#------------------------------------------------------------------------------ #$Date: 2017-12-28 12:54:13 +0200 (Thu, 28 Dec 2017) $ #$Revision: 204569 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/85/1548553.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1548553 loop_ _publ_author_name 'I.V. Plokhikh' 'D.O. Charkin' 'V.Yu. Verchenko' 'A.N. Kuznetsov' 'A.A. Tsirlin' 'S.M. Kazakov' 'A.V. Shevelkov' _publ_section_title ; Synthesis, crystal structure and physical properties of europium - manganese fluoride pnictides, EuMnPnF (Pn = P, As, Sb) ; _journal_name_full 'Journal of Solid State Chemistry' _journal_page_first 682 _journal_page_last 690 _journal_paper_doi 10.1016/j.jssc.2017.12.004 _journal_volume 258 _journal_year 2018 _chemical_absolute_configuration . _chemical_formula_sum 'As Eu F Mn' _chemical_formula_weight 300.8 _space_group_IT_number 129 _symmetry_cell_setting tetragonal _symmetry_Int_Tables_number 129 _symmetry_space_group_name_Hall 'P 4ab 2ab -1ab' _symmetry_space_group_name_H-M 'P 4/n m m :1' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 4.12265(7) _cell_length_b 4.12265(7) _cell_length_c 9.08462(17) _cell_measurement_temperature 293 _cell_volume 154.404(5) _computing_cell_refinement unknown _computing_data_collection unknown _computing_data_reduction unknown _computing_molecular_graphics unknown _computing_structure_solution unknown _diffrn_ambient_temperature 293 _diffrn_measurement_device 'X-ray Powder diffraction' _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 1.5418 _exptl_absorpt_coefficient_mu 187.025 _exptl_crystal_density_diffrn 6.4703 _exptl_crystal_F_000 432 _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.013 _pd_meas_2theta_range_max 114.985 _pd_meas_2theta_range_min 8.008 _pd_meas_number_of_points 8230 _pd_proc_2theta_range_inc 0.013 _pd_proc_2theta_range_max 114.985 _pd_proc_2theta_range_min 8.008 _pd_proc_ls_background_function '27 Legendre polynoms' _pd_proc_ls_pref_orient_corr 'March & Dollase' _pd_proc_ls_profile_function Lorentzian _pd_proc_ls_prof_R_factor 0.0116 _pd_proc_ls_prof_wR_expected 0.0106 _pd_proc_ls_prof_wR_factor 0.0156 _refine_diff_density_max 1.15 _refine_diff_density_min -1.36 _refine_ls_goodness_of_fit_all 1.47 _refine_ls_number_constraints 0 _refine_ls_number_parameters 54 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0259 _refine_ls_R_factor_gt 0.0247 _refine_ls_shift/su_max 0.0486 _refine_ls_shift/su_mean 0.0072 _refine_ls_weighting_scheme sigma _refine_ls_wR_factor_all 0.0296 _refine_ls_wR_factor_gt 0.0295 _cod_data_source_file 2.cif _cod_data_source_block 2 _cod_depositor_comments ; The following automatic conversions were performed: '_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according to the built-in table from CIF Core dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29. Automatic conversion script Id: cif_fix_values 5376 2017-05-30 11:51:03Z andrius ; _cod_original_cell_volume 154.405(5) _cod_original_sg_symbol_Hall '-P 4a;-2a' _cod_original_sg_symbol_H-M 'P 4/n m m' _cod_original_formula_sum 'As1 Eu1 F1 Mn1' _cod_database_code 1548553 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,z 3 -y+1/2,x+1/2,z 4 y+1/2,-x+1/2,z 5 -x+1/2,y+1/2,-z 6 x+1/2,-y+1/2,-z 7 y,x,-z 8 -y,-x,-z 9 -x+1/2,-y+1/2,-z 10 x+1/2,y+1/2,-z 11 y,-x,-z 12 -y,x,-z 13 x,-y,z 14 -x,y,z 15 -y+1/2,-x+1/2,z 16 y+1/2,x+1/2,z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Eu1 Eu 0.5 0 0.34531(18) Uiso 0.0101(10) 2 1 d . . . As1 As 0 0.5 0.1684(3) Uiso 0.0094(14) 2 1 d . . . Mn Mn 0 0 0 Uiso 0.0092(18) 2 1 d . . . F1 F 0.5 0.5 0.5 Uiso 0.010(3) 2 1 d . . . loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source As -0.9300 1.0051 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Eu -8.9294 11.1857 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' F 0.0727 0.0534 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Mn -0.5299 2.8052 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle Eu1 Eu1 Eu1 1_455 . 1_545 90 Eu1 Eu1 Eu1 1_455 . 1_565 90 Eu1 Eu1 Eu1 1_455 . 1_655 180.0(5) Eu1 Eu1 Eu1 1_455 . 5_546 59.400(7) Eu1 Eu1 Eu1 1_455 . 5_556 59.400(7) Eu1 Eu1 Eu1 1_455 . 5_646 120.600(10) Eu1 Eu1 Eu1 1_455 . 5_656 120.600(10) Eu1 Eu1 As1 1_455 . 1_545 51.742(7) Eu1 Eu1 As1 1_455 . . 51.742(7) Eu1 Eu1 As1 1_455 . 1_645 128.258(10) Eu1 Eu1 As1 1_455 . 1_655 128.258(10) Eu1 Eu1 Mn 1_455 . . 56.691(7) Eu1 Eu1 Mn 1_455 . 1_655 123.309(13) Eu1 Eu1 Mn 1_455 . 3_545 90.000(8) Eu1 Eu1 Mn 1_455 . 3_555 90.000(8) Eu1 Eu1 F1 1_455 . 1_545 90.000(5) Eu1 Eu1 F1 1_455 . . 90.000(5) Eu1 Eu1 F1 1_455 . 3_545 34.284(7) Eu1 Eu1 F1 1_455 . 3_645 145.716(18) Eu1 Eu1 Eu1 1_545 . 1_565 180.0(5) Eu1 Eu1 Eu1 1_545 . 1_655 90 Eu1 Eu1 Eu1 1_545 . 5_546 59.400(7) Eu1 Eu1 Eu1 1_545 . 5_556 120.600(10) Eu1 Eu1 Eu1 1_545 . 5_646 59.400(7) Eu1 Eu1 Eu1 1_545 . 5_656 120.600(10) Eu1 Eu1 As1 1_545 . 1_545 51.742(7) Eu1 Eu1 As1 1_545 . . 128.258(10) Eu1 Eu1 As1 1_545 . 1_645 51.742(7) Eu1 Eu1 As1 1_545 . 1_655 128.258(10) Eu1 Eu1 Mn 1_545 . . 90.000(8) Eu1 Eu1 Mn 1_545 . 1_655 90.000(8) Eu1 Eu1 Mn 1_545 . 3_545 56.691(7) Eu1 Eu1 Mn 1_545 . 3_555 123.309(13) Eu1 Eu1 F1 1_545 . 1_545 34.284(7) Eu1 Eu1 F1 1_545 . . 145.716(18) Eu1 Eu1 F1 1_545 . 3_545 90.000(5) Eu1 Eu1 F1 1_545 . 3_645 90.000(5) Eu1 Eu1 Eu1 1_565 . 1_655 90 Eu1 Eu1 Eu1 1_565 . 5_546 120.600(10) Eu1 Eu1 Eu1 1_565 . 5_556 59.400(7) Eu1 Eu1 Eu1 1_565 . 5_646 120.600(10) Eu1 Eu1 Eu1 1_565 . 5_656 59.400(7) Eu1 Eu1 As1 1_565 . 1_545 128.258(10) Eu1 Eu1 As1 1_565 . . 51.742(7) Eu1 Eu1 As1 1_565 . 1_645 128.258(10) Eu1 Eu1 As1 1_565 . 1_655 51.742(7) Eu1 Eu1 Mn 1_565 . . 90.000(8) Eu1 Eu1 Mn 1_565 . 1_655 90.000(8) Eu1 Eu1 Mn 1_565 . 3_545 123.309(13) Eu1 Eu1 Mn 1_565 . 3_555 56.691(7) Eu1 Eu1 F1 1_565 . 1_545 145.716(18) Eu1 Eu1 F1 1_565 . . 34.284(7) Eu1 Eu1 F1 1_565 . 3_545 90.000(5) Eu1 Eu1 F1 1_565 . 3_645 90.000(5) Eu1 Eu1 Eu1 1_655 . 5_546 120.600(10) Eu1 Eu1 Eu1 1_655 . 5_556 120.600(10) Eu1 Eu1 Eu1 1_655 . 5_646 59.400(7) Eu1 Eu1 Eu1 1_655 . 5_656 59.400(7) Eu1 Eu1 As1 1_655 . 1_545 128.258(10) Eu1 Eu1 As1 1_655 . . 128.258(10) Eu1 Eu1 As1 1_655 . 1_645 51.742(7) Eu1 Eu1 As1 1_655 . 1_655 51.742(7) Eu1 Eu1 Mn 1_655 . . 123.309(13) Eu1 Eu1 Mn 1_655 . 1_655 56.691(7) Eu1 Eu1 Mn 1_655 . 3_545 90.000(8) Eu1 Eu1 Mn 1_655 . 3_555 90.000(8) Eu1 Eu1 F1 1_655 . 1_545 90.000(5) Eu1 Eu1 F1 1_655 . . 90.000(5) Eu1 Eu1 F1 1_655 . 3_545 145.716(18) Eu1 Eu1 F1 1_655 . 3_645 34.284(7) Eu1 Eu1 Eu1 5_546 . 5_556 61.201(7) Eu1 Eu1 Eu1 5_546 . 5_646 61.201(7) Eu1 Eu1 Eu1 5_546 . 5_656 92.093(12) Eu1 Eu1 As1 5_546 . 1_545 72.828(14) Eu1 Eu1 As1 5_546 . . 109.583(9) Eu1 Eu1 As1 5_546 . 1_645 109.583(9) Eu1 Eu1 As1 5_546 . 1_655 164.921(18) Eu1 Eu1 Mn 5_546 . . 107.488(5) Eu1 Eu1 Mn 5_546 . 1_655 149.272(5) Eu1 Eu1 Mn 5_546 . 3_545 107.488(5) Eu1 Eu1 Mn 5_546 . 3_555 149.272(5) Eu1 Eu1 F1 5_546 . 1_545 35.750(5) Eu1 Eu1 F1 5_546 . . 91.698(13) Eu1 Eu1 F1 5_546 . 3_545 35.750(5) Eu1 Eu1 F1 5_546 . 3_645 91.698(13) Eu1 Eu1 Eu1 5_556 . 5_646 92.093(12) Eu1 Eu1 Eu1 5_556 . 5_656 61.201(7) Eu1 Eu1 As1 5_556 . 1_545 109.583(9) Eu1 Eu1 As1 5_556 . . 72.828(14) Eu1 Eu1 As1 5_556 . 1_645 164.921(18) Eu1 Eu1 As1 5_556 . 1_655 109.583(9) Eu1 Eu1 Mn 5_556 . . 107.488(5) Eu1 Eu1 Mn 5_556 . 1_655 149.272(5) Eu1 Eu1 Mn 5_556 . 3_545 149.272(5) Eu1 Eu1 Mn 5_556 . 3_555 107.488(5) Eu1 Eu1 F1 5_556 . 1_545 91.698(13) Eu1 Eu1 F1 5_556 . . 35.750(5) Eu1 Eu1 F1 5_556 . 3_545 35.750(5) Eu1 Eu1 F1 5_556 . 3_645 91.698(13) Eu1 Eu1 Eu1 5_646 . 5_656 61.201(7) Eu1 Eu1 As1 5_646 . 1_545 109.583(9) Eu1 Eu1 As1 5_646 . . 164.921(18) Eu1 Eu1 As1 5_646 . 1_645 72.828(14) Eu1 Eu1 As1 5_646 . 1_655 109.583(9) Eu1 Eu1 Mn 5_646 . . 149.272(5) Eu1 Eu1 Mn 5_646 . 1_655 107.488(5) Eu1 Eu1 Mn 5_646 . 3_545 107.488(5) Eu1 Eu1 Mn 5_646 . 3_555 149.272(5) Eu1 Eu1 F1 5_646 . 1_545 35.750(5) Eu1 Eu1 F1 5_646 . . 91.698(13) Eu1 Eu1 F1 5_646 . 3_545 91.698(13) Eu1 Eu1 F1 5_646 . 3_645 35.750(5) Eu1 Eu1 As1 5_656 . 1_545 164.921(18) Eu1 Eu1 As1 5_656 . . 109.583(9) Eu1 Eu1 As1 5_656 . 1_645 109.583(9) Eu1 Eu1 As1 5_656 . 1_655 72.828(14) Eu1 Eu1 Mn 5_656 . . 149.272(5) Eu1 Eu1 Mn 5_656 . 1_655 107.488(5) Eu1 Eu1 Mn 5_656 . 3_545 149.272(5) Eu1 Eu1 Mn 5_656 . 3_555 107.488(5) Eu1 Eu1 F1 5_656 . 1_545 91.698(13) Eu1 Eu1 F1 5_656 . . 35.750(5) Eu1 Eu1 F1 5_656 . 3_545 91.698(13) Eu1 Eu1 F1 5_656 . 3_645 35.750(5) As1 Eu1 As1 1_545 . . 76.515(10) As1 Eu1 As1 1_545 . 1_645 76.515(10) As1 Eu1 As1 1_545 . 1_655 122.25(2) As1 Eu1 Mn 1_545 . . 41.961(11) As1 Eu1 Mn 1_545 . 1_655 86.357(15) As1 Eu1 Mn 1_545 . 3_545 41.961(11) As1 Eu1 Mn 1_545 . 3_555 86.357(15) As1 Eu1 F1 1_545 . 1_545 76.137(10) As1 Eu1 F1 1_545 . . 141.594(5) As1 Eu1 F1 1_545 . 3_545 76.137(10) As1 Eu1 F1 1_545 . 3_645 141.594(5) As1 Eu1 As1 . . 1_645 122.25(2) As1 Eu1 As1 . . 1_655 76.515(10) As1 Eu1 Mn . . . 41.961(11) As1 Eu1 Mn . . 1_655 86.357(15) As1 Eu1 Mn . . 3_545 86.357(15) As1 Eu1 Mn . . 3_555 41.961(11) As1 Eu1 F1 . . 1_545 141.594(5) As1 Eu1 F1 . . . 76.137(10) As1 Eu1 F1 . . 3_545 76.137(10) As1 Eu1 F1 . . 3_645 141.594(5) As1 Eu1 As1 1_645 . 1_655 76.515(10) As1 Eu1 Mn 1_645 . . 86.357(15) As1 Eu1 Mn 1_645 . 1_655 41.961(11) As1 Eu1 Mn 1_645 . 3_545 41.961(11) As1 Eu1 Mn 1_645 . 3_555 86.357(15) As1 Eu1 F1 1_645 . 1_545 76.137(10) As1 Eu1 F1 1_645 . . 141.594(5) As1 Eu1 F1 1_645 . 3_545 141.594(5) As1 Eu1 F1 1_645 . 3_645 76.137(10) As1 Eu1 Mn 1_655 . . 86.357(15) As1 Eu1 Mn 1_655 . 1_655 41.961(11) As1 Eu1 Mn 1_655 . 3_545 86.357(15) As1 Eu1 Mn 1_655 . 3_555 41.961(11) As1 Eu1 F1 1_655 . 1_545 141.594(5) As1 Eu1 F1 1_655 . . 76.137(10) As1 Eu1 F1 1_655 . 3_545 141.594(5) As1 Eu1 F1 1_655 . 3_645 76.137(10) Mn Eu1 Mn . . 1_655 66.618(8) Mn Eu1 Mn . . 3_545 45.699(5) Mn Eu1 Mn . . 3_555 45.699(5) Mn Eu1 F1 . . 1_545 118.083(6) Mn Eu1 F1 . . . 118.083(6) Mn Eu1 F1 . . 3_545 90.975(5) Mn Eu1 F1 . . 3_645 157.593(13) Mn Eu1 Mn 1_655 . 3_545 45.699(5) Mn Eu1 Mn 1_655 . 3_555 45.699(5) Mn Eu1 F1 1_655 . 1_545 118.083(6) Mn Eu1 F1 1_655 . . 118.083(6) Mn Eu1 F1 1_655 . 3_545 157.593(13) Mn Eu1 F1 1_655 . 3_645 90.975(5) Mn Eu1 Mn 3_545 . 3_555 66.618(8) Mn Eu1 F1 3_545 . 1_545 90.975(5) Mn Eu1 F1 3_545 . . 157.593(13) Mn Eu1 F1 3_545 . 3_545 118.083(6) Mn Eu1 F1 3_545 . 3_645 118.083(6) Mn Eu1 F1 3_555 . 1_545 157.593(13) Mn Eu1 F1 3_555 . . 90.975(5) Mn Eu1 F1 3_555 . 3_545 118.083(6) Mn Eu1 F1 3_555 . 3_645 118.083(6) F1 Eu1 F1 1_545 . . 111.432(19) F1 Eu1 F1 1_545 . 3_545 71.500(9) F1 Eu1 F1 1_545 . 3_645 71.500(9) F1 Eu1 F1 . . 3_545 71.500(9) F1 Eu1 F1 . . 3_645 71.500(9) F1 Eu1 F1 3_545 . 3_645 111.432(19) Eu1 As1 Eu1 1_455 . 1_465 76.515(12) Eu1 As1 Eu1 1_455 . . 76.515(12) Eu1 As1 Eu1 1_455 . 1_565 122.25(3) Eu1 As1 Mn 1_455 . . 77.905(6) Eu1 As1 Mn 1_455 . 1_565 141.721(5) Eu1 As1 Mn 1_455 . 3_455 77.905(6) Eu1 As1 Mn 1_455 . 3_555 141.721(5) Eu1 As1 Eu1 1_465 . . 122.25(3) Eu1 As1 Eu1 1_465 . 1_565 76.515(12) Eu1 As1 Mn 1_465 . . 141.721(5) Eu1 As1 Mn 1_465 . 1_565 77.905(6) Eu1 As1 Mn 1_465 . 3_455 77.905(6) Eu1 As1 Mn 1_465 . 3_555 141.721(5) Eu1 As1 Eu1 . . 1_565 76.515(12) Eu1 As1 Mn . . . 77.905(6) Eu1 As1 Mn . . 1_565 141.721(5) Eu1 As1 Mn . . 3_455 141.721(5) Eu1 As1 Mn . . 3_555 77.905(6) Eu1 As1 Mn 1_565 . . 141.721(5) Eu1 As1 Mn 1_565 . 1_565 77.905(6) Eu1 As1 Mn 1_565 . 3_455 141.721(5) Eu1 As1 Mn 1_565 . 3_555 77.905(6) Mn As1 Mn . . 1_565 106.85(3) Mn As1 Mn . . 3_455 69.203(15) Mn As1 Mn . . 3_555 69.203(15) Mn As1 Mn 1_565 . 3_455 69.203(15) Mn As1 Mn 1_565 . 3_555 69.203(15) Mn As1 Mn 3_455 . 3_555 106.85(3) Eu1 Mn Eu1 1_455 . . 66.618(6) Eu1 Mn Eu1 1_455 . 5_545 134.301(4) Eu1 Mn Eu1 1_455 . 5_555 134.301(4) Eu1 Mn As1 1_455 . 1_545 60.134(11) Eu1 Mn As1 1_455 . . 60.134(11) Eu1 Mn As1 1_455 . 5_445 93.266(15) Eu1 Mn As1 1_455 . 5_545 159.883(15) Eu1 Mn Mn 1_455 . 3_445 67.151(3) Eu1 Mn Mn 1_455 . 3_455 67.151(3) Eu1 Mn Mn 1_455 . 3_545 112.849(3) Eu1 Mn Mn 1_455 . 3_555 112.849(3) Eu1 Mn Eu1 . . 5_545 134.301(4) Eu1 Mn Eu1 . . 5_555 134.301(4) Eu1 Mn As1 . . 1_545 60.134(11) Eu1 Mn As1 . . . 60.134(11) Eu1 Mn As1 . . 5_445 159.883(15) Eu1 Mn As1 . . 5_545 93.266(15) Eu1 Mn Mn . . 3_445 112.849(3) Eu1 Mn Mn . . 3_455 112.849(3) Eu1 Mn Mn . . 3_545 67.151(3) Eu1 Mn Mn . . 3_555 67.151(3) Eu1 Mn Eu1 5_545 . 5_555 66.618(6) Eu1 Mn As1 5_545 . 1_545 93.266(15) Eu1 Mn As1 5_545 . . 159.883(15) Eu1 Mn As1 5_545 . 5_445 60.134(11) Eu1 Mn As1 5_545 . 5_545 60.134(11) Eu1 Mn Mn 5_545 . 3_445 67.151(3) Eu1 Mn Mn 5_545 . 3_455 112.849(3) Eu1 Mn Mn 5_545 . 3_545 67.151(3) Eu1 Mn Mn 5_545 . 3_555 112.849(3) Eu1 Mn As1 5_555 . 1_545 159.883(15) Eu1 Mn As1 5_555 . . 93.266(15) Eu1 Mn As1 5_555 . 5_445 60.134(11) Eu1 Mn As1 5_555 . 5_545 60.134(11) Eu1 Mn Mn 5_555 . 3_445 112.849(3) Eu1 Mn Mn 5_555 . 3_455 67.151(3) Eu1 Mn Mn 5_555 . 3_545 112.849(3) Eu1 Mn Mn 5_555 . 3_555 67.151(3) As1 Mn As1 1_545 . . 106.85(2) As1 Mn As1 1_545 . 5_445 110.797(11) As1 Mn As1 1_545 . 5_545 110.797(11) As1 Mn Mn 1_545 . 3_445 55.398(8) As1 Mn Mn 1_545 . 3_455 124.602(8) As1 Mn Mn 1_545 . 3_545 55.398(8) As1 Mn Mn 1_545 . 3_555 124.602(8) As1 Mn As1 . . 5_445 110.797(11) As1 Mn As1 . . 5_545 110.797(11) As1 Mn Mn . . 3_445 124.602(8) As1 Mn Mn . . 3_455 55.398(8) As1 Mn Mn . . 3_545 124.602(8) As1 Mn Mn . . 3_555 55.398(8) As1 Mn As1 5_445 . 5_545 106.85(2) As1 Mn Mn 5_445 . 3_445 55.398(8) As1 Mn Mn 5_445 . 3_455 55.398(8) As1 Mn Mn 5_445 . 3_545 124.602(8) As1 Mn Mn 5_445 . 3_555 124.602(8) As1 Mn Mn 5_545 . 3_445 124.602(8) As1 Mn Mn 5_545 . 3_455 124.602(8) As1 Mn Mn 5_545 . 3_545 55.398(8) As1 Mn Mn 5_545 . 3_555 55.398(8) Mn Mn Mn 3_445 . 3_455 90.0000(4) Mn Mn Mn 3_445 . 3_545 90.0000(4) Mn Mn Mn 3_445 . 3_555 180.0(5) Mn Mn Mn 3_455 . 3_545 180.0(5) Mn Mn Mn 3_455 . 3_555 90.0000(4) Mn Mn Mn 3_545 . 3_555 90.0000(4) Eu1 F1 Eu1 . . 1_565 111.432(13) Eu1 F1 Eu1 . . 5_556 108.500(6) Eu1 F1 Eu1 . . 5_656 108.500(6) Eu1 F1 Eu1 1_565 . 5_556 108.500(6) Eu1 F1 Eu1 1_565 . 5_656 108.500(6) Eu1 F1 Eu1 5_556 . 5_656 111.432(13) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance Eu1 Eu1 . 1_455 4.12265(4) Eu1 Eu1 . 1_545 4.12265(4) Eu1 Eu1 . 1_565 4.12265(4) Eu1 Eu1 . 1_655 4.12265(4) Eu1 Eu1 . 5_546 4.0494(5) Eu1 Eu1 . 5_556 4.0494(5) Eu1 Eu1 . 5_646 4.0494(5) Eu1 Eu1 . 5_656 4.0494(5) Eu1 As1 . 1_545 3.3290(5) Eu1 As1 . . 3.3290(5) Eu1 As1 . 1_645 3.3290(5) Eu1 As1 . 1_655 3.3290(5) Eu1 Mn . . 3.7537(4) Eu1 Mn . 1_655 3.7537(4) Eu1 Mn . 3_545 3.7537(4) Eu1 Mn . 3_555 3.7537(4) Eu1 F1 . 1_545 2.4948(3) Eu1 F1 . . 2.4948(3) Eu1 F1 . 3_545 2.4948(3) Eu1 F1 . 3_645 2.4948(3) As1 Mn . . 2.5668(5) As1 Mn . 1_565 2.5668(5) As1 Mn . 3_455 2.5668(5) As1 Mn . 3_555 2.5668(5) Mn Mn . 3_445 2.91515(2) Mn Mn . 3_455 2.91515(2) Mn Mn . 3_545 2.91515(2) Mn Mn . 3_555 2.91515(2)