#------------------------------------------------------------------------------ #$Date: 2016-11-02 04:35:01 +0200 (Wed, 02 Nov 2016) $ #$Revision: 187748 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/44/1544437.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1544437 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.7947 _cell_length_b 14.2221 _cell_length_c 18.7864 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.7473 _cod_data_source_file bx4004Isup2.hkl _cod_data_source_block I _shelx_title ' Pbca in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.88 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6291.32 5313.52 70.34 o 4 0 0 24018.61 23775.62 309.91 o 6 0 0 19395.14 19624.45 271.23 o 8 0 0 6653.06 6650.75 96.82 o 10 0 0 747.44 753.62 23.79 o 12 0 0 1520.64 1499.42 61.13 o 14 0 0 3.22 -36.07 95.67 o 2 1 0 51969.53 47529.95 1949.74 o 4 1 0 2670.85 2487.89 25.73 o 6 1 0 1239.89 1467.09 19.02 o 8 1 0 29.95 21.25 9.01 o 10 1 0 1858.49 1859.08 34.99 o 12 1 0 1.66 18.41 28.88 o 14 1 0 276.22 194.35 80.81 o 0 2 0 4304.20 3536.94 45.93 o 2 2 0 604.09 639.75 10.13 o 4 2 0 443.60 401.79 7.32 o 6 2 0 573.11 711.72 12.73 o 8 2 0 5372.03 5762.92 61.68 o 10 2 0 679.21 699.66 19.14 o 12 2 0 222.55 274.10 25.45 o 14 2 0 150.05 147.57 78.72 o 2 3 0 5269.29 5180.70 50.70 o 4 3 0 3.69 18.46 4.26 o 6 3 0 50.97 123.17 8.62 o 8 3 0 2250.25 2378.84 30.61 o 10 3 0 5.00 13.12 12.48 o 12 3 0 53.96 71.99 27.95 o 14 3 0 1.21 -66.24 66.24 o 0 4 0 2585.16 2422.73 35.55 o 2 4 0 115.23 110.42 3.65 o 4 4 0 106.48 105.35 7.50 o 6 4 0 5922.96 5896.47 71.63 o 8 4 0 2932.85 2679.27 35.25 o 10 4 0 9.25 -1.09 16.08 o 12 4 0 7.53 1.35 26.56 o 14 4 0 1.76 62.35 67.94 o 2 5 0 1393.06 1399.20 14.61 o 4 5 0 19.37 19.57 7.66 o 6 5 0 9.97 9.41 11.16 o 8 5 0 159.88 145.99 10.39 o 10 5 0 2449.76 2251.91 38.40 o 12 5 0 629.85 632.13 26.64 o 14 5 0 0.09 22.20 46.12 o 0 6 0 57940.42 53786.74 638.33 o 2 6 0 381.46 477.43 8.94 o 4 6 0 6847.33 6472.93 73.66 o 6 6 0 12116.84 12190.80 139.21 o 8 6 0 882.69 843.12 22.16 o 10 6 0 44.96 48.69 18.94 o 12 6 0 3128.04 2872.74 70.01 o 14 6 0 13.92 232.58 82.16 o 2 7 0 24.42 30.83 6.70 o 4 7 0 460.62 524.16 12.27 o 6 7 0 269.22 285.95 16.40 o 8 7 0 30.90 8.08 17.98 o 10 7 0 1854.18 1733.97 36.82 o 12 7 0 607.40 523.98 35.37 o 14 7 0 107.44 123.12 99.07 o 0 8 0 16098.43 15539.42 197.37 o 2 8 0 2579.88 2402.73 27.26 o 4 8 0 4646.94 4489.11 47.88 o 6 8 0 55.22 74.50 16.77 o 8 8 0 1790.60 1793.71 38.32 o 10 8 0 115.15 105.39 18.93 o 12 8 0 205.47 154.90 39.78 o 14 8 0 381.17 373.01 122.90 o 2 9 0 5478.31 5873.31 53.78 o 4 9 0 278.12 272.33 11.44 o 6 9 0 2020.13 2108.35 37.51 o 8 9 0 101.73 143.81 23.37 o 10 9 0 1043.73 948.19 39.54 o 12 9 0 89.71 18.33 33.79 o 0 10 0 12.60 57.42 19.44 o 2 10 0 156.24 183.68 11.54 o 4 10 0 136.58 175.06 16.18 o 6 10 0 892.30 872.61 25.90 o 8 10 0 59.16 99.65 26.35 o 10 10 0 42.48 19.48 46.94 o 12 10 0 457.83 435.89 60.89 o 2 11 0 1490.50 1525.70 24.75 o 4 11 0 135.95 177.23 16.43 o 6 11 0 478.47 419.77 22.97 o 8 11 0 331.53 288.10 22.88 o 10 11 0 379.44 409.60 44.79 o 12 11 0 0.49 -29.92 62.85 o 0 12 0 1863.56 1794.22 44.10 o 2 12 0 2558.44 2260.77 36.19 o 4 12 0 5.83 80.35 17.61 o 6 12 0 2732.52 2530.33 77.64 o 8 12 0 60.37 106.45 26.17 o 10 12 0 94.81 -38.20 56.88 o 12 12 0 418.48 175.77 144.88 o 2 13 0 612.09 556.36 26.08 o 4 13 0 1620.97 1394.17 36.22 o 6 13 0 354.17 346.27 35.63 o 8 13 0 1357.69 1204.75 58.04 o 10 13 0 865.53 871.63 61.07 o 0 14 0 325.69 458.45 34.15 o 2 14 0 60.88 122.13 29.40 o 4 14 0 52.35 98.46 28.61 o 6 14 0 99.30 95.26 25.37 o 8 14 0 450.65 490.90 40.13 o 10 14 0 327.79 223.19 83.36 o 2 15 0 110.74 182.59 29.64 o 4 15 0 579.55 593.42 40.09 o 6 15 0 33.55 34.05 46.87 o 8 15 0 824.07 801.33 67.38 o 0 16 0 155.42 283.30 57.34 o 2 16 0 429.70 584.56 44.35 o 4 16 0 7.86 60.41 46.60 o 6 16 0 38.71 70.64 48.50 o 8 16 0 203.55 58.11 119.89 o 2 17 0 20.72 14.80 55.24 o 4 17 0 257.31 235.49 60.08 o 6 17 0 285.36 202.72 157.24 o 0 18 0 295.52 512.83 111.07 o 2 18 0 42.54 65.13 123.36 o 4 18 0 1369.98 1409.12 295.10 o 1 1 1 879.36 897.84 7.35 o 2 1 1 7631.18 7402.38 49.91 o 3 1 1 1003.53 858.62 7.15 o 4 1 1 832.03 821.89 7.59 o 5 1 1 454.05 387.36 6.02 o 6 1 1 315.37 332.96 6.26 o 7 1 1 7039.73 7448.82 56.61 o 8 1 1 810.35 789.44 11.95 o 9 1 1 74.99 88.97 7.99 o 10 1 1 443.19 491.94 13.86 o 11 1 1 320.83 337.13 14.35 o 12 1 1 94.75 86.67 15.71 o 13 1 1 382.03 419.11 31.36 o 14 1 1 92.86 88.02 48.65 o 15 1 1 287.87 409.34 91.48 o 0 2 1 15146.80 13043.48 117.18 o 1 2 1 11914.20 11284.30 72.82 o 2 2 1 27.13 62.00 2.43 o 3 2 1 3633.53 3366.78 23.65 o 4 2 1 786.02 721.37 7.00 o 5 2 1 2579.83 2659.53 19.23 o 6 2 1 964.14 1043.13 11.01 o 7 2 1 75.08 136.62 6.21 o 8 2 1 15.13 36.31 6.21 o 9 2 1 578.07 619.55 12.06 o 10 2 1 346.35 329.23 11.25 o 11 2 1 4.75 -12.45 12.45 o 12 2 1 78.63 79.02 20.47 o 13 2 1 3.25 -10.86 25.14 o 14 2 1 2.16 -49.05 49.05 o 15 2 1 7.19 90.65 65.83 o 1 3 1 15260.20 14352.34 86.48 o 2 3 1 6333.47 6064.11 41.59 o 3 3 1 28072.03 27366.99 202.85 o 4 3 1 12.09 15.95 2.79 o 5 3 1 3003.82 2997.24 22.23 o 6 3 1 1402.49 1528.86 14.03 o 7 3 1 469.90 432.85 8.31 o 8 3 1 514.54 506.08 9.83 o 9 3 1 2546.11 2516.21 25.33 o 10 3 1 2116.56 2036.73 23.94 o 11 3 1 307.35 273.30 13.78 o 12 3 1 2455.44 2452.08 39.65 o 13 3 1 533.79 456.08 28.65 o 14 3 1 377.04 412.85 43.87 o 15 3 1 5.06 -54.58 62.35 o 0 4 1 3767.33 3730.02 31.69 o 1 4 1 1556.88 1541.99 10.42 o 2 4 1 322.01 298.92 4.37 o 3 4 1 548.51 552.53 6.98 o 4 4 1 1323.81 1413.12 13.76 o 5 4 1 1320.96 1401.48 14.42 o 6 4 1 180.02 160.55 5.80 o 7 4 1 112.53 155.96 5.71 o 8 4 1 400.29 385.43 9.00 o 9 4 1 8.98 15.08 8.27 o 10 4 1 727.01 743.35 15.82 o 11 4 1 31.28 63.25 13.60 o 12 4 1 24.20 17.91 16.15 o 13 4 1 1345.55 1300.76 42.56 o 14 4 1 109.80 133.80 42.44 o 15 4 1 89.99 200.66 118.04 o 1 5 1 12296.38 11601.72 67.15 o 2 5 1 2990.78 2942.16 19.08 o 3 5 1 1.22 6.12 3.21 o 4 5 1 80.19 100.30 5.69 o 5 5 1 2067.78 1947.91 19.44 o 6 5 1 72.78 119.30 6.16 o 7 5 1 1526.54 1564.62 17.47 o 8 5 1 572.94 597.32 11.46 o 9 5 1 143.94 109.58 8.87 o 10 5 1 350.90 352.43 13.17 o 11 5 1 414.47 434.18 15.32 o 12 5 1 1413.44 1327.43 34.93 o 13 5 1 388.14 382.52 26.28 o 14 5 1 5.70 70.89 36.72 o 15 5 1 1.73 -21.40 78.08 o 0 6 1 256.13 312.79 7.10 o 1 6 1 113.49 96.81 3.60 o 2 6 1 660.06 595.72 7.01 o 3 6 1 621.08 664.06 7.33 o 4 6 1 1767.83 2044.33 19.03 o 5 6 1 3831.22 3856.74 32.53 o 6 6 1 636.48 706.88 13.11 o 7 6 1 1248.79 1371.27 19.73 o 8 6 1 115.04 84.13 9.68 o 9 6 1 701.08 743.64 16.99 o 10 6 1 1190.23 1129.76 20.86 o 11 6 1 2.28 18.63 16.62 o 12 6 1 305.36 321.49 24.71 o 13 6 1 389.37 338.73 29.79 o 14 6 1 44.19 43.24 61.28 o 1 7 1 320.47 342.90 5.54 o 2 7 1 782.12 686.61 9.15 o 3 7 1 0.33 -4.36 5.05 o 4 7 1 249.92 253.66 6.22 o 5 7 1 1284.06 1323.09 17.01 o 6 7 1 644.63 675.35 15.39 o 7 7 1 332.93 327.12 11.53 o 8 7 1 243.69 278.83 11.79 o 9 7 1 16.98 20.47 12.75 o 10 7 1 3.04 54.57 14.85 o 11 7 1 3.60 -15.32 17.97 o 12 7 1 16.70 28.70 24.07 o 13 7 1 1207.65 1138.22 46.39 o 14 7 1 476.80 456.05 71.96 o 0 8 1 10589.51 10480.01 95.59 o 1 8 1 824.65 830.99 9.26 o 2 8 1 415.32 498.64 8.99 o 3 8 1 31.70 23.86 5.42 o 4 8 1 680.78 688.72 10.53 o 5 8 1 1025.62 1021.01 14.77 o 6 8 1 1050.32 1072.81 17.64 o 7 8 1 124.98 170.11 11.12 o 8 8 1 125.74 165.44 11.74 o 9 8 1 77.02 129.10 13.41 o 10 8 1 562.65 536.00 18.48 o 11 8 1 6.75 -18.87 18.87 o 12 8 1 165.57 141.02 25.19 o 13 8 1 172.42 162.37 41.51 o 14 8 1 12.24 43.66 80.99 o 1 9 1 571.10 542.42 8.31 o 2 9 1 137.79 180.81 6.82 o 3 9 1 273.54 222.23 6.69 o 4 9 1 764.95 687.34 11.15 o 5 9 1 2084.67 2046.52 21.16 o 6 9 1 55.92 52.49 11.38 o 7 9 1 1509.63 1366.65 21.70 o 8 9 1 1347.88 1279.90 22.94 o 9 9 1 3.65 13.23 14.07 o 10 9 1 364.22 389.57 22.50 o 11 9 1 16.46 31.93 22.76 o 12 9 1 0.05 11.04 24.72 o 13 9 1 141.23 137.38 73.09 o 0 10 1 4633.59 4586.64 47.71 o 1 10 1 77.16 67.75 6.97 o 2 10 1 4147.02 4267.44 32.46 o 3 10 1 0.01 -7.41 7.41 o 4 10 1 2155.25 2063.13 19.57 o 5 10 1 169.16 148.96 9.32 o 6 10 1 1102.14 1133.20 22.69 o 7 10 1 1823.41 1619.74 26.34 o 8 10 1 1665.43 1657.45 33.93 o 9 10 1 757.47 620.87 21.10 o 10 10 1 4.57 -18.51 18.51 o 11 10 1 3.48 25.81 25.25 o 12 10 1 14.58 -8.65 42.54 o 13 10 1 1414.54 1301.19 99.35 o 1 11 1 654.08 664.30 13.12 o 2 11 1 82.29 136.14 9.94 o 3 11 1 152.79 163.32 9.81 o 4 11 1 70.94 75.96 10.04 o 5 11 1 1656.67 1642.39 26.01 o 6 11 1 324.82 317.28 15.73 o 7 11 1 99.75 67.19 18.88 o 8 11 1 35.60 18.21 17.66 o 9 11 1 158.29 117.28 24.61 o 10 11 1 30.11 57.01 24.21 o 11 11 1 10.97 50.37 28.64 o 12 11 1 210.76 162.55 48.01 o 0 12 1 108.89 309.86 30.26 o 1 12 1 669.97 569.98 12.64 o 2 12 1 9.75 76.58 14.04 o 3 12 1 1211.86 1146.07 21.52 o 4 12 1 321.27 293.53 13.72 o 5 12 1 5021.25 5036.85 78.30 o 6 12 1 740.89 861.40 42.11 o 7 12 1 472.66 462.97 20.97 o 8 12 1 215.08 228.70 20.36 o 9 12 1 425.52 449.14 29.61 o 10 12 1 306.66 251.55 27.03 o 11 12 1 13.35 45.91 44.97 o 12 12 1 13.43 -71.90 71.90 o 1 13 1 1066.47 1078.48 22.24 o 2 13 1 115.66 143.56 15.93 o 3 13 1 524.51 692.89 41.83 o 4 13 1 116.95 156.20 17.10 o 5 13 1 33.88 121.31 23.22 o 6 13 1 104.92 77.69 18.21 o 7 13 1 45.80 39.01 25.44 o 8 13 1 184.99 189.51 29.43 o 9 13 1 0.07 20.06 25.87 o 10 13 1 114.33 116.11 41.23 o 11 13 1 106.07 -37.91 63.77 o 0 14 1 1039.98 1153.29 34.92 o 1 14 1 404.80 393.94 18.78 o 2 14 1 496.91 423.68 18.76 o 3 14 1 114.95 94.06 19.02 o 4 14 1 116.48 117.18 19.83 o 5 14 1 935.46 914.70 28.28 o 6 14 1 889.06 893.20 25.90 o 7 14 1 77.30 72.70 26.74 o 8 14 1 276.62 244.00 34.78 o 9 14 1 94.63 90.52 44.37 o 10 14 1 287.56 270.80 55.96 o 1 15 1 24.26 39.66 20.61 o 2 15 1 80.85 148.64 20.57 o 3 15 1 537.39 567.72 24.77 o 4 15 1 136.27 184.63 24.72 o 5 15 1 9.52 5.83 31.90 o 6 15 1 133.91 78.20 24.70 o 7 15 1 102.69 64.61 33.42 o 8 15 1 1.11 56.76 40.66 o 9 15 1 6.59 51.87 59.01 o 0 16 1 775.25 892.49 49.65 o 1 16 1 51.95 47.52 28.86 o 2 16 1 1188.27 1085.84 36.55 o 3 16 1 0.20 8.18 28.30 o 4 16 1 424.44 509.34 30.96 o 5 16 1 1.47 -3.28 32.29 o 6 16 1 287.19 258.81 37.86 o 7 16 1 393.59 398.24 46.44 o 8 16 1 629.11 505.43 73.70 o 1 17 1 85.45 108.31 38.15 o 2 17 1 1.71 60.83 42.19 o 3 17 1 57.83 96.35 36.38 o 4 17 1 0.04 20.20 37.59 o 5 17 1 0.23 78.31 37.59 o 6 17 1 55.04 69.37 60.48 o 0 18 1 693.33 876.17 134.14 o 1 18 1 66.28 166.21 58.13 o 2 18 1 147.23 240.64 64.12 o 3 18 1 60.56 50.08 65.21 o 4 18 1 157.86 357.81 86.43 o 1 0 2 3071.26 2722.42 28.09 o 2 0 2 15932.06 15138.53 143.20 o 3 0 2 13941.95 13321.17 130.03 o 4 0 2 1357.32 1297.18 15.36 o 5 0 2 546.83 518.41 9.51 o 6 0 2 141.70 118.64 6.96 o 7 0 2 903.46 930.61 16.04 o 8 0 2 246.00 290.89 10.33 o 9 0 2 6158.41 6386.42 73.32 o 10 0 2 3030.23 3252.12 41.91 o 11 0 2 5857.57 5783.14 85.38 o 12 0 2 1025.94 932.91 34.26 o 13 0 2 734.97 762.65 44.42 o 14 0 2 84.67 106.90 55.57 o 15 0 2 3467.67 3843.14 240.07 o 1 1 2 1726.75 1505.42 10.72 o 2 1 2 1233.96 1260.34 9.30 o 3 1 2 25.17 11.54 2.45 o 4 1 2 1969.95 2138.53 15.55 o 5 1 2 0.08 -3.17 3.17 o 6 1 2 449.45 470.61 7.91 o 7 1 2 635.70 676.60 10.04 o 8 1 2 131.58 156.22 6.93 o 9 1 2 944.77 897.82 15.08 o 10 1 2 38.32 23.45 11.47 o 11 1 2 556.66 555.38 16.13 o 12 1 2 95.50 115.56 17.26 o 13 1 2 6.48 -15.08 24.45 o 14 1 2 1.82 -42.85 42.85 o 15 1 2 20.16 2.66 80.45 o 0 2 2 4869.86 4442.50 39.02 o 1 2 2 2196.34 1983.04 13.63 o 2 2 2 771.55 774.30 6.63 o 3 2 2 959.61 907.55 7.74 o 4 2 2 544.52 643.65 7.05 o 5 2 2 308.15 330.30 5.61 o 6 2 2 1394.00 1342.87 13.01 o 7 2 2 1993.68 2023.40 18.29 o 8 2 2 1320.07 1376.11 15.70 o 9 2 2 0.74 10.32 8.75 o 10 2 2 460.93 438.98 12.58 o 11 2 2 13.14 8.30 13.82 o 12 2 2 12.10 1.22 17.41 o 13 2 2 2886.18 2811.53 50.47 o 14 2 2 31.61 38.53 39.39 o 15 2 2 35.88 129.21 64.92 o 1 3 2 1628.48 1533.55 10.94 o 2 3 2 41.61 44.67 2.49 o 3 3 2 1088.98 935.04 8.62 o 4 3 2 0.15 3.51 3.08 o 5 3 2 243.43 260.03 6.70 o 6 3 2 106.88 144.93 4.80 o 7 3 2 423.51 453.02 8.75 o 8 3 2 257.17 254.81 8.07 o 9 3 2 37.19 44.88 8.88 o 10 3 2 83.32 96.69 11.37 o 11 3 2 1757.83 1697.09 26.44 o 12 3 2 0.79 38.22 17.68 o 13 3 2 53.85 9.90 25.74 o 14 3 2 36.26 29.33 43.58 o 15 3 2 18.83 70.66 75.13 o 0 4 2 3859.33 4128.65 40.40 o 1 4 2 148.29 130.39 2.95 o 2 4 2 4417.61 4130.52 26.45 o 3 4 2 303.73 377.03 5.50 o 4 4 2 14.70 34.46 4.02 o 5 4 2 6636.51 6897.35 51.76 o 6 4 2 984.76 896.82 11.32 o 7 4 2 261.28 266.24 6.80 o 8 4 2 177.04 171.50 7.08 o 9 4 2 2588.93 2684.53 26.53 o 10 4 2 1.69 12.42 11.50 o 11 4 2 99.89 113.00 15.08 o 12 4 2 71.71 76.12 18.48 o 13 4 2 393.34 386.09 26.60 o 14 4 2 27.11 42.75 40.83 o 15 4 2 620.39 527.24 66.98 o 1 5 2 6897.03 6564.93 39.90 o 2 5 2 67.84 109.56 3.45 o 3 5 2 15420.64 15247.17 93.72 o 4 5 2 1260.94 1274.92 12.01 o 5 5 2 15.82 1.52 4.75 o 6 5 2 4.82 8.82 5.62 o 7 5 2 707.72 715.33 11.96 o 8 5 2 2376.65 2418.16 24.10 o 9 5 2 709.90 812.66 15.29 o 10 5 2 209.38 205.17 11.70 o 11 5 2 8.69 17.44 14.47 o 12 5 2 185.78 187.32 19.52 o 13 5 2 0.42 21.50 24.38 o 14 5 2 5.04 2.44 37.68 o 15 5 2 1.69 59.01 72.50 o 0 6 2 5514.74 5315.92 46.17 o 1 6 2 4613.29 4692.27 29.67 o 2 6 2 3338.99 3453.12 22.92 o 3 6 2 63.61 60.62 3.91 o 4 6 2 249.90 307.83 6.53 o 5 6 2 193.26 198.58 6.74 o 6 6 2 109.59 118.51 6.47 o 7 6 2 1360.80 1326.40 16.97 o 8 6 2 0.26 -8.31 8.31 o 9 6 2 329.74 344.54 11.46 o 10 6 2 920.10 928.21 17.48 o 11 6 2 126.66 84.05 15.08 o 12 6 2 547.57 525.26 30.55 o 13 6 2 291.51 289.49 28.27 o 14 6 2 119.87 94.22 72.91 o 1 7 2 882.95 769.62 8.64 o 2 7 2 43.86 20.56 4.88 o 3 7 2 9165.66 9745.15 71.16 o 4 7 2 518.96 513.85 8.59 o 5 7 2 277.75 269.76 7.69 o 6 7 2 31.84 39.23 7.40 o 7 7 2 426.32 467.70 11.87 o 8 7 2 1710.22 1746.69 22.07 o 9 7 2 215.17 261.12 14.46 o 10 7 2 982.51 1022.74 21.11 o 11 7 2 406.00 344.92 18.60 o 12 7 2 278.89 252.13 38.63 o 13 7 2 723.93 685.10 35.58 o 14 7 2 0.96 4.30 85.52 o 0 8 2 607.14 627.16 14.25 o 1 8 2 1010.84 1233.04 11.53 o 2 8 2 184.29 174.66 6.58 o 3 8 2 74.43 68.28 5.85 o 4 8 2 73.01 80.81 5.98 o 5 8 2 465.63 484.96 10.63 o 6 8 2 0.19 10.85 8.62 o 7 8 2 5067.77 5131.50 46.30 o 8 8 2 252.47 237.51 12.11 o 9 8 2 310.64 278.28 15.45 o 10 8 2 930.97 892.58 21.57 o 11 8 2 702.21 652.92 25.23 o 12 8 2 403.66 367.55 32.25 o 13 8 2 850.19 887.58 48.41 o 14 8 2 91.16 10.34 88.77 o 1 9 2 753.70 759.90 10.16 o 2 9 2 243.98 245.37 7.22 o 3 9 2 561.73 519.52 9.14 o 4 9 2 6.33 6.19 7.90 o 5 9 2 987.67 889.00 15.59 o 6 9 2 0.85 -9.20 9.20 o 7 9 2 1173.19 1041.87 19.25 o 8 9 2 224.75 224.74 13.70 o 9 9 2 47.88 37.97 14.72 o 10 9 2 6.04 24.61 17.09 o 11 9 2 523.24 569.12 25.79 o 12 9 2 1.07 32.15 27.04 o 13 9 2 13.61 73.28 63.63 o 0 10 2 199.11 255.33 15.15 o 1 10 2 1.58 41.56 7.74 o 2 10 2 66.51 122.48 8.86 o 3 10 2 467.95 533.57 10.44 o 4 10 2 67.93 67.12 8.37 o 5 10 2 1052.02 1024.74 16.36 o 6 10 2 301.98 338.83 12.67 o 7 10 2 327.14 374.25 13.84 o 8 10 2 551.05 625.31 18.74 o 9 10 2 115.16 176.10 18.46 o 10 10 2 82.76 107.30 20.76 o 11 10 2 44.23 23.86 26.69 o 12 10 2 0.20 48.33 53.19 o 13 10 2 0.07 32.28 90.81 o 1 11 2 53.03 62.00 9.59 o 2 11 2 452.02 468.78 11.61 o 3 11 2 2911.49 2965.60 25.77 o 4 11 2 26.74 14.30 10.27 o 5 11 2 939.94 933.72 19.57 o 6 11 2 12.60 21.59 13.97 o 7 11 2 300.91 303.32 16.31 o 8 11 2 3.19 5.56 18.52 o 9 11 2 1186.95 1270.12 37.07 o 10 11 2 17.84 22.62 23.51 o 11 11 2 260.32 224.25 35.98 o 12 11 2 237.68 221.72 56.37 o 0 12 2 92.09 104.02 17.41 o 1 12 2 59.32 20.71 10.73 o 2 12 2 220.74 247.86 12.60 o 3 12 2 73.58 116.98 11.86 o 4 12 2 343.00 338.30 13.90 o 5 12 2 373.70 419.97 29.14 o 6 12 2 140.81 182.08 16.80 o 7 12 2 350.65 392.70 19.55 o 8 12 2 137.25 112.19 18.33 o 9 12 2 183.85 184.47 24.50 o 10 12 2 0.73 9.23 28.38 o 11 12 2 5.79 -21.85 51.72 o 12 12 2 11.63 -2.86 74.69 o 1 13 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5 310.05 282.78 15.96 o 6 12 5 351.45 348.61 17.36 o 7 12 5 474.50 440.83 19.00 o 8 12 5 608.52 546.48 22.38 o 9 12 5 126.40 109.35 21.19 o 10 12 5 103.48 60.82 34.49 o 11 12 5 154.80 158.15 56.05 o 1 13 5 207.45 251.89 13.78 o 2 13 5 205.20 184.50 14.81 o 3 13 5 15.50 68.40 16.34 o 4 13 5 315.11 267.77 15.80 o 5 13 5 41.69 70.47 17.32 o 6 13 5 70.55 70.85 18.90 o 7 13 5 84.85 103.49 23.68 o 8 13 5 164.60 233.67 39.58 o 9 13 5 90.35 118.02 43.37 o 10 13 5 581.82 591.04 59.51 o 11 13 5 28.76 134.26 192.18 o 0 14 5 3300.83 3336.86 54.14 o 1 14 5 209.26 254.45 16.86 o 2 14 5 185.50 242.70 17.82 o 3 14 5 192.60 239.19 17.64 o 4 14 5 532.51 518.88 19.67 o 5 14 5 1.83 33.61 21.88 o 6 14 5 592.34 580.28 24.19 o 7 14 5 946.47 899.35 37.71 o 8 14 5 482.66 413.14 37.13 o 9 14 5 10.31 -43.05 43.05 o 10 14 5 221.22 191.00 66.52 o 1 15 5 7.31 119.58 21.70 o 2 15 5 596.37 637.67 23.46 o 3 15 5 25.26 70.24 22.48 o 4 15 5 96.79 62.14 23.67 o 5 15 5 33.03 102.41 26.69 o 6 15 5 0.14 13.23 28.07 o 7 15 5 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17.53 o 5 1 9 6012.31 6157.15 45.75 o 6 1 9 105.19 73.00 6.79 o 7 1 9 66.08 88.56 7.10 o 8 1 9 2658.93 2739.31 25.84 o 9 1 9 958.51 924.91 20.10 o 10 1 9 808.52 839.51 24.50 o 11 1 9 68.27 62.11 16.95 o 12 1 9 1004.94 1043.32 36.07 o 13 1 9 51.57 71.15 26.18 o 14 1 9 960.23 973.28 43.76 o 0 2 9 383.38 401.22 9.12 o 1 2 9 526.76 599.01 8.03 o 2 2 9 7493.83 7629.60 52.41 o 3 2 9 6094.42 6424.49 47.03 o 4 2 9 198.62 168.86 5.94 o 5 2 9 286.22 355.30 7.45 o 6 2 9 1935.94 1960.92 18.19 o 7 2 9 349.48 358.75 8.45 o 8 2 9 0.64 -1.05 9.26 o 9 2 9 59.02 74.19 12.03 o 10 2 9 885.59 883.98 17.53 o 11 2 9 13.86 1.62 16.58 o 12 2 9 80.11 91.78 21.01 o 13 2 9 0.41 -28.61 28.61 o 14 2 9 24.61 52.41 42.73 o 1 3 9 64.15 63.25 4.93 o 2 3 9 1590.61 1609.17 14.25 o 3 3 9 91.09 102.47 4.91 o 4 3 9 1343.96 1480.71 14.06 o 5 3 9 306.62 317.18 7.30 o 6 3 9 576.91 673.84 11.10 o 7 3 9 1016.08 1045.43 14.16 o 8 3 9 2248.76 2271.32 24.06 o 9 3 9 59.98 63.16 11.25 o 10 3 9 1.98 2.14 13.34 o 11 3 9 81.06 95.47 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8 9 87.84 168.55 77.57 o 1 9 9 36.17 48.93 7.90 o 2 9 9 1621.59 1702.09 19.37 o 3 9 9 414.25 442.98 12.20 o 4 9 9 122.37 130.45 10.35 o 5 9 9 48.38 49.04 12.72 o 6 9 9 708.59 698.94 17.09 o 7 9 9 491.37 468.82 15.94 o 8 9 9 524.77 491.63 17.84 o 9 9 9 24.72 7.73 17.07 o 10 9 9 60.80 70.58 22.20 o 11 9 9 66.87 51.50 26.10 o 12 9 9 312.28 403.80 52.63 o 0 10 9 399.06 382.46 17.77 o 1 10 9 1475.66 1469.63 18.12 o 2 10 9 6765.46 6765.97 58.76 o 3 10 9 1913.84 1855.96 23.09 o 4 10 9 29.46 -7.00 13.45 o 5 10 9 72.12 49.77 13.95 o 6 10 9 22.27 5.89 12.98 o 7 10 9 6.24 -11.11 14.49 o 8 10 9 1380.63 1351.40 33.56 o 9 10 9 17.40 35.81 20.57 o 10 10 9 475.99 466.71 24.05 o 11 10 9 14.08 65.34 33.00 o 12 10 9 112.20 146.99 63.14 o 1 11 9 69.72 61.61 11.23 o 2 11 9 630.71 580.70 15.23 o 3 11 9 830.17 773.47 17.43 o 4 11 9 115.33 121.23 13.96 o 5 11 9 703.77 652.90 17.05 o 6 11 9 53.32 83.46 15.17 o 7 11 9 7.31 32.46 16.10 o 8 11 9 36.65 36.52 19.54 o 9 11 9 12.71 -7.68 20.93 o 10 11 9 131.92 142.01 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