 -10 948.448 65.541 1 -11 -4 -10 987.308 62.493 4 11 4 10 1155.96 68.55 1 11 4 10 1009.83 63.84 5 -12 -4 -10 37.5208 17.7755 1 -13 -4 -10 437.303 41.482 1 13 4 10 570.186 43.472 1 13 4 10 495.653 38.489 5 -14 -4 -10 80.6936 19.0810 1 14 4 10 106.358 18.571 5 -15 -4 -10 387.765 40.126 1 15 4 10 405.239 35.392 5 15 4 10 387.227 38.569 1 -16 -4 -10 337.169 37.254 1 16 4 10 350.366 37.802 1 16 4 10 285.096 30.598 5 -17 -4 -10 266.022 36.584 1 17 4 10 271.967 36.009 1 -18 -4 -10 42.1975 23.8159 1 18 4 10 70.7239 22.7893 1 -19 -4 -10 9.5006 15.3986 1 17 -5 -10 107.718 22.939 1 16 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255.336 21.192 1 -2 9 -11 208.901 22.586 3 -2 9 -11 210.307 25.853 2 -2 9 -11 245.920 21.779 1 2 -9 11 249.555 25.439 5 2 -9 11 227.970 20.704 1 -3 9 -11 34.8789 13.1740 2 -3 9 -11 21.8234 10.5756 3 -3 9 -11 34.4748 11.6607 1 3 -9 11 9.19519 8.53819 1 -4 9 -11 327.486 26.101 3 -4 9 -11 289.038 33.122 2 -4 9 -11 299.595 26.392 1 4 -9 11 275.330 24.240 1 4 -9 11 279.583 28.180 5 -5 9 -11 499.214 42.701 2 -5 9 -11 418.804 31.794 3 -5 9 -11 430.058 34.066 1 5 -9 11 427.702 38.142 5 5 -9 11 504.101 35.721 1 -6 9 -11 1.61580 9.97746 1 -6 9 -11 1.2820 15.9301 2 6 -9 11 -17.608 11.412 1 6 -9 11 -9.1623 17.6474 5 -7 9 -11 428.913 36.115 1 -7 9 -11 468.264 42.600 2 7 -9 11 411.091 34.678 1 7 -9 11 433.209 37.719 5 -8 9 -11 3.9224 18.1192 1 -8 9 -11 -8.8975 16.3985 2 8 -9 11 15.5752 13.7672 1 8 -9 11 -14.421 16.756 5 -9 9 -11 275.311 34.563 2 -9 9 -11 288.645 30.271 1 9 -9 11 248.441 32.763 5 9 -9 11 274.962 29.186 1 -10 9 -11 107.539 23.483 1 -10 9 -11 93.9924 20.7054 2 10 -9 11 91.4012 18.6923 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3 -5 -8 11 77.9809 7.9214 1 -5 -8 11 87.2470 10.5545 5 4 8 -11 30.8344 15.4410 3 4 8 -11 42.3444 6.1150 1 -4 -8 11 35.8479 5.6760 1 -4 -8 11 34.3240 8.6591 5 3 8 -11 627.862 46.186 3 3 8 -11 638.966 35.783 1 3 8 -11 607.339 48.877 2 -3 -8 11 586.699 38.883 5 2 8 -11 18.3021 5.6694 1 2 8 -11 19.6268 15.5457 2 2 8 -11 12.3651 13.1647 3 -2 -8 11 21.3589 9.4239 5 -2 -8 11 15.3175 4.7835 1 1 8 -11 186.297 15.267 1 1 8 -11 218.198 16.763 1 1 8 -11 251.972 27.802 2 1 8 -11 223.101 24.293 3 -1 -8 11 209.025 16.175 1 -1 -8 11 228.406 20.883 5 0 8 -11 177.947 22.826 3 0 8 -11 229.752 27.027 2 0 8 -11 183.641 16.119 1 0 8 -11 183.050 15.009 1 0 -8 11 184.958 15.587 1 0 -8 11 219.894 20.587 5 -1 8 -11 425.478 34.024 3 -1 8 -11 462.497 30.268 1 -1 8 -11 371.446 27.581 1 -1 8 -11 446.209 39.241 2 1 -8 11 419.483 29.263 1 1 -8 11 464.023 33.694 5 -2 8 -11 24.1488 11.6192 3 -2 8 -11 15.9891 8.8396 1 -2 8 -11 10.4817 14.8849 2 -2 8 -11 10.8991 5.8351 1 2 -8 11 -1.7598 11.4618 5 2 -8 11 20.4696 7.9486 1 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21.3286 1 12 -8 11 93.4873 19.9495 1 12 -8 11 98.6843 23.3531 5 -13 8 -11 224.724 31.207 1 13 -8 11 183.957 30.079 5 13 -8 11 226.758 28.181 1 14 -8 11 -27.620 21.760 5 14 -8 11 13.8613 15.6172 1 15 -8 11 61.8348 23.9082 5 15 -8 11 37.0466 20.8883 1 -16 8 -11 0.8998 17.8266 1 16 -8 11 -14.760 19.902 5 16 -8 11 6.3813 18.2257 1 -17 8 -11 139.452 31.939 1 17 -8 11 183.707 34.417 5 17 -8 11 97.8033 24.0590 1 17 7 -11 192.743 33.284 3 16 7 -11 -1.8583 21.3862 3 16 7 -11 61.3026 15.7352 1 15 7 -11 162.679 31.441 3 15 7 -11 206.167 22.658 1 14 7 -11 37.6272 12.9374 1 13 7 -11 429.757 43.948 3 13 7 -11 458.883 33.834 1 12 7 -11 54.2484 11.7286 1 12 7 -11 13.4355 15.8831 3 11 7 -11 263.023 32.589 3 11 7 -11 213.980 19.871 1 10 7 -11 31.7366 8.4445 1 10 7 -11 12.9488 13.0929 3 9 7 -11 307.667 22.004 1 9 7 -11 264.928 32.450 3 8 7 -11 210.278 16.525 1 8 7 -11 214.059 28.510 3 7 7 -11 40.3622 6.5130 1 7 7 -11 51.8342 17.1049 3 -7 -7 11 38.8806 6.0248 5 6 7 -11 151.056 22.158 3 6 7 -11 126.598 9.970 1 -6 -7 11 115.315 11.156 5 -6 -7 11 100.969 9.095 1 5 7 -11 99.0867 8.1950 1 5 7 -11 87.5418 7.9494 1 -5 -7 11 92.6441 10.7270 5 -5 -7 11 90.6653 7.6035 1 4 7 -11 1156.77 73.00 3 4 7 -11 1083.96 76.62 2 -4 -7 11 1100.58 62.77 5 3 7 -11 102.266 19.158 2 -3 -7 11 85.9773 11.7964 5 2 7 -11 81.7475 14.1905 3 2 7 -11 92.5047 18.3143 2 2 7 -11 65.2635 6.8933 1 2 7 -11 88.2832 7.9480 1 -2 -7 11 79.2047 12.0373 5 -2 -7 11 83.3959 7.5437 1 1 7 -11 174.671 23.255 2 1 7 -11 174.516 19.091 3 1 7 -11 159.262 12.378 1 -1 -7 11 127.985 11.270 1 -1 -7 11 130.925 16.076 5 0 7 -11 524.270 38.626 3 0 7 -11 529.273 31.765 1 0 7 -11 437.623 29.678 1 0 7 -11 544.247 43.793 2 0 -7 11 503.100 35.083 5 0 -7 11 517.420 31.000 1 -1 7 -11 573.335 41.278 3 -1 7 -11 548.961 35.949 1 -1 7 -11 670.612 48.512 2 -1 7 -11 543.365 34.863 1 1 -7 11 586.198 36.017 1 1 -7 11 608.247 40.749 5 -2 7 -11 196.283 17.404 1 -2 7 -11 213.412 26.009 2 -2 7 -11 183.534 16.138 1 -2 7 -11 173.951 20.113 3 2 -7 11 210.645 21.315 5 2 -7 11 232.776 17.621 1 -3 7 -11 29.9251 7.3621 1 -3 7 -11 40.1292 9.1328 1 -3 7 -11 22.1058 14.8118 2 -3 7 -11 50.3230 10.4941 3 3 -7 11 19.4745 13.3960 5 3 -7 11 40.8147 8.8062 1 -4 7 -11 42.2658 16.8953 2 -4 7 -11 80.1509 11.1361 1 -4 7 -11 55.1781 11.0498 3 -4 7 -11 66.2163 12.3570 1 4 -7 11 70.3555 16.2454 5 4 -7 11 65.7197 10.4790 1 -5 7 -11 613.929 41.899 3 -5 7 -11 722.115 53.390 2 -5 7 -11 644.583 43.573 1 5 -7 11 699.412 43.841 1 5 -7 11 635.699 45.962 5 -6 7 -11 -13.041 16.691 2 6 -7 11 -4.1715 9.4074 1 6 -7 11 -18.061 11.558 5 -7 7 -11 172.411 25.846 2 -7 7 -11 151.078 19.114 1 7 -7 11 146.207 20.505 5 7 -7 11 163.882 19.363 1 -8 7 -11 174.046 26.554 2 -8 7 -11 169.325 20.517 1 8 -7 11 158.786 21.540 5 8 -7 11 178.549 21.136 1 -9 7 -11 71.8256 17.5659 2 -9 7 -11 33.9442 16.0742 1 9 -7 11 33.3882 14.5380 1 9 -7 11 47.0240 14.8089 5 -10 7 -11 188.420 25.620 1 10 -7 11 197.567 24.801 1 10 -7 11 188.618 27.732 5 -11 7 -11 276.821 31.239 1 11 -7 11 257.330 32.009 5 11 -7 11 190.922 24.615 1 -12 7 -11 169.764 26.865 1 12 -7 11 192.337 30.248 5 12 -7 11 177.012 24.045 1 -13 7 -11 30.7873 18.7326 1 13 -7 11 63.4060 22.3035 5 13 -7 11 46.8128 14.5446 1 -14 7 -11 378.655 40.596 1 14 -7 11 383.795 40.404 5 14 -7 11 346.167 37.011 1 -15 7 -11 71.0868 20.1758 1 15 -7 11 38.0295 24.3525 5 15 -7 11 71.4414 21.3599 1 -16 7 -11 30.5524 21.6949 1 16 -7 11 14.3959 18.7975 1 16 -7 11 46.2954 21.5113 5 17 -7 11 21.8403 22.5830 5 17 -7 11 -8.1315 17.2623 1 17 6 -11 157.882 23.089 1 17 6 -11 228.203 33.875 3 16 6 -11 277.122 36.935 3 16 6 -11 293.390 28.971 1 15 6 -11 28.2393 11.9907 1 14 6 -11 358.229 29.802 1 14 6 -11 313.786 37.136 3 13 6 -11 34.1482 15.4478 3 12 6 -11 524.700 37.086 1 12 6 -11 575.253 48.734 3 11 6 -11 16.0764 16.9449 3 11 6 -11 26.6743 8.6824 1 10 6 -11 8.6805 16.1056 3 9 6 -11 176.335 15.690 1 9 6 -11 226.345 27.430 3 8 6 -11 255.723 28.968 3 8 6 -11 215.660 16.438 1 -8 -6 11 225.308 14.793 5 7 6 -11 109.126 20.450 3 7 6 -11 99.5969 9.1147 1 -7 -6 11 102.175 9.617 5 -7 -6 11 87.3311 8.2958 1 6 6 -11 44.7643 5.4604 1 6 6 -11 71.0930 16.8476 3 6 6 -11 62.2053 6.3180 1 -6 -6 11 55.2732 5.4761 1 5 6 -11 400.933 35.029 3 -5 -6 11 399.663 26.154 5 4 6 -11 28.4762 16.7651 2 -4 -6 11 -11.393 5.994 5 3 6 -11 317.182 30.747 2 3 6 -11 252.844 27.243 3 -3 -6 11 299.691 22.011 5 2 6 -11 77.5979 18.0591 2 2 6 -11 76.0803 16.1749 3 -2 -6 11 93.5283 12.2569 5 1 6 -11 349.945 29.492 3 1 6 -11 302.824 19.914 1 1 6 -11 383.360 34.026 2 -1 -6 11 337.600 25.446 5 -1 -6 11 321.991 19.963 1 0 6 -11 822.387 54.930 2 0 6 -11 633.286 40.218 1 0 6 -11 736.834 48.860 3 0 -6 11 731.433 45.499 5 0 -6 11 678.304 40.247 1 -1 6 -11 359.618 29.015 3 -1 6 -11 423.335 35.937 2 -1 6 -11 346.113 24.241 1 1 -6 11 356.793 24.000 1 1 -6 11 379.473 28.764 5 -2 6 -11 258.181 27.490 2 -2 6 -11 218.635 21.230 3 -2 6 -11 193.016 15.906 1 -2 6 -11 188.788 16.851 1 2 -6 11 208.849 16.628 1 2 -6 11 223.628 21.268 5 -3 6 -11 172.263 16.063 1 -3 6 -11 146.504 14.276 1 -3 6 -11 170.617 17.858 3 -3 6 -11 211.708 25.204 2 3 -6 11 175.513 15.312 1 3 -6 11 185.928 20.192 5 -4 6 -11 1233.90 76.64 2 -4 6 -11 1092.02 65.55 3 -4 6 -11 968.609 62.988 1 4 -6 11 1147.14 64.05 1 4 -6 11 1074.20 67.43 5 -5 6 -11 137.563 16.641 1 -5 6 -11 155.712 23.450 2 5 -6 11 109.650 19.865 5 5 -6 11 146.560 16.074 1 -6 6 -11 169.600 25.349 2 -6 6 -11 161.401 19.158 1 6 -6 11 215.802 20.181 1 6 -6 11 190.229 22.919 5 -7 6 -11 2.3768 15.0100 2 -7 6 -11 -10.132 9.831 1 7 -6 11 3.11919 4.68233 3 7 -6 11 -8.1311 14.7379 5 7 -6 11 5.01402 9.25074 1 -8 6 -11 161.621 25.771 2 -8 6 -11 140.130 19.812 1 8 -6 11 181.881 22.769 5 8 -6 11 174.556 20.015 1 -9 6 -11 691.553 49.983 1 9 -6 11 717.608 51.437 5 9 -6 11 687.430 48.455 1 -10 6 -11 260.279 29.552 1 10 -6 11 293.035 33.288 5 10 -6 11 300.096 29.630 1 -11 6 -11 69.2891 19.0589 1 11 -6 11 67.0606 17.5760 1 11 -6 11 58.6267 20.8643 5 -12 6 -11 204.382 28.335 1 12 -6 11 235.281 28.340 1 12 -6 11 233.486 28.820 5 -13 6 -11 370.230 38.116 1 13 -6 11 322.552 37.838 5 13 -6 11 403.852 36.965 1 14 -6 11 -4.5245 13.2394 1 14 -6 11 13.9850 19.9055 5 -15 6 -11 122.672 22.429 1 15 -6 11 80.7126 23.4493 5 -16 6 -11 60.8563 23.3651 1 16 -6 11 87.8880 25.2123 5 16 -6 11 41.4074 18.3697 1 17 -6 11 103.239 25.234 5 17 -6 11 105.640 25.510 1 17 5 -11 231.289 27.053 1 17 5 -11 227.681 31.670 3 16 5 -11 112.466 18.591 1 16 5 -11 91.1353 21.2696 3 15 5 -11 183.564 21.679 1 15 5 -11 148.344 24.672 3 14 5 -11 47.4724 12.7688 1 13 5 -11 419.453 32.029 1 13 5 -11 424.141 41.698 3 12 5 -11 104.195 14.108 1 12 5 -11 105.933 22.426 3 11 5 -11 160.268 24.187 3 11 5 -11 135.689 15.129 1 10 5 -11 81.0190 11.1237 1 9 5 -11 164.568 14.471 1 9 5 -11 174.590 25.454 3 8 5 -11 693.631 49.291 3 8 5 -11 629.556 37.017 1 -8 -5 11 599.256 35.254 5 7 5 -11 47.0373 13.1142 3 7 5 -11 23.1337 5.0157 1 -7 -5 11 19.6430 4.4254 1 -7 -5 11 29.7968 5.9701 5 6 5 -11 9.33719 9.85714 3 -6 -5 11 25.0930 6.1436 5 5 5 -11 -2.3450 12.2963 3 4 5 -11 655.067 49.728 2 4 5 -11 630.324 46.017 3 -4 -5 11 608.939 37.874 5 3 5 -11 55.4949 15.2188 3 3 5 -11 33.7622 11.9344 2 -3 -5 11 31.4668 7.6972 5 2 5 -11 448.997 39.187 2 2 5 -11 455.890 36.420 3 -2 -5 11 475.477 31.353 5 1 5 -11 537.568 40.416 3 1 5 -11 595.391 45.519 2 1 5 -11 515.839 40.847 4 -1 -5 11 592.917 37.067 5 0 5 -11 599.262 40.403 3 0 5 -11 500.628 31.240 1 0 5 -11 508.545 40.118 4 0 5 -11 632.501 45.725 2 0 -5 11 519.856 31.146 1 0 -5 11 584.023 37.121 5 -1 5 -11 798.984 51.879 3 -1 5 -11 759.594 44.736 1 -1 5 -11 906.413 59.348 2 1 -5 11 835.956 50.127 5 1 -5 11 736.700 44.426 1 -2 5 -11 187.104 15.015 1 -2 5 -11 199.463 15.794 1 -2 5 -11 204.916 24.802 2 -2 5 -11 219.110 20.512 3 2 -5 11 206.977 15.569 1 2 -5 11 205.386 20.472 5 -3 5 -11 384.430 27.375 1 -3 5 -11 472.367 38.166 2 -3 5 -11 427.551 30.749 3 3 -5 11 380.535 31.388 5 3 -5 11 433.474 27.719 1 -4 5 -11 67.0342 18.2830 2 -4 5 -11 53.8439 10.2065 1 -4 5 -11 30.1758 7.2604 1 4 -5 11 41.8067 8.6651 1 4 -5 11 37.8628 13.1829 5 -5 5 -11 1515.09 96.36 1 -5 5 -11 1981.33 110.73 2 -5 5 -11 1597.58 94.87 1 5 -5 11 1697.73 97.96 5 5 -5 11 1814.97 95.49 1 -6 5 -11 16.5665 16.5334 2 6 -5 11 5.5465 13.1488 5 -7 5 -11 127.150 17.134 1 -7 5 -11 135.466 23.100 2 7 -5 11 136.282 16.624 1 7 -5 11 116.902 19.913 5 -8 5 -11 385.468 32.646 1 8 -5 11 423.507 32.741 1 8 -5 11 428.887 36.256 5 -9 5 -11 120.858 18.817 1 9 -5 11 115.375 18.601 5 9 -5 11 104.158 17.551 1 -10 5 -11 364.533 33.973 1 10 -5 11 318.905 31.232 1 10 -5 11 383.368 35.470 5 -11 5 -11 217.296 27.531 1 11 -5 11 299.803 28.430 1 11 -5 11 228.907 29.285 5 -12 5 -11 93.7657 19.7763 1 12 -5 11 115.365 19.986 1 12 -5 11 77.4580 20.8013 5 -13 5 -11 3.7658 15.1002 1 13 -5 11 8.4875 13.8744 1 13 -5 11 -35.838 20.059 5 -14 5 -11 95.5603 23.6356 1 14 -5 11 87.2297 22.9945 5 14 -5 11 86.9485 18.1400 1 15 -5 11 48.9051 20.3528 1 15 -5 11 40.7158 21.8473 5 16 -5 11 125.824 23.133 1 16 -5 11 175.758 30.128 5 -17 5 -11 87.9744 22.4797 1 17 -5 11 77.7652 24.0337 1 17 -5 11 82.9245 23.7572 5 18 -5 11 4.8980 17.8333 1 18 -5 11 11.6043 22.2253 5 17 4 -11 101.912 24.250 3 17 4 -11 110.804 19.876 1 16 4 -11 298.646 29.618 1 16 4 -11 324.748 37.175 3 15 4 -11 43.0894 13.6154 1 15 4 -11 0.0219 15.4288 3 14 4 -11 107.753 16.951 1 14 4 -11 137.069 24.895 3 13 4 -11 204.554 20.616 1 13 4 -11 212.487 27.488 3 12 4 -11 458.107 33.179 1 12 4 -11 475.362 43.176 3 11 4 -11 290.334 32.005 3 11 4 -11 274.990 22.490 1 10 4 -11 115.675 21.021 3 10 4 -11 79.9796 10.8428 1 9 4 -11 296.411 29.365 3 9 4 -11 294.744 20.498 1 -9 -4 11 250.976 17.086 5 8 4 -11 20.0613 5.4278 1 8 4 -11 49.2236 17.0145 3 -8 -4 11 23.3768 5.1790 5 -8 -4 11 34.2180 5.8207 1 7 4 -11 267.955 17.004 1 7 4 -11 288.594 28.759 3 -7 -4 11 232.306 16.273 1 -7 -4 11 249.411 17.998 5 6 4 -11 7.8462 12.8351 3 -6 -4 11 -1.2586 4.8631 5 5 4 -11 428.192 34.950 4 5 4 -11 421.765 34.579 3 -5 -4 11 405.425 27.046 5 4 4 -11 411.882 35.516 2 4 4 -11 400.112 32.953 4 4 4 -11 407.634 34.327 3 -4 -4 11 407.095 27.298 5 3 4 -11 60.0946 16.6133 2 3 4 -11 69.5592 14.9528 4 -3 -4 11 42.1802 8.5033 5 2 4 -11 4.83328 8.30235 4 2 4 -11 -17.318 12.545 3 2 4 -11 9.7474 13.4967 2 -2 -4 11 -12.379 6.783 5 1 4 -11 905.923 57.849 4 1 4 -11 867.217 55.662 3 1 4 -11 914.128 61.410 2 -1 -4 11 761.844 50.084 5 0 4 -11 1657.27 97.55 2 0 4 -11 1503.72 92.73 4 0 4 -11 1572.12 89.88 3 0 -4 11 1409.51 84.43 5 -1 4 -11 101.887 15.203 3 -1 4 -11 86.6048 17.5840 2 -1 4 -11 72.1033 7.9306 1 -1 4 -11 106.923 15.015 4 1 -4 11 98.8400 13.6581 5 1 -4 11 79.5991 7.6595 1 -2 4 -11 544.770 39.725 4 -2 4 -11 582.824 37.789 3 -2 4 -11 653.659 45.635 2 -2 4 -11 480.329 31.871 1 -2 4 -11 523.655 32.347 1 2 -4 11 507.110 31.987 1 2 -4 11 566.129 37.645 5 -3 4 -11 5.19382 4.21782 1 -3 4 -11 -0.7229 5.5823 1 -3 4 -11 7.35258 8.66913 4 -3 4 -11 17.6870 9.0736 3 -3 4 -11 -9.8137 11.1516 2 3 -4 11 -5.7527 10.4166 5 3 -4 11 10.8369 5.1997 1 -4 4 -11 795.722 50.994 1 -4 4 -11 932.201 52.232 1 -4 4 -11 955.130 58.026 4 -4 4 -11 804.604 61.203 2 4 -4 11 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7 -12 15.5221 14.8738 2 0 -7 12 15.3992 4.8417 1 0 -7 12 21.9467 8.4551 5 -1 7 -12 682.000 43.557 1 -1 7 -12 837.907 58.619 2 -1 7 -12 733.357 50.176 3 1 -7 12 749.844 48.927 5 1 -7 12 731.375 43.639 1 -2 7 -12 275.640 21.192 1 -2 7 -12 264.796 31.346 2 -2 7 -12 299.123 26.107 3 2 -7 12 250.271 24.056 5 2 -7 12 251.396 20.156 1 -3 7 -12 3.50094 9.68878 3 -3 7 -12 20.4528 6.3501 1 3 -7 12 17.3201 7.1094 1 3 -7 12 30.7373 14.1376 5 -4 7 -12 626.448 42.721 1 -4 7 -12 665.355 44.837 3 4 -7 12 720.132 43.607 1 4 -7 12 687.495 47.843 5 -5 7 -12 68.6941 13.7863 1 5 -7 12 78.7923 12.6701 1 5 -7 12 80.9950 17.9253 5 -6 7 -12 742.631 49.881 1 -6 7 -12 817.105 59.458 2 6 -7 12 736.453 51.697 5 6 -7 12 691.913 47.921 1 -7 7 -12 -14.930 16.366 2 -7 7 -12 -13.457 12.288 1 7 -7 12 -23.137 13.693 5 7 -7 12 4.5372 10.4343 1 -8 7 -12 137.686 20.887 1 -8 7 -12 168.829 25.766 2 8 -7 12 181.783 23.171 5 8 -7 12 204.312 22.162 1 -9 7 -12 88.3190 19.1492 1 -9 7 -12 128.839 24.577 2 9 -7 12 82.7096 16.0574 1 9 -7 12 79.7332 19.8457 5 -10 7 -12 338.799 32.181 1 -10 7 -12 348.310 39.691 2 10 -7 12 350.895 36.733 5 10 -7 12 360.536 33.286 1 -11 7 -12 4.5653 14.7089 1 11 -7 12 20.6581 18.3850 5 -12 7 -12 78.0489 21.4387 1 12 -7 12 58.0422 16.4675 1 12 -7 12 90.1332 24.0870 5 -13 7 -12 61.4268 21.9761 1 13 -7 12 78.9958 18.6703 1 13 -7 12 75.6423 21.3673 5 14 -7 12 68.3422 20.1354 1 14 -7 12 63.7248 23.0080 5 -15 7 -12 106.857 22.733 1 15 -7 12 135.682 24.877 1 -16 7 -12 11.6921 20.4509 1 16 -7 12 -37.501 18.354 1 16 -7 12 16.3235 16.9986 5 -17 7 -12 11.4339 22.2717 1 17 -7 12 75.1191 22.9514 1 17 -7 12 39.3559 26.4593 5 17 6 -12 166.647 30.147 3 16 6 -12 101.114 17.807 1 16 6 -12 92.7592 25.8271 3 15 6 -12 129.903 25.250 3 15 6 -12 133.986 18.224 1 14 6 -12 1.3299 16.4407 3 14 6 -12 8.33242 9.64581 1 13 6 -12 447.352 33.691 1 13 6 -12 512.685 47.331 3 12 6 -12 73.8847 22.6190 3 11 6 -12 76.7097 21.4387 3 11 6 -12 76.5260 10.5780 1 10 6 -12 79.0604 10.2582 1 9 6 -12 127.243 11.886 1 8 6 -12 420.984 25.818 1 8 6 -12 468.537 40.531 3 -8 -6 12 409.607 25.594 5 7 6 -12 114.147 21.103 3 -7 -6 12 74.2934 8.9517 5 6 6 -12 365.173 33.684 3 -6 -6 12 314.680 22.551 5 5 6 -12 166.155 25.001 3 -5 -6 12 122.157 13.029 5 4 6 -12 854.872 57.479 3 4 6 -12 815.625 61.982 2 -4 -6 12 812.815 48.818 5 3 6 -12 149.712 21.043 3 3 6 -12 118.153 21.345 2 -3 -6 12 141.841 14.832 5 2 6 -12 385.796 34.018 3 2 6 -12 416.933 38.544 2 -2 -6 12 417.959 29.260 5 1 6 -12 79.5616 16.3612 2 1 6 -12 87.5625 16.7051 3 -1 -6 12 102.625 13.818 5 0 6 -12 456.583 34.842 3 0 6 -12 426.991 26.754 1 0 6 -12 524.749 42.136 2 0 -6 12 447.436 32.759 5 0 -6 12 414.951 26.279 1 -1 6 -12 351.417 24.076 1 -1 6 -12 367.786 34.672 2 -1 6 -12 393.334 31.249 3 1 -6 12 386.899 24.105 1 1 -6 12 344.907 28.950 5 -2 6 -12 90.2303 10.3235 1 -2 6 -12 152.786 22.359 2 -2 6 -12 119.299 12.267 1 -2 6 -12 122.524 16.042 3 2 -6 12 112.817 11.401 1 2 -6 12 103.349 14.892 5 -3 6 -12 216.709 21.526 3 -3 6 -12 254.238 19.340 1 -3 6 -12 246.689 28.763 2 3 -6 12 234.248 18.640 1 3 -6 12 219.865 23.219 5 -4 6 -12 10.1356 8.0359 3 -4 6 -12 6.3894 13.2328 2 -4 6 -12 4.62906 8.62068 1 4 -6 12 -12.568 12.704 5 4 -6 12 14.8350 7.0512 1 -5 6 -12 931.334 65.684 2 -5 6 -12 780.274 53.421 1 5 -6 12 958.915 54.745 1 5 -6 12 871.898 58.558 5 -6 6 -12 -12.992 11.469 1 -6 6 -12 -7.6438 11.9051 2 6 -6 12 -7.5891 26.0414 5 -7 6 -12 206.564 28.403 2 -7 6 -12 220.202 23.445 1 7 -6 12 259.766 23.874 1 7 -6 12 248.670 27.066 5 -8 6 -12 141.091 19.124 1 -8 6 -12 99.9098 20.5972 2 8 -6 12 88.5754 17.2326 5 8 -6 12 120.631 16.845 1 -9 6 -12 137.783 21.658 1 -9 6 -12 203.086 29.056 2 9 -6 12 197.753 25.975 5 9 -6 12 150.908 20.425 1 -10 6 -12 207.723 25.579 1 10 -6 12 113.546 25.431 5 10 -6 12 166.545 21.232 1 -11 6 -12 228.709 27.265 1 11 -6 12 177.907 27.852 5 11 -6 12 161.033 23.299 1 12 -6 12 76.7801 18.2109 1 12 -6 12 56.2836 17.4595 5 -13 6 -12 32.4256 18.2304 1 13 -6 12 40.6433 20.5771 5 -14 6 -12 349.300 37.798 1 14 -6 12 329.804 38.530 5 14 -6 12 303.822 34.579 1 15 -6 12 9.4292 19.6574 5 -16 6 -12 23.7838 20.9633 1 16 -6 12 67.5176 23.8350 5 -17 6 -12 36.6827 17.0153 1 17 -6 12 -2.4144 18.5238 5 17 -6 12 10.5104 18.7337 1 17 5 -12 239.726 34.838 3 16 5 -12 247.070 25.899 1 16 5 -12 254.917 34.543 3 15 5 -12 72.6553 22.0985 3 14 5 -12 60.8973 12.8145 1 13 5 -12 27.4430 10.1192 1 12 5 -12 505.388 44.559 3 12 5 -12 422.564 31.679 1 11 5 -12 25.7662 7.8767 1 11 5 -12 47.2791 18.8331 3 10 5 -12 55.8594 19.1418 3 10 5 -12 33.3917 7.7105 1 9 5 -12 481.583 40.806 3 9 5 -12 429.378 28.050 1 8 5 -12 209.142 14.705 1 8 5 -12 220.202 27.765 3 -8 -5 12 191.917 14.550 5 7 5 -12 348.018 33.725 3 -7 -5 12 325.322 22.314 5 6 5 -12 -6.4119 13.1047 3 5 5 -12 288.671 28.266 3 -5 -5 12 277.528 20.650 5 4 5 -12 105.976 21.366 2 -4 -5 12 118.669 12.782 5 3 5 -12 817.156 60.817 2 3 5 -12 899.687 58.291 3 3 5 -12 828.885 58.444 4 -3 -5 12 858.909 50.499 5 2 5 -12 2.5390 13.8747 2 2 5 -12 12.9049 12.7202 4 2 5 -12 -26.953 13.725 3 -2 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17 4 -12 288.477 36.645 3 16 4 -12 132.576 19.994 1 16 4 -12 118.829 26.418 3 15 4 -12 157.105 26.912 3 15 4 -12 135.139 18.674 1 14 4 -12 19.4325 9.5394 1 13 4 -12 185.726 27.982 3 13 4 -12 176.560 18.921 1 12 4 -12 149.021 16.216 1 12 4 -12 141.601 25.479 3 11 4 -12 398.049 29.002 1 11 4 -12 445.210 39.458 3 10 4 -12 147.868 23.496 3 10 4 -12 116.182 12.449 1 9 4 -12 98.3893 10.4227 1 9 4 -12 104.362 21.698 3 -9 -4 12 97.1874 9.3941 5 8 4 -12 443.615 37.924 3 8 4 -12 391.451 24.510 1 -8 -4 12 378.115 24.984 5 7 4 -12 382.113 34.656 3 -7 -4 12 344.112 23.791 5 6 4 -12 79.4396 17.4197 4 6 4 -12 58.3504 16.9365 3 -6 -4 12 64.5529 9.1847 5 5 4 -12 64.4145 15.9040 3 5 4 -12 47.5326 14.8293 4 -5 -4 12 59.9461 9.3154 5 4 4 -12 679.010 48.638 3 4 4 -12 688.190 49.650 4 4 4 -12 679.685 52.660 2 -4 -4 12 681.456 41.742 5 3 4 -12 233.331 24.049 3 3 4 -12 220.023 23.221 4 3 4 -12 215.786 26.320 2 -3 -4 12 224.064 18.597 5 2 4 -12 278.192 30.154 2 2 4 -12 317.995 28.247 3 2 4 -12 274.459 27.609 4 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3 -12 90.8375 23.1296 3 16 3 -12 346.464 31.664 1 16 3 -12 355.033 38.762 3 15 3 -12 27.6764 19.1181 3 15 3 -12 44.3945 13.4446 1 14 3 -12 93.2434 21.8638 3 14 3 -12 128.147 17.211 1 13 3 -12 114.749 22.386 3 13 3 -12 87.8841 14.2401 1 12 3 -12 193.687 27.765 3 12 3 -12 201.698 19.464 1 11 3 -12 318.690 25.014 1 11 3 -12 364.943 35.547 3 10 3 -12 185.397 16.899 1 10 3 -12 218.063 27.436 3 9 3 -12 103.304 11.335 1 9 3 -12 131.610 21.970 3 8 3 -12 119.493 17.733 4 8 3 -12 99.9695 17.5898 3 8 3 -12 120.759 10.931 1 7 3 -12 269.809 27.302 4 7 3 -12 227.391 25.707 3 7 3 -12 226.939 14.860 1 7 3 -12 223.978 14.695 1 -7 -3 12 194.859 14.137 1 6 3 -12 -8.9390 16.1146 4 5 3 -12 99.6929 18.1276 4 5 3 -12 126.349 19.861 3 4 3 -12 133.579 21.530 2 4 3 -12 91.9835 17.7503 3 -4 -3 12 121.702 13.404 5 3 3 -12 356.863 32.016 3 3 3 -12 420.438 36.360 2 -3 -3 12 395.941 27.772 5 2 3 -12 875.110 56.721 4 2 3 -12 815.956 54.561 3 2 3 -12 757.838 57.457 2 -2 -3 12 820.435 49.441 5 1 3 -12 454.423 35.902 3 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2 -12 1559.45 97.29 4 1 2 -12 1579.73 94.06 3 1 2 -12 1707.87 102.08 2 0 2 -12 248.937 23.642 3 0 2 -12 242.520 24.320 4 0 2 -12 242.551 26.167 2 0 -2 12 219.487 20.033 5 -1 2 -12 614.554 42.920 4 -1 2 -12 604.006 32.697 1 -1 2 -12 605.052 40.555 3 -1 2 -12 593.893 45.530 2 1 -2 12 525.845 32.096 1 1 -2 12 587.741 39.280 5 -2 2 -12 269.021 18.031 1 -2 2 -12 294.172 29.230 2 -2 2 -12 304.206 25.889 4 -2 2 -12 252.793 17.649 1 2 -2 12 273.109 23.044 5 2 -2 12 231.109 17.084 1 -3 2 -12 1031.33 65.24 4 -3 2 -12 938.965 56.692 1 -3 2 -12 1041.66 57.18 1 -3 2 -12 1054.58 70.44 2 3 -2 12 1093.97 62.78 5 3 -2 12 978.382 56.616 1 -4 2 -12 114.457 15.779 4 -4 2 -12 75.3624 19.0626 2 -4 2 -12 109.212 12.438 1 -4 2 -12 109.035 11.746 1 4 -2 12 148.048 17.752 5 4 -2 12 117.080 11.961 1 -5 2 -12 679.870 44.628 1 -5 2 -12 762.635 55.770 2 -5 2 -12 770.827 45.572 1 -5 2 -12 781.208 49.928 4 5 -2 12 691.548 44.255 1 5 -2 12 731.329 48.089 5 -6 2 -12 457.001 33.179 4 -6 2 -12 467.797 31.995 1 -6 2 -12 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119.269 15.606 3 -5 8 -13 124.004 16.522 1 -5 8 -13 98.7422 23.2095 2 5 -8 13 127.789 16.469 1 5 -8 13 138.943 22.355 5 -6 8 -13 949.279 70.296 2 -6 8 -13 950.707 59.744 1 6 -8 13 966.660 59.485 1 6 -8 13 849.387 63.088 5 -7 8 -13 10.1026 18.8993 2 -7 8 -13 2.6250 13.7826 1 7 -8 13 -4.3027 16.8493 5 7 -8 13 -17.399 10.914 1 -8 8 -13 319.457 30.618 1 -8 8 -13 352.215 39.173 2 8 -8 13 337.333 35.525 5 8 -8 13 321.738 30.125 1 -9 8 -13 2.4610 17.2948 2 -9 8 -13 16.8779 15.0783 1 9 -8 13 -4.6098 17.8542 5 9 -8 13 -20.878 13.285 1 -10 8 -13 290.553 33.167 1 -10 8 -13 375.466 41.729 2 10 -8 13 351.125 33.216 1 10 -8 13 370.990 38.317 5 -11 8 -13 2.8064 16.0174 1 -11 8 -13 -7.7206 18.5851 2 11 -8 13 -22.173 15.162 1 -12 8 -13 78.8253 25.0655 2 -12 8 -13 82.7610 18.8058 1 12 -8 13 46.7646 17.4509 1 12 -8 13 46.9127 22.6573 5 -13 8 -13 -13.260 16.784 2 -13 8 -13 -4.4258 14.4738 1 13 -8 13 57.7214 19.2412 1 13 -8 13 42.9308 22.4818 5 -14 8 -13 74.8916 18.8232 1 14 -8 13 66.2982 21.6265 1 14 -8 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13 13 190.583 23.972 1 -2 -13 -13 101.258 18.587 1 2 13 13 86.0305 20.1571 1 -3 -13 -13 324.430 32.960 1 3 13 13 286.179 29.890 1 -4 -13 -13 -21.080 13.337 1 4 13 13 -8.1012 17.1416 1 -5 -13 -13 693.986 52.322 1 5 13 13 619.431 49.231 1 -6 -13 -13 -3.1975 12.7292 1 6 13 13 -37.373 17.498 1 -7 -13 -13 -15.272 17.661 1 7 13 13 27.1981 14.6973 1 -8 -13 -13 98.5477 21.9262 1 8 13 13 72.3579 20.2248 1 -9 -13 -13 195.361 26.384 1 9 13 13 200.384 28.293 1 -10 -13 -13 81.2540 21.7031 1 11 13 13 91.5065 21.8062 1 -12 -13 -13 85.8776 25.4459 1 12 13 13 54.6066 19.4365 1 -13 -13 -13 32.5921 22.2604 1 13 13 13 67.7710 21.8949 1 -14 -13 -13 226.133 35.334 1 14 13 13 280.275 35.797 1 -15 -13 -13 13.4261 22.2654 1 15 13 13 39.6363 23.5520 1 16 13 13 152.872 31.335 1 -17 -13 -13 76.7607 24.3893 1 17 13 13 69.9521 26.1865 1 12 -14 -13 61.5955 25.3581 1 11 -14 -13 17.5812 15.5230 1 10 -14 -13 14.5686 20.8536 1 9 -14 -13 122.989 23.851 4 9 -14 -13 172.901 29.123 1 8 -14 -13 39.0357 17.5836 4 8 -14 -13 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466.392 32.772 1 -4 7 -14 451.959 35.847 3 4 -7 14 477.612 32.205 1 4 -7 14 472.892 37.296 5 -5 7 -14 253.340 30.720 2 -5 7 -14 186.100 20.325 1 5 -7 14 199.525 25.569 5 5 -7 14 185.397 18.952 1 -6 7 -14 299.228 26.160 1 -6 7 -14 316.309 35.351 2 6 -7 14 269.259 30.664 5 6 -7 14 267.382 24.602 1 -7 7 -14 62.5725 13.4297 1 -7 7 -14 87.7524 23.1098 2 7 -7 14 65.0992 19.9314 5 -8 7 -14 254.662 33.808 2 -8 7 -14 257.840 26.303 1 8 -7 14 271.105 26.500 1 8 -7 14 258.618 31.701 5 -9 7 -14 24.1785 14.1205 1 -9 7 -14 -31.620 21.182 2 9 -7 14 9.6745 17.3318 5 9 -7 14 -5.9959 11.7464 1 -10 7 -14 184.828 26.550 1 -10 7 -14 181.525 32.108 2 10 -7 14 193.333 28.645 5 10 -7 14 173.535 22.281 1 -11 7 -14 -17.003 16.980 1 -11 7 -14 14.7845 20.4425 2 11 -7 14 34.2316 15.1574 1 11 -7 14 -18.292 13.729 5 -12 7 -14 11.4497 21.6700 2 12 -7 14 -3.2111 13.6885 1 12 -7 14 -31.683 19.857 5 -13 7 -14 77.9744 19.6773 1 -13 7 -14 92.8047 28.2013 2 13 -7 14 80.2388 20.2537 1 13 -7 14 36.4850 22.4791 5 -14 7 -14 41.5251 21.7476 1 14 -7 14 54.1047 24.5605 5 -15 7 -14 162.870 30.558 1 15 -7 14 167.829 27.899 5 15 -7 14 193.120 28.742 1 -16 7 -14 8.2464 21.3272 1 16 -7 14 -44.242 25.142 5 16 -7 14 11.1105 17.1985 1 16 6 -14 84.5091 26.0552 3 15 6 -14 51.2286 24.3727 3 13 6 -14 331.646 38.559 3 12 6 -14 110.452 25.691 3 11 6 -14 147.904 25.693 3 10 6 -14 -14.692 17.510 3 9 6 -14 213.177 29.208 3 7 6 -14 244.889 30.441 3 -7 -6 14 222.746 18.246 5 6 6 -14 53.2821 18.2859 3 -6 -6 14 47.7482 8.8593 5 5 6 -14 45.2379 14.9597 3 5 6 -14 63.3859 17.6487 2 4 6 -14 479.070 44.413 2 4 6 -14 500.561 41.393 3 -4 -6 14 445.023 32.127 5 3 6 -14 462.344 43.327 2 3 6 -14 465.064 39.202 3 -3 -6 14 507.530 34.090 5 2 6 -14 416.628 38.596 2 2 6 -14 362.853 33.648 3 -2 -6 14 395.632 29.788 5 1 6 -14 178.408 22.009 3 1 6 -14 143.890 23.267 2 -1 -6 14 196.098 19.628 5 0 6 -14 134.060 20.906 3 0 6 -14 187.616 26.566 2 0 -6 14 132.238 18.304 5 -1 6 -14 326.934 22.707 1 -1 6 -14 360.410 31.890 3 -1 6 -14 397.404 38.293 2 1 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90.0341 23.5766 2 -7 5 -14 84.9607 15.2867 1 7 -5 14 63.2811 19.0376 5 7 -5 14 83.4123 14.1383 1 -8 5 -14 92.7702 24.2933 2 -8 5 -14 73.4255 15.2799 1 8 -5 14 62.7526 18.9750 5 8 -5 14 100.582 15.725 1 -9 5 -14 4.2896 16.7265 2 9 -5 14 11.3065 15.6720 5 -10 5 -14 278.226 37.310 2 -10 5 -14 294.095 29.732 1 10 -5 14 285.990 28.126 1 10 -5 14 269.683 31.505 5 -11 5 -14 116.419 20.703 1 11 -5 14 76.7974 16.6344 1 11 -5 14 66.1793 21.8425 5 -12 5 -14 -33.098 17.519 1 12 -5 14 0.00503 9.36853 1 12 -5 14 30.4072 18.8780 5 -13 5 -14 290.538 33.606 1 13 -5 14 295.242 35.554 5 13 -5 14 275.384 31.102 1 -14 5 -14 25.2185 15.1279 1 14 -5 14 20.8603 20.4634 5 14 -5 14 8.3000 15.8968 1 -15 5 -14 155.529 28.283 1 15 -5 14 94.9771 25.8555 5 15 -5 14 147.235 24.843 1 -16 5 -14 -32.550 20.013 1 16 -5 14 -15.578 20.868 5 16 -5 14 -14.752 18.497 1 -17 5 -14 149.935 30.148 1 17 -5 14 126.351 26.022 1 17 -5 14 167.675 30.577 5 15 4 -14 24.2399 20.3265 3 14 4 -14 20.4233 20.2706 3 13 4 -14 80.4368 23.5194 3 12 4 -14 52.9676 21.1908 3 11 4 -14 185.170 28.577 3 10 4 -14 76.7637 9.1003 1 9 4 -14 84.6094 21.5060 3 8 4 -14 466.206 40.945 3 -8 -4 14 378.348 27.086 5 7 4 -14 574.032 45.584 3 7 4 -14 528.328 44.253 4 -7 -4 14 451.634 32.512 5 6 4 -14 230.708 28.097 4 6 4 -14 257.957 29.559 3 -6 -4 14 239.725 20.065 5 5 4 -14 -1.7636 11.3556 3 5 4 -14 2.5549 11.7883 4 -5 -4 14 1.32291 7.04792 5 4 4 -14 411.841 36.867 4 4 4 -14 406.235 39.659 2 4 4 -14 400.793 36.621 3 -4 -4 14 408.896 29.661 5 3 4 -14 42.0639 15.7488 4 3 4 -14 30.7631 17.5262 2 3 4 -14 50.2448 16.8378 3 -3 -4 14 26.7176 8.9970 5 2 4 -14 493.708 41.668 4 2 4 -14 494.906 44.012 2 2 4 -14 514.616 41.273 3 -2 -4 14 534.512 36.191 5 1 4 -14 361.849 32.642 4 1 4 -14 362.165 36.553 2 1 4 -14 377.730 33.345 3 -1 -4 14 389.037 29.332 5 0 4 -14 183.265 21.699 4 0 4 -14 168.236 21.327 3 0 4 -14 188.406 26.633 2 0 -4 14 218.711 20.448 5 -1 4 -14 838.401 47.543 1 -1 4 -14 828.272 59.840 4 -1 4 -14 846.602 47.689 1 -1 4 -14 979.164 60.168 3 -1 4 -14 990.384 66.772 2 1 -4 14 850.693 55.165 5 -2 4 -14 195.821 23.200 4 -2 4 -14 241.040 29.544 2 -2 4 -14 166.638 21.615 3 2 -4 14 176.695 19.962 5 2 -4 14 188.018 14.153 1 -3 4 -14 600.531 48.513 2 -3 4 -14 559.245 42.771 4 -3 4 -14 491.675 33.321 1 -3 4 -14 555.837 34.156 1 3 -4 14 497.830 33.145 1 3 -4 14 602.427 41.000 5 -4 4 -14 41.1242 14.1484 4 -4 4 -14 44.0016 19.6188 2 -4 4 -14 35.3799 8.8210 1 4 -4 14 24.8023 7.5844 1 4 -4 14 32.0445 19.6296 5 -5 4 -14 614.640 43.665 4 -5 4 -14 559.472 47.879 2 -5 4 -14 557.596 37.083 1 5 -4 14 526.142 36.092 1 5 -4 14 536.198 41.800 5 -6 4 -14 403.972 32.868 4 -6 4 -14 385.940 29.160 1 -6 4 -14 398.824 39.713 2 6 -4 14 312.577 31.920 5 6 -4 14 357.451 28.023 1 -7 4 -14 145.233 25.672 2 -7 4 -14 108.357 16.255 1 7 -4 14 130.776 19.462 5 7 -4 14 113.788 14.791 1 -8 4 -14 34.6492 11.3504 1 8 -4 14 12.0312 9.9649 1 8 -4 14 6.7062 15.5491 5 -9 4 -14 120.501 18.049 1 -9 4 -14 91.7095 21.6667 2 9 -4 14 85.4380 15.8577 1 9 -4 14 52.5709 17.5853 5 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31.2016 9.9011 1 5 -7 19 -1.5222 16.1059 5 -6 7 -19 178.775 28.518 2 -6 7 -19 134.954 17.787 1 6 -7 19 142.905 22.900 5 -7 7 -19 23.1398 21.3919 2 -7 7 -19 4.3011 10.6799 1 7 -7 19 -7.4245 17.6154 5 -8 7 -19 23.3012 22.1766 2 -8 7 -19 11.0574 11.9891 1 8 -7 19 6.4413 18.8563 5 -9 7 -19 319.515 43.204 2 -9 7 -19 240.012 27.615 1 9 -7 19 264.831 34.433 5 -10 7 -19 22.7841 24.9571 2 -10 7 -19 42.6624 16.7911 1 10 -7 19 63.5543 22.5429 5 -11 7 -19 145.693 33.074 2 11 -7 19 107.533 27.095 5 -12 7 -19 20.7518 17.2806 1 -12 7 -19 7.3036 22.6978 2 12 -7 19 -2.2269 17.6193 5 -13 7 -19 105.476 24.106 1 -13 7 -19 138.330 36.178 2 12 6 -19 55.3733 23.2464 3 11 6 -19 43.2076 23.3260 3 10 6 -19 189.381 33.298 3 8 6 -19 331.052 40.918 3 7 6 -19 12.2265 20.2684 3 6 6 -19 390.420 42.367 3 5 6 -19 164.595 26.186 3 -5 -6 19 177.496 20.204 5 4 6 -19 205.450 31.721 3 4 6 -19 156.417 28.752 2 -4 -6 19 232.720 23.071 5 3 6 -19 19.6287 18.8146 3 3 6 -19 -6.6712 19.1035 2 -3 -6 19 35.6091 12.5815 5 2 6 -19 121.074 27.537 2 2 6 -19 170.454 24.579 3 -2 -6 19 146.203 20.255 5 1 6 -19 115.930 26.358 2 1 6 -19 109.981 21.305 3 -1 -6 19 126.082 19.583 5 0 6 -19 9.6021 18.1255 3 0 6 -19 -11.937 19.219 2 0 -6 19 -12.097 10.972 5 -1 6 -19 116.152 23.763 2 1 -6 19 115.099 20.651 5 -2 6 -19 55.3589 23.5297 2 2 -6 19 67.5658 15.5676 5 -3 6 -19 131.453 12.504 1 -3 6 -19 180.001 30.695 2 3 -6 19 106.746 21.228 5 -4 6 -19 59.3305 24.2186 2 -4 6 -19 79.8145 11.2530 1 4 -6 19 77.1830 19.4899 5 -5 6 -19 128.250 15.208 1 5 -6 19 139.714 24.331 5 -6 6 -19 5.4343 21.2514 2 6 -6 19 11.9737 12.8065 5 -7 6 -19 102.699 17.003 1 -7 6 -19 124.125 29.139 2 7 -6 19 137.484 22.575 5 -8 6 -19 265.750 39.837 2 -8 6 -19 278.060 26.825 1 8 -6 19 239.503 32.006 5 -9 6 -19 20.7273 13.7038 1 -9 6 -19 8.3542 22.1335 2 9 -6 19 4.1450 13.9508 5 -10 6 -19 250.591 40.357 2 -10 6 -19 238.095 28.153 1 10 -6 19 256.936 31.746 5 -11 6 -19 -6.8864 15.7740 1 -11 6 -19 -1.6914 21.8912 2 11 -6 19 -1.5720 18.7866 5 -12 6 -19 72.3142 20.8356 1 -13 6 -19 74.2074 32.0406 2 -13 6 -19 51.1533 20.4275 1 13 -6 19 82.7731 25.7256 5 -14 6 -19 71.8594 23.5624 1 14 -6 19 95.3527 27.9011 5 13 5 -19 172.885 33.624 3 11 5 -19 92.9127 27.1030 3 10 5 -19 99.8039 27.3694 3 9 5 -19 290.410 37.812 3 8 5 -19 5.0164 20.2227 3 7 5 -19 312.739 38.610 3 6 5 -19 25.3639 19.0716 3 -6 -5 19 21.1943 9.9331 5 5 5 -19 292.930 34.880 3 -5 -5 19 232.094 23.784 5 4 5 -19 68.6591 23.0535 4 4 5 -19 64.8244 25.2358 2 4 5 -19 74.4854 22.5611 3 -4 -5 19 82.4344 14.6986 5 3 5 -19 64.3195 22.2867 3 3 5 -19 44.8466 19.7877 4 3 5 -19 38.8226 21.8974 2 -3 -5 19 61.7985 14.6844 5 2 5 -19 14.1601 12.8887 4 2 5 -19 64.3428 20.9154 3 -2 -5 19 38.4334 13.0529 5 1 5 -19 50.9039 20.5116 4 1 5 -19 41.3629 19.4033 3 1 5 -19 15.9345 18.9244 2 -1 -5 19 39.7920 13.1633 5 0 5 -19 83.1165 24.3375 2 0 5 -19 66.3526 21.3623 4 0 -5 19 102.417 18.582 5 -1 5 -19 -9.7693 19.5633 2 -1 5 -19 21.7711 16.2680 4 1 -5 19 10.9215 10.9386 5 -2 5 -19 160.938 30.015 2 -2 5 -19 176.234 24.245 4 2 -5 19 166.779 23.539 5 -3 5 -19 8.1306 16.8940 4 -3 5 -19 44.3174 7.0948 1 3 -5 19 30.9174 16.4433 5 -4 5 -19 184.078 27.906 2 -4 5 -19 136.299 14.109 1 -4 5 -19 149.391 24.682 4 4 -5 19 179.862 24.414 5 -5 5 -19 195.140 29.609 2 5 -5 19 203.257 25.293 5 -6 5 -19 35.8802 17.9076 2 -6 5 -19 39.4311 11.1518 1 6 -5 19 36.5395 14.7855 5 -7 5 -19 167.132 20.426 1 -7 5 -19 231.166 35.879 2 7 -5 19 194.819 25.991 5 -8 5 -19 42.3264 24.9752 2 8 -5 19 48.6436 17.3628 5 -9 5 -19 336.245 43.530 2 -9 5 -19 310.882 29.609 1 9 -5 19 284.039 35.227 5 -10 5 -19 3.9315 16.7994 2 -10 5 -19 0.5134 13.4251 1 10 -5 19 -35.160 22.468 5 -11 5 -19 140.359 23.510 1 -11 5 -19 219.304 38.042 2 11 -5 19 192.221 31.700 5 -12 5 -19 17.6702 13.8478 1 -12 5 -19 -43.767 27.926 2 12 -5 19 38.1737 22.8427 5 -13 5 -19 61.1102 25.3923 2 -13 5 -19 71.3960 18.0378 1 13 -5 19 52.4791 19.0087 5 -14 5 -19 2.4013 16.9762 1 -14 5 -19 -58.941 30.769 2 14 -5 19 42.7520 23.6674 5 13 4 -19 21.1365 22.7029 3 12 4 -19 63.1124 24.3596 3 11 4 -19 97.6996 26.8231 3 10 4 -19 288.673 38.414 3 9 4 -19 86.2718 24.7770 3 8 4 -19 282.833 36.918 3 7 4 -19 13.3330 19.5275 3 7 4 -19 16.7026 19.0664 4 6 4 -19 165.912 26.446 4 6 4 -19 182.424 26.980 3 -6 -4 19 175.685 20.060 5 5 4 -19 152.360 27.576 3 5 4 -19 157.079 27.980 4 -5 -4 19 176.474 20.218 5 4 4 -19 31.2322 20.3408 4 4 4 -19 17.5804 19.6160 2 -4 -4 19 11.4446 10.2706 5 3 4 -19 104.679 24.885 2 3 4 -19 95.6285 22.8803 4 3 4 -19 97.2823 23.3000 3 -3 -4 19 125.105 18.283 5 2 4 -19 52.3433 18.0890 4 2 4 -19 9.2739 19.3625 2 2 4 -19 7.2484 17.8485 3 -2 -4 19 44.8391 13.9257 5 1 4 -19 195.028 32.345 2 1 4 -19 212.347 29.767 4 -1 -4 19 234.388 24.930 5 0 4 -19 -8.5340 18.4097 2 0 4 -19 1.4239 15.1577 4 0 -4 19 20.1622 12.5502 5 -1 4 -19 217.461 29.266 4 -1 4 -19 229.911 33.782 2 1 -4 19 234.942 26.575 5 -2 4 -19 35.5644 20.6210 2 -2 4 -19 16.5161 15.5438 4 2 -4 19 16.6301 14.3385 5 -3 4 -19 200.029 29.101 2 -3 4 -19 193.897 15.235 1 -3 4 -19 224.442 26.622 4 3 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33.848 3 10 3 -19 99.2314 23.0882 3 9 3 -19 220.555 33.207 3 9 3 -19 190.325 29.968 4 8 3 -19 80.1247 22.4604 3 8 3 -19 60.2771 21.4118 4 7 3 -19 131.591 23.736 3 7 3 -19 131.348 25.366 4 -7 -3 19 108.185 16.282 5 6 3 -19 75.1555 23.2909 3 6 3 -19 77.9524 19.7197 4 -6 -3 19 59.7686 13.4457 5 5 3 -19 69.8295 22.1754 3 -5 -3 19 68.2482 13.9532 5 4 3 -19 118.262 26.792 2 4 3 -19 183.427 28.041 4 4 3 -19 152.179 26.876 3 -4 -3 19 147.475 19.246 5 3 3 -19 11.5564 18.2724 2 3 3 -19 25.4041 15.3983 3 3 3 -19 -1.5076 14.0504 4 -3 -3 19 44.9915 14.1648 5 2 3 -19 485.893 49.728 2 2 3 -19 534.435 46.714 4 -2 -3 19 472.365 38.375 5 1 3 -19 -3.5620 18.6481 2 1 3 -19 -15.322 16.801 4 -1 -3 19 2.1973 12.0064 5 0 3 -19 152.729 24.268 4 0 3 -19 123.615 26.853 2 0 -3 19 128.889 20.455 5 -1 3 -19 -26.944 17.267 4 -1 3 -19 4.8678 17.8719 2 1 -3 19 3.76215 9.91797 5 -2 3 -19 99.8347 21.1675 4 -2 3 -19 84.1908 23.0930 2 2 -3 19 99.0096 18.9925 5 -3 3 -19 227.225 29.016 4 -3 3 -19 242.686 33.703 2 -3 3 -19 191.682 15.767 1 3 -3 19 272.710 29.142 5 -4 3 -19 264.664 29.849 4 -4 3 -19 256.130 36.258 2 -4 3 -19 281.759 21.194 1 4 -3 19 307.530 32.023 5 -5 3 -19 333.713 33.732 4 -5 3 -19 250.524 22.372 1 -5 3 -19 256.328 36.222 2 5 -3 19 323.832 32.235 5 -6 3 -19 16.1259 14.8871 4 6 -3 19 28.3004 14.9319 5 -7 3 -19 411.365 46.536 2 -7 3 -19 424.161 37.450 4 -7 3 -19 352.377 29.724 1 7 -3 19 338.218 35.148 5 -8 3 -19 6.7202 13.8674 4 -8 3 -19 11.4755 21.4790 2 -8 3 -19 2.1841 10.7703 1 8 -3 19 4.1026 17.5272 5 -9 3 -19 88.8033 17.6419 1 -9 3 -19 106.907 19.362 4 -9 3 -19 136.348 30.251 2 9 -3 19 86.3878 22.7362 5 -10 3 -19 4.9014 12.4771 1 10 -3 19 -8.5300 17.5237 5 -11 3 -19 118.893 32.126 2 -11 3 -19 103.493 20.180 1 11 -3 19 149.155 27.262 5 -12 3 -19 257.870 43.399 2 -12 3 -19 215.664 29.030 1 12 -3 19 212.520 31.985 5 -13 3 -19 59.1594 20.2681 1 -13 3 -19 69.9452 31.5534 2 13 -3 19 60.8316 19.6019 5 -14 3 -19 50.2283 24.9159 2 -14 3 -19 38.5572 15.9946 1 14 -3 19 49.3759 23.8411 5 -15 3 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-0.6939 15.5489 4 2 0 -19 62.1515 22.2781 2 2 0 -19 29.8672 18.2108 4 1 0 -19 425.065 39.658 4 1 0 -19 374.293 39.492 2 0 0 -19 337.885 39.326 2 0 0 -19 449.800 40.792 4 -1 0 -19 228.622 32.175 2 -1 0 -19 244.612 29.959 4 -2 0 -19 442.125 38.933 4 -2 0 -19 386.781 41.601 2 -2 0 -19 309.152 22.622 1 2 0 19 381.882 36.420 5 -3 0 -19 105.269 20.875 4 -3 0 -19 92.2311 10.9833 1 -3 0 -19 96.7289 22.4987 2 -4 0 -19 464.812 41.874 4 -4 0 -19 427.640 29.443 1 -4 0 -19 381.269 44.159 2 4 0 19 492.680 40.773 5 -5 0 -19 9.2138 14.6561 4 -5 0 -19 0.11453 6.92650 1 -5 0 -19 9.2277 14.0741 2 5 0 19 0.7880 15.5094 5 -6 0 -19 61.8908 11.7437 1 -6 0 -19 84.4977 18.8904 4 6 0 19 70.1605 20.0315 5 -7 0 -19 34.7520 16.2436 4 -7 0 -19 27.5115 11.1570 1 -7 0 -19 54.8831 22.9184 2 7 0 19 67.6703 19.7845 5 -8 0 -19 146.118 27.472 2 -8 0 -19 208.654 25.473 4 -8 0 -19 156.283 19.867 1 8 0 19 183.001 26.535 5 -9 0 -19 177.015 22.397 1 -9 0 -19 187.644 24.125 4 9 0 19 151.998 24.970 5 -10 0 -19 38.1667 13.1499 4 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5.0932 17.4556 2 3 10 -23 -29.806 21.211 3 2 10 -23 127.309 30.481 3 2 10 -23 129.173 29.056 2 1 10 -23 -15.610 21.473 3 1 10 -23 0.5016 19.6830 2 0 -10 23 154.585 25.526 5 1 -10 23 14.2420 16.6450 5 -2 10 -23 75.7361 29.6045 2 2 -10 23 112.294 22.906 5 -3 10 -23 4.9794 21.1845 2 3 -10 23 32.0975 19.0914 5 -4 10 -23 179.701 35.267 2 4 -10 23 120.103 27.067 5 5 -10 23 42.3469 21.4587 5 6 -10 23 52.5719 23.1976 5 6 9 -23 66.4333 26.7060 3 4 9 -23 -3.9295 16.2862 3 4 9 -23 9.6973 24.7421 2 3 9 -23 116.026 33.210 2 3 9 -23 84.1864 27.6079 3 2 9 -23 32.5784 23.3020 3 2 9 -23 2.8553 22.4590 2 -2 -9 23 -4.2669 13.3868 5 1 9 -23 58.3396 26.5570 2 -1 -9 23 50.1067 18.3570 5 0 9 -23 11.4776 23.4715 2 0 -9 23 7.9118 15.4063 5 -1 9 -23 275.380 39.430 2 1 -9 23 246.251 31.895 5 -2 9 -23 77.2551 28.2824 2 2 -9 23 40.5493 18.4529 5 -3 9 -23 63.6496 28.1587 2 3 -9 23 120.934 24.473 5 4 -9 23 4.6596 17.4658 5 -5 9 -23 37.6744 22.6208 2 5 -9 23 127.907 23.425 5 6 -9 23 -2.6639 20.6761 5 -7 9 -23 55.4460 27.4878 2 7 -9 23 7.3643 19.7153 5 6 8 -23 28.7556 23.8900 3 5 8 -23 22.3311 24.2545 3 4 8 -23 102.374 31.375 2 3 8 -23 21.4594 22.1186 3 3 8 -23 31.2965 25.1799 2 2 8 -23 50.6541 26.5707 2 -2 -8 23 23.9972 16.0998 5 0 8 -23 257.189 40.790 2 0 -8 23 202.956 28.256 5 -1 8 -23 71.2278 29.5733 2 1 -8 23 59.5360 19.9995 5 -2 8 -23 45.4798 25.6468 2 2 -8 23 31.7362 18.8495 5 3 -8 23 18.2012 17.5268 5 -4 8 -23 74.8850 29.0969 2 4 -8 23 75.9447 22.6143 5 -5 8 -23 178.534 35.942 2 5 -8 23 186.288 29.626 5 -6 8 -23 -25.170 19.088 2 6 -8 23 0.4806 18.1446 5 -7 8 -23 27.2749 23.6430 2 7 -8 23 -20.986 19.960 5 -8 8 -23 -38.607 29.427 2 8 -8 23 0.1589 21.0300 5 7 7 -23 -17.771 24.405 3 6 7 -23 29.4533 22.8918 3 5 7 -23 20.9786 17.8036 3 4 7 -23 -17.951 24.719 3 4 7 -23 -37.665 27.832 2 3 7 -23 134.929 35.055 2 -3 -7 23 165.193 23.090 5 2 7 -23 44.4695 26.4335 2 -2 -7 23 15.7937 13.4995 5 1 7 -23 -39.508 26.184 2 -1 -7 23 31.5011 14.6338 5 0 7 -23 -6.3229 23.4122 2 0 -7 23 27.3073 15.3087 5 -1 7 -23 221.305 39.809 2 1 -7 23 238.819 30.254 5 -2 7 -23 72.8906 30.8151 2 2 -7 23 107.666 22.770 5 -3 7 -23 -44.241 27.798 2 3 -7 23 -3.7390 15.1603 5 -4 7 -23 189.512 35.315 2 4 -7 23 213.659 31.499 5 -5 7 -23 -2.3256 20.8380 2 5 -7 23 2.9589 17.9539 5 6 -7 23 181.911 27.679 5 -7 7 -23 -20.687 21.019 2 -8 7 -23 -8.8611 23.4752 2 8 -7 23 6.5273 20.5810 5 9 -7 23 54.2675 25.1627 5 8 6 -23 -3.0317 22.0423 3 7 6 -23 -23.341 25.713 3 4 6 -23 182.454 38.118 2 3 6 -23 2.4730 24.8845 2 -3 -6 23 35.3961 15.6289 5 2 6 -23 53.5058 27.5729 2 1 6 -23 46.5426 27.1450 2 -1 -6 23 57.6305 17.7977 5 0 6 -23 91.3995 29.1880 2 0 -6 23 99.0894 20.9114 5 -1 6 -23 133.899 33.560 2 1 -6 23 138.006 24.072 5 -2 6 -23 57.5869 27.6702 2 2 -6 23 85.1693 21.2005 5 3 -6 23 140.968 24.791 5 -4 6 -23 14.9264 24.6121 2 4 -6 23 21.5080 19.1815 5 -5 6 -23 303.893 42.063 2 5 -6 23 283.256 36.151 5 6 -6 23 22.1114 19.2499 5 -7 6 -23 113.690 31.483 2 7 -6 23 70.9646 19.5308 5 -8 6 -23 -30.522 25.634 2 8 -6 23 -48.595 21.928 5 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-2 26 207.331 31.715 5 -5 2 -26 27.2919 21.7633 4 -5 2 -26 -21.248 27.084 2 5 -2 26 45.6514 23.6005 5 -6 2 -26 48.2180 26.6126 2 -6 2 -26 19.2864 19.5281 4 6 -2 26 47.8425 19.8764 5 -7 2 -26 87.4560 23.4152 4 -7 2 -26 -5.7602 24.2772 2 -8 2 -26 89.7854 25.1798 4 5 1 -26 88.2801 27.3911 4 4 1 -26 101.874 28.909 4 -4 -1 26 112.830 21.852 5 3 1 -26 45.1732 19.5624 4 -3 -1 26 73.1995 19.4700 5 2 1 -26 29.5618 26.8251 2 2 1 -26 49.8346 25.5519 4 -2 -1 26 -4.8909 17.4177 5 1 1 -26 196.482 37.639 2 1 1 -26 169.584 32.932 4 -1 -1 26 215.660 31.723 5 0 1 -26 39.2552 25.8674 2 0 1 -26 134.492 29.052 4 0 -1 26 88.6156 22.8928 5 -1 1 -26 120.923 26.909 4 -1 1 -26 127.004 30.273 2 1 -1 26 185.724 30.702 5 -2 1 -26 35.6324 21.4009 4 -2 1 -26 74.1020 27.3393 2 2 -1 26 13.3211 20.1920 5 -3 1 -26 105.494 27.051 4 -3 1 -26 101.997 32.627 2 3 -1 26 121.566 23.582 5 -4 1 -26 20.0826 21.8122 4 -4 1 -26 -17.262 27.597 2 4 -1 26 43.3798 22.4938 5 -5 1 -26 221.503 32.835 4 -5 1 -26 142.036 37.462 2 5 -1 26 236.328 34.891 5 -6 1 -26 16.5489 25.1508 2 6 -1 26 46.1439 23.0944 5 -7 1 -26 15.3587 17.1785 4 -7 1 -26 -52.195 28.684 2 7 -1 26 31.1953 23.3447 5 -8 1 -26 82.7288 32.9086 2 8 -1 26 70.1071 27.8265 5 4 0 -26 15.5271 16.8134 4 3 0 -26 26.8671 22.9669 4 -3 0 26 33.9676 16.1313 5 2 0 -26 235.081 35.207 4 2 0 -26 233.690 40.528 2 -2 0 26 304.116 35.565 5 1 0 -26 31.1565 24.1204 4 1 0 -26 19.1983 26.1874 2 -1 0 26 5.9996 18.8910 5 0 0 -26 236.922 36.430 4 0 0 26 239.519 33.824 5 -1 0 -26 14.2205 25.8866 2 -1 0 -26 66.9240 24.9730 4 -2 0 -26 168.046 36.855 2 -2 0 -26 192.163 33.079 4 2 0 26 244.419 34.336 5 -3 0 -26 15.6288 21.1663 4 -3 0 -26 24.5406 27.0079 2 -4 0 -26 75.4509 30.8101 2 -4 0 -26 131.800 28.924 4 4 0 26 93.2523 22.1715 5 -5 0 -26 9.4696 24.2736 2 -5 0 -26 33.5314 18.2053 4 5 0 26 50.3072 21.9526 5 -6 0 -26 11.7621 21.2136 4 -6 0 -26 -13.613 21.135 2 6 0 26 -18.562 20.162 5 -7 0 -26 61.1792 29.6059 2 7 0 26 115.955 27.267 5 -8 0 -26 -26.533 27.243 2 -8 0 -26 -22.512 19.742 4 8 0 26 46.2360 22.4277 5 -5 1 26 46.9367 19.5602 5 -4 1 26 101.542 22.801 5 3 -1 -26 201.643 31.838 4 -3 1 26 202.676 29.367 5 2 -1 -26 13.3078 20.8285 4 2 -1 -26 -42.951 25.639 2 -2 1 26 -7.2594 19.2445 5 1 -1 -26 168.461 30.948 4 -1 1 26 142.798 27.717 5 0 -1 -26 43.3169 22.6987 2 0 -1 -26 70.6736 23.9464 4 -1 -1 -26 272.426 37.937 4 -1 -1 -26 190.279 38.749 2 1 1 26 240.933 31.822 5 -2 -1 -26 1.4280 23.2258 2 -2 -1 -26 2.6823 19.6686 4 2 1 26 31.4372 22.9106 5 -3 -1 -26 88.3608 26.5026 4 3 1 26 137.391 28.969 5 -4 -1 -26 0.3346 13.9862 4 -4 -1 -26 -14.844 24.679 2 -5 -1 -26 19.4104 20.0384 4 -5 -1 -26 -8.0877 24.6222 2 -6 -1 -26 257.736 41.378 2 -6 -1 -26 248.639 37.038 4 6 1 26 288.367 38.794 5 -7 -1 -26 42.1604 28.9187 2 -7 -1 -26 -2.9519 19.4552 4 7 1 26 10.7202 21.2633 5 -8 -1 -26 173.802 29.523 4 -8 -1 -26 152.235 35.897 2 -9 -1 -26 15.9975 18.8812 4 -9 -1 -26 -22.209 28.532 2 4 -2 -26 82.8068 22.8402 4 2 -2 -26 153.472 28.221 4 2 -2 -26 169.188 31.836 2 1 -2 -26 -15.977 24.911 2 1 -2 -26 30.1728 23.5861 4 -1 2 26 33.7392 20.1835 5 0 -2 -26 144.157 33.192 2 0 -2 -26 143.784 31.059 4 0 2 26 166.195 31.262 5 -1 -2 -26 29.8160 22.1814 4 1 2 26 4.5671 21.3342 5 -2 -2 -26 113.288 30.004 2 -2 -2 -26 144.033 27.558 4 2 2 26 170.173 28.959 5 -3 -2 -26 25.9513 22.9739 2 -3 -2 -26 3.1559 18.0573 4 3 2 26 11.2709 18.5947 5 -4 -2 -26 87.0037 28.2075 2 -4 -2 -26 111.161 27.229 4 -5 -2 -26 165.689 37.422 2 -5 -2 -26 275.643 36.947 4 5 2 26 227.655 35.789 5 -6 -2 -26 -4.9824 25.7436 2 -6 -2 -26 -6.3129 18.8089 4 6 2 26 15.7258 23.9541 5 -7 -2 -26 195.167 38.738 2 -7 -2 -26 238.235 35.843 4 7 2 26 261.305 37.036 5 -8 -2 -26 43.2028 21.3533 2 -8 -2 -26 -6.7152 17.0437 4 8 2 26 -20.567 18.774 5 -9 -2 -26 148.067 28.338 4 3 -3 -26 292.454 37.669 4 1 -3 -26 71.4161 22.6998 4 0 -3 -26 -27.874 21.560 4 0 -3 -26 -36.242 25.080 2 -1 -3 -26 134.127 27.890 2 -2 -3 -26 62.4245 28.0484 2 -2 -3 -26 106.219 26.666 4 2 3 26 103.916 28.465 5 -3 -3 -26 79.6357 25.2537 4 -3 -3 -26 95.6499 29.6238 2 3 3 26 61.9339 26.9828 5 -4 -3 -26 47.2185 22.2938 4 -5 -3 -26 26.9151 20.1662 4 -5 -3 -26 13.1872 24.8512 2 5 3 26 -24.108 23.939 5 -6 -3 -26 504.078 50.254 4 -6 -3 -26 380.204 51.939 2 6 3 26 493.141 50.861 5 -7 -3 -26 16.1257 22.4934 2 -7 -3 -26 -25.971 22.652 4 7 3 26 -43.413 24.809 5 -8 -3 -26 24.8381 25.5850 2 -8 -3 -26 22.8841 20.9173 4 -9 -3 -26 14.6200 25.4907 2 -9 -3 -26 -21.326 12.588 1 2 -4 -26 143.789 26.868 4 1 -4 -26 -35.145 21.910 2 -1 -4 -26 71.4725 26.3945 2 -1 -4 -26 49.1575 19.7953 4 -2 -4 -26 69.8423 22.5363 4 -2 -4 -26 50.5806 25.6677 2 -3 -4 -26 58.8741 21.6710 4 -3 -4 -26 13.8047 23.8116 2 -4 -4 -26 96.5299 29.3069 2 -4 -4 -26 81.2976 21.0668 4 -5 -4 -26 165.997 30.811 4 -5 -4 -26 133.750 31.669 2 5 4 26 208.784 36.112 5 -6 -4 -26 54.7539 25.4683 2 -6 -4 -26 87.4358 25.8052 4 6 4 26 105.433 28.326 5 -7 -4 -26 106.511 24.880 4 -7 -4 -26 108.986 30.383 2 7 4 26 97.5081 25.2662 5 -8 -4 -26 22.1714 24.8228 2 -8 -4 -26 4.8142 12.0437 1 -8 -4 -26 -0.1273 19.0450 4 8 4 26 -39.745 23.075 5 -9 -4 -26 95.7205 25.9048 4 -9 -4 -26 75.8266 17.2373 1 -9 -4 -26 74.3318 25.4670 2 0 -5 -26 -10.857 16.424 2 -1 -5 -26 -19.403 20.850 2 -2 -5 -26 201.748 35.118 2 -3 -5 -26 -24.239 19.942 4 -3 -5 -26 -17.795 20.401 2 -4 -5 -26 174.166 31.722 4 -4 -5 -26 137.569 30.173 2 -5 -5 -26 -18.024 23.423 2 5 5 26 -30.218 26.557 5 -6 -5 -26 102.368 29.547 2 -6 -5 -26 87.3809 24.2244 4 6 5 26 58.6613 28.3431 5 -7 -5 -26 -24.740 23.246 2 -7 -5 -26 46.5595 23.1395 4 -8 -5 -26 66.6951 24.3248 4 -8 -5 -26 77.2979 17.1469 1 8 5 26 86.5373 28.1963 5 -9 -5 -26 26.3199 21.4341 4 -9 -5 -26 48.4590 16.1119 1 -1 -6 -26 224.054 33.140 4 -1 -6 -26 197.349 33.625 2 -2 -6 -26 33.9355 22.9575 2 -2 -6 -26 -20.458 17.002 4 -3 -6 -26 144.297 28.566 2 -4 -6 -26 4.2580 22.2975 2 -5 -6 -26 275.613 36.900 4 -5 -6 -26 297.157 41.703 2 6 6 26 37.0893 22.3279 5 -7 -6 -26 9.1333 12.0842 1 -7 -6 -26 -0.4508 19.4933 4 -7 -6 -26 -15.865 22.766 2 7 6 26 -0.8691 22.1587 5 -8 -6 -26 38.5574 21.4515 4 -8 -6 -26 -15.841 12.613 1 8 6 26 -12.689 25.327 5 -9 -6 -26 89.4008 27.1671 2 -9 -6 -26 79.1605 24.5763 4 -9 -6 -26 46.3862 17.5707 1 2 -7 -26 34.1648 17.4087 4 0 -7 -26 121.370 26.568 4 -6 -7 -26 113.105 19.782 1 -7 -7 -26 -0.5938 12.1754 1 -7 -7 -26 21.5140 20.1882 4 8 7 26 75.5547 30.9946 5 0 -8 -26 25.0321 22.1976 4 -2 -8 -26 26.0470 21.6636 4 -3 -8 -26 1.7224 19.4162 4 -4 -8 -26 14.2574 20.1515 4 -5 -8 -26 217.065 26.596 1 -6 -8 -26 148.730 22.361 1 -7 -8 -26 49.1618 16.8584 1 -8 -8 -26 -0.9347 18.9326 4 1 -9 -26 58.5642 22.7416 4 -2 -9 -26 192.906 31.081 4 -3 -9 -26 1.4218 17.2425 4 -4 -9 -26 68.4440 24.2224 4 -5 -9 -26 99.4002 19.7353 1 -5 -9 -26 118.361 27.861 4 -6 -9 -26 63.0288 17.8533 1 -6 -9 -26 86.1501 25.9160 4 -7 -9 -26 33.4343 16.7203 1 -7 -9 -26 19.1667 22.6128 4 -1 -10 -26 204.633 36.350 4 -2 -10 -26 59.3292 25.2899 4 -4 -10 -26 76.7862 18.5072 1 -5 -10 -26 89.0650 19.7156 1 -6 -10 -26 73.1349 18.8631 1 -6 -10 -26 88.6085 27.2358 4 1 -4 27 4.0269 16.2052 5 1 3 -27 190.027 41.181 2 -1 -3 27 215.578 30.589 5 0 3 -27 -9.5801 26.0530 2 0 3 -27 18.7760 22.1629 4 0 -3 27 -8.8764 18.6012 5 -1 3 -27 29.6486 22.0760 4 -1 3 -27 -27.376 26.108 2 1 -3 27 1.2509 14.0272 5 -2 3 -27 47.9523 27.3618 2 -2 3 -27 40.7880 22.4429 4 3 -3 27 -0.3671 15.5844 5 -4 3 -27 21.1543 22.1044 4 -4 3 -27 18.5962 27.7643 2 4 -3 27 36.5531 23.6434 5 1 2 -27 57.4041 27.5800 4 1 2 -27 35.6738 29.3961 2 -1 -2 27 54.8418 21.5852 5 0 2 -27 61.0447 24.7605 4 0 -2 27 89.5763 24.3842 5 -1 2 -27 23.0508 26.3016 2 -1 2 -27 11.2107 20.6533 4 1 -2 27 19.5568 18.4640 5 -2 2 -27 -6.8537 24.4533 2 -2 2 -27 53.6568 23.9436 4 2 -2 27 11.5055 20.4901 5 -3 2 -27 179.779 32.468 4 -3 2 -27 108.425 28.535 2 -4 2 -27 -5.4614 18.1531 4 -4 2 -27 -53.691 30.254 2 4 -2 27 -10.047 15.456 5 -5 2 -27 80.0199 32.6866 2 -5 2 -27 150.570 30.376 4 5 -2 27 99.1456 28.5467 5 2 1 -27 52.1858 24.5065 2 -2 -1 27 35.7302 18.9486 5 1 1 -27 35.7947 25.0856 2 1 1 -27 18.6341 16.8649 4 0 1 -27 68.8878 27.1244 2 0 1 -27 37.3948 22.6026 4 0 -1 27 21.7597 18.4173 5 1 -1 27 57.3195 21.9385 5 -2 1 -27 123.063 28.516 2 -2 1 -27 123.199 29.214 4 2 -1 27 113.827 24.860 5 -3 1 -27 -22.152 24.324 2 -3 1 -27 -5.6481 17.3174 4 3 -1 27 -6.4692 22.1475 5 -4 1 -27 191.338 31.852 4 -4 1 -27 139.481 35.306 2 4 -1 27 138.602 30.191 5 -5 1 -27 -15.259 26.759 2 5 -1 27 26.4187 20.1348 5 -6 1 -27 55.4731 23.5565 2 -6 1 -27 46.3430 18.9796 4 6 -1 27 86.2514 23.2103 5 -3 0 27 24.6181 15.2270 5 2 0 -27 65.0760 26.8851 4 2 0 -27 25.8999 24.7434 2 -2 0 27 78.7452 22.9275 5 1 0 -27 89.6799 31.5122 2 1 0 -27 117.147 28.966 4 -1 0 27 108.337 25.746 5 0 0 -27 16.4575 25.5872 2 0 0 -27 30.6880 23.9566 4 0 0 27 54.0859 19.2154 5 -1 0 -27 57.5216 24.3680 4 -1 0 -27 128.368 33.374 2 1 0 27 98.0501 26.8417 5 -2 0 -27 -9.9733 24.4991 2 -2 0 -27 -8.1565 19.7773 4 2 0 27 2.0585 19.7646 5 -3 0 -27 147.652 34.469 2 3 0 27 157.797 28.477 5 -4 0 -27 5.5117 20.8376 4 -4 0 -27 -13.307 24.171 2 -5 0 -27 127.819 29.142 4 5 0 27 67.7015 26.6521 5 -6 0 -27 51.1941 22.7743 4 -6 0 -27 30.5955 24.4808 2 6 0 27 12.8228 24.0755 5 -3 1 27 91.6712 22.8592 5 2 -1 -27 116.707 30.147 2 -2 1 27 167.295 29.591 5 1 -1 -27 20.8577 24.7642 2 1 -1 -27 31.0516 17.5371 4 -1 1 27 60.3817 22.5773 5 0 -1 -27 119.601 29.922 4 0 1 27 115.989 28.064 5 -1 -1 -27 -6.5725 24.4692 2 1 1 27 36.7398 21.7273 5 -2 -1 -27 72.9267 28.2214 2 -2 -1 -27 69.6105 24.9920 4 2 1 27 90.8147 25.8682 5 -3 -1 -27 48.1839 24.4246 4 -3 -1 -27 -14.110 23.531 2 3 1 27 -16.610 21.673 5 -4 -1 -27 91.1679 26.6300 4 -4 -1 -27 92.0494 29.9488 2 -5 -1 -27 69.3149 24.5887 2 -5 -1 -27 105.905 25.314 4 5 1 27 80.4214 24.2726 5 -6 -1 -27 -29.615 27.641 2 -6 -1 -27 26.9661 22.4797 4 6 1 27 48.8932 24.2523 5 -7 -1 -27 227.312 32.508 4 -7 -1 -27 154.569 37.160 2 -3 2 27 187.240 32.073 5 -2 2 27 40.5117 23.3204 5 1 -2 -27 178.524 35.499 2 -1 2 27 138.099 27.913 5 0 -2 -27 -53.408 27.821 2 0 2 27 -0.8635 22.7278 5 -1 -2 -27 135.739 26.837 4 -1 -2 -27 115.690 32.836 2 1 2 27 146.902 29.119 5 -2 -2 -27 8.4809 15.8902 4 -2 -2 -27 13.0724 22.6443 2 -3 -2 -27 41.1807 18.8446 4 -3 -2 -27 17.6988 22.9260 2 3 2 27 89.5693 27.5336 5 -4 -2 -27 61.7795 27.9753 2 4 2 27 54.5311 25.1387 5 -5 -2 -27 -52.433 29.100 2 -5 -2 -27 -16.302 21.123 4 5 2 27 16.0336 24.1495 5 -6 -2 -27 317.918 41.050 4 6 2 27 320.687 42.664 5 -7 -2 -27 52.9287 26.1743 2 -7 -2 -27 37.1290 23.7208 4 1 -3 -27 -19.065 23.463 2 1 -3 -27 40.9713 19.7141 4 0 -3 -27 72.1411 23.8031 2 0 3 27 94.8432 23.7280 5 -1 -3 -27 11.5482 22.4829 2 1 3 27 96.8232 26.6889 5 -2 -3 -27 235.931 36.877 4 -2 -3 -27 212.558 39.593 2 2 3 27 215.937 37.730 5 -3 -3 -27 76.7407 25.6150 4 -3 -3 -27 60.2987 28.3533 2 3 3 27 52.5147 23.8067 5 -4 -3 -27 30.9552 25.7297 2 -4 -3 -27 -0.9330 20.7216 4 4 3 27 45.8386 19.5802 5 -5 -3 -27 159.075 31.311 4 -5 -3 -27 155.548 34.414 2 5 3 27 114.907 28.458 5 -6 -3 -27 -22.685 20.084 4 -6 -3 -27 4.8296 21.5942 2 6 3 27 -35.122 21.125 5 -7 -3 -27 302.622 41.425 4 -7 -3 -27 255.313 42.651 2 2 -4 -27 18.8241 19.4284 4 0 -4 -27 35.3736 22.7846 2 -1 -4 -27 51.6373 19.3077 4 -1 -4 -27 49.6087 24.4583 2 -2 -4 -27 137.189 28.754 4 -2 -4 -27 117.571 30.780 2 -3 -4 -27 68.4890 22.6923 4 -3 -4 -27 57.7537 26.7319 2 -4 -4 -27 3.6318 22.6315 2 4 4 27 40.2685 26.0899 5 -5 -4 -27 0.4754 24.4189 2 -5 -4 -27 23.8541 20.5891 4 5 4 27 7.1621 24.2768 5 -6 -4 -27 176.189 38.226 2 -6 -4 -27 257.176 38.005 4 6 4 27 302.988 41.957 5 -7 -4 -27 -23.397 26.883 2 -7 -4 -27 16.4037 19.3951 4 0 -5 -27 58.7320 23.6822 2 -1 -5 -27 95.4469 28.0692 2 -2 -5 -27 78.4039 27.1740 2 -3 -5 -27 115.039 27.725 2 -4 -5 -27 22.8409 21.9234 4 -4 -5 -27 18.2216 18.2923 2 4 5 27 39.2985 22.7714 5 -5 -5 -27 130.921 29.169 2 5 5 27 107.857 30.443 5 -6 -5 -27 -5.9774 17.8998 2 -6 -5 -27 -20.529 19.848 4 6 5 27 14.1845 26.2310 5 -2 -6 -27 138.014 26.699 4 -3 -6 -27 3.0521 14.5969 4 -4 -6 -27 137.362 26.962 4 -5 -6 -27 -9.2058 18.4660 4 -1 -7 -27 262.604 37.921 4 -2 -7 -27 -14.793 20.602 4 -3 -8 -27 -3.5085 21.7693 4 0 0 0 0.00 0.00 0 ; loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group U1 U 0.776708(14) 0.277701(13) 0.229688(10) 0.01620(5) Uani 1 1 d . . . K1 K 0.54963(8) 0.22463(7) 0.21778(6) 0.0207(2) Uani 1 1 d . . . S1 S 0.83745(10) 0.32840(10) 0.32958(7) 0.0269(3) Uani 1 1 d . . . Si1 Si 0.66802(10) 0.11856(9) 0.34655(7) 0.0190(3) Uani 1 1 d . . . Si2 Si 0.55832(10) 0.42343(9) 0.23173(7) 0.0189(3) Uani 1 1 d . . . Si3 Si 0.69655(10) 0.19454(9) 0.07498(7) 0.0190(3) Uani 1 1 d . . . Si4 Si 1.01337(10) 0.29058(9) 0.14124(7) 0.0176(3) Uani 1 1 d . . . O1 O 0.7109(3) 0.1769(2) 0.2892(2) 0.0237(8) Uani 1 1 d . . . O2 O 0.7120(3) 0.0267(2) 0.34246(19) 0.0246(8) Uani 1 1 d . . . O3 O 0.6732(3) 0.1373(2) 0.42438(19) 0.0241(8) Uani 1 1 d . . . O4 O 0.5560(3) 0.1287(2) 0.3354(2) 0.0244(8) Uani 1 1 d . . . O21 O 0.6476(3) 0.3609(2) 0.22544(19) 0.0218(8) Uani 1 1 d . . . O22 O 0.5393(3) 0.4622(2) 0.30428(19) 0.0253(9) Uani 1 1 d . . . O23 O 0.4715(3) 0.3746(2) 0.2191(2) 0.0252(9) Uani 1 1 d . . . O24 O 0.5542(3) 0.4971(2) 0.17362(19) 0.0225(8) Uani 1 1 d . . . O41 O 0.7220(2) 0.2260(2) 0.14248(18) 0.0192(8) Uani 1 1 d . . . O42 O 0.5844(3) 0.1840(2) 0.0887(2) 0.0241(8) Uani 1 1 d . . . O43 O 0.7197(3) 0.2517(2) 0.00625(19) 0.0255(9) Uani 1 1 d . . . O44 O 0.7446(3) 0.1072(2) 0.0577(2) 0.0238(8) Uani 1 1 d . . . O61 O 0.9073(3) 0.2837(2) 0.16502(19) 0.0231(8) Uani 1 1 d . . . O62 O 1.0246(3) 0.3130(3) 0.0597(2) 0.0396(12) Uani 1 1 d . . . O63 O 1.0775(3) 0.2071(3) 0.1520(2) 0.0357(11) Uani 1 1 d . . . O64 O 1.0602(3) 0.3533(3) 0.1806(2) 0.0343(10) Uani 1 1 d . . . C1 C 0.7416(5) -0.0157(4) 0.2839(3) 0.0311(14) Uani 1 1 d . . . C2 C 0.6742(5) 0.0048(4) 0.2293(3) 0.0393(16) Uani 1 1 d . . . H2A H 0.6733 0.0605 0.2136 0.059 Uiso 1 1 calc R . . H2B H 0.6119 -0.0058 0.2483 0.059 Uiso 1 1 calc R . . H2C H 0.6939 -0.0272 0.1911 0.059 Uiso 1 1 calc R . . C3 C 0.8373(5) 0.0040(5) 0.2564(4) 0.0430(17) Uani 1 1 d . . . H3A H 0.8342 0.0598 0.2405 0.064 Uiso 1 1 calc R . . H3B H 0.8602 -0.0278 0.2185 0.064 Uiso 1 1 calc R . . H3C H 0.8794 -0.0074 0.2924 0.064 Uiso 1 1 calc R . . C4 C 0.7450(7) -0.1027(4) 0.3089(4) 0.053(2) Uani 1 1 d . . . H4A H 0.7908 -0.1154 0.3423 0.079 Uiso 1 1 calc R . . H4B H 0.7624 -0.1347 0.2704 0.079 Uiso 1 1 calc R . . H4C H 0.6839 -0.1137 0.3301 0.079 Uiso 1 1 calc R . . C5 C 0.7499(4) 0.1315(4) 0.4659(3) 0.0245(12) Uani 1 1 d . . . C6 C 0.8426(4) 0.1209(4) 0.4237(3) 0.0302(13) Uani 1 1 d . . . H6A H 0.8482 0.1666 0.3908 0.045 Uiso 1 1 calc R . . H6B H 0.8465 0.0734 0.3994 0.045 Uiso 1 1 calc R . . H6C H 0.8928 0.1158 0.4536 0.045 Uiso 1 1 calc R . . C7 C 0.7356(5) 0.0627(4) 0.5186(3) 0.0396(17) Uani 1 1 d . . . H7A H 0.6744 0.0718 0.5435 0.059 Uiso 1 1 calc R . . H7B H 0.7835 0.0579 0.5505 0.059 Uiso 1 1 calc R . . H7C H 0.7399 0.0142 0.4958 0.059 Uiso 1 1 calc R . . C8 C 0.7403(5) 0.2083(5) 0.4991(4) 0.0441(18) Uani 1 1 d . . . H8A H 0.6790 0.2165 0.5240 0.066 Uiso 1 1 calc R . . H8B H 0.7476 0.2517 0.4640 0.066 Uiso 1 1 calc R . . H8C H 0.7882 0.2062 0.5306 0.066 Uiso 1 1 calc R . . C9 C 0.4806(4) 0.0956(4) 0.3772(3) 0.0319(14) Uani 1 1 d . . . C10 C 0.5100(5) 0.0112(4) 0.4041(4) 0.0384(16) Uani 1 1 d . . . H10A H 0.5314 -0.0204 0.3659 0.058 Uiso 1 1 calc R . . H10B H 0.4571 -0.0106 0.4302 0.058 Uiso 1 1 calc R . . H10C H 0.5602 0.0104 0.4334 0.058 Uiso 1 1 calc R . . C11 C 0.4495(5) 0.1466(5) 0.4358(4) 0.0442(18) Uani 1 1 d . . . H11A H 0.4297 0.2003 0.4177 0.066 Uiso 1 1 calc R . . H11B H 0.5010 0.1470 0.4636 0.066 Uiso 1 1 calc R . . H11C H 0.3976 0.1253 0.4636 0.066 Uiso 1 1 calc R . . C12 C 0.4028(5) 0.0985(5) 0.3304(4) 0.054(2) Uani 1 1 d . . . H12A H 0.4248 0.0681 0.2916 0.082 Uiso 1 1 calc R . . H12B H 0.3842 0.1532 0.3142 0.082 Uiso 1 1 calc R . . H12C H 0.3495 0.0762 0.3556 0.082 Uiso 1 1 calc R . . C21 C 0.5411(4) 0.4289(4) 0.3741(3) 0.0249(12) Uani 1 1 d . . . C22 C 0.5475(6) 0.3400(4) 0.3797(3) 0.0396(16) Uani 1 1 d . . . H22A H 0.6066 0.3187 0.3570 0.059 Uiso 1 1 calc R . . H22B H 0.4964 0.3237 0.3581 0.059 Uiso 1 1 calc R . . H22C H 0.5436 0.3203 0.4277 0.059 Uiso 1 1 calc R . . C23 C 0.6234(4) 0.4563(4) 0.4021(3) 0.0353(15) Uani 1 1 d . . . H23A H 0.6808 0.4335 0.3781 0.053 Uiso 1 1 calc R . . H23B H 0.6231 0.4394 0.4506 0.053 Uiso 1 1 calc R . . H23C H 0.6195 0.5137 0.3958 0.053 Uiso 1 1 calc R . . C24 C 0.4510(5) 0.4641(5) 0.4110(3) 0.0405(17) Uani 1 1 d . . . H24A H 0.3985 0.4435 0.3945 0.061 Uiso 1 1 calc R . . H24B H 0.4448 0.5214 0.4023 0.061 Uiso 1 1 calc R . . H24C H 0.4519 0.4499 0.4599 0.061 Uiso 1 1 calc R . . C25 C 0.3804(4) 0.4030(4) 0.1982(3) 0.0256(12) Uani 1 1 d . . . C26 C 0.3397(4) 0.4763(4) 0.2327(3) 0.0333(14) Uani 1 1 d . . . H26A H 0.3359 0.4646 0.2821 0.050 Uiso 1 1 calc R . . H26B H 0.2776 0.4934 0.2186 0.050 Uiso 1 1 calc R . . H26C H 0.3795 0.5182 0.2197 0.050 Uiso 1 1 calc R . . C27 C 0.3878(4) 0.4197(4) 0.1207(3) 0.0264(12) Uani 1 1 d . . . H27A H 0.4129 0.3715 0.0995 0.040 Uiso 1 1 calc R . . H27B H 0.4290 0.4604 0.1073 0.040 Uiso 1 1 calc R . . H27C H 0.3262 0.4377 0.1059 0.040 Uiso 1 1 calc R . . C28 C 0.3214(4) 0.3359(4) 0.2187(4) 0.0368(16) Uani 1 1 d . . . H28A H 0.3152 0.3262 0.2683 0.055 Uiso 1 1 calc R . . H28B H 0.3512 0.2883 0.1986 0.055 Uiso 1 1 calc R . . H28C H 0.2599 0.3500 0.2025 0.055 Uiso 1 1 calc R . . C29 C 0.6060(4) 0.5635(4) 0.1614(3) 0.0277(13) Uani 1 1 d . . . C30 C 0.7082(5) 0.5370(5) 0.1681(5) 0.053(2) Uani 1 1 d . . . H30A H 0.7177 0.5221 0.2160 0.079 Uiso 1 1 calc R . . H30B H 0.7447 0.5801 0.1511 0.079 Uiso 1 1 calc R . . H30C H 0.7280 0.4917 0.1416 0.079 Uiso 1 1 calc R . . C31 C 0.5697(8) 0.6235(5) 0.2099(5) 0.069(3) Uani 1 1 d . . . H31A H 0.5037 0.6392 0.2052 0.103 Uiso 1 1 calc R . . H31B H 0.6036 0.6696 0.1998 0.103 Uiso 1 1 calc R . . H31C H 0.5780 0.6013 0.2564 0.103 Uiso 1 1 calc R . . C32 C 0.5929(5) 0.5967(5) 0.0890(4) 0.0439(18) Uani 1 1 d . . . H32A H 0.5267 0.6087 0.0835 0.066 Uiso 1 1 calc R . . H32B H 0.6206 0.5580 0.0575 0.066 Uiso 1 1 calc R . . H32C H 0.6232 0.6448 0.0793 0.066 Uiso 1 1 calc R . . C41 C 0.5256(4) 0.1434(4) 0.0524(3) 0.0295(13) Uani 1 1 d . . . C42 C 0.4278(5) 0.1801(5) 0.0706(5) 0.054(2) Uani 1 1 d . . . H42A H 0.4127 0.1723 0.1198 0.081 Uiso 1 1 calc R . . H42B H 0.3845 0.1553 0.0472 0.081 Uiso 1 1 calc R . . H42C H 0.4229 0.2364 0.0565 0.081 Uiso 1 1 calc R . . C43 C 0.5509(6) 0.1557(5) -0.0242(3) 0.0466(19) Uani 1 1 d . . . H43A H 0.5435 0.2120 -0.0385 0.070 Uiso 1 1 calc R . . H43B H 0.5101 0.1290 -0.0481 0.070 Uiso 1 1 calc R . . H43C H 0.6154 0.1341 -0.0350 0.070 Uiso 1 1 calc R . . C44 C 0.5375(5) 0.0571(4) 0.0769(4) 0.0417(17) Uani 1 1 d . . . H44A H 0.5207 0.0509 0.1260 0.063 Uiso 1 1 calc R . . H44B H 0.6022 0.0356 0.0670 0.063 Uiso 1 1 calc R . . H44C H 0.4974 0.0289 0.0536 0.063 Uiso 1 1 calc R . . C45 C 0.7095(4) 0.3361(4) -0.0062(3) 0.0269(12) Uani 1 1 d . . . C46 C 0.7937(5) 0.3672(5) 0.0164(4) 0.0458(19) Uani 1 1 d . . . H46A H 0.8502 0.3409 -0.0062 0.069 Uiso 1 1 calc R . . H46B H 0.7946 0.3569 0.0657 0.069 Uiso 1 1 calc R . . H46C H 0.7906 0.4239 0.0042 0.069 Uiso 1 1 calc R . . C47 C 0.6195(4) 0.3713(4) 0.0296(3) 0.0310(14) Uani 1 1 d . . . H47A H 0.5677 0.3471 0.0159 0.046 Uiso 1 1 calc R . . H47B H 0.6107 0.4280 0.0172 0.046 Uiso 1 1 calc R . . H47C H 0.6219 0.3617 0.0789 0.046 Uiso 1 1 calc R . . C48 C 0.7074(5) 0.3521(4) -0.0829(3) 0.0402(17) Uani 1 1 d . . . H48A H 0.6551 0.3293 -0.0974 0.060 Uiso 1 1 calc R . . H48B H 0.7653 0.3283 -0.1056 0.060 Uiso 1 1 calc R . . H48C H 0.7005 0.4089 -0.0949 0.060 Uiso 1 1 calc R . . C49 C 0.8382(4) 0.0809(4) 0.0321(3) 0.0273(12) Uani 1 1 d . . . C50 C 0.8515(6) 0.1038(5) -0.0436(3) 0.0460(19) Uani 1 1 d . . . H50A H 0.8431 0.1612 -0.0517 0.069 Uiso 1 1 calc R . . H50B H 0.8060 0.0814 -0.0667 0.069 Uiso 1 1 calc R . . H50C H 0.9142 0.0838 -0.0613 0.069 Uiso 1 1 calc R . . C51 C 0.8482(5) -0.0084(4) 0.0456(4) 0.0393(16) Uani 1 1 d . . . H51A H 0.8384 -0.0226 0.0945 0.059 Uiso 1 1 calc R . . H51B H 0.9104 -0.0301 0.0285 0.059 Uiso 1 1 calc R . . H51C H 0.8020 -0.0298 0.0223 0.059 Uiso 1 1 calc R . . C52 C 0.9072(4) 0.1162(4) 0.0698(4) 0.0360(15) Uani 1 1 d . . . H52A H 0.8944 0.1040 0.1187 0.054 Uiso 1 1 calc R . . H52B H 0.9012 0.1733 0.0594 0.054 Uiso 1 1 calc R . . H52C H 0.9703 0.0940 0.0553 0.054 Uiso 1 1 calc R . . C61 C 1.1020(4) 0.3022(4) 0.0096(3) 0.0303(14) Uani 1 1 d . . . C62 C 1.0839(5) 0.3715(5) -0.0431(4) 0.0442(18) Uani 1 1 d . . . H62A H 1.0264 0.3674 -0.0633 0.066 Uiso 1 1 calc R . . H62B H 1.1355 0.3709 -0.0786 0.066 Uiso 1 1 calc R . . H62C H 1.0782 0.4207 -0.0211 0.066 Uiso 1 1 calc R . . C63 C 1.1026(6) 0.2259(5) -0.0211(4) 0.0482(19) Uani 1 1 d . . . H63A H 1.1121 0.1823 0.0139 0.072 Uiso 1 1 calc R . . H63B H 1.1529 0.2210 -0.0575 0.072 Uiso 1 1 calc R . . H63C H 1.0433 0.2244 -0.0396 0.072 Uiso 1 1 calc R . . C64 C 1.1944(4) 0.3066(5) 0.0386(3) 0.0366(16) Uani 1 1 d . . . H64A H 1.2052 0.2632 0.0735 0.055 Uiso 1 1 calc R . . H64B H 1.1924 0.3567 0.0587 0.055 Uiso 1 1 calc R . . H64C H 1.2447 0.3029 0.0021 0.055 Uiso 1 1 calc R . . C65 C 1.1008(4) 0.1569(4) 0.2123(3) 0.0270(13) Uani 1 1 d . . . C66 C 1.1324(7) 0.0780(5) 0.1818(5) 0.059(2) Uani 1 1 d . . . H66A H 1.1781 0.0858 0.1429 0.088 Uiso 1 1 calc R . . H66B H 1.0788 0.0574 0.1668 0.088 Uiso 1 1 calc R . . H66C H 1.1602 0.0404 0.2163 0.088 Uiso 1 1 calc R . . C67 C 1.1818(5) 0.1832(6) 0.2409(4) 0.057(2) Uani 1 1 d . . . H67A H 1.1638 0.2347 0.2583 0.085 Uiso 1 1 calc R . . H67B H 1.2329 0.1868 0.2052 0.085 Uiso 1 1 calc R . . H67C H 1.2017 0.1451 0.2780 0.085 Uiso 1 1 calc R . . C68 C 1.0193(5) 0.1502(4) 0.2640(4) 0.0381(16) Uani 1 1 d . . . H68A H 1.0031 0.2000 0.2848 0.057 Uiso 1 1 calc R . . H68B H 1.0352 0.1082 0.2992 0.057 Uiso 1 1 calc R . . H68C H 0.9665 0.1379 0.2419 0.057 Uiso 1 1 calc R . . C69 C 1.0347(4) 0.4365(3) 0.1874(3) 0.0203(11) Uani 1 1 d . . . C70 C 1.0988(4) 0.4834(4) 0.1384(3) 0.0333(14) Uani 1 1 d . . . H70A H 1.1634 0.4645 0.1456 0.050 Uiso 1 1 calc R . . H70B H 1.0866 0.5391 0.1466 0.050 Uiso 1 1 calc R . . H70C H 1.0877 0.4768 0.0916 0.050 Uiso 1 1 calc R . . C71 C 1.0512(5) 0.4448(5) 0.2603(3) 0.0423(17) Uani 1 1 d . . . H71A H 1.0122 0.4117 0.2908 0.063 Uiso 1 1 calc R . . H71B H 1.0355 0.4997 0.2702 0.063 Uiso 1 1 calc R . . H71C H 1.1165 0.4283 0.2669 0.063 Uiso 1 1 calc R . . C72 C 0.9344(4) 0.4638(4) 0.1769(3) 0.0354(15) Uani 1 1 d . . . H72A H 0.8945 0.4313 0.2071 0.053 Uiso 1 1 calc R . . H72B H 0.9238 0.4590 0.1296 0.053 Uiso 1 1 calc R . . H72C H 0.9201 0.5187 0.1871 0.053 Uiso 1 1 calc R . . K2 K -0.01024(14) 0.71576(9) 0.39479(8) 0.0459(4) Uani 1 1 d . . . O65A O 0.1677(6) 0.6636(5) 0.3818(4) 0.0300(18) Uani 0.559(6) 1 d PU A 1 O66A O 0.0532(7) 0.6004(5) 0.4950(5) 0.038(2) Uani 0.559(6) 1 d PU A 1 O67A O -0.2008(8) 0.6668(7) 0.3999(6) 0.040(2) Uani 0.559(6) 1 d PU A 1 O68A O -0.0659(11) 0.8327(15) 0.4907(13) 0.037(3) Uani 0.559(6) 1 d PU A 1 N1A N 0.0879(10) 0.7526(8) 0.2660(6) 0.031(3) Uani 0.559(6) 1 d PU A 1 N2A N -0.1319(11) 0.6825(7) 0.5296(5) 0.042(2) Uani 0.559(6) 1 d PU A 1 C73A C 0.1875(8) 0.7308(8) 0.2710(6) 0.032(2) Uani 0.559(6) 1 d PU A 1 H73A H 0.2129 0.7731 0.2910 0.039 Uiso 0.559(6) 1 calc PR A 1 H73B H 0.2189 0.7260 0.2248 0.039 Uiso 0.559(6) 1 calc PR A 1 C74A C 0.2080(13) 0.6549(11) 0.3134(9) 0.037(3) Uani 0.559(6) 1 d PU A 1 H74A H 0.1819 0.6122 0.2943 0.044 Uiso 0.559(6) 1 calc PR A 1 H74B H 0.2758 0.6411 0.3131 0.044 Uiso 0.559(6) 1 calc PR A 1 C75A C 0.201(2) 0.6027(16) 0.4268(12) 0.043(4) Uani 0.559(6) 1 d PU A 1 H75A H 0.2681 0.6033 0.4289 0.052 Uiso 0.559(6) 1 calc PR A 1 H75B H 0.1908 0.5518 0.4110 0.052 Uiso 0.559(6) 1 calc PR A 1 C76A C 0.1503(11) 0.6115(9) 0.4974(8) 0.048(3) Uani 0.559(6) 1 d PU A 1 H76A H 0.1790 0.5720 0.5308 0.057 Uiso 0.559(6) 1 calc PR A 1 H76B H 0.1550 0.6644 0.5115 0.057 Uiso 0.559(6) 1 calc PR A 1 C77A C 0.0098(14) 0.5951(12) 0.5602(9) 0.039(3) Uani 0.559(6) 1 d PU A 1 H77A H 0.0268 0.6371 0.5857 0.046 Uiso 0.559(6) 1 calc PR A 1 H77B H 0.0307 0.5439 0.5840 0.046 Uiso 0.559(6) 1 calc PR A 1 C78A C -0.0956(10) 0.6033(8) 0.5579(6) 0.042(3) Uani 0.559(6) 1 d PU A 1 H78A H -0.1118 0.5635 0.5296 0.050 Uiso 0.559(6) 1 calc PR A 1 H78B H -0.1255 0.5931 0.6043 0.050 Uiso 0.559(6) 1 calc PR A 1 C79A C 0.0572(11) 0.7076(10) 0.2136(7) 0.038(3) Uani 0.559(6) 1 d PU A 1 H79A H 0.0856 0.6525 0.2195 0.046 Uiso 0.559(6) 1 calc PR A 1 H79B H 0.0800 0.7298 0.1681 0.046 Uiso 0.559(6) 1 calc PR A 1 C80A C -0.0453(14) 0.7087(13) 0.2168(12) 0.042(4) Uani 0.559(6) 1 d PU A 1 H80A H -0.0742 0.7637 0.2107 0.050 Uiso 0.559(6) 1 calc PR A 1 H80B H -0.0613 0.6803 0.1793 0.050 Uiso 0.559(6) 1 calc PR A 1 C81A C -0.2098(12) 0.6216(11) 0.3448(10) 0.043(3) Uani 0.559(6) 1 d PU A 1 H81A H -0.1751 0.5688 0.3517 0.051 Uiso 0.559(6) 1 calc PR A 1 H81B H -0.2757 0.6153 0.3420 0.051 Uiso 0.559(6) 1 calc PR A 1 C82A C -0.2463(11) 0.6350(10) 0.4612(8) 0.052(3) Uani 0.559(6) 1 d PU A 1 H82A H -0.2210 0.5796 0.4713 0.063 Uiso 0.559(6) 1 calc PR A 1 H82B H -0.3135 0.6369 0.4568 0.063 Uiso 0.559(6) 1 calc PR A 1 C83A C -0.2301(11) 0.6840(9) 0.5184(7) 0.053(3) Uani 0.559(6) 1 d PU A 1 H83A H -0.2561 0.7391 0.5075 0.063 Uiso 0.559(6) 1 calc PR A 1 H83B H -0.2641 0.6642 0.5610 0.063 Uiso 0.559(6) 1 calc PR A 1 C84A C 0.0702(12) 0.8372(11) 0.2459(8) 0.033(3) Uani 0.559(6) 1 d PU A 1 H84A H 0.0091 0.8467 0.2273 0.040 Uiso 0.559(6) 1 calc PR A 1 H84B H 0.1171 0.8503 0.2084 0.040 Uiso 0.559(6) 1 calc PR A 1 C85A C -0.1373(15) 0.8244(11) 0.5435(10) 0.060(4) Uani 0.559(6) 1 d PU A 1 H85A H -0.1983 0.8348 0.5246 0.072 Uiso 0.559(6) 1 calc PR A 1 H85B H -0.1349 0.8629 0.5771 0.072 Uiso 0.559(6) 1 calc PR A 1 C86A C -0.1260(14) 0.7434(9) 0.5771(7) 0.056(3) Uani 0.559(6) 1 d PU A 1 H86A H -0.1746 0.7386 0.6153 0.067 Uiso 0.559(6) 1 calc PR A 1 H86B H -0.0651 0.7338 0.5961 0.067 Uiso 0.559(6) 1 calc PR A 1 O65B O 0.1909(10) 0.6685(8) 0.3350(8) 0.032(3) Uani 0.441(6) 1 d PU A 2 O66B O 0.1152(9) 0.5953(6) 0.4588(6) 0.038(2) Uani 0.441(6) 1 d PU A 2 O67B O -0.1606(10) 0.6448(9) 0.4082(7) 0.040(3) Uani 0.441(6) 1 d PU A 2 O68B O -0.0373(12) 0.8282(17) 0.4887(15) 0.025(3) Uani 0.441(6) 1 d PU A 2 N1B N 0.0767(12) 0.7737(10) 0.2454(7) 0.027(3) Uani 0.441(6) 1 d PU A 2 N2B N -0.0667(12) 0.6634(9) 0.5287(6) 0.039(3) Uani 0.441(6) 1 d PU A 2 C73B C 0.1778(11) 0.7578(9) 0.2360(9) 0.034(3) Uani 0.441(6) 1 d PU A 2 H73C H 0.2055 0.7964 0.2593 0.041 Uiso 0.441(6) 1 calc PR A 2 H73D H 0.1982 0.7650 0.1870 0.041 Uiso 0.441(6) 1 calc PR A 2 C74B C 0.2123(11) 0.6771(9) 0.2628(8) 0.034(3) Uani 0.441(6) 1 d PU A 2 H74C H 0.1828 0.6381 0.2413 0.041 Uiso 0.441(6) 1 calc PR A 2 H74D H 0.2801 0.6675 0.2517 0.041 Uiso 0.441(6) 1 calc PR A 2 C75B C 0.2297(11) 0.5941(9) 0.3630(8) 0.035(3) Uani 0.441(6) 1 d PU A 2 H75C H 0.2974 0.5867 0.3506 0.042 Uiso 0.441(6) 1 calc PR A 2 H75D H 0.2016 0.5514 0.3455 0.042 Uiso 0.441(6) 1 calc PR A 2 C76B C 0.209(2) 0.593(2) 0.4407(14) 0.039(4) Uani 0.441(6) 1 d PU A 2 H76C H 0.2415 0.5447 0.4625 0.046 Uiso 0.441(6) 1 calc PR A 2 H76D H 0.2325 0.6387 0.4571 0.046 Uiso 0.441(6) 1 calc PR A 2 C77B C 0.0973(15) 0.5969(11) 0.5293(9) 0.049(3) Uani 0.441(6) 1 d PU A 2 H77C H 0.1114 0.6474 0.5434 0.059 Uiso 0.441(6) 1 calc PR A 2 H77D H 0.1366 0.5538 0.5526 0.059 Uiso 0.441(6) 1 calc PR A 2 C78B C -0.010(2) 0.5867(17) 0.5492(13) 0.047(4) Uani 0.441(6) 1 d PU A 2 H78C H -0.0279 0.5438 0.5253 0.056 Uiso 0.441(6) 1 calc PR A 2 H78D H -0.0211 0.5734 0.5986 0.056 Uiso 0.441(6) 1 calc PR A 2 C79B C 0.0329(13) 0.7330(12) 0.1951(8) 0.034(3) Uani 0.441(6) 1 d PU A 2 H79C H 0.0653 0.6793 0.1922 0.041 Uiso 0.441(6) 1 calc PR A 2 H79D H 0.0414 0.7617 0.1497 0.041 Uiso 0.441(6) 1 calc PR A 2 C80B C -0.0693(17) 0.7278(16) 0.2134(15) 0.034(4) Uani 0.441(6) 1 d PU A 2 H80C H -0.1020 0.7805 0.2205 0.041 Uiso 0.441(6) 1 calc PR A 2 H80D H -0.0963 0.7065 0.1762 0.041 Uiso 0.441(6) 1 calc PR A 2 C81B C -0.1776(16) 0.6034(14) 0.3512(13) 0.040(4) Uani 0.441(6) 1 d PU A 2 H81C H -0.2392 0.5841 0.3593 0.048 Uiso 0.441(6) 1 calc PR A 2 H81D H -0.1302 0.5576 0.3459 0.048 Uiso 0.441(6) 1 calc PR A 2 C82B C -0.1785(14) 0.5982(11) 0.4711(9) 0.051(4) Uani 0.441(6) 1 d PU A 2 H82C H -0.1377 0.5479 0.4715 0.061 Uiso 0.441(6) 1 calc PR A 2 H82D H -0.2437 0.5865 0.4766 0.061 Uiso 0.441(6) 1 calc PR A 2 C83B C -0.1592(15) 0.6461(12) 0.5299(9) 0.047(4) Uani 0.441(6) 1 d PU A 2 H83C H -0.2006 0.6961 0.5283 0.056 Uiso 0.441(6) 1 calc PR A 2 H83D H -0.1754 0.6162 0.5737 0.056 Uiso 0.441(6) 1 calc PR A 2 C84B C 0.0481(15) 0.8589(12) 0.2344(11) 0.032(4) Uani 0.441(6) 1 d PU A 2 H84C H -0.0189 0.8691 0.2286 0.038 Uiso 0.441(6) 1 calc PR A 2 H84D H 0.0830 0.8818 0.1935 0.038 Uiso 0.441(6) 1 calc PR A 2 C85B C -0.0946(12) 0.8062(12) 0.5496(9) 0.034(3) Uani 0.441(6) 1 d PU A 2 H85C H -0.1599 0.8097 0.5393 0.040 Uiso 0.441(6) 1 calc PR A 2 H85D H -0.0908 0.8428 0.5845 0.040 Uiso 0.441(6) 1 calc PR A 2 C86B C -0.0632(13) 0.7251(9) 0.5759(7) 0.033(3) Uani 0.441(6) 1 d PU A 2 H86C H -0.1019 0.7121 0.6183 0.039 Uiso 0.441(6) 1 calc PR A 2 H86D H 0.0014 0.7233 0.5876 0.039 Uiso 0.441(6) 1 calc PR A 2 O69 O -0.0796(3) 0.6746(3) 0.2773(2) 0.0379(11) Uani 1 1 d U A . O70 O 0.0047(3) 0.8760(2) 0.3536(2) 0.0266(9) Uani 1 1 d U A . C87 C -0.1736(5) 0.6617(5) 0.2840(4) 0.0454(17) Uani 1 1 d U . . H87A H -0.1839 0.6319 0.2458 0.054 Uiso 0.559(6) 1 calc PR A 1 H87B H -0.2109 0.7135 0.2784 0.054 Uiso 0.559(6) 1 calc PR A 1 H87C H -0.1900 0.6369 0.2445 0.054 Uiso 0.441(6) 1 calc PR A 2 H87D H -0.2149 0.7110 0.2899 0.054 Uiso 0.441(6) 1 calc PR A 2 C88 C 0.0706(5) 0.8949(4) 0.2995(4) 0.0403(16) Uani 1 1 d U . . H88A H 0.1329 0.8910 0.3160 0.048 Uiso 0.559(6) 1 calc PR A 1 H88B H 0.0546 0.9493 0.2799 0.048 Uiso 0.559(6) 1 calc PR A 1 H88C H 0.1335 0.8735 0.3113 0.048 Uiso 0.441(6) 1 calc PR A 2 H88D H 0.0687 0.9526 0.2910 0.048 Uiso 0.441(6) 1 calc PR A 2 C89 C 0.0074(4) 0.9244(4) 0.4081(3) 0.0295(13) Uani 1 1 d U . . H89A H -0.0005 0.9805 0.3908 0.035 Uiso 1 1 calc R A . H89B H 0.0682 0.9131 0.4271 0.035 Uiso 1 1 calc R . . C90 C -0.0674(5) 0.9088(4) 0.4618(3) 0.0337(14) Uani 1 1 d U A . H90A H -0.0649 0.9436 0.4982 0.040 Uiso 0.559(6) 1 calc PR A 1 H90B H -0.1274 0.9236 0.4423 0.040 Uiso 0.559(6) 1 calc PR A 1 H90C H -0.0720 0.9460 0.4973 0.040 Uiso 0.441(6) 1 calc PR A 2 H90D H -0.1279 0.9120 0.4427 0.040 Uiso 0.441(6) 1 calc PR A 2 C91 C 0.6558(9) 0.0771(10) -0.1966(7) 0.124(5) Uani 1 1 d U . . H91A H 0.6960 0.0545 -0.2340 0.185 Uiso 1 1 calc R . . H91B H 0.6383 0.0349 -0.1629 0.185 Uiso 1 1 calc R . . H91C H 0.6889 0.1130 -0.1753 0.185 Uiso 1 1 calc R . . C92 C 0.5749(10) 0.1188(11) -0.2221(8) 0.122(5) Uani 1 1 d U . . H92A H 0.5463 0.1542 -0.1874 0.147 Uiso 1 1 calc R . . H92B H 0.5310 0.0801 -0.2252 0.147 Uiso 1 1 calc R . . C93 C 0.5809(10) 0.1658(11) -0.2870(8) 0.128(5) Uani 1 1 d U . . H93A H 0.6152 0.1320 -0.3208 0.154 Uiso 1 1 calc R . . H93B H 0.6194 0.2082 -0.2824 0.154 Uiso 1 1 calc R . . C94 C 0.4945(13) 0.2031(11) -0.3161(9) 0.140(5) Uani 1 1 d U B . H94A H 0.4517 0.1621 -0.3105 0.168 Uiso 1 1 calc R . . H94B H 0.4674 0.2436 -0.2854 0.168 Uiso 1 1 calc R . . C95 C 0.4877(15) 0.2375(14) -0.3800(10) 0.165(7) Uani 1 1 d DU . . H95A H 0.5220 0.2019 -0.4126 0.198 Uiso 0.55(2) 1 calc PR B 1 H95B H 0.4219 0.2445 -0.3894 0.198 Uiso 0.55(2) 1 calc PR B 1 H95C H 0.5486 0.2577 -0.3906 0.198 Uiso 0.45(2) 1 calc PR B 2 H95D H 0.4915 0.1915 -0.4069 0.198 Uiso 0.45(2) 1 calc PR B 2 C96A C 0.5198(18) 0.3055(12) -0.3904(12) 0.092(8) Uani 0.55(2) 1 d PDU B 1 H96A H 0.4731 0.3462 -0.3727 0.138 Uiso 0.55(2) 1 calc PR B 1 H96B H 0.5343 0.3178 -0.4392 0.138 Uiso 0.55(2) 1 calc PR B 1 H96C H 0.5761 0.3037 -0.3670 0.138 Uiso 0.55(2) 1 calc PR B 1 C96B C 0.432(2) 0.2915(15) -0.4152(14) 0.114(11) Uani 0.45(2) 1 d PDU B 2 H96D H 0.4650 0.3369 -0.4312 0.171 Uiso 0.45(2) 1 calc PR B 2 H96E H 0.3765 0.3084 -0.3857 0.171 Uiso 0.45(2) 1 calc PR B 2 H96F H 0.4135 0.2683 -0.4543 0.171 Uiso 0.45(2) 1 calc PR B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 U1 0.01221(8) 0.02099(10) 0.01591(9) -0.00248(6) -0.00140(6) -0.00313(6) K1 0.0167(5) 0.0262(6) 0.0205(5) -0.0029(4) -0.0032(4) -0.0051(4) S1 0.0215(7) 0.0421(9) 0.0207(7) -0.0100(6) -0.0019(5) -0.0122(6) Si1 0.0186(7) 0.0228(8) 0.0166(7) 0.0011(6) -0.0023(5) -0.0075(6) Si2 0.0146(7) 0.0227(8) 0.0197(7) -0.0047(6) -0.0026(5) -0.0006(6) Si3 0.0174(7) 0.0241(8) 0.0158(7) -0.0043(6) -0.0011(5) -0.0020(6) Si4 0.0134(6) 0.0222(7) 0.0172(7) -0.0014(6) -0.0013(5) -0.0029(5) O1 0.0190(19) 0.024(2) 0.030(2) -0.0030(16) -0.0111(16) -0.0030(16) O2 0.033(2) 0.024(2) 0.0180(19) -0.0027(15) -0.0031(16) -0.0050(17) O3 0.0197(19) 0.033(2) 0.0198(19) -0.0017(16) -0.0033(15) -0.0013(16) O4 0.0198(19) 0.029(2) 0.025(2) 0.0048(16) -0.0058(16) -0.0082(16) O21 0.0213(19) 0.023(2) 0.0207(19) -0.0057(15) -0.0014(15) 0.0008(15) O22 0.030(2) 0.026(2) 0.0198(19) -0.0062(16) -0.0004(16) -0.0007(17) O23 0.0155(18) 0.029(2) 0.032(2) -0.0032(17) -0.0066(16) -0.0011(16) O24 0.0169(18) 0.027(2) 0.025(2) -0.0001(16) -0.0048(15) -0.0037(15) O41 0.0156(17) 0.024(2) 0.0192(18) -0.0035(15) -0.0043(14) -0.0029(15) O42 0.0201(19) 0.030(2) 0.025(2) -0.0121(16) -0.0046(15) -0.0039(16) O43 0.030(2) 0.025(2) 0.0201(19) -0.0021(16) 0.0002(16) 0.0015(17) O44 0.0221(19) 0.025(2) 0.024(2) -0.0051(16) 0.0003(16) -0.0005(16) O61 0.0171(18) 0.034(2) 0.0197(19) -0.0057(16) -0.0011(15) -0.0056(16) O62 0.023(2) 0.076(4) 0.020(2) -0.002(2) 0.0001(17) -0.010(2) O63 0.031(2) 0.038(3) 0.036(3) 0.004(2) -0.0033(19) 0.000(2) O64 0.029(2) 0.034(3) 0.040(3) -0.005(2) -0.0074(19) -0.0014(19) C1 0.049(4) 0.021(3) 0.024(3) -0.007(2) -0.007(3) 0.001(3) C2 0.041(4) 0.046(4) 0.033(4) -0.014(3) -0.011(3) -0.005(3) C3 0.046(4) 0.050(5) 0.032(4) -0.010(3) -0.006(3) 0.003(3) C4 0.087(6) 0.027(4) 0.048(5) -0.006(3) -0.019(4) -0.004(4) C5 0.029(3) 0.033(3) 0.015(2) -0.002(2) -0.009(2) -0.010(2) C6 0.021(3) 0.046(4) 0.025(3) 0.001(3) -0.004(2) -0.008(3) C7 0.035(4) 0.056(5) 0.030(3) 0.016(3) -0.012(3) -0.019(3) C8 0.048(4) 0.049(5) 0.040(4) -0.019(3) 0.001(3) -0.018(4) C9 0.017(3) 0.042(4) 0.036(3) 0.009(3) 0.000(2) -0.014(3) C10 0.037(4) 0.036(4) 0.041(4) 0.010(3) 0.002(3) -0.017(3) C11 0.031(4) 0.049(5) 0.050(4) 0.001(4) 0.009(3) -0.006(3) C12 0.028(4) 0.077(6) 0.062(5) 0.024(4) -0.017(3) -0.032(4) C21 0.027(3) 0.031(3) 0.018(3) -0.008(2) 0.000(2) -0.004(2) C22 0.062(5) 0.032(4) 0.024(3) -0.004(3) 0.003(3) -0.007(3) C23 0.029(3) 0.045(4) 0.035(3) -0.013(3) -0.009(3) -0.004(3) C24 0.028(3) 0.071(5) 0.021(3) -0.006(3) 0.002(3) -0.004(3) C25 0.016(3) 0.032(3) 0.030(3) -0.005(2) -0.006(2) -0.003(2) C26 0.021(3) 0.048(4) 0.032(3) -0.013(3) -0.006(2) 0.001(3) C27 0.017(3) 0.036(3) 0.027(3) -0.009(2) -0.005(2) 0.000(2) C28 0.019(3) 0.042(4) 0.050(4) 0.003(3) -0.007(3) -0.012(3) C29 0.025(3) 0.030(3) 0.029(3) -0.002(2) -0.001(2) -0.012(2) C30 0.032(4) 0.054(5) 0.076(6) 0.015(4) -0.027(4) -0.018(3) C31 0.105(8) 0.030(4) 0.067(6) -0.012(4) 0.026(6) -0.016(5) C32 0.052(4) 0.045(4) 0.038(4) 0.014(3) -0.011(3) -0.025(4) C41 0.026(3) 0.032(3) 0.034(3) -0.015(3) -0.012(2) -0.003(2) C42 0.027(4) 0.065(6) 0.079(6) -0.036(5) -0.017(4) -0.004(3) C43 0.056(5) 0.057(5) 0.032(4) -0.011(3) -0.021(3) -0.011(4) C44 0.045(4) 0.041(4) 0.045(4) -0.010(3) -0.015(3) -0.015(3) C45 0.027(3) 0.033(3) 0.019(3) 0.001(2) 0.000(2) 0.000(2) C46 0.034(4) 0.043(4) 0.060(5) 0.018(4) -0.014(3) -0.010(3) C47 0.035(3) 0.031(3) 0.025(3) -0.002(2) -0.002(3) 0.006(3) C48 0.055(4) 0.041(4) 0.021(3) 0.003(3) 0.000(3) 0.008(3) C49 0.028(3) 0.028(3) 0.024(3) -0.004(2) -0.001(2) 0.005(2) C50 0.051(4) 0.053(5) 0.028(4) -0.005(3) 0.008(3) 0.010(4) C51 0.040(4) 0.030(4) 0.044(4) -0.007(3) 0.003(3) 0.006(3) C52 0.022(3) 0.044(4) 0.043(4) -0.011(3) 0.000(3) -0.003(3) C61 0.021(3) 0.050(4) 0.021(3) -0.005(3) 0.002(2) -0.007(3) C62 0.039(4) 0.054(5) 0.038(4) -0.004(3) -0.006(3) 0.002(3) C63 0.055(5) 0.043(4) 0.050(5) -0.006(4) -0.003(4) -0.017(4) C64 0.018(3) 0.062(5) 0.028(3) -0.001(3) 0.006(2) -0.008(3) C65 0.023(3) 0.026(3) 0.031(3) 0.009(2) -0.006(2) -0.004(2) C66 0.068(6) 0.045(5) 0.062(6) -0.007(4) 0.008(5) -0.007(4) C67 0.036(4) 0.084(7) 0.056(5) -0.008(5) -0.011(4) -0.025(4) C68 0.030(3) 0.039(4) 0.042(4) 0.010(3) 0.001(3) -0.006(3) C69 0.015(2) 0.018(3) 0.028(3) -0.003(2) -0.001(2) -0.004(2) C70 0.027(3) 0.043(4) 0.031(3) 0.002(3) -0.007(3) -0.010(3) C71 0.032(4) 0.062(5) 0.032(4) 0.003(3) -0.005(3) -0.006(3) C72 0.021(3) 0.047(4) 0.035(4) 0.006(3) -0.001(3) -0.002(3) K2 0.0840(12) 0.0247(7) 0.0347(8) -0.0037(6) -0.0326(8) -0.0053(7) O65A 0.036(4) 0.026(4) 0.029(4) -0.005(3) -0.005(3) -0.002(3) O66A 0.050(5) 0.039(4) 0.033(4) 0.004(3) -0.024(4) -0.023(4) O67A 0.038(6) 0.041(6) 0.039(5) 0.001(4) 0.001(5) -0.012(4) O68A 0.051(9) 0.036(6) 0.025(5) -0.003(4) 0.000(8) -0.017(8) N1A 0.031(5) 0.039(7) 0.022(6) -0.007(4) -0.003(4) -0.001(5) N2A 0.072(7) 0.037(5) 0.020(4) -0.003(4) 0.006(5) -0.020(5) C73A 0.028(5) 0.039(6) 0.029(5) -0.003(5) 0.002(4) -0.003(5) C74A 0.034(6) 0.035(7) 0.037(7) -0.009(6) 0.005(6) 0.008(5) C75A 0.048(7) 0.034(7) 0.049(9) 0.011(7) -0.017(7) -0.010(6) C76A 0.060(7) 0.043(6) 0.047(6) 0.015(5) -0.026(5) -0.026(5) C77A 0.062(7) 0.041(6) 0.023(6) 0.006(5) -0.028(5) -0.031(5) C78A 0.068(7) 0.038(6) 0.024(5) 0.005(4) -0.011(5) -0.026(5) C79A 0.043(7) 0.052(8) 0.023(6) -0.014(5) -0.004(5) -0.004(6) C80A 0.048(9) 0.055(9) 0.024(6) -0.009(7) -0.007(7) -0.007(7) C81A 0.041(8) 0.046(8) 0.046(7) -0.004(6) -0.009(6) -0.021(6) C82A 0.044(6) 0.059(7) 0.054(7) -0.003(6) 0.003(6) -0.017(6) C83A 0.065(8) 0.051(7) 0.035(6) 0.002(6) 0.025(6) -0.008(6) C84A 0.034(7) 0.043(8) 0.022(6) 0.004(6) -0.005(5) -0.004(6) C85A 0.086(10) 0.047(8) 0.044(7) -0.009(6) 0.024(8) -0.016(8) C86A 0.089(9) 0.046(7) 0.034(6) -0.012(5) 0.017(7) -0.019(7) O65B 0.031(6) 0.027(6) 0.037(7) -0.004(5) -0.005(5) 0.006(5) O66B 0.055(6) 0.029(5) 0.032(5) -0.001(4) -0.026(5) 0.004(5) O67B 0.044(7) 0.043(7) 0.034(5) -0.006(5) -0.001(5) -0.012(5) O68B 0.034(8) 0.025(5) 0.018(5) -0.008(4) -0.004(7) 0.000(7) N1B 0.034(6) 0.031(7) 0.016(6) -0.005(5) -0.002(5) 0.003(5) N2B 0.059(7) 0.043(6) 0.013(5) -0.005(4) 0.002(5) -0.005(6) C73B 0.035(6) 0.029(7) 0.038(7) -0.006(6) 0.002(6) 0.002(6) C74B 0.034(6) 0.027(6) 0.038(7) -0.004(6) 0.004(6) 0.004(5) C75B 0.035(6) 0.026(6) 0.044(7) -0.002(5) -0.011(5) -0.001(5) C76B 0.052(8) 0.028(8) 0.038(9) 0.013(7) -0.028(7) -0.005(6) C77B 0.066(8) 0.041(7) 0.037(7) -0.004(6) -0.012(7) 0.008(7) C78B 0.070(9) 0.047(8) 0.028(8) -0.003(6) -0.011(7) -0.016(8) C79B 0.039(8) 0.045(8) 0.019(7) -0.004(6) -0.002(6) -0.006(6) C80B 0.036(9) 0.049(10) 0.017(6) -0.003(7) -0.011(7) 0.002(7) C81B 0.043(9) 0.038(8) 0.040(7) -0.004(6) -0.001(8) -0.014(7) C82B 0.056(8) 0.046(8) 0.049(8) 0.002(7) 0.005(7) -0.017(7) C83B 0.067(8) 0.043(7) 0.027(6) -0.001(6) 0.017(6) -0.013(7) C84B 0.037(8) 0.029(9) 0.025(8) 0.002(6) -0.001(6) 0.005(6) C85B 0.037(7) 0.040(7) 0.022(6) 0.000(5) -0.006(6) 0.000(6) C86B 0.056(8) 0.035(7) 0.010(5) -0.003(5) -0.002(6) -0.011(6) O69 0.039(3) 0.051(3) 0.027(2) -0.009(2) -0.0083(19) -0.010(2) O70 0.028(2) 0.030(2) 0.024(2) -0.0047(17) -0.0043(16) -0.0065(17) C87 0.047(4) 0.051(4) 0.046(4) -0.018(3) -0.008(3) -0.019(3) C88 0.044(4) 0.041(4) 0.038(4) -0.007(3) 0.008(3) -0.017(3) C89 0.036(3) 0.027(3) 0.028(3) -0.006(2) -0.014(3) -0.004(3) C90 0.042(4) 0.035(3) 0.028(3) -0.009(3) -0.009(3) -0.006(3) C91 0.069(8) 0.202(16) 0.108(10) -0.068(11) -0.002(7) -0.011(10) C92 0.086(9) 0.169(13) 0.120(10) -0.043(10) -0.019(8) -0.010(9) C93 0.083(8) 0.207(13) 0.098(9) -0.060(9) 0.009(8) -0.008(9) C94 0.147(11) 0.154(12) 0.122(10) -0.070(10) -0.019(10) 0.017(10) C95 0.166(13) 0.182(14) 0.132(12) -0.046(13) 0.035(12) 0.022(13) C96A 0.124(18) 0.061(12) 0.086(14) -0.040(11) 0.009(13) 0.020(13) C96B 0.18(2) 0.044(13) 0.094(18) -0.003(12) 0.057(17) 0.035(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O61 U1 O21 127.48(14) O61 U1 O1 132.68(15) O21 U1 O1 96.64(14) O61 U1 O41 87.06(14) O21 U1 O41 83.77(13) O1 U1 O41 81.09(14) O61 U1 S1 93.87(10) O21 U1 S1 97.75(11) O1 U1 S1 96.33(10) O41 U1 S1 177.16(10) O61 U1 K1 138.31(10) O21 U1 K1 54.41(10) O1 U1 K1 53.08(9) O41 U1 K1 51.36(9) S1 U1 K1 127.81(4) O23 K1 O42 110.30(13) O23 K1 O4 120.63(13) O42 K1 O4 128.07(13) O23 K1 O41 107.37(12) O42 K1 O41 55.82(11) O4 K1 O41 113.00(12) O23 K1 O1 118.89(12) O42 K1 O1 109.19(12) O4 K1 O1 54.31(12) O41 K1 O1 62.76(11) O23 K1 O21 54.34(11) O42 K1 O21 106.37(12) O4 K1 O21 110.66(12) O41 K1 O21 63.45(11) O1 K1 O21 70.91(11) O23 K1 Si3 112.17(10) O42 K1 Si3 28.56(8) O4 K1 Si3 123.81(10) O41 K1 Si3 27.29(8) O1 K1 Si3 84.85(9) O21 K1 Si3 84.63(8) O23 K1 Si2 27.56(9) O42 K1 Si2 113.21(10) O4 K1 Si2 116.44(10) O41 K1 Si2 86.44(9) O1 K1 Si2 93.62(9) O21 K1 Si2 27.00(8) Si3 K1 Si2 101.20(5) O23 K1 Si1 125.87(10) O42 K1 Si1 120.01(10) O4 K1 Si1 27.81(8) O41 K1 Si1 86.56(8) O1 K1 Si1 26.63(8) O21 K1 Si1 91.73(8) Si3 K1 Si1 103.41(5) Si2 K1 Si1 108.13(5) O23 K1 U1 92.75(9) O42 K1 U1 95.15(9) O4 K1 U1 92.09(8) O41 K1 U1 39.42(8) O1 K1 U1 39.15(8) O21 K1 U1 38.41(7) Si3 K1 U1 66.69(3) Si2 K1 U1 65.29(3) Si1 K1 U1 65.32(3) O1 Si1 O3 116.9(2) O1 Si1 O2 114.0(2) O3 Si1 O2 105.5(2) O1 Si1 O4 104.4(2) O3 Si1 O4 105.3(2) O2 Si1 O4 110.4(2) O1 Si1 K1 54.47(14) O3 Si1 K1 130.33(16) O2 Si1 K1 122.90(15) O4 Si1 K1 50.24(14) O21 Si2 O22 114.7(2) O21 Si2 O24 116.0(2) O22 Si2 O24 105.8(2) O21 Si2 O23 104.6(2) O22 Si2 O23 110.7(2) O24 Si2 O23 104.6(2) O21 Si2 K1 56.38(15) O22 Si2 K1 122.41(16) O24 Si2 K1 130.05(16) O23 Si2 K1 48.81(14) O41 Si3 O44 116.7(2) O41 Si3 O43 114.0(2) O44 Si3 O43 105.1(2) O41 Si3 O42 104.9(2) O44 Si3 O42 103.7(2) O43 Si3 O42 112.1(2) O41 Si3 K1 53.94(14) O44 Si3 K1 122.12(15) O43 Si3 K1 131.83(16) O42 Si3 K1 51.03(14) O61 Si4 O63 112.2(2) O61 Si4 O62 109.0(2) O63 Si4 O62 104.3(3) O61 Si4 O64 114.5(2) O63 Si4 O64 106.0(2) O62 Si4 O64 110.2(3) Si1 O1 U1 165.4(2) Si1 O1 K1 98.90(17) U1 O1 K1 87.77(12) C1 O2 Si1 129.2(4) C5 O3 Si1 131.9(4) C9 O4 Si1 129.2(4) C9 O4 K1 128.8(3) Si1 O4 K1 101.95(17) Si2 O21 U1 172.5(2) Si2 O21 K1 96.62(18) U1 O21 K1 87.18(13) C21 O22 Si2 132.7(4) C25 O23 Si2 130.2(4) C25 O23 K1 124.9(3) Si2 O23 K1 103.63(18) C29 O24 Si2 131.6(4) Si3 O41 U1 171.6(2) Si3 O41 K1 98.77(17) U1 O41 K1 89.22(12) C41 O42 Si3 131.0(4) C41 O42 K1 126.4(3) Si3 O42 K1 100.41(17) C45 O43 Si3 131.3(4) C49 O44 Si3 130.5(4) Si4 O61 U1 161.5(2) C61 O62 Si4 132.1(4) C65 O63 Si4 132.6(4) C69 O64 Si4 131.2(4) O2 C1 C3 108.8(5) O2 C1 C2 111.1(5) C3 C1 C2 110.2(6) O2 C1 C4 105.8(5) C3 C1 C4 110.3(6) C2 C1 C4 110.5(6) C1 C2 H2A 109.5 C1 C2 H2B 109.5 H2A C2 H2B 109.5 C1 C2 H2C 109.5 H2A C2 H2C 109.5 H2B C2 H2C 109.5 C1 C3 H3A 109.5 C1 C3 H3B 109.5 H3A C3 H3B 109.5 C1 C3 H3C 109.5 H3A C3 H3C 109.5 H3B C3 H3C 109.5 C1 C4 H4A 109.5 C1 C4 H4B 109.5 H4A C4 H4B 109.5 C1 C4 H4C 109.5 H4A C4 H4C 109.5 H4B C4 H4C 109.5 O3 C5 C8 105.8(5) O3 C5 C6 111.8(4) C8 C5 C6 109.6(5) O3 C5 C7 105.5(5) C8 C5 C7 111.1(5) C6 C5 C7 112.8(5) C5 C6 H6A 109.5 C5 C6 H6B 109.5 H6A C6 H6B 109.5 C5 C6 H6C 109.5 H6A C6 H6C 109.5 H6B C6 H6C 109.5 C5 C7 H7A 109.5 C5 C7 H7B 109.5 H7A C7 H7B 109.5 C5 C7 H7C 109.5 H7A C7 H7C 109.5 H7B C7 H7C 109.5 C5 C8 H8A 109.5 C5 C8 H8B 109.5 H8A C8 H8B 109.5 C5 C8 H8C 109.5 H8A C8 H8C 109.5 H8B C8 H8C 109.5 O4 C9 C11 109.0(5) O4 C9 C10 111.1(5) C11 C9 C10 110.5(6) O4 C9 C12 105.3(5) C11 C9 C12 110.2(6) C10 C9 C12 110.6(6) C9 C10 H10A 109.5 C9 C10 H10B 109.5 H10A C10 H10B 109.5 C9 C10 H10C 109.5 H10A C10 H10C 109.5 H10B C10 H10C 109.5 C9 C11 H11A 109.5 C9 C11 H11B 109.5 H11A C11 H11B 109.5 C9 C11 H11C 109.5 H11A C11 H11C 109.5 H11B C11 H11C 109.5 C9 C12 H12A 109.5 C9 C12 H12B 109.5 H12A C12 H12B 109.5 C9 C12 H12C 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 O22 C21 C22 112.1(5) O22 C21 C23 107.3(5) C22 C21 C23 111.0(6) O22 C21 C24 105.3(5) C22 C21 C24 110.8(6) C23 C21 C24 110.1(5) C21 C22 H22A 109.5 C21 C22 H22B 109.5 H22A C22 H22B 109.5 C21 C22 H22C 109.5 H22A C22 H22C 109.5 H22B C22 H22C 109.5 C21 C23 H23A 109.5 C21 C23 H23B 109.5 H23A C23 H23B 109.5 C21 C23 H23C 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 C21 C24 H24A 109.5 C21 C24 H24B 109.5 H24A C24 H24B 109.5 C21 C24 H24C 109.5 H24A C24 H24C 109.5 H24B C24 H24C 109.5 O23 C25 C26 111.3(5) O23 C25 C28 105.6(5) C26 C25 C28 110.8(5) O23 C25 C27 108.8(5) C26 C25 C27 110.8(5) C28 C25 C27 109.4(5) C25 C26 H26A 109.5 C25 C26 H26B 109.5 H26A C26 H26B 109.5 C25 C26 H26C 109.5 H26A C26 H26C 109.5 H26B C26 H26C 109.5 C25 C27 H27A 109.5 C25 C27 H27B 109.5 H27A C27 H27B 109.5 C25 C27 H27C 109.5 H27A C27 H27C 109.5 H27B C27 H27C 109.5 C25 C28 H28A 109.5 C25 C28 H28B 109.5 H28A C28 H28B 109.5 C25 C28 H28C 109.5 H28A C28 H28C 109.5 H28B C28 H28C 109.5 O24 C29 C31 110.1(5) O24 C29 C32 106.3(5) C31 C29 C32 110.3(7) O24 C29 C30 109.8(5) C31 C29 C30 110.8(7) C32 C29 C30 109.5(6) C29 C30 H30A 109.5 C29 C30 H30B 109.5 H30A C30 H30B 109.5 C29 C30 H30C 109.5 H30A C30 H30C 109.5 H30B C30 H30C 109.5 C29 C31 H31A 109.5 C29 C31 H31B 109.5 H31A C31 H31B 109.5 C29 C31 H31C 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 C29 C32 H32A 109.5 C29 C32 H32B 109.5 H32A C32 H32B 109.5 C29 C32 H32C 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 O42 C41 C42 105.5(5) O42 C41 C44 108.4(5) C42 C41 C44 111.1(6) O42 C41 C43 110.2(5) C42 C41 C43 110.3(6) C44 C41 C43 111.2(6) C41 C42 H42A 109.5 C41 C42 H42B 109.5 H42A C42 H42B 109.5 C41 C42 H42C 109.5 H42A C42 H42C 109.5 H42B C42 H42C 109.5 C41 C43 H43A 109.5 C41 C43 H43B 109.5 H43A C43 H43B 109.5 C41 C43 H43C 109.5 H43A C43 H43C 109.5 H43B C43 H43C 109.5 C41 C44 H44A 109.5 C41 C44 H44B 109.5 H44A C44 H44B 109.5 C41 C44 H44C 109.5 H44A C44 H44C 109.5 H44B C44 H44C 109.5 O43 C45 C47 110.5(5) O43 C45 C46 108.7(5) C47 C45 C46 112.3(6) O43 C45 C48 105.2(5) C47 C45 C48 110.0(5) C46 C45 C48 109.9(6) C45 C46 H46A 109.5 C45 C46 H46B 109.5 H46A C46 H46B 109.5 C45 C46 H46C 109.5 H46A C46 H46C 109.5 H46B C46 H46C 109.5 C45 C47 H47A 109.5 C45 C47 H47B 109.5 H47A C47 H47B 109.5 C45 C47 H47C 109.5 H47A C47 H47C 109.5 H47B C47 H47C 109.5 C45 C48 H48A 109.5 C45 C48 H48B 109.5 H48A C48 H48B 109.5 C45 C48 H48C 109.5 H48A C48 H48C 109.5 H48B C48 H48C 109.5 O44 C49 C50 109.6(5) O44 C49 C51 105.4(5) C50 C49 C51 110.2(6) O44 C49 C52 110.1(5) C50 C49 C52 110.8(6) C51 C49 C52 110.6(5) C49 C50 H50A 109.5 C49 C50 H50B 109.5 H50A C50 H50B 109.5 C49 C50 H50C 109.5 H50A C50 H50C 109.5 H50B C50 H50C 109.5 C49 C51 H51A 109.5 C49 C51 H51B 109.5 H51A C51 H51B 109.5 C49 C51 H51C 109.5 H51A C51 H51C 109.5 H51B C51 H51C 109.5 C49 C52 H52A 109.5 C49 C52 H52B 109.5 H52A C52 H52B 109.5 C49 C52 H52C 109.5 H52A C52 H52C 109.5 H52B C52 H52C 109.5 O62 C61 C63 110.2(6) O62 C61 C62 103.3(5) C63 C61 C62 110.8(6) O62 C61 C64 112.3(5) C63 C61 C64 110.7(6) C62 C61 C64 109.3(6) C61 C62 H62A 109.5 C61 C62 H62B 109.5 H62A C62 H62B 109.5 C61 C62 H62C 109.5 H62A C62 H62C 109.5 H62B C62 H62C 109.5 C61 C63 H63A 109.5 C61 C63 H63B 109.5 H63A C63 H63B 109.5 C61 C63 H63C 109.5 H63A C63 H63C 109.5 H63B C63 H63C 109.5 C61 C64 H64A 109.5 C61 C64 H64B 109.5 H64A C64 H64B 109.5 C61 C64 H64C 109.5 H64A C64 H64C 109.5 H64B C64 H64C 109.5 O63 C65 C67 110.3(5) O63 C65 C68 112.7(5) C67 C65 C68 112.7(6) O63 C65 C66 101.1(6) C67 C65 C66 108.4(6) C68 C65 C66 111.0(6) C65 C66 H66A 109.5 C65 C66 H66B 109.5 H66A C66 H66B 109.5 C65 C66 H66C 109.5 H66A C66 H66C 109.5 H66B C66 H66C 109.5 C65 C67 H67A 109.5 C65 C67 H67B 109.5 H67A C67 H67B 109.5 C65 C67 H67C 109.5 H67A C67 H67C 109.5 H67B C67 H67C 109.5 C65 C68 H68A 109.5 C65 C68 H68B 109.5 H68A C68 H68B 109.5 C65 C68 H68C 109.5 H68A C68 H68C 109.5 H68B C68 H68C 109.5 O64 C69 C72 113.6(5) O64 C69 C71 103.0(5) C72 C69 C71 109.3(5) O64 C69 C70 109.2(5) C72 C69 C70 110.7(5) C71 C69 C70 110.7(5) C69 C70 H70A 109.5 C69 C70 H70B 109.5 H70A C70 H70B 109.5 C69 C70 H70C 109.5 H70A C70 H70C 109.5 H70B C70 H70C 109.5 C69 C71 H71A 109.5 C69 C71 H71B 109.5 H71A C71 H71B 109.5 C69 C71 H71C 109.5 H71A C71 H71C 109.5 H71B C71 H71C 109.5 C69 C72 H72A 109.5 C69 C72 H72B 109.5 H72A C72 H72B 109.5 C69 C72 H72C 109.5 H72A C72 H72C 109.5 H72B C72 H72C 109.5 O67B K2 O65A 132.7(4) O67B K2 O68B 106.4(6) O65A K2 O68B 108.2(4) O67B K2 N2B 65.5(4) O65A K2 N2B 103.3(4) O68B K2 N2B 63.6(7) O67B K2 O66A 85.2(4) O65A K2 O66A 63.5(3) O68B K2 O66A 90.6(6) N2B K2 O66A 42.4(4) O67B K2 O69 61.2(3) O65A K2 O69 104.6(2) O68B K2 O69 142.1(5) N2B K2 O69 125.7(3) O66A K2 O69 121.3(2) O67B K2 O70 127.2(3) O65A K2 O70 98.2(2) O68B K2 O70 59.0(6) N2B K2 O70 122.4(3) O66A K2 O70 138.88(19) O69 K2 O70 98.28(14) O67B K2 N1A 122.9(4) O65A K2 N1A 63.6(3) O68B K2 N1A 118.5(7) N2B K2 N1A 166.9(4) O66A K2 N1A 125.2(3) O69 K2 N1A 61.7(3) O70 K2 N1A 62.3(3) O67B K2 O66B 99.9(4) O65A K2 O66B 41.9(3) O68B K2 O66B 102.0(6) N2B K2 O66B 64.3(4) O66A K2 O66B 22.2(3) O69 K2 O66B 115.1(2) O70 K2 O66B 131.7(3) N1A K2 O66B 103.1(4) O67B K2 O68A 99.1(5) O65A K2 O68A 116.2(4) O68B K2 O68A 8.1(6) N2B K2 O68A 62.2(6) O66A K2 O68A 93.5(5) O69 K2 O68A 135.5(4) O70 K2 O68A 60.4(5) N1A K2 O68A 121.9(6) O66B K2 O68A 107.2(5) O67B K2 O67A 11.7(4) O65A K2 O67A 143.5(3) O68B K2 O67A 101.2(5) N2B K2 O67A 70.9(4) O66A K2 O67A 95.8(3) O69 K2 O67A 59.0(2) O70 K2 O67A 115.5(2) N1A K2 O67A 119.4(3) O66B K2 O67A 111.5(3) O68A K2 O67A 93.4(4) O67B K2 O65B 133.0(4) O65A K2 O65B 16.9(3) O68B K2 O65B 117.5(5) N2B K2 O65B 119.7(4) O66A K2 O65B 78.6(4) O69 K2 O65B 90.6(3) O70 K2 O65B 91.2(3) N1A K2 O65B 47.3(4) O66B K2 O65B 56.5(4) O68A K2 O65B 125.5(4) O67A K2 O65B 140.8(4) C75A O65A C74A 112.1(15) C75A O65A K2 118.6(13) C74A O65A K2 115.8(9) C77A O66A C76A 109.7(10) C77A O66A K2 121.7(10) C76A O66A K2 104.4(7) C82A O67A C81A 110.9(12) C82A O67A K2 121.7(9) C81A O67A K2 111.6(9) C90 O68A C85A 112.2(16) C90 O68A K2 113.5(14) C85A O68A K2 122.7(15) C73A N1A C84A 109.6(12) C73A N1A C79A 109.0(11) C84A N1A C79A 109.3(11) C73A N1A K2 109.1(8) C84A N1A K2 110.0(9) C79A N1A K2 109.9(9) C83A N2A C78A 110.0(12) C83A N2A C86A 107.2(13) C78A N2A C86A 111.6(11) C83A N2A K2 111.9(7) C78A N2A K2 106.0(9) C86A N2A K2 110.3(9) N1A C73A C74A 112.7(12) N1A C73A H73A 109.0 C74A C73A H73A 109.0 N1A C73A H73B 109.0 C74A C73A H73B 109.0 H73A C73A H73B 107.8 O65A C74A C73A 109.1(12) C73A C74A K2 81.8(8) O65A C74A H74A 109.9 C73A C74A H74A 109.9 K2 C74A H74A 90.3 O65A C74A H74B 109.9 C73A C74A H74B 109.9 K2 C74A H74B 151.9 H74A C74A H74B 108.3 O65A C75A C76A 110(2) C76A C75A K2 76.0(11) O65A C75A H75A 109.7 C76A C75A H75A 109.7 K2 C75A H75A 145.6 O65A C75A H75B 109.7 C76A C75A H75B 109.7 K2 C75A H75B 100.9 H75A C75A H75B 108.2 O66A C76A C75A 108.7(14) O66A C76A K2 51.6(5) C75A C76A K2 78.8(10) O66A C76A H76A 109.9 C75A C76A H76A 109.9 K2 C76A H76A 161.5 O66A C76A H76B 109.9 C75A C76A H76B 109.9 K2 C76A H76B 82.5 H76A C76A H76B 108.3 O66A C77A C78A 110.1(11) O66A C77A H77A 109.6 C78A C77A H77A 109.6 O66A C77A H77B 109.6 C78A C77A H77B 109.6 H77A C77A H77B 108.2 N2A C78A C77A 111.8(12) N2A C78A H78A 109.2 C77A C78A H78A 109.2 N2A C78A H78B 109.2 C77A C78A H78B 109.2 H78A C78A H78B 107.9 N1A C79A C80A 113.4(14) N1A C79A H79A 108.9 C80A C79A H79A 108.9 N1A C79A H79B 108.9 C80A C79A H79B 108.9 H79A C79A H79B 107.7 O69 C80A C79A 111.2(15) O69 C80A H80A 109.4 C79A C80A H80A 109.4 O69 C80A H80B 109.4 C79A C80A H80B 109.4 H80A C80A H80B 108.0 C87 C81A O67A 108.1(13) C87 C81A H81A 110.1 O67A C81A H81A 110.1 C87 C81A H81B 110.1 O67A C81A H81B 110.1 H81A C81A H81B 108.4 O67A C82A C83A 108.0(12) O67A C82A H82A 110.1 C83A C82A H82A 110.1 O67A C82A H82B 110.1 C83A C82A H82B 110.1 H82A C82A H82B 108.4 N2A C83A C82A 113.6(12) N2A C83A H83A 108.8 C82A C83A H83A 108.8 N2A C83A H83B 108.8 C82A C83A H83B 108.8 H83A C83A H83B 107.7 N1A C84A C88 118.6(11) N1A C84A H84A 107.7 C88 C84A H84A 107.7 N1A C84A H84B 107.7 C88 C84A H84B 107.7 H84A C84A H84B 107.1 O68A C85A C86A 109.5(17) O68A C85A H85A 109.8 C86A C85A H85A 109.8 O68A C85A H85B 109.8 C86A C85A H85B 109.8 H85A C85A H85B 108.2 C85A C86A N2A 112.5(14) C85A C86A H86A 109.1 N2A C86A H86A 109.1 C85A C86A H86B 109.1 N2A C86A H86B 109.1 H86A C86A H86B 107.8 C75B O65B C74B 111.1(13) C75B O65B K2 113.1(11) C74B O65B K2 119.0(9) C76B O66B C77B 110.0(17) C76B O66B K2 119.5(12) C77B O66B K2 108.3(10) C82B O67B C81B 110.5(15) C82B O67B K2 116.7(11) C81B O67B K2 116.5(11) C85B O68B C90 110.8(15) C85B O68B K2 113.8(17) C90 O68B K2 115.7(15) C73B N1B C84B 110.1(15) C73B N1B C79B 110.4(14) C84B N1B C79B 108.1(14) C73B N1B K2 113.5(10) C84B N1B K2 107.3(11) C79B N1B K2 107.1(10) C83B N2B C86B 109.1(15) C83B N2B C78B 106.1(16) C86B N2B C78B 112.8(14) C83B N2B K2 107.4(10) C86B N2B K2 111.1(9) C78B N2B K2 110.0(13) N1B C73B C74B 112.6(14) N1B C73B H73C 109.1 C74B C73B H73C 109.1 N1B C73B H73D 109.1 C74B C73B H73D 109.1 H73C C73B H73D 107.8 O65B C74B C73B 109.6(13) O65B C74B H74C 109.7 C73B C74B H74C 109.7 O65B C74B H74D 109.7 C73B C74B H74D 109.7 H74C C74B H74D 108.2 O65B C75B C76B 107.0(17) O65B C75B H75C 110.3 C76B C75B H75C 110.3 O65B C75B H75D 110.3 C76B C75B H75D 110.3 H75C C75B H75D 108.6 O66B C76B C75B 111(2) O66B C76B H76C 109.5 C75B C76B H76C 109.5 O66B C76B H76D 109.5 C75B C76B H76D 109.5 H76C C76B H76D 108.1 O66B C77B C78B 108.3(17) O66B C77B H77C 110.0 C78B C77B H77C 110.0 O66B C77B H77D 110.0 C78B C77B H77D 110.0 H77C C77B H77D 108.4 N2B C78B C77B 108.2(19) N2B C78B H78C 110.1 C77B C78B H78C 110.1 N2B C78B H78D 110.1 C77B C78B H78D 110.1 H78C C78B H78D 108.4 N1B C79B C80B 113.3(17) N1B C79B H79C 108.9 C80B C79B H79C 108.9 N1B C79B H79D 108.9 C80B C79B H79D 108.9 H79C C79B H79D 107.7 O69 C80B C79B 108.0(15) O69 C80B H80C 110.1 C79B C80B H80C 110.1 O69 C80B H80D 110.1 C79B C80B H80D 110.1 H80C C80B H80D 108.4 O67B C81B C87 109.1(15) C87 C81B K2 82.2(9) O67B C81B H81C 109.9 C87 C81B H81C 109.9 K2 C81B H81C 151.2 O67B C81B H81D 109.9 C87 C81B H81D 109.9 K2 C81B H81D 90.7 H81C C81B H81D 108.3 O67B C82B C83B 107.8(14) C83B C82B K2 76.7(10) O67B C82B H82C 110.1 C83B C82B H82C 110.1 K2 C82B H82C 96.2 O67B C82B H82D 110.1 C83B C82B H82D 110.1 K2 C82B H82D 149.2 H82C C82B H82D 108.5 N2B C83B C82B 115.0(15) N2B C83B K2 49.8(7) C82B C83B K2 77.6(9) N2B C83B H83C 108.5 C82B C83B H83C 108.5 K2 C83B H83C 92.0 N2B C83B H83D 108.5 C82B C83B H83D 108.5 K2 C83B H83D 155.6 H83C C83B H83D 107.5 N1B C84B C88 105.7(13) N1B C84B H84C 110.6 C88 C84B H84C 110.6 N1B C84B H84D 110.6 C88 C84B H84D 110.6 H84C C84B H84D 108.7 O68B C85B C86B 110.0(16) O68B C85B H85C 109.7 C86B C85B H85C 109.7 O68B C85B H85D 109.7 C86B C85B H85D 109.7 H85C C85B H85D 108.2 C85B C86B N2B 115.4(13) C85B C86B H86C 108.4 N2B C86B H86C 108.4 C85B C86B H86D 108.4 N2B C86B H86D 108.4 H86C C86B H86D 107.5 C80A O69 C87 117.5(10) C87 O69 C80B 104.3(11) C80A O69 K2 116.6(11) C87 O69 K2 115.8(4) C80B O69 K2 118.4(12) C88 O70 C89 110.4(5) C88 O70 K2 118.6(4) C89 O70 K2 114.7(3) O69 C87 C81A 118.8(9) O69 C87 C81B 101.0(10) O69 C87 H87A 107.6 C81A C87 H87A 107.6 C81B C87 H87A 107.6 O69 C87 H87B 107.6 C81A C87 H87B 107.6 C81B C87 H87B 124.9 H87A C87 H87B 107.1 O69 C87 H87C 111.6 C81A C87 H87C 109.3 C81B C87 H87C 111.6 H87B C87 H87C 100.3 O69 C87 H87D 111.6 C81A C87 H87D 94.9 C81B C87 H87D 111.6 H87A C87 H87D 116.3 H87C C87 H87D 109.4 O70 C88 C84A 107.9(8) O70 C88 C84B 109.0(10) O70 C88 H88A 110.1 C84A C88 H88A 110.1 C84B C88 H88A 124.9 O70 C88 H88B 110.1 C84A C88 H88B 110.1 C84B C88 H88B 92.5 H88A C88 H88B 108.4 O70 C88 H88C 109.9 C84A C88 H88C 93.2 C84B C88 H88C 109.9 H88B C88 H88C 123.6 O70 C88 H88D 109.9 C84A C88 H88D 125.9 C84B C88 H88D 109.9 H88A C88 H88D 91.4 H88C C88 H88D 108.3 O70 C89 C90 109.7(5) O70 C89 H89A 109.7 C90 C89 H89A 109.7 O70 C89 H89B 109.7 C90 C89 H89B 109.7 H89A C89 H89B 108.2 O68A C90 C89 116.5(10) O68B C90 C89 102.5(10) O68A C90 H90A 108.2 O68B C90 H90A 107.3 C89 C90 H90A 108.2 O68A C90 H90B 108.2 O68B C90 H90B 122.7 C89 C90 H90B 108.2 H90A C90 H90B 107.3 O68A C90 H90C 110.5 O68B C90 H90C 111.3 C89 C90 H90C 111.3 H90B C90 H90C 101.0 O68A C90 H90D 97.2 O68B C90 H90D 111.3 C89 C90 H90D 111.3 H90A C90 H90D 115.5 H90C C90 H90D 109.2 C92 C91 H91A 109.5 C92 C91 H91B 109.5 H91A C91 H91B 109.5 C92 C91 H91C 109.5 H91A C91 H91C 109.5 H91B C91 H91C 109.5 C91 C92 C93 120.4(14) C91 C92 H92A 107.2 C93 C92 H92A 107.2 C91 C92 H92B 107.2 C93 C92 H92B 107.2 H92A C92 H92B 106.9 C92 C93 C94 119.7(14) C92 C93 H93A 107.4 C94 C93 H93A 107.4 C92 C93 H93B 107.4 C94 C93 H93B 107.4 H93A C93 H93B 106.9 C95 C94 C93 126.3(18) C95 C94 H94A 105.7 C93 C94 H94A 105.7 C95 C94 H94B 105.7 C93 C94 H94B 105.7 H94A C94 H94B 106.2 C96A C95 C96B 68(2) C96A C95 C94 114(2) C96B C95 C94 140(2) C96A C95 H95A 108.8 C96B C95 H95A 107.7 C94 C95 H95A 108.8 C96A C95 H95B 108.8 C94 C95 H95B 108.8 H95A C95 H95B 107.7 C96B C95 H95C 102.0 C94 C95 H95C 102.0 H95A C95 H95C 75.6 H95B C95 H95C 145.6 C96A C95 H95D 134.2 C96B C95 H95D 102.0 C94 C95 H95D 102.0 H95B C95 H95D 83.9 H95C C95 H95D 104.8 C95 C96A H96A 109.5 C95 C96A H96B 109.5 C95 C96A H96C 109.5 C95 C96B H96D 109.5 C95 C96B H96E 109.5 H96D C96B H96E 109.5 C95 C96B H96F 109.5 H96D C96B H96F 109.5 H96E C96B H96F 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance U1 O61 2.197(4) U1 O21 2.229(4) U1 O1 2.264(4) U1 O41 2.275(4) U1 S1 2.5220(14) U1 K1 3.5828(13) K1 O23 2.694(4) K1 O42 2.705(4) K1 O4 2.735(4) K1 O41 2.799(4) K1 O1 2.867(4) K1 O21 2.917(4) K1 Si3 3.4213(19) K1 Si2 3.480(2) K1 Si1 3.4801(19) Si1 O1 1.579(4) Si1 O3 1.620(4) Si1 O2 1.640(4) Si1 O4 1.660(4) Si2 O21 1.590(4) Si2 O22 1.630(4) Si2 O24 1.633(4) Si2 O23 1.657(4) Si3 O41 1.587(4) Si3 O44 1.633(4) Si3 O43 1.637(4) Si3 O42 1.663(4) Si4 O61 1.590(4) Si4 O63 1.626(5) Si4 O62 1.627(4) Si4 O64 1.641(5) O2 C1 1.434(7) O3 C5 1.445(6) O4 C9 1.451(7) O22 C21 1.452(7) O23 C25 1.448(6) O24 C29 1.434(7) O42 C41 1.454(7) O43 C45 1.443(7) O44 C49 1.445(7) O62 C61 1.436(7) O63 C65 1.453(7) O64 C69 1.451(7) C1 C3 1.514(10) C1 C2 1.525(9) C1 C4 1.530(9) C2 H2A 0.9800 C2 H2B 0.9800 C2 H2C 0.9800 C3 H3A 0.9800 C3 H3B 0.9800 C3 H3C 0.9800 C4 H4A 0.9800 C4 H4B 0.9800 C4 H4C 0.9800 C5 C8 1.519(9) C5 C6 1.520(8) C5 C7 1.525(8) C6 H6A 0.9800 C6 H6B 0.9800 C6 H6C 0.9800 C7 H7A 0.9800 C7 H7B 0.9800 C7 H7C 0.9800 C8 H8A 0.9800 C8 H8B 0.9800 C8 H8C 0.9800 C9 C11 1.523(10) C9 C10 1.526(9) C9 C12 1.533(9) C10 H10A 0.9800 C10 H10B 0.9800 C10 H10C 0.9800 C11 H11A 0.9800 C11 H11B 0.9800 C11 H11C 0.9800 C12 H12A 0.9800 C12 H12B 0.9800 C12 H12C 0.9800 C21 C22 1.516(9) C21 C23 1.517(8) C21 C24 1.527(8) C22 H22A 0.9800 C22 H22B 0.9800 C22 H22C 0.9800 C23 H23A 0.9800 C23 H23B 0.9800 C23 H23C 0.9800 C24 H24A 0.9800 C24 H24B 0.9800 C24 H24C 0.9800 C25 C26 1.522(9) C25 C28 1.526(9) C25 C27 1.535(8) C26 H26A 0.9800 C26 H26B 0.9800 C26 H26C 0.9800 C27 H27A 0.9800 C27 H27B 0.9800 C27 H27C 0.9800 C28 H28A 0.9800 C28 H28B 0.9800 C28 H28C 0.9800 C29 C31 1.494(10) C29 C32 1.518(9) C29 C30 1.523(9) C30 H30A 0.9800 C30 H30B 0.9800 C30 H30C 0.9800 C31 H31A 0.9800 C31 H31B 0.9800 C31 H31C 0.9800 C32 H32A 0.9800 C32 H32B 0.9800 C32 H32C 0.9800 C41 C42 1.513(9) C41 C44 1.514(9) C41 C43 1.531(9) C42 H42A 0.9800 C42 H42B 0.9800 C42 H42C 0.9800 C43 H43A 0.9800 C43 H43B 0.9800 C43 H43C 0.9800 C44 H44A 0.9800 C44 H44B 0.9800 C44 H44C 0.9800 C45 C47 1.517(8) C45 C46 1.524(9) C45 C48 1.526(8) C46 H46A 0.9800 C46 H46B 0.9800 C46 H46C 0.9800 C47 H47A 0.9800 C47 H47B 0.9800 C47 H47C 0.9800 C48 H48A 0.9800 C48 H48B 0.9800 C48 H48C 0.9800 C49 C50 1.517(9) C49 C51 1.527(9) C49 C52 1.528(9) C50 H50A 0.9800 C50 H50B 0.9800 C50 H50C 0.9800 C51 H51A 0.9800 C51 H51B 0.9800 C51 H51C 0.9800 C52 H52A 0.9800 C52 H52B 0.9800 C52 H52C 0.9800 C61 C63 1.499(10) C61 C62 1.527(10) C61 C64 1.533(8) C62 H62A 0.9800 C62 H62B 0.9800 C62 H62C 0.9800 C63 H63A 0.9800 C63 H63B 0.9800 C63 H63C 0.9800 C64 H64A 0.9800 C64 H64B 0.9800 C64 H64C 0.9800 C65 C67 1.497(9) C65 C68 1.501(9) C65 C66 1.542(10) C66 H66A 0.9800 C66 H66B 0.9800 C66 H66C 0.9800 C67 H67A 0.9800 C67 H67B 0.9800 C67 H67C 0.9800 C68 H68A 0.9800 C68 H68B 0.9800 C68 H68C 0.9800 C69 C72 1.511(8) C69 C71 1.514(9) C69 C70 1.526(8) C70 H70A 0.9800 C70 H70B 0.9800 C70 H70C 0.9800 C71 H71A 0.9800 C71 H71B 0.9800 C71 H71C 0.9800 C72 H72A 0.9800 C72 H72B 0.9800 C72 H72C 0.9800 K2 O67B 2.621(15) K2 O65A 2.640(8) K2 O68B 2.78(3) K2 N2B 2.802(12) K2 O66A 2.818(8) K2 O69 2.819(5) K2 O70 2.831(4) K2 N1A 2.861(13) K2 O66B 2.885(10) K2 O68A 2.89(3) K2 O67A 2.995(11) K2 O65B 3.100(14) O65A C75A 1.39(2) O65A C74A 1.440(16) O66A C77A 1.38(2) O66A C76A 1.461(17) O67A C82A 1.422(17) O67A C81A 1.43(2) O68A C90 1.38(3) O68A C85A 1.41(2) N1A C73A 1.468(18) N1A C84A 1.473(19) N1A C79A 1.488(18) N2A C83A 1.47(2) N2A C78A 1.481(18) N2A C86A 1.491(19) C73A C74A 1.50(2) C73A H73A 0.9900 C73A H73B 0.9900 C74A H74A 0.9900 C74A H74B 0.9900 C75A C76A 1.53(3) C75A H75A 0.9900 C75A H75B 0.9900 C76A H76A 0.9900 C76A H76B 0.9900 C77A C78A 1.54(2) C77A H77A 0.9900 C77A H77B 0.9900 C78A H78A 0.9900 C78A H78B 0.9900 C79A C80A 1.49(2) C79A H79A 0.9900 C79A H79B 0.9900 C80A O69 1.36(2) C80A H80A 0.9900 C80A H80B 0.9900 C81A C87 1.42(2) C81A H81A 0.9900 C81A H81B 0.9900 C82A C83A 1.53(2) C82A H82A 0.9900 C82A H82B 0.9900 C83A H83A 0.9900 C83A H83B 0.9900 C84A C88 1.52(2) C84A H84A 0.9900 C84A H84B 0.9900 C85A C86A 1.49(2) C85A H85A 0.9900 C85A H85B 0.9900 C86A H86A 0.9900 C86A H86B 0.9900 O65B C75B 1.42(2) O65B C74B 1.44(2) O66B C76B 1.38(4) O66B C77B 1.40(2) O67B C82B 1.44(2) O67B C81B 1.45(3) O68B C85B 1.45(3) O68B C90 1.47(3) N1B C73B 1.46(2) N1B C84B 1.48(2) N1B C79B 1.51(2) N2B C83B 1.42(3) N2B C86B 1.490(19) N2B C78B 1.52(3) C73B C74B 1.49(2) C73B H73C 0.9900 C73B H73D 0.9900 C74B H74C 0.9900 C74B H74D 0.9900 C75B C76B 1.54(3) C75B H75C 0.9900 C75B H75D 0.9900 C76B H76C 0.9900 C76B H76D 0.9900 C77B C78B 1.60(4) C77B H77C 0.9900 C77B H77D 0.9900 C78B H78C 0.9900 C78B H78D 0.9900 C79B C80B 1.51(3) C79B H79C 0.9900 C79B H79D 0.9900 C80B O69 1.50(3) C80B H80C 0.9900 C80B H80D 0.9900 C81B C87 1.59(2) C81B H81C 0.9900 C81B H81D 0.9900 C82B C83B 1.56(3) C82B H82C 0.9900 C82B H82D 0.9900 C83B H83C 0.9900 C83B H83D 0.9900 C84B C88 1.57(2) C84B H84C 0.9900 C84B H84D 0.9900 C85B C86B 1.48(2) C85B H85C 0.9900 C85B H85D 0.9900 C86B H86C 0.9900 C86B H86D 0.9900 O69 C87 1.408(8) O70 C88 1.411(8) O70 C89 1.435(7) C87 H87A 0.9900 C87 H87B 0.9900 C87 H87C 0.9900 C87 H87D 0.9900 C88 H88A 0.9900 C88 H88B 0.9900 C88 H88C 0.9900 C88 H88D 0.9900 C89 C90 1.478(9) C89 H89A 0.9900 C89 H89B 0.9900 C90 H90A 0.9900 C90 H90B 0.9900 C90 H90C 0.9900 C90 H90D 0.9900 C91 C92 1.419(18) C91 H91A 0.9800 C91 H91B 0.9800 C91 H91C 0.9800 C92 C93 1.46(2) C92 H92A 0.9900 C92 H92B 0.9900 C93 C94 1.49(2) C93 H93A 0.9900 C93 H93B 0.9900 C94 C95 1.36(2) C94 H94A 0.9900 C94 H94B 0.9900 C95 C96A 1.30(2) C95 C96B 1.35(2) C95 H95A 0.9900 C95 H95B 0.9900 C95 H95C 0.9900 C95 H95D 0.9900 C96A H96A 0.9800 C96A H96B 0.9800 C96A H96C 0.9800 C96B H96D 0.9800 C96B H96E 0.9800 C96B H96F 0.9800 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O61 U1 K1 O23 -109.44(18) O21 U1 K1 O23 -0.69(15) O1 U1 K1 O23 135.00(16) O41 U1 K1 O23 -114.35(15) S1 U1 K1 O23 69.10(11) O61 U1 K1 O42 1.23(19) O21 U1 K1 O42 109.99(15) O1 U1 K1 O42 -114.32(16) O41 U1 K1 O42 -3.67(15) S1 U1 K1 O42 179.78(10) O61 U1 K1 O4 129.75(19) O21 U1 K1 O4 -121.49(15) O1 U1 K1 O4 14.20(16) O41 U1 K1 O4 124.85(15) S1 U1 K1 O4 -51.70(11) O61 U1 K1 O41 4.9(2) O21 U1 K1 O41 113.66(17) O1 U1 K1 O41 -110.65(18) S1 U1 K1 O41 -176.55(13) O61 U1 K1 O1 115.6(2) O21 U1 K1 O1 -135.69(18) O41 U1 K1 O1 110.65(18) S1 U1 K1 O1 -65.90(14) O61 U1 K1 O21 -108.8(2) O1 U1 K1 O21 135.69(18) O41 U1 K1 O21 -113.66(17) S1 U1 K1 O21 69.79(13) O61 U1 K1 Si3 3.56(17) O21 U1 K1 Si3 112.31(12) O1 U1 K1 Si3 -112.00(14) O41 U1 K1 Si3 -1.35(12) S1 U1 K1 Si3 -177.90(6) O61 U1 K1 Si2 -111.98(16) O21 U1 K1 Si2 -3.22(12) O1 U1 K1 Si2 132.47(14) O41 U1 K1 Si2 -116.88(12) S1 U1 K1 Si2 66.57(6) O61 U1 K1 Si1 121.98(16) O21 U1 K1 Si1 -129.27(12) O1 U1 K1 Si1 6.42(13) O41 U1 K1 Si1 117.08(13) S1 U1 K1 Si1 -59.47(6) O23 K1 Si1 O1 -83.6(2) O42 K1 Si1 O1 72.2(2) O4 K1 Si1 O1 -172.2(3) O41 K1 Si1 O1 25.4(2) O21 K1 Si1 O1 -37.8(2) Si3 K1 Si1 O1 47.06(19) Si2 K1 Si1 O1 -59.69(19) U1 K1 Si1 O1 -9.07(19) O23 K1 Si1 O3 13.5(2) O42 K1 Si1 O3 169.3(2) O4 K1 Si1 O3 -75.2(3) O41 K1 Si1 O3 122.5(2) O1 K1 Si1 O3 97.0(3) O21 K1 Si1 O3 59.2(2) Si3 K1 Si1 O3 144.1(2) Si2 K1 Si1 O3 37.4(2) U1 K1 Si1 O3 88.0(2) O23 K1 Si1 O2 178.8(2) O42 K1 Si1 O2 -25.4(2) O4 K1 Si1 O2 90.1(3) O41 K1 Si1 O2 -72.2(2) O1 K1 Si1 O2 -97.6(3) O21 K1 Si1 O2 -135.5(2) Si3 K1 Si1 O2 -50.56(19) Si2 K1 Si1 O2 -157.31(18) U1 K1 Si1 O2 -106.69(19) O23 K1 Si1 O4 88.7(2) O42 K1 Si1 O4 -115.5(2) O41 K1 Si1 O4 -162.3(2) O1 K1 Si1 O4 172.2(3) O21 K1 Si1 O4 134.4(2) Si3 K1 Si1 O4 -140.7(2) Si2 K1 Si1 O4 112.5(2) U1 K1 Si1 O4 163.2(2) O23 K1 Si2 O21 -170.1(3) O42 K1 Si2 O21 -80.44(19) O4 K1 Si2 O21 83.81(19) O41 K1 Si2 O21 -30.16(18) O1 K1 Si2 O21 32.23(19) Si3 K1 Si2 O21 -53.23(17) Si1 K1 Si2 O21 55.05(17) U1 K1 Si2 O21 4.41(16) O23 K1 Si2 O22 90.0(3) O42 K1 Si2 O22 179.7(2) O4 K1 Si2 O22 -16.1(2) O41 K1 Si2 O22 -130.0(2) O1 K1 Si2 O22 -67.6(2) O21 K1 Si2 O22 -99.9(3) Si3 K1 Si2 O22 -153.11(19) Si1 K1 Si2 O22 -44.83(19) U1 K1 Si2 O22 -95.47(19) O23 K1 Si2 O24 -72.7(3) O42 K1 Si2 O24 17.0(2) O4 K1 Si2 O24 -178.7(2) O41 K1 Si2 O24 67.3(2) O1 K1 Si2 O24 129.7(2) O21 K1 Si2 O24 97.5(3) Si3 K1 Si2 O24 44.2(2) Si1 K1 Si2 O24 152.50(19) U1 K1 Si2 O24 101.87(19) O42 K1 Si2 O23 89.7(2) O4 K1 Si2 O23 -106.1(2) O41 K1 Si2 O23 140.0(2) O1 K1 Si2 O23 -157.7(2) O21 K1 Si2 O23 170.1(3) Si3 K1 Si2 O23 116.9(2) Si1 K1 Si2 O23 -134.8(2) U1 K1 Si2 O23 174.5(2) O23 K1 Si3 O41 85.0(2) O42 K1 Si3 O41 177.0(3) O4 K1 Si3 O41 -74.2(2) O1 K1 Si3 O41 -34.13(19) O21 K1 Si3 O41 37.13(19) Si2 K1 Si3 O41 58.55(18) Si1 K1 Si3 O41 -53.37(18) U1 K1 Si3 O41 1.87(17) O23 K1 Si3 O44 -173.5(2) O42 K1 Si3 O44 -81.5(3) O4 K1 Si3 O44 27.3(2) O41 K1 Si3 O44 101.5(3) O1 K1 Si3 O44 67.3(2) O21 K1 Si3 O44 138.6(2) Si2 K1 Si3 O44 160.02(18) Si1 K1 Si3 O44 48.10(19) U1 K1 Si3 O44 103.34(18) O23 K1 Si3 O43 -6.3(2) O42 K1 Si3 O43 85.7(3) O4 K1 Si3 O43 -165.5(2) O41 K1 Si3 O43 -91.3(3) O1 K1 Si3 O43 -125.4(2) O21 K1 Si3 O43 -54.2(2) Si2 K1 Si3 O43 -32.8(2) Si1 K1 Si3 O43 -144.7(2) U1 K1 Si3 O43 -89.4(2) O23 K1 Si3 O42 -92.0(2) O4 K1 Si3 O42 108.8(2) O41 K1 Si3 O42 -177.0(3) O1 K1 Si3 O42 148.8(2) O21 K1 Si3 O42 -139.9(2) Si2 K1 Si3 O42 -118.48(19) Si1 K1 Si3 O42 129.60(19) U1 K1 Si3 O42 -175.16(19) O3 Si1 O1 U1 -5.7(10) O2 Si1 O1 U1 -129.3(9) O4 Si1 O1 U1 110.1(9) K1 Si1 O1 U1 116.3(10) O3 Si1 O1 K1 -121.98(19) O2 Si1 O1 K1 114.4(2) O4 Si1 O1 K1 -6.2(2) O61 U1 O1 Si1 117.1(9) O21 U1 O1 Si1 -82.7(9) O41 U1 O1 Si1 -165.3(9) S1 U1 O1 Si1 15.9(9) K1 U1 O1 Si1 -117.6(10) O61 U1 O1 K1 -125.29(15) O21 U1 O1 K1 34.88(13) O41 U1 O1 K1 -47.71(12) S1 U1 O1 K1 133.48(8) O23 K1 O1 Si1 113.12(19) O42 K1 O1 Si1 -119.18(19) O4 K1 O1 Si1 4.45(16) O41 K1 O1 Si1 -151.2(2) O21 K1 O1 Si1 139.6(2) Si3 K1 O1 Si1 -134.36(18) Si2 K1 O1 Si1 124.71(17) U1 K1 O1 Si1 166.9(3) O23 K1 O1 U1 -53.77(17) O42 K1 O1 U1 73.93(15) O4 K1 O1 U1 -162.44(19) O41 K1 O1 U1 41.93(12) O21 K1 O1 U1 -27.34(11) Si3 K1 O1 U1 58.75(10) Si2 K1 O1 U1 -42.18(11) Si1 K1 O1 U1 -166.9(3) O1 Si1 O2 C1 -36.5(6) O3 Si1 O2 C1 -166.0(5) O4 Si1 O2 C1 80.6(5) K1 Si1 O2 C1 25.5(6) O1 Si1 O3 C5 -71.1(5) O2 Si1 O3 C5 56.7(5) O4 Si1 O3 C5 173.6(5) K1 Si1 O3 C5 -136.0(4) O1 Si1 O4 C9 -173.2(5) O3 Si1 O4 C9 -49.6(6) O2 Si1 O4 C9 63.9(6) K1 Si1 O4 C9 -179.8(6) O1 Si1 O4 K1 6.5(2) O3 Si1 O4 K1 130.17(19) O2 Si1 O4 K1 -116.36(19) O23 K1 O4 C9 70.1(5) O42 K1 O4 C9 -97.3(5) O41 K1 O4 C9 -161.0(5) O1 K1 O4 C9 175.5(5) O21 K1 O4 C9 130.0(5) Si3 K1 O4 C9 -132.4(5) Si2 K1 O4 C9 101.2(5) Si1 K1 O4 C9 179.8(6) U1 K1 O4 C9 164.5(5) O23 K1 O4 Si1 -109.7(2) O42 K1 O4 Si1 82.9(2) O41 K1 O4 Si1 19.2(2) O1 K1 O4 Si1 -4.28(16) O21 K1 O4 Si1 -49.8(2) Si3 K1 O4 Si1 47.8(2) Si2 K1 O4 Si1 -78.6(2) U1 K1 O4 Si1 -15.27(18) O22 Si2 O21 K1 113.8(2) O24 Si2 O21 K1 -122.35(19) O23 Si2 O21 K1 -7.7(2) O61 U1 O21 K1 127.47(15) O1 U1 O21 K1 -34.21(13) O41 U1 O21 K1 46.03(11) S1 U1 O21 K1 -131.56(7) O23 K1 O21 Si2 5.61(15) O42 K1 O21 Si2 109.16(17) O4 K1 O21 Si2 -107.94(18) O41 K1 O21 Si2 145.9(2) O1 K1 O21 Si2 -145.72(19) Si3 K1 O21 Si2 127.88(16) Si1 K1 O21 Si2 -128.81(15) U1 K1 O21 Si2 -173.5(2) O23 K1 O21 U1 179.15(18) O42 K1 O21 U1 -77.30(13) O4 K1 O21 U1 65.61(14) O41 K1 O21 U1 -40.56(11) O1 K1 O21 U1 27.82(11) Si3 K1 O21 U1 -58.58(9) Si2 K1 O21 U1 173.5(2) Si1 K1 O21 U1 44.73(10) O21 Si2 O22 C21 -45.2(6) O24 Si2 O22 C21 -174.4(5) O23 Si2 O22 C21 72.9(5) K1 Si2 O22 C21 19.3(6) O21 Si2 O23 C25 -158.7(5) O22 Si2 O23 C25 77.3(5) O24 Si2 O23 C25 -36.2(5) K1 Si2 O23 C25 -167.2(6) O21 Si2 O23 K1 8.5(2) O22 Si2 O23 K1 -115.5(2) O24 Si2 O23 K1 130.97(19) O42 K1 O23 C25 66.6(4) O4 K1 O23 C25 -102.8(4) O41 K1 O23 C25 125.8(4) O1 K1 O23 C25 -166.2(4) O21 K1 O23 C25 162.6(4) Si3 K1 O23 C25 97.2(4) Si2 K1 O23 C25 168.1(5) Si1 K1 O23 C25 -135.6(4) U1 K1 O23 C25 163.1(4) O42 K1 O23 Si2 -101.50(19) O4 K1 O23 Si2 89.1(2) O41 K1 O23 Si2 -42.3(2) O1 K1 O23 Si2 25.7(2) O21 K1 O23 Si2 -5.50(15) Si3 K1 O23 Si2 -70.88(19) Si1 K1 O23 Si2 56.3(2) U1 K1 O23 Si2 -4.98(18) O21 Si2 O24 C29 -70.9(5) O22 Si2 O24 C29 57.5(5) O23 Si2 O24 C29 174.4(5) K1 Si2 O24 C29 -137.6(4) O44 Si3 O41 K1 -111.7(2) O43 Si3 O41 K1 125.39(19) O42 Si3 O41 K1 2.4(2) O61 U1 O41 K1 -176.74(13) O21 U1 O41 K1 -48.53(12) O1 U1 O41 K1 49.22(12) O23 K1 O41 Si3 -104.84(18) O42 K1 O41 Si3 -1.72(15) O4 K1 O41 Si3 119.71(18) O1 K1 O41 Si3 141.1(2) O21 K1 O41 Si3 -137.8(2) Si2 K1 O41 Si3 -123.02(16) Si1 K1 O41 Si3 128.56(16) U1 K1 O41 Si3 -177.3(2) O23 K1 O41 U1 72.45(14) O42 K1 O41 U1 175.58(18) O4 K1 O41 U1 -62.99(15) O1 K1 O41 U1 -41.64(11) O21 K1 O41 U1 39.51(11) Si3 K1 O41 U1 177.3(2) Si2 K1 O41 U1 54.28(9) Si1 K1 O41 U1 -54.15(10) O41 Si3 O42 C41 -166.1(5) O44 Si3 O42 C41 -43.2(5) O43 Si3 O42 C41 69.7(5) K1 Si3 O42 C41 -163.6(6) O41 Si3 O42 K1 -2.5(2) O44 Si3 O42 K1 120.43(18) O43 Si3 O42 K1 -126.7(2) O23 K1 O42 C41 -96.0(4) O4 K1 O42 C41 72.4(4) O41 K1 O42 C41 166.3(5) O1 K1 O42 C41 131.6(4) O21 K1 O42 C41 -153.4(4) Si3 K1 O42 C41 164.7(5) Si2 K1 O42 C41 -125.5(4) Si1 K1 O42 C41 104.8(4) U1 K1 O42 C41 169.2(4) O23 K1 O42 Si3 99.32(19) O4 K1 O42 Si3 -92.3(2) O41 K1 O42 Si3 1.65(15) O1 K1 O42 Si3 -33.1(2) O21 K1 O42 Si3 41.9(2) Si2 K1 O42 Si3 69.76(19) Si1 K1 O42 Si3 -59.9(2) U1 K1 O42 Si3 4.46(18) O41 Si3 O43 C45 -39.4(5) O44 Si3 O43 C45 -168.4(5) O42 Si3 O43 C45 79.6(5) K1 Si3 O43 C45 22.8(6) O41 Si3 O44 C49 -75.1(5) O43 Si3 O44 C49 52.3(5) O42 Si3 O44 C49 170.1(4) K1 Si3 O44 C49 -137.5(4) O63 Si4 O61 U1 82.2(8) O62 Si4 O61 U1 -162.8(8) O64 Si4 O61 U1 -38.8(9) O21 U1 O61 Si4 117.7(8) O1 U1 O61 Si4 -87.5(8) O41 U1 O61 Si4 -162.5(8) S1 U1 O61 Si4 14.8(8) K1 U1 O61 Si4 -166.3(7) O61 Si4 O62 C61 -156.9(6) O63 Si4 O62 C61 -36.8(7) O64 Si4 O62 C61 76.6(7) O61 Si4 O63 C65 -64.9(6) O62 Si4 O63 C65 177.2(5) O64 Si4 O63 C65 60.9(6) O61 Si4 O64 C69 -56.9(5) O63 Si4 O64 C69 178.7(5) O62 Si4 O64 C69 66.4(5) Si1 O2 C1 C3 80.3(6) Si1 O2 C1 C2 -41.3(8) Si1 O2 C1 C4 -161.3(5) Si1 O3 C5 C8 132.6(5) Si1 O3 C5 C6 13.3(7) Si1 O3 C5 C7 -109.6(6) Si1 O4 C9 C11 82.4(6) K1 O4 C9 C11 -97.4(6) Si1 O4 C9 C10 -39.7(8) K1 O4 C9 C10 140.6(4) Si1 O4 C9 C12 -159.4(5) K1 O4 C9 C12 20.9(8) Si2 O22 C21 C22 -10.9(8) Si2 O22 C21 C23 111.1(5) Si2 O22 C21 C24 -131.6(5) Si2 O23 C25 C26 -40.6(7) K1 O23 C25 C26 154.7(4) Si2 O23 C25 C28 -160.9(4) K1 O23 C25 C28 34.3(6) Si2 O23 C25 C27 81.7(6) K1 O23 C25 C27 -83.0(5) Si2 O24 C29 C31 -78.1(7) Si2 O24 C29 C32 162.5(5) Si2 O24 C29 C30 44.1(8) Si3 O42 C41 C42 -158.4(5) K1 O42 C41 C42 41.7(7) Si3 O42 C41 C44 82.5(7) K1 O42 C41 C44 -77.4(6) Si3 O42 C41 C43 -39.4(7) K1 O42 C41 C43 160.7(4) Si3 O43 C45 C47 -40.5(7) Si3 O43 C45 C46 83.2(6) Si3 O43 C45 C48 -159.1(4) Si3 O44 C49 C50 -77.2(7) Si3 O44 C49 C51 164.3(4) Si3 O44 C49 C52 44.9(7) Si4 O62 C61 C63 92.0(7) Si4 O62 C61 C62 -149.5(5) Si4 O62 C61 C64 -31.9(9) Si4 O63 C65 C67 -85.4(7) Si4 O63 C65 C68 41.5(8) Si4 O63 C65 C66 160.0(5) Si4 O64 C69 C72 22.2(7) Si4 O64 C69 C71 140.4(5) Si4 O64 C69 C70 -101.9(5) O67B K2 O65A C75A -49.0(16) O68B K2 O65A C75A 86.0(16) N2B K2 O65A C75A 19.8(16) O66A K2 O65A C75A 4.8(15) O69 K2 O65A C75A -113.2(15) O70 K2 O65A C75A 146.0(15) N1A K2 O65A C75A -160.6(16) O66B K2 O65A C75A -1.8(15) O68A K2 O65A C75A 85.1(16) O67A K2 O65A C75A -56.1(16) O65B K2 O65A C75A -148(2) O67B K2 O65A C74A 88.6(11) O68B K2 O65A C74A -136.4(12) N2B K2 O65A C74A 157.4(11) O66A K2 O65A C74A 142.4(11) O69 K2 O65A C74A 24.4(11) O70 K2 O65A C74A -76.4(10) N1A K2 O65A C74A -23.0(10) O66B K2 O65A C74A 135.8(12) O68A K2 O65A C74A -137.3(12) O67A K2 O65A C74A 81.5(11) O65B K2 O65A C74A -10.2(16) O67B K2 O66A C77A -63.9(9) O65A K2 O66A C77A 152.6(9) O68B K2 O66A C77A 42.4(10) N2B K2 O66A C77A -5.6(9) O69 K2 O66A C77A -115.9(9) O70 K2 O66A C77A 81.8(9) N1A K2 O66A C77A 168.6(9) O66B K2 O66A C77A 164.4(13) O68A K2 O66A C77A 34.9(10) O67A K2 O66A C77A -58.9(9) O65B K2 O66A C77A 160.4(9) O67B K2 O66A C76A 171.6(9) O65A K2 O66A C76A 28.1(8) O68B K2 O66A C76A -82.1(10) N2B K2 O66A C76A -130.1(10) O69 K2 O66A C76A 119.6(8) O70 K2 O66A C76A -42.7(10) N1A K2 O66A C76A 44.1(10) O66B K2 O66A C76A 39.9(9) O68A K2 O66A C76A -89.6(9) O67A K2 O66A C76A 176.6(9) O65B K2 O66A C76A 35.9(9) O67B K2 O67A C82A 58(2) O65A K2 O67A C82A 84.5(12) O68B K2 O67A C82A -59.0(12) N2B K2 O67A C82A -2.2(10) O66A K2 O67A C82A 32.7(11) O69 K2 O67A C82A 156.0(11) O70 K2 O67A C82A -119.8(10) N1A K2 O67A C82A 169.0(10) O66B K2 O67A C82A 48.9(11) O68A K2 O67A C82A -61.2(12) O65B K2 O67A C82A 111.8(11) O67B K2 O67A C81A -76(2) O65A K2 O67A C81A -49.6(11) O68B K2 O67A C81A 166.9(11) N2B K2 O67A C81A -136.2(10) O66A K2 O67A C81A -101.3(9) O69 K2 O67A C81A 21.9(9) O70 K2 O67A C81A 106.1(9) N1A K2 O67A C81A 34.9(10) O66B K2 O67A C81A -85.2(10) O68A K2 O67A C81A 164.8(10) O65B K2 O67A C81A -22.3(12) O67B K2 O68A C90 -119.2(10) O65A K2 O68A C90 93.0(10) O68B K2 O68A C90 86(8) N2B K2 O68A C90 -175.2(12) O66A K2 O68A C90 155.1(10) O69 K2 O68A C90 -61.4(12) O70 K2 O68A C90 8.6(8) N1A K2 O68A C90 19.1(12) O66B K2 O68A C90 137.3(10) O67A K2 O68A C90 -108.9(10) O65B K2 O68A C90 76.5(12) O67B K2 O68A C85A 21.0(18) O65A K2 O68A C85A -126.7(15) O68B K2 O68A C85A -133(9) N2B K2 O68A C85A -35.0(16) O66A K2 O68A C85A -64.6(17) O69 K2 O68A C85A 78.9(19) O70 K2 O68A C85A 148.9(18) N1A K2 O68A C85A 159.4(15) O66B K2 O68A C85A -82.4(17) O67A K2 O68A C85A 31.4(17) O65B K2 O68A C85A -143.2(15) O67B K2 N1A C73A -134.7(9) O65A K2 N1A C73A -9.1(8) O68B K2 N1A C73A 88.2(10) N2B K2 N1A C73A -8(2) O66A K2 N1A C73A -25.1(11) O69 K2 N1A C73A -135.1(10) O70 K2 N1A C73A 107.0(9) O66B K2 N1A C73A -23.5(10) O68A K2 N1A C73A 96.7(10) O67A K2 N1A C73A -147.8(8) O65B K2 N1A C73A -14.2(8) O67B K2 N1A C84A 105.1(10) O65A K2 N1A C84A -129.4(10) O68B K2 N1A C84A -32.0(11) N2B K2 N1A C84A -127.9(18) O66A K2 N1A C84A -145.4(8) O69 K2 N1A C84A 104.6(9) O70 K2 N1A C84A -13.3(8) O66B K2 N1A C84A -143.8(9) O68A K2 N1A C84A -23.6(11) O67A K2 N1A C84A 91.9(9) O65B K2 N1A C84A -134.4(11) O67B K2 N1A C79A -15.3(11) O65A K2 N1A C79A 110.3(10) O68B K2 N1A C79A -152.4(9) N2B K2 N1A C79A 111.8(19) O66A K2 N1A C79A 94.3(9) O69 K2 N1A C79A -15.7(8) O70 K2 N1A C79A -133.6(10) O66B K2 N1A C79A 95.9(9) O68A K2 N1A C79A -143.9(9) O67A K2 N1A C79A -28.4(10) O65B K2 N1A C79A 105.3(10) O67B K2 N2A C83A -31.8(9) O65A K2 N2A C83A -154.6(9) O68B K2 N2A C83A 110.5(11) N2B K2 N2A C83A -156.8(19) O66A K2 N2A C83A -139.8(10) O69 K2 N2A C83A -26.9(10) O70 K2 N2A C83A 86.9(10) O66B K2 N2A C83A -140.7(10) O68A K2 N2A C83A 102.4(11) O67A K2 N2A C83A -17.9(9) O65B K2 N2A C83A -149.0(9) O67B K2 N2A C78A 88.0(9) O65A K2 N2A C78A -34.7(9) O68B K2 N2A C78A -129.7(10) N2B K2 N2A C78A -37.0(12) O66A K2 N2A C78A -19.9(7) O69 K2 N2A C78A 92.9(8) O70 K2 N2A C78A -153.3(7) O66B K2 N2A C78A -20.8(8) O68A K2 N2A C78A -137.7(10) O67A K2 N2A C78A 101.9(9) O65B K2 N2A C78A -29.1(11) O67B K2 N2A C86A -151.0(13) O65A K2 N2A C86A 86.2(11) O68B K2 N2A C86A -8.7(11) N2B K2 N2A C86A 84.0(17) O66A K2 N2A C86A 101.0(11) O69 K2 N2A C86A -146.2(10) O70 K2 N2A C86A -32.3(12) O66B K2 N2A C86A 100.1(11) O68A K2 N2A C86A -16.8(11) O67A K2 N2A C86A -137.2(12) O65B K2 N2A C86A 91.8(12) C84A N1A C73A C74A 159.9(13) C79A N1A C73A C74A -80.5(15) K2 N1A C73A C74A 39.5(14) C75A O65A C74A C73A -166.6(17) K2 O65A C74A C73A 53.1(16) C75A O65A C74A K2 140.3(18) N1A C73A C74A O65A -62.7(18) N1A C73A C74A K2 -29.6(10) O67B K2 C74A O65A -110.0(10) O68B K2 C74A O65A 51.4(13) N2B K2 C74A O65A -26.5(12) O66A K2 C74A O65A -33.5(10) O69 K2 C74A O65A -156.3(10) O70 K2 C74A O65A 105.6(10) N1A K2 C74A O65A 149.9(13) O66B K2 C74A O65A -32.9(9) O68A K2 C74A O65A 53.5(13) O67A K2 C74A O65A -122.7(9) O65B K2 C74A O65A 30(5) O67B K2 C74A C73A 119.7(9) O65A K2 C74A C73A -130.2(17) O68B K2 C74A C73A -78.9(12) N2B K2 C74A C73A -156.8(8) O66A K2 C74A C73A -163.7(10) O69 K2 C74A C73A 73.4(9) O70 K2 C74A C73A -24.6(9) N1A K2 C74A C73A 19.6(8) O66B K2 C74A C73A -163.1(11) O68A K2 C74A C73A -76.8(12) O67A K2 C74A C73A 107.0(9) O65B K2 C74A C73A -100(6) C74A O65A C75A C76A -175.6(17) K2 O65A C75A C76A -37(2) C74A O65A C75A K2 -139.1(17) O67B K2 C75A O65A 141.1(13) O68B K2 C75A O65A -100.1(15) N2B K2 C75A O65A -160.7(15) O66A K2 C75A O65A -173.7(19) O69 K2 C75A O65A 73.1(15) O70 K2 C75A O65A -37.5(16) N1A K2 C75A O65A 17.5(14) O66B K2 C75A O65A 177(3) O68A K2 C75A O65A -104.1(15) O67A K2 C75A O65A 140.1(12) O65B K2 C75A O65A 15.4(10) O67B K2 C75A C76A -74.3(13) O65A K2 C75A C76A 145(2) O68B K2 C75A C76A 44.5(14) N2B K2 C75A C76A -16.0(12) O66A K2 C75A C76A -29.0(9) O69 K2 C75A C76A -142.2(11) O70 K2 C75A C76A 107.1(11) N1A K2 C75A C76A 162.2(13) O66B K2 C75A C76A -38.5(10) O68A K2 C75A C76A 40.5(14) O67A K2 C75A C76A -75.2(14) O65B K2 C75A C76A 160.1(19) C77A O66A C76A C75A 170.1(15) K2 O66A C76A C75A -58.0(14) C77A O66A C76A K2 -131.9(13) O65A C75A C76A O66A 67(2) K2 C75A C76A O66A 42.7(9) O65A C75A C76A K2 23.9(16) O67B K2 C76A O66A -8.9(10) O65A K2 C76A O66A -142.0(10) O68B K2 C76A O66A 97.5(10) N2B K2 C76A O66A 36.5(8) O69 K2 C76A O66A -76.8(9) O70 K2 C76A O66A 149.2(7) N1A K2 C76A O66A -143.6(8) O66B K2 C76A O66A -65.2(13) O68A K2 C76A O66A 91.8(9) O67A K2 C76A O66A -3.9(10) O65B K2 C76A O66A -138.3(10) O67B K2 C76A C75A 116.2(13) O65A K2 C76A C75A -17.0(12) O68B K2 C76A C75A -137.5(14) N2B K2 C76A C75A 161.6(14) O66A K2 C76A C75A 125.0(16) O69 K2 C76A C75A 48.3(13) O70 K2 C76A C75A -85.7(13) N1A K2 C76A C75A -18.5(13) O66B K2 C76A C75A 59.8(19) O68A K2 C76A C75A -143.1(13) O67A K2 C76A C75A 121.2(13) O65B K2 C76A C75A -13.2(13) C76A O66A C77A C78A 166.5(12) K2 O66A C77A C78A 44.4(16) C83A N2A C78A C77A 171.2(11) C86A N2A C78A C77A -70.0(16) K2 N2A C78A C77A 50.1(12) O66A C77A C78A N2A -65.7(17) C73A N1A C79A C80A 164.8(14) C84A N1A C79A C80A -75.5(17) K2 N1A C79A C80A 45.3(16) N1A C79A C80A O69 -62(2) C82A O67A C81A C87 172.7(12) K2 O67A C81A C87 -48.2(13) C81A O67A C82A C83A 177.5(13) K2 O67A C82A C83A 43.2(15) C78A N2A C83A C82A -68.6(14) C86A N2A C83A C82A 169.9(12) K2 N2A C83A C82A 48.8(14) O67A C82A C83A N2A -61.4(16) C73A N1A C84A C88 -77.4(15) C79A N1A C84A C88 163.3(12) K2 N1A C84A C88 42.6(14) C90 O68A C85A C86A -174.2(17) K2 O68A C85A C86A 45(2) O68A C85A C86A N2A -61(2) C83A N2A C86A C85A -75.1(17) C78A N2A C86A C85A 164.4(15) K2 N2A C86A C85A 46.9(18) O67B K2 O65B C75B -52.7(13) O65A K2 O65B C75B 44.4(11) O68B K2 O65B C75B 104.2(12) N2B K2 O65B C75B 30.4(12) O66A K2 O65B C75B 19.6(10) O69 K2 O65B C75B -102.3(10) O70 K2 O65B C75B 159.4(10) N1A K2 O65B C75B -151.3(13) O66B K2 O65B C75B 17.8(10) O68A K2 O65B C75B 105.8(12) O67A K2 O65B C75B -65.6(12) O67B K2 O65B C74B 80.4(13) O65A K2 O65B C74B 178(2) O68B K2 O65B C74B -122.7(13) N2B K2 O65B C74B 163.5(11) O66A K2 O65B C74B 152.7(12) O69 K2 O65B C74B 30.8(11) O70 K2 O65B C74B -67.5(11) N1A K2 O65B C74B -18.2(10) O66B K2 O65B C74B 150.9(13) O68A K2 O65B C74B -121.2(12) O67A K2 O65B C74B 67.5(13) O67B K2 O66B C76B 154.2(18) O65A K2 O66B C76B 7.4(18) O68B K2 O66B C76B -96.5(19) N2B K2 O66B C76B -149.2(19) O66A K2 O66B C76B -157(2) O69 K2 O66B C76B 91.5(18) O70 K2 O66B C76B -37.6(19) N1A K2 O66B C76B 26.9(18) O68A K2 O66B C76B -102.9(19) O67A K2 O66B C76B 156.2(18) O65B K2 O66B C76B 18.7(18) O67B K2 O66B C77B -78.8(13) O65A K2 O66B C77B 134.4(14) O68B K2 O66B C77B 30.5(14) N2B K2 O66B C77B -22.2(12) O66A K2 O66B C77B -29.7(11) O69 K2 O66B C77B -141.6(12) O70 K2 O66B C77B 89.4(13) N1A K2 O66B C77B 153.8(12) O68A K2 O66B C77B 24.1(14) O67A K2 O66B C77B -76.8(13) O65B K2 O66B C77B 145.6(13) O65A K2 O67B C82B 68.9(13) O68B K2 O67B C82B -66.8(14) N2B K2 O67B C82B -16.7(12) O66A K2 O67B C82B 22.4(12) O69 K2 O67B C82B 152.2(13) O70 K2 O67B C82B -129.9(11) N1A K2 O67B C82B 151.8(12) O66B K2 O67B C82B 39.0(13) O68A K2 O67B C82B -70.4(13) O67A K2 O67B C82B -132(3) O65B K2 O67B C82B 92.0(13) O65A K2 O67B C81B -64.7(13) O68B K2 O67B C81B 159.6(13) N2B K2 O67B C81B -150.3(13) O66A K2 O67B C81B -111.2(12) O69 K2 O67B C81B 18.6(11) O70 K2 O67B C81B 96.5(12) N1A K2 O67B C81B 18.2(14) O66B K2 O67B C81B -94.6(12) O68A K2 O67B C81B 156.0(13) O67A K2 O67B C81B 94(3) O65B K2 O67B C81B -41.7(14) O67B K2 O68B C85B 31.4(14) O65A K2 O68B C85B -115.9(12) N2B K2 O68B C85B -19.7(12) O66A K2 O68B C85B -53.8(13) O69 K2 O68B C85B 95.3(16) O70 K2 O68B C85B 155.4(14) N1A K2 O68B C85B 174.8(11) O66B K2 O68B C85B -72.9(13) O68A K2 O68B C85B 58(7) O67A K2 O68B C85B 42.2(14) O65B K2 O68B C85B -131.2(11) O67B K2 O68B C90 -98.7(12) O65A K2 O68B C90 114.0(11) N2B K2 O68B C90 -149.8(13) O66A K2 O68B C90 176.2(12) O69 K2 O68B C90 -34.7(18) O70 K2 O68B C90 25.3(10) N1A K2 O68B C90 44.8(13) O66B K2 O68B C90 157.1(11) O68A K2 O68B C90 -72(7) O67A K2 O68B C90 -87.8(12) O65B K2 O68B C90 98.7(11) O67B K2 N1B C73B -137.4(11) O65A K2 N1B C73B -8.4(11) O68B K2 N1B C73B 93.3(12) O66A K2 N1B C73B -23.9(14) O69 K2 N1B C73B -129.5(12) O70 K2 N1B C73B 105.0(12) N1A K2 N1B C73B -21(3) O66B K2 N1B C73B -22.0(13) O68A K2 N1B C73B 102.0(12) O67A K2 N1B C73B -149.4(11) O65B K2 N1B C73B -13.5(10) O67B K2 N1B C84B 100.7(12) O65A K2 N1B C84B -130.3(12) O68B K2 N1B C84B -28.6(13) O66A K2 N1B C84B -145.8(11) O69 K2 N1B C84B 108.6(12) O70 K2 N1B C84B -16.9(11) N1A K2 N1B C84B -143(5) O66B K2 N1B C84B -143.9(11) O68A K2 N1B C84B -20.0(13) O67A K2 N1B C84B 88.7(12) O65B K2 N1B C84B -135.4(13) O67B K2 N1B C79B -15.2(12) O65A K2 N1B C79B 113.8(11) O68B K2 N1B C79B -144.5(11) O66A K2 N1B C79B 98.3(11) O69 K2 N1B C79B -7.3(9) O70 K2 N1B C79B -132.8(11) N1A K2 N1B C79B 101(4) O66B K2 N1B C79B 100.2(11) O68A K2 N1B C79B -135.9(11) O67A K2 N1B C79B -27.2(12) O65B K2 N1B C79B 108.7(12) O67B K2 N2B C83B -15.2(11) O65A K2 N2B C83B -146.4(12) O68B K2 N2B C83B 109.6(13) O66A K2 N2B C83B -126.5(13) O69 K2 N2B C83B -27.1(13) O70 K2 N2B C83B 104.7(11) N1A K2 N2B C83B -147.8(18) O66B K2 N2B C83B -130.6(13) O68A K2 N2B C83B 100.7(13) O67A K2 N2B C83B -4.0(11) O65B K2 N2B C83B -142.3(12) O67B K2 N2B C86B -134.5(12) O65A K2 N2B C86B 94.3(11) O68B K2 N2B C86B -9.7(11) O66A K2 N2B C86B 114.2(13) O69 K2 N2B C86B -146.4(10) O70 K2 N2B C86B -14.6(13) N1A K2 N2B C86B 93(2) O66B K2 N2B C86B 110.1(12) O68A K2 N2B C86B -18.6(11) O67A K2 N2B C86B -123.3(12) O65B K2 N2B C86B 98.4(11) O67B K2 N2B C78B 99.8(13) O65A K2 N2B C78B -31.4(13) O68B K2 N2B C78B -135.3(14) O66A K2 N2B C78B -11.4(11) O69 K2 N2B C78B 87.9(13) O70 K2 N2B C78B -140.3(12) N1A K2 N2B C78B -33(3) O66B K2 N2B C78B -15.6(12) O68A K2 N2B C78B -144.3(14) O67A K2 N2B C78B 111.0(13) O65B K2 N2B C78B -27.2(14) C84B N1B C73B C74B 165.6(14) C79B N1B C73B C74B -75.1(18) K2 N1B C73B C74B 45.2(16) C75B O65B C74B C73B -175.1(13) K2 O65B C74B C73B 50.9(16) N1B C73B C74B O65B -64.3(18) C74B O65B C75B C76B 176.0(19) K2 O65B C75B C76B -47.2(19) C77B O66B C76B C75B -178.0(18) K2 O66B C76B C75B -52(3) O65B C75B C76B O66B 66(3) C76B O66B C77B C78B -172(2) K2 O66B C77B C78B 56.0(17) C83B N2B C78B C77B 164.7(15) C86B N2B C78B C77B -76(2) K2 N2B C78B C77B 48.8(17) O66B C77B C78B N2B -74.8(19) C73B N1B C79B C80B 164.1(16) C84B N1B C79B C80B -75(2) K2 N1B C79B C80B 40.0(17) N1B C79B C80B O69 -67(2) C82B O67B C81B C87 170.7(14) K2 O67B C81B C87 -53.0(16) C82B O67B C81B K2 -136.3(18) O65A K2 C81B O67B 129.2(11) O68B K2 C81B O67B -24.5(16) N2B K2 C81B O67B 26.9(12) O66A K2 C81B O67B 68.5(12) O69 K2 C81B O67B -154.8(15) O70 K2 C81B O67B -100.0(12) N1A K2 C81B O67B -164.4(12) O66B K2 C81B O67B 89.4(12) O68A K2 C81B O67B -27.3(14) O67A K2 C81B O67B -28.4(10) O65B K2 C81B O67B 147.4(11) O67B K2 C81B C87 130.4(17) O65A K2 C81B C87 -100.4(8) O68B K2 C81B C87 105.8(11) N2B K2 C81B C87 157.3(9) O66A K2 C81B C87 -161.2(9) O69 K2 C81B C87 -24.4(6) O70 K2 C81B C87 30.3(11) N1A K2 C81B C87 -34.1(10) O66B K2 C81B C87 -140.2(8) O68A K2 C81B C87 103.1(10) O67A K2 C81B C87 102.0(13) O65B K2 C81B C87 -82.3(9) C81B O67B C82B C83B -179.9(16) K2 O67B C82B C83B 43.9(18) C81B O67B C82B K2 136.2(18) O65A K2 C82B O67B -125.8(12) O68B K2 C82B O67B 117.3(13) N2B K2 C82B O67B 158.3(15) O66A K2 C82B O67B -155.3(13) O69 K2 C82B O67B -24.4(12) O70 K2 C82B O67B 67.4(14) N1A K2 C82B O67B -39.0(15) O66B K2 C82B O67B -141.4(13) O68A K2 C82B O67B 111.5(13) O67A K2 C82B O67B 17.3(11) O65B K2 C82B O67B -107.2(13) O67B K2 C82B C83B -137.3(19) O65A K2 C82B C83B 96.9(11) O68B K2 C82B C83B -20.0(12) N2B K2 C82B C83B 21.0(10) O66A K2 C82B C83B 67.4(11) O69 K2 C82B C83B -161.7(11) O70 K2 C82B C83B -69.9(12) N1A K2 C82B C83B -176.3(10) O66B K2 C82B C83B 81.4(11) O68A K2 C82B C83B -25.8(12) O67A K2 C82B C83B -120.0(15) O65B K2 C82B C83B 115.5(11) C86B N2B C83B C82B 165.8(14) C78B N2B C83B C82B -72.3(19) K2 N2B C83B C82B 45.3(18) C86B N2B C83B K2 120.6(14) C78B N2B C83B K2 -117.6(15) O67B C82B C83B N2B -62(2) K2 C82B C83B N2B -33.8(14) O67B C82B C83B K2 -28.4(12) O67B K2 C83B N2B 159.8(15) O65A K2 C83B N2B 39.2(13) O68B K2 C83B N2B -62.0(12) O66A K2 C83B N2B 39.6(11) O69 K2 C83B N2B 157.4(11) O70 K2 C83B N2B -90.7(12) N1A K2 C83B N2B 148.9(17) O66B K2 C83B N2B 44.0(11) O68A K2 C83B N2B -69.1(12) O67A K2 C83B N2B 174.9(14) O65B K2 C83B N2B 50.2(14) O67B K2 C83B C82B 21.0(10) O65A K2 C83B C82B -99.5(11) O68B K2 C83B C82B 159.2(13) N2B K2 C83B C82B -138.8(19) O66A K2 C83B C82B -99.1(11) O69 K2 C83B C82B 18.7(12) O70 K2 C83B C82B 130.5(10) N1A K2 C83B C82B 10(3) O66B K2 C83B C82B -94.8(11) O68A K2 C83B C82B 152.1(13) O67A K2 C83B C82B 36.1(10) O65B K2 C83B C82B -88.5(12) C73B N1B C84B C88 -75.2(17) C79B N1B C84B C88 164.1(13) K2 N1B C84B C88 48.8(14) C90 O68B C85B C86B -180.0(16) K2 O68B C85B C86B 47.5(17) O68B C85B C86B N2B -60(2) C83B N2B C86B C85B -78.5(18) C78B N2B C86B C85B 163.9(18) K2 N2B C86B C85B 39.8(18) C79A C80A O69 C87 -171.5(11) C79A C80A O69 C80B 145(8) C79A C80A O69 K2 44.4(18) C79B C80B O69 C80A -29(6) C79B C80B O69 C87 -169.9(15) C79B C80B O69 K2 60(2) O67B K2 O69 C80A 165.3(10) O65A K2 O69 C80A -63.6(10) O68B K2 O69 C80A 85.8(13) N2B K2 O69 C80A 177.7(10) O66A K2 O69 C80A -131.2(10) O70 K2 O69 C80A 37.2(9) N1A K2 O69 C80A -15.1(10) O66B K2 O69 C80A -107.0(10) O68A K2 O69 C80A 92.8(12) O67A K2 O69 C80A 152.0(10) O65B K2 O69 C80A -54.2(10) O67B K2 O69 C87 20.6(6) O65A K2 O69 C87 151.7(5) O68B K2 O69 C87 -58.9(11) N2B K2 O69 C87 33.0(7) O66A K2 O69 C87 84.1(6) O70 K2 O69 C87 -107.5(5) N1A K2 O69 C87 -159.8(6) O66B K2 O69 C87 108.3(6) O68A K2 O69 C87 -51.9(9) O67A K2 O69 C87 7.3(5) O65B K2 O69 C87 161.1(6) O67B K2 O69 C80B 145.7(11) O65A K2 O69 C80B -83.3(10) O68B K2 O69 C80B 66.1(14) N2B K2 O69 C80B 158.0(11) O66A K2 O69 C80B -150.8(10) O70 K2 O69 C80B 17.5(10) N1A K2 O69 C80B -34.8(11) O66B K2 O69 C80B -126.6(11) O68A K2 O69 C80B 73.1(12) O67A K2 O69 C80B 132.4(11) O65B K2 O69 C80B -73.8(11) O67B K2 O70 C88 -127.3(6) O65A K2 O70 C88 38.9(5) O68B K2 O70 C88 145.3(6) N2B K2 O70 C88 150.4(6) O66A K2 O70 C88 97.5(6) O69 K2 O70 C88 -67.3(4) N1A K2 O70 C88 -15.5(5) O66B K2 O70 C88 67.4(6) O68A K2 O70 C88 154.5(6) O67A K2 O70 C88 -126.8(5) O65B K2 O70 C88 23.5(5) O67B K2 O70 C89 99.3(5) O65A K2 O70 C89 -94.5(4) O68B K2 O70 C89 11.8(5) N2B K2 O70 C89 17.0(6) O66A K2 O70 C89 -35.9(5) O69 K2 O70 C89 159.3(4) N1A K2 O70 C89 -148.9(5) O66B K2 O70 C89 -66.0(5) O68A K2 O70 C89 21.1(5) O67A K2 O70 C89 99.8(4) O65B K2 O70 C89 -109.9(5) C80A O69 C87 C81A 175.9(15) C80B O69 C87 C81A -171.7(16) K2 O69 C87 C81A -39.7(12) C80A O69 C87 C81B 166.1(15) C80B O69 C87 C81B 178.5(15) K2 O69 C87 C81B -49.5(11) O67A C81A C87 O69 61.4(15) O67A C81A C87 C81B 91(4) O67B C81B C87 O69 66.1(15) K2 C81B C87 O69 33.6(6) O67B C81B C87 C81A -88(5) K2 C81B C87 C81A -121(5) C89 O70 C88 C84A 175.3(7) K2 O70 C88 C84A 40.0(8) C89 O70 C88 C84B -164.6(8) K2 O70 C88 C84B 60.2(9) N1A C84A C88 O70 -56.8(15) N1A C84A C88 C84B -153(5) N1B C84B C88 O70 -74.2(15) N1B C84B C88 C84A 16(3) C88 O70 C89 C90 175.1(5) K2 O70 C89 C90 -47.7(6) C85A O68A C90 O68B 145(9) K2 O68A C90 O68B -71(7) C85A O68A C90 C89 177.2(14) K2 O68A C90 C89 -38.3(13) C85B O68B C90 O68A -38(7) K2 O68B C90 O68A 93(8) C85B O68B C90 C89 170.9(15) K2 O68B C90 C89 -57.6(11) O70 C89 C90 O68A 59.2(13) O70 C89 C90 O68B 68.0(12) C91 C92 C93 C94 174.2(16) C92 C93 C94 C95 -169(2) C93 C94 C95 C96A -73(3) C93 C94 C95 C96B -156(3) loop_ _publcif_info_exptl_table_extra_item sin_theta_over_lambda_max