#------------------------------------------------------------------------------ #$Date: 2017-11-06 07:27:01 +0200 (Mon, 06 Nov 2017) $ #$Revision: 202633 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/78/1547873.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1547873 loop_ _publ_author_name 'Chai, Jinsong' 'Lv, Ying' 'Yang, Sha' 'Song, Yongbo' 'Zan, Xiaofeng' 'Li, Qinzhen' 'Yu, Haizhu' 'Wu, Mingzai' 'Zhu, Manzhou' _publ_section_title ; X-ray Crystal Structure and Optical Properties of Au38--xCux(2,4-(CH3)2C6H3S)24 (x = 0--6) Alloy Nanocluster ; _journal_issue 39 _journal_name_full 'The Journal of Physical Chemistry C' _journal_page_first 21665 _journal_paper_doi 10.1021/acs.jpcc.7b05074 _journal_volume 121 _journal_year 2017 _chemical_formula_moiety 'C192 H216 Au37 Cu1 S24' _chemical_formula_sum 'C192 H216 Au37.01 Cu S24' _chemical_formula_weight 10645.04 _space_group_crystal_system trigonal _space_group_IT_number 167 _space_group_name_Hall '-R 3 2"c' _space_group_name_H-M_alt 'R -3 c' _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2016-09-24 _audit_creation_method ; Olex2 1.2 (compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5227) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 19.4293(16) _cell_length_b 19.4293(16) _cell_length_c 129.434(11) _cell_measurement_reflns_used 9890 _cell_measurement_temperature 130 _cell_measurement_theta_max 27.031 _cell_measurement_theta_min 2.30 _cell_volume 42315(6) _computing_cell_refinement 'SAINT v7.68A (Bruker, 2009)' _computing_data_reduction 'SAINT v7.68A (Bruker, 2009)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 130 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1119 _diffrn_reflns_av_unetI/netI 0.0622 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 25 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 118 _diffrn_reflns_limit_l_min -167 _diffrn_reflns_number 87418 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 27.545 _diffrn_reflns_theta_min 1.364 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 19.439 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.5199 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.1479 before and 0.0625 after correction. The Ratio of minimum to maximum transmission is 0.6973. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour black _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 2.506 _exptl_crystal_description block _exptl_crystal_F_000 28226 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.05 _refine_diff_density_max 2.666 _refine_diff_density_min -2.335 _refine_diff_density_rms 0.383 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.027 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 392 _refine_ls_number_reflns 10812 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.027 _refine_ls_R_factor_all 0.0917 _refine_ls_R_factor_gt 0.0527 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0510P)^2^+3959.0769P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1213 _refine_ls_wR_factor_ref 0.1395 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7129 _reflns_number_total 10812 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; mo_dm16605_0m.res created by SHELXL-2014/7 TITL mo_dm16605_0m_a.res in R-3c REM Old TITL mo_dm16605_0m in R-3c #167 REM SHELXT solution in R-3c REM R1 0.148, Rweak 0.005, Alpha 0.028, Orientation as input REM Formula found by SHELXT: C60 S12 I19 CELL 0.71073 19.4293 19.4293 129.4337 90 90 120 ZERR 6 0.0016 0.0016 0.0106 0 0 0 LATT 3 SYMM -Y,+X-Y,+Z SYMM +Y-X,-X,+Z SYMM +Y,+X,0.5-Z SYMM -Y+X,-Y,0.5-Z SYMM -X,-X+Y,0.5-Z SFAC C H Au Cu S UNIT 1152 1296 222.03 5.97 144 EADP Cu4 Au4 EADP Cu5 Au5 EXYZ Cu4 Au4 EXYZ Cu5 Au5 L.S. 4 PLAN 20 SIZE 0.05 0.08 0.1 TEMP -143.15 BOND $H list 4 MORE -1 ABIN fmap 2 acta 52 OMIT -2 2 2 OMIT 0 1 20 OMIT 0 1 2 OMIT -1 3 2 OMIT 0 0 18 OMIT 0 1 32 OMIT -3 3 6 OMIT 0 1 14 OMIT 0 2 4 OMIT -1 2 3 OMIT -2 3 13 OMIT -1 2 0 OMIT -1 2 12 OMIT -1 15 29 OMIT -2 4 21 OMIT -1 4 4 OMIT -1 2 6 OMIT -2 3 1 OMIT 0 0 12 REM REM REM WGHT 0.051000 3959.076904 FVAR 0.01240 0.91701 AU1 3 0.578591 0.911925 0.416667 10.50000 0.03323 0.03323 = 0.03734 -0.00217 0.00217 0.00741 AU2 3 0.470338 0.815254 0.396000 11.00000 0.02734 0.02713 = 0.02832 0.00094 0.00124 0.01040 AU3 3 0.432072 0.678259 0.384431 11.00000 0.03502 0.03369 = 0.02794 0.00040 0.00412 0.01808 PART 1 AU4 3 0.340416 0.508182 0.372515 21.00000 0.03736 0.04146 = 0.03922 0.00035 0.00162 0.01808 AU5 3 0.187162 0.391705 0.389281 21.00000 0.03753 0.03006 = 0.02865 -0.00137 0.00237 0.01422 PART 0 PART 2 CU4 4 0.340416 0.508182 0.372515 -21.00000 0.03736 0.04146 = 0.03922 0.00035 0.00162 0.01808 CU5 4 0.187162 0.391705 0.389281 -21.00000 0.03753 0.03006 = 0.02865 -0.00137 0.00237 0.01422 PART 0 AU6 3 0.194449 0.525374 0.405232 11.00000 0.02951 0.02792 = 0.03035 -0.00129 -0.00116 0.01109 AU7 3 0.333333 0.570464 0.416667 10.50000 0.02888 0.02583 = 0.02501 0.00041 0.00083 0.01444 AU8 3 0.333333 0.666667 0.400506 10.33333 0.02431 0.02431 = 0.02573 0.00000 0.00000 0.01215 S1 5 0.556275 0.951959 0.400914 11.00000 0.03454 0.03015 = 0.04167 -0.00020 -0.00026 0.01085 S2 5 0.442148 0.630591 0.367918 11.00000 0.04534 0.03483 = 0.03264 -0.00104 0.00187 0.01824 S3 5 0.244847 0.378597 0.374351 11.00000 0.03963 0.04205 = 0.03279 -0.00442 0.00216 0.01994 S4 5 0.130481 0.384528 0.405229 11.00000 0.04084 0.02824 = 0.03430 -0.00156 0.00007 0.00944 C1 1 0.648353 0.993834 0.394394 11.00000 0.03358 0.03270 = 0.03715 0.00097 0.00616 0.00392 C2 1 0.709247 0.982250 0.397820 11.00000 0.04077 0.03028 = 0.04250 0.00090 -0.00323 0.00461 AFIX 43 H2 2 0.702109 0.951508 0.403851 11.00000 -1.20000 AFIX 0 C3 1 0.782324 1.016087 0.392365 11.00000 0.04062 0.03569 = 0.04324 0.00096 0.00940 -0.00920 AFIX 43 H3 2 0.822655 1.005072 0.394481 11.00000 -1.20000 AFIX 0 C4 1 0.795217 1.066196 0.383783 11.00000 0.04333 0.06146 = 0.04701 -0.01988 0.02200 -0.01138 C5 1 0.732888 1.075950 0.380765 11.00000 0.03870 0.04410 = 0.05020 -0.00123 -0.00711 0.00187 AFIX 43 H5 2 0.740457 1.107599 0.374814 11.00000 -1.20000 AFIX 0 C6 1 0.659722 1.043424 0.385683 11.00000 0.01420 0.06027 = 0.05241 -0.00255 -0.00227 0.00419 C7 1 0.594972 1.058745 0.381960 11.00000 0.07296 0.05432 = 0.05725 0.01378 0.00650 0.03606 AFIX 137 H7A 2 0.551567 1.009903 0.378978 11.00000 -1.50000 H7B 2 0.616515 1.100595 0.376695 11.00000 -1.50000 H7C 2 0.574792 1.075685 0.387789 11.00000 -1.50000 AFIX 0 C8 1 0.873557 1.104175 0.377993 11.00000 0.05617 0.06430 = 0.05497 -0.01143 0.02022 -0.01159 AFIX 137 H8A 2 0.908206 1.158007 0.380640 11.00000 -1.50000 H8B 2 0.863776 1.106761 0.370614 11.00000 -1.50000 H8C 2 0.899317 1.072301 0.378984 11.00000 -1.50000 AFIX 0 C9 1 0.523194 0.611463 0.367578 11.00000 0.04137 0.03602 = 0.03388 0.00260 0.01413 0.01396 C10 1 0.571125 0.624293 0.376301 11.00000 0.05316 0.02892 = 0.03630 -0.00508 0.00714 0.01963 AFIX 43 H10 2 0.559739 0.641925 0.382579 11.00000 -1.20000 AFIX 0 C11 1 0.637292 0.610845 0.375760 11.00000 0.02593 0.05296 = 0.06253 -0.00290 -0.00483 0.01502 AFIX 43 H11 2 0.670293 0.620185 0.381617 11.00000 -1.20000 AFIX 0 C12 1 0.652385 0.584067 0.366583 11.00000 0.05424 0.07731 = 0.07769 -0.01666 0.00021 0.04701 C13 1 0.602755 0.569645 0.357896 11.00000 0.06742 0.08863 = 0.05930 -0.02959 0.00591 0.04067 AFIX 43 H13 2 0.613749 0.551748 0.351612 11.00000 -1.20000 AFIX 0 C14 1 0.535655 0.581947 0.358528 11.00000 0.05700 0.05630 = 0.06246 -0.00997 0.00460 0.02947 C15 1 0.483783 0.561869 0.348951 11.00000 0.06106 0.12525 = 0.07524 -0.02427 0.00044 0.06156 AFIX 137 H15A 2 0.495720 0.611015 0.345358 11.00000 -1.50000 H15B 2 0.427682 0.533317 0.350984 11.00000 -1.50000 H15C 2 0.494510 0.528331 0.344338 11.00000 -1.50000 AFIX 0 C16 1 0.724703 0.572123 0.366348 11.00000 0.08848 0.16941 = 0.11952 -0.03866 0.00369 0.09972 AFIX 137 H16A 2 0.746584 0.578614 0.373333 11.00000 -1.50000 H16B 2 0.765279 0.611555 0.361738 11.00000 -1.50000 H16C 2 0.708426 0.518572 0.363822 11.00000 -1.50000 AFIX 0 C17 1 0.177295 0.354163 0.363691 11.00000 0.04393 0.06644 = 0.03537 0.00106 0.01732 0.03678 C18 1 0.201699 0.401303 0.354750 11.00000 0.07223 0.06011 = 0.04237 -0.00619 -0.00165 0.03136 AFIX 43 H18 2 0.252960 0.447381 0.354544 11.00000 -1.20000 AFIX 0 C19 1 0.152966 0.382076 0.346323 11.00000 0.05129 0.07597 = 0.06929 0.00572 0.00728 0.02070 AFIX 43 H19 2 0.168663 0.417083 0.340571 11.00000 -1.20000 AFIX 0 C20 1 0.079133 0.310071 0.346153 11.00000 0.08612 0.12429 = 0.04372 0.01608 -0.00175 0.06965 C21 1 0.058025 0.262756 0.355380 11.00000 0.04406 0.08289 = 0.05634 -0.02071 0.00376 0.02389 AFIX 43 H21 2 0.007975 0.215157 0.355613 11.00000 -1.20000 AFIX 0 C22 1 0.106626 0.282919 0.363886 11.00000 0.01511 0.07552 = 0.04735 -0.00850 0.00860 0.00743 C23 1 0.078891 0.230045 0.373150 11.00000 0.04554 0.05411 = 0.04998 -0.01254 0.00892 -0.00979 AFIX 137 H23A 2 0.020695 0.201747 0.373425 11.00000 -1.50000 H23B 2 0.100461 0.262184 0.379410 11.00000 -1.50000 H23C 2 0.097318 0.191506 0.372695 11.00000 -1.50000 AFIX 0 C24 1 0.021711 0.288541 0.337034 11.00000 0.07580 0.17791 = 0.07842 0.00271 -0.04621 0.05520 AFIX 137 H24A 2 0.001627 0.232963 0.335088 11.00000 -1.50000 H24B 2 0.049652 0.323052 0.331150 11.00000 -1.50000 H24C 2 -0.022887 0.295833 0.339030 11.00000 -1.50000 AFIX 0 C25 1 0.028044 0.340479 0.403288 11.00000 0.05003 0.03218 = 0.02299 0.00083 -0.00579 -0.00355 C26 1 -0.009463 0.388183 0.403310 11.00000 0.03557 0.07005 = 0.02607 0.00369 0.01195 0.01784 AFIX 43 H26 2 0.022907 0.444271 0.403843 11.00000 -1.20000 AFIX 0 C27 1 -0.093704 0.354331 0.402559 11.00000 0.05546 0.11044 = 0.03574 -0.00634 -0.00750 0.03330 AFIX 43 H27 2 -0.114973 0.388988 0.402614 11.00000 -1.20000 AFIX 0 C28 1 -0.144331 0.275500 0.401777 11.00000 0.04229 0.08228 = 0.08271 -0.04273 0.01759 -0.03483 C29 1 -0.104468 0.225046 0.402201 11.00000 0.06772 0.05688 = 0.08782 -0.03231 0.02707 0.00135 AFIX 43 H29 2 -0.137302 0.168874 0.402000 11.00000 -1.20000 AFIX 0 C30 1 -0.020402 0.257607 0.402885 11.00000 0.04214 0.04060 = 0.05544 -0.00119 0.02498 -0.00457 C31 1 0.013921 0.202621 0.402535 11.00000 0.09293 0.03887 = 0.06454 -0.02061 0.01038 -0.00467 AFIX 137 H31A 2 0.055237 0.220975 0.397209 11.00000 -1.50000 H31B 2 -0.028367 0.148549 0.400899 11.00000 -1.50000 H31C 2 0.037069 0.202812 0.409269 11.00000 -1.50000 AFIX 0 C32 1 -0.231865 0.233236 0.402461 11.00000 0.04263 0.15420 = 0.16679 -0.12283 -0.01431 0.00209 AFIX 137 H32A 2 -0.254576 0.195507 0.396722 11.00000 -1.50000 H32B 2 -0.250398 0.271721 0.402085 11.00000 -1.50000 H32C 2 -0.248747 0.204414 0.409030 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_dm16605_0m_a.res in R-3c REM R1 = 0.0527 for 7129 Fo > 4sig(Fo) and 0.0917 for all 10812 data REM 392 parameters refined using 0 restraints END WGHT 0.0511 3959.9814 REM Highest difference peak 2.666, deepest hole -2.335, 1-sigma level 0.383 Q1 1 0.1903 0.3893 0.3840 11.00000 0.05 2.67 Q2 1 0.1855 0.3865 0.3941 11.00000 0.05 2.41 Q3 1 0.1579 0.3992 0.3893 11.00000 0.05 2.22 Q4 1 0.3377 0.5707 0.4101 11.00000 0.05 2.19 Q5 1 0.5740 0.9211 0.4105 11.00000 0.05 2.05 Q6 1 0.4298 0.6794 0.3910 11.00000 0.05 2.01 Q7 1 0.3368 0.5247 0.3802 11.00000 0.05 1.95 Q8 1 0.4196 0.6484 0.3770 11.00000 0.05 1.79 Q9 1 0.4689 0.8152 0.3882 11.00000 0.05 1.76 Q10 1 0.1971 0.5172 0.4125 11.00000 0.05 1.74 Q11 1 0.1952 0.4253 0.3888 11.00000 0.05 1.72 Q12 1 0.2427 0.5690 0.4071 11.00000 0.05 1.72 Q13 1 0.4313 0.6766 0.3610 11.00000 0.05 1.71 Q14 1 0.3333 0.6667 0.4072 10.33333 0.05 1.69 Q15 1 0.1898 0.5147 0.3982 11.00000 0.05 1.66 Q16 1 0.3333 0.6667 0.3945 10.33333 0.05 1.60 Q17 1 0.1379 0.2343 0.4015 11.00000 0.05 1.49 Q18 1 0.3236 0.4705 0.3646 11.00000 0.05 1.44 Q19 1 0.0649 0.2107 0.4119 11.00000 0.05 1.42 Q20 1 0.4776 0.8216 0.4019 11.00000 0.05 1.41 REM The information below was added by Olex2. REM REM R1 = 0.0527 for 7129 Fo > 4sig(Fo) and 0.0917 for all 87418 data REM n/a parameters refined using n/a restraints REM Highest difference peak 2.67, deepest hole -2.33 REM Mean Shift 0, Max Shift -0.004. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0917 REM R1_gt = 0.0527 REM wR_ref = 0.1395 REM GOOF = 1.027 REM Shift_max = -0.004 REM Shift_mean = 0 REM Reflections_all = 87418 REM Reflections_gt = 7129 REM Parameters = n/a REM Hole = -2.33 REM Peak = 2.67 REM Flack = n/a ; _cod_data_source_file jp7b05074_si_002.cif _cod_data_source_block mo_dm16605_0m _cod_original_cell_volume 42315(8) _cod_database_code 1547873 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.443 _shelx_estimated_absorpt_t_min 0.247 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Shared sites {Cu4, Au4} {Cu5, Au5} 3. Uiso/Uaniso restraints and constraints Uanis(Cu4) = Uanis(Au4) Uanis(Cu5) = Uanis(Au5) 4. Others Sof(Cu4)=Sof(Cu5)=1-FVAR(1) Sof(Au4)=Sof(Au5)=FVAR(1) 5.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C5(H5), C10(H10), C11(H11), C13(H13), C18(H18), C19(H19), C21(H21), C26(H26), C27(H27), C29(H29) 5.b Idealised Me refined as rotating group: C7(H7A,H7B,H7C), C8(H8A,H8B,H8C), C15(H15A,H15B,H15C), C16(H16A,H16B,H16C), C23(H23A,H23B,H23C), C24(H24A,H24B,H24C), C31(H31A,H31B,H31C), C32(H32A,H32B, H32C) ; _shelx_fab_checksum 56626 _shelx_fab_file ; 0 0 12 1333.3001 139.9753 0 0 18 -610.0986 92.5856 0 0 24 -568.1273 -83.7991 0 0 30 -1971.1567 -44.5014 0 0 36 -145.0786 -26.7736 0 0 42 -500.6037 133.5734 0 0 48 -174.6069 -67.1256 0 0 54 -27.5982 16.5372 0 0 60 26.4080 -105.1145 0 0 66 -82.7467 111.6002 0 0 72 -153.5837 -6.3182 0 0 78 -202.5389 49.1935 0 0 84 -0.5081 -214.1115 0 0 90 -54.9145 222.3202 0 0 96 53.5718 -68.1936 0 0 102 -103.9606 23.1192 0 0 108 29.1308 -114.4378 0 0 114 34.6351 145.9444 0 0 120 18.5061 -72.7990 0 0 126 -93.4479 14.3230 0 0 132 61.9865 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-68.7850 2.9771 20 0 -28 -40.8012 -17.5260 20 0 -22 -56.8936 41.5535 20 0 -16 58.3513 -50.8837 20 0 -10 26.9618 36.8724 20 0 -4 48.3255 -24.8100 20 0 2 -31.6010 30.1482 20 0 8 -37.4988 -39.2162 20 0 14 21.0426 38.6045 20 0 20 71.6118 -36.7020 20 0 26 20.6340 29.7925 20 0 32 82.4627 -12.8203 20 0 38 -12.8274 4.5411 20 0 44 2.8937 -13.1846 20 0 50 -41.7919 29.2726 20 0 56 35.0581 -27.5702 20 0 62 16.7154 11.2225 20 1 -56 64.9754 -24.4434 20 1 -53 -32.8321 31.0479 20 1 -50 5.8252 -10.9616 20 1 -47 -3.1468 -10.3050 20 1 -44 -4.1461 -8.2624 20 1 -41 14.6491 11.0726 20 1 -38 -21.5443 10.5495 20 1 -35 56.8458 -0.4236 20 1 -32 -26.4382 -4.5149 20 1 -29 52.3280 5.0499 20 1 -26 45.4190 10.3978 20 1 -23 15.7923 -9.4957 20 1 -20 -0.0978 0.1734 20 1 -17 -15.9261 -5.6717 20 1 -14 11.7781 -15.7189 20 1 -11 -71.2612 14.6205 20 1 -8 28.8691 24.3920 20 1 -5 -82.2793 -10.5903 20 1 -2 94.3434 -25.7730 20 1 1 -109.0664 -1.3738 20 1 4 4.4801 29.2158 20 1 7 -50.2634 6.3895 20 1 10 -9.8380 -23.2957 20 1 13 -17.3228 -8.6518 20 1 16 -12.4965 -2.2025 20 1 19 24.3431 6.4714 20 1 22 22.7096 8.1086 20 1 25 37.6413 -9.9206 20 1 28 -58.9624 9.5813 20 1 31 -12.2468 8.8546 20 1 34 -8.9517 -7.0524 20 1 37 -14.3385 -13.3368 20 1 40 -27.1829 -7.9887 20 1 43 -19.8767 15.6958 20 1 46 -3.2586 1.0113 20 1 49 -20.0741 -33.8460 20 1 52 -18.7531 2.6185 20 1 55 -20.0349 32.2723 20 1 58 -6.6034 16.1328 20 2 -45 -9.0822 -8.6555 20 2 -42 19.8933 -16.5972 20 2 -39 -13.5423 -4.3300 20 2 -36 54.2405 8.9792 20 2 -33 -59.3266 13.6374 20 2 -30 26.8974 -11.4294 20 2 -27 -30.0276 8.1421 20 2 -24 -3.4222 10.3203 20 2 -21 -58.0999 6.2127 20 2 -18 -18.6696 -9.8816 20 2 -15 60.4681 -20.1499 20 2 -12 11.0195 4.8402 20 2 -9 12.7137 19.3753 20 2 -6 -28.9920 -1.2986 20 2 -3 111.2246 -16.1164 20 2 0 18.9327 -1.0087 20 2 3 -26.7891 18.3214 20 2 6 -94.5744 3.5801 20 2 9 57.3242 -15.4942 20 2 12 -51.8640 2.6716 20 2 15 -4.3262 7.8853 20 2 18 -53.4136 -8.6770 20 2 21 63.9787 -4.8961 20 2 24 57.2684 18.3537 20 2 27 -42.2563 17.0681 20 2 30 44.3575 1.5656 20 2 33 -6.3120 -13.7635 20 2 36 -29.4787 -22.9406 20 2 39 -46.5164 -5.4328 20 2 42 -44.2701 -12.9172 20 2 45 100.6691 -17.3527 20 3 -22 11.0911 6.1615 20 3 -19 -37.9751 27.5068 20 3 -16 17.7343 -6.7715 20 3 -13 23.0111 15.4972 20 3 -10 -29.4829 21.6305 20 3 -7 36.5185 2.3509 20 3 -4 -21.0239 -32.6836 20 3 -1 83.1514 -16.8215 20 3 2 -9.8934 32.4631 20 3 5 -0.5359 13.9901 20 3 8 -5.2576 -30.0660 20 3 11 -3.0636 -13.7655 20 3 14 68.2707 14.1696 20 3 17 -1.9230 24.9030 20 3 20 77.8574 10.9596 20 3 23 6.5102 -1.7137 21 0 -42 24.0181 1.1151 21 0 -36 53.5499 -16.6514 21 0 -30 19.1742 4.4561 21 0 -24 72.5342 2.7563 21 0 -18 54.7019 20.0870 21 0 -12 62.4690 -46.3790 21 0 -6 4.0010 51.5500 21 0 0 59.6801 -51.0766 21 0 6 -53.9248 49.8233 21 0 12 -0.1690 -29.0699 21 0 18 -21.4967 3.2255 21 0 24 21.2984 -6.9372 21 0 30 -31.8859 26.1555 21 0 36 -87.2108 -19.5178 21 0 42 -103.2510 -7.9923 21 1 -28 6.4725 -2.2213 21 1 -25 8.3197 -11.6791 21 1 -22 -19.8846 0.2181 21 1 -19 -55.5875 23.7836 21 1 -16 -9.1338 -0.8429 21 1 -13 25.9704 -14.1300 21 1 -10 22.4153 6.8099 21 1 -7 11.9220 13.8437 21 1 -4 22.2291 -3.2628 21 1 -1 99.4187 -28.8291 21 1 2 -5.0288 17.1513 21 1 5 2.6064 40.8295 21 1 8 -2.2112 -15.9309 21 1 11 41.0224 -32.7355 21 1 14 -25.5949 -1.5476 21 1 17 5.9792 21.9411 21 1 20 12.6082 6.8890 21 1 23 62.5978 -30.7322 21 1 26 -34.6508 23.2528 21 1 29 4.2844 30.5150 ; _shelx_shelxl_version_number 2014/7 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z+1/2' 'x-y, -y, -z+1/2' '-x, -x+y, -z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+5/6' 'x-y+2/3, -y+1/3, -z+5/6' '-x+2/3, -x+y+1/3, -z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+7/6' 'x-y+1/3, -y+2/3, -z+7/6' '-x+1/3, -x+y+2/3, -z+7/6' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z-1/2' '-x+y, y, z-1/2' 'x, x-y, z-1/2' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z-1/6' '-x+y+2/3, y+1/3, z-1/6' 'x+2/3, x-y+1/3, z-1/6' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+1/6' '-x+y+1/3, y+2/3, z+1/6' 'x+1/3, x-y+2/3, z+1/6' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au1 Au 0.57859(4) 0.91192(4) 0.4167 0.0387(2) Uani 1 2 d S T P . . Au2 Au 0.47034(3) 0.81525(3) 0.39600(2) 0.02903(15) Uani 1 1 d . . . . . Au3 Au 0.43207(4) 0.67826(4) 0.38443(2) 0.03181(15) Uani 1 1 d . . . . . Au4 Au 0.34042(4) 0.50818(4) 0.37251(2) 0.0401(2) Uani 0.917(4) 1 d . . . A 1 Au5 Au 0.18716(4) 0.39170(4) 0.38928(2) 0.0333(2) Uani 0.917(4) 1 d . . . A 1 Cu4 Cu 0.34042(4) 0.50818(4) 0.37251(2) 0.0401(2) Uani 0.083(4) 1 d . . . A 2 Cu5 Cu 0.18716(4) 0.39170(4) 0.38928(2) 0.0333(2) Uani 0.083(4) 1 d . . . A 2 Au6 Au 0.19445(3) 0.52537(3) 0.40523(2) 0.03071(15) Uani 1 1 d . . . . . Au7 Au 0.3333 0.57046(4) 0.4167 0.02623(18) Uani 1 2 d S T P A . Au8 Au 0.3333 0.6667 0.40051(2) 0.0248(2) Uani 1 3 d S T P A . S1 S 0.5563(2) 0.9520(2) 0.40091(3) 0.0378(9) Uani 1 1 d . . . . . S2 S 0.4421(3) 0.6306(2) 0.36792(3) 0.0384(9) Uani 1 1 d . . . . . S3 S 0.2448(3) 0.3786(3) 0.37435(3) 0.0384(9) Uani 1 1 d . . . . . S4 S 0.1305(3) 0.3845(2) 0.40523(3) 0.0379(9) Uani 1 1 d . . . . . C1 C 0.6484(10) 0.9938(10) 0.39439(13) 0.040(4) Uani 1 1 d . . . . . C2 C 0.7092(10) 0.9823(10) 0.39782(14) 0.044(4) Uani 1 1 d . . . . . H2 H 0.7021 0.9515 0.4039 0.052 Uiso 1 1 calc R . . . . C3 C 0.7823(11) 1.0161(10) 0.39237(14) 0.052(5) Uani 1 1 d . . . . . H3 H 0.8227 1.0051 0.3945 0.063 Uiso 1 1 calc R . . . . C4 C 0.7952(12) 1.0662(13) 0.38378(15) 0.067(7) Uani 1 1 d . . . . . C5 C 0.7329(11) 1.0760(11) 0.38076(15) 0.053(5) Uani 1 1 d . . . . . H5 H 0.7405 1.1076 0.3748 0.063 Uiso 1 1 calc R . . . . C6 C 0.6597(9) 1.0434(11) 0.38568(14) 0.049(5) Uani 1 1 d . . . . . C7 C 0.5950(13) 1.0587(12) 0.38196(16) 0.060(5) Uani 1 1 d . . . . . H7A H 0.5516 1.0099 0.3790 0.089 Uiso 1 1 calc GR . . . . H7B H 0.6165 1.1006 0.3767 0.089 Uiso 1 1 calc GR . . . . H7C H 0.5748 1.0757 0.3878 0.089 Uiso 1 1 calc GR . . . . C8 C 0.8736(13) 1.1042(13) 0.37799(16) 0.077(8) Uani 1 1 d . . . . . H8A H 0.9082 1.1580 0.3806 0.116 Uiso 1 1 calc GR . . . . H8B H 0.8638 1.1068 0.3706 0.116 Uiso 1 1 calc GR . . . . H8C H 0.8993 1.0723 0.3790 0.116 Uiso 1 1 calc GR . . . . C9 C 0.5232(10) 0.6115(10) 0.36758(13) 0.039(4) Uani 1 1 d . . . . . C10 C 0.5711(10) 0.6243(9) 0.37630(13) 0.040(4) Uani 1 1 d . . . . . H10 H 0.5597 0.6419 0.3826 0.048 Uiso 1 1 calc R . . . . C11 C 0.6373(10) 0.6108(11) 0.37576(16) 0.049(5) Uani 1 1 d . . . . . H11 H 0.6703 0.6202 0.3816 0.059 Uiso 1 1 calc R . . . . C12 C 0.6524(13) 0.5841(14) 0.36658(18) 0.063(6) Uani 1 1 d . . . . . C13 C 0.6028(13) 0.5696(14) 0.35790(17) 0.071(7) Uani 1 1 d . . . . . H13 H 0.6137 0.5517 0.3516 0.085 Uiso 1 1 calc R . . . . C14 C 0.5357(13) 0.5819(12) 0.35853(17) 0.058(5) Uani 1 1 d . . . . . C15 C 0.4838(13) 0.5619(17) 0.34895(18) 0.081(8) Uani 1 1 d . . . . . H15A H 0.4957 0.6110 0.3454 0.121 Uiso 1 1 calc GR . . . . H15B H 0.4277 0.5333 0.3510 0.121 Uiso 1 1 calc GR . . . . H15C H 0.4945 0.5283 0.3443 0.121 Uiso 1 1 calc GR . . . . C16 C 0.7247(16) 0.572(2) 0.3663(2) 0.110(11) Uani 1 1 d . . . . . H16A H 0.7466 0.5786 0.3733 0.165 Uiso 1 1 calc GR . . . . H16B H 0.7653 0.6116 0.3617 0.165 Uiso 1 1 calc GR . . . . H16C H 0.7084 0.5186 0.3638 0.165 Uiso 1 1 calc GR . . . . C17 C 0.1773(11) 0.3542(12) 0.36369(13) 0.044(4) Uani 1 1 d . . . . . C18 C 0.2017(14) 0.4013(13) 0.35475(14) 0.059(5) Uani 1 1 d . . . . . H18 H 0.2530 0.4474 0.3545 0.071 Uiso 1 1 calc R . . . . C19 C 0.1530(13) 0.3821(15) 0.34632(19) 0.070(6) Uani 1 1 d . . . . . H19 H 0.1687 0.4171 0.3406 0.085 Uiso 1 1 calc R . . . . C20 C 0.0791(16) 0.3101(18) 0.34615(17) 0.077(7) Uani 1 1 d . . . . . C21 C 0.0580(12) 0.2628(14) 0.35538(16) 0.065(6) Uani 1 1 d . . . . . H21 H 0.0080 0.2152 0.3556 0.077 Uiso 1 1 calc R . . . . C22 C 0.1066(9) 0.2829(12) 0.36389(14) 0.053(5) Uani 1 1 d . . . . . C23 C 0.0789(12) 0.2300(12) 0.37315(15) 0.065(6) Uani 1 1 d . . . . . H23A H 0.0207 0.2017 0.3734 0.098 Uiso 1 1 calc GR . . . . H23B H 0.1005 0.2622 0.3794 0.098 Uiso 1 1 calc GR . . . . H23C H 0.0973 0.1915 0.3727 0.098 Uiso 1 1 calc GR . . . . C24 C 0.0217(16) 0.289(2) 0.3370(2) 0.114(12) Uani 1 1 d . . . . . H24A H 0.0016 0.2330 0.3351 0.172 Uiso 1 1 calc GR . . . . H24B H 0.0497 0.3231 0.3311 0.172 Uiso 1 1 calc GR . . . . H24C H -0.0229 0.2958 0.3390 0.172 Uiso 1 1 calc GR . . . . C25 C 0.0280(11) 0.3405(10) 0.40329(12) 0.046(5) Uani 1 1 d . . . . . C26 C -0.0095(10) 0.3882(13) 0.40331(12) 0.048(5) Uani 1 1 d . . . . . H26 H 0.0229 0.4443 0.4038 0.057 Uiso 1 1 calc R . . . . C27 C -0.0937(13) 0.3543(16) 0.40256(15) 0.071(7) Uani 1 1 d . . . . . H27 H -0.1150 0.3890 0.4026 0.085 Uiso 1 1 calc R . . . . C28 C -0.1443(13) 0.2755(16) 0.4018(2) 0.098(11) Uani 1 1 d . . . . . C29 C -0.1045(14) 0.2250(14) 0.40220(19) 0.084(9) Uani 1 1 d . . . . . H29 H -0.1373 0.1689 0.4020 0.101 Uiso 1 1 calc R . . . . C30 C -0.0204(11) 0.2576(11) 0.40288(15) 0.057(6) Uani 1 1 d . . . . . C31 C 0.0139(15) 0.2026(12) 0.40253(18) 0.082(8) Uani 1 1 d . . . . . H31A H 0.0552 0.2210 0.3972 0.123 Uiso 1 1 calc GR . . . . H31B H -0.0284 0.1485 0.4009 0.123 Uiso 1 1 calc GR . . . . H31C H 0.0371 0.2028 0.4093 0.123 Uiso 1 1 calc GR . . . . C32 C -0.2319(14) 0.233(2) 0.4025(3) 0.142(16) Uani 1 1 d . . . . . H32A H -0.2546 0.1955 0.3967 0.213 Uiso 1 1 calc GR . . . . H32B H -0.2504 0.2717 0.4021 0.213 Uiso 1 1 calc GR . . . . H32C H -0.2487 0.2044 0.4090 0.213 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.0332(3) 0.0332(3) 0.0373(5) -0.0022(2) 0.0022(2) 0.0074(4) Au2 0.0273(3) 0.0271(3) 0.0283(3) 0.0009(2) 0.0012(2) 0.0104(2) Au3 0.0350(3) 0.0337(3) 0.0279(3) 0.0004(2) 0.0041(2) 0.0181(3) Au4 0.0374(4) 0.0415(4) 0.0392(4) 0.0004(3) 0.0016(3) 0.0181(3) Au5 0.0375(4) 0.0301(3) 0.0286(3) -0.0014(3) 0.0024(3) 0.0142(3) Cu4 0.0374(4) 0.0415(4) 0.0392(4) 0.0004(3) 0.0016(3) 0.0181(3) Cu5 0.0375(4) 0.0301(3) 0.0286(3) -0.0014(3) 0.0024(3) 0.0142(3) Au6 0.0295(3) 0.0279(3) 0.0303(3) -0.0013(2) -0.0012(2) 0.0111(2) Au7 0.0289(4) 0.0258(3) 0.0250(4) 0.00041(16) 0.0008(3) 0.0144(2) Au8 0.0243(3) 0.0243(3) 0.0257(5) 0.000 0.000 0.01215(14) S1 0.035(2) 0.030(2) 0.042(2) -0.0002(17) -0.0003(18) 0.0108(17) S2 0.045(2) 0.035(2) 0.033(2) -0.0010(17) 0.0019(18) 0.0182(19) S3 0.040(2) 0.042(2) 0.033(2) -0.0044(17) 0.0022(17) 0.0199(19) S4 0.041(2) 0.028(2) 0.034(2) -0.0016(16) 0.0001(18) 0.0094(18) C1 0.034(9) 0.033(9) 0.037(9) 0.001(7) 0.006(7) 0.004(7) C2 0.041(10) 0.030(9) 0.043(10) 0.001(7) -0.003(8) 0.005(8) C3 0.041(10) 0.036(10) 0.043(10) 0.001(8) 0.009(8) -0.009(8) C4 0.043(11) 0.061(13) 0.047(12) -0.020(10) 0.022(9) -0.011(10) C5 0.039(10) 0.044(11) 0.050(11) -0.001(9) -0.007(9) 0.002(9) C6 0.014(7) 0.060(12) 0.052(11) -0.003(9) -0.002(7) 0.004(8) C7 0.073(14) 0.054(12) 0.057(13) 0.014(10) 0.006(11) 0.036(11) C8 0.056(13) 0.064(14) 0.055(13) -0.011(11) 0.020(11) -0.012(11) C9 0.041(9) 0.036(9) 0.034(9) 0.003(7) 0.014(7) 0.014(8) C10 0.053(11) 0.029(8) 0.036(9) -0.005(7) 0.007(8) 0.020(8) C11 0.026(9) 0.053(11) 0.063(12) -0.003(9) -0.005(8) 0.015(8) C12 0.054(13) 0.077(15) 0.078(15) -0.017(12) 0.000(11) 0.047(12) C13 0.067(15) 0.089(17) 0.059(14) -0.030(12) 0.006(11) 0.041(13) C14 0.057(13) 0.056(12) 0.062(13) -0.010(10) 0.005(10) 0.029(11) C15 0.061(14) 0.13(2) 0.075(16) -0.024(15) 0.000(12) 0.062(16) C16 0.09(2) 0.17(3) 0.12(2) -0.04(2) 0.004(18) 0.10(2) C17 0.044(10) 0.066(12) 0.035(9) 0.001(8) 0.017(8) 0.037(10) C18 0.072(14) 0.060(13) 0.042(11) -0.006(9) -0.002(10) 0.031(12) C19 0.051(13) 0.076(16) 0.069(15) 0.006(12) 0.007(11) 0.021(12) C20 0.086(18) 0.12(2) 0.044(12) 0.016(13) -0.002(12) 0.070(18) C21 0.044(11) 0.083(16) 0.056(13) -0.021(12) 0.004(10) 0.024(11) C22 0.015(8) 0.076(14) 0.047(11) -0.008(10) 0.009(7) 0.007(8) C23 0.046(11) 0.054(12) 0.050(12) -0.013(10) 0.009(9) -0.010(10) C24 0.076(18) 0.18(3) 0.078(19) 0.003(19) -0.046(15) 0.06(2) C25 0.050(11) 0.032(9) 0.023(8) 0.001(7) -0.006(7) -0.004(8) C26 0.036(9) 0.070(13) 0.026(8) 0.004(8) 0.012(7) 0.018(9) C27 0.055(13) 0.11(2) 0.036(11) -0.006(12) -0.008(9) 0.033(14) C28 0.042(13) 0.082(18) 0.083(18) -0.043(14) 0.018(12) -0.035(13) C29 0.068(16) 0.057(14) 0.088(18) -0.032(13) 0.027(13) 0.001(12) C30 0.042(11) 0.041(11) 0.055(12) -0.001(9) 0.025(9) -0.005(9) C31 0.093(18) 0.039(11) 0.065(15) -0.021(10) 0.010(13) -0.005(12) C32 0.043(14) 0.15(3) 0.17(3) -0.12(3) -0.014(17) 0.002(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Au2 Au1 Au2 106.83(3) 10_455 . Au7 Au1 Au2 53.407(16) 2_665 10_455 Au7 Au1 Au2 53.420(16) 2_665 . S1 Au1 Au2 46.20(10) 10_455 10_455 S1 Au1 Au2 141.38(11) . 10_455 S1 Au1 Au2 141.39(11) 10_455 . S1 Au1 Au2 46.20(10) . . S1 Au1 Au7 94.30(11) . 2_665 S1 Au1 Au7 94.29(11) 10_455 2_665 S1 Au1 S1 171.4(2) 10_455 . Au3 Au2 Au1 138.87(2) . . Au3 Au2 Au1 148.76(2) 2_665 . Au3 Au2 Au3 66.49(3) . 2_665 Au3 Au2 Au4 65.77(2) 2_665 2_665 Au3 Au2 Au4 62.01(2) . 2_665 Au3 Au2 Au5 123.95(3) 2_665 2_665 Au3 Au2 Au5 63.73(2) . 2_665 Au3 Au2 Cu4 62.01(2) . 2_665 Au3 Au2 Cu4 65.77(2) 2_665 2_665 Au3 Au2 Cu5 63.73(2) . 2_665 Au3 Au2 Cu5 123.95(3) 2_665 2_665 Au3 Au2 Au6 111.36(3) . 3_565 Au3 Au2 Au6 57.10(2) . 2_665 Au3 Au2 Au6 107.13(2) 2_665 2_665 Au3 Au2 Au7 105.61(3) . 2_665 Au3 Au2 Au8 58.50(2) . . Au4 Au2 Au1 136.09(3) 2_665 . Au4 Au2 Au6 114.43(3) 2_665 2_665 Au5 Au2 Au1 87.29(2) 2_665 . Au5 Au2 Au4 69.28(2) 2_665 2_665 Au5 Au2 Au6 64.21(2) 2_665 2_665 Cu4 Au2 Au1 136.09(3) 2_665 . Cu4 Au2 Au6 114.43(3) 2_665 2_665 Cu5 Au2 Au1 87.29(2) 2_665 . Cu5 Au2 Cu4 69.28(2) 2_665 2_665 Cu5 Au2 Au6 64.21(2) 2_665 2_665 Au6 Au2 Au1 84.799(19) 2_665 . Au6 Au2 Au1 90.68(2) 3_565 . Au6 Au2 Au3 58.76(2) 3_565 2_665 Au6 Au2 Au4 119.46(3) 3_565 2_665 Au6 Au2 Au5 167.70(3) 3_565 2_665 Au6 Au2 Cu4 119.46(3) 3_565 2_665 Au6 Au2 Cu5 167.70(3) 3_565 2_665 Au6 Au2 Au6 103.53(3) 3_565 2_665 Au7 Au2 Au1 55.23(2) 2_665 . Au7 Au2 Au3 107.17(3) 2_665 2_665 Au7 Au2 Au4 167.15(3) 2_665 2_665 Au7 Au2 Au5 109.46(2) 2_665 2_665 Au7 Au2 Cu4 167.15(3) 2_665 2_665 Au7 Au2 Cu5 109.46(2) 2_665 2_665 Au7 Au2 Au6 59.948(18) 2_665 3_565 Au7 Au2 Au6 56.021(16) 2_665 2_665 Au7 Au2 Au8 59.28(3) 2_665 . Au8 Au2 Au1 114.43(3) . . Au8 Au2 Au3 57.21(2) . 2_665 Au8 Au2 Au4 108.72(3) . 2_665 Au8 Au2 Au5 111.71(2) . 2_665 Au8 Au2 Cu4 108.72(3) . 2_665 Au8 Au2 Cu5 111.71(2) . 2_665 Au8 Au2 Au6 58.372(17) . 3_565 Au8 Au2 Au6 55.565(16) . 2_665 S1 Au2 Au1 43.51(10) . . S1 Au2 Au3 153.30(11) . . S1 Au2 Au3 125.68(11) . 2_665 S1 Au2 Au4 99.27(11) . 2_665 S1 Au2 Au5 92.66(11) . 2_665 S1 Au2 Cu4 99.27(11) . 2_665 S1 Au2 Cu5 92.66(11) . 2_665 S1 Au2 Au6 94.21(11) . 3_565 S1 Au2 Au6 125.65(11) . 2_665 S1 Au2 Au7 93.55(11) . 2_665 S1 Au2 Au8 147.78(11) . . Au2 Au3 Au2 114.24(3) . 3_565 Au2 Au3 Au3 105.50(2) 3_565 2_665 Au2 Au3 Au3 58.50(2) . 2_665 Au2 Au3 Au3 108.38(2) . 3_565 Au2 Au3 Au3 55.01(2) 3_565 3_565 Au2 Au3 Au4 59.16(2) 3_565 . Au2 Au3 Au4 168.76(3) 3_565 2_665 Au2 Au3 Au4 164.94(3) . . Au2 Au3 Au4 63.09(2) . 2_665 Au2 Au3 Au5 120.39(3) 3_565 2_665 Au2 Au3 Au5 61.43(2) . 2_665 Au2 Au3 Cu4 63.09(2) . 2_665 Au2 Au3 Cu4 168.76(3) 3_565 2_665 Au2 Au3 Cu5 120.39(3) 3_565 2_665 Au2 Au3 Cu5 61.43(2) . 2_665 Au2 Au3 Au6 66.93(2) . 2_665 Au3 Au3 Au3 60.0 3_565 2_665 Au3 Au3 Au4 56.57(2) 3_565 . Au3 Au3 Au4 108.62(2) 2_665 . Au4 Au3 Au3 114.51(2) 2_665 3_565 Au4 Au3 Au3 63.51(2) 2_665 2_665 Au4 Au3 Au4 120.39(3) 2_665 . Au4 Au3 Au5 68.85(2) 2_665 2_665 Au5 Au3 Au3 167.381(18) 2_665 3_565 Au5 Au3 Au3 114.81(3) 2_665 2_665 Au5 Au3 Au4 133.51(3) 2_665 . Cu4 Au3 Au3 63.51(2) 2_665 2_665 Cu4 Au3 Au3 114.51(2) 2_665 3_565 Cu4 Au3 Cu5 68.85(2) 2_665 2_665 Cu5 Au3 Au3 167.381(18) 2_665 3_565 Cu5 Au3 Au3 114.81(3) 2_665 2_665 Au6 Au3 Au2 59.82(2) 2_665 3_565 Au6 Au3 Au3 103.16(2) 2_665 3_565 Au6 Au3 Au3 108.431(17) 2_665 2_665 Au6 Au3 Au4 114.40(3) 2_665 . Au6 Au3 Au4 124.22(3) 2_665 2_665 Au6 Au3 Au5 66.65(2) 2_665 2_665 Au6 Au3 Cu4 124.22(3) 2_665 2_665 Au6 Au3 Cu5 66.65(2) 2_665 2_665 Au8 Au3 Au2 61.312(17) . . Au8 Au3 Au2 59.882(17) . 3_565 Au8 Au3 Au3 55.283(15) . 3_565 Au8 Au3 Au3 55.283(15) . 2_665 Au8 Au3 Au4 105.62(2) . . Au8 Au3 Au4 111.78(2) . 2_665 Au8 Au3 Au5 112.11(3) . 2_665 Au8 Au3 Cu4 111.78(2) . 2_665 Au8 Au3 Cu5 112.11(3) . 2_665 Au8 Au3 Au6 59.63(2) . 2_665 S2 Au3 Au2 101.27(11) . 3_565 S2 Au3 Au2 144.49(11) . . S2 Au3 Au3 112.96(11) . 2_665 S2 Au3 Au3 91.41(11) . 3_565 S2 Au3 Au4 44.57(11) . . S2 Au3 Au4 82.05(10) . 2_665 S2 Au3 Au5 101.16(11) . 2_665 S2 Au3 Cu4 82.05(10) . 2_665 S2 Au3 Cu5 101.16(11) . 2_665 S2 Au3 Au6 137.97(11) . 2_665 S2 Au3 Au8 146.63(11) . . Au2 Au4 Au3 55.066(19) 3_565 . Au3 Au4 Au2 54.90(2) 3_565 3_565 Au3 Au4 Au3 59.93(3) 3_565 . S2 Au4 Au2 99.54(11) . 3_565 S2 Au4 Au3 96.18(11) . 3_565 S2 Au4 Au3 46.89(10) . . S3 Au4 Au2 89.94(11) . 3_565 S3 Au4 Au3 143.56(11) . . S3 Au4 Au3 93.19(11) . 3_565 S3 Au4 S2 169.38(15) . . Au2 Au5 Au3 54.829(19) 3_565 3_565 Au2 Au5 Au6 59.392(19) 3_565 . Au3 Au5 Au6 53.221(19) 3_565 . S3 Au5 Au2 90.32(11) . 3_565 S3 Au5 Au3 91.18(11) . 3_565 S3 Au5 Au6 141.80(11) . . S3 Au5 S4 169.44(16) . . S4 Au5 Au2 92.18(11) . 3_565 S4 Au5 Au3 98.65(10) . 3_565 S4 Au5 Au6 46.60(10) . . Au3 Cu4 Au2 54.90(2) 3_565 3_565 S2 Cu4 Au2 99.54(11) . 3_565 S2 Cu4 Au3 96.18(11) . 3_565 S3 Cu4 Au2 89.94(11) . 3_565 S3 Cu4 Au3 93.19(11) . 3_565 S3 Cu4 S2 169.38(15) . . Au2 Cu5 Au3 54.829(19) 3_565 3_565 S3 Cu5 Au2 90.32(11) . 3_565 S3 Cu5 Au3 91.18(11) . 3_565 S3 Cu5 S4 169.44(16) . . S4 Cu5 Au2 92.18(11) . 3_565 S4 Cu5 Au3 98.65(10) . 3_565 Au2 Au6 Au2 106.74(3) 2_665 3_565 Au2 Au6 Au5 56.392(19) 3_565 . Au2 Au6 Au5 115.97(3) 2_665 . Au2 Au6 Au6 113.12(3) 2_665 10_455 Au3 Au6 Au2 61.41(2) 3_565 2_665 Au3 Au6 Au2 55.957(19) 3_565 3_565 Au3 Au6 Au5 60.12(2) 3_565 . Au3 Au6 Au6 161.163(17) 3_565 10_455 Au3 Au6 Au7 108.70(2) 3_565 3_565 Au6 Au6 Au2 113.86(3) 10_455 3_565 Au6 Au6 Au5 130.54(3) 10_455 . Au7 Au6 Au2 110.82(3) 3_565 3_565 Au7 Au6 Au2 114.79(3) . 2_665 Au7 Au6 Au2 56.768(18) . 3_565 Au7 Au6 Au2 59.197(19) 3_565 2_665 Au7 Au6 Au3 105.26(2) . 3_565 Au7 Au6 Au5 165.86(3) 3_565 . Au7 Au6 Au5 103.55(3) . . Au7 Au6 Au6 59.218(17) . 10_455 Au7 Au6 Au6 57.682(16) 3_565 10_455 Au7 Au6 Au7 69.79(3) . 3_565 Au8 Au6 Au2 57.145(16) . 3_565 Au8 Au6 Au2 60.142(18) . 2_665 Au8 Au6 Au3 58.65(3) . 3_565 Au8 Au6 Au5 106.26(3) . . Au8 Au6 Au6 102.64(2) . 10_455 Au8 Au6 Au7 60.16(2) . . Au8 Au6 Au7 59.61(2) . 3_565 S4 Au6 Au2 88.52(11) . 3_565 S4 Au6 Au2 141.58(11) . 2_665 S4 Au6 Au3 103.88(10) . 3_565 S4 Au6 Au5 45.03(10) . . S4 Au6 Au6 90.87(10) . 10_455 S4 Au6 Au7 147.39(10) . 3_565 S4 Au6 Au7 103.15(11) . . S4 Au6 Au8 145.67(11) . . Au1 Au7 Au7 150.000(1) 3_565 2_665 Au1 Au7 Au7 150.000(1) 3_565 3_565 Au2 Au7 Au1 71.358(19) 3_565 3_565 Au2 Au7 Au1 71.345(19) 11_565 3_565 Au2 Au7 Au2 142.70(4) 11_565 3_565 Au2 Au7 Au6 127.495(18) 3_565 10_455 Au2 Au7 Au6 127.491(18) 11_565 2_665 Au2 Au7 Au6 60.868(18) 3_565 2_665 Au2 Au7 Au6 60.864(17) 11_565 10_455 Au2 Au7 Au7 104.037(18) 3_565 2_665 Au2 Au7 Au7 104.030(17) 11_565 3_565 Au2 Au7 Au7 108.138(17) 11_565 2_665 Au2 Au7 Au7 108.143(17) 3_565 3_565 Au6 Au7 Au1 99.70(2) 12 3_565 Au6 Au7 Au1 100.977(19) 10_455 3_565 Au6 Au7 Au1 100.983(19) 2_665 3_565 Au6 Au7 Au1 99.71(2) . 3_565 Au6 Au7 Au2 67.222(18) . 3_565 Au6 Au7 Au2 67.214(18) 12 11_565 Au6 Au7 Au2 119.679(18) 12 3_565 Au6 Au7 Au2 119.666(18) . 11_565 Au6 Au7 Au6 63.11(2) 12 2_665 Au6 Au7 Au6 112.83(3) 12 10_455 Au6 Au7 Au6 160.59(4) 12 . Au6 Au7 Au6 112.84(3) . 2_665 Au6 Au7 Au6 158.04(4) 10_455 2_665 Au6 Au7 Au6 63.11(2) . 10_455 Au6 Au7 Au7 105.680(19) 12 3_565 Au6 Au7 Au7 104.576(19) 10_455 2_665 Au6 Au7 Au7 55.781(19) 12 2_665 Au6 Au7 Au7 54.434(19) 10_455 3_565 Au6 Au7 Au7 105.688(19) . 2_665 Au6 Au7 Au7 55.783(19) . 3_565 Au6 Au7 Au7 104.582(19) 2_665 3_565 Au6 Au7 Au7 54.437(19) 2_665 2_665 Au7 Au7 Au7 60.000(1) 2_665 3_565 Au8 Au7 Au1 131.780(18) 10_455 3_565 Au8 Au7 Au1 131.789(18) . 3_565 Au8 Au7 Au2 156.59(3) 10_455 3_565 Au8 Au7 Au2 60.554(18) . 3_565 Au8 Au7 Au2 60.558(18) 10_455 11_565 Au8 Au7 Au2 156.59(3) . 11_565 Au8 Au7 Au6 59.081(15) . 2_665 Au8 Au7 Au6 59.629(15) . . Au8 Au7 Au6 106.32(2) . 12 Au8 Au7 Au6 106.31(2) 10_455 . Au8 Au7 Au6 59.077(14) 10_455 10_455 Au8 Au7 Au6 105.07(2) 10_455 2_665 Au8 Au7 Au6 59.621(15) 10_455 12 Au8 Au7 Au6 105.07(2) . 10_455 Au8 Au7 Au7 54.760(14) . 3_565 Au8 Au7 Au7 54.761(14) . 2_665 Au8 Au7 Au7 54.752(14) 10_455 2_665 Au8 Au7 Au7 54.751(14) 10_455 3_565 Au8 Au7 Au8 96.43(4) 10_455 . Au2 Au8 Au2 115.894(15) 2_665 3_565 Au2 Au8 Au2 115.898(15) 2_665 . Au2 Au8 Au2 115.898(15) . 3_565 Au3 Au8 Au2 62.91(2) . 3_565 Au3 Au8 Au2 60.19(2) . . Au3 Au8 Au2 119.25(4) 3_565 . Au3 Au8 Au2 60.19(2) 2_665 2_665 Au3 Au8 Au2 119.24(4) . 2_665 Au3 Au8 Au2 60.19(2) 3_565 3_565 Au3 Au8 Au2 62.91(2) 3_565 2_665 Au3 Au8 Au2 119.24(4) 2_665 3_565 Au3 Au8 Au2 62.92(2) 2_665 . Au3 Au8 Au3 69.43(3) 2_665 . Au3 Au8 Au3 69.43(3) 3_565 . Au3 Au8 Au3 69.43(3) 2_665 3_565 Au3 Au8 Au6 115.67(2) 2_665 . Au3 Au8 Au6 61.718(19) . 2_665 Au3 Au8 Au6 115.66(2) . 3_565 Au3 Au8 Au6 122.41(3) 2_665 2_665 Au3 Au8 Au6 61.725(19) 3_565 . Au3 Au8 Au6 122.41(3) . . Au3 Au8 Au6 115.66(2) 3_565 2_665 Au3 Au8 Au6 61.719(19) 2_665 3_565 Au3 Au8 Au6 122.41(3) 3_565 3_565 Au3 Au8 Au7 107.649(17) 2_665 3_565 Au3 Au8 Au7 107.649(17) . 2_665 Au3 Au8 Au7 107.647(17) 3_565 . Au3 Au8 Au7 175.866(15) . 3_565 Au3 Au8 Au7 175.866(15) 2_665 . Au3 Au8 Au7 175.866(14) 3_565 2_665 Au3 Au8 Au7 112.626(16) 2_665 2_665 Au3 Au8 Au7 112.623(16) . . Au3 Au8 Au7 112.626(17) 3_565 3_565 Au6 Au8 Au2 61.484(18) 3_565 . Au6 Au8 Au2 61.487(17) 2_665 3_565 Au6 Au8 Au2 176.81(2) 2_665 2_665 Au6 Au8 Au2 67.287(18) 2_665 . Au6 Au8 Au2 176.80(2) . . Au6 Au8 Au2 176.81(2) 3_565 3_565 Au6 Au8 Au2 61.489(17) . 2_665 Au6 Au8 Au2 67.290(17) 3_565 2_665 Au6 Au8 Au2 67.293(17) . 3_565 Au6 Au8 Au6 115.338(16) . 2_665 Au6 Au8 Au6 115.336(16) 3_565 . Au6 Au8 Au6 115.339(16) 3_565 2_665 Au6 Au8 Au7 119.12(4) 2_665 3_565 Au6 Au8 Au7 119.12(4) 3_565 . Au6 Au8 Au7 60.206(17) . . Au6 Au8 Au7 61.314(17) 3_565 2_665 Au6 Au8 Au7 60.210(17) 2_665 2_665 Au6 Au8 Au7 119.11(4) . 2_665 Au6 Au8 Au7 61.312(17) 2_665 . Au6 Au8 Au7 60.210(17) 3_565 3_565 Au6 Au8 Au7 61.308(17) . 3_565 Au7 Au8 Au2 121.19(2) . . Au7 Au8 Au2 116.03(2) 2_665 3_565 Au7 Au8 Au2 60.175(18) . 3_565 Au7 Au8 Au2 121.20(2) 3_565 3_565 Au7 Au8 Au2 60.168(18) 2_665 . Au7 Au8 Au2 121.20(2) 2_665 2_665 Au7 Au8 Au2 116.02(2) 3_565 . Au7 Au8 Au2 116.03(2) . 2_665 Au7 Au8 Au2 60.178(18) 3_565 2_665 Au7 Au8 Au7 70.48(3) . 2_665 Au7 Au8 Au7 70.48(3) 3_565 2_665 Au7 Au8 Au7 70.49(3) . 3_565 Au1 S1 Au2 90.29(14) . . C1 S1 Au1 105.1(6) . . C1 S1 Au2 111.4(6) . . Au4 S2 Au3 88.54(15) . . Cu4 S2 Au3 88.54(15) . . C9 S2 Au3 110.8(6) . . C9 S2 Au4 100.6(6) . . C9 S2 Cu4 100.6(6) . . Au4 S3 Au5 97.93(16) . . Cu4 S3 Cu5 97.93(16) . . C17 S3 Au4 107.3(7) . . C17 S3 Au5 109.9(5) . . C17 S3 Cu4 107.3(7) . . C17 S3 Cu5 109.9(5) . . Au5 S4 Au6 88.37(14) . . Cu5 S4 Au6 88.37(14) . . C25 S4 Au5 107.0(6) . . C25 S4 Cu5 107.0(6) . . C25 S4 Au6 112.1(7) . . C2 C1 S1 121.6(13) . . C2 C1 C6 120.5(15) . . C6 C1 S1 117.9(14) . . C1 C2 H2 119.9 . . C1 C2 C3 120.3(17) . . C3 C2 H2 119.9 . . C2 C3 H3 119.9 . . C4 C3 C2 120(2) . . C4 C3 H3 120.0 . . C3 C4 C8 121(2) . . C5 C4 C3 117.0(18) . . C5 C4 C8 122(2) . . C4 C5 H5 117.3 . . C4 C5 C6 125.4(19) . . C6 C5 H5 117.3 . . C1 C6 C7 121.5(16) . . C5 C6 C1 116.6(17) . . C5 C6 C7 121.9(18) . . C6 C7 H7A 109.5 . . C6 C7 H7B 109.5 . . C6 C7 H7C 109.5 . . H7A C7 H7B 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . C4 C8 H8A 109.5 . . C4 C8 H8B 109.5 . . C4 C8 H8C 109.5 . . H8A C8 H8B 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . C10 C9 S2 121.2(12) . . C14 C9 S2 117.6(15) . . C14 C9 C10 121.2(17) . . C9 C10 H10 119.9 . . C9 C10 C11 120.2(16) . . C11 C10 H10 119.9 . . C10 C11 H11 120.4 . . C12 C11 C10 119.1(18) . . C12 C11 H11 120.4 . . C11 C12 C13 120.3(18) . . C11 C12 C16 117(2) . . C13 C12 C16 123(2) . . C12 C13 H13 119.8 . . C12 C13 C14 120.4(18) . . C14 C13 H13 119.8 . . C9 C14 C13 119(2) . . C9 C14 C15 124.6(19) . . C13 C14 C15 116.7(18) . . C14 C15 H15A 109.5 . . C14 C15 H15B 109.5 . . C14 C15 H15C 109.5 . . H15A C15 H15B 109.5 . . H15A C15 H15C 109.5 . . H15B C15 H15C 109.5 . . C12 C16 H16A 109.5 . . C12 C16 H16B 109.5 . . C12 C16 H16C 109.5 . . H16A C16 H16B 109.5 . . H16A C16 H16C 109.5 . . H16B C16 H16C 109.5 . . C18 C17 S3 119.8(15) . . C22 C17 S3 118.7(14) . . C22 C17 C18 120.8(18) . . C17 C18 H18 119.4 . . C19 C18 C17 121(2) . . C19 C18 H18 119.4 . . C18 C19 H19 119.9 . . C18 C19 C20 120(2) . . C20 C19 H19 119.9 . . C19 C20 C21 116(2) . . C19 C20 C24 121(2) . . C21 C20 C24 122(3) . . C20 C21 H21 118.4 . . C22 C21 C20 123(2) . . C22 C21 H21 118.4 . . C17 C22 C23 122.7(17) . . C21 C22 C17 118(2) . . C21 C22 C23 119.2(18) . . C22 C23 H23A 109.5 . . C22 C23 H23B 109.5 . . C22 C23 H23C 109.5 . . H23A C23 H23B 109.5 . . H23A C23 H23C 109.5 . . H23B C23 H23C 109.5 . . C20 C24 H24A 109.5 . . C20 C24 H24B 109.5 . . C20 C24 H24C 109.5 . . H24A C24 H24B 109.5 . . H24A C24 H24C 109.5 . . H24B C24 H24C 109.5 . . C26 C25 S4 120.3(13) . . C30 C25 S4 120.9(17) . . C30 C25 C26 118.4(18) . . C25 C26 H26 118.8 . . C27 C26 C25 122(2) . . C27 C26 H26 118.8 . . C26 C27 H27 118.5 . . C28 C27 C26 123(3) . . C28 C27 H27 118.5 . . C27 C28 C29 114(2) . . C27 C28 C32 128(3) . . C32 C28 C29 117(3) . . C28 C29 H29 118.2 . . C30 C29 C28 124(2) . . C30 C29 H29 118.2 . . C25 C30 C29 118(2) . . C25 C30 C31 122.1(18) . . C29 C30 C31 119.6(19) . . C30 C31 H31A 109.5 . . C30 C31 H31B 109.5 . . C30 C31 H31C 109.5 . . H31A C31 H31B 109.5 . . H31A C31 H31C 109.5 . . H31B C31 H31C 109.5 . . C28 C32 H32A 109.5 . . C28 C32 H32B 109.5 . . C28 C32 H32C 109.5 . . H32A C32 H32B 109.5 . . H32A C32 H32C 109.5 . . H32B C32 H32C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Au1 Au2 3.3400(8) 10_455 Au1 Au2 3.3401(8) . Au1 Au7 2.8960(12) 2_665 Au1 S1 2.299(4) . Au1 S1 2.300(4) 10_455 Au2 Au3 2.9251(9) 2_665 Au2 Au3 2.8108(8) . Au2 Au4 3.0633(9) 2_665 Au2 Au5 3.0198(9) 2_665 Au2 Cu4 3.0633(9) 2_665 Au2 Cu5 3.0198(9) 2_665 Au2 Au6 3.1204(9) 2_665 Au2 Au6 2.8791(9) 3_565 Au2 Au7 2.8309(7) 2_665 Au2 Au8 2.8418(6) . Au2 S1 2.411(4) . Au3 Au2 2.9248(9) 3_565 Au3 Au3 3.1459(11) 3_565 Au3 Au3 3.1459(11) 2_665 Au3 Au4 3.2535(10) . Au3 Au4 3.0335(10) 2_665 Au3 Au5 3.0832(9) 2_665 Au3 Cu4 3.0335(10) 2_665 Au3 Cu5 3.0832(9) 2_665 Au3 Au6 2.8478(9) 2_665 Au3 Au8 2.7619(9) . Au3 S2 2.376(4) . Au4 Au2 3.0632(9) 3_565 Au4 Au3 3.0337(10) 3_565 Au4 S2 2.284(4) . Au4 S3 2.273(5) . Au5 Au2 3.0198(9) 3_565 Au5 Au3 3.0832(9) 3_565 Au5 Au6 3.2649(9) . Au5 S3 2.311(4) . Au5 S4 2.311(4) . Cu4 Au2 3.0632(9) 3_565 Cu4 Au3 3.0337(10) 3_565 Cu4 S2 2.284(4) . Cu4 S3 2.273(5) . Cu5 Au2 3.0198(9) 3_565 Cu5 Au3 3.0832(9) 3_565 Cu5 S3 2.311(4) . Cu5 S4 2.311(4) . Au6 Au2 2.8794(9) 2_665 Au6 Au2 3.1207(9) 3_565 Au6 Au3 2.8481(9) 3_565 Au6 Au6 2.9618(12) 10_455 Au6 Au7 2.8063(6) . Au6 Au7 2.8529(6) 3_565 Au6 Au8 2.7900(6) . Au6 S4 2.373(4) . Au7 Au1 2.8960(12) 3_565 Au7 Au2 2.8305(6) 11_565 Au7 Au2 2.8311(7) 3_565 Au7 Au6 2.8529(6) 2_665 Au7 Au6 2.8531(6) 10_455 Au7 Au6 2.8066(6) 12 Au7 Au7 3.2375(14) 2_665 Au7 Au7 3.2375(14) 3_565 Au7 Au8 2.8051(9) 10_455 Au7 Au8 2.8052(9) . Au8 Au2 2.8418(6) 3_565 Au8 Au2 2.8418(6) 2_665 Au8 Au3 2.7619(9) 2_665 Au8 Au3 2.7619(9) 3_565 Au8 Au6 2.7900(6) 3_565 Au8 Au6 2.7900(6) 2_665 Au8 Au7 2.8054(9) 3_565 Au8 Au7 2.8054(9) 2_665 S1 C1 1.766(17) . S2 C9 1.790(18) . S3 C17 1.797(19) . S4 C25 1.747(19) . C1 C2 1.38(3) . C1 C6 1.43(3) . C2 H2 0.9500 . C2 C3 1.42(2) . C3 H3 0.9500 . C3 C4 1.41(3) . C4 C5 1.37(3) . C4 C8 1.52(3) . C5 H5 0.9500 . C5 C6 1.39(2) . C6 C7 1.51(3) . C7 H7A 0.9800 . C7 H7B 0.9800 . C7 H7C 0.9800 . C8 H8A 0.9800 . C8 H8B 0.9800 . C8 H8C 0.9800 . C9 C10 1.40(2) . C9 C14 1.38(2) . C10 H10 0.9500 . C10 C11 1.44(2) . C11 H11 0.9500 . C11 C12 1.39(3) . C12 C13 1.42(3) . C12 C16 1.53(3) . C13 H13 0.9500 . C13 C14 1.44(3) . C14 C15 1.52(3) . C15 H15A 0.9800 . C15 H15B 0.9800 . C15 H15C 0.9800 . C16 H16A 0.9800 . C16 H16B 0.9800 . C16 H16C 0.9800 . C17 C18 1.40(3) . C17 C22 1.38(3) . C18 H18 0.9500 . C18 C19 1.37(3) . C19 H19 0.9500 . C19 C20 1.42(3) . C20 C21 1.44(3) . C20 C24 1.53(3) . C21 H21 0.9500 . C21 C22 1.37(3) . C22 C23 1.49(3) . C23 H23A 0.9800 . C23 H23B 0.9800 . C23 H23C 0.9800 . C24 H24A 0.9800 . C24 H24B 0.9800 . C24 H24C 0.9800 . C25 C26 1.44(3) . C25 C30 1.40(2) . C26 H26 0.9500 . C26 C27 1.43(3) . C27 H27 0.9500 . C27 C28 1.35(3) . C28 C29 1.52(4) . C28 C32 1.48(3) . C29 H29 0.9500 . C29 C30 1.43(3) . C30 C31 1.52(3) . C31 H31A 0.9800 . C31 H31B 0.9800 . C31 H31C 0.9800 . C32 H32A 0.9800 . C32 H32B 0.9800 . C32 H32C 0.9800 . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 1 -2 0 1907.71 91.69 1 1 0 2134.59 91.59 1 1 0 2174.68 116.09 2 -1 0 1969.1 91.79 2 -1 0 2133.49 115.99 -1 -1 0 2068.19 91.69 -1 -1 0 1858.31 91.59 0 -3 0 19.8 2.8 3 0 0 10.2 4.2 3 0 0 13.3 2.4 3 -3 0 21 3.6 0 3 0 46.6 7 2 2 0 115.49 10 2 -4 0 108.69 7.5 4 -2 0 115.19 7 4 -2 0 113.79 8.5 -2 -2 0 95.19 5.8 1 4 0 24.3 8.4 4 -5 0 21.4 5.7 -1 -4 0 19.1 4 5 -1 0 11.9 6.6 5 -1 0 14.7 3.9 1 -5 0 17.3 4.6 4 1 0 10.1 6.8 4 1 0 11.5 2.8 5 -4 0 5.7 6.7 5 -4 0 15 5.5 -1 5 0 28.4 10.7 3 3 0 1350.46 78.19 3 -6 0 1306.97 61.39 6 -3 0 1325.67 61.29 6 -3 0 1433.76 77.89 -3 -3 0 1297.17 60.89 0 -6 0 2620.24 120.19 6 0 0 2837.12 120.29 6 0 0 2538.25 152.68 0 6 0 2529.35 153.58 6 -6 0 2759.42 120.79 2 5 0 26 8.1 5 -7 0 43 5.7 7 -2 0 43.6 4.6 7 -2 0 18.4 6.7 -2 -5 0 23.7 3.8 2 -7 0 31.8 5 5 2 0 18 2.8 5 2 0 22.2 7.1 -2 7 0 30.3 9.7 7 -5 0 15.7 5 7 -5 0 20.6 6.3 7 -8 0 5820.62 260.87 1 7 0 5394.46 330.17 -1 -7 0 5660.03 260.07 8 -1 0 5925.71 329.77 8 -1 0 6059.19 260.47 4 4 0 1020.3 60.49 4 -8 0 965.4 47.2 -4 -4 0 1023.2 46.4 8 -4 0 1048.9 59.99 8 -4 0 1023.5 47.2 7 1 0 5534.45 329.67 7 1 0 6077.09 260.17 1 -8 0 5705.93 260.27 -1 8 0 5697.53 330.37 8 -7 0 5836.52 260.87 3 6 0 76.89 11.3 6 -9 0 81.19 8.1 -3 -6 0 90.39 6.2 9 -3 0 88.49 10.3 9 -3 0 103.99 7.6 6 3 0 83.69 10.7 3 -9 0 79.99 7.3 9 -6 0 108.79 12 -6 -3 0 80.69 6.2 -3 9 0 79.29 13.4 9 0 0 900.31 56.39 9 0 0 960.7 43.5 0 -9 0 949.8 43.5 9 -9 0 978 44.8 0 9 0 911.31 58.09 2 8 0 44.1 11 8 -10 0 52.39 7.8 10 -2 0 43.9 9.3 -2 -8 0 44.8 4.9 10 -2 0 53.19 5.7 5 -10 0 102.29 9 5 5 0 102.29 12.6 10 -5 0 123.09 13.4 -5 -5 0 121.39 7.6 10 -5 0 117.19 9.3 2 -10 0 39.9 6.4 8 2 0 32.5 9.5 8 2 0 54.89 4.9 10 -8 0 45.3 7.2 -2 10 0 47.7 13.6 10 -11 0 288.37 17.8 1 10 0 314.67 25.8 11 -1 0 264.27 22.6 11 -1 0 296.07 15.3 -1 -10 0 279.97 15.2 4 7 0 106.99 14.4 7 -11 0 133.09 11.5 -4 -7 0 120.49 7.2 11 -4 0 108.19 9 11 -4 0 89.39 11.6 7 4 0 108.19 13.5 4 -11 0 128.29 10.5 11 -7 0 112.39 10.2 11 -7 0 88.09 12.2 -7 -4 0 129.69 8.3 -4 11 0 121.59 17.5 10 1 0 290.77 14.8 10 1 0 282.97 23 1 -11 0 283.77 15.9 -1 11 0 268.77 26.6 11 -10 0 302.17 17.8 3 9 0 112.59 16 9 -12 0 132.19 12.3 12 -3 0 121.09 9.4 -3 -9 0 116.99 8 12 -3 0 109.59 13.5 6 -12 0 382.96 20.1 6 6 0 335.17 27.7 -6 -6 0 342.57 17.4 12 -6 0 356.96 25 12 -6 0 360.16 18.8 9 3 0 117.49 14.6 9 3 0 135.69 8.3 3 -12 0 127.49 11.4 -3 12 0 133.99 19.4 -9 -3 0 117.89 8.9 12 -9 0 129.49 11.4 12 -9 0 142.39 17.1 12 0 0 1352.46 83.19 0 -12 0 1377.56 63.89 12 0 0 1420.06 63.89 0 12 0 1298.27 84.19 12 -12 0 1481.75 65.69 11 -13 0 178.98 15.1 2 11 0 227.58 24 -2 -11 0 162.88 11 13 -2 0 185.08 12 13 -2 0 166.08 19.8 5 8 0 251.07 24.4 8 -13 0 296.27 18.3 13 -5 0 282.07 23.4 13 -5 0 269.67 15.9 8 5 0 276.77 24.2 5 -13 0 276.37 17.1 -5 13 0 246.78 28 13 -8 0 265.57 16.2 -8 -5 0 275.47 14.7 13 -8 0 284.27 23.4 11 2 0 186.98 20.7 2 -13 0 182.08 13 11 2 0 160.18 10.3 13 -11 0 181.88 14.4 -2 13 0 219.88 26 13 -14 0 1188.58 55.89 1 13 0 1196.78 72.69 14 -1 0 1122.89 53.79 14 -1 0 1131.99 70.99 -1 -13 0 1148.09 53.49 10 -14 0 106.99 11.6 4 10 0 95.59 17.4 14 -4 0 84.49 14.3 14 -4 0 110.69 9.6 7 -14 0 1436.96 65.79 7 7 0 1349.56 84.49 14 -7 0 1354.76 64.99 14 -7 0 1438.36 83.89 10 4 0 100.39 15.9 4 -14 0 102.39 10.2 14 -10 0 127.59 12.1 -10 -4 0 100.99 9.6 -4 14 0 88.99 20.7 13 1 0 1164.98 69.59 1 -14 0 1144.29 52.69 13 1 0 1047.7 52.09 -1 14 0 1073.69 70.89 14 -13 0 1204.08 54.49 12 -15 0 33.3 10.2 3 12 0 46.6 16.3 15 -3 0 14.1 11.8 15 -3 0 25.7 6.9 9 -15 0 0.3 9.4 6 9 0 -4 13.9 15 -6 0 4.4 7.1 15 -6 0 -6.1 12.3 9 6 0 17.7 13.7 6 -15 0 -2.8 8.8 15 -9 0 -10.5 12.5 15 -9 0 10.6 7.8 -6 15 0 9.2 19.9 12 3 0 28.8 13.9 3 -15 0 26.4 8.1 -3 15 0 10.9 20.1 15 -12 0 29.8 8.9 -12 -3 0 28.2 7 15 0 0 560.44 38.2 15 0 0 540.85 26.5 0 15 0 535.05 39.1 15 -15 0 520.05 29.1 2 14 0 18.2 14.3 14 -16 0 24 9.4 16 -2 0 23.6 12.8 16 -2 0 22.4 6.4 5 11 0 39.1 15.6 11 -16 0 35.3 10.5 16 -5 0 46.7 7.7 16 -5 0 42 13.6 8 -16 0 178.58 16.4 8 8 0 199.18 23.6 -8 16 0 197.78 26.4 16 -8 0 193.78 14.2 16 -8 0 200.98 22.7 5 -16 0 49.2 9.3 11 5 0 40 14.9 -5 16 0 46.7 21.3 16 -11 0 47 9.4 14 2 0 30.2 13.2 2 -16 0 10.6 7.1 16 -14 0 23.5 9.1 -2 16 0 23.1 17.8 1 16 0 93.69 18.9 16 -17 0 86.69 11.9 17 -1 0 95.79 16.4 13 -17 0 14.7 9.2 4 13 0 3.1 13.6 17 -4 0 -5.4 6.3 17 -4 0 4.4 12.2 10 -17 0 159.98 15 7 10 0 130.79 19.3 17 -7 0 139.19 17 17 -7 0 151.38 12.1 10 7 0 134.59 18.9 7 -17 0 127.89 12.3 17 -10 0 123.89 17.6 -7 17 0 150.68 25.9 17 -10 0 155.88 12.4 4 -17 0 -10.3 7.4 13 4 0 5.6 13.2 17 -13 0 2.5 8.1 -4 17 0 -14.8 18 16 1 0 89.09 16.3 17 -16 0 76.89 11 -1 17 0 73.19 18.6 3 15 0 273.27 28.6 15 -18 0 245.28 18.5 18 -3 0 248.38 15.6 18 -3 0 270.27 25.3 6 12 0 39.3 16.3 12 -18 0 -3 9.2 18 -6 0 35.7 13 18 -6 0 19.8 7.2 9 9 0 36.5 15 9 -18 0 48.2 9.9 -9 18 0 52.59 22.5 18 -9 0 44.6 14.1 18 -9 0 45 8.3 6 -18 0 18.7 8.2 12 6 0 17.2 14.7 18 -12 0 22.9 8.5 -6 18 0 18.4 21.3 15 3 0 279.37 25.4 -3 18 0 186.98 25.2 18 -15 0 252.07 17.7 18 0 0 -4 14.4 0 18 0 -24.2 15.4 18 -18 0 -12 9.5 17 -19 0 -10.2 10 2 17 0 -23.3 15.9 19 -2 0 7.5 14.4 14 -19 0 -7 9.6 5 14 0 7.9 15.4 19 -5 0 9.3 12.8 19 -5 0 4.7 7.2 8 11 0 17.8 15.5 11 -19 0 41.3 10.4 19 -8 0 40.9 14.5 -11 19 0 32.7 23 19 -8 0 27.4 7.9 8 -19 0 43.4 9.7 11 8 0 42.1 15.7 -8 19 0 29.6 23.5 19 -11 0 30.5 8.7 19 -11 0 39.9 14.5 14 5 0 2 15.1 5 -19 0 -6.2 8 -5 19 0 -11.2 22 19 -14 0 -3.7 8.7 17 2 0 -0.3 14.5 19 -17 0 -4.8 9.4 -2 19 0 -5.7 16.9 19 -20 0 140.59 14.8 1 19 0 130.49 21.3 20 -1 0 142.69 20.6 4 16 0 5.4 16.9 16 -20 0 1.3 9.8 20 -4 0 6 7.4 20 -4 0 19 14.9 7 13 0 360.46 32.6 13 -20 0 376.96 24.1 20 -7 0 399.36 22.4 20 -7 0 408.76 31.3 10 10 0 110.89 20.6 10 -20 0 121.99 13 20 -10 0 165.28 13.3 -10 20 0 120.29 28 20 -10 0 134.19 19.1 13 7 0 438.96 34.9 7 -20 0 389.16 22.9 20 -13 0 367.56 22.7 -7 20 0 361.76 42.7 16 4 0 15.9 15.1 -4 20 0 -14.3 19.6 20 -16 0 -5.6 9.3 19 1 0 134.69 20.7 -1 20 0 90.89 21.6 20 -19 0 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1.2 6.2 5 3 32 -0.9 5.1 3 -8 32 5.5 4.4 -5 0 -32 3587.04 162.78 0 5 -32 3301.07 206.78 5 -5 -32 3655.23 205.18 5 -5 -32 3603.54 162.98 0 -5 32 3490.35 162.08 5 0 32 3871.61 162.68 5 0 32 3607.84 204.88 3 2 -32 328.97 22.8 2 -5 -32 309.57 17.6 3 2 -32 334.27 16.4 5 -3 32 295.17 15.8 6 -1 -32 1935.61 115.39 -1 -5 -32 2008.2 91.39 6 -1 -32 1984 90.29 5 -6 32 2021.4 90.69 1 5 32 1980.8 113.49 9 -4 -32 55.09 6.6 9 -4 -32 39.8 9.3 -5 9 -32 44.6 14 -4 -5 -32 50.09 8.4 5 -9 32 54.29 6.3 4 5 32 49.6 7.1 -4 10 -32 66.79 16.2 10 -6 -32 37.9 8.6 10 -6 -32 36.9 7.1 -6 -4 -32 42.2 8.1 6 4 32 37.1 7.4 4 -10 32 34.2 5.8 -1 7 -32 2807.72 176.48 7 -6 -32 3006 138.29 7 -6 -32 3108.99 174.48 -6 -1 -32 2988.8 138.19 1 -7 32 3147.08 137.59 6 1 32 3171.28 173.98 4 -6 -32 238.68 16 2 4 -32 235.88 19.1 2 4 -32 266.97 12.8 4 -6 -32 251.17 15.1 6 -2 32 228.68 12.9 5 1 -32 1966.8 112.69 1 -6 -32 1873.71 89.09 5 1 -32 1916.61 87.69 6 -5 32 2090.89 88.39 -1 6 32 1823.62 110.79 8 -2 -32 2019.1 93.29 -2 -6 -32 2017.5 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32 2262.07 103.79 6 7 32 2197.98 131.09 14 -8 -32 903.41 43.3 14 -8 -32 921.91 56.29 -8 -6 -32 862.21 43.5 -6 14 -32 918.31 63.69 6 -14 32 874.41 42.7 8 6 32 864.51 54.19 11 -8 -32 312.47 22.5 11 -8 -32 321.57 17.9 -3 11 -32 297.07 29.7 -8 -3 -32 305.87 18.4 8 3 32 316.07 22.1 3 -11 32 315.07 16.9 8 -8 -32 139.99 11.8 8 -8 -32 143.19 14.2 0 8 -32 135.19 16.9 8 0 32 144.69 9.7 8 0 32 146.09 13.1 0 -8 32 140.59 8.2 5 -8 -32 15.3 6.8 3 5 -32 -4.2 10.3 8 -3 32 -4.5 4.4 6 2 -32 2041.6 91.89 2 -8 -32 2103.99 93.49 6 2 -32 1996.5 118.79 -2 8 32 1905.01 116.99 8 -6 32 2115.99 93.09 9 -1 -32 37.9 5.2 -1 -8 -32 44.2 9.1 9 -1 -32 34.5 9.6 1 8 32 36.6 8 8 -9 32 34.4 6.4 12 -4 -32 69.29 12.4 -4 -8 -32 63.39 10.7 12 -4 -32 65.59 7.6 4 8 32 52.49 10.6 8 -12 32 66.19 8.4 -7 -8 -32 291.77 18.9 -8 15 -32 261.47 31.8 15 -7 -32 263.37 17 15 -7 -32 273.27 25.2 8 -15 32 250.77 16.7 7 8 32 249.97 22.7 16 -9 -32 108.89 16.9 16 -9 -32 112.49 11.8 -7 16 -32 112.19 27.7 -9 -7 -32 119.69 13.1 7 -16 32 141.19 12.7 9 7 32 120.89 14.4 -4 13 -32 148.69 24.9 13 -9 -32 104.09 14.6 -9 -4 -32 100.59 11.7 13 -9 -32 108.89 11.2 4 -13 32 92.29 8.6 9 4 32 95.39 12.4 10 -9 -32 297.97 17.4 -1 10 -32 311.87 28.1 10 -9 -32 308.77 22.2 -9 -1 -32 284.07 17.4 1 -10 32 308.07 15.3 9 1 32 278.37 21.4 9 1 32 292.77 16.1 7 -9 -32 695.23 34.8 2 7 -32 656.43 46.6 2 7 -32 716.13 33.1 9 -2 32 703.53 34.3 9 -2 32 802.32 43.8 4 -9 -32 57.99 8.4 5 4 -32 45.4 11.2 9 -5 32 55.59 6.4 1 -9 -32 41.1 8.3 8 1 -32 28.6 11 8 1 -32 35.6 4.4 -1 9 32 41.1 10.2 9 -8 32 32 6.5 -2 -9 -32 891.21 43.8 11 -2 -32 899.01 56.79 11 -2 -32 973.9 42.7 2 9 32 871.71 54.59 9 -11 32 903.71 43.6 -5 -9 -32 236.38 17.3 14 -5 -32 253.07 15.4 14 -5 -32 222.68 23.9 9 -14 32 298.37 18.1 5 9 32 206.88 21.2 -9 17 -32 40.7 23.6 17 -8 -32 8 7.9 17 -8 -32 25.6 13.3 8 9 32 8.4 10.6 9 -17 32 10.2 6.8 18 -10 -32 2.9 8.6 -8 18 -32 -14.1 25.6 18 -10 -32 -2.2 13.1 8 -18 32 1.5 7.6 10 8 32 7.3 11.1 15 -10 -32 291.67 20.1 15 -10 -32 335.97 27.8 -5 15 -32 385.96 39.4 -10 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