#------------------------------------------------------------------------------ #$Date: 2017-11-14 10:01:52 +0200 (Tue, 14 Nov 2017) $ #$Revision: 203147 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/80/1548022.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1548022 loop_ _publ_author_name 'Christopher H. Hendon' 'Aron Walsh' 'Norinobu Akiyama' 'Yosuke Konno' 'Takashi Kajiwara' 'Tasuku Ito' 'Hiroshi Kitagawa' 'Ken Sakai' _publ_section_title ; One-dimensional Magnus-type platinum double salts ; _journal_name_full 'Nature Communications' _journal_page_first 11950 _journal_paper_doi 10.1038/ncomms11950 _journal_volume 7 _journal_year 2016 _chemical_formula_sum 'C34 H36 N6 O10 Pt3' _chemical_formula_weight 1273.96 _space_group_IT_number 15 _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90.00 _cell_angle_beta 116.718(4) _cell_angle_gamma 90.00 _cell_formula_units_Z 4 _cell_length_a 23.042(5) _cell_length_b 9.2011(19) _cell_length_c 20.049(4) _cell_measurement_reflns_used 2253 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 27.75 _cell_measurement_theta_min 2.27 _cell_volume 3796.8(14) _diffrn_ambient_temperature 296(2) _diffrn_detector_area_resol_mean 8.366 _diffrn_measured_fraction_theta_full 0.961 _diffrn_measured_fraction_theta_max 0.961 _diffrn_measurement_device 'Bruker SMART APEX CCD-detector diffractometer' _diffrn_measurement_method \w _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0903 _diffrn_reflns_av_sigmaI/netI 0.1217 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 11724 _diffrn_reflns_theta_full 27.75 _diffrn_reflns_theta_max 27.75 _diffrn_reflns_theta_min 2.27 _exptl_absorpt_coefficient_mu 11.089 _exptl_absorpt_correction_T_max 0.694171 _exptl_absorpt_correction_T_min 0.224352 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details '(SADABS; Sheldrick, 1996)' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 2.229 _exptl_crystal_description needle _exptl_crystal_F_000 2384 _exptl_crystal_size_max 0.45 _exptl_crystal_size_mid 0.038 _exptl_crystal_size_min 0.01 _refine_diff_density_max 3.056 _refine_diff_density_min -2.523 _refine_diff_density_rms 0.278 _refine_ls_extinction_coef 'not refined' _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.905 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 244 _refine_ls_number_reflns 4296 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.905 _refine_ls_R_factor_all 0.1263 _refine_ls_R_factor_gt 0.0596 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0758P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1269 _refine_ls_wR_factor_ref 0.1499 _reflns_d_resolution_high 0.7633 _reflns_number_gt 2308 _reflns_number_total 4296 _reflns_threshold_expression >2\s(I) _cod_data_source_file ncomms11950-s2.cif _cod_data_source_block yellow_needle_compound_3 _cod_depositor_comments ; The following automatic conversions were performed: '_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic' according to the built-in table from CIF Core dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29. Automatic conversion script Id: cif_fix_values 5376 2017-05-30 11:51:03Z andrius ; _cod_original_cell_volume 3796.7(13) _cod_original_sg_symbol_H-M 'C2/c ' _cod_database_code 1548022 _shelx_title ' konno1 in C2/c 2000/11/27 12:05:55 015 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 858.29 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Pt1 Pt 1.02048(2) 0.17249(7) 0.33509(3) 0.03881(19) Uani 1 1 d . . . Pt2 Pt 1.0000 0.0000 0.5000 0.0439(3) Uani 1 2 d S . . N1 N 0.9510(5) 0.0151(12) 0.2973(7) 0.040(3) Uani 1 1 d . . . H1 H 0.9461 -0.0342 0.3309 0.049 Uiso 1 1 calc R . . O1 O 0.9144(5) 0.0345(12) 0.1705(6) 0.055(3) Uani 1 1 d . . . O2 O 1.0688(5) 0.1557(11) 0.5299(6) 0.054(3) Uani 1 1 d . . . O3 O 1.0722(5) -0.1263(12) 0.5036(7) 0.063(3) Uani 1 1 d . . . O4 O 1.1713(6) 0.1843(12) 0.5587(7) 0.069(3) Uani 1 1 d . . . O5 O 1.1765(6) -0.1148(15) 0.5320(9) 0.100(5) Uani 1 1 d . . . N2 N 0.9657(6) 0.3142(13) 0.3556(6) 0.047(3) Uani 1 1 d . . . N3 N 1.0859(5) 0.3289(14) 0.3850(6) 0.044(3) Uani 1 1 d . . . C8 C 0.9015(7) 0.3023(19) 0.3338(10) 0.060(5) Uani 1 1 d . . . H8 H 0.8793 0.2235 0.3043 0.072 Uiso 1 1 calc R . . C9 C 0.8680(9) 0.401(2) 0.3530(11) 0.071(6) Uani 1 1 d . . . H9 H 0.8246 0.3838 0.3406 0.086 Uiso 1 1 calc R . . C10 C 0.8982(8) 0.5261(18) 0.3910(9) 0.054(4) Uani 1 1 d . . . H10 H 0.8752 0.5957 0.4031 0.065 Uiso 1 1 calc R . . C11 C 0.9644(7) 0.5454(16) 0.4108(8) 0.042(4) Uani 1 1 d . . . H11 H 0.9864 0.6286 0.4358 0.051 Uiso 1 1 calc R . . C12 C 0.9961(6) 0.4359(17) 0.3917(8) 0.043(4) Uani 1 1 d . . . C13 C 1.0642(7) 0.4437(15) 0.4088(8) 0.037(3) Uani 1 1 d . . . C14 C 1.1062(8) 0.5567(16) 0.4481(8) 0.049(4) Uani 1 1 d . . . H14 H 1.0912 0.6357 0.4649 0.059 Uiso 1 1 calc R . . C15 C 1.1707(8) 0.549(2) 0.4616(9) 0.060(5) Uani 1 1 d . . . H15 H 1.1993 0.6233 0.4877 0.071 Uiso 1 1 calc R . . C16 C 1.1922(8) 0.433(2) 0.4365(9) 0.060(5) Uani 1 1 d . . . H16 H 1.2353 0.4276 0.4447 0.072 Uiso 1 1 calc R . . C17 C 1.1497(7) 0.3245(18) 0.3993(8) 0.048(4) Uani 1 1 d . . . H17 H 1.1646 0.2447 0.3829 0.058 Uiso 1 1 calc R . . C1 C 0.9133(6) -0.0195(14) 0.2283(9) 0.040(4) Uani 1 1 d . . . C2 C 0.8658(7) -0.1464(18) 0.2157(8) 0.050(4) Uani 1 1 d . . . C3 C 0.9031(10) -0.2872(18) 0.2224(11) 0.074(6) Uani 1 1 d . . . H3A H 0.8745 -0.3686 0.2135 0.111 Uiso 1 1 calc R . . H3B H 0.9385 -0.2944 0.2716 0.111 Uiso 1 1 calc R . . H3C H 0.9197 -0.2872 0.1862 0.111 Uiso 1 1 calc R . . C4 C 0.8089(8) -0.133(2) 0.1371(9) 0.076(6) Uani 1 1 d . . . H4A H 0.8251 -0.1355 0.1006 0.114 Uiso 1 1 calc R . . H4B H 0.7866 -0.0429 0.1330 0.114 Uiso 1 1 calc R . . H4C H 0.7793 -0.2125 0.1285 0.114 Uiso 1 1 calc R . . C5 C 0.8393(9) -0.146(2) 0.2739(10) 0.079(6) Uani 1 1 d . . . H5A H 0.8030 -0.2114 0.2583 0.119 Uiso 1 1 calc R . . H5B H 0.8255 -0.0496 0.2784 0.119 Uiso 1 1 calc R . . H5C H 0.8728 -0.1769 0.3214 0.119 Uiso 1 1 calc R . . C6 C 1.1220(9) 0.1108(17) 0.5374(9) 0.050(4) Uani 1 1 d . . . C7 C 1.1263(8) -0.0570(19) 0.5246(10) 0.058(5) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pt1 0.0297(3) 0.0466(3) 0.0319(3) -0.0076(3) 0.0065(2) 0.0018(3) Pt2 0.0389(5) 0.0456(5) 0.0399(5) -0.0058(4) 0.0113(4) 0.0064(4) N1 0.042(7) 0.032(6) 0.039(7) 0.000(6) 0.011(6) -0.007(5) O1 0.061(7) 0.067(7) 0.031(6) 0.013(5) 0.015(5) -0.014(6) O2 0.046(6) 0.038(6) 0.075(8) -0.006(6) 0.025(6) 0.013(5) O3 0.040(6) 0.054(7) 0.082(8) -0.023(6) 0.016(6) 0.003(5) O4 0.061(7) 0.058(7) 0.091(9) -0.013(7) 0.037(7) -0.012(6) O5 0.053(8) 0.085(10) 0.169(15) -0.027(10) 0.057(10) 0.006(7) N2 0.044(7) 0.053(8) 0.032(6) -0.011(6) 0.007(6) 0.001(6) N3 0.035(6) 0.058(8) 0.028(6) 0.002(6) 0.004(5) 0.005(6) C8 0.032(8) 0.072(12) 0.069(11) -0.013(10) 0.016(8) 0.001(8) C9 0.045(10) 0.082(14) 0.095(15) -0.003(12) 0.039(11) 0.005(9) C10 0.061(11) 0.049(10) 0.059(11) -0.005(8) 0.032(9) 0.005(8) C11 0.046(9) 0.041(8) 0.036(8) 0.002(6) 0.015(7) 0.005(7) C12 0.026(7) 0.064(10) 0.036(8) -0.001(7) 0.010(6) 0.011(7) C13 0.047(9) 0.040(8) 0.030(7) 0.001(6) 0.023(7) 0.007(7) C14 0.064(11) 0.041(8) 0.034(8) 0.003(7) 0.015(8) -0.007(8) C15 0.045(10) 0.078(12) 0.044(10) -0.005(9) 0.009(8) -0.010(9) C16 0.032(9) 0.091(13) 0.053(10) 0.002(10) 0.015(8) -0.007(8) C17 0.035(8) 0.059(9) 0.042(8) -0.012(8) 0.010(7) -0.006(8) C1 0.025(7) 0.032(8) 0.052(9) 0.006(7) 0.008(7) 0.007(6) C2 0.054(9) 0.061(10) 0.044(9) -0.008(8) 0.030(8) -0.018(8) C3 0.090(15) 0.053(11) 0.074(13) -0.009(10) 0.033(12) -0.004(10) C4 0.042(9) 0.132(18) 0.046(10) -0.002(11) 0.013(8) -0.043(11) C5 0.071(12) 0.116(17) 0.066(12) -0.010(12) 0.044(10) -0.034(12) C6 0.063(11) 0.045(9) 0.045(9) -0.010(7) 0.027(9) -0.002(8) C7 0.040(10) 0.072(12) 0.058(11) -0.005(9) 0.019(9) 0.006(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 N2 Pt1 N3 80.2(5) . . N2 Pt1 O1 171.7(4) . 2_755 N3 Pt1 O1 94.0(5) . 2_755 N2 Pt1 N1 94.5(5) . . N3 Pt1 N1 171.6(5) . . O1 Pt1 N1 90.7(5) 2_755 . N2 Pt1 Pt1 108.7(3) . 2_755 N3 Pt1 Pt1 109.8(3) . 2_755 O1 Pt1 Pt1 78.7(3) 2_755 2_755 N1 Pt1 Pt1 78.0(4) . 2_755 N2 Pt1 Pt2 76.1(4) . . N3 Pt1 Pt2 102.8(3) . . O1 Pt1 Pt2 99.7(3) 2_755 . N1 Pt1 Pt2 69.5(4) . . Pt1 Pt1 Pt2 147.416(19) 2_755 . O3 Pt2 O3 180.0(7) 5_756 . O3 Pt2 O2 97.3(4) 5_756 . O3 Pt2 O2 82.7(4) . . O3 Pt2 O2 82.7(4) 5_756 5_756 O3 Pt2 O2 97.3(4) . 5_756 O2 Pt2 O2 180.0(8) . 5_756 O3 Pt2 Pt1 98.6(4) 5_756 . O3 Pt2 Pt1 81.4(4) . . O2 Pt2 Pt1 65.3(3) . . O2 Pt2 Pt1 114.7(3) 5_756 . C1 N1 Pt1 127.4(10) . . C1 O1 Pt1 128.4(10) . 2_755 C6 O2 Pt2 113.7(10) . . C7 O3 Pt2 112.9(10) . . C8 N2 C12 118.2(13) . . C8 N2 Pt1 126.0(11) . . C12 N2 Pt1 115.6(9) . . C13 N3 C17 119.1(13) . . C13 N3 Pt1 115.3(9) . . C17 N3 Pt1 125.6(10) . . N2 C8 C9 122.5(16) . . C8 C9 C10 120.4(16) . . C9 C10 C11 118.2(15) . . C12 C11 C10 117.9(14) . . N2 C12 C11 122.5(13) . . N2 C12 C13 114.5(12) . . C11 C12 C13 123.0(14) . . N3 C13 C14 120.7(14) . . N3 C13 C12 114.4(13) . . C14 C13 C12 124.9(14) . . C15 C14 C13 118.8(15) . . C16 C15 C14 120.1(16) . . C17 C16 C15 118.9(15) . . C16 C17 N3 122.4(15) . . O1 C1 N1 126.6(13) . . O1 C1 C2 116.8(13) . . N1 C1 C2 116.5(13) . . C3 C2 C4 110.2(15) . . C3 C2 C1 107.4(12) . . C4 C2 C1 108.9(13) . . C3 C2 C5 109.5(15) . . C4 C2 C5 109.3(14) . . C1 C2 C5 111.6(14) . . O4 C6 O2 124.9(15) . . O4 C6 C7 118.8(15) . . O2 C6 C7 116.1(15) . . O5 C7 O3 123.2(17) . . O5 C7 C6 122.3(16) . . O3 C7 C6 114.5(14) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Pt1 N2 1.983(12) . Pt1 N3 1.997(12) . Pt1 O1 2.007(10) 2_755 Pt1 N1 2.035(11) . Pt1 Pt1 3.1043(13) 2_755 Pt1 Pt2 3.8827(9) . Pt2 O3 2.004(10) 5_756 Pt2 O3 2.004(10) . Pt2 O2 2.017(10) . Pt2 O2 2.017(10) 5_756 N1 C1 1.301(18) . O1 C1 1.271(17) . O1 Pt1 2.007(10) 2_755 O2 C6 1.237(18) . O3 C7 1.292(19) . O4 C6 1.224(18) . O5 C7 1.220(18) . N2 C8 1.345(18) . N2 C12 1.346(18) . N3 C13 1.344(17) . N3 C17 1.367(17) . C8 C9 1.35(2) . C9 C10 1.39(2) . C10 C11 1.40(2) . C11 C12 1.40(2) . C12 C13 1.449(19) . C13 C14 1.40(2) . C14 C15 1.39(2) . C15 C16 1.37(2) . C16 C17 1.36(2) . C1 C2 1.542(19) . C2 C3 1.53(2) . C2 C4 1.54(2) . C2 C5 1.54(2) . C6 C7 1.58(2) . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 152392.78 202765.73 3266.90 o 6 0 0 347910.34 428181.06 6339.41 o 8 0 0 112254.62 123315.95 2536.56 o 10 0 0 133319.97 134662.75 3462.82 o 12 0 0 70349.58 68947.63 2933.61 o 14 0 0 3468.73 3927.68 1089.69 o 16 0 0 63.18 -1235.60 1235.60 o 18 0 0 6247.16 4360.57 2842.97 o 20 0 0 10148.12 8407.50 3379.19 o 22 0 0 5502.47 4714.67 3874.94 o 24 0 0 5973.07 6404.27 4229.04 o 26 0 0 4861.83 8063.51 4846.20 o 1 1 0 336979.78 348666.94 7279.54 o 3 1 0 201546.02 209491.67 3792.19 o 5 1 0 168271.77 183337.55 4793.76 o 7 1 0 93829.80 111226.39 7049.57 o 9 1 0 45507.39 50224.54 2262.73 o 11 1 0 45868.40 48280.37 1463.36 o 13 1 0 30348.64 33998.00 1286.10 o 15 1 0 13666.62 14354.71 1326.27 o 17 1 0 3003.63 4979.95 1260.98 o 19 1 0 139.25 1378.78 2438.28 o 21 1 0 319.60 2723.12 2275.96 o 23 1 0 21.48 5519.71 2761.21 o 25 1 0 43.12 -2130.29 3047.21 o 0 2 0 13945.78 12181.26 1203.96 o 2 2 0 3401.84 2679.37 618.60 o 4 2 0 239.73 352.81 568.06 o 6 2 0 31.98 -1.30 522.79 o 8 2 0 6060.22 5883.71 667.06 o 10 2 0 24947.51 27146.67 2374.35 o 12 2 0 21150.32 20513.24 1065.95 o 14 2 0 33619.38 34990.27 1400.69 o 16 2 0 50440.96 49810.39 1862.54 o 18 2 0 39707.40 39432.12 1889.72 o 20 2 0 34076.39 30432.89 2996.17 o 22 2 0 30185.84 32926.92 3325.66 o 24 2 0 21979.97 22343.07 8827.37 o 26 2 0 12291.23 14196.15 6485.21 o 1 3 0 56433.51 50053.09 2584.98 o 3 3 0 7689.96 7923.82 729.94 o 5 3 0 54113.54 46612.14 2043.96 o 7 3 0 7375.20 6763.46 1083.54 o 9 3 0 8392.22 10539.72 1078.17 o 11 3 0 7821.15 8134.30 1086.57 o 13 3 0 32035.20 31842.65 1363.65 o 15 3 0 35693.34 34489.89 1460.05 o 17 3 0 30460.40 28686.63 1475.28 o 19 3 0 59876.21 54390.79 2349.64 o 21 3 0 64787.40 59787.82 2993.69 o 23 3 0 46718.01 45843.05 3811.47 o 25 3 0 29750.44 25620.83 4729.85 o 0 4 0 423.28 202.35 1123.02 o 2 4 0 14395.20 13716.92 1140.00 o 4 4 0 12914.93 12198.64 881.29 o 6 4 0 570.48 528.94 713.73 o 8 4 0 13674.08 12127.06 824.66 o 10 4 0 18992.77 18820.34 1250.55 o 12 4 0 16254.68 15719.20 1339.14 o 14 4 0 11640.01 11927.25 1183.32 o 16 4 0 9356.53 8278.07 1151.03 o 18 4 0 19907.67 20402.66 1908.63 o 20 4 0 20427.84 19500.81 1812.41 o 22 4 0 14363.83 9757.40 1793.94 o 24 4 0 10025.86 12735.66 3037.32 o 1 5 0 153893.69 144338.20 2848.94 o 3 5 0 163554.34 155293.64 8095.31 o 5 5 0 140052.53 129966.50 3071.31 o 7 5 0 81891.91 84489.78 3763.64 o 9 5 0 39962.29 37937.19 1702.75 o 11 5 0 19692.94 19412.01 1366.83 o 13 5 0 11298.71 10045.27 1160.07 o 15 5 0 3909.38 3295.29 1075.79 o 17 5 0 383.13 -428.66 1127.12 o 19 5 0 175.92 -221.50 1391.94 o 21 5 0 495.89 -418.45 2205.07 o 23 5 0 300.38 1717.85 1786.75 o 0 6 0 259958.89 245183.25 5554.41 o 2 6 0 217482.66 205973.03 10476.49 o 4 6 0 137764.27 137041.84 2744.13 o 6 6 0 89906.73 89152.77 2225.34 o 8 6 0 46660.71 41151.34 1731.60 o 10 6 0 24918.55 22920.25 1602.16 o 12 6 0 17883.69 15706.47 1519.06 o 14 6 0 2693.05 1661.60 1155.87 o 16 6 0 570.42 150.51 1070.56 o 18 6 0 1982.30 1836.71 1223.29 o 20 6 0 2695.56 2415.17 1563.30 o 22 6 0 2487.53 4034.39 1824.62 o 3 7 0 34820.55 34983.93 3313.42 o 5 7 0 23317.69 21451.57 1393.20 o 7 7 0 13781.61 11860.29 1251.73 o 9 7 0 10950.80 8429.98 1260.85 o 11 7 0 12774.82 11915.65 1947.68 o 13 7 0 7691.13 7999.83 1414.13 o 15 7 0 5155.23 2955.47 1212.41 o 17 7 0 2668.94 1984.86 1315.99 o 19 7 0 928.69 618.44 1687.46 o 21 7 0 653.71 1123.02 2842.97 o 0 8 0 5090.48 5255.15 1381.01 o 2 8 0 2108.69 2478.45 748.14 o 4 8 0 514.40 653.64 1062.94 o 6 8 0 170.66 -993.52 993.52 o 8 8 0 206.85 -638.20 1102.95 o 10 8 0 1524.96 689.87 1065.36 o 12 8 0 3974.80 4590.68 1312.59 o 14 8 0 9369.65 5308.48 1639.92 o 16 8 0 11439.54 8031.05 1399.75 o 18 8 0 9211.95 8205.15 2089.56 o 1 9 0 1395.01 1660.28 764.58 o 3 9 0 2289.79 703.59 1039.18 o 5 9 0 1025.50 -419.48 955.56 o 7 9 0 336.82 83.25 987.23 o 9 9 0 32.04 1400.34 1157.57 o 11 9 0 1639.36 2191.15 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