#------------------------------------------------------------------------------ #$Date: 2017-12-29 11:03:35 +0200 (Fri, 29 Dec 2017) $ #$Revision: 204579 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/85/1548555.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1548555 loop_ _publ_author_name 'Marina Barsukova' 'Tatiana Goncharova' 'Denis Samsonenko' 'Danil Dybtsev' 'Andrei Potapov' _publ_section_title ; Synthesis, Crystal Structure, and Luminescent Properties of New Zinc(II) and Cadmium(II) Metal-Organic Frameworks Based on Flexible Bis(imidazol-1-yl)alkane Ligands ; _journal_name_full Crystals _journal_page_first 132 _journal_paper_doi 10.3390/cryst6100132 _journal_volume 6 _journal_year 2016 _chemical_formula_sum 'C22 H27 N5 O5 Zn' _chemical_formula_weight 506.85 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 105.3925(17) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.73257(16) _cell_length_b 23.2562(3) _cell_length_c 9.76351(17) _cell_measurement_reflns_used 13981 _cell_measurement_temperature 130(2) _cell_measurement_theta_max 30.75 _cell_measurement_theta_min 4.02 _cell_volume 2349.55(6) _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_molecular_graphics 'ShelXle (H\"ubschle, 2011)' _computing_publication_material 'CIFTAB-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_structure_solution 'SHELXS-2013 (Sheldrick, 2013)' _diffrn_ambient_temperature 130(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.6168 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.907 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'New Xcalibur, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0160 _diffrn_reflns_av_unetI/netI 0.0162 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.907 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 32 _diffrn_reflns_limit_k_min -32 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 24131 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.907 _diffrn_reflns_theta_full 26.500 _diffrn_reflns_theta_max 30.991 _diffrn_reflns_theta_min 3.404 _diffrn_source 'sealed X-ray tube' _exptl_absorpt_coefficient_mu 1.088 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.85550 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.433 _exptl_crystal_description block _exptl_crystal_F_000 1056 _exptl_crystal_size_max 0.34 _exptl_crystal_size_mid 0.31 _exptl_crystal_size_min 0.21 _refine_diff_density_max 1.227 _refine_diff_density_min -0.532 _refine_diff_density_rms 0.072 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.075 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 310 _refine_ls_number_reflns 6791 _refine_ls_number_restraints 30 _refine_ls_restrained_S_all 1.111 _refine_ls_R_factor_all 0.0409 _refine_ls_R_factor_gt 0.0374 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0551P)^2^+1.9547P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1059 _refine_ls_wR_factor_ref 0.1082 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 6249 _reflns_number_total 6791 _reflns_threshold_expression >2\s(I) _cod_data_source_file 1.cif _cod_data_source_block bmo280_3 _cod_database_code 1548555 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.709 _shelx_estimated_absorpt_t_max 0.804 _shelxl_version_number 2013-3 _shelx_res_file ; TITL bmo280_3 in P2(1)/c; 130K; Xcalibur CELL 0.71073 10.73257 23.2562 9.76351 90.0000 105.3925 90.0000 ZERR 4.00 0.00016 0.0003 0.00017 0.0000 0.0017 0.0000 LATT 1 SYMM -X, 0.50000+Y, 0.50000-Z SFAC C H N O Zn UNIT 88 108 20 20 4 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -143 L.S. 6 FMAP 2 PLAN 5 BOND $H REM [Zn(C11H16N4)(C8H4O4)]*C3H7NO SIMU 0.01 0.02 O12 O12' SIMU 0.003 0.005 O1D > C13D ACTA 53 SIZE 0.34 0.31 0.21 WGHT 0.055100 1.954750 FVAR 4.25472 0.41249 ZN1 5 0.329591 0.100659 -0.031610 11.00000 0.02277 0.01507 = 0.01470 -0.00043 -0.00157 -0.00022 O11 4 0.400382 0.052286 0.135051 11.00000 0.05723 0.03962 = 0.01759 0.00747 0.00646 0.01730 O12 4 0.318534 0.110986 0.264961 21.00000 0.08180 0.06011 = 0.03462 0.01496 0.00816 0.04550 O12' 4 0.261725 0.085617 0.238698 -21.00000 0.05003 0.08509 = 0.03997 0.03371 0.02126 0.04313 C11 1 0.365615 0.061963 0.244361 11.00000 0.02994 0.03490 = 0.02431 0.00967 0.00685 0.00839 C12 1 0.435548 0.029442 0.377008 11.00000 0.02228 0.02388 = 0.01652 0.00162 0.00251 0.00110 C13 1 0.421583 0.046539 0.509081 11.00000 0.02861 0.02546 = 0.02133 0.00177 0.00660 0.00701 AFIX 43 H13 2 0.368169 0.078457 0.515467 11.00000 -1.20000 AFIX 0 C14 1 0.514462 -0.017044 0.368617 11.00000 0.02764 0.02542 = 0.01661 -0.00076 0.00471 0.00228 AFIX 43 H14 2 0.524756 -0.028716 0.279017 11.00000 -1.20000 AFIX 0 O21 4 0.201889 0.049655 -0.156579 11.00000 0.03305 0.02488 = 0.01553 0.00028 -0.00141 -0.00941 O22 4 0.232232 0.109914 -0.321052 11.00000 0.03270 0.02070 = 0.02133 -0.00098 0.00341 -0.00695 C21 1 0.180435 0.067006 -0.285644 11.00000 0.02181 0.01772 = 0.01683 -0.00212 0.00027 -0.00035 C22 1 0.086960 0.032222 -0.396108 11.00000 0.02187 0.01705 = 0.01557 -0.00086 -0.00033 -0.00070 C23 1 0.084035 0.038451 -0.539803 11.00000 0.02345 0.02086 = 0.01832 0.00048 0.00295 -0.00339 AFIX 43 H23 2 0.140995 0.064677 -0.567012 11.00000 -1.20000 AFIX 0 C24 1 0.002386 -0.006169 -0.357613 11.00000 0.02477 0.02111 = 0.01447 0.00044 0.00186 -0.00091 AFIX 43 H24 2 0.003802 -0.010316 -0.260413 11.00000 -1.20000 AFIX 0 N11 3 0.503067 0.110604 -0.074544 11.00000 0.02401 0.01994 = 0.02283 0.00091 -0.00053 -0.00111 N12 3 0.703332 0.094202 -0.079843 11.00000 0.02349 0.02235 = 0.02572 0.00047 0.00169 -0.00223 N13 3 1.140213 0.242357 0.421329 11.00000 0.02856 0.02068 = 0.02623 -0.00009 0.00623 -0.00459 N14 3 1.262399 0.319330 0.471386 11.00000 0.02680 0.01746 = 0.02044 0.00218 0.00137 -0.00070 C101 1 0.607559 0.078715 -0.023018 11.00000 0.02383 0.01939 = 0.02041 -0.00131 0.00112 -0.00207 AFIX 43 H101 2 0.613662 0.048916 0.045001 11.00000 -1.20000 AFIX 0 C102 1 0.534812 0.148168 -0.168898 11.00000 0.02922 0.02446 = 0.03428 0.00932 0.00000 -0.00136 AFIX 43 H102 2 0.478736 0.176332 -0.223141 11.00000 -1.20000 AFIX 0 C103 1 0.658815 0.138688 -0.172358 11.00000 0.03075 0.02923 = 0.03331 0.00940 0.00418 -0.00530 AFIX 43 H103 2 0.705363 0.158785 -0.227640 11.00000 -1.20000 AFIX 0 C104 1 0.832878 0.068130 -0.047878 11.00000 0.02410 0.02672 = 0.03342 -0.00429 0.00529 0.00063 AFIX 23 H10A 2 0.846809 0.051286 -0.135758 11.00000 -1.20000 H10B 2 0.838383 0.036686 0.021828 11.00000 -1.20000 AFIX 0 C105 1 0.938358 0.112202 0.011946 11.00000 0.02193 0.03050 = 0.03504 -0.00339 0.00716 -0.00350 AFIX 23 H10C 2 0.935641 0.142258 -0.060596 11.00000 -1.20000 H10D 2 1.023522 0.092958 0.030987 11.00000 -1.20000 AFIX 0 C106 1 0.926099 0.140875 0.148344 11.00000 0.02404 0.02218 = 0.03173 -0.00014 0.00597 -0.00350 AFIX 23 H10E 2 0.921392 0.110805 0.218570 11.00000 -1.20000 H10F 2 0.844701 0.163206 0.127748 11.00000 -1.20000 AFIX 0 C107 1 1.039577 0.180904 0.212518 11.00000 0.02454 0.02671 = 0.03359 -0.00385 0.00711 -0.00475 AFIX 23 H10G 2 1.121668 0.159492 0.225945 11.00000 -1.20000 H10H 2 1.039866 0.213052 0.146135 11.00000 -1.20000 AFIX 0 C108 1 1.030797 0.204783 0.354091 11.00000 0.03128 0.02760 = 0.03522 -0.00297 0.01111 -0.01044 AFIX 23 H10I 2 0.949413 0.226822 0.339625 11.00000 -1.20000 H10J 2 1.027560 0.172415 0.418914 11.00000 -1.20000 AFIX 0 C109 1 1.241432 0.228407 0.534489 11.00000 0.04087 0.02233 = 0.04026 0.01053 0.00034 -0.00130 AFIX 43 H109 2 1.256811 0.192438 0.582122 11.00000 -1.20000 AFIX 0 C110 1 1.315479 0.276454 0.564887 11.00000 0.03727 0.02539 = 0.03725 0.01070 -0.00890 -0.00247 AFIX 43 H110 2 1.392488 0.279829 0.639717 11.00000 -1.20000 AFIX 0 C111 1 1.155984 0.297315 0.386199 11.00000 0.02562 0.01977 = 0.02116 0.00066 0.00457 -0.00096 AFIX 43 H111 2 1.098671 0.317540 0.310681 11.00000 -1.20000 AFIX 0 O1D 4 0.872280 0.192058 0.655429 11.00000 0.06003 0.10392 = 0.04370 0.00892 -0.00635 -0.03733 N1D 3 0.726273 0.160716 0.458290 11.00000 0.03572 0.03681 = 0.04209 -0.00009 0.00225 -0.00422 C11D 1 0.786562 0.202039 0.545704 11.00000 0.05422 0.05192 = 0.04687 0.00216 0.00866 -0.01582 AFIX 43 H11D 2 0.762514 0.240876 0.522554 11.00000 -1.20000 AFIX 0 C12D 1 0.756668 0.101297 0.487012 11.00000 0.05106 0.04446 = 0.08311 0.00204 0.01917 0.00266 AFIX 137 H12A 2 0.761561 0.082006 0.399353 11.00000 -1.50000 H12B 2 0.689218 0.083211 0.523089 11.00000 -1.50000 H12C 2 0.840049 0.097966 0.558275 11.00000 -1.50000 AFIX 0 C13D 1 0.622388 0.173920 0.334195 11.00000 0.07006 0.07542 = 0.07062 0.00108 -0.01798 -0.00278 AFIX 37 H13A 2 0.627145 0.148169 0.256291 11.00000 -1.50000 H13B 2 0.630311 0.213879 0.305766 11.00000 -1.50000 H13C 2 0.539257 0.168666 0.356372 11.00000 -1.50000 AFIX 0 HKLF 4 REM bmo280_3 in P2(1)/c; 130K; Xcalibur REM R1 = 0.0374 for 6249 Fo > 4sig(Fo) and 0.0409 for all 6791 data REM 310 parameters refined using 30 restraints END WGHT 0.0551 1.9547 REM Highest difference peak 1.227, deepest hole -0.532, 1-sigma level 0.072 Q1 1 0.8330 0.1383 0.5574 11.00000 0.05 1.23 Q2 1 0.8935 0.1510 0.6578 11.00000 0.05 0.92 Q3 1 0.6607 0.1279 0.3285 11.00000 0.05 0.77 Q4 1 0.7010 0.2200 0.4652 11.00000 0.05 0.67 Q5 1 0.3842 0.1040 -0.0774 11.00000 0.05 0.66 ; _shelx_res_checksum 83428 _shelx_hkl_file ; -15 0 4 4266.71 367.668 2 -15 0 5 457.220 182.856 2 -15 -1 3 947.990 203.043 2 -15 -1 5 9240.23 529.451 2 -15 -1 6 4321.37 380.706 2 -15 2 1 382.680 146.464 3 -15 -2 2 1530.33 251.380 2 -15 -2 3 157.044 141.269 2 -15 -2 4 400.932 144.551 2 -15 -2 6 363.279 156.286 2 -15 3 1 445.772 141.915 3 -15 -3 2 969.359 217.756 2 -15 -3 3 678.369 170.039 2 -15 -3 5 782.755 181.157 2 -15 -3 6 3084.60 317.656 2 -15 -4 3 437.979 154.294 2 -15 -4 4 6045.64 417.277 2 -15 -4 5 1384.37 220.215 2 -15 -4 6 7050.43 454.574 2 -15 -5 2 436.472 157.654 2 -15 -5 3 4518.81 362.800 2 -15 -6 2 1057.43 211.575 2 -15 -6 3 662.508 171.004 2 -14 0 -1-291.930 150.075 3 -14 0 -1 222.847 151.335 1 -14 0 0 1436.47 221.968 2 -14 0 0 1717.40 241.220 1 -14 0 0 1333.20 205.582 3 -14 0 1 136.534 130.338 2 -14 0 1 3.18639 117.422 1 -14 0 1-58.4933 86.5341 3 -14 0 2 372.044 153.217 2 -14 0 2 191.145 116.817 1 -14 0 3-159.178 131.482 1 -14 0 3 40.0599 103.058 2 -14 0 4 1264.02 221.079 2 -14 0 4 1087.16 219.723 1 -14 0 5-20.3785 122.348 1 -14 1 -2 817.852 176.157 3 -14 -1 -1 6662.96 455.324 1 -14 1 -1 6604.92 427.998 3 -14 1 -1 6274.79 430.638 1 -14 1 0 288.051 138.649 1 -14 -1 0-29.3170 91.7248 3 -14 -1 0 200.698 122.878 1 -14 1 0 175.301 111.179 3 -14 1 0 274.574 134.651 2 -14 1 1 3376.85 304.320 3 -14 -1 1 3622.12 338.957 2 -14 1 1 3873.23 356.777 2 -14 1 1 3390.62 317.438 1 -14 -1 1 3637.85 336.984 1 -14 -1 1 3618.24 306.323 3 -14 1 2 1220.84 212.070 2 -14 -1 2 1095.21 197.339 1 -14 1 2 1166.46 197.199 1 -14 -1 2 1644.38 233.294 2 -14 1 3 31.5602 110.100 1 -14 -1 3 58.4487 119.844 1 -14 -1 3 36.2166 114.610 2 -14 1 3 26.7564 96.5012 2 -14 1 4 1568.24 235.578 2 -14 -1 4 1787.62 244.609 1 -14 -1 4 1976.00 252.053 2 -14 1 4 1523.79 238.210 1 -14 1 5 1353.38 225.855 1 -14 -1 5 1549.11 224.474 2 -14 -1 5 1171.69 200.178 1 -14 2 -2 884.770 188.092 3 -14 2 -2 974.456 182.320 1 -14 2 -1 2604.97 295.144 1 -14 -2 -1 2889.11 318.663 2 -14 2 -1 2380.17 272.164 3 -14 -2 0 12.9065 120.925 2 -14 2 0-10.9486 102.463 3 -14 2 0-70.4818 124.285 1 -14 2 0 138.496 127.465 2 -14 -2 0 199.981 110.744 1 -14 2 1 9870.09 546.014 2 -14 2 1 8862.91 506.340 1 -14 -2 1 8841.44 507.748 2 -14 -2 1 9784.06 545.855 1 -14 2 1 8398.39 466.483 3 -14 2 2 238.270 144.683 1 -14 -2 2 176.333 125.633 1 -14 -2 2 327.828 157.048 2 -14 2 3 3547.10 330.037 2 -14 -2 3 3901.26 342.040 1 -14 2 3 3804.35 334.189 1 -14 -2 3 3561.21 321.892 2 -14 -2 4 650.731 162.496 2 -14 2 4 982.697 202.314 1 -14 -2 4 836.966 194.158 1 -14 2 5 4286.41 377.869 1 -14 -2 5 3781.54 348.426 1 -14 3 -2 1127.60 207.827 1 -14 3 -1 1129.19 203.265 1 -14 -3 -1 1002.50 201.472 2 -14 3 -1 1128.71 199.713 3 -14 -3 0 3515.56 334.002 1 -14 3 0 3316.08 310.451 3 -14 -3 0 3531.70 333.426 2 -14 3 0 4061.61 344.947 1 -14 -3 1 385.866 161.461 2 -14 3 1 421.457 132.692 3 -14 3 1 354.382 147.384 2 -14 -3 1 477.916 162.212 1 -14 3 1 308.973 141.893 1 -14 3 2 6795.23 443.831 1 -14 3 2 6185.04 433.232 2 -14 -3 2 6463.63 445.938 1 -14 -3 2 6012.50 417.093 2 -14 -3 3 223.675 128.402 1 -14 3 3 131.505 114.665 2 -14 -3 3 95.4544 125.803 2 -14 3 3 160.155 121.099 1 -14 -3 4 5912.96 402.510 2 -14 3 4 6590.42 438.748 2 -14 -3 4 6313.59 438.533 1 -14 3 4 6104.30 422.808 1 -14 3 5 93.4294 127.177 1 -14 -3 5-47.0044 129.580 1 -14 4 -2 2915.24 306.910 1 -14 4 -1 149.774 130.608 1 -14 -4 -1 78.5212 119.749 2 -14 4 -1 347.426 136.847 3 -14 4 0 4435.14 368.203 3 -14 4 0 4778.34 374.004 1 -14 -4 1 6028.14 431.979 1 -14 -4 1 6852.86 443.787 2 -14 4 1 6277.25 448.193 2 -14 4 1 6055.73 413.699 1 -14 4 2 65.8808 109.192 2 -14 -4 2 408.476 162.224 1 -14 4 2 87.1234 104.608 1 -14 4 3 189.542 116.099 2 -14 4 3 73.2251 101.685 1 -14 -4 3-98.9208 142.812 1 -14 -4 4 228.323 123.236 2 -14 4 4-38.6760 114.305 2 -14 -4 4-65.8510 132.640 1 -14 4 4 312.136 142.054 1 -14 -4 5 499.991 169.702 1 -14 4 5 879.301 201.307 1 -14 -4 5 500.255 143.125 2 -14 5 -1 944.202 191.493 1 -14 5 -1 1427.84 229.982 3 -14 -5 -1 952.622 188.228 2 -14 5 0 361.615 152.828 1 -14 -5 0 131.091 123.284 2 -14 5 0 81.9402 116.472 3 -14 -5 1 304.720 156.357 2 -14 5 1 191.320 117.853 1 -14 5 1 158.033 125.196 2 -14 5 2 1133.68 215.344 2 -14 -5 2 1385.63 234.722 1 -14 -5 2 1320.95 208.710 2 -14 5 2 1188.57 200.977 1 -14 -5 3 153.227 118.446 1 -14 -5 3 512.468 161.829 2 -14 5 3 203.091 130.849 1 -14 5 3 468.830 173.757 2 -14 -5 4 142.847 114.563 2 -14 5 4 142.343 130.068 1 -14 -5 4 52.8271 124.989 1 -14 -5 5 484.128 166.141 1 -14 5 5 683.185 193.043 1 -14 -5 5 458.452 143.105 2 -14 -5 6 1678.28 224.206 2 -14 6 -1 271.629 129.352 1 -14 -6 -1-67.2218 144.092 2 -14 -6 0 3997.16 346.814 2 -14 6 0 3563.50 346.417 3 -14 6 0 3290.75 315.491 1 -14 -6 1 265.865 130.351 2 -14 6 1 374.756 135.209 1 -14 -6 2-95.6808 108.733 2 -14 6 2-41.5595 101.491 1 -14 6 2 200.536 137.929 2 -14 -6 3 1513.41 239.579 1 -14 6 3 1539.02 231.660 2 -14 6 3 1352.86 216.345 1 -14 -6 3 1406.12 214.508 2 -14 6 4 182.301 120.223 2 -14 -6 4 181.294 121.562 2 -14 6 4 239.721 136.940 1 -14 -6 4 15.7761 126.254 1 -14 -6 5 87.5034 108.597 2 -14 6 5 218.830 138.441 1 -14 -6 6 113.767 110.412 2 -14 7 -1 2269.12 260.627 1 -14 -7 0 1833.18 240.297 2 -14 7 0 1529.63 227.505 1 -14 7 0 1736.31 250.256 3 -14 -7 1-5.20715 117.513 2 -14 7 1 225.243 135.090 1 -14 7 2 5144.02 376.347 1 -14 -7 2 5408.80 382.704 2 -14 7 3 2718.86 304.609 2 -14 7 3 2788.79 293.821 1 -14 -7 3 2595.85 263.858 2 -14 7 4 728.136 181.614 1 -14 -7 4 453.990 139.206 2 -14 7 4 889.928 193.507 2 -14 -7 5 158.929 111.484 2 -14 -8 0 1300.32 221.320 2 -14 8 0 978.355 190.457 1 -14 -8 1 295.459 121.517 2 -14 8 1 304.349 125.830 1 -14 8 2 398.452 145.120 1 -14 -8 2 394.152 142.386 2 -14 -8 3 884.148 178.860 2 -14 8 4 170.085 115.442 1 -14 9 0 2824.80 286.166 1 -14 9 1 103.419 125.414 1 -14 9 2 4056.54 344.695 1 -14 9 3 257.419 132.199 1 -14 10 0 3596.03 311.034 1 -14 10 1 349.525 142.697 1 -14 10 2 445.056 148.079 1 -14 11 1 836.939 178.060 1 -13 0 -4 520.343 159.077 3 -13 0 -3 41.9294 106.511 3 -13 0 -2 718.014 167.939 3 -13 0 -2 725.220 178.821 1 -13 0 -2 805.297 193.275 2 -13 0 -1 133.601 131.707 1 -13 0 -1 219.508 139.375 2 -13 0 -1-42.4517 102.367 3 -13 0 0 167.572 117.659 1 -13 0 0 90.0320 103.687 3 -13 0 0 199.178 139.951 2 -13 0 1-59.1862 106.498 2 -13 0 1-178.539 121.699 1 -13 0 2 1258.26 198.184 1 -13 0 2 1842.72 232.463 2 -13 0 3 58.9727 112.491 1 -13 0 3 279.984 134.921 2 -13 0 4 11984.1 562.671 1 -13 0 4 12386.5 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476.563 153.702 1 -12 -5 -5 151.997 137.791 5 -12 5 -4 163.958 116.141 3 -12 -5 -4 175.648 115.551 5 -12 5 -3 4863.57 386.966 3 -12 5 -3 4472.14 320.978 1 -12 -5 -3 4534.56 325.065 5 -12 5 -3 4741.94 398.366 2 -12 -5 -2 171.703 94.4799 3 -12 -5 -2 68.0078 91.9817 5 -12 5 -2 203.512 125.979 3 -12 5 -2-126.702 108.938 1 -12 -5 -2-212.136 153.253 2 -12 5 -2-10.7455 113.798 2 -12 5 -1 11951.8 509.616 1 -12 5 -1 11573.8 544.882 3 -12 -5 -1 12109.7 545.892 2 -12 5 -1 12842.6 598.815 2 -12 -5 -1 12091.0 465.157 5 -12 5 0 326.857 118.705 1 -12 -5 0 359.756 103.167 5 -12 5 0 295.962 130.365 2 -12 -5 0 534.481 124.156 3 -12 -5 0 195.393 110.472 2 -12 -5 1 10787.1 488.992 2 -12 -5 1 11169.5 410.878 5 -12 5 1 10846.3 488.390 1 -12 -5 1 11252.0 430.307 3 -12 5 1 11496.4 536.259 2 -12 -5 2 2207.61 228.732 2 -12 -5 2 2151.35 246.222 1 -12 -5 2 2286.04 188.830 5 -12 5 2 2261.29 242.412 2 -12 5 2 2147.98 234.016 1 -12 -5 3 5402.00 330.547 2 -12 -5 3 5988.54 383.198 1 -12 -5 3 5878.33 273.606 5 -12 5 3 5569.99 361.677 1 -12 -5 4 1236.58 184.097 2 -12 -5 4 1114.65 193.442 1 -12 5 4 1343.76 208.051 1 -12 5 5 10317.8 506.870 1 -12 -5 5 10486.5 506.257 1 -12 -5 6 103.408 116.444 1 -12 -5 7 4743.70 359.306 1 -12 -5 8 1251.78 207.945 1 -12 -6 -5 3335.41 312.631 5 -12 -6 -4 5607.88 384.625 5 -12 6 -4 5710.36 427.252 3 -12 6 -3 5455.85 347.632 1 -12 6 -3 6194.07 430.592 3 -12 -6 -3 5855.36 371.328 5 -12 6 -3 5765.43 434.293 2 -12 6 -2 3611.46 323.131 3 -12 6 -2 3472.03 340.310 2 -12 6 -2 3765.95 298.286 1 -12 -6 -2 3228.06 267.194 5 -12 6 -1 1323.79 206.966 3 -12 -6 -1 1090.28 179.356 2 -12 6 -1 1120.27 173.821 1 -12 6 -1 1157.75 211.795 2 -12 -6 -1 1246.99 166.883 5 -12 -6 0 8020.06 370.957 5 -12 -6 0 8143.78 364.076 3 -12 6 0 8631.05 484.739 2 -12 -6 0 8545.37 447.338 2 -12 6 0 8409.09 427.537 1 -12 -6 1 758.821 121.033 5 -12 -6 1 818.508 135.955 3 -12 6 1 543.649 153.549 2 -12 -6 1 884.006 166.840 2 -12 6 1 719.076 149.832 1 -12 -6 2 6599.56 371.136 2 -12 6 2 6023.27 366.840 1 -12 6 2 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637.722 2 -12 -9 1 14727.3 521.568 5 -12 9 1 14802.3 563.503 1 -12 -9 2 2737.68 239.182 2 -12 9 2 2455.31 275.208 2 -12 9 2 2590.82 246.727 1 -12 -9 2 2896.88 231.274 5 -12 -9 3 6611.14 339.658 5 -12 9 3 7443.21 419.541 1 -12 -9 3 7098.16 438.186 1 -12 -9 3 7158.14 368.583 2 -12 -9 4 5824.65 328.459 2 -12 -9 4 5792.27 398.504 1 -12 -9 5 2723.68 273.212 1 -12 -9 5 2637.59 227.820 2 -12 -9 6 1267.05 196.221 1 -12 -9 7 2511.15 274.652 1 -12 -9 8 1196.16 203.792 1 -12 -9 9 2678.31 293.208 1 -12 -10 -4 1090.93 194.540 5 -12 -10 -3 2400.74 260.736 5 -12 10 -3 2492.68 308.659 3 -12 -10 -2 5789.12 377.510 5 -12 10 -2 5647.47 437.342 2 -12 10 -2 6016.14 441.549 3 -12 10 -1 370.184 147.906 2 -12 10 -1 268.152 113.468 1 -12 -10 -1 260.540 113.956 5 -12 10 0 8064.22 488.375 2 -12 -10 0 7862.52 410.885 2 -12 -10 0 7550.09 397.558 5 -12 10 0 7738.57 403.589 1 -12 -10 1 1281.05 179.672 2 -12 10 1 1107.54 211.649 2 -12 10 1 1050.84 178.652 1 -12 -10 1 1246.30 178.714 5 -12 10 2 4033.18 306.826 1 -12 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164.927 1 -12 -13 5 141.220 109.805 1 -12 -13 6 3179.72 301.843 1 -12 -13 7 515.983 154.777 1 -12 -13 8 9238.35 504.435 1 -12 -13 9 521.400 171.864 1 -12 -14 -3 1233.80 215.701 5 -12 -14 -2 15241.6 646.191 5 -12 14 -1 155.357 123.404 3 -12 14 -1 271.349 158.565 2 -12 -14 -1 320.599 132.854 5 -12 -14 0 4563.56 344.715 5 -12 14 0 4800.79 394.804 2 -12 -14 1 112.074 95.6271 5 -12 14 1 132.644 112.338 2 -12 14 2 10681.6 569.121 2 -12 -14 2 9963.62 476.461 5 -12 -14 4 13380.0 610.251 1 -12 -14 5 268.616 128.457 1 -12 -14 6 1931.93 251.719 1 -12 -14 7 2982.30 296.464 1 -12 -14 8 538.745 153.418 1 -12 -15 -2 52.2138 126.665 5 -12 -15 -1 496.869 151.510 5 -12 -15 0 93.1209 121.154 5 -12 15 0 138.060 134.896 2 -12 -15 1 1340.52 207.007 5 -12 15 1 1144.70 218.752 2 -12 -15 2 1584.58 207.441 5 -12 15 2 1756.73 260.363 2 -12 -15 4 837.305 177.427 1 -12 -15 5 4394.65 359.028 1 -12 -15 6 1086.17 193.439 1 -12 -15 8-31.2412 115.137 1 -12 -16 -1 249.886 123.359 5 -12 -16 0 5230.47 383.913 5 -12 16 1 710.547 188.297 2 -12 -16 1 675.172 169.562 5 -12 -16 2 1940.24 244.009 5 -12 16 2 1863.24 265.586 2 -12 -16 5 3885.84 344.255 1 -12 -16 6 1002.17 185.906 1 -12 -16 7 795.668 176.013 1 -12 -16 8 2013.39 259.202 1 -12 -17 -1 650.244 154.559 5 -12 -17 0 1189.68 210.395 5 -12 -17 1 584.757 166.181 5 -12 -17 2 128.556 113.691 5 -12 17 2 158.891 132.367 2 -12 -17 5 599.244 182.077 1 -12 -17 6 2266.94 258.831 1 -12 -17 7-91.2981 126.928 1 -12 -18 0 1569.44 218.136 5 -12 -18 1 4821.60 376.546 5 -12 -18 2 925.623 178.644 5 -12 -18 5 229.115 139.146 1 -12 -18 6 825.990 192.712 1 -12 -19 1 3454.86 320.999 5 -12 -19 2 658.384 164.818 5 -11 0 -7-78.9541 108.185 5 -11 0 -6 5214.78 373.448 5 -11 0 -5 58.9504 125.765 3 -11 0 -5-5.23944 91.4853 5 -11 0 -4 19052.1 610.370 5 -11 0 -4 18543.0 679.193 3 -11 0 -3 101.306 112.214 3 -11 0 -3 52.7259 112.932 2 -11 0 -3 211.028 106.490 5 -11 0 -2 40896.7 1000.48 2 -11 0 -2 37898.5 889.722 3 -11 0 -2 38958.5 768.345 5 -11 0 -1 98.1750 78.7729 5 -11 0 -1 251.481 128.892 2 -11 0 -1 137.233 88.0579 3 -11 0 0 11794.4 462.939 3 -11 0 0 12231.8 372.025 5 -11 0 0 11710.8 490.972 1 -11 0 0 12421.7 515.645 2 -11 0 1-63.1115 95.5468 1 -11 0 1 74.5492 98.1510 2 -11 0 1 89.7609 54.3407 5 -11 0 2 1738.87 203.379 1 -11 0 2 1739.34 120.887 5 -11 0 2 2071.09 215.267 2 -11 0 3 71.9521 43.4525 5 -11 0 3-47.8089 94.1633 1 -11 0 4 4595.59 325.694 1 -11 0 5-38.9753 93.5451 1 -11 0 6-28.2450 106.473 1 -11 0 7 84.7255 107.755 1 -11 1 -6 58.0695 110.595 5 -11 -1 -6 140.939 121.960 5 -11 -1 -5 9228.87 492.059 3 -11 1 -5 8867.02 448.246 5 -11 -1 -5 9146.34 458.686 5 -11 1 -5 8973.49 497.662 3 -11 -1 -4 186.035 104.159 5 -11 1 -4 64.1311 92.5399 5 -11 1 -4 289.129 136.743 3 -11 -1 -4 206.752 123.424 3 -11 1 -3 11958.9 567.194 2 -11 -1 -3 11023.3 446.922 5 -11 -1 -3 11495.0 504.045 3 -11 1 -3 11631.6 524.939 3 -11 1 -3 11259.5 436.980 5 -11 -1 -3 12143.1 568.013 2 -11 1 -2 6579.86 421.202 2 -11 -1 -2 6813.48 417.399 2 -11 -1 -2 6288.47 318.478 5 -11 -1 -2 6061.76 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2 -1 139520. 739.383 6 5 -2 -1 145611. 1081.34 4 5 2 0 16139.9 256.393 6 5 -2 1 49275.2 549.689 5 5 -2 2 205.229 49.3608 5 5 2 2 258.931 76.4619 2 5 2 2 200.063 50.2558 5 5 -2 3 11182.7 338.519 5 5 2 3 11523.6 359.729 5 5 -3 -14 735.829 184.212 4 5 -3 -13 624.901 155.952 4 5 -3 -13 547.872 153.759 5 5 3 -12 1345.88 175.196 4 5 -3 -12 1455.16 205.448 4 5 -3 -12 1523.65 206.863 5 5 3 -11 2083.31 194.135 4 5 -3 -11 2015.07 210.467 4 5 -3 -11 2020.64 212.252 5 5 3 -10 168.610 78.3685 4 5 -3 -10 246.124 106.475 4 5 -3 -10 165.806 85.4990 5 5 3 -9 4869.18 248.708 4 5 -3 -9 4994.48 288.007 4 5 -3 -9 4742.67 265.242 5 5 3 -8 9603.59 323.175 4 5 -3 -8 9560.91 372.651 4 5 -3 -8 9315.47 335.449 5 5 -3 -7 3401.71 217.879 4 5 -3 -7 3246.91 183.871 5 5 3 -7 3326.95 182.144 4 5 -3 -6 78399.5 926.149 4 5 3 -6 78665.7 959.865 6 5 -3 -6 80252.3 776.897 5 5 3 -6 80843.7 811.599 4 5 -3 -5 384.398 86.8279 4 5 3 -5 226.148 70.2224 6 5 -3 -5 285.915 52.1707 5 5 3 -5 323.450 68.5265 4 5 -3 -4 167484. 1281.09 1 5 3 -4 161883. 1044.18 4 5 3 -4 163525. 1142.47 6 5 -3 -4 165452. 1208.22 4 5 -3 -3 187.826 67.9556 1 5 3 -3 62.1337 54.2575 4 5 3 -3 266.804 65.4024 6 5 -3 -3 268.133 80.1737 4 5 3 -2 134799. 963.431 4 5 3 -2 133279. 848.905 6 5 -3 -2 135886. 1046.46 4 5 3 -1 61190.8 536.485 6 5 -3 -1 59602.6 700.236 4 5 3 0 42156.9 448.200 6 5 -3 0 41004.5 401.103 5 5 -3 0 41907.3 602.947 4 5 -3 1 70199.6 646.517 5 5 -3 2 1657.52 120.650 5 5 3 2 1605.49 134.776 2 5 -3 3 296.280 64.1344 5 5 -4 -14 67.1210 118.985 5 5 -4 -13 3668.42 324.610 4 5 -4 -13 3520.82 313.615 5 5 4 -12 2972.96 236.494 4 5 -4 -12 2837.69 267.644 4 5 4 -12 3214.07 321.008 6 5 -4 -12 2686.53 257.651 5 5 4 -11-102.111 91.9353 4 5 -4 -11-49.2146 106.838 4 5 -4 -11-98.9849 94.6184 5 5 4 -10 24430.3 576.539 4 5 -4 -10 24029.3 664.801 4 5 -4 -10 23534.3 630.757 5 5 4 -9 1407.79 140.188 4 5 -4 -9 1473.56 168.638 4 5 -4 -9 1414.21 156.475 5 5 4 -8 12191.0 354.739 4 5 -4 -8 11428.1 410.903 4 5 4 -8 11616.0 440.265 6 5 -4 -8 11495.9 371.262 5 5 -4 -7 3570.10 223.758 4 5 4 -7 3655.94 233.938 6 5 -4 -7 3577.64 191.639 5 5 4 -7 3669.74 186.497 4 5 -4 -6 15420.4 422.891 4 5 4 -6 15451.6 432.951 6 5 4 -6 15553.7 345.288 4 5 -4 -6 14963.2 334.730 5 5 4 -5 51565.1 593.246 4 5 4 -5 50480.8 711.000 6 5 -4 -5 51903.9 523.965 5 5 -4 -5 52246.9 736.182 4 5 -4 -4 891.991 112.463 4 5 4 -4 996.131 93.4876 4 5 4 -4 1035.43 116.045 6 5 -4 -4 1005.83 120.678 1 5 -4 -3 194788. 1321.84 1 5 4 -3 187921. 1097.68 4 5 4 -3 192273. 1153.53 6 5 -4 -3 193813. 1286.30 4 5 4 -2 5983.50 206.771 6 5 -4 -2 5710.46 222.589 4 5 4 -1 11165.3 251.162 6 5 -4 -1 10808.5 303.636 4 5 -4 0 120893. 670.092 5 5 4 0 123189. 834.005 6 5 -4 0 124999. 1045.71 4 5 -4 1 35306.8 453.704 5 5 4 1 36814.3 484.312 6 5 -4 2 35088.0 527.289 5 5 4 2 34425.6 600.549 2 5 -4 3 478.618 77.9084 5 5 -5 -13 6003.74 408.559 4 5 -5 -13 6009.92 404.868 5 5 -5 -12 339.118 125.149 4 5 5 -12 598.488 182.828 6 5 -5 -12 266.831 121.555 5 5 5 -11 4604.35 263.686 4 5 -5 -11 4325.30 311.616 4 5 5 -11 4812.45 357.393 6 5 -5 -11 4251.70 295.739 5 5 5 -10 2561.89 191.915 4 5 -5 -10 2694.33 241.269 4 5 5 -10 2494.84 252.257 6 5 -5 -10 2766.70 227.154 5 5 5 -9 19686.2 467.086 4 5 -5 -9 20089.2 586.528 4 5 5 -9 19402.4 612.931 6 5 -5 -9 19295.6 524.794 5 5 -5 -8 4471.80 268.379 4 5 5 -8 4763.74 296.925 6 5 -5 -8 4319.78 229.904 5 5 5 -8 4510.94 212.197 4 5 -5 -7 41242.8 747.180 4 5 5 -7 42207.8 782.276 6 5 5 -7 42333.1 591.009 4 5 -5 -7 41553.8 623.587 5 5 -5 -6 6105.25 279.016 4 5 5 -6 5458.47 268.367 6 5 5 -6 5712.30 208.030 4 5 -5 -6 5662.99 205.000 5 5 5 -5 44478.5 534.762 4 5 5 -5 43956.8 679.965 6 5 -5 -5 43649.0 472.851 5 5 -5 -5 45721.1 702.017 4 5 -5 -4 248.410 71.5284 4 5 -5 -4 267.217 70.8355 1 5 5 -4 282.305 55.1813 4 5 5 -4 309.158 70.6289 6 5 -5 -4 252.515 33.1996 5 5 -5 -3 4364.96 205.902 1 5 5 -3 3968.53 162.606 4 5 5 -3 4102.92 189.265 6 5 -5 -3 4286.52 205.630 4 5 -5 -2 51723.7 396.604 6 5 5 -2 52357.6 591.367 6 5 -5 -2 53543.9 678.548 4 5 -5 -2 53145.5 663.448 1 5 5 -1 85065.8 730.769 6 5 -5 -1 85481.9 856.996 4 5 -5 0 4753.54 132.409 5 5 5 0 4727.68 173.946 6 5 -5 0 4603.23 207.671 4 5 -5 1 44106.7 505.423 5 5 5 1 43849.6 555.888 6 5 -5 2 3009.26 155.787 5 5 5 2 2961.43 180.413 2 5 -5 3 53446.4 727.900 5 5 5 4 491.572 91.5914 3 5 -6 -13-159.703 137.327 4 5 -6 -13-125.317 128.257 5 5 -6 -12 3982.04 324.086 4 5 6 -12 3876.44 343.420 6 5 -6 -12 3874.13 303.284 5 5 -6 -11-201.730 100.298 5 5 6 -11 36.6722 66.6443 4 5 -6 -11 137.264 120.097 4 5 6 -11-64.6153 118.187 6 5 6 -10 5189.33 253.503 4 5 -6 -10 5558.41 336.031 4 5 6 -10 5665.84 361.851 6 5 -6 -10 5476.48 308.739 5 5 -6 -9 3103.80 253.379 4 5 6 -9 2496.96 242.199 6 5 -6 -9 2584.55 198.904 5 5 6 -9 2538.92 170.489 4 5 -6 -8 30690.8 691.978 4 5 6 -8 29452.6 710.502 6 5 6 -8 31141.4 525.269 4 5 -6 -8 30149.9 591.402 5 5 -6 -7 16321.6 479.737 4 5 6 -7 15655.8 489.498 6 5 6 -7 16574.6 356.621 4 5 -6 -7 15778.6 388.039 5 5 -6 -6 44484.7 742.978 4 5 6 -6 43944.0 752.826 6 5 6 -6 44095.3 541.246 4 5 -6 -6 43564.9 558.087 5 5 -6 -5 156653. 1326.53 4 5 6 -5 152852. 955.192 4 5 6 -5 150509. 1286.90 6 5 -6 -5 153417. 876.724 5 5 6 -4 11905.9 265.201 4 5 6 -4 11882.1 340.958 6 5 -6 -4 11397.4 181.965 5 5 -6 -4 12610.2 358.781 4 5 -6 -3 86547.0 904.481 1 5 6 -3 81636.0 819.399 6 5 -6 -3 84632.8 885.645 4 5 -6 -2 2803.84 130.684 6 5 6 -2 2775.35 183.529 6 5 6 -1 2191.33 135.686 6 5 -6 -1 2216.46 151.960 4 5 -6 0 1645.24 79.0638 5 5 -6 0 1775.95 141.231 4 5 -6 1 24465.3 375.250 5 5 6 1 23952.3 432.729 6 5 -6 2 58419.9 673.558 5 5 6 2 56589.9 759.788 2 5 -6 3 505.370 79.1441 5 5 6 4 34878.1 642.707 3 5 -7 -13-144.867 139.067 4 5 -7 -13 27.4649 102.168 5 5 -7 -12 2354.45 253.207 4 5 7 -12 2151.74 267.396 6 5 -7 -12 2093.56 229.080 5 5 -7 -11 1994.22 208.760 5 5 -7 -11 1587.38 216.435 4 5 7 -11 1517.51 226.608 6 5 -7 -10 387.936 102.681 5 5 7 -10 201.017 71.0252 4 5 -7 -10 555.555 132.795 4 5 7 -10 443.143 145.588 6 5 -7 -9 346.153 92.3165 5 5 7 -9 37.6598 51.6278 4 5 -7 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294.022 5 5 7 2 10253.6 327.692 2 5 -7 3 19430.9 442.656 5 5 7 4 6410.63 278.157 3 5 -8 -13 789.244 175.798 4 5 -8 -13 1046.17 180.638 5 5 -8 -12 562.803 148.196 5 5 -8 -12 505.655 147.896 4 5 8 -12 600.762 154.524 6 5 -8 -11 578.240 128.923 5 5 -8 -11 607.297 151.278 4 5 8 -11 893.385 185.487 6 5 -8 -10 2965.31 262.970 4 5 8 -10 2699.12 261.992 6 5 8 -10 2568.54 169.718 4 5 -8 -10 2366.18 206.177 5 5 8 -9 231.587 67.8377 4 5 -8 -9 226.235 91.4235 5 5 -8 -9 335.122 123.386 4 5 8 -9 324.689 148.436 6 5 -8 -8 2725.10 185.008 5 5 -8 -8 2576.87 220.294 4 5 8 -8 2880.40 243.208 6 5 8 -8 2835.34 150.922 4 5 -8 -7 30198.9 531.216 5 5 -8 -7 30221.1 677.481 4 5 8 -7 29543.3 682.893 6 5 8 -7 29761.3 434.369 4 5 -8 -6 15734.6 337.618 5 5 -8 -6 16305.6 474.347 4 5 8 -6 15584.7 296.436 4 5 8 -6 15563.5 472.093 6 5 -8 -5 88414.4 1035.34 4 5 -8 -5 88577.1 671.786 5 5 8 -5 86975.5 665.887 4 5 8 -5 87050.9 1019.09 6 5 -8 -4 9414.55 171.607 5 5 -8 -4 9550.34 285.284 6 5 8 -4 9728.37 326.303 6 5 -8 -4 10016.8 339.427 4 5 -8 -3 93555.1 751.144 6 5 -8 -3 98329.3 991.715 1 5 8 -3 95176.5 952.456 6 5 -8 -3 94920.0 978.738 4 5 -8 -2 445.186 55.8578 6 5 8 -2 562.675 96.4034 6 5 -8 -2 520.246 100.261 1 5 -8 -2 577.345 111.530 4 5 8 -1 36850.2 569.063 6 5 -8 -1 35129.9 320.916 6 5 -8 -1 37169.2 597.470 4 5 -8 -1 36033.6 534.492 1 5 -8 0 106117. 650.971 5 5 8 0 109319. 976.957 6 5 -8 0 104228. 1000.28 4 5 -8 1 80372.5 699.168 5 5 8 1 74697.6 832.424 6 5 -8 1 78607.1 884.687 4 5 8 1 78635.8 803.037 2 5 -8 2 19846.1 404.794 5 5 8 2 19840.8 454.751 6 5 8 2 19082.9 439.953 2 5 -8 3 6358.77 257.979 5 5 8 4 20569.6 490.908 3 5 -9 -13 3694.57 323.894 5 5 -9 -12 2724.13 260.788 5 5 -9 -12 3097.05 303.863 4 5 9 -12 3224.05 322.879 6 5 -9 -11 13439.5 572.386 4 5 9 -11 14001.4 612.666 6 5 -9 -11 13352.4 512.903 5 5 -9 -10 4205.34 316.676 4 5 9 -10 4277.07 330.634 6 5 -9 -10 3730.03 256.115 5 5 -9 -9 61307.7 929.126 5 5 -9 -9 62560.1 1099.07 4 5 9 -9 60797.6 1124.99 6 5 9 -9 60484.7 689.601 4 5 -9 -8 2013.00 162.187 5 5 -9 -8 2217.07 213.501 4 5 9 -8 2108.96 123.930 4 5 9 -8 2142.51 214.978 6 5 -9 -7 3259.27 182.102 5 5 -9 -7 3278.32 236.771 4 5 9 -7 3270.59 137.308 4 5 9 -7 3045.22 230.971 6 5 -9 -6 1000.75 90.3805 5 5 -9 -6 1338.24 151.546 4 5 9 -6 1000.16 73.5105 4 5 9 -6 872.112 129.700 6 5 -9 -5 26511.1 578.681 4 5 -9 -5 25624.6 371.742 5 5 -9 -5 24394.8 519.024 6 5 9 -5 26204.9 349.040 4 5 9 -5 25381.3 571.184 6 5 -9 -4 10058.4 184.151 5 5 -9 -4 10371.6 301.455 6 5 9 -4 10681.7 351.574 6 5 -9 -4 10596.1 352.096 4 5 -9 -3 6493.27 215.517 6 5 -9 -3 6684.50 266.004 1 5 9 -3 6734.85 278.946 6 5 -9 -3 6707.23 275.985 4 5 -9 -2 67483.3 786.915 1 5 -9 -2 64908.8 563.475 6 5 9 -2 66040.2 795.101 6 5 -9 -2 65338.8 808.414 4 5 -9 -1 170383. 1170.18 1 5 9 -1 176723. 1281.69 6 5 -9 -1 173205. 1300.55 4 5 -9 0 2834.89 113.338 5 5 9 0 3497.05 193.977 6 5 -9 0 2909.07 175.648 4 5 -9 0 2949.13 101.305 6 5 -9 1 111905. 832.527 5 5 9 1 110644. 1054.02 6 5 -9 1 111370. 1064.11 4 5 9 1 108103. 928.273 2 5 -9 2 2279.19 141.560 5 5 9 2 2275.13 183.553 6 5 9 2 2313.46 158.269 2 5 9 3 38797.7 692.904 2 5 -9 3 40173.9 647.462 5 5 9 4 2.97413 44.6265 3 5 -10 -12 5082.79 384.059 4 5 10 -12 4662.57 390.234 6 5 -10 -12 4409.17 322.394 5 5 -10 -11 91.1922 96.2244 5 5 -10 -11 279.981 133.030 4 5 10 -11 396.356 162.170 6 5 -10 -10 16781.2 533.199 5 5 -10 -10 16780.1 615.812 4 5 10 -10 17839.6 657.516 6 5 -10 -9 1946.40 182.038 5 5 -10 -9 2152.83 228.116 4 5 10 -9 2030.65 126.209 4 5 10 -9 1854.62 219.802 6 5 -10 -8 8974.33 330.850 5 5 -10 -8 9825.05 426.722 4 5 10 -8 9602.93 234.089 4 5 10 -8 9593.97 432.056 6 5 -10 -7 1000.17 112.516 5 5 -10 -7 1071.69 155.100 4 5 10 -7 967.951 72.0883 4 5 10 -7 1184.40 164.542 6 5 -10 -6 14677.5 470.450 4 5 -10 -6 13823.8 324.378 5 5 10 -6 13662.0 240.538 4 5 10 -6 13723.7 457.040 6 5 -10 -5 3211.52 216.317 4 5 -10 -5 3038.05 133.105 5 5 -10 -5 2943.34 185.379 6 5 10 -5 3004.10 210.010 6 5 -10 -4 4101.74 127.919 5 5 -10 -4 4578.02 213.037 6 5 10 -4 4593.07 247.990 6 5 -10 -4 4113.11 235.593 4 5 -10 -3 7265.88 134.282 5 5 -10 -3 7544.98 234.440 6 5 10 -3 7667.90 297.519 6 5 -10 -3 7968.71 302.603 4 5 -10 -2 121.720 23.8626 5 5 -10 -2 177.338 71.1997 1 5 -10 -2 137.362 21.6914 5 5 -10 -2 573.533 87.6536 6 5 10 -2 635.218 119.115 6 5 -10 -2 243.918 89.2342 4 5 -10 -1 50585.2 388.204 5 5 -10 -1 51678.7 655.399 1 5 10 -1 51479.7 724.779 6 5 -10 -1 50397.1 469.635 6 5 -10 -1 50904.9 718.464 4 5 -10 0 59439.6 521.972 5 5 10 0 58701.4 778.744 6 5 -10 0 57202.0 760.783 4 5 -10 0 56957.4 475.153 6 5 -10 1 41261.0 520.089 5 5 10 1 39919.8 659.950 6 5 -10 1 40778.2 655.428 4 5 10 1 39947.2 559.393 2 5 -10 2 77561.4 807.055 5 5 10 2 78645.0 985.589 6 5 10 2 75114.1 861.210 2 5 10 3 46.6770 36.3624 3 5 -10 3 51.8208 43.0598 5 5 10 3 142.606 73.5552 2 5 10 4 21834.9 489.736 3 5 -11 -12 206.883 115.794 5 5 -11 -12-55.0645 132.899 4 5 11 -12 28.4250 132.891 6 5 -11 -11 7782.76 447.980 4 5 11 -11 7336.38 455.147 6 5 -11 -11 7175.39 380.053 5 5 -11 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879.502 169.889 4 11 5 -7 2813.35 229.411 4 11 -5 -7 2946.39 270.901 4 11 5 -7 2668.10 215.338 6 11 5 -6 824.778 121.600 6 11 -5 -6 666.436 142.703 4 11 5 -5 1163.14 128.419 6 11 -5 -5 1027.75 165.161 4 11 5 -4-36.0543 61.2268 6 11 -5 -4 41.6177 91.4476 4 11 5 -3 3299.54 183.804 6 11 -5 -3 2880.88 257.201 4 11 5 -2 1191.82 112.582 6 11 6 -11 22.8367 123.684 6 11 -6 -11 358.984 158.928 4 11 6 -10 1409.93 203.748 6 11 -6 -10 1676.05 229.322 4 11 6 -9 644.145 131.099 4 11 6 -9 644.805 148.040 6 11 -6 -9 814.008 187.451 4 11 6 -8 2929.78 234.118 4 11 6 -8 2805.71 240.043 6 11 -6 -8 3260.07 293.907 4 11 6 -7 490.688 112.516 6 11 -6 -7 865.201 170.200 4 11 6 -6 149.730 85.0358 6 11 -6 -6 356.570 131.650 4 11 6 -5 3154.80 205.203 6 11 -6 -5 3400.30 278.619 4 11 6 -4 3437.12 204.620 6 11 -6 -4 3461.29 278.518 4 11 6 -3 16005.5 407.615 6 11 -6 -3 15320.2 574.767 4 11 6 -2 20941.8 450.839 6 11 6 -1 17112.6 401.230 6 11 7 -11 1508.10 226.550 6 11 -7 -11 1505.80 239.865 4 11 7 -10 729.592 163.338 6 11 -7 -10 723.505 167.247 4 11 7 -9 28.0217 102.924 6 11 -7 -9 357.125 147.147 4 11 7 -8 2278.84 228.118 6 11 -7 -8 1865.95 228.714 4 11 7 -7 211.966 89.6519 6 11 -7 -7 223.999 109.310 4 11 7 -6 10897.7 411.418 6 11 -7 -6 10800.9 495.849 4 11 7 -5-36.5715 61.9627 6 11 -7 -5 1.91178 92.8065 4 11 7 -4 15977.1 445.027 6 11 -7 -4 16258.4 591.111 4 11 7 -3 2644.27 185.559 6 11 -7 -3 2653.85 250.610 4 11 7 -2 14274.4 391.706 6 11 7 -1 851.538 115.820 6 11 8 -11-242.369 127.849 6 11 8 -10 330.366 132.903 6 11 -8 -10 344.170 146.316 4 11 8 -9 1109.95 188.130 6 11 -8 -9 910.173 180.120 4 11 8 -8 5878.48 351.031 6 11 -8 -8 6293.76 408.634 4 11 8 -7 8994.56 404.678 6 11 -8 -7 9223.09 469.533 4 11 8 -6 1935.14 190.601 6 11 -8 -6 1844.25 219.960 4 11 8 -5 5788.93 294.815 6 11 -8 -5 5672.48 363.760 4 11 8 -4 2435.62 194.902 6 11 -8 -4 2139.19 233.045 4 11 8 -3 4834.56 248.374 6 11 -8 -3 4829.87 334.406 4 11 8 -2 515.533 97.8565 6 11 8 -1 28837.9 575.366 6 11 9 -11 883.276 185.958 6 11 9 -10 1264.45 213.682 6 11 -9 -10 1328.92 225.716 4 11 9 -9 3916.55 315.504 6 11 -9 -9 4652.97 363.918 4 11 9 -8 3850.05 293.768 6 11 -9 -8 3967.66 329.634 4 11 9 -7 2047.47 215.579 6 11 -9 -7 2165.05 244.177 4 11 9 -6 4525.38 282.479 6 11 -9 -6 5191.26 360.869 4 11 9 -5 3605.30 244.899 6 11 -9 -5 3663.45 297.650 4 11 9 -4 1234.08 143.917 6 11 -9 -4 1467.11 194.095 4 11 9 -3 326.617 96.2524 6 11 -9 -3 337.811 121.510 4 11 9 -2 3918.27 228.740 6 11 -9 -2 4354.72 321.196 4 11 9 -1 2418.36 189.098 6 11 10 -11-98.3734 112.869 6 11 10 -10 6175.52 417.116 6 11 -10 -10 6528.75 439.205 4 11 10 -9 101.183 107.592 6 11 -10 -9-250.374 138.770 4 11 10 -8 4718.76 329.032 6 11 -10 -8 4891.15 365.351 4 11 10 -7 594.791 132.571 6 11 -10 -7 592.907 164.749 4 11 10 -6 1442.76 171.726 6 11 -10 -6 1331.51 204.542 4 11 10 -5 213.663 87.9851 6 11 -10 -5 245.140 109.851 4 11 10 -4 165.261 80.3047 6 11 -10 -4 478.672 150.250 4 11 10 -3 567.998 108.414 6 11 -10 -3 466.693 134.440 4 11 10 -2 773.791 128.316 6 11 -10 -2 822.054 167.579 4 11 10 -1 242.151 81.2889 6 11 11 -10 37.3459 116.540 6 11 11 -9 1667.00 225.667 6 11 -11 -9 1573.93 225.775 4 11 11 -8 335.228 123.701 6 11 -11 -8 644.804 168.874 4 11 11 -7 3777.06 286.049 6 11 -11 -7 4196.03 338.790 4 11 11 -6 219.595 110.138 6 11 -11 -6 142.131 121.151 4 11 11 -5 496.505 117.787 6 11 -11 -5 319.215 130.507 4 11 11 -4 3756.08 252.680 6 11 -11 -4 4232.40 322.187 4 11 11 -3 291.323 107.495 6 11 -11 -3 560.176 156.510 4 11 11 -2 4360.11 265.181 6 11 -11 -2 4951.86 342.965 4 11 11 -1 1148.59 150.399 6 11 11 0 3291.18 234.385 6 11 12 -10 276.707 139.346 6 11 12 -9 62.9753 117.413 6 11 -12 -9-67.4672 112.571 4 11 12 -8 2491.21 259.135 6 11 -12 -8 3094.13 308.287 4 11 12 -7 8127.79 421.855 6 11 -12 -7 8606.42 480.081 4 11 12 -6 3551.82 272.498 6 11 -12 -6 3860.46 326.340 4 11 12 -5 3081.73 247.825 6 11 -12 -5 3461.56 300.433 4 11 12 -4 172.007 97.5490 6 11 -12 -4 31.4687 96.0321 4 11 12 -3 20626.0 584.960 6 11 -12 -3 21824.6 719.272 4 11 12 -2 49.1846 76.6356 6 11 -12 -2 114.640 125.117 4 11 12 -1 29088.2 680.259 6 11 12 0 603.858 137.126 6 11 13 -10 1533.54 237.190 6 11 13 -9 94.1076 122.504 6 11 13 -8 287.043 128.355 6 11 -13 -8 721.081 182.275 4 11 13 -7 1600.73 215.747 6 11 -13 -7 1669.48 237.275 4 11 13 -6 7375.90 396.094 6 11 -13 -6 7786.16 455.267 4 11 13 -5 3739.12 279.115 6 11 -13 -5 4574.87 351.014 4 11 13 -4 10376.2 437.996 6 11 -13 -4 10311.6 504.697 4 11 13 -3 502.133 138.236 6 11 -13 -3 142.384 128.501 4 11 13 -2 8412.84 384.431 6 11 -13 -2 8399.46 453.010 4 11 13 -1 1151.72 165.752 6 11 13 0 17950.4 565.634 6 11 14 -9 2354.05 275.470 6 11 14 -8 3566.08 307.927 6 11 -14 -8 4730.89 378.946 4 11 14 -7 3962.47 313.957 6 11 -14 -7 3787.16 337.668 4 11 14 -6 2457.68 242.390 6 11 -14 -6 2607.63 288.797 4 11 14 -5 5180.79 339.466 6 11 -14 -5 5583.53 388.322 4 11 14 -4 391.761 117.036 6 11 -14 -4 550.755 166.170 4 11 14 -3 4236.15 292.990 6 11 -14 -3 4733.32 348.233 4 11 14 -2 535.697 128.178 6 11 -14 -2 517.923 161.964 4 11 14 -1 9067.89 409.855 6 11 14 0 15481.8 541.269 6 11 15 -9 2585.29 286.216 6 11 15 -8 508.108 153.992 6 11 15 -7 6519.89 406.847 6 11 -15 -7 6583.86 444.852 4 11 15 -6 266.747 128.543 6 11 -15 -6 123.909 119.684 4 11 15 -5 5971.57 367.189 6 11 -15 -5 7220.14 439.369 4 11 15 -4 514.169 133.431 6 11 -15 -4 591.902 155.039 4 11 15 -3 1699.02 197.081 6 11 -15 -3 1468.99 219.260 4 11 15 -2 297.850 106.794 6 11 -15 -2 604.408 164.016 4 11 15 -1 8733.77 415.196 6 11 15 0 339.871 133.067 6 11 16 -9 834.272 191.067 6 11 16 -8 1070.65 200.878 6 11 16 -7 1084.30 178.542 6 11 -16 -7 1183.64 221.488 4 11 16 -6 53.4679 104.611 6 11 -16 -6 318.289 145.325 4 11 16 -5 3793.19 306.585 6 11 -16 -5 4202.74 348.475 4 11 16 -4 510.059 147.426 6 11 -16 -4 231.851 123.807 4 11 16 -3 4186.61 303.064 6 11 -16 -3 5144.05 373.567 4 11 16 -2 39.0154 87.7200 6 11 -16 -2-76.6340 117.760 4 11 16 -1 245.931 107.294 6 11 16 0 2367.80 240.044 6 11 17 -8 380.058 145.373 6 11 17 -7 206.976 120.222 6 11 17 -6 1640.50 226.577 6 11 -17 -6 1757.77 253.381 4 11 17 -5 61.5667 117.880 6 11 -17 -5 377.295 169.539 4 11 17 -4 5157.15 350.673 6 11 -17 -4 4245.97 344.109 4 11 17 -3 548.834 146.541 6 11 -17 -3 347.098 143.096 4 11 17 -2 5564.14 356.610 6 11 -17 -2 5928.02 401.109 4 11 17 -1-163.998 108.047 6 11 17 0 6852.54 400.568 6 11 18 -8 311.855 132.576 6 11 18 -7 2682.75 281.202 6 11 18 -6 804.254 180.348 6 11 -18 -6 500.675 157.013 4 11 18 -5 14620.8 606.813 6 11 -18 -5 14733.7 646.879 4 11 18 -4 78.2527 116.782 6 11 -18 -4 206.781 121.371 4 11 18 -3 5827.50 377.536 6 11 -18 -3 6310.56 425.128 4 11 18 -2 3738.25 306.103 6 11 -18 -2 3879.99 335.475 4 11 18 -1 9750.27 477.372 6 11 18 0 2829.37 279.004 6 11 19 -7 203.213 131.428 6 11 19 -6 279.762 137.367 6 11 19 -5 1227.58 215.032 6 11 -19 -5 1198.21 211.095 4 11 19 -4 3541.14 312.143 6 11 -19 -4 3559.82 337.715 4 11 19 -3 307.147 131.842 6 11 -19 -3 464.613 161.169 4 11 19 -2 11110.2 524.775 6 11 -19 -2 12285.6 587.618 4 11 19 -1 1996.65 233.994 6 11 19 0 3897.92 325.031 6 11 20 -6 961.956 209.132 6 11 20 -5 45.0756 112.251 6 11 20 -4 307.147 148.196 6 11 -20 -4 256.976 141.257 4 11 20 -3 656.022 170.496 6 11 -20 -3 674.188 191.342 4 11 20 -2 3587.05 315.144 6 11 -20 -2 3536.88 328.046 4 11 20 -1 912.697 173.477 6 11 20 0 5647.84 395.314 6 11 21 -6 4865.02 385.488 6 11 21 -5 466.474 159.559 6 11 21 -4 3746.53 342.811 6 11 21 -3 348.680 141.479 6 11 -21 -3 405.136 150.606 4 11 21 -2 291.492 140.812 6 11 -21 -2 171.561 121.068 4 11 21 -1 562.284 174.578 6 11 21 0-19.7868 110.760 6 11 22 -5 1435.15 224.402 6 11 22 -4 706.968 179.204 6 11 22 -3 4774.98 378.186 6 11 22 -2-80.9503 127.690 6 11 22 -1 5520.39 403.111 6 11 22 0 50.3014 121.818 6 11 23 -3 3171.46 326.005 6 11 23 -2 2659.37 295.434 6 11 23 -1 192.077 130.678 6 12 0 -11-59.1206 112.838 4 12 0 -10 233.267 129.946 4 12 0 -9-69.9087 102.493 4 12 0 -8 239.749 122.469 4 12 0 -7 28.0154 97.1304 4 12 0 -6 11733.5 509.729 4 12 -1 -11 875.573 187.118 4 12 1 -10 2626.59 264.137 4 12 -1 -10 2418.27 266.127 4 12 1 -9-48.3140 102.140 4 12 -1 -9-120.206 121.907 4 12 1 -8 5440.12 354.678 4 12 -1 -8 5056.33 351.588 4 12 1 -7 64.9680 114.950 4 12 -1 -7 196.693 126.151 4 12 1 -6 11483.3 496.419 4 12 -1 -6 11121.6 498.734 4 12 -1 -5 654.476 157.861 4 12 -2 -11 6257.76 421.604 4 12 2 -10 246.523 117.879 4 12 -2 -10 330.500 145.794 4 12 2 -9 1970.17 229.211 4 12 -2 -9 1702.17 210.090 4 12 2 -8 512.465 150.617 4 12 -2 -8 306.489 130.249 4 12 2 -7 7488.57 411.077 4 12 -2 -7 7624.47 431.183 4 12 -2 -6 4839.51 340.106 4 12 -2 -5 17285.4 621.947 4 12 -3 -11 895.666 207.197 4 12 3 -10 4990.80 339.662 4 12 -3 -10 5057.65 373.339 4 12 3 -9-38.4756 93.7624 4 12 -3 -9 69.5933 109.978 4 12 3 -8 14009.8 545.625 4 12 -3 -8 14557.6 591.936 4 12 3 -7 4597.29 321.769 4 12 -3 -7 4862.64 347.107 4 12 -3 -6 5255.23 355.831 4 12 -3 -5 854.536 175.538 4 12 -4 -11 1592.66 237.916 4 12 -4 -10 607.832 158.515 4 12 4 -9 782.248 149.581 4 12 -4 -9 400.059 143.840 4 12 4 -8 321.406 132.362 4 12 -4 -8 428.489 151.401 4 12 -4 -7 2197.21 243.249 4 12 -4 -6 1468.76 219.654 4 12 -4 -5 1786.65 222.105 4 12 -4 -4 6319.61 390.924 4 12 -5 -10-23.7136 116.332 4 12 5 -9 42.6557 92.4249 4 12 -5 -9 251.955 139.809 4 12 -5 -8 1325.74 210.783 4 12 -5 -7 4897.93 359.621 4 12 -5 -6 200.436 134.456 4 12 -5 -5 9875.19 490.722 4 12 -5 -4 1357.38 208.108 4 12 -6 -10 288.646 139.829 4 12 6 -9 2548.80 244.191 6 12 -6 -9 3050.73 308.862 4 12 6 -8 676.150 141.410 6 12 -6 -8 1027.17 195.593 4 12 -6 -7 9808.77 497.317 4 12 -6 -6 2182.53 259.161 4 12 -6 -5 1013.54 183.467 4 12 -6 -4 11431.0 526.043 4 12 7 -10 2888.83 282.252 6 12 -7 -10 3346.94 320.409 4 12 7 -9 322.727 131.004 6 12 -7 -9 101.773 136.257 4 12 7 -8 9886.11 439.710 6 12 -7 -8 10326.6 529.006 4 12 7 -7 293.639 109.628 6 12 -7 -7 79.3952 120.671 4 12 -7 -6 1018.79 182.260 4 12 -7 -5-159.960 125.218 4 12 -7 -4 2624.76 270.270 4 12 8 -10 1144.80 192.554 6 12 8 -9 11005.5 501.316 6 12 -8 -9 12123.6 592.591 4 12 8 -8 1652.66 200.980 6 12 -8 -8 1831.37 254.183 4 12 8 -7 7945.15 385.062 6 12 -8 -7 8547.69 477.771 4 12 8 -6 1056.03 148.513 6 12 -8 -6 1016.75 181.332 4 12 -8 -5 1870.12 233.417 4 12 -8 -4 583.528 158.058 4 12 -8 -3 2565.11 273.232 4 12 9 -10 878.411 168.251 6 12 9 -9 2941.69 279.860 6 12 -9 -9 2463.74 290.357 4 12 9 -8 804.890 154.454 6 12 -9 -8 1449.27 228.689 4 12 9 -7 2909.83 246.560 6 12 -9 -7 2429.06 275.328 4 12 9 -6 1303.69 163.458 6 12 -9 -6 1410.72 221.110 4 12 9 -5 2465.65 204.794 6 12 -9 -5 2940.49 284.931 4 12 -9 -4 6022.57 397.017 4 12 -9 -3 7033.94 425.420 4 12 10 -10 38.2538 112.971 6 12 10 -9-188.090 135.716 6 12 10 -8 553.829 135.208 6 12 -10 -8 749.947 184.686 4 12 10 -7 798.924 143.239 6 12 -10 -7 848.307 192.255 4 12 10 -6 729.659 138.530 6 12 -10 -6 870.008 176.794 4 12 10 -5 77.5095 77.7163 6 12 -10 -5-4.38227 104.327 4 12 -10 -4 4141.05 338.226 4 12 -10 -3 421.113 148.366 4 12 11 -10 1320.76 206.416 6 12 11 -9-86.9426 116.375 6 12 11 -8 1709.19 209.215 6 12 -11 -8 2428.85 276.281 4 12 11 -7 648.224 139.575 6 12 -11 -7 753.070 194.020 4 12 11 -6 1793.52 197.415 6 12 -11 -6 2076.10 253.904 4 12 11 -5 3710.39 260.818 6 12 -11 -5 3429.78 313.088 4 12 11 -4 909.856 137.928 6 12 -11 -4 855.195 182.650 4 12 -11 -3 11318.1 550.889 4 12 12 -10 2682.32 290.405 6 12 12 -9 3990.76 333.203 6 12 12 -8-40.4616 96.9382 6 12 12 -7 1986.06 216.250 6 12 -12 -7 2603.13 293.845 4 12 12 -6 782.318 138.118 6 12 -12 -6 984.926 190.196 4 12 12 -5 1914.46 203.413 6 12 -12 -5 2107.61 264.638 4 12 12 -4-38.8667 82.4905 6 12 -12 -4 169.227 128.683 4 12 -12 -3 1052.91 199.656 4 12 13 -9 447.130 155.668 6 12 13 -8 8677.55 470.116 6 12 13 -7 997.562 171.504 6 12 -13 -7 1140.94 220.613 4 12 13 -6 2578.88 247.344 6 12 -13 -6 3106.77 310.066 4 12 13 -5 293.689 113.641 6 12 -13 -5 201.171 134.343 4 12 13 -4 220.558 104.670 6 12 -13 -4 600.992 167.311 4 12 13 -3 903.050 145.820 6 12 -13 -3 936.428 191.346 4 12 14 -9 1850.06 255.367 6 12 14 -8 653.711 179.280 6 12 14 -7 2926.79 280.192 6 12 14 -6 1822.40 217.306 6 12 -14 -6 1758.61 247.234 4 12 14 -5 215.712 110.314 6 12 -14 -5 206.708 134.065 4 12 14 -4 13290.2 517.695 6 12 -14 -4 13348.1 605.899 4 12 14 -3 82.4109 95.7264 6 12 -14 -3 154.607 122.454 4 12 15 -9 424.304 157.755 6 12 15 -8-179.969 130.299 6 12 15 -7 1173.46 184.038 6 12 15 -6 1170.28 188.537 6 12 -15 -6 1442.07 223.124 4 12 15 -5 4097.90 308.626 6 12 -15 -5 4212.04 353.012 4 12 15 -4 1410.10 189.874 6 12 -15 -4 1359.14 234.551 4 12 15 -3 4099.51 299.832 6 12 -15 -3 4823.08 377.630 4 12 16 -8 2110.43 263.829 6 12 16 -7 653.942 151.727 6 12 16 -6 991.523 175.421 6 12 16 -5 3691.63 306.281 6 12 -16 -5 4106.34 360.510 4 12 16 -4 4687.84 331.410 6 12 -16 -4 4746.40 378.472 4 12 16 -3 331.370 129.754 6 12 -16 -3 136.931 130.471 4 12 17 -8 3443.38 332.985 6 12 17 -7-50.0603 116.686 6 12 17 -6 2528.02 273.096 6 12 17 -5 272.307 122.962 6 12 17 -4 986.713 183.517 6 12 17 -3 406.698 147.860 6 12 -17 -3-136.510 144.005 4 12 17 -2 219.017 112.847 6 12 18 -7-1.33395 116.229 6 12 18 -6 726.634 179.829 6 12 18 -5 446.222 155.814 6 12 18 -4 2703.48 278.458 6 12 18 -3 570.954 156.483 6 12 18 -2 1058.77 177.833 6 12 19 -6 2450.36 276.699 6 12 19 -5 1471.12 223.104 6 12 19 -4 151.179 140.392 6 12 19 -3 3445.33 311.313 6 12 19 -2 589.386 152.050 6 12 20 -6 3390.71 328.333 6 12 20 -5 948.009 196.611 6 12 20 -4 10839.9 546.230 6 12 20 -3 227.198 136.178 6 12 20 -2 7546.23 451.695 6 12 21 -4 5407.09 404.114 6 12 21 -3 201.642 143.779 6 13 0 -10 914.846 185.382 4 13 0 -9 1.05715 105.756 4 13 0 -8 4757.69 350.734 4 13 0 -7-273.911 138.338 4 13 1 -10 60.9180 107.523 4 13 -1 -10 295.976 134.713 4 13 1 -9 549.908 149.678 4 13 -1 -9 252.356 125.003 4 13 1 -8 1499.49 210.630 4 13 -1 -8 1451.35 217.371 4 13 1 -7 318.766 135.419 4 13 -1 -7-96.3621 121.453 4 13 -1 -6 720.952 167.914 4 13 -2 -10 86.2053 107.588 4 13 2 -9 300.949 117.069 4 13 -2 -9 141.553 107.762 4 13 2 -8 372.453 113.500 4 13 -2 -8 270.247 122.303 4 13 -2 -7 153.741 130.332 4 13 -2 -6 2168.75 249.942 4 13 -3 -10 813.520 190.245 4 13 3 -9 957.220 170.294 4 13 -3 -9 1103.63 192.323 4 13 -3 -8 5.77222 114.625 4 13 -3 -7 388.577 137.103 4 13 -3 -6 835.128 177.482 4 13 4 -9 358.995 121.874 4 13 -4 -9 672.313 177.745 4 13 -4 -8 509.124 156.278 4 13 -4 -7 235.966 137.999 4 13 -4 -6-150.096 123.545 4 13 -4 -5 247.334 127.546 4 13 -5 -9 985.417 197.281 4 13 -5 -8 547.191 141.733 4 13 -5 -7 6168.22 412.224 4 13 -5 -6 936.494 171.070 4 13 -5 -5 3772.01 327.208 4 13 -6 -8 4064.20 352.738 4 13 -6 -7 1820.56 244.871 4 13 -6 -6 38.7432 108.786 4 13 -6 -5 3338.69 312.013 4 13 -7 -8 109.951 122.199 4 13 -7 -7 984.529 199.685 4 13 -7 -6 65.0007 113.538 4 13 -7 -5 2351.44 264.549 4 13 -8 -7 391.424 157.537 4 13 -8 -6 148.312 109.887 4 13 -8 -5 358.460 150.467 4 13 -8 -4 264.043 136.624 4 13 -9 -7 6626.78 450.015 4 13 -9 -6 14.8485 116.306 4 13 -9 -5 5246.26 389.322 4 13 -9 -4 90.8420 121.444 4 13 -10 -6 1466.25 228.195 4 13 -10 -5 166.567 151.977 4 13 -10 -4 4530.97 368.147 4 13 -11 -6 304.098 169.489 4 13 -11 -5 4712.19 381.617 4 13 -11 -4 1488.93 234.954 4 13 -12 -5 1038.86 213.884 4 13 -12 -4 815.529 202.270 4 14 0 -9 31.7958 133.145 4 14 0 -8 3981.51 344.171 4 14 1 -9 3769.34 336.732 4 14 -1 -8 5820.30 414.315 4 14 -2 -8 703.382 173.131 4 14 -2 -7 4675.12 375.310 4 14 -3 -7 2659.73 295.586 4 14 -4 -7 183.415 124.740 4 14 -5 -6 1434.18 222.724 4 0 0 0 0.00 0.00 0 TITL bmo280_3 in Pc REM Pc (#7 in standard setting) CELL 0.71073 10.732573 23.256205 9.763514 90.0000 105.3925 90.0000 ZERR 2.00 0.000162 0.000317 0.000169 0.0000 0.0017 0.0000 LATT -1 SYMM x,-y, z+1/2 SFAC C H N O Zn UNIT 74.00 100.00 16.00 24.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 30118 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.32959(2) 0.10066(2) -0.03161(2) 0.01876(7) Uani 1 1 d . . . . . O11 O 0.40038(17) 0.05229(7) 0.13505(15) 0.0388(4) Uani 1 1 d . . . . . O12 O 0.3185(14) 0.1110(5) 0.2650(7) 0.060(3) Uani 0.412(16) 1 d . U P . . O12' O 0.2617(7) 0.0856(4) 0.2387(7) 0.057(2) Uani 0.588(16) 1 d . U P . . C11 C 0.36561(19) 0.06196(9) 0.2444(2) 0.0298(4) Uani 1 1 d . . . . . C12 C 0.43555(16) 0.02944(8) 0.37701(18) 0.0214(3) Uani 1 1 d . . . . . C13 C 0.42158(18) 0.04654(8) 0.50908(19) 0.0251(3) Uani 1 1 d . . . . . H13 H 0.3682 0.0785 0.5155 0.030 Uiso 1 1 calc R U . . . C14 C 0.51446(17) -0.01704(8) 0.36862(18) 0.0234(3) Uani 1 1 d . . . . . H14 H 0.5248 -0.0287 0.2790 0.028 Uiso 1 1 calc R U . . . O21 O 0.20189(13) 0.04966(6) -0.15658(13) 0.0260(3) Uani 1 1 d . . . . . O22 O 0.23223(14) 0.10991(6) -0.32105(14) 0.0256(3) Uani 1 1 d . . . . . C21 C 0.18044(16) 0.06701(7) -0.28564(17) 0.0197(3) Uani 1 1 d . . . . . C22 C 0.08696(16) 0.03222(7) -0.39611(17) 0.0192(3) Uani 1 1 d . . . . . C23 C 0.08403(16) 0.03845(7) -0.53980(18) 0.0214(3) Uani 1 1 d . . . . . H23 H 0.1410 0.0647 -0.5670 0.026 Uiso 1 1 calc R U . . . C24 C 0.00239(16) -0.00617(7) -0.35761(17) 0.0208(3) Uani 1 1 d . . . . . H24 H 0.0038 -0.0103 -0.2604 0.025 Uiso 1 1 calc R U . . . N11 N 0.50307(15) 0.11060(7) -0.07454(17) 0.0235(3) Uani 1 1 d . . . . . N12 N 0.70333(15) 0.09420(7) -0.07984(18) 0.0248(3) Uani 1 1 d . . . . . N13 N 1.14021(16) 0.24236(7) 0.42133(17) 0.0254(3) Uani 1 1 d . . . . . N14 N 1.26240(15) 0.31933(6) 0.47139(16) 0.0225(3) Uani 1 1 d . . . . . C101 C 0.60756(17) 0.07871(7) -0.02302(18) 0.0221(3) Uani 1 1 d . . . . . H101 H 0.6137 0.0489 0.0450 0.027 Uiso 1 1 calc R U . . . C102 C 0.53481(19) 0.14817(8) -0.1689(2) 0.0309(4) Uani 1 1 d . . . . . H102 H 0.4787 0.1763 -0.2231 0.037 Uiso 1 1 calc R U . . . C103 C 0.6588(2) 0.13869(9) -0.1724(2) 0.0319(4) Uani 1 1 d . . . . . H103 H 0.7054 0.1588 -0.2276 0.038 Uiso 1 1 calc R U . . . C104 C 0.83288(17) 0.06813(9) -0.0479(2) 0.0285(4) Uani 1 1 d . . . . . H10A H 0.8468 0.0513 -0.1358 0.034 Uiso 1 1 calc R U . . . H10B H 0.8384 0.0367 0.0218 0.034 Uiso 1 1 calc R U . . . C105 C 0.93836(18) 0.11220(9) 0.0119(2) 0.0292(4) Uani 1 1 d . . . . . H10C H 0.9356 0.1423 -0.0606 0.035 Uiso 1 1 calc R U . . . H10D H 1.0235 0.0930 0.0310 0.035 Uiso 1 1 calc R U . . . C106 C 0.92610(18) 0.14087(8) 0.1483(2) 0.0263(3) Uani 1 1 d . . . . . H10E H 0.9214 0.1108 0.2186 0.032 Uiso 1 1 calc R U . . . H10F H 0.8447 0.1632 0.1277 0.032 Uiso 1 1 calc R U . . . C107 C 1.03958(18) 0.18090(9) 0.2125(2) 0.0284(4) Uani 1 1 d . . . . . H10G H 1.1217 0.1595 0.2259 0.034 Uiso 1 1 calc R U . . . H10H H 1.0399 0.2131 0.1461 0.034 Uiso 1 1 calc R U . . . C108 C 1.0308(2) 0.20478(9) 0.3541(2) 0.0309(4) Uani 1 1 d . . . . . H10I H 0.9494 0.2268 0.3396 0.037 Uiso 1 1 calc R U . . . H10J H 1.0276 0.1724 0.4189 0.037 Uiso 1 1 calc R U . . . C109 C 1.2414(2) 0.22841(9) 0.5345(2) 0.0365(5) Uani 1 1 d . . . . . H109 H 1.2568 0.1924 0.5821 0.044 Uiso 1 1 calc R U . . . C110 C 1.3155(2) 0.27645(9) 0.5649(2) 0.0369(5) Uani 1 1 d . . . . . H110 H 1.3925 0.2798 0.6397 0.044 Uiso 1 1 calc R U . . . C111 C 1.15598(17) 0.29731(7) 0.38620(19) 0.0225(3) Uani 1 1 d . . . . . H111 H 1.0987 0.3175 0.3107 0.027 Uiso 1 1 calc R U . . . O1D O 0.8723(2) 0.19206(12) 0.6554(2) 0.0730(7) Uani 1 1 d . U . . . N1D N 0.72627(19) 0.16072(9) 0.4583(2) 0.0397(4) Uani 1 1 d . U . . . C11D C 0.7866(3) 0.20204(13) 0.5457(3) 0.0519(6) Uani 1 1 d . U . . . H11D H 0.7625 0.2409 0.5226 0.062 Uiso 1 1 calc R U . . . C12D C 0.7567(3) 0.10130(12) 0.4870(4) 0.0593(8) Uani 1 1 d . U . . . H12A H 0.7616 0.0820 0.3994 0.089 Uiso 1 1 calc R U . . . H12B H 0.6892 0.0832 0.5231 0.089 Uiso 1 1 calc R U . . . H12C H 0.8400 0.0980 0.5583 0.089 Uiso 1 1 calc R U . . . C13D C 0.6224(4) 0.17392(18) 0.3342(4) 0.0790(11) Uani 1 1 d . U . . . H13A H 0.6271 0.1482 0.2563 0.119 Uiso 1 1 calc R U . . . H13B H 0.6303 0.2139 0.3058 0.119 Uiso 1 1 calc R U . . . H13C H 0.5393 0.1687 0.3564 0.119 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.02277(11) 0.01507(10) 0.01470(10) -0.00043(6) -0.00157(7) -0.00022(6) O11 0.0572(10) 0.0396(8) 0.0176(6) 0.0075(6) 0.0065(6) 0.0173(7) O12 0.082(6) 0.060(4) 0.035(3) 0.015(3) 0.008(3) 0.045(4) O12' 0.050(3) 0.085(4) 0.040(2) 0.034(3) 0.021(2) 0.043(3) C11 0.0299(9) 0.0349(10) 0.0243(9) 0.0097(7) 0.0069(7) 0.0084(8) C12 0.0223(7) 0.0239(8) 0.0165(7) 0.0016(6) 0.0025(6) 0.0011(6) C13 0.0286(8) 0.0255(8) 0.0213(8) 0.0018(6) 0.0066(7) 0.0070(7) C14 0.0276(8) 0.0254(8) 0.0166(7) -0.0008(6) 0.0047(6) 0.0023(6) O21 0.0330(6) 0.0249(6) 0.0155(6) 0.0003(5) -0.0014(5) -0.0094(5) O22 0.0327(7) 0.0207(6) 0.0213(6) -0.0010(5) 0.0034(5) -0.0070(5) C21 0.0218(7) 0.0177(7) 0.0168(7) -0.0021(6) 0.0003(6) -0.0004(6) C22 0.0219(7) 0.0171(7) 0.0156(7) -0.0009(5) -0.0003(6) -0.0007(6) C23 0.0235(7) 0.0209(7) 0.0183(7) 0.0005(6) 0.0030(6) -0.0034(6) C24 0.0248(7) 0.0211(7) 0.0145(7) 0.0004(6) 0.0019(6) -0.0009(6) N11 0.0240(7) 0.0199(6) 0.0228(7) 0.0009(5) -0.0005(6) -0.0011(5) N12 0.0235(7) 0.0224(7) 0.0257(8) 0.0005(6) 0.0017(6) -0.0022(5) N13 0.0286(7) 0.0207(7) 0.0262(8) -0.0001(6) 0.0062(6) -0.0046(6) N14 0.0268(7) 0.0175(6) 0.0204(7) 0.0022(5) 0.0014(5) -0.0007(5) C101 0.0238(7) 0.0194(7) 0.0204(8) -0.0013(6) 0.0011(6) -0.0021(6) C102 0.0292(9) 0.0245(9) 0.0343(10) 0.0093(7) 0.0000(7) -0.0014(7) C103 0.0308(9) 0.0292(9) 0.0333(10) 0.0094(8) 0.0042(8) -0.0053(7) C104 0.0241(8) 0.0267(9) 0.0334(10) -0.0043(7) 0.0053(7) 0.0006(7) C105 0.0219(8) 0.0305(9) 0.0350(10) -0.0034(8) 0.0072(7) -0.0035(7) C106 0.0240(8) 0.0222(8) 0.0317(9) -0.0001(7) 0.0060(7) -0.0035(6) C107 0.0245(8) 0.0267(9) 0.0336(10) -0.0039(7) 0.0071(7) -0.0047(7) C108 0.0313(9) 0.0276(9) 0.0352(10) -0.0030(8) 0.0111(8) -0.0104(7) C109 0.0409(11) 0.0223(9) 0.0403(11) 0.0105(8) 0.0003(9) -0.0013(8) C110 0.0373(10) 0.0254(9) 0.0373(11) 0.0107(8) -0.0089(8) -0.0025(8) C111 0.0256(8) 0.0198(7) 0.0212(8) 0.0007(6) 0.0046(6) -0.0010(6) O1D 0.0600(12) 0.1039(18) 0.0437(11) 0.0089(11) -0.0064(9) -0.0373(12) N1D 0.0357(9) 0.0368(9) 0.0421(10) -0.0001(8) 0.0022(8) -0.0042(7) C11D 0.0542(13) 0.0519(13) 0.0469(13) 0.0022(11) 0.0087(11) -0.0158(11) C12D 0.0511(15) 0.0445(15) 0.083(2) 0.0020(13) 0.0192(15) 0.0027(11) C13D 0.070(2) 0.075(2) 0.071(2) 0.0011(17) -0.0180(17) -0.0028(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O11 Zn1 O21 102.79(7) . . yes O11 Zn1 N11 93.57(7) . . yes O11 Zn1 N14 125.78(6) . 4_465 yes O21 Zn1 N11 117.80(6) . . yes O21 Zn1 N14 112.02(6) . 4_465 yes N14 Zn1 N11 104.57(6) 4_465 . yes C11 O11 Zn1 118.13(13) . . ? O12' O12 C11 67.2(6) . . ? O12 O12' C11 74.0(6) . . ? O11 C11 O12 121.1(4) . . ? O11 C11 C12 116.79(17) . . ? O12 C11 C12 115.8(3) . . ? O12' C11 O11 121.2(3) . . ? O12' C11 O12 38.9(4) . . ? O12' C11 C12 119.9(2) . . ? C13 C12 C11 119.83(16) . . ? C14 C12 C11 120.62(16) . . ? C14 C12 C13 119.55(15) . . ? C12 C13 H13 119.9 . . ? C14 C13 C12 120.25(16) 3_656 . ? C14 C13 H13 119.9 3_656 . ? C12 C14 C13 120.21(16) . 3_656 ? C12 C14 H14 119.9 . . ? C13 C14 H14 119.9 3_656 . ? C21 O21 Zn1 109.41(11) . . ? O21 C21 C22 116.59(15) . . ? O22 C21 O21 123.47(15) . . ? O22 C21 C22 119.95(15) . . ? C23 C22 C21 119.78(15) . . ? C24 C22 C21 120.71(15) . . ? C24 C22 C23 119.51(15) . . ? C22 C23 H23 120.1 . . ? C24 C23 C22 119.89(15) 3_554 . ? C24 C23 H23 120.1 3_554 . ? C22 C24 H24 119.7 . . ? C23 C24 C22 120.61(15) 3_554 . ? C23 C24 H24 119.7 3_554 . ? C101 N11 Zn1 126.01(13) . . ? C101 N11 C102 105.90(16) . . ? C102 N11 Zn1 127.94(13) . . ? C101 N12 C103 107.67(16) . . ? C101 N12 C104 125.90(16) . . ? C103 N12 C104 126.43(17) . . ? C109 N13 C108 126.06(17) . . ? C111 N13 C108 126.15(17) . . ? C111 N13 C109 107.74(16) . . ? C110 N14 Zn1 126.85(13) . 4_666 ? C111 N14 Zn1 127.24(12) . 4_666 ? C111 N14 C110 105.90(15) . . ? N11 C101 N12 110.89(16) . . ? N11 C101 H101 124.6 . . ? N12 C101 H101 124.6 . . ? N11 C102 H102 125.3 . . ? C103 C102 N11 109.38(17) . . ? C103 C102 H102 125.3 . . ? N12 C103 H103 126.9 . . ? C102 C103 N12 106.15(17) . . ? C102 C103 H103 126.9 . . ? N12 C104 H10A 109.3 . . ? N12 C104 H10B 109.3 . . ? N12 C104 C105 111.59(16) . . ? H10A C104 H10B 108.0 . . ? C105 C104 H10A 109.3 . . ? C105 C104 H10B 109.3 . . ? C104 C105 H10C 108.8 . . ? C104 C105 H10D 108.8 . . ? C104 C105 C106 113.64(16) . . ? H10C C105 H10D 107.7 . . ? C106 C105 H10C 108.8 . . ? C106 C105 H10D 108.8 . . ? C105 C106 H10E 109.1 . . ? C105 C106 H10F 109.1 . . ? C105 C106 C107 112.33(16) . . ? H10E C106 H10F 107.9 . . ? C107 C106 H10E 109.1 . . ? C107 C106 H10F 109.1 . . ? C106 C107 H10G 109.4 . . ? C106 C107 H10H 109.4 . . ? H10G C107 H10H 108.0 . . ? C108 C107 C106 111.18(16) . . ? C108 C107 H10G 109.4 . . ? C108 C107 H10H 109.4 . . ? N13 C108 C107 112.90(16) . . ? N13 C108 H10I 109.0 . . ? N13 C108 H10J 109.0 . . ? C107 C108 H10I 109.0 . . ? C107 C108 H10J 109.0 . . ? H10I C108 H10J 107.8 . . ? N13 C109 H109 127.0 . . ? C110 C109 N13 105.95(17) . . ? C110 C109 H109 127.0 . . ? N14 C110 H110 125.1 . . ? C109 C110 N14 109.74(18) . . ? C109 C110 H110 125.1 . . ? N13 C111 H111 124.7 . . ? N14 C111 N13 110.67(16) . . ? N14 C111 H111 124.7 . . ? C11D N1D C12D 121.6(3) . . ? C11D N1D C13D 121.3(3) . . ? C12D N1D C13D 117.0(3) . . ? O1D C11D N1D 122.9(3) . . ? O1D C11D H11D 118.6 . . ? N1D C11D H11D 118.6 . . ? N1D C12D H12A 109.5 . . ? N1D C12D H12B 109.5 . . ? N1D C12D H12C 109.5 . . ? H12A C12D H12B 109.5 . . ? H12A C12D H12C 109.5 . . ? H12B C12D H12C 109.5 . . ? N1D C13D H13A 109.5 . . ? N1D C13D H13B 109.5 . . ? N1D C13D H13C 109.5 . . ? H13A C13D H13B 109.5 . . ? H13A C13D H13C 109.5 . . ? H13B C13D H13C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 O11 1.9581(14) . yes Zn1 O21 1.9714(12) . yes Zn1 N11 2.0273(16) . yes Zn1 N14 1.9987(15) 4_465 yes O11 C11 1.241(2) . ? O12 O12' 0.838(9) . ? O12 C11 1.284(7) . ? O12' C11 1.231(4) . ? C11 C12 1.515(2) . ? C12 C13 1.395(2) . ? C12 C14 1.389(2) . ? C13 H13 0.9500 . ? C13 C14 1.390(2) 3_656 ? C14 C13 1.390(2) 3_656 ? C14 H14 0.9500 . ? O21 C21 1.284(2) . ? O22 C21 1.235(2) . ? C21 C22 1.500(2) . ? C22 C23 1.402(2) . ? C22 C24 1.394(2) . ? C23 H23 0.9500 . ? C23 C24 1.391(2) 3_554 ? C24 C23 1.391(2) 3_554 ? C24 H24 0.9500 . ? N11 C101 1.327(2) . ? N11 C102 1.376(2) . ? N12 C101 1.340(2) . ? N12 C103 1.373(2) . ? N12 C104 1.472(2) . ? N13 C108 1.471(2) . ? N13 C109 1.367(3) . ? N13 C111 1.346(2) . ? N14 Zn1 1.9985(15) 4_666 ? N14 C110 1.370(2) . ? N14 C111 1.324(2) . ? C101 H101 0.9500 . ? C102 H102 0.9500 . ? C102 C103 1.358(3) . ? C103 H103 0.9500 . ? C104 H10A 0.9900 . ? C104 H10B 0.9900 . ? C104 C105 1.524(3) . ? C105 H10C 0.9900 . ? C105 H10D 0.9900 . ? C105 C106 1.526(3) . ? C106 H10E 0.9900 . ? C106 H10F 0.9900 . ? C106 C107 1.529(3) . ? C107 H10G 0.9900 . ? C107 H10H 0.9900 . ? C107 C108 1.516(3) . ? C108 H10I 0.9900 . ? C108 H10J 0.9900 . ? C109 H109 0.9500 . ? C109 C110 1.358(3) . ? C110 H110 0.9500 . ? C111 H111 0.9500 . ? O1D C11D 1.235(4) . ? N1D C11D 1.333(3) . ? N1D C12D 1.430(3) . ? N1D C13D 1.445(4) . ? C11D H11D 0.9500 . ? C12D H12A 0.9800 . ? C12D H12B 0.9800 . ? C12D H12C 0.9800 . ? C13D H13A 0.9800 . ? C13D H13B 0.9800 . ? C13D H13C 0.9800 . ?