Crystallography Open Database

Information card for entry 1548637

Preview

Coordinates	1548637.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H20 Ag N O3 Si
Calculated formula	C18 H20 Ag N O3 Si
Title of publication	Photochemical syntheses, transformations, and bioorthogonal chemistry of <i>trans</i>-cycloheptene and sila <i>trans</i>-cycloheptene Ag(i) complexes.
Authors of publication	Fang, Yinzhi; Zhang, Han; Huang, Zhen; Scinto, Samuel L.; Yang, Jeffrey C.; Am Ende, Christopher W.; Dmitrenko, Olga; Johnson, Douglas S.; Fox, Joseph M.
Journal of publication	Chemical science
Year of publication	2018
Journal volume	9
Journal issue	7
Pages of publication	1953 - 1963
a	16.509 ± 0.001 Å
b	8.4282 ± 0.0005 Å
c	13.9655 ± 0.0008 Å
α	90°
β	114.69 ± 0.001°
γ	90°
Cell volume	1765.53 ± 0.18 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0395
Residual factor for significantly intense reflections	0.0369
Weighted residual factors for significantly intense reflections	0.1133
Weighted residual factors for all reflections included in the refinement	0.1174
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228793 (current)	2019-11-17	cif/ Updating files of 1548636, 1548637 Original log message: Adding full bibliography for 1548636--1548637.cif.	1548637.cif
204957	2018-01-09	cif/ Adding structures of 1548636, 1548637 via cif-deposit CGI script.	1548637.cif