#------------------------------------------------------------------------------ #$Date: 2018-01-13 08:32:49 +0200 (Sat, 13 Jan 2018) $ #$Revision: 205182 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/86/1548674.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1548674 loop_ _publ_author_name 'Guerrab, Walid' 'Akrad, Rachida' 'Ansar, Mhammed' 'Taoufik, Jamal' 'Mague, Joel T.' 'Ramli, Youssef' _publ_section_title ; 3-Benzyl-5,5-diphenylimidazolidine-2,4-dione ; _journal_coeditor_code VM4031 _journal_issue 1 _journal_name_full IUCrData _journal_page_first x171832 _journal_paper_doi 10.1107/S2414314617018326 _journal_volume 3 _journal_year 2018 _chemical_formula_iupac 'C22 H18 N2 O2' _chemical_formula_moiety 'C22 H18 N2 O2' _chemical_formula_sum 'C22 H18 N2 O2' _chemical_formula_weight 342.38 _chemical_name_systematic ; 3-Benzyl-5,5-diphenylimidazolidine-2,4-dione ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 67.9000(10) _cell_angle_beta 81.0270(10) _cell_angle_gamma 74.2940(10) _cell_formula_units_Z 4 _cell_length_a 8.8897(5) _cell_length_b 13.2911(7) _cell_length_c 16.6864(9) _cell_measurement_reflns_used 9954 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.2020 _cell_measurement_theta_min 2.3843 _cell_volume 1755.27(17) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2016 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.974 _diffrn_measurement_device_type 'Bruker SMART APEX CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0347 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 34377 _diffrn_reflns_theta_full 28.500 _diffrn_reflns_theta_max 29.340 _diffrn_reflns_theta_min 1.700 _exptl_absorpt_coefficient_mu 0.084 _exptl_absorpt_correction_T_max 0.98 _exptl_absorpt_correction_T_min 0.90 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.296 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 720 _exptl_crystal_size_max 0.372 _exptl_crystal_size_mid 0.213 _exptl_crystal_size_min 0.185 _refine_diff_density_max 0.426 _refine_diff_density_min -0.204 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 613 _refine_ls_number_reflns 9388 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.032 _refine_ls_R_factor_all 0.0613 _refine_ls_R_factor_gt 0.0469 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0832P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1224 _refine_ls_wR_factor_ref 0.1293 _reflns_number_gt 7122 _reflns_number_total 9388 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file vm4031sup1.cif _cod_data_source_block I _cod_database_code 1548674 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.969 _shelx_estimated_absorpt_t_max 0.985 _shelx_hkl_file ; -1 0 0 165.18 8.70 -1 0 0 162.78 8.90 -1 0 0 163.58 8.80 1 0 0 150.68 8.70 1 0 0 162.28 8.80 1 0 0 159.58 8.80 -2 0 0 5978.30 326.97 -2 0 0 6104.69 327.27 -2 0 0 6002.70 326.97 2 0 0 6080.09 327.07 2 0 0 5933.61 327.07 2 0 0 6125.19 327.17 -3 0 0 221.18 12.20 -3 0 0 221.48 12.00 -3 0 0 215.28 12.40 3 0 0 216.68 12.20 3 0 0 214.68 12.00 3 0 0 229.88 12.20 -4 0 0 687.63 37.80 -4 0 0 671.63 38.10 -4 0 0 718.73 38.30 -4 0 0 732.33 37.80 4 0 0 676.93 38.10 4 0 0 685.23 37.90 4 0 0 698.33 38.00 -5 0 0 9.20 1.80 -5 0 0 10.80 0.90 -5 0 0 14.70 1.20 -5 0 0 10.40 1.60 5 0 0 11.90 1.60 5 0 0 7.70 1.50 5 0 0 9.60 1.10 -6 0 0 0.60 1.60 -6 0 0 -0.50 1.40 -6 0 0 0.20 0.60 6 0 0 0.50 1.50 6 0 0 0.30 0.80 6 0 0 0.20 1.30 -7 0 0 35.30 3.70 -7 0 0 33.50 2.30 7 0 0 31.30 3.20 7 0 0 33.50 3.20 7 0 0 36.30 2.70 -8 0 0 70.79 4.20 -8 0 0 72.29 5.90 8 0 0 72.19 5.30 -9 0 0 -0.80 2.80 -9 0 0 -0.80 1.00 9 0 0 -0.20 1.60 9 0 0 0.00 2.60 -10 0 0 22.10 1.80 -10 0 0 16.50 4.30 10 0 0 23.40 2.70 10 0 0 17.90 3.70 -11 0 0 5.40 1.10 -11 0 0 7.30 5.00 11 0 0 6.70 2.70 11 0 0 6.60 3.70 11 -1 0 13.80 2.80 11 -1 0 8.70 4.10 -11 1 0 11.30 5.50 10 -1 0 0.60 2.00 10 -1 0 -1.20 3.00 -10 1 0 0.30 3.50 -10 1 0 -0.20 0.70 9 -1 0 6.90 2.80 9 -1 0 9.30 1.80 -9 1 0 9.70 1.10 -9 1 0 6.00 3.10 8 -1 0 5.30 2.30 8 -1 0 3.40 1.40 8 -1 0 4.50 2.60 -8 1 0 4.00 2.70 -8 1 0 3.40 0.80 7 -1 0 224.88 13.50 7 -1 0 230.78 13.00 7 -1 0 249.78 13.50 -7 1 0 231.48 13.90 -7 1 0 232.38 12.70 -7 1 0 220.58 13.50 6 -1 0 76.29 4.60 6 -1 0 83.59 5.10 6 -1 0 64.79 5.00 -6 1 0 79.59 5.20 -6 1 0 77.09 5.50 -6 1 0 82.89 4.40 5 -1 0 34.60 2.70 5 -1 0 31.20 2.80 5 -1 0 33.70 2.30 -5 1 0 30.00 2.70 -5 1 0 33.50 2.20 -5 1 0 38.40 2.10 -5 1 0 31.90 3.10 4 -1 0 26.10 2.10 4 -1 0 28.10 1.80 4 -1 0 21.40 2.00 -4 1 0 21.90 2.10 -4 1 0 29.20 1.70 -4 1 0 27.60 2.50 -4 1 0 29.80 1.70 3 -1 0 1315.87 71.99 3 -1 0 1293.97 71.79 -3 1 0 1386.26 71.79 -3 1 0 1343.77 72.19 -3 1 0 1336.87 71.79 -3 1 0 1266.17 71.99 2 -1 0 5.00 0.80 2 -1 0 4.80 0.50 -2 1 0 4.50 0.40 -2 1 0 5.70 0.40 -2 1 0 3.10 0.70 -2 1 0 4.70 0.90 1 -1 0 504.85 27.50 1 -1 0 477.85 27.40 -1 1 0 510.05 27.50 -1 1 0 511.55 27.30 -1 1 0 520.65 27.50 0 -1 0 6.60 0.40 0 1 0 6.90 0.50 0 1 0 7.30 0.50 0 1 0 6.80 0.40 -1 -1 0 2064.89 110.39 -1 -1 0 2058.99 110.29 1 1 0 1983.20 110.29 1 1 0 2018.10 110.39 1 1 0 2058.89 110.29 -2 -1 0 120.29 7.00 -2 -1 0 130.09 6.80 2 1 0 118.49 6.80 2 1 0 123.89 6.90 2 1 0 126.79 6.90 -3 -1 0 57.79 3.70 -3 -1 0 56.19 3.30 3 1 0 62.09 3.30 3 1 0 54.99 3.50 3 1 0 56.29 3.40 -4 -1 0 14.70 1.20 -4 -1 0 13.40 1.70 4 1 0 18.00 1.30 4 1 0 15.10 1.50 4 1 0 17.70 1.60 4 1 0 14.20 1.20 -5 -1 0 370.66 21.70 -5 -1 0 383.86 21.20 5 1 0 387.46 21.30 5 1 0 391.76 21.40 5 1 0 404.26 21.20 5 1 0 384.66 21.50 -6 -1 0 9.20 2.10 -6 -1 0 8.60 1.00 6 1 0 8.90 1.20 6 1 0 10.20 1.80 6 1 0 7.50 1.60 -7 -1 0 30.10 2.10 -7 -1 0 29.20 3.30 7 1 0 29.50 2.90 7 1 0 22.60 2.70 7 1 0 24.30 2.30 -8 -1 0 102.49 7.40 -8 -1 0 98.79 6.00 8 1 0 107.29 6.30 8 1 0 106.99 6.90 -9 -1 0 1.20 2.70 -9 -1 0 0.00 1.00 9 1 0 -1.00 1.50 9 1 0 -1.20 2.30 -10 -1 0 57.99 6.20 -10 -1 0 55.39 3.70 10 1 0 62.49 5.50 10 1 0 57.69 4.60 -11 -1 0 -2.20 4.10 -11 -1 0 -0.60 1.30 11 1 0 0.60 3.50 11 1 0 1.30 2.40 11 -2 0 76.99 6.10 11 -2 0 85.99 7.60 10 -2 0 1.80 3.30 10 -2 0 0.90 2.00 -10 2 0 -1.80 3.60 9 -2 0 3.50 2.70 9 -2 0 1.40 1.60 -9 2 0 3.20 3.00 8 -2 0 12.40 2.60 8 -2 0 12.50 1.70 8 -2 0 9.60 2.90 -8 2 0 8.40 2.60 -8 2 0 10.50 0.90 -8 2 0 9.60 2.90 7 -2 0 449.46 25.20 7 -2 0 453.55 25.70 7 -2 0 451.45 25.70 -7 2 0 456.35 25.70 -7 2 0 478.35 26.20 -7 2 0 460.95 24.90 6 -2 0 84.59 4.80 6 -2 0 80.89 5.30 6 -2 0 74.69 5.40 -6 2 0 81.89 4.60 -6 2 0 79.59 5.70 -6 2 0 78.69 4.50 -6 2 0 80.29 5.30 5 -2 0 37.50 3.00 5 -2 0 35.30 2.90 5 -2 0 35.50 2.30 -5 2 0 28.90 3.10 -5 2 0 35.30 2.10 -5 2 0 31.00 2.80 -5 2 0 38.10 2.10 4 -2 0 123.39 6.80 4 -2 0 111.29 7.20 -4 2 0 125.29 6.70 -4 2 0 116.49 7.20 -4 2 0 123.69 6.70 -4 2 0 126.99 7.40 3 -2 0 179.18 9.90 3 -2 0 174.28 9.90 3 -2 0 171.88 10.10 -3 2 0 186.38 9.80 -3 2 0 192.38 9.80 -3 2 0 179.38 10.30 -3 2 0 164.98 10.10 2 -2 0 652.83 35.70 2 -2 0 652.93 35.90 2 -2 0 640.34 35.70 -2 2 0 677.73 35.60 -2 2 0 665.73 36.00 -2 2 0 661.73 35.60 -2 2 0 650.93 35.90 1 -2 0 1074.49 58.89 1 -2 0 1052.09 58.89 1 -2 0 1049.40 59.09 -1 2 0 1108.89 58.89 -1 2 0 1091.69 58.89 -1 2 0 1129.49 59.09 -1 2 0 1080.39 59.09 -1 2 0 1113.09 59.09 0 -2 0 936.71 52.19 0 2 0 979.00 52.29 0 2 0 974.30 52.19 0 2 0 960.50 52.29 -1 -2 0 341.77 18.20 -1 -2 0 324.47 18.20 -1 -2 0 328.97 18.20 1 2 0 357.46 18.20 1 2 0 325.07 18.20 1 2 0 325.67 18.20 -2 -2 0 149.99 8.70 -2 -2 0 159.68 8.90 -2 -2 0 153.78 8.70 2 2 0 165.58 8.80 2 2 0 152.08 8.70 2 2 0 164.28 8.80 2 2 0 165.38 8.70 -3 -2 0 130.49 7.10 -3 -2 0 125.19 7.30 -3 -2 0 117.69 7.00 3 2 0 133.09 7.10 3 2 0 125.59 7.00 3 2 0 129.29 7.10 3 2 0 124.39 7.20 -4 -2 0 23.80 1.70 -4 -2 0 22.80 2.20 -4 -2 0 21.20 1.50 4 2 0 21.90 1.60 4 2 0 22.20 1.70 4 2 0 22.10 1.80 4 2 0 20.10 1.80 -5 -2 0 99.29 5.80 -5 -2 0 97.19 6.40 5 2 0 105.49 6.20 5 2 0 109.29 5.90 5 2 0 108.29 6.00 5 2 0 98.59 6.10 -6 -2 0 6.00 1.80 -6 -2 0 4.40 0.90 6 2 0 5.30 1.50 6 2 0 6.40 1.10 6 2 0 7.30 1.60 -7 -2 0 0.40 1.90 -7 -2 0 -0.30 0.90 7 2 0 2.50 1.80 7 2 0 1.40 1.10 7 2 0 0.60 1.60 -8 -2 0 0.70 1.00 -8 -2 0 -0.80 2.20 8 2 0 1.70 1.40 8 2 0 -0.60 1.90 -9 -2 0 1.60 2.70 -9 -2 0 3.50 1.20 9 2 0 5.60 1.80 9 2 0 3.40 2.40 -10 -2 0 2.30 1.40 -10 -2 0 0.30 3.30 10 2 0 1.60 2.00 10 2 0 -0.60 2.80 -11 -2 0 55.69 6.60 -11 -2 0 45.60 3.60 11 2 0 49.90 5.50 11 2 0 52.59 4.50 10 -3 0 20.20 4.10 10 -3 0 19.20 2.70 -10 3 0 26.20 5.00 9 -3 0 19.50 3.50 9 -3 0 20.50 2.40 -9 3 0 26.20 3.90 -9 3 0 23.30 4.30 8 -3 0 5.00 2.70 8 -3 0 1.20 2.80 8 -3 0 2.30 1.40 -8 3 0 -0.80 2.60 -8 3 0 3.60 2.50 7 -3 0 5.90 1.30 7 -3 0 8.80 2.60 7 -3 0 9.40 2.40 -7 3 0 9.30 2.70 -7 3 0 9.00 2.40 6 -3 0 421.66 23.20 6 -3 0 408.16 23.10 6 -3 0 415.96 22.70 -6 3 0 401.76 23.20 -6 3 0 418.86 23.50 -6 3 0 418.16 22.40 -6 3 0 406.46 22.40 5 -3 0 38.50 2.50 5 -3 0 35.10 3.10 -5 3 0 41.30 2.20 -5 3 0 36.20 3.10 -5 3 0 37.80 2.20 -5 3 0 39.90 3.50 4 -3 0 -0.10 0.60 4 -3 0 0.40 0.80 4 -3 0 0.40 1.10 -4 3 0 -0.50 1.00 -4 3 0 0.60 0.30 -4 3 0 0.60 0.30 -4 3 0 1.70 1.30 3 -3 0 -0.20 0.40 3 -3 0 0.20 0.60 3 -3 0 -0.30 1.00 -3 3 0 -0.20 0.90 -3 3 0 -0.20 0.30 -3 3 0 0.10 0.20 -3 3 0 0.20 1.00 2 -3 0 788.22 43.40 2 -3 0 797.02 43.70 2 -3 0 791.32 43.40 -2 3 0 796.92 43.70 -2 3 0 800.02 43.40 -2 3 0 799.92 43.70 -2 3 0 827.02 43.40 1 -3 0 32.20 2.40 1 -3 0 35.00 2.20 -1 3 0 36.80 2.40 -1 3 0 34.70 2.40 -1 3 0 38.80 2.10 -1 3 0 39.20 2.10 -1 3 0 38.90 2.30 0 -3 0 1174.48 65.09 0 3 0 1232.08 65.19 0 3 0 1206.08 65.09 0 3 0 1190.48 65.19 -1 -3 0 154.38 8.70 1 3 0 157.88 8.70 1 3 0 159.98 8.80 1 3 0 160.88 8.80 -2 -3 0 40.60 2.40 -2 -3 0 39.70 2.30 -2 -3 0 37.50 2.50 2 3 0 35.50 2.40 2 3 0 41.20 2.30 2 3 0 38.90 2.40 2 3 0 38.60 2.30 -3 -3 0 14.20 1.20 -3 -3 0 10.90 1.30 -3 -3 0 10.60 1.00 3 3 0 13.90 1.30 3 3 0 12.20 1.30 3 3 0 12.40 1.10 3 3 0 12.90 1.10 -4 -3 0 79.89 5.30 -4 -3 0 80.09 4.90 -4 -3 0 92.19 5.00 4 3 0 90.79 5.00 4 3 0 90.59 5.20 4 3 0 83.89 5.10 4 3 0 85.99 5.00 -5 -3 0 18.10 1.70 -5 -3 0 19.90 2.30 -5 -3 0 15.70 1.50 5 3 0 19.00 1.80 5 3 0 17.90 1.90 5 3 0 21.70 1.80 5 3 0 23.90 1.80 -6 -3 0 -1.00 0.80 -6 -3 0 0.10 1.60 6 3 0 -0.50 1.00 6 3 0 -0.10 1.40 6 3 0 -1.10 1.40 -7 -3 0 37.20 2.40 -7 -3 0 32.80 3.90 7 3 0 33.40 3.10 7 3 0 27.70 2.70 7 3 0 30.70 3.10 -8 -3 0 1.50 2.40 -8 -3 0 1.90 1.10 8 3 0 2.50 2.00 8 3 0 2.60 1.40 -9 -3 0 5.80 3.30 -9 -3 0 7.10 1.40 9 3 0 4.00 2.50 9 3 0 2.90 1.90 -10 -3 0 3.00 1.50 -10 -3 0 1.50 3.30 10 3 0 3.60 3.20 10 3 0 3.00 2.10 -11 -3 0 4.60 4.30 -11 -3 0 5.20 1.80 11 3 0 4.30 2.90 11 3 0 1.30 3.90 12 3 0 6.60 5.20 10 -4 0 39.70 3.80 10 -4 0 50.29 5.50 -10 4 0 56.29 5.80 -10 4 0 39.20 6.00 9 -4 0 -0.30 3.00 9 -4 0 -0.40 1.70 -9 4 0 -1.10 2.80 -9 4 0 0.90 3.40 8 -4 0 1.20 1.40 8 -4 0 2.30 2.40 8 -4 0 4.30 2.80 -8 4 0 2.10 2.80 -8 4 0 1.70 3.20 7 -4 0 51.99 4.70 7 -4 0 53.89 3.40 7 -4 0 45.80 4.30 -7 4 0 46.20 4.70 -7 4 0 41.00 4.20 6 -4 0 73.79 4.60 6 -4 0 83.49 5.60 -6 4 0 74.89 5.90 -6 4 0 76.69 5.40 5 -4 0 47.40 3.10 5 -4 0 38.70 3.80 -5 4 0 52.09 3.70 -5 4 0 54.39 4.20 4 -4 0 8.40 0.90 4 -4 0 6.60 1.60 -4 4 0 11.00 2.00 -4 4 0 8.90 1.60 3 -4 0 0.00 0.50 3 -4 0 0.00 1.10 3 -4 0 0.00 0.60 -3 4 0 0.40 1.20 -3 4 0 0.70 1.00 2 -4 0 483.95 25.60 2 -4 0 460.05 25.60 2 -4 0 474.65 25.90 -2 4 0 472.15 25.90 -2 4 0 466.95 25.50 -2 4 0 467.55 25.50 -2 4 0 452.75 25.90 -2 4 0 488.05 25.90 1 -4 0 6.40 1.10 1 -4 0 8.50 0.70 1 -4 0 9.50 0.80 -1 4 0 9.40 0.70 -1 4 0 10.30 1.20 -1 4 0 10.00 1.20 -1 4 0 9.50 0.70 -1 4 0 10.00 1.00 0 -4 0 202.28 11.60 0 4 0 216.68 11.60 0 4 0 212.48 11.80 0 4 0 212.58 11.80 0 4 0 217.18 11.60 -1 -4 0 47.10 2.80 1 4 0 48.80 2.70 1 4 0 49.70 2.90 1 4 0 43.20 2.90 -2 -4 0 3596.24 187.98 -2 -4 0 3589.44 187.98 -2 -4 0 3514.75 187.98 2 4 0 3558.74 188.08 2 4 0 3312.77 187.98 2 4 0 3348.86 188.08 2 4 0 3361.66 187.98 -3 -4 0 2.60 0.60 -3 -4 0 1.70 0.70 -3 -4 0 2.10 0.90 3 4 0 2.20 0.70 3 4 0 2.00 0.70 3 4 0 1.70 0.90 3 4 0 2.30 0.80 -4 -4 0 455.75 25.70 -4 -4 0 471.15 25.70 -4 -4 0 469.05 26.00 4 4 0 473.05 25.70 4 4 0 471.35 25.80 4 4 0 473.25 25.90 4 4 0 476.25 25.70 -5 -4 0 25.90 2.00 -5 -4 0 25.90 2.60 -5 -4 0 30.40 2.40 5 4 0 30.50 2.10 5 4 0 28.30 2.40 5 4 0 31.70 2.50 -6 -4 0 15.80 1.60 -6 -4 0 16.70 2.40 6 4 0 17.40 2.10 6 4 0 23.10 1.90 6 4 0 24.50 2.10 6 4 0 14.20 2.10 -7 -4 0 60.39 4.90 -7 -4 0 51.09 3.50 7 4 0 55.99 4.20 7 4 0 49.70 4.00 7 4 0 56.29 3.70 -8 -4 0 17.20 3.30 -8 -4 0 16.00 1.80 8 4 0 17.20 2.20 8 4 0 12.30 2.50 -9 -4 0 52.29 3.50 -9 -4 0 51.49 5.10 9 4 0 43.40 4.00 9 4 0 44.30 4.50 -10 -4 0 15.20 4.30 -10 -4 0 12.50 1.90 10 4 0 16.40 3.40 10 4 0 15.70 2.70 -11 -4 0 -0.50 4.10 -11 -4 0 1.10 1.80 11 4 0 -1.40 3.80 11 4 0 -1.30 2.70 -12 -4 0 40.60 7.60 12 4 0 45.20 5.90 10 -5 0 1.70 3.90 10 -5 0 3.20 2.40 -10 5 0 4.80 4.90 -10 5 0 4.00 4.70 9 -5 0 3.20 3.30 9 -5 0 2.60 1.90 -9 5 0 0.80 3.30 -9 5 0 5.40 4.50 8 -5 0 45.70 3.70 8 -5 0 52.29 5.20 8 -5 0 41.60 4.60 -8 5 0 45.50 5.40 -8 5 0 56.59 5.30 7 -5 0 31.50 3.60 7 -5 0 35.70 3.80 7 -5 0 29.60 2.70 -7 5 0 33.30 4.20 -7 5 0 26.10 3.50 6 -5 0 448.56 24.80 6 -5 0 432.46 24.10 -6 5 0 433.46 25.00 -6 5 0 441.96 24.70 5 -5 0 51.49 4.10 5 -5 0 51.39 3.30 -5 5 0 52.39 4.50 -5 5 0 55.79 4.20 4 -5 0 103.79 6.50 4 -5 0 114.99 7.10 -4 5 0 120.49 7.10 -4 5 0 128.69 7.30 3 -5 0 441.86 23.80 3 -5 0 413.46 23.80 3 -5 0 442.66 24.20 -3 5 0 435.96 24.20 -3 5 0 445.96 24.20 2 -5 0 -0.20 1.00 2 -5 0 -0.10 0.60 2 -5 0 0.10 0.50 -2 5 0 0.20 0.20 -2 5 0 -1.00 0.90 -2 5 0 -0.50 1.10 -2 5 0 0.00 0.20 -2 5 0 0.40 0.90 1 -5 0 0.90 0.50 1 -5 0 0.50 0.60 1 -5 0 0.70 0.90 -1 5 0 1.30 1.00 -1 5 0 1.10 0.40 -1 5 0 1.20 0.80 -1 5 0 1.30 0.30 -1 5 0 0.30 1.00 0 -5 0 7.10 0.80 0 5 0 7.90 0.70 0 5 0 6.00 1.20 0 5 0 9.00 1.30 0 5 0 8.50 0.70 -1 -5 0 467.65 25.10 1 5 0 447.06 25.30 1 5 0 462.85 25.30 1 5 0 461.05 25.00 -2 -5 0 234.08 13.10 -2 -5 0 246.38 13.10 -2 -5 0 232.58 13.10 2 5 0 243.68 13.10 2 5 0 243.28 13.10 2 5 0 236.48 13.30 2 5 0 227.68 13.30 -3 -5 0 267.47 14.50 -3 -5 0 264.87 14.70 -3 -5 0 265.07 14.60 3 5 0 265.77 14.70 3 5 0 269.17 14.60 3 5 0 262.87 14.70 3 5 0 254.37 14.60 -4 -5 0 54.69 3.80 -4 -5 0 53.89 3.50 -4 -5 0 57.09 3.60 4 5 0 58.59 3.80 4 5 0 61.49 3.60 4 5 0 58.69 3.80 4 5 0 59.49 3.60 -5 -5 0 136.69 7.90 -5 -5 0 128.29 8.40 -5 -5 0 140.49 8.10 5 5 0 137.19 8.20 5 5 0 143.49 8.00 5 5 0 147.09 8.20 5 5 0 147.09 8.00 -6 -5 0 15.70 2.50 -6 -5 0 14.00 1.60 6 5 0 16.90 1.70 6 5 0 16.60 2.10 6 5 0 12.20 1.80 6 5 0 16.60 2.10 -7 -5 0 12.70 2.70 -7 -5 0 10.10 1.40 7 5 0 10.70 1.60 7 5 0 10.10 2.00 -8 -5 0 23.20 3.40 -8 -5 0 20.10 2.10 8 5 0 24.10 2.40 8 5 0 25.70 3.10 -9 -5 0 2.00 2.90 -9 -5 0 1.00 1.50 9 5 0 0.40 2.30 9 5 0 1.80 1.80 -10 -5 0 4.20 1.70 -10 -5 0 2.20 3.40 10 5 0 3.10 2.40 10 5 0 4.70 2.90 -11 -5 0 2.60 4.20 -11 -5 0 2.90 2.00 11 5 0 4.80 4.00 -12 -5 0 6.10 6.00 12 5 0 -0.70 4.80 -10 6 0 2.50 5.80 9 -6 0 2.00 2.10 9 -6 0 0.30 3.80 -9 6 0 2.60 4.20 -9 6 0 0.60 3.60 8 -6 0 11.60 3.60 8 -6 0 11.10 1.90 8 -6 0 10.30 3.60 -8 6 0 6.20 4.10 -8 6 0 9.10 3.10 7 -6 0 0.40 1.30 7 -6 0 2.30 3.10 -7 6 0 1.70 3.20 -7 6 0 0.40 2.40 6 -6 0 0.10 1.10 6 -6 0 0.80 2.60 -6 6 0 1.90 2.60 -6 6 0 1.10 2.00 5 -6 0 247.18 14.00 5 -6 0 265.47 14.70 -5 6 0 251.47 14.90 -5 6 0 251.77 14.70 4 -6 0 31.70 3.20 4 -6 0 35.60 2.40 -4 6 0 36.70 3.40 -4 6 0 31.50 3.10 3 -6 0 10.90 1.10 3 -6 0 14.20 2.00 -3 6 0 14.30 1.90 -3 6 0 13.50 1.90 2 -6 0 32.40 2.10 2 -6 0 24.30 2.50 2 -6 0 26.90 1.90 -2 6 0 24.80 2.50 -2 6 0 29.60 2.50 -2 6 0 31.60 2.50 1 -6 0 163.38 9.70 1 -6 0 171.38 9.40 1 -6 0 172.88 9.40 -1 6 0 151.98 9.70 -1 6 0 165.88 9.20 -1 6 0 181.98 9.50 -1 6 0 172.38 9.20 -1 6 0 161.78 9.70 0 -6 0 10.60 1.00 0 6 0 7.80 1.40 0 6 0 11.10 0.90 0 6 0 10.00 0.90 0 6 0 12.50 1.60 -1 -6 0 388.46 21.00 1 6 0 396.76 21.20 1 6 0 376.96 20.90 1 6 0 369.76 21.20 -2 -6 0 676.43 35.70 -2 -6 0 677.13 35.80 -2 -6 0 642.84 35.90 2 6 0 670.93 36.10 2 6 0 663.03 35.80 2 6 0 650.13 36.10 2 6 0 620.54 35.90 -3 -6 0 70.59 4.20 -3 -6 0 72.09 4.20 -3 -6 0 70.99 4.30 3 6 0 61.49 4.40 3 6 0 82.19 4.30 3 6 0 66.39 4.40 3 6 0 67.79 4.20 -4 -6 0 92.29 5.40 -4 -6 0 90.39 5.60 -4 -6 0 94.19 5.40 4 6 0 91.19 5.40 4 6 0 95.19 5.70 4 6 0 93.39 5.40 4 6 0 87.59 5.60 -5 -6 0 124.39 7.70 -5 -6 0 120.79 7.20 -5 -6 0 122.69 7.30 5 6 0 126.79 7.50 5 6 0 123.59 7.50 5 6 0 129.59 7.30 5 6 0 135.59 7.40 -6 -6 0 65.39 4.20 -6 -6 0 65.39 4.90 6 6 0 63.49 4.60 6 6 0 71.39 4.30 6 6 0 72.79 4.70 6 6 0 60.29 4.30 -7 -6 0 197.98 12.00 -7 -6 0 202.58 11.20 7 6 0 197.98 11.30 7 6 0 187.18 11.60 -8 -6 0 61.59 5.60 -8 -6 0 67.89 4.30 8 6 0 56.09 5.20 8 6 0 65.09 4.70 -9 -6 0 6.00 3.00 -9 -6 0 5.80 1.80 9 6 0 9.10 2.70 -10 -6 0 29.40 4.90 -10 -6 0 19.00 2.50 10 6 0 16.30 3.80 -11 -6 0 4.80 2.20 -11 -6 0 4.80 4.40 11 6 0 1.40 3.70 -12 -6 0 8.40 6.10 9 -7 0 15.00 4.30 9 -7 0 12.00 2.50 -9 7 0 8.10 4.30 -9 7 0 13.30 4.90 8 -7 0 -0.20 3.30 8 -7 0 1.40 1.80 8 -7 0 -1.70 3.90 -8 7 0 -0.10 3.60 -8 7 0 -1.20 3.10 7 -7 0 12.10 1.80 7 -7 0 12.40 3.40 -7 7 0 10.90 3.10 -7 7 0 10.90 3.40 6 -7 0 42.70 4.30 6 -7 0 32.90 2.80 -6 7 0 28.60 3.90 -6 7 0 33.90 3.70 5 -7 0 0.80 2.10 5 -7 0 1.30 1.10 -5 7 0 1.50 2.30 -5 7 0 0.70 1.90 4 -7 0 432.46 23.50 4 -7 0 408.76 22.80 -4 7 0 422.76 23.40 -4 7 0 403.06 23.40 3 -7 0 0.20 0.80 3 -7 0 2.00 1.70 -3 7 0 2.40 1.70 -3 7 0 0.00 1.50 2 -7 0 23.50 2.40 2 -7 0 19.50 1.70 -2 7 0 19.40 2.30 -2 7 0 21.50 2.20 -2 7 0 26.50 2.60 1 -7 0 371.26 21.00 1 -7 0 364.66 20.60 -1 7 0 390.26 20.70 -1 7 0 375.26 20.40 -1 7 0 368.76 21.00 -1 7 0 368.66 21.00 -1 7 0 383.76 20.40 0 -7 0 8.10 1.00 0 -7 0 6.00 1.50 0 7 0 5.30 1.40 0 7 0 7.40 0.80 0 7 0 9.60 1.50 0 7 0 7.80 0.80 -1 -7 0 179.78 9.50 1 7 0 168.78 9.40 1 7 0 163.98 9.40 1 7 0 175.08 9.80 1 7 0 157.08 9.80 -2 -7 0 121.19 6.60 -2 -7 0 115.49 6.50 2 7 0 108.29 6.80 2 7 0 112.69 6.80 2 7 0 109.79 6.40 -3 -7 0 -0.30 0.90 -3 -7 0 -0.40 0.90 -3 -7 0 -0.10 0.90 3 7 0 0.30 0.90 3 7 0 0.20 0.90 3 7 0 0.40 1.40 3 7 0 0.70 1.20 -4 -7 0 155.98 9.30 -4 -7 0 176.28 9.60 -4 -7 0 162.48 9.40 4 7 0 172.68 9.70 4 7 0 154.88 9.40 4 7 0 176.48 9.40 4 7 0 157.88 9.60 -5 -7 0 91.09 5.80 -5 -7 0 100.09 6.10 -5 -7 0 96.19 5.70 5 7 0 92.69 5.70 5 7 0 93.59 6.10 5 7 0 104.79 6.10 5 7 0 89.49 5.80 -6 -7 0 10.40 2.20 -6 -7 0 12.50 1.60 6 7 0 11.80 2.30 6 7 0 12.20 1.80 6 7 0 12.90 2.20 6 7 0 10.60 1.90 -7 -7 0 983.70 51.19 -7 -7 0 930.41 51.79 7 7 0 896.41 51.59 -8 -7 0 109.69 6.20 -8 -7 0 101.09 7.40 8 7 0 91.69 6.90 -9 -7 0 339.17 19.80 -9 -7 0 328.97 18.60 9 7 0 329.27 19.30 -10 -7 0 9.50 2.30 -10 -7 0 17.00 4.20 10 7 0 16.50 3.60 -11 -7 0 0.70 4.80 -11 -7 0 1.10 2.30 11 7 0 4.10 4.30 8 -8 0 95.69 8.00 8 -8 0 90.99 6.20 8 -8 0 96.79 7.70 -8 8 0 92.29 7.70 7 -8 0 21.40 2.40 7 -8 0 26.40 4.30 -7 8 0 17.90 3.60 6 -8 0 14.30 1.80 6 -8 0 16.10 3.60 -6 8 0 10.60 2.90 5 -8 0 2.80 1.20 5 -8 0 4.40 2.60 -5 8 0 3.10 2.20 4 -8 0 52.29 4.40 4 -8 0 46.60 3.30 -4 8 0 54.49 4.30 3 -8 0 27.40 3.10 3 -8 0 30.10 2.20 -3 8 0 26.30 2.90 2 -8 0 2.90 1.70 2 -8 0 3.20 0.90 -2 8 0 2.30 1.80 -2 8 0 2.90 1.80 1 -8 0 26.00 2.80 -1 8 0 29.60 1.80 -1 8 0 30.20 2.80 -1 8 0 27.20 2.90 -1 8 0 30.10 1.80 0 -8 0 359.06 19.80 0 -8 0 343.77 19.40 0 8 0 345.07 19.30 0 8 0 340.67 19.80 0 8 0 367.56 19.30 0 8 0 357.26 19.80 -1 -8 0 221.78 12.70 1 8 0 222.98 12.50 1 8 0 228.08 13.10 1 8 0 239.98 13.10 -2 -8 0 122.59 6.90 2 8 0 118.89 7.30 2 8 0 119.69 7.30 2 8 0 116.99 6.80 -3 -8 0 0.00 1.10 -3 -8 0 0.30 1.10 3 8 0 0.10 1.50 3 8 0 0.20 1.30 3 8 0 -0.40 0.90 -4 -8 0 17.90 1.90 -4 -8 0 20.90 1.80 4 8 0 19.80 1.90 4 8 0 16.40 2.20 4 8 0 15.70 2.20 -5 -8 0 25.20 2.50 -5 -8 0 29.10 2.40 5 8 0 31.30 2.60 5 8 0 29.50 2.90 5 8 0 31.90 3.00 -6 -8 0 94.19 5.80 6 8 0 91.79 6.20 6 8 0 105.39 6.30 6 8 0 85.39 5.80 -7 -8 0 13.70 2.00 -7 -8 0 12.70 2.80 7 8 0 13.50 2.40 7 8 0 11.20 2.50 -8 -8 0 3.50 1.70 -8 -8 0 0.90 2.60 8 8 0 0.40 2.40 -9 -8 0 9.30 2.20 -9 -8 0 6.50 3.80 9 8 0 8.00 3.00 -10 -8 0 130.79 7.70 10 8 0 111.09 9.00 -11 -8 0 29.90 3.30 11 8 0 16.30 5.10 8 -9 0 2.20 4.00 8 -9 0 2.90 2.20 8 -9 0 3.60 5.10 -8 9 0 0.30 4.00 7 -9 0 -0.80 4.10 7 -9 0 1.30 1.90 -7 9 0 1.40 3.30 6 -9 0 28.40 2.60 6 -9 0 32.50 4.30 -6 9 0 28.80 4.00 5 -9 0 29.60 3.90 5 -9 0 26.20 2.30 -5 9 0 24.50 3.40 4 -9 0 70.79 5.30 4 -9 0 61.19 4.10 -4 9 0 58.19 5.00 3 -9 0 0.20 1.00 3 -9 0 -0.20 2.00 -3 9 0 -0.90 2.10 2 -9 0 10.50 2.40 2 -9 0 13.20 1.50 -2 9 0 16.50 2.40 -2 9 0 16.30 2.60 1 -9 0 1.10 1.70 1 -9 0 1.00 1.00 -1 9 0 3.20 2.00 -1 9 0 1.80 0.50 -1 9 0 1.90 0.50 -1 9 0 2.50 1.80 0 -9 0 69.89 4.90 0 -9 0 74.09 4.30 0 9 0 66.59 4.00 0 9 0 64.09 4.90 0 9 0 70.99 4.90 -1 -9 0 153.38 8.80 1 9 0 173.88 9.40 1 9 0 156.78 8.70 1 9 0 137.39 9.20 -2 -9 0 0.20 1.00 2 9 0 0.70 1.60 2 9 0 0.50 0.90 2 9 0 0.00 1.50 -3 -9 0 131.29 7.70 3 9 0 128.49 7.60 3 9 0 125.49 8.10 3 9 0 145.69 8.10 -4 -9 0 7.50 1.50 4 9 0 9.30 2.10 4 9 0 8.00 1.40 4 9 0 9.60 2.00 -5 -9 0 3.40 1.50 5 9 0 3.90 1.60 5 9 0 4.00 1.90 5 9 0 5.00 2.10 -6 -9 0 2.70 1.70 6 9 0 3.30 2.10 6 9 0 2.50 1.60 6 9 0 1.40 2.30 -7 -9 0 8.60 2.00 7 9 0 4.70 2.00 7 9 0 4.20 2.40 -8 -9 0 34.30 3.10 8 9 0 27.20 4.00 -9 -9 0 22.50 2.70 9 9 0 19.50 3.60 -10 -9 0 15.60 2.80 10 9 0 15.80 4.00 -11 -9 0 3.20 2.70 11 9 0 1.90 4.30 7 -10 0 -0.10 4.90 7 -10 0 2.70 2.20 -7 10 0 4.00 3.70 6 -10 0 3.90 3.60 6 -10 0 3.30 1.80 -6 10 0 4.30 3.10 5 -10 0 0.20 3.00 5 -10 0 1.10 1.40 -5 10 0 0.20 2.60 4 -10 0 2.20 3.00 4 -10 0 4.20 1.40 -4 10 0 0.10 2.40 3 -10 0 57.49 3.70 3 -10 0 52.99 4.80 -3 10 0 47.00 4.80 2 -10 0 1.50 1.10 2 -10 0 -0.80 2.00 -2 10 0 0.30 2.30 -2 10 0 2.30 2.00 1 -10 0 26.60 3.10 1 -10 0 31.60 2.30 -1 10 0 24.80 1.60 -1 10 0 26.30 1.60 -1 10 0 27.50 3.30 -1 10 0 20.20 3.10 0 -10 0 12.50 1.60 0 -10 0 14.40 2.50 0 10 0 22.70 2.90 0 10 0 11.70 2.50 0 10 0 15.80 1.30 -1 -10 0 301.07 16.90 -1 -10 0 303.57 16.40 1 10 0 287.67 16.90 1 10 0 286.67 16.20 1 10 0 292.07 16.90 -2 -10 0 10.70 1.60 2 10 0 10.90 1.30 2 10 0 10.40 2.00 2 10 0 11.40 2.30 -3 -10 0 25.90 2.30 3 10 0 23.90 2.10 3 10 0 25.60 2.90 3 10 0 20.90 2.90 -4 -10 0 74.09 4.90 4 10 0 69.79 5.50 4 10 0 76.69 4.80 4 10 0 81.99 5.60 -5 -10 0 49.99 3.90 5 10 0 41.70 4.10 5 10 0 51.89 3.60 5 10 0 47.50 4.40 6 10 0 7.30 2.00 6 10 0 7.80 2.70 7 10 0 3.40 2.00 7 10 0 3.10 2.50 8 10 0 8.30 3.00 -9 -10 0 78.99 5.60 9 10 0 67.89 6.40 -10 -10 0 7.30 2.80 10 10 0 2.00 3.90 -11 -10 0 14.20 3.40 11 10 0 24.40 5.20 7 -11 0 12.30 5.20 6 -11 0 -1.80 2.00 6 -11 0 1.70 4.00 -6 11 0 -2.40 3.30 5 -11 0 2.30 1.70 5 -11 0 2.20 3.50 -5 11 0 3.20 3.10 4 -11 0 39.80 4.50 4 -11 0 34.30 3.10 -4 11 0 27.40 3.90 3 -11 0 42.30 3.20 3 -11 0 31.90 4.10 -3 11 0 36.90 4.10 2 -11 0 93.49 5.60 2 -11 0 96.89 6.70 -2 11 0 81.99 6.40 -2 11 0 87.99 6.60 1 -11 0 154.38 9.30 1 -11 0 149.49 8.50 -1 11 0 130.79 9.20 -1 11 0 144.09 9.20 0 -11 0 8.90 1.50 0 -11 0 9.20 2.50 0 11 0 6.70 2.60 0 11 0 5.50 0.90 0 11 0 8.50 2.50 -1 -11 0 288.07 16.00 -1 -11 0 290.07 16.60 1 11 0 292.97 16.60 1 11 0 280.57 16.50 1 11 0 275.37 15.70 -2 -11 0 28.40 2.60 2 11 0 31.70 2.30 2 11 0 26.40 3.30 2 11 0 24.40 3.20 -3 -11 0 49.50 3.80 3 11 0 46.60 4.30 3 11 0 56.09 4.40 3 11 0 47.60 3.40 -4 -11 0 66.09 4.80 4 11 0 68.19 4.60 4 11 0 69.89 5.50 4 11 0 75.39 5.60 -5 -11 0 0.80 1.80 5 11 0 0.40 2.20 5 11 0 0.10 2.60 5 11 0 -2.30 1.60 6 11 0 -1.00 1.80 6 11 0 -1.70 2.70 7 11 0 119.49 8.40 7 11 0 129.69 7.90 8 11 0 4.30 3.00 8 11 0 7.30 2.80 9 11 0 60.69 6.10 10 11 0 8.00 4.30 6 -12 0 12.30 5.00 6 -12 0 5.10 3.60 -6 12 0 8.80 5.30 5 -12 0 53.39 5.90 5 -12 0 39.00 3.40 -5 12 0 31.50 4.90 4 -12 0 22.10 2.40 4 -12 0 15.20 3.90 -4 12 0 18.20 3.80 3 -12 0 2.70 3.00 3 -12 0 0.70 1.70 -3 12 0 1.00 2.80 2 -12 0 102.69 7.60 2 -12 0 104.39 6.50 -2 12 0 106.79 7.40 1 -12 0 11.80 3.00 1 -12 0 8.30 1.70 -1 12 0 2.80 2.90 -1 12 0 8.40 3.00 0 -12 0 43.90 4.50 0 12 0 38.90 2.60 0 12 0 43.00 4.50 0 12 0 49.90 4.40 -1 -12 0 67.79 5.60 -1 -12 0 74.89 4.90 1 12 0 68.39 5.70 1 12 0 74.59 4.40 1 12 0 70.99 5.60 -2 -12 0 14.60 3.10 -2 -12 0 15.60 2.10 2 12 0 14.10 1.60 2 12 0 15.50 2.90 2 12 0 13.00 2.80 -3 -12 0 48.50 3.90 3 12 0 48.50 3.40 3 12 0 45.00 4.50 3 12 0 48.80 4.60 -4 -12 0 0.90 1.90 4 12 0 2.60 2.50 4 12 0 4.40 2.90 4 12 0 2.40 1.60 -5 -12 0 61.79 5.20 5 12 0 70.59 4.80 5 12 0 65.59 5.60 5 12 0 78.39 6.10 6 12 0 3.70 2.80 6 12 0 1.30 2.00 7 12 0 2.70 2.30 7 12 0 2.00 2.90 8 12 0 1.30 2.70 8 12 0 0.40 3.30 9 12 0 1.40 4.40 10 12 0 -0.60 4.50 5 -13 0 12.50 3.00 5 -13 0 6.60 4.90 -5 13 0 9.60 4.80 4 -13 0 13.00 4.40 4 -13 0 8.50 2.30 -4 13 0 12.40 3.90 3 -13 0 3.60 1.90 3 -13 0 5.80 3.50 -3 13 0 1.40 3.60 2 -13 0 -1.10 1.80 2 -13 0 -0.40 3.20 -2 13 0 0.40 2.90 1 -13 0 12.10 3.60 1 -13 0 21.80 2.30 -1 13 0 20.90 3.80 -1 13 0 14.20 3.70 0 -13 0 5.80 1.80 0 -13 0 7.30 3.00 0 13 0 4.30 3.10 0 13 0 5.60 2.80 0 13 0 4.60 0.70 -1 -13 0 210.38 12.20 -1 -13 0 231.98 13.30 1 13 0 214.28 13.00 1 13 0 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5.20 5 14 -3 28.10 3.50 4 14 -3 20.20 4.30 4 14 -3 29.10 3.10 3 14 -3 35.10 5.30 3 14 -3 61.59 4.30 3 14 -3 43.00 8.00 -3 -14 3 57.79 4.80 -3 -14 3 48.80 5.40 2 14 -3 11.00 4.20 2 14 -3 5.90 1.90 2 14 -3 6.80 3.90 -2 -14 3 16.00 3.20 -2 -14 3 8.50 3.70 1 14 -3 5.10 4.20 1 14 -3 7.20 1.70 -1 -14 3 3.30 3.80 -1 -14 3 9.30 2.60 0 14 -3 77.69 7.50 0 14 -3 91.89 5.50 0 -14 3 87.49 7.80 0 -14 3 110.69 6.80 -1 14 -3 0.40 3.70 1 -14 3 0.60 2.50 1 -14 3 -0.80 3.90 -2 14 -3 42.70 5.70 2 -14 3 63.19 7.00 2 -14 3 50.79 4.60 8 13 -3 15.90 5.00 7 13 -3 3.00 3.20 7 13 -3 4.60 4.00 6 13 -3 1.40 2.60 6 13 -3 1.80 3.60 5 13 -3 44.90 4.00 5 13 -3 47.20 5.70 4 13 -3 27.10 4.30 4 13 -3 26.40 2.90 3 13 -3 1.90 3.00 3 13 -3 2.30 1.80 3 13 -3 1.70 3.70 -3 -13 3 -1.60 3.30 -3 -13 3 -1.00 2.20 2 13 -3 4.60 3.70 2 13 -3 3.80 3.10 2 13 -3 4.60 1.80 -2 -13 3 2.80 2.30 -2 -13 3 6.40 3.50 1 13 -3 11.00 3.80 1 13 -3 12.10 3.60 1 13 -3 7.60 1.60 -1 -13 3 8.10 3.30 -1 -13 3 8.40 2.40 0 13 -3 9.50 1.60 0 13 -3 13.70 3.70 0 -13 3 12.60 2.50 0 -13 3 17.30 3.70 -1 13 -3 11.30 1.40 -1 13 -3 12.40 3.60 1 -13 3 14.90 2.60 1 -13 3 19.10 4.00 -2 13 -3 1.40 3.40 2 -13 3 2.00 2.30 2 -13 3 0.30 3.60 -3 13 -3 15.60 4.70 3 -13 3 19.80 3.00 3 -13 3 15.70 4.70 -4 13 -3 16.30 4.60 4 -13 3 12.50 5.00 4 -13 3 19.40 3.10 9 12 -3 -1.90 4.90 8 12 -3 5.40 4.10 7 12 -3 11.90 3.10 7 12 -3 7.00 3.80 6 12 -3 22.30 3.10 6 12 -3 19.60 3.80 5 12 -3 11.90 2.40 5 12 -3 8.30 3.20 4 12 -3 8.00 2.00 4 12 -3 10.60 3.20 3 12 -3 37.50 4.50 3 12 -3 37.40 3.20 3 12 -3 43.00 4.70 -3 -12 3 44.30 4.60 2 12 -3 99.79 7.30 2 12 -3 94.69 7.30 2 12 -3 104.29 6.20 -2 -12 3 105.09 7.50 -2 -12 3 99.09 6.70 1 12 -3 382.86 22.40 1 12 -3 388.86 22.40 1 12 -3 390.96 21.40 -1 -12 3 389.56 22.40 -1 -12 3 383.46 21.80 0 12 -3 8.80 1.50 0 12 -3 8.00 3.20 0 -12 3 14.40 3.60 0 -12 3 8.50 2.20 -1 12 -3 7.80 3.10 -1 12 -3 9.10 1.30 1 -12 3 8.00 2.10 1 -12 3 6.30 3.20 -2 12 -3 10.40 3.20 -2 12 -3 6.50 0.90 2 -12 3 5.40 2.10 2 -12 3 6.10 3.80 -3 12 -3 12.20 4.00 3 -12 3 7.50 2.30 3 -12 3 12.90 4.00 -4 12 -3 1.80 3.50 4 -12 3 -0.70 3.90 4 -12 3 -0.60 2.20 -5 12 -3 12.50 4.40 5 -12 3 17.00 5.10 5 -12 3 20.90 3.10 9 11 -3 110.49 8.80 8 11 -3 16.20 4.10 7 11 -3 18.50 4.10 7 11 -3 16.10 3.40 6 11 -3 38.10 3.40 6 11 -3 32.80 4.30 5 11 -3 2.90 2.60 5 11 -3 1.60 2.00 4 11 -3 206.28 11.90 4 11 -3 202.58 12.60 -4 -11 3 210.68 13.00 3 11 -3 43.50 4.60 3 11 -3 54.99 4.60 3 11 -3 46.20 3.60 -3 -11 3 43.10 3.90 -3 -11 3 52.69 4.40 2 11 -3 34.40 3.80 2 11 -3 30.60 2.60 2 11 -3 24.60 3.50 -2 -11 3 35.60 3.70 -2 -11 3 32.00 3.10 1 11 -3 5.90 2.70 1 11 -3 9.30 1.60 1 11 -3 7.60 3.00 -1 -11 3 13.40 2.20 -1 -11 3 9.40 3.00 0 11 -3 16.10 1.70 0 11 -3 13.00 3.10 0 11 -3 16.80 3.10 0 -11 3 15.40 2.20 0 -11 3 13.10 3.00 -1 11 -3 28.00 3.50 -1 11 -3 24.30 2.00 1 -11 3 23.40 2.50 1 -11 3 19.50 3.40 -2 11 -3 2.20 2.60 -2 11 -3 7.10 1.00 2 -11 3 5.80 1.80 2 -11 3 3.00 2.90 -3 11 -3 30.80 4.10 3 -11 3 42.50 3.70 3 -11 3 41.40 4.80 -4 11 -3 28.60 4.30 4 -11 3 28.70 4.50 4 -11 3 25.70 2.80 -5 11 -3 17.70 4.50 5 -11 3 10.30 4.20 5 -11 3 11.20 2.50 -6 11 -3 7.80 4.50 6 -11 3 14.00 5.00 6 -11 3 13.10 2.80 10 10 -3 4.80 4.50 -10 -10 3 4.10 3.10 9 10 -3 161.18 11.60 -9 -10 3 170.18 10.20 8 10 -3 61.09 5.90 -8 -10 3 57.09 4.70 7 10 -3 28.50 3.90 6 10 -3 10.10 2.30 6 10 -3 12.30 3.00 5 10 -3 1.10 2.00 5 10 -3 1.40 2.40 4 10 -3 282.67 17.20 4 10 -3 300.77 16.80 4 10 -3 314.37 17.50 -4 -10 3 299.17 17.00 -4 -10 3 305.67 17.20 3 10 -3 141.89 9.70 3 10 -3 172.68 9.70 3 10 -3 153.08 9.00 -3 -10 3 152.08 9.20 -3 -10 3 157.78 9.60 2 10 -3 18.80 2.10 2 10 -3 27.70 3.40 2 10 -3 20.40 3.00 -2 -10 3 31.10 3.40 1 10 -3 499.55 26.80 1 10 -3 493.15 27.50 1 10 -3 491.85 27.40 -1 -10 3 480.85 27.40 -1 -10 3 470.55 26.90 0 10 -3 0.00 2.30 0 10 -3 1.40 2.10 0 10 -3 -0.30 1.00 0 -10 3 0.40 1.50 0 -10 3 -0.30 2.10 -1 10 -3 8.30 2.50 -1 10 -3 8.40 1.20 1 -10 3 12.70 1.90 1 -10 3 11.30 2.70 -2 10 -3 35.80 3.80 -2 10 -3 32.10 2.20 2 -10 3 26.90 2.70 2 -10 3 37.30 4.00 -3 10 -3 19.70 3.30 -3 10 -3 23.50 1.60 3 -10 3 19.00 3.50 3 -10 3 22.00 2.40 -4 10 -3 148.69 9.40 4 -10 3 146.69 9.80 4 -10 3 132.29 8.50 -5 10 -3 24.00 3.90 5 -10 3 17.60 4.10 5 -10 3 14.40 2.40 -6 10 -3 27.90 4.70 6 -10 3 20.40 4.70 6 -10 3 23.90 3.00 -7 10 -3 1.30 4.40 7 -10 3 1.20 4.80 7 -10 3 -2.20 2.60 10 9 -3 48.40 5.90 -10 -9 3 53.89 4.50 9 9 -3 9.70 3.70 -9 -9 3 9.30 2.50 8 9 -3 1.20 3.00 -8 -9 3 4.80 2.00 7 9 -3 1.60 2.70 -7 -9 3 3.60 2.10 6 9 -3 31.00 3.00 6 9 -3 24.60 3.40 -6 -9 3 30.10 2.90 5 9 -3 65.99 4.20 5 9 -3 51.39 4.70 4 9 -3 1.90 2.10 4 9 -3 1.80 1.50 4 9 -3 1.70 2.10 -4 -9 3 2.40 1.70 3 9 -3 77.99 4.60 3 9 -3 64.79 5.10 3 9 -3 66.09 5.10 -3 -9 3 72.69 4.80 -3 -9 3 69.19 5.00 2 9 -3 12.30 2.40 2 9 -3 10.40 1.50 2 9 -3 14.40 2.40 -2 -9 3 13.50 1.80 -2 -9 3 14.80 2.30 1 9 -3 5.90 2.10 1 9 -3 9.50 2.20 1 9 -3 6.80 1.30 -1 -9 3 5.90 2.00 -1 -9 3 8.90 1.60 0 9 -3 87.59 5.60 0 9 -3 81.59 5.60 0 9 -3 79.89 4.70 0 -9 3 75.99 5.50 0 -9 3 69.49 4.90 -1 9 -3 133.99 7.40 -1 9 -3 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1.00 4.50 -7 11 3 4.10 4.10 6 -11 -3 0.30 3.70 6 -11 -3 -1.00 1.70 -6 11 3 -0.20 3.30 5 -11 -3 13.40 1.80 5 -11 -3 15.20 3.70 -5 11 3 11.30 3.60 4 -11 -3 -0.20 2.70 4 -11 -3 0.50 1.20 -4 11 3 0.80 2.40 3 -11 -3 130.69 7.30 3 -11 -3 126.29 8.40 -3 11 3 110.39 8.10 -3 11 3 133.29 8.70 2 -11 -3 49.60 4.40 2 -11 -3 45.80 3.10 -2 11 3 47.50 4.50 -2 11 3 38.20 4.00 1 -11 -3 191.18 10.80 1 -11 -3 202.08 11.60 -1 11 3 181.28 11.30 -1 11 3 191.08 11.60 0 -11 -3 9.60 1.40 0 11 3 13.10 2.30 0 11 3 11.50 2.50 -1 -11 -3 120.49 6.90 1 11 3 119.69 6.50 1 11 3 104.09 7.60 1 11 3 121.29 7.50 -2 -11 -3 10.50 1.50 2 11 3 12.20 2.20 2 11 3 10.20 2.50 2 11 3 7.60 1.00 -3 -11 -3 86.59 5.10 3 11 3 85.89 5.80 3 11 3 73.79 5.60 3 11 3 76.99 4.80 -4 -11 -3 12.90 1.80 4 11 3 12.00 1.60 4 11 3 14.70 2.70 4 11 3 13.70 2.60 -5 -11 -3 111.59 6.80 5 11 3 106.69 7.50 5 11 3 104.89 6.60 5 11 3 118.09 7.30 -6 -11 -3 134.09 8.20 6 11 3 129.49 7.80 6 11 3 127.09 8.50 6 11 3 137.19 8.40 7 11 3 6.80 2.80 7 11 3 7.70 2.10 7 11 3 9.20 2.90 8 11 3 72.09 5.40 8 11 3 67.59 6.10 9 11 3 -0.80 3.10 10 11 3 3.70 4.40 6 -12 -3 86.09 7.90 6 -12 -3 85.69 5.60 -6 12 3 67.29 7.30 5 -12 -3 -0.10 1.60 5 -12 -3 2.00 3.70 -5 12 3 -0.40 3.10 4 -12 -3 39.40 5.20 4 -12 -3 48.20 3.40 -4 12 3 38.90 4.60 3 -12 -3 3.90 1.40 3 -12 -3 4.90 2.90 -3 12 3 6.50 3.00 -3 12 3 6.30 3.10 2 -12 -3 0.30 1.20 2 -12 -3 -1.30 2.60 -2 12 3 -1.10 2.70 -2 12 3 1.50 2.40 1 -12 -3 -0.90 1.20 1 -12 -3 0.80 2.40 -1 12 3 0.30 2.20 -1 12 3 0.60 2.60 0 -12 -3 104.09 7.30 0 -12 -3 103.99 6.30 0 12 3 106.29 7.10 0 12 3 109.79 7.50 -1 -12 -3 105.09 6.30 1 12 3 109.69 7.20 1 12 3 96.09 6.90 -2 -12 -3 261.37 14.80 2 12 3 253.97 15.30 2 12 3 269.07 14.50 2 12 3 261.87 15.50 -3 -12 -3 33.00 2.80 3 12 3 32.00 3.90 3 12 3 29.20 3.30 3 12 3 28.80 2.40 -4 -12 -3 134.89 8.10 4 12 3 129.69 8.50 4 12 3 132.89 7.90 4 12 3 146.39 8.80 -5 -12 -3 0.00 1.80 5 12 3 1.20 2.50 5 12 3 -1.50 2.50 5 12 3 1.30 1.50 -6 -12 -3 -0.70 2.10 6 12 3 1.70 2.70 6 12 3 -0.10 2.60 6 12 3 0.00 1.70 7 12 3 13.90 2.40 7 12 3 8.20 2.90 7 12 3 12.00 3.60 8 12 3 0.80 2.90 8 12 3 -1.20 2.10 9 12 3 0.80 3.70 9 12 3 1.70 2.80 5 -13 -3 2.30 2.00 5 -13 -3 2.40 4.50 -5 13 3 2.60 4.20 4 -13 -3 -0.60 1.60 4 -13 -3 0.30 3.50 -4 13 3 1.90 3.30 3 -13 -3 0.50 1.50 3 -13 -3 -1.20 3.20 -3 13 3 0.80 3.30 -3 13 3 -0.90 2.90 2 -13 -3 23.10 2.20 2 -13 -3 18.70 3.80 -2 13 3 21.80 3.90 -2 13 3 19.70 3.50 1 -13 -3 26.30 3.90 1 -13 -3 30.60 2.70 -1 13 3 30.80 3.70 -1 13 3 24.10 4.00 0 -13 -3 113.69 6.50 0 -13 -3 109.39 7.60 0 13 3 91.59 7.40 0 13 3 105.19 7.50 -1 -13 -3 28.30 2.60 1 13 3 33.00 3.60 1 13 3 27.90 3.80 -2 -13 -3 1.20 1.60 2 13 3 2.50 2.70 2 13 3 2.50 0.90 2 13 3 3.90 2.40 -3 -13 -3 10.00 2.00 3 13 3 13.00 3.00 3 13 3 11.70 1.40 3 13 3 18.00 3.30 -4 -13 -3 25.20 2.80 4 13 3 28.40 3.50 4 13 3 27.20 2.30 4 13 3 26.30 4.00 -5 -13 -3 36.20 3.40 5 13 3 37.50 4.20 5 13 3 34.50 4.40 5 13 3 33.50 2.90 -6 -13 -3 4.10 2.30 6 13 3 7.40 2.00 6 13 3 9.80 2.90 6 13 3 8.50 3.30 7 13 3 0.70 3.00 7 13 3 3.00 4.30 7 13 3 3.40 2.20 8 13 3 0.20 2.60 8 13 3 1.50 3.60 9 13 3 0.60 2.90 4 -14 -3 27.00 5.70 4 -14 -3 26.30 2.90 -4 14 3 25.20 5.10 3 -14 -3 3.90 1.90 3 -14 -3 2.50 4.00 -3 14 3 1.10 3.40 2 -14 -3 120.09 7.30 2 -14 -3 137.79 9.30 -2 14 3 116.59 9.30 -2 14 3 109.69 8.40 1 -14 -3 51.69 3.70 1 -14 -3 55.49 5.40 -1 14 3 36.60 4.60 -1 14 3 40.00 5.10 0 -14 -3 8.00 3.30 0 -14 -3 4.80 1.70 0 14 3 4.10 3.20 0 14 3 2.00 3.20 -1 -14 -3 106.89 8.10 -1 -14 -3 110.79 7.10 1 14 3 119.69 8.00 1 14 3 130.39 8.30 -2 -14 -3 12.40 2.10 2 14 3 12.00 1.10 2 14 3 12.30 3.30 2 14 3 10.30 3.10 -3 -14 -3 12.10 2.20 3 14 3 12.30 3.10 3 14 3 10.20 3.60 3 14 3 10.90 1.50 -4 -14 -3 13.80 2.40 4 14 3 12.10 3.50 4 14 3 14.20 1.80 4 14 3 20.90 3.70 -5 -14 -3 147.39 9.00 5 14 3 150.78 9.80 5 14 3 152.18 9.80 5 14 3 133.99 8.50 -6 -14 -3 -1.80 2.50 6 14 3 0.70 3.30 6 14 3 0.10 3.70 6 14 3 -0.40 2.00 7 14 3 47.00 5.40 7 14 3 56.59 4.50 8 14 3 15.30 3.10 9 14 3 1.90 3.30 3 -15 -3 10.30 2.40 3 -15 -3 15.40 4.90 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16 3 0.70 3.80 -3 -16 -3 1.30 2.50 3 16 3 2.00 3.90 3 16 3 1.20 4.00 3 16 3 1.00 1.10 -4 -16 -3 76.79 5.90 4 16 3 65.59 4.70 4 16 3 76.59 6.70 4 16 3 78.39 7.80 -5 -16 -3 24.50 3.60 5 16 3 15.40 2.30 5 16 3 14.90 4.90 5 16 3 18.90 4.70 6 16 3 10.60 2.60 6 16 3 17.20 5.40 7 16 3 0.50 2.70 0 17 3 25.10 5.60 -1 -17 -3 17.60 5.10 1 17 3 17.00 4.60 1 17 3 7.00 5.20 -2 -17 -3 6.00 2.90 -2 -17 -3 0.70 4.50 2 17 3 -1.10 4.70 2 17 3 3.60 4.60 -3 -17 -3 5.00 3.00 -3 -17 -3 8.60 4.60 3 17 3 8.10 4.40 3 17 3 5.10 4.60 -4 -17 -3 -0.90 3.00 4 17 3 -0.90 1.60 4 17 3 -0.50 4.50 4 17 3 -2.30 4.60 -5 -17 -3 -0.30 3.50 5 17 3 1.00 2.00 5 17 3 -1.40 5.40 4 15 -4 4.80 4.60 4 15 -4 0.10 3.20 3 15 -4 5.00 4.50 3 15 -4 4.80 2.60 2 15 -4 10.30 4.60 2 15 -4 7.10 2.20 -2 -15 4 7.20 5.10 1 15 -4 0.50 1.90 1 15 -4 5.60 4.70 -1 -15 4 5.40 5.20 -1 -15 4 3.90 3.50 0 15 -4 0.50 1.60 0 -15 4 -0.10 4.80 0 -15 4 2.50 3.50 6 14 -4 81.99 6.20 6 14 -4 53.49 7.30 5 14 -4 15.10 3.20 5 14 -4 15.90 5.20 4 14 -4 1.70 2.50 4 14 -4 1.50 4.10 3 14 -4 94.69 8.60 3 14 -4 121.79 7.20 2 14 -4 41.40 3.50 2 14 -4 36.70 5.30 -2 -14 4 49.60 4.50 -2 -14 4 45.50 5.40 1 14 -4 165.68 12.20 1 14 -4 182.88 10.70 -1 -14 4 194.88 12.70 -1 -14 4 192.28 11.30 0 14 -4 16.00 4.30 0 14 -4 12.90 1.90 0 -14 4 22.30 3.50 0 -14 4 16.10 4.60 -1 14 -4 10.80 1.50 -1 14 -4 8.10 4.20 1 -14 4 11.90 4.70 1 -14 4 15.20 3.20 -2 14 -4 4.90 4.70 2 -14 4 2.60 5.30 2 -14 4 12.30 3.20 7 13 -4 -0.30 3.40 7 13 -4 1.40 4.00 6 13 -4 -2.00 3.70 6 13 -4 -0.20 2.80 5 13 -4 0.90 3.70 5 13 -4 10.00 2.70 4 13 -4 5.00 2.40 4 13 -4 6.80 4.00 3 13 -4 82.39 7.30 3 13 -4 95.39 6.00 2 13 -4 -1.00 1.80 2 13 -4 -1.60 3.70 2 13 -4 1.10 3.60 -2 -13 4 0.50 3.50 -2 -13 4 1.60 2.60 1 13 -4 44.10 3.70 1 13 -4 47.50 5.30 -1 -13 4 55.89 5.60 -1 -13 4 48.70 4.40 0 13 -4 4.60 3.50 0 13 -4 3.70 1.60 0 -13 4 12.10 4.10 0 -13 4 5.40 2.50 -1 13 -4 39.40 3.00 -1 13 -4 44.10 5.10 1 -13 4 49.20 5.50 1 -13 4 43.90 4.10 -2 13 -4 68.29 4.00 -2 13 -4 63.99 6.60 2 -13 4 83.09 7.80 2 -13 4 74.59 5.90 -3 13 -4 23.00 4.90 3 -13 4 22.00 5.10 3 -13 4 32.40 3.60 8 12 -4 18.20 5.30 7 12 -4 2.50 3.90 6 12 -4 9.00 3.60 6 12 -4 8.70 2.90 5 12 -4 23.40 4.10 5 12 -4 25.30 3.00 4 12 -4 30.90 4.30 4 12 -4 29.10 3.00 3 12 -4 4.40 3.10 3 12 -4 7.20 2.00 -3 -12 4 8.00 2.40 -3 -12 4 6.50 3.30 2 12 -4 16.10 3.50 2 12 -4 28.30 2.60 2 12 -4 25.70 4.20 -2 -12 4 29.30 4.10 -2 -12 4 24.80 3.10 1 12 -4 6.40 3.00 1 12 -4 4.10 1.50 -1 -12 4 6.40 3.40 -1 -12 4 2.80 2.20 0 12 -4 -1.90 2.90 0 12 -4 0.60 1.40 0 -12 4 1.40 2.20 0 -12 4 -0.80 2.90 -1 12 -4 24.60 4.00 -1 12 -4 23.40 2.10 1 -12 4 23.40 3.00 1 -12 4 30.80 4.20 -2 12 -4 4.30 3.20 -2 12 -4 4.40 1.10 2 -12 4 6.90 3.60 2 -12 4 2.70 2.20 -3 12 -4 20.20 4.00 3 -12 4 19.70 2.90 3 -12 4 20.40 4.50 -4 12 -4 3.50 3.80 4 -12 4 2.20 4.20 4 -12 4 1.10 2.50 5 -12 4 0.90 3.30 9 11 -4 17.80 5.30 -9 -11 4 14.20 5.70 8 11 -4 28.00 4.70 7 11 -4 13.50 3.90 6 11 -4 66.09 5.10 6 11 -4 47.20 5.30 5 11 -4 23.60 3.70 5 11 -4 28.80 3.10 4 11 -4 4.50 2.80 4 11 -4 2.10 1.90 3 11 -4 78.19 6.70 3 11 -4 103.59 6.90 3 11 -4 86.19 5.80 -3 -11 4 85.19 6.00 -3 -11 4 97.39 6.40 2 11 -4 1.00 1.60 2 11 -4 -0.20 2.40 2 11 -4 3.90 3.00 -2 -11 4 2.60 1.90 -2 -11 4 0.70 2.70 1 11 -4 -0.10 2.40 1 11 -4 -0.10 1.40 1 11 -4 1.10 2.70 -1 -11 4 -1.10 2.40 -1 -11 4 0.40 1.80 0 11 -4 18.20 2.00 0 11 -4 17.90 3.40 0 -11 4 24.00 2.70 0 -11 4 23.60 3.50 -1 11 -4 66.09 5.80 -1 11 -4 74.29 4.50 1 -11 4 76.29 5.20 1 -11 4 71.69 6.00 -2 11 -4 20.10 3.50 -2 11 -4 19.40 1.70 2 -11 4 28.90 2.80 2 -11 4 16.50 3.60 -3 11 -4 3.00 0.80 -3 11 -4 2.50 2.80 3 -11 4 0.60 2.00 3 -11 4 2.10 3.30 -4 11 -4 14.70 3.70 4 -11 4 18.90 4.30 4 -11 4 16.30 2.60 -5 11 -4 6.40 3.90 5 -11 4 7.60 4.50 5 -11 4 2.60 2.50 6 -11 4 54.09 6.20 -10 -10 4 50.99 4.80 9 10 -4 34.30 5.20 -9 -10 4 41.00 4.00 8 10 -4 49.60 5.50 -8 -10 4 58.79 4.50 7 10 -4 23.70 3.90 6 10 -4 31.90 3.30 6 10 -4 25.70 3.80 5 10 -4 9.40 2.90 5 10 -4 8.00 2.30 4 10 -4 13.10 2.80 4 10 -4 12.70 2.20 3 10 -4 4.30 2.50 3 10 -4 2.40 1.70 3 10 -4 1.70 2.60 -3 -10 4 4.30 2.40 2 10 -4 1.00 2.50 2 10 -4 1.00 2.30 2 10 -4 1.40 1.50 -2 -10 4 -0.20 1.70 -2 -10 4 4.40 2.40 1 10 -4 177.68 11.20 1 10 -4 193.08 10.40 1 10 -4 168.78 11.20 -1 -10 4 185.18 11.20 -1 -10 4 185.28 10.70 0 10 -4 129.09 8.80 0 10 -4 146.89 8.00 0 -10 4 129.29 8.20 0 -10 4 142.99 8.80 -1 10 -4 32.70 2.50 -1 10 -4 28.40 3.70 1 -10 4 31.20 2.90 1 -10 4 28.30 3.60 -2 10 -4 26.00 2.10 -2 10 -4 22.50 3.40 2 -10 4 30.60 2.80 2 -10 4 27.70 3.70 -3 10 -4 8.70 1.10 -3 10 -4 12.40 3.00 3 -10 4 11.80 3.30 3 -10 4 7.20 2.00 -4 10 -4 11.20 3.20 4 -10 4 4.20 1.90 4 -10 4 2.10 3.20 -5 10 -4 42.00 4.90 5 -10 4 49.60 5.40 5 -10 4 37.40 3.70 -6 10 -4 15.60 4.10 6 -10 4 14.50 2.80 6 -10 4 15.50 4.80 10 9 -4 -0.60 4.60 -10 -9 4 -0.20 2.70 9 9 -4 1.90 4.10 -9 -9 4 1.00 2.40 8 9 -4 17.00 3.80 -8 -9 4 13.70 2.50 7 9 -4 46.40 5.10 -7 -9 4 51.69 4.00 6 9 -4 2.90 2.60 6 9 -4 0.50 2.10 -6 -9 4 1.40 1.80 5 9 -4 1.00 2.30 5 9 -4 2.70 1.90 4 9 -4 2.20 2.20 4 9 -4 1.90 1.60 3 9 -4 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1.60 5 8 -4 4.40 2.10 5 8 -4 4.20 1.70 -5 -8 4 4.20 1.70 4 8 -4 5.60 1.80 4 8 -4 6.60 2.20 -4 -8 4 8.90 1.80 3 8 -4 3.00 1.30 3 8 -4 3.70 1.90 3 8 -4 5.90 1.90 -3 -8 4 7.20 1.90 -3 -8 4 5.30 1.50 2 8 -4 -0.10 1.80 2 8 -4 -0.30 1.60 2 8 -4 -0.40 1.20 -2 -8 4 0.70 1.70 -2 -8 4 0.60 1.40 1 8 -4 33.10 2.50 1 8 -4 28.10 3.10 1 8 -4 34.10 3.20 -1 -8 4 29.90 2.90 -1 -8 4 30.30 2.60 0 8 -4 -0.60 1.70 0 8 -4 -0.40 1.00 0 -8 4 0.50 1.70 0 -8 4 0.90 1.20 -1 8 -4 4.10 1.10 -1 8 -4 3.30 1.90 1 -8 4 4.70 2.20 1 -8 4 4.80 1.40 -2 8 -4 15.60 1.40 -2 8 -4 12.90 2.40 2 -8 4 15.70 1.90 2 -8 4 10.90 2.50 -3 8 -4 58.59 3.60 -3 8 -4 59.89 4.70 3 -8 4 59.29 4.90 3 -8 4 56.29 4.00 -4 8 -4 0.60 2.30 -4 8 -4 0.80 0.80 4 -8 4 -0.30 2.50 4 -8 4 -0.70 1.40 -5 8 -4 2.30 0.70 -5 8 -4 2.90 2.60 5 -8 4 4.40 2.90 5 -8 4 2.00 1.70 -6 8 -4 18.50 3.50 6 -8 4 20.30 2.60 6 -8 4 29.20 4.60 -7 8 -4 1.20 3.30 7 -8 4 2.60 2.20 7 -8 4 0.90 3.80 -8 8 -4 11.70 4.90 8 -8 4 12.40 2.80 8 -8 4 19.50 5.20 10 7 -4 -1.80 3.50 -10 -7 4 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15.10 2.50 -6 9 -5 9.90 3.80 6 -9 5 10.30 2.60 6 -9 5 7.70 4.20 -7 9 -5 5.70 4.60 7 -9 5 3.00 4.60 7 -9 5 0.70 2.70 10 8 -5 0.10 4.00 -10 -8 5 1.10 2.60 9 8 -5 12.10 4.00 -9 -8 5 8.80 2.50 8 8 -5 -0.50 3.00 -8 -8 5 0.30 1.90 7 8 -5 127.29 8.80 -7 -8 5 133.59 8.00 6 8 -5 21.50 3.20 -6 -8 5 12.30 2.20 5 8 -5 108.09 6.70 5 8 -5 100.09 7.20 -5 -8 5 114.19 6.70 4 8 -5 95.49 6.60 4 8 -5 100.49 6.00 -4 -8 5 93.19 6.00 3 8 -5 30.60 3.40 3 8 -5 34.40 2.80 3 8 -5 32.60 3.20 -3 -8 5 34.50 3.00 -3 -8 5 31.50 3.20 2 8 -5 276.17 16.80 2 8 -5 317.87 16.50 2 8 -5 291.47 17.00 -2 -8 5 301.57 16.60 -2 -8 5 294.07 16.80 1 8 -5 90.99 6.10 1 8 -5 81.29 5.40 -1 -8 5 94.29 6.00 -1 -8 5 88.19 5.60 0 8 -5 183.68 11.60 0 8 -5 197.78 10.90 0 -8 5 191.18 11.10 0 -8 5 200.08 11.50 -1 8 -5 29.70 3.30 -1 8 -5 29.60 2.30 1 -8 5 26.60 3.10 1 -8 5 22.50 2.30 -2 8 -5 20.70 1.80 -2 8 -5 22.30 3.00 2 -8 5 24.30 2.30 2 -8 5 20.60 3.00 -3 8 -5 18.50 1.70 -3 8 -5 11.10 2.80 3 -8 5 25.60 3.40 3 -8 5 22.90 2.20 -4 8 -5 21.40 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3.60 1 -7 5 63.49 3.90 1 -7 5 55.99 4.50 -2 7 -5 2.50 1.00 -2 7 -5 4.10 1.90 2 -7 5 1.50 2.20 2 -7 5 2.10 1.30 -3 7 -5 28.50 3.20 -3 7 -5 27.80 2.20 3 -7 5 33.90 2.80 3 -7 5 33.70 3.50 -4 7 -5 148.39 8.40 -4 7 -5 156.68 9.40 4 -7 5 146.29 8.80 4 -7 5 152.08 9.60 -5 7 -5 0.00 2.30 -5 7 -5 1.40 0.90 5 -7 5 0.40 2.60 5 -7 5 -0.50 1.60 -6 7 -5 1.50 2.60 -6 7 -5 2.30 0.90 6 -7 5 3.80 1.90 6 -7 5 0.50 3.00 -7 7 -5 16.50 3.60 7 -7 5 12.40 2.60 7 -7 5 9.20 3.80 -8 7 -5 1.60 3.80 8 -7 5 4.00 4.70 8 -7 5 0.70 2.40 -11 -6 5 -1.10 5.00 10 6 -5 -2.00 3.70 -10 -6 5 -1.80 2.00 -10 -6 5 0.90 4.00 9 6 -5 19.00 4.10 -9 -6 5 19.30 2.30 -9 -6 5 18.40 4.00 8 6 -5 34.80 4.10 8 6 -5 32.80 3.40 -8 -6 5 45.20 5.00 -8 -6 5 34.10 2.90 7 6 -5 125.79 8.60 7 6 -5 141.49 8.10 -7 -6 5 130.39 7.80 -7 -6 5 128.79 8.90 6 6 -5 94.89 5.80 6 6 -5 89.39 6.10 -6 -6 5 81.49 6.30 -6 -6 5 83.29 5.40 5 6 -5 83.09 4.90 5 6 -5 71.89 5.30 -5 -6 5 67.69 4.60 -5 -6 5 73.99 5.40 4 6 -5 69.79 4.40 4 6 -5 68.59 4.80 4 6 -5 69.99 4.80 4 6 -5 54.99 4.30 -4 -6 5 66.79 4.30 -4 -6 5 68.59 4.80 3 6 -5 156.38 8.70 3 6 -5 150.98 8.70 3 6 -5 142.69 8.70 3 6 -5 153.28 8.80 3 6 -5 144.19 9.00 -3 -6 5 153.48 8.60 -3 -6 5 152.98 8.90 -3 -6 5 151.58 8.70 -3 -6 5 141.19 8.70 2 6 -5 3.60 1.60 2 6 -5 4.70 1.40 2 6 -5 3.70 1.30 2 6 -5 3.50 1.50 2 6 -5 3.80 1.20 -2 -6 5 3.90 1.30 -2 -6 5 3.30 1.40 -2 -6 5 3.60 1.30 1 6 -5 0.70 1.50 1 6 -5 -0.20 1.10 1 6 -5 -0.60 0.90 -1 -6 5 -0.40 1.10 -1 -6 5 0.00 1.00 -1 -6 5 0.00 1.40 0 6 -5 0.40 1.00 0 6 -5 -0.30 1.10 0 6 -5 0.30 1.40 0 -6 5 0.40 1.10 0 -6 5 0.60 1.10 0 -6 5 0.10 1.30 -1 6 -5 1.90 1.30 -1 6 -5 1.70 1.60 -1 6 -5 -0.10 0.90 1 -6 5 0.00 1.40 1 -6 5 1.50 1.10 -2 6 -5 69.09 4.10 -2 6 -5 70.29 4.80 -2 6 -5 70.09 4.70 2 -6 5 73.49 4.40 2 -6 5 57.69 4.70 -3 6 -5 4.10 1.90 -3 6 -5 6.80 1.00 -3 6 -5 2.90 1.80 3 -6 5 6.10 1.40 3 -6 5 5.00 2.00 -4 6 -5 62.39 4.60 -4 6 -5 60.49 4.80 -4 6 -5 58.19 3.60 4 -6 5 57.09 3.90 4 -6 5 49.70 4.60 -5 6 -5 7.00 1.10 -5 6 -5 8.90 2.80 -5 6 -5 5.50 2.30 5 -6 5 4.30 1.60 5 -6 5 6.50 2.60 -6 6 -5 16.50 3.10 -6 6 -5 21.30 1.90 -6 6 -5 26.60 4.00 6 -6 5 19.40 3.50 6 -6 5 24.10 2.50 -7 6 -5 54.09 5.20 -7 6 -5 47.90 3.10 -7 6 -5 53.39 5.90 7 -6 5 53.69 4.20 7 -6 5 57.59 5.60 -8 6 -5 128.69 9.10 -8 6 -5 114.79 11.70 8 -6 5 123.69 8.00 8 -6 5 128.09 9.40 -9 6 -5 2.20 4.60 9 -6 5 7.80 5.00 9 -6 5 0.40 4.50 9 -6 5 5.40 2.90 -11 -5 5 -0.50 5.70 10 5 -5 -1.50 2.60 10 5 -5 0.00 3.40 -10 -5 5 2.40 1.80 -10 -5 5 0.20 4.40 9 5 -5 7.00 2.50 9 5 -5 5.90 3.10 -9 -5 5 3.10 3.40 -9 -5 5 7.50 1.80 8 5 -5 17.50 3.20 8 5 -5 20.20 2.50 -8 -5 5 22.50 2.20 -8 -5 5 21.80 4.00 7 5 -5 51.89 4.60 7 5 -5 49.80 4.10 -7 -5 5 52.89 3.60 -7 -5 5 53.39 4.80 6 5 -5 71.49 5.20 6 5 -5 72.89 4.90 -6 -5 5 67.39 5.40 -6 -5 5 79.29 4.60 5 5 -5 0.60 1.60 5 5 -5 0.00 1.30 -5 -5 5 0.50 1.10 -5 -5 5 -0.60 1.60 4 5 -5 0.40 1.30 4 5 -5 1.70 1.20 4 5 -5 1.90 1.50 -4 -5 5 0.20 1.50 -4 -5 5 0.80 1.10 3 5 -5 240.48 13.70 3 5 -5 258.47 13.90 3 5 -5 224.48 14.00 3 5 -5 248.18 13.70 3 5 -5 235.18 13.70 -3 -5 5 241.28 13.60 -3 -5 5 258.77 13.80 -3 -5 5 254.17 13.70 -3 -5 5 243.58 13.90 2 5 -5 8.50 1.40 2 5 -5 8.60 1.50 2 5 -5 7.30 1.20 2 5 -5 10.10 1.70 2 5 -5 6.70 1.20 -2 -5 5 8.30 1.20 -2 -5 5 7.00 1.30 -2 -5 5 7.00 1.30 1 5 -5 140.19 7.70 1 5 -5 131.99 7.70 1 5 -5 135.29 7.80 1 5 -5 124.79 8.00 -1 -5 5 135.69 7.70 -1 -5 5 134.09 7.60 -1 -5 5 139.19 7.90 0 5 -5 0.50 1.10 0 5 -5 3.10 1.10 0 5 -5 1.10 0.80 0 5 -5 1.50 1.20 0 -5 5 0.50 1.00 0 -5 5 0.70 1.30 0 -5 5 1.40 1.00 -1 5 -5 15.50 1.50 -1 5 -5 12.60 1.90 -1 5 -5 17.00 2.00 1 -5 5 16.90 1.60 1 -5 5 16.20 2.00 1 -5 5 19.40 1.70 -2 5 -5 210.38 12.50 -2 5 -5 220.98 12.40 -2 5 -5 212.48 12.10 2 -5 5 224.28 12.20 2 -5 5 217.38 12.50 -3 5 -5 1.00 1.50 -3 5 -5 1.10 1.60 -3 5 -5 0.90 0.80 3 -5 5 2.30 1.60 3 -5 5 0.30 1.10 -4 5 -5 34.90 3.30 -4 5 -5 32.70 2.40 -4 5 -5 35.70 3.60 4 -5 5 40.20 3.60 4 -5 5 35.90 2.80 -5 5 -5 -0.80 1.90 -5 5 -5 -0.70 0.90 -5 5 -5 0.60 2.00 5 -5 5 -0.30 2.20 5 -5 5 0.20 1.40 -6 5 -5 0.90 2.80 -6 5 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0.20 1.20 -3 -4 5 1.30 0.90 -3 -4 5 -0.70 1.20 -3 -4 5 -0.70 0.80 -3 -4 5 0.20 1.00 2 4 -5 22.00 1.80 2 4 -5 16.20 2.00 2 4 -5 23.20 2.10 2 4 -5 27.10 2.00 -2 -4 5 21.60 2.10 -2 -4 5 21.10 1.90 -2 -4 5 23.20 1.70 -2 -4 5 23.30 2.00 1 4 -5 196.58 11.10 1 4 -5 187.38 11.30 1 4 -5 201.88 11.10 1 4 -5 202.68 11.30 -1 -4 5 190.88 11.00 -1 -4 5 203.38 11.20 -1 -4 5 208.18 11.10 0 4 -5 388.16 22.30 0 4 -5 415.16 22.40 0 4 -5 419.06 22.60 0 4 -5 392.56 22.60 0 -4 5 417.36 22.60 0 -4 5 419.06 22.40 0 -4 5 403.26 22.40 -1 4 -5 39.70 3.00 -1 4 -5 37.10 2.80 -1 4 -5 42.50 2.70 -1 4 -5 36.70 2.50 1 -4 5 38.50 3.00 1 -4 5 34.80 2.60 1 -4 5 37.60 2.60 -2 4 -5 20.50 2.30 -2 4 -5 22.00 1.80 -2 4 -5 21.80 2.30 2 -4 5 29.60 2.40 2 -4 5 28.80 2.10 2 -4 5 25.30 2.00 -3 4 -5 15.40 1.40 -3 4 -5 14.90 2.00 -3 4 -5 11.90 2.00 3 -4 5 18.80 1.60 3 -4 5 18.50 2.30 -4 4 -5 23.10 2.70 -4 4 -5 30.30 2.00 -4 4 -5 26.20 3.00 4 -4 5 28.50 3.00 4 -4 5 25.70 2.30 -5 4 -5 4.20 1.80 -5 4 -5 2.10 2.20 -5 4 -5 2.00 0.90 5 -4 5 1.50 2.00 5 -4 5 1.40 1.30 -6 4 -5 209.48 12.80 -6 4 -5 208.88 11.70 -6 4 -5 216.68 12.60 6 -4 5 209.68 12.00 6 -4 5 206.98 12.60 -7 4 -5 5.70 3.00 -7 4 -5 4.80 1.10 -7 4 -5 7.30 2.50 7 -4 5 4.10 1.60 7 -4 5 7.90 2.90 -8 4 -5 122.09 7.20 -8 4 -5 129.19 9.60 -8 4 -5 138.79 8.80 8 -4 5 118.19 8.90 8 -4 5 135.49 8.00 -9 4 -5 3.30 4.00 -9 4 -5 1.90 3.40 -9 4 -5 5.20 1.10 9 -4 5 5.80 3.50 9 -4 5 7.80 2.50 9 -4 5 3.30 4.00 -10 4 -5 50.69 7.30 -10 4 -5 52.09 6.80 10 -4 5 61.99 6.80 10 -4 5 61.39 7.60 10 -4 5 69.19 5.60 11 3 -5 1.40 3.00 11 3 -5 0.30 3.90 -11 -3 5 -0.10 4.90 -11 -3 5 -0.60 1.50 10 3 -5 16.90 3.80 10 3 -5 19.90 3.10 -10 -3 5 11.80 4.40 -10 -3 5 16.80 1.90 9 3 -5 2.40 2.10 9 3 -5 1.80 2.70 -9 -3 5 2.90 3.30 -9 -3 5 2.20 1.30 8 3 -5 -0.90 1.70 8 3 -5 1.70 2.30 -8 -3 5 -0.50 3.00 -8 -3 5 0.70 1.20 7 3 -5 23.70 2.90 7 3 -5 18.60 2.20 -7 -3 5 22.30 1.90 -7 -3 5 26.80 3.70 6 3 -5 4.20 1.30 6 3 -5 4.80 1.80 -6 -3 5 5.40 1.10 -6 -3 5 5.80 2.40 5 3 -5 1.90 1.10 5 3 -5 1.80 1.50 -5 -3 5 3.60 0.90 -5 -3 5 2.20 1.70 4 3 -5 271.17 15.90 4 3 -5 294.57 15.60 4 3 -5 283.87 15.60 -4 -3 5 283.57 16.00 -4 -3 5 273.97 15.50 3 3 -5 1108.59 62.29 3 3 -5 1176.98 62.09 3 3 -5 1114.89 62.09 -3 -3 5 1125.19 61.99 -3 -3 5 1147.19 62.39 -3 -3 5 1185.68 61.89 -3 -3 5 1124.29 62.09 2 3 -5 1.40 1.10 2 3 -5 1.60 0.80 2 3 -5 0.70 1.00 2 3 -5 0.90 0.80 -2 -3 5 -0.30 0.60 -2 -3 5 2.40 0.90 -2 -3 5 1.30 0.70 -2 -3 5 1.60 1.10 1 3 -5 767.92 43.30 1 3 -5 807.82 43.30 1 3 -5 788.62 43.50 1 3 -5 817.52 43.50 -1 -3 5 773.32 43.30 -1 -3 5 794.12 43.30 -1 -3 5 817.82 43.30 0 3 -5 0.70 0.70 0 3 -5 0.60 0.90 0 3 -5 0.70 1.00 0 3 -5 -0.10 0.80 0 -3 5 0.50 0.70 0 -3 5 -0.20 0.80 0 -3 5 0.50 0.60 -1 3 -5 28.70 2.20 -1 3 -5 27.30 1.90 -1 3 -5 26.50 2.20 -1 3 -5 27.40 1.90 1 -3 5 21.50 1.80 1 -3 5 24.80 1.90 1 -3 5 25.90 2.10 -2 3 -5 273.67 15.30 -2 3 -5 278.17 15.70 -2 3 -5 294.67 15.60 2 -3 5 286.37 15.40 2 -3 5 277.27 15.40 2 -3 5 262.27 15.60 -3 3 -5 3.40 1.40 -3 3 -5 4.60 1.40 -3 3 -5 4.80 0.90 3 -3 5 4.40 1.00 3 -3 5 4.60 1.40 3 -3 5 5.00 1.20 -4 3 -5 65.39 4.50 -4 3 -5 65.59 4.80 -4 3 -5 69.69 4.00 4 -3 5 68.59 4.20 4 -3 5 68.29 4.70 -5 3 -5 19.60 1.60 -5 3 -5 17.00 2.60 -5 3 -5 16.60 2.40 5 -3 5 17.70 1.90 5 -3 5 19.60 2.60 -6 3 -5 287.97 15.30 -6 3 -5 287.17 15.90 -6 3 -5 270.37 16.20 6 -3 5 267.67 16.10 6 -3 5 266.97 15.50 -7 3 -5 4.70 1.10 -7 3 -5 2.00 2.60 -7 3 -5 4.60 2.60 7 -3 5 4.20 1.70 7 -3 5 5.70 2.70 -8 3 -5 5.80 3.50 -8 3 -5 5.30 1.20 -8 3 -5 5.70 2.70 8 -3 5 8.10 3.10 8 -3 5 4.80 1.90 8 -3 5 8.80 3.20 -9 3 -5 -0.30 1.20 -9 3 -5 0.60 4.10 -9 3 -5 1.70 3.10 9 -3 5 0.10 2.10 9 -3 5 -0.70 4.00 9 -3 5 0.30 3.40 -10 3 -5 33.20 2.50 -10 3 -5 35.40 5.50 -10 3 -5 27.60 5.60 10 -3 5 28.90 3.60 10 -3 5 46.30 5.80 10 -3 5 32.30 5.20 11 2 -5 17.00 3.20 11 2 -5 18.90 4.70 -11 -2 5 13.50 1.50 -11 -2 5 16.00 5.90 10 2 -5 -2.30 3.10 10 2 -5 -0.40 2.10 -10 -2 5 1.50 3.90 -10 -2 5 2.00 1.20 9 2 -5 38.10 4.10 9 2 -5 30.20 3.00 -9 -2 5 38.40 4.70 -9 -2 5 26.40 2.40 8 2 -5 18.70 2.10 8 2 -5 12.10 2.80 -8 -2 5 14.50 1.50 -8 -2 5 15.80 3.40 7 2 -5 19.90 2.00 7 2 -5 26.70 3.10 -7 -2 5 19.90 3.20 -7 -2 5 18.90 1.70 6 2 -5 62.99 4.60 6 2 -5 61.19 4.10 -6 -2 5 65.39 5.10 -6 -2 5 67.39 3.90 5 2 -5 98.19 6.30 5 2 -5 106.29 5.90 -5 -2 5 97.29 5.70 -5 -2 5 100.99 6.70 4 2 -5 26.50 2.40 4 2 -5 27.40 2.00 4 2 -5 32.30 2.30 -4 -2 5 25.40 2.60 -4 -2 5 24.50 1.90 3 2 -5 718.63 40.50 3 2 -5 751.22 40.20 3 2 -5 774.22 40.20 -3 -2 5 721.33 40.20 -3 -2 5 727.83 40.60 2 2 -5 983.20 54.79 2 2 -5 1011.90 54.89 2 2 -5 999.70 54.69 2 2 -5 1028.10 54.59 -2 -2 5 1032.90 54.59 -2 -2 5 1007.00 54.89 -2 -2 5 947.01 54.59 -2 -2 5 1030.80 54.69 1 2 -5 1215.48 65.89 1 2 -5 1162.88 65.69 1 2 -5 1223.88 65.69 1 2 -5 1212.48 65.89 -1 -2 5 1243.48 65.69 -1 -2 5 1204.48 65.69 -1 -2 5 1209.78 65.69 0 2 -5 81.59 4.60 0 2 -5 81.69 4.50 0 2 -5 77.59 4.40 0 2 -5 80.69 4.70 0 -2 5 79.79 4.50 0 -2 5 61.19 4.30 0 -2 5 76.49 4.40 -1 2 -5 3.40 1.10 -1 2 -5 1.00 0.60 -1 2 -5 2.90 0.90 -1 2 -5 5.30 0.80 1 -2 5 4.50 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-0.60 1.80 6 6 -7 -0.30 2.30 -6 -6 7 0.30 1.50 -6 -6 7 1.20 2.90 5 6 -7 21.70 3.10 5 6 -7 29.00 3.50 5 6 -7 26.20 2.70 -5 -6 7 22.80 3.90 -5 -6 7 18.10 2.20 4 6 -7 33.30 3.10 4 6 -7 44.70 3.80 4 6 -7 36.50 3.70 -4 -6 7 36.90 2.90 3 6 -7 140.19 8.60 3 6 -7 128.39 8.10 3 6 -7 144.59 9.90 -3 -6 7 144.09 8.10 2 6 -7 4.40 1.60 2 6 -7 5.60 1.90 -2 -6 7 4.10 1.40 -2 -6 7 8.40 1.70 -2 -6 7 5.20 1.60 1 6 -7 61.99 4.50 1 6 -7 51.79 3.90 -1 -6 7 60.69 4.20 -1 -6 7 62.29 4.10 -1 -6 7 53.29 3.80 0 6 -7 2.10 1.30 0 6 -7 2.00 1.80 0 -6 7 1.70 1.80 0 -6 7 1.90 1.30 -1 6 -7 473.85 26.80 -1 6 -7 495.45 26.30 1 -6 7 471.75 26.70 1 -6 7 473.05 26.40 -2 6 -7 0.60 1.10 -2 6 -7 0.50 1.90 2 -6 7 -1.60 1.90 2 -6 7 -0.90 1.40 -3 6 -7 138.29 7.90 -3 6 -7 136.29 8.80 3 -6 7 136.69 8.20 3 -6 7 138.69 8.80 -4 6 -7 116.49 6.70 -4 6 -7 114.09 7.60 4 -6 7 107.99 7.00 4 -6 7 119.99 8.00 -5 6 -7 155.68 8.80 -5 6 -7 152.08 9.80 5 -6 7 162.28 9.30 5 -6 7 149.59 10.00 -6 6 -7 8.20 1.40 -6 6 -7 10.80 3.00 6 -6 7 5.20 3.10 6 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5 -9 1.90 1.70 3 5 -9 1.90 2.10 -3 -5 9 1.70 1.30 2 5 -9 240.68 14.50 2 5 -9 259.27 14.60 2 5 -9 246.18 14.10 -2 -5 9 248.58 14.00 1 5 -9 1.40 1.90 1 5 -9 1.50 1.90 1 5 -9 0.10 1.40 -1 -5 9 1.20 1.80 -1 -5 9 0.70 1.40 0 5 -9 24.00 3.00 0 5 -9 18.80 2.70 0 5 -9 18.60 2.20 0 -5 9 23.70 2.30 0 -5 9 28.50 2.50 0 -5 9 20.30 2.50 -1 5 -9 52.19 4.20 -1 5 -9 47.60 4.10 -1 5 -9 49.40 3.60 1 -5 9 48.20 4.20 1 -5 9 45.60 3.80 -2 5 -9 3.10 2.10 -2 5 -9 1.20 1.30 -2 5 -9 1.10 2.00 2 -5 9 0.10 2.00 2 -5 9 2.10 1.70 -3 5 -9 75.59 4.80 -3 5 -9 81.49 5.80 -3 5 -9 80.39 5.50 3 -5 9 70.99 5.60 3 -5 9 66.69 5.00 -4 5 -9 28.20 3.30 -4 5 -9 23.50 3.40 -4 5 -9 22.30 2.20 4 -5 9 21.80 3.40 4 -5 9 27.40 2.90 -5 5 -9 49.60 4.70 -5 5 -9 53.89 5.30 -5 5 -9 44.40 3.60 5 -5 9 66.19 5.30 5 -5 9 53.19 4.40 -6 5 -9 177.18 11.20 -6 5 -9 170.18 10.80 -6 5 -9 176.78 9.80 6 -5 9 161.08 11.20 6 -5 9 163.48 10.30 -7 5 -9 13.30 1.90 -7 5 -9 13.00 3.40 7 -5 9 7.80 2.80 7 -5 9 10.80 3.90 -8 5 -9 11.10 4.50 -8 5 -9 19.80 2.20 8 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177.18 10.00 -1 4 -9 156.88 10.30 1 -4 9 192.58 10.00 1 -4 9 171.38 10.30 1 -4 9 177.58 10.10 -2 4 -9 39.70 4.00 -2 4 -9 36.10 3.70 -2 4 -9 46.90 3.30 2 -4 9 54.79 3.90 2 -4 9 53.89 3.60 -3 4 -9 165.28 10.10 -3 4 -9 174.38 9.60 -3 4 -9 172.18 10.30 3 -4 9 160.08 10.20 3 -4 9 166.78 9.80 -4 4 -9 0.10 2.00 -4 4 -9 0.50 2.00 -4 4 -9 0.50 1.30 4 -4 9 1.00 2.20 4 -4 9 0.40 1.60 -5 4 -9 305.67 17.80 -5 4 -9 305.87 17.20 5 -4 9 308.37 17.40 5 -4 9 315.17 18.10 -6 4 -9 12.20 3.60 -6 4 -9 19.60 3.40 -6 4 -9 20.90 2.00 6 -4 9 17.10 2.70 6 -4 9 10.30 3.30 -7 4 -9 75.29 7.10 -7 4 -9 75.39 4.60 -7 4 -9 64.79 6.20 7 -4 9 69.69 6.40 7 -4 9 60.99 5.20 -8 4 -9 36.20 3.10 -8 4 -9 48.10 5.80 -8 4 -9 40.80 4.80 8 -4 9 35.90 5.50 8 -4 9 34.40 4.00 -9 4 -9 27.50 5.30 -9 4 -9 21.30 2.40 -9 4 -9 17.80 5.50 9 -4 9 19.80 5.60 9 -4 9 23.40 3.80 9 -4 9 16.70 5.10 10 3 -9 10.70 7.70 10 3 -9 15.20 3.50 -10 -3 9 14.80 6.30 -10 -3 9 16.00 1.90 9 3 -9 0.00 2.40 9 3 -9 -0.30 3.70 -9 -3 9 0.40 1.40 -9 -3 9 1.50 4.20 8 3 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19.70 2.10 2 -3 9 27.00 2.80 2 -3 9 32.40 2.50 2 -3 9 29.20 2.40 -3 3 -9 11.00 1.60 -3 3 -9 12.80 2.10 -3 3 -9 17.60 2.50 3 -3 9 20.80 2.10 3 -3 9 15.30 2.40 -4 3 -9 2.70 2.10 -4 3 -9 4.00 1.90 -4 3 -9 2.40 1.20 4 -3 9 4.50 1.70 4 -3 9 3.90 2.40 -5 3 -9 98.29 7.30 -5 3 -9 113.79 6.90 -5 3 -9 99.89 6.30 5 -3 9 107.69 6.60 5 -3 9 110.69 7.30 -6 3 -9 93.99 5.90 -6 3 -9 98.89 7.20 -6 3 -9 101.69 6.70 6 -3 9 97.19 7.10 6 -3 9 92.39 6.20 -7 3 -9 5.10 2.70 -7 3 -9 3.10 1.50 -7 3 -9 3.50 3.50 7 -3 9 5.80 3.10 7 -3 9 3.10 2.10 -8 3 -9 19.60 3.70 -8 3 -9 20.70 2.30 -8 3 -9 20.60 4.30 8 -3 9 12.60 2.80 8 -3 9 20.20 4.40 -9 3 -9 3.70 3.80 -9 3 -9 3.80 1.90 -9 3 -9 1.70 5.00 9 -3 9 1.80 3.10 9 -3 9 4.30 3.80 9 -3 9 2.20 4.90 10 2 -9 2.00 2.90 10 2 -9 -0.60 4.20 -10 -2 9 3.70 5.20 9 2 -9 9.20 3.80 9 2 -9 10.40 2.60 -9 -2 9 12.20 1.50 -9 -2 9 12.50 4.60 8 2 -9 63.59 5.60 8 2 -9 55.19 4.50 -8 -2 9 53.49 3.70 -8 -2 9 70.49 6.40 7 2 -9 2.50 1.70 7 2 -9 -0.80 2.40 -7 -2 9 1.20 3.00 -7 -2 9 2.40 1.10 6 2 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1.70 7 17 9 97.09 9.30 -3 -18 -9 1.40 4.10 -4 -18 -9 1.30 2.80 -5 -18 -9 12.30 3.40 3 12 -10 4.80 3.70 2 12 -10 1.90 3.20 1 12 -10 30.60 3.80 5 11 -10 3.80 5.90 4 11 -10 3.10 4.50 3 11 -10 4.80 4.40 3 11 -10 4.70 3.30 2 11 -10 25.20 3.70 2 11 -10 22.20 4.90 1 11 -10 1.00 2.60 1 11 -10 1.70 4.30 0 11 -10 13.40 2.90 0 11 -10 11.70 4.70 -1 11 -10 9.20 2.70 -1 11 -10 7.50 4.50 1 -11 10 13.00 5.30 -2 11 -10 0.70 4.30 -2 11 -10 3.70 2.80 2 -11 10 -1.80 5.30 6 10 -10 35.30 5.60 5 10 -10 7.60 4.90 4 10 -10 1.40 4.00 3 10 -10 1.10 4.20 3 10 -10 5.10 3.00 2 10 -10 4.40 2.70 2 10 -10 3.80 3.50 1 10 -10 1.10 3.50 1 10 -10 1.20 2.40 0 10 -10 -1.60 4.00 0 10 -10 -0.50 2.20 -1 10 -10 101.69 6.80 -1 10 -10 102.79 8.30 1 -10 10 105.69 8.70 -2 10 -10 1.20 2.10 -2 10 -10 3.40 4.30 2 -10 10 2.20 4.60 -3 10 -10 26.20 5.40 -3 10 -10 23.40 2.90 3 -10 10 43.80 6.20 -4 10 -10 0.10 4.50 4 -10 10 1.00 4.80 7 9 -10 82.89 8.10 -7 -9 10 81.79 6.40 6 9 -10 10.50 4.40 -6 -9 10 11.80 3.00 5 9 -10 3.00 3.60 -5 -9 10 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-4 8 -10 26.80 4.40 -4 8 -10 24.90 2.70 4 -8 10 32.40 3.80 4 -8 10 26.40 4.70 -5 8 -10 95.79 6.30 -5 8 -10 91.29 8.40 5 -8 10 96.49 8.50 5 -8 10 114.49 7.50 -6 8 -10 34.50 3.50 -6 8 -10 47.90 5.80 6 -8 10 38.30 6.90 8 7 -10 5.40 4.20 -8 -7 10 8.20 2.50 7 7 -10 25.70 4.60 -7 -7 10 25.20 3.00 6 7 -10 71.19 6.50 -6 -7 10 74.59 5.20 5 7 -10 30.20 4.20 -5 -7 10 27.00 2.90 4 7 -10 0.00 2.70 -4 -7 10 2.50 2.00 3 7 -10 14.80 3.10 -3 -7 10 10.90 2.10 2 7 -10 0.50 2.20 2 7 -10 2.60 2.70 1 7 -10 5.40 2.70 1 7 -10 5.30 2.00 0 7 -10 12.10 2.10 0 7 -10 9.00 2.90 0 -7 10 12.20 3.00 -1 7 -10 -0.40 2.50 -1 7 -10 -0.30 1.80 1 -7 10 -1.70 2.50 -2 7 -10 86.09 5.40 -2 7 -10 74.29 6.60 2 -7 10 79.29 6.30 -3 7 -10 0.60 1.60 -3 7 -10 0.20 2.70 3 -7 10 1.70 2.30 3 -7 10 0.30 2.90 -4 7 -10 7.50 3.10 -4 7 -10 6.30 1.80 4 -7 10 7.00 2.70 4 -7 10 1.70 3.20 -5 7 -10 7.80 2.00 -5 7 -10 8.30 3.50 5 -7 10 5.90 4.20 5 -7 10 7.30 2.80 -6 7 -10 2.20 3.70 -6 7 -10 -0.20 1.70 6 -7 10 -2.60 3.00 6 -7 10 -1.10 4.10 -7 7 -10 3.30 4.30 7 -7 10 7.00 3.80 8 6 -10 10.50 4.70 -8 -6 10 7.60 2.20 7 6 -10 0.30 3.50 -7 -6 10 2.40 1.90 6 6 -10 -0.40 3.00 -6 -6 10 0.60 1.70 5 6 -10 44.80 4.90 -5 -6 10 46.40 3.70 4 6 -10 101.29 7.40 -4 -6 10 107.59 6.40 3 6 -10 42.90 4.50 -3 -6 10 50.49 3.70 2 6 -10 43.30 4.50 2 6 -10 48.20 3.90 -2 -6 10 40.80 3.40 1 6 -10 56.29 4.90 1 6 -10 66.09 4.30 -1 -6 10 54.39 4.10 0 6 -10 78.49 5.80 0 6 -10 72.69 5.10 0 -6 10 75.39 5.70 -1 6 -10 171.28 10.90 -1 6 -10 173.98 10.30 1 -6 10 184.48 10.80 -2 6 -10 5.00 2.60 -2 6 -10 9.10 1.90 2 -6 10 5.30 2.60 2 -6 10 7.70 2.10 -3 6 -10 19.70 3.20 -3 6 -10 21.40 2.30 3 -6 10 20.30 3.50 3 -6 10 21.30 2.80 -4 6 -10 18.00 2.20 -4 6 -10 18.50 3.40 4 -6 10 19.80 3.70 4 -6 10 33.40 3.20 -5 6 -10 24.70 3.80 -5 6 -10 29.20 2.60 5 -6 10 22.70 4.20 5 -6 10 25.30 3.40 -6 6 -10 7.90 1.90 -6 6 -10 6.80 3.70 6 -6 10 8.30 4.00 6 -6 10 6.20 2.90 -7 6 -10 1.40 1.90 -7 6 -10 -1.30 3.60 7 -6 10 -0.40 3.00 7 -6 10 -0.30 4.30 9 5 -10 0.30 4.30 -9 -5 10 -0.20 1.80 8 5 -10 3.00 4.50 8 5 -10 2.60 3.60 -8 -5 10 2.50 1.80 7 5 -10 -1.80 2.40 7 5 -10 -0.20 3.90 7 5 -10 -2.00 3.00 -7 -5 10 -1.30 1.60 -7 -5 10 0.90 3.70 6 5 -10 48.40 5.30 6 5 -10 36.70 3.80 6 5 -10 45.60 4.70 -6 -5 10 41.80 3.30 -6 -5 10 36.10 5.00 5 5 -10 1.60 2.50 5 5 -10 2.10 2.20 5 5 -10 -0.10 3.00 -5 -5 10 -1.30 3.20 -5 -5 10 1.40 1.50 4 5 -10 79.19 5.70 4 5 -10 73.39 5.10 4 5 -10 77.59 6.10 -4 -5 10 65.59 4.80 3 5 -10 1.70 2.50 3 5 -10 -0.40 2.40 -3 -5 10 1.10 1.40 2 5 -10 192.58 11.20 2 5 -10 167.78 11.00 -2 -5 10 183.38 10.40 1 5 -10 26.60 3.30 1 5 -10 21.70 2.50 1 5 -10 25.40 3.30 -1 -5 10 28.40 2.60 0 5 -10 48.30 3.80 0 5 -10 52.49 4.20 0 5 -10 52.39 4.40 0 -5 10 40.20 3.50 0 -5 10 44.00 4.10 -1 5 -10 25.20 2.60 -1 5 -10 31.80 3.50 -1 5 -10 27.70 3.30 1 -5 10 22.90 3.00 -2 5 -10 83.39 5.10 -2 5 -10 75.19 5.90 -2 5 -10 70.29 6.00 2 -5 10 78.59 5.60 2 -5 10 77.29 5.40 -3 5 -10 38.90 4.80 -3 5 -10 36.30 3.10 -3 5 -10 34.90 3.80 3 -5 10 44.40 3.90 3 -5 10 38.40 4.20 -4 5 -10 -0.90 2.30 -4 5 -10 0.20 1.50 4 -5 10 -0.30 1.90 4 -5 10 0.00 2.90 -5 5 -10 10.80 1.90 -5 5 -10 7.40 2.90 5 -5 10 7.70 3.20 5 -5 10 9.60 2.40 -6 5 -10 41.10 3.20 -6 5 -10 41.20 4.70 6 -5 10 27.70 4.60 6 -5 10 31.60 3.60 -7 5 -10 6.00 3.80 -7 5 -10 9.10 2.00 7 -5 10 9.70 2.80 7 -5 10 12.30 4.50 -8 5 -10 0.40 1.90 -8 5 -10 0.10 3.90 8 -5 10 1.20 5.30 8 -5 10 2.70 3.00 9 4 -10 11.70 4.50 9 4 -10 21.50 3.60 -9 -4 10 24.80 6.10 -9 -4 10 16.90 2.20 8 4 -10 14.20 2.80 8 4 -10 18.50 4.40 -8 -4 10 14.50 4.90 -8 -4 10 10.10 1.80 7 4 -10 11.30 3.30 7 4 -10 11.30 2.60 7 4 -10 14.10 3.90 -7 -4 10 10.00 1.70 -7 -4 10 14.10 3.90 6 4 -10 28.80 4.20 6 4 -10 27.10 3.10 6 4 -10 24.00 3.90 -6 -4 10 30.60 2.50 -6 -4 10 34.20 4.40 5 4 -10 211.08 12.70 5 4 -10 220.18 13.00 5 4 -10 221.68 12.20 -5 -4 10 190.18 11.80 -5 -4 10 209.88 13.00 4 4 -10 14.90 3.20 4 4 -10 15.00 2.30 4 4 -10 12.40 2.70 -4 -4 10 14.00 1.70 -4 -4 10 21.20 3.50 3 4 -10 153.18 9.70 3 4 -10 160.18 9.60 3 4 -10 159.68 9.00 -3 -4 10 140.69 8.70 2 4 -10 195.38 11.20 2 4 -10 187.88 11.30 2 4 -10 176.78 10.80 -2 -4 10 191.08 10.60 1 4 -10 246.48 14.80 1 4 -10 251.27 14.30 1 4 -10 261.27 14.40 1 4 -10 249.78 14.60 -1 -4 10 247.68 14.10 -1 -4 10 257.67 14.40 0 4 -10 201.18 11.80 0 4 -10 190.78 11.60 0 4 -10 205.18 11.30 0 -4 10 192.58 11.40 0 -4 10 193.48 11.10 -1 4 -10 123.39 7.40 -1 4 -10 121.99 8.00 -1 4 -10 121.59 7.80 1 -4 10 126.59 7.30 1 -4 10 116.39 8.20 1 -4 10 127.79 7.70 -2 4 -10 295.67 16.70 -2 4 -10 300.37 17.30 -2 4 -10 307.47 17.10 2 -4 10 291.47 17.20 2 -4 10 296.97 16.80 -3 4 -10 13.60 2.60 -3 4 -10 14.00 2.70 -3 4 -10 9.10 1.60 3 -4 10 14.30 2.10 3 -4 10 14.30 2.60 -4 4 -10 2.20 1.50 -4 4 -10 3.50 2.20 -4 4 -10 0.90 2.40 4 -4 10 3.70 2.00 4 -4 10 7.00 2.60 -5 4 -10 0.00 1.50 -5 4 -10 3.30 2.70 -5 4 -10 1.50 2.90 5 -4 10 0.50 2.60 5 -4 10 3.10 2.20 -6 4 -10 6.40 3.60 -6 4 -10 6.90 1.70 -6 4 -10 3.10 2.70 6 -4 10 8.40 2.50 6 -4 10 1.70 3.10 -7 4 -10 24.70 4.60 -7 4 -10 37.10 4.30 -7 4 -10 36.10 2.90 7 -4 10 37.90 3.70 7 -4 10 32.80 4.90 -8 4 -10 5.40 3.60 -8 4 -10 5.40 4.80 -8 4 -10 8.20 2.00 8 -4 10 6.60 3.20 8 -4 10 5.10 4.40 -9 4 -10 36.70 6.60 9 3 -10 23.80 4.80 9 3 -10 23.90 3.60 -9 -3 10 27.30 2.40 -9 -3 10 32.60 5.70 8 3 -10 0.80 3.60 8 3 -10 2.20 2.40 -8 -3 10 3.10 4.30 -8 -3 10 1.30 1.40 7 3 -10 52.39 5.10 7 3 -10 38.50 3.70 -7 -3 10 45.60 3.20 -7 -3 10 46.90 5.60 6 3 -10 5.60 2.70 6 3 -10 4.20 1.80 6 3 -10 1.50 2.90 -6 -3 10 6.10 3.10 -6 -3 10 1.10 1.20 5 3 -10 44.70 4.30 5 3 -10 46.00 3.70 5 3 -10 50.19 4.80 -5 -3 10 43.30 3.20 -5 -3 10 50.09 4.80 4 3 -10 112.79 6.80 4 3 -10 93.89 7.10 4 3 -10 96.49 6.20 -4 -3 10 106.19 7.30 -4 -3 10 95.59 5.90 3 3 -10 17.30 2.50 3 3 -10 15.80 3.00 3 3 -10 15.80 2.00 -3 -3 10 16.30 3.00 -3 -3 10 20.50 1.80 2 3 -10 37.00 3.10 2 3 -10 40.90 3.60 2 3 -10 32.00 3.80 -2 -3 10 38.00 2.80 1 3 -10 4.00 1.40 1 3 -10 2.80 1.50 1 3 -10 1.00 1.60 1 3 -10 3.70 2.10 -1 -3 10 2.10 1.30 -1 -3 10 1.80 1.50 0 3 -10 98.79 6.70 0 3 -10 103.59 6.40 0 3 -10 109.69 6.60 0 3 -10 113.99 7.10 0 -3 10 102.79 6.40 0 -3 10 113.09 6.70 -1 3 -10 322.07 18.50 -1 3 -10 336.77 19.10 -1 3 -10 332.47 18.90 1 -3 10 348.57 18.50 1 -3 10 316.87 18.80 1 -3 10 348.07 18.70 -2 3 -10 -0.70 2.00 -2 3 -10 0.60 1.40 -2 3 -10 -0.20 1.90 2 -3 10 0.40 1.70 2 -3 10 0.00 1.40 2 -3 10 0.60 1.60 -3 3 -10 6.40 1.50 -3 3 -10 4.80 2.30 -3 3 -10 8.40 2.00 3 -3 10 5.60 1.80 3 -3 10 8.40 2.30 -4 3 -10 26.40 3.50 -4 3 -10 37.20 2.80 -4 3 -10 35.50 3.40 4 -3 10 34.20 2.90 4 -3 10 24.20 3.40 -5 3 -10 26.60 2.60 -5 3 -10 28.90 3.30 -5 3 -10 31.10 3.80 5 -3 10 33.50 3.90 5 -3 10 31.80 3.00 -6 3 -10 30.40 3.60 -6 3 -10 29.20 2.60 -6 3 -10 26.60 4.00 6 -3 10 33.60 3.30 6 -3 10 24.50 3.90 -7 3 -10 4.30 1.70 -7 3 -10 4.10 2.80 -7 3 -10 5.60 3.70 7 -3 10 4.40 3.40 7 -3 10 5.60 2.20 -8 3 -10 22.00 2.70 -8 3 -10 32.90 4.30 -8 3 -10 29.70 5.40 8 -3 10 33.70 3.80 8 -3 10 27.40 4.80 -9 3 -10 -2.10 4.70 -9 3 -10 -0.30 1.90 9 -3 10 -1.30 4.60 -10 -2 10 -1.50 8.70 9 2 -10 2.60 3.90 9 2 -10 0.90 2.60 -9 -2 10 2.50 1.20 -9 -2 10 0.70 4.50 8 2 -10 7.90 3.30 8 2 -10 12.80 2.50 -8 -2 10 10.00 1.50 -8 -2 10 8.20 4.00 7 2 -10 51.89 4.90 7 2 -10 47.80 3.90 -7 -2 10 55.99 6.10 -7 -2 10 41.20 3.10 6 2 -10 0.90 1.50 6 2 -10 2.60 2.40 -6 -2 10 0.50 1.10 -6 -2 10 1.70 3.20 5 2 -10 3.40 2.20 5 2 -10 5.60 2.60 5 2 -10 3.00 1.60 -5 -2 10 6.00 2.70 -5 -2 10 3.00 1.10 4 2 -10 33.50 3.30 4 2 -10 28.00 2.70 4 2 -10 31.60 3.70 -4 -2 10 34.10 2.40 -4 -2 10 33.50 3.90 3 2 -10 37.60 3.60 3 2 -10 30.60 3.10 3 2 -10 31.80 2.80 -3 -2 10 29.40 2.40 -3 -2 10 30.70 3.60 2 2 -10 116.49 7.40 2 2 -10 109.99 7.20 2 2 -10 117.69 6.90 -2 -2 10 116.09 6.70 1 2 -10 8.70 2.20 1 2 -10 10.60 1.70 1 2 -10 7.90 1.50 1 2 -10 6.20 1.90 -1 -2 10 5.40 1.10 -1 -2 10 9.70 1.60 0 2 -10 98.09 6.00 0 2 -10 89.39 5.40 0 2 -10 86.89 5.40 0 2 -10 86.69 5.60 0 -2 10 80.99 5.10 0 -2 10 79.49 5.40 -1 2 -10 -0.10 1.60 -1 2 -10 1.40 1.70 -1 2 -10 0.30 1.30 -1 2 -10 0.00 1.30 1 -2 10 -0.40 1.20 1 -2 10 0.30 1.60 1 -2 10 -0.40 1.10 -2 2 -10 1.60 1.30 -2 2 -10 1.80 1.70 -2 2 -10 3.40 2.00 2 -2 10 2.80 1.50 2 -2 10 1.50 1.30 2 -2 10 1.20 1.60 -3 2 -10 127.99 8.40 -3 2 -10 139.19 8.10 -3 2 -10 130.69 7.80 3 -2 10 132.79 8.40 3 -2 10 137.09 7.90 3 -2 10 131.69 7.90 -4 2 -10 33.20 2.60 -4 2 -10 28.30 3.00 -4 2 -10 28.20 3.40 4 -2 10 33.60 3.60 4 -2 10 31.70 2.80 -5 2 -10 13.20 1.80 -5 2 -10 13.00 2.50 -5 2 -10 9.70 2.70 5 -2 10 12.20 2.80 5 -2 10 13.00 2.20 -6 2 -10 9.90 3.00 -6 2 -10 13.30 2.60 -6 2 -10 10.40 1.80 6 -2 10 15.90 3.30 6 -2 10 13.50 2.40 -7 2 -10 8.50 1.80 -7 2 -10 13.30 3.50 -7 2 -10 14.40 3.20 7 -2 10 8.00 2.40 7 -2 10 10.90 3.30 -8 2 -10 0.00 3.50 -8 2 -10 -1.20 3.40 -8 2 -10 -0.50 1.70 8 -2 10 -0.30 3.50 8 -2 10 -0.30 2.60 -9 2 -10 3.20 2.00 -9 2 -10 -0.10 4.30 9 -2 10 0.90 4.30 -10 2 -10 3.70 6.10 9 1 -10 0.50 2.30 9 1 -10 3.00 3.70 -9 -1 10 -0.60 4.30 8 1 -10 0.10 1.90 8 1 -10 -0.10 3.00 -8 -1 10 1.30 4.00 -8 -1 10 0.20 0.90 7 1 -10 20.40 3.30 7 1 -10 17.00 2.30 -7 -1 10 14.80 3.70 -7 -1 10 12.80 1.40 6 1 -10 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-10 49.90 3.80 5 11 10 36.40 4.50 5 11 10 53.69 3.40 -6 -11 -10 125.49 7.80 6 11 10 123.59 8.70 6 11 10 126.79 7.40 -7 -11 -10 5.40 2.10 7 11 10 4.50 1.70 7 11 10 2.90 3.00 8 11 10 15.60 4.20 8 11 10 14.20 2.50 9 11 10 0.70 3.80 9 11 10 1.40 2.50 10 11 10 2.20 4.40 10 11 10 -2.80 3.00 11 11 10 1.30 6.10 6 -12 -10 28.20 8.40 -6 12 10 21.30 4.90 -5 12 10 3.70 3.70 -4 12 10 112.79 8.60 3 -12 -10 0.70 0.70 3 -12 -10 1.70 3.30 -3 12 10 0.40 3.40 2 -12 -10 1.40 0.80 -2 12 10 1.00 2.70 1 -12 -10 13.70 1.30 -1 12 10 9.10 3.40 0 -12 -10 -0.40 0.90 0 12 10 1.70 2.50 -1 -12 -10 10.30 1.40 1 12 10 9.00 2.90 -2 -12 -10 13.60 1.60 2 12 10 17.50 3.10 -3 -12 -10 18.10 2.00 3 12 10 26.70 3.70 -4 -12 -10 43.20 3.50 4 12 10 48.20 2.90 4 12 10 37.00 4.30 -5 -12 -10 1.10 1.60 5 12 10 -0.60 2.70 5 12 10 1.10 1.20 -6 -12 -10 23.60 2.80 6 12 10 20.80 2.20 6 12 10 15.60 3.90 -7 -12 -10 60.29 5.00 7 12 10 54.69 4.30 7 12 10 55.99 5.80 8 12 10 -0.20 3.50 8 12 10 -0.90 2.10 9 12 10 22.30 5.30 10 12 10 20.90 5.40 4 -13 -10 1.80 3.80 4 -13 -10 -0.10 0.90 -4 13 10 -0.10 3.80 3 -13 -10 23.90 4.20 3 -13 -10 24.60 1.90 -3 13 10 26.30 4.40 2 -13 -10 15.80 3.60 2 -13 -10 17.40 1.50 -2 13 10 12.90 3.40 1 -13 -10 49.40 3.30 -1 13 10 52.29 5.20 0 -13 -10 219.98 12.40 0 13 10 222.98 13.50 -1 -13 -10 36.60 2.80 1 13 10 34.90 4.20 -2 -13 -10 12.30 1.70 2 13 10 9.30 3.20 -3 -13 -10 1.50 1.40 3 13 10 1.10 2.70 -4 -13 -10 156.88 9.60 4 13 10 168.18 10.50 4 13 10 163.58 9.00 -5 -13 -10 27.50 3.00 5 13 10 34.30 2.60 5 13 10 33.80 4.20 -6 -13 -10 203.48 12.10 6 13 10 202.48 11.70 6 13 10 213.58 13.00 -7 -13 -10 16.30 2.90 7 13 10 14.00 3.80 7 13 10 19.70 2.40 8 13 10 32.10 3.40 8 13 10 41.00 5.60 9 13 10 12.60 2.90 9 13 10 5.80 5.00 10 13 10 3.10 5.10 10 13 10 1.20 3.30 4 -14 -10 9.70 4.50 4 -14 -10 5.40 1.20 -4 14 10 6.90 4.60 3 -14 -10 -0.10 4.30 -3 14 10 1.70 4.60 2 -14 -10 5.50 1.30 2 -14 -10 7.00 3.60 -2 14 10 5.60 3.70 1 -14 -10 59.59 3.80 -1 14 10 45.60 5.40 0 -14 -10 0.60 1.30 0 14 10 1.30 3.20 -1 -14 -10 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21.50 3.50 9 15 10 23.70 5.90 2 -16 -10 66.09 4.70 2 -16 -10 70.39 7.40 -2 16 10 64.49 7.30 1 -16 -10 -0.30 1.70 1 -16 -10 2.00 4.80 -1 16 10 -1.40 4.60 0 -16 -10 176.78 10.00 0 16 10 159.88 11.70 -1 -16 -10 52.79 4.10 1 16 10 46.80 5.90 -2 -16 -10 20.70 2.60 2 16 10 21.40 4.50 -3 -16 -10 45.10 4.00 3 16 10 38.00 5.30 -4 -16 -10 6.20 2.30 4 16 10 3.10 3.90 -5 -16 -10 1.90 2.40 5 16 10 0.90 0.90 5 16 10 -0.80 4.00 -6 -16 -10 0.80 2.70 6 16 10 0.60 1.60 6 16 10 -1.20 4.20 -7 -16 -10 -0.10 3.10 7 16 10 0.70 2.10 7 16 10 0.40 4.60 8 16 10 58.29 7.10 0 -17 -10 -0.70 2.00 0 17 10 1.40 4.50 -1 -17 -10 3.40 2.20 1 17 10 3.40 4.50 -2 -17 -10 37.80 3.50 2 17 10 35.40 5.80 -3 -17 -10 18.80 2.90 3 17 10 19.50 5.00 -4 -17 -10 3.40 2.60 4 17 10 3.00 4.50 -5 -17 -10 0.70 2.60 5 17 10 -1.10 5.20 -6 -17 -10 5.80 3.20 6 17 10 8.10 1.70 6 17 10 7.50 5.10 -7 -17 -10 0.80 3.50 7 17 10 0.90 5.20 -4 -18 -10 12.70 3.90 -5 -18 -10 6.00 3.70 3 11 -11 20.60 5.20 3 11 -11 37.50 4.50 2 11 -11 2.40 4.50 2 11 -11 6.50 3.30 1 11 -11 1.40 3.00 1 11 -11 9.70 5.40 0 11 -11 0.30 2.90 0 11 -11 1.90 4.80 -1 11 -11 2.90 5.10 5 10 -11 107.79 9.20 4 10 -11 13.10 5.40 3 10 -11 97.99 8.50 3 10 -11 103.59 8.40 2 10 -11 -0.20 3.10 2 10 -11 3.80 4.00 1 10 -11 4.10 2.90 1 10 -11 2.40 3.90 0 10 -11 31.90 3.80 0 10 -11 47.50 6.10 -1 10 -11 0.20 2.50 -1 10 -11 1.00 4.20 -2 10 -11 3.20 4.30 -2 10 -11 0.30 2.30 2 -10 11 0.90 5.00 -3 10 -11 -0.10 4.30 3 -10 11 0.60 4.90 6 9 -11 122.39 9.70 -6 -9 11 115.09 8.00 5 9 -11 3.60 3.90 -5 -9 11 0.20 2.70 4 9 -11 3.60 3.80 3 9 -11 23.80 4.60 2 9 -11 -1.00 3.40 2 9 -11 4.00 2.80 1 9 -11 3.10 2.50 1 9 -11 -0.60 3.40 0 9 -11 11.70 2.60 0 9 -11 17.90 4.10 -1 9 -11 17.20 2.80 -1 9 -11 18.40 4.20 1 -9 11 16.40 4.10 -2 9 -11 1.00 3.60 -2 9 -11 2.80 2.20 2 -9 11 3.60 3.90 -3 9 -11 4.30 2.20 -3 9 -11 -0.30 3.90 3 -9 11 2.40 4.20 -4 9 -11 4.60 4.90 -4 9 -11 1.50 2.30 4 -9 11 11.40 4.90 7 8 -11 14.50 5.40 -7 -8 11 14.30 3.00 6 8 -11 53.69 6.30 -6 -8 11 63.09 5.00 5 8 -11 11.80 4.10 -5 -8 11 6.50 2.50 4 8 -11 25.50 4.30 -4 -8 11 26.80 3.00 3 8 -11 41.80 5.30 2 8 -11 8.80 3.80 2 8 -11 13.90 2.90 1 8 -11 6.10 2.40 1 8 -11 6.30 3.50 0 8 -11 6.10 2.40 0 8 -11 3.90 3.10 -1 8 -11 -0.10 2.10 -1 8 -11 -0.50 3.40 1 -8 11 1.90 3.60 -2 8 -11 41.50 3.60 -2 8 -11 36.40 4.70 2 -8 11 49.80 5.40 -3 8 -11 44.50 5.10 -3 8 -11 40.90 3.60 3 -8 11 42.70 5.30 -4 8 -11 30.60 4.80 -4 8 -11 33.30 3.10 4 -8 11 31.00 5.20 -5 8 -11 35.70 5.30 -5 8 -11 38.30 3.40 5 -8 11 41.30 6.40 -8 -7 11 4.50 2.80 7 7 -11 9.80 4.30 -7 -7 11 10.80 2.50 6 7 -11 18.40 4.30 -6 -7 11 17.50 2.70 5 7 -11 14.70 3.70 -5 -7 11 6.60 2.10 4 7 -11 3.80 3.10 -4 -7 11 4.30 2.10 3 7 -11 2.80 3.20 -3 -7 11 2.50 2.20 2 7 -11 0.40 2.90 1 7 -11 60.29 4.40 1 7 -11 46.60 5.00 0 7 -11 6.50 3.20 0 7 -11 5.90 2.20 -1 7 -11 97.89 7.50 -1 7 -11 96.69 6.30 1 -7 11 90.99 6.90 -2 7 -11 12.10 2.30 -2 7 -11 9.00 3.20 2 -7 11 10.90 3.70 -3 7 -11 6.80 3.20 -3 7 -11 10.70 2.10 3 -7 11 7.00 3.40 -4 7 -11 -1.40 3.50 -4 7 -11 -1.00 1.80 4 -7 11 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12 78.59 8.00 4 -9 -12 18.30 1.50 4 -9 -12 16.10 4.20 -4 9 12 17.10 4.30 3 -9 -12 289.97 17.50 3 -9 -12 291.77 15.90 2 -9 -12 45.20 2.80 2 -9 -12 49.80 4.70 -2 9 12 42.50 4.40 -2 9 12 37.10 4.70 1 -9 -12 859.31 46.50 1 -9 -12 822.02 45.40 -1 9 12 825.32 46.00 0 -9 -12 8.80 2.60 0 -9 -12 9.40 1.20 0 9 12 13.60 2.60 -1 -9 -12 123.19 7.00 -1 -9 -12 116.69 8.00 1 9 12 126.69 8.00 -2 -9 -12 38.50 4.20 -2 -9 -12 35.30 2.70 2 9 12 40.60 3.80 -3 -9 -12 11.00 2.80 -3 -9 -12 14.00 1.70 3 9 12 12.90 2.60 -4 -9 -12 187.88 11.70 -4 -9 -12 194.58 10.90 4 9 12 190.38 11.50 4 9 12 184.28 10.60 -5 -9 -12 94.49 6.80 5 9 12 84.09 5.40 5 9 12 85.69 6.40 -6 -9 -12 54.69 5.00 -6 -9 -12 47.00 4.10 6 9 12 49.40 4.80 6 9 12 50.79 3.70 -7 -9 -12 44.40 4.90 7 9 12 37.40 3.40 7 9 12 38.80 4.60 -8 -9 -12 6.00 3.30 8 9 12 3.90 2.30 8 9 12 2.90 3.20 -9 -9 -12 63.59 7.10 9 9 12 53.69 6.10 9 9 12 63.59 5.20 -10 -9 -12 5.60 4.90 10 9 12 7.80 4.50 -11 -9 -12 8.20 6.10 11 9 12 1.60 5.80 6 -10 -12 35.50 5.90 6 -10 -12 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3.20 0 -2 14 26.90 2.50 -1 2 -14 2.80 2.90 -1 2 -14 2.40 3.00 1 -2 14 3.90 1.90 1 -2 14 5.00 2.60 -2 2 -14 45.10 5.40 2 -2 14 51.79 4.10 2 -2 14 53.09 4.90 -3 2 -14 5.30 2.20 -3 2 -14 4.60 3.00 3 -2 14 4.40 2.80 3 -2 14 0.20 2.30 -4 2 -14 -0.20 1.90 -4 2 -14 2.30 3.00 4 -2 14 1.90 2.90 -5 2 -14 6.30 2.20 -5 2 -14 5.90 3.50 5 -2 14 7.70 3.40 -6 2 -14 14.70 4.40 -6 2 -14 12.80 2.50 6 -2 14 13.80 4.40 -7 2 -14 1.80 2.40 -7 2 -14 3.60 4.60 7 -2 14 0.40 4.00 -8 2 -14 28.50 5.90 -8 2 -14 27.00 3.40 8 -2 14 17.80 6.10 8 1 -14 6.90 3.20 8 1 -14 3.50 5.40 8 1 -14 3.60 5.00 -8 -1 14 4.80 6.20 7 1 -14 110.59 10.20 7 1 -14 110.99 8.60 7 1 -14 110.19 7.70 -7 -1 14 102.99 10.30 -7 -1 14 116.19 6.50 6 1 -14 10.20 2.60 6 1 -14 7.70 4.50 6 1 -14 10.00 3.80 -6 -1 14 13.30 4.80 -6 -1 14 10.30 1.50 5 1 -14 -0.10 3.20 5 1 -14 1.60 3.80 5 1 -14 -0.30 2.00 -5 -1 14 -0.10 1.20 -5 -1 14 0.80 3.50 4 1 -14 8.50 2.10 4 1 -14 9.30 3.00 4 1 -14 9.50 3.40 -4 -1 14 5.50 1.40 3 1 -14 1.10 1.90 3 1 -14 4.10 3.00 3 1 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14 26.80 6.70 8 -1 -14 63.89 6.80 8 -1 -14 79.79 8.50 8 -1 -14 71.89 5.60 -8 1 14 55.19 7.90 7 -1 -14 4.80 4.40 7 -1 -14 6.50 2.30 7 -1 -14 9.70 3.80 -7 1 14 7.40 4.70 6 -1 -14 54.09 5.40 6 -1 -14 57.99 6.50 6 -1 -14 54.09 4.40 -6 1 14 57.09 6.70 5 -1 -14 11.50 3.70 5 -1 -14 13.40 2.20 5 -1 -14 18.30 3.20 -5 1 14 14.70 1.10 -5 1 14 11.20 4.10 4 -1 -14 11.70 2.00 4 -1 -14 14.70 3.10 4 -1 -14 16.10 3.70 -4 1 14 12.00 3.60 -4 1 14 12.80 1.30 3 -1 -14 20.10 2.20 3 -1 -14 20.30 3.70 3 -1 -14 19.90 2.90 -3 1 14 14.40 1.60 2 -1 -14 9.60 2.40 2 -1 -14 7.70 2.80 2 -1 -14 4.80 1.70 -2 1 14 7.80 1.20 1 -1 -14 6.40 1.70 1 -1 -14 7.30 3.00 -1 1 14 11.90 1.40 0 -1 -14 6.60 1.70 0 -1 -14 7.00 2.70 0 1 14 6.80 1.30 -1 -1 -14 156.58 9.00 -1 -1 -14 142.99 9.70 1 1 14 146.09 8.60 1 1 14 154.28 9.20 -2 -1 -14 23.40 3.50 -2 -1 -14 27.30 2.70 2 1 14 20.40 2.20 2 1 14 25.90 3.20 -3 -1 -14 2.00 2.30 -3 -1 -14 2.10 2.70 3 1 14 1.60 1.70 3 1 14 3.50 2.30 -4 -1 -14 306.07 18.30 4 1 14 292.07 17.80 4 1 14 322.37 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1.80 -1 -3 -21 0.70 3.20 -1 -3 -21 1.80 4.80 1 3 21 1.70 2.00 -2 -3 -21 27.80 6.20 2 3 21 29.00 3.20 -3 -3 -21 4.20 4.70 3 3 21 0.00 2.50 -4 -3 -21 1.40 4.90 4 3 21 6.30 3.00 -5 -3 -21 63.79 9.00 5 3 21 75.89 8.10 5 3 21 71.89 6.10 2 -4 -21 54.99 5.10 2 -4 -21 52.69 7.50 1 -4 -21 4.30 5.70 1 -4 -21 5.70 2.90 -1 4 21 2.90 1.30 0 -4 -21 3.40 4.70 0 -4 -21 6.90 3.10 0 4 21 8.00 1.80 -1 -4 -21 40.90 6.50 -1 -4 -21 47.20 4.50 1 4 21 49.60 3.80 -2 -4 -21 0.30 4.50 -2 -4 -21 0.20 2.80 2 4 21 0.70 2.10 -3 -4 -21 3.60 4.40 3 4 21 5.20 2.50 -4 -4 -21 9.60 5.10 4 4 21 15.00 3.00 -5 -4 -21 35.40 6.90 5 4 21 25.70 3.60 5 4 21 29.00 6.20 2 -5 -21 7.90 5.20 2 -5 -21 6.40 3.00 1 -5 -21 13.60 6.00 1 -5 -21 12.40 3.00 0 -5 -21 -1.60 4.40 0 -5 -21 1.10 2.80 0 5 21 0.70 1.30 -1 -5 -21 15.10 5.00 -1 -5 -21 22.40 3.40 1 5 21 12.30 1.90 -2 -5 -21 26.30 5.60 -2 -5 -21 21.90 3.70 2 5 21 23.30 2.60 -3 -5 -21 5.70 4.70 3 5 21 8.00 2.30 -4 -5 -21 4.50 4.70 4 5 21 0.70 2.40 -5 -5 -21 14.50 5.40 5 5 21 13.60 5.30 5 5 21 14.80 3.20 6 5 21 3.10 5.00 6 5 21 3.30 3.30 2 -6 -21 5.80 2.80 2 -6 -21 3.20 5.80 1 -6 -21 3.40 5.10 1 -6 -21 7.00 2.80 0 -6 -21 13.80 3.00 0 -6 -21 12.40 5.20 -1 -6 -21 14.90 5.10 -1 -6 -21 14.50 3.10 1 6 21 19.30 1.80 -2 -6 -21 1.10 5.10 -2 -6 -21 -0.10 2.80 2 6 21 0.00 1.60 -3 -6 -21 1.00 3.10 -3 -6 -21 0.90 5.10 3 6 21 -0.20 1.90 -4 -6 -21 12.10 5.20 4 6 21 8.80 2.50 -5 -6 -21 1.30 5.00 5 6 21 -2.20 4.90 5 6 21 2.90 2.70 6 6 21 -1.80 3.00 6 6 21 -2.30 4.90 2 -7 -21 0.60 2.60 2 -7 -21 0.00 5.70 1 -7 -21 1.90 5.20 1 -7 -21 3.60 2.70 0 -7 -21 12.20 5.20 0 -7 -21 18.20 2.90 -1 -7 -21 -0.70 2.40 -1 -7 -21 -0.30 5.10 -2 -7 -21 11.00 2.80 -2 -7 -21 6.30 4.80 2 7 21 4.70 1.50 -3 -7 -21 2.60 4.60 -3 -7 -21 4.10 3.00 3 7 21 3.90 1.80 -4 -7 -21 5.40 3.20 -4 -7 -21 3.70 4.80 4 7 21 0.80 4.90 4 7 21 1.90 2.00 -5 -7 -21 11.60 5.70 5 7 21 5.00 2.50 5 7 21 12.50 5.50 -6 -7 -21 157.78 13.40 6 7 21 163.18 12.00 2 -8 -21 2.20 5.50 1 -8 -21 77.99 5.80 1 -8 -21 58.49 8.10 0 -8 -21 10.20 2.80 0 -8 -21 13.40 5.50 -1 -8 -21 -0.60 2.40 -1 -8 -21 2.50 4.60 -2 -8 -21 0.20 2.60 -2 -8 -21 -0.60 4.60 2 8 21 0.00 1.50 -3 -8 -21 3.00 2.80 -3 -8 -21 1.50 4.60 3 8 21 3.40 1.60 -4 -8 -21 55.89 4.80 -4 -8 -21 32.60 6.10 4 8 21 44.90 3.80 4 8 21 42.80 5.80 -5 -8 -21 18.30 6.10 5 8 21 26.20 5.40 5 8 21 23.60 3.00 -6 -8 -21 24.30 6.10 6 8 21 15.90 3.60 6 8 21 30.10 5.80 1 -9 -21 53.19 7.60 1 -9 -21 37.50 3.80 0 -9 -21 3.20 5.20 0 -9 -21 0.00 2.40 -1 -9 -21 34.60 6.70 -1 -9 -21 30.00 3.50 -2 -9 -21 5.40 2.50 -2 -9 -21 3.40 4.80 -3 -9 -21 20.60 5.90 -3 -9 -21 24.50 3.40 3 9 21 23.00 1.90 -4 -9 -21 3.50 5.30 -4 -9 -21 0.30 2.90 4 9 21 -0.60 4.20 4 9 21 2.00 1.80 -5 -9 -21 75.59 6.30 -5 -9 -21 71.19 8.50 5 9 21 71.59 5.20 5 9 21 69.89 7.70 -6 -9 -21 15.20 5.80 6 9 21 15.60 5.40 1 -10 -21 4.50 6.40 0 -10 -21 -1.60 2.40 0 -10 -21 2.60 5.50 -1 -10 -21 20.60 3.20 -1 -10 -21 33.00 6.70 -2 -10 -21 47.20 6.90 -2 -10 -21 44.70 4.20 -3 -10 -21 33.10 6.60 -3 -10 -21 34.70 4.00 -4 -10 -21 37.20 6.80 -4 -10 -21 30.70 3.90 4 10 21 27.30 5.40 4 10 21 28.70 2.40 -5 -10 -21 17.00 3.80 -5 -10 -21 13.80 5.60 5 10 21 8.90 2.20 5 10 21 9.10 4.90 -6 -10 -21 10.90 5.70 6 10 21 6.10 5.70 0 -11 -21 1.40 5.60 0 -11 -21 2.90 3.10 -1 -11 -21 21.00 6.00 -1 -11 -21 14.10 2.80 -2 -11 -21 93.19 9.40 -2 -11 -21 93.49 6.70 -3 -11 -21 12.60 5.40 -3 -11 -21 10.80 3.00 -4 -11 -21 4.10 5.10 -4 -11 -21 3.20 3.10 4 11 21 2.90 5.30 -5 -11 -21 16.60 5.80 -5 -11 -21 19.50 3.90 5 11 21 15.10 2.10 5 11 21 22.30 6.20 -6 -11 -21 20.60 6.80 -6 -11 -21 17.80 4.40 0 -12 -21 5.30 6.00 -1 -12 -21 3.20 6.20 -2 -12 -21 3.50 2.60 -2 -12 -21 8.00 6.30 -3 -12 -21 -0.70 5.20 -3 -12 -21 3.20 2.80 3 12 21 2.70 5.80 -4 -12 -21 12.40 5.70 -4 -12 -21 21.30 3.60 4 12 21 20.90 5.50 -5 -12 -21 8.40 5.60 -5 -12 -21 9.90 3.60 5 12 21 5.50 5.30 -2 -13 -21 -1.40 5.80 -3 -13 -21 12.40 6.70 3 13 21 7.30 5.20 -4 -13 -21 5.10 6.50 -1 -2 -22 4.70 6.30 -1 3 22 3.00 2.10 0 -3 -22 49.50 5.50 0 -3 -22 57.39 7.80 -1 -3 -22 3.30 5.40 -2 -3 -22 13.30 5.70 1 -4 -22 46.10 4.80 -1 4 22 42.20 3.50 0 -4 -22 10.30 3.70 0 -4 -22 9.20 5.50 0 4 22 9.90 2.00 -1 -4 -22 0.70 3.50 -1 -4 -22 1.60 5.20 1 4 22 0.50 2.00 -2 -4 -22 1.10 5.10 2 4 22 -0.50 2.10 -3 -4 -22 5.70 5.80 3 4 22 2.80 2.80 1 -5 -22 9.70 3.40 0 -5 -22 1.70 5.10 0 -5 -22 3.70 3.20 0 5 22 5.60 1.40 -1 -5 -22 21.50 3.70 -1 -5 -22 15.40 6.10 1 5 22 13.80 2.20 -2 -5 -22 3.80 3.50 -2 -5 -22 6.80 5.70 2 5 22 5.10 2.10 -3 -5 -22 -1.40 4.80 3 5 22 -0.70 2.30 1 -6 -22 6.00 3.20 0 -6 -22 12.40 3.30 0 -6 -22 4.60 5.00 -1 -6 -22 -1.50 5.30 -1 -6 -22 1.10 2.90 1 6 22 0.50 1.40 -2 -6 -22 -0.20 4.80 -2 -6 -22 7.00 3.40 2 6 22 7.00 1.90 -3 -6 -22 10.70 5.30 -3 -6 -22 8.20 3.70 3 6 22 12.90 2.30 -4 -6 -22 7.00 5.80 4 6 22 7.20 2.80 0 -7 -22 2.90 2.90 0 -7 -22 -0.40 5.20 -1 -7 -22 10.50 3.10 -1 -7 -22 9.90 5.50 -2 -7 -22 1.40 2.80 -2 -7 -22 6.00 5.40 2 7 22 0.70 1.50 -3 -7 -22 -0.70 5.60 -3 -7 -22 0.60 3.10 3 7 22 0.90 1.90 -4 -7 -22 0.30 5.00 4 7 22 1.60 2.20 5 7 22 2.90 5.80 0 -8 -22 42.20 7.20 0 -8 -22 52.39 4.60 -1 -8 -22 1.50 2.90 -1 -8 -22 1.30 5.20 -2 -8 -22 10.20 3.30 -2 -8 -22 9.50 5.50 -3 -8 -22 37.80 7.10 -3 -8 -22 32.20 4.20 3 8 22 31.00 2.70 -4 -8 -22 30.50 4.50 -4 -8 -22 37.20 6.60 4 8 22 33.20 3.10 5 8 22 2.70 5.90 0 -9 -22 15.20 6.70 -1 -9 -22 13.00 3.00 -1 -9 -22 6.40 5.50 -2 -9 -22 13.90 6.40 -2 -9 -22 10.50 3.10 -3 -9 -22 1.60 3.00 -3 -9 -22 1.00 5.30 3 9 22 2.10 1.30 -4 -9 -22 9.30 6.10 -4 -9 -22 12.00 3.80 4 9 22 8.40 2.00 5 9 22 9.20 5.30 -1 -10 -22 31.70 6.70 -2 -10 -22 0.60 2.90 -2 -10 -22 3.00 6.20 -3 -10 -22 5.20 5.40 -3 -10 -22 1.30 3.00 -4 -10 -22 0.10 3.40 -4 -10 -22 -2.40 5.80 4 10 22 -1.50 1.50 4 10 22 -0.40 8.30 -1 -11 -22 34.80 8.50 -2 -11 -22 0.10 5.70 -3 -11 -22 -1.50 5.50 -3 -11 -22 0.80 3.40 -4 -11 -22 2.20 5.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 56890 _shelx_res_file ; TITL JTM875_0m_a.res in P-1 JTM875_0m_a.res created by SHELXL-2016/6 at 10:19:34 on 29-Nov-2017 REM Old TITL JTM875_0m in P-1 REM SHELXT solution in P-1 REM R1 0.109, Rweak 0.003, Alpha 0.027, Orientation as input REM Formula found by SHELXT: C44 N4 O4 CELL 0.71073 8.8897 13.2911 16.6864 67.900 81.027 74.294 ZERR 4.000 0.0005 0.0007 0.0009 0.001 0.001 0.001 LATT 1 SFAC C H N O UNIT 88 72 8 8 TEMP -173 SIZE 0.185 0.213 0.372 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 CONF EQIV $1 -x+1, -y+1, -z HTAB N2 O2_$1 EQIV $2 -x+2, -y, -z+1 HTAB N4 O4_$2 OMIT 1 1 1 OMIT 0 1 2 ACTA 57 WGHT 0.083200 FVAR 0.54230 O1 4 0.463065 0.621581 0.263765 11.00000 0.02684 0.01959 = 0.01433 -0.00684 0.00016 -0.00543 O2 4 0.415520 0.416998 0.105856 11.00000 0.02390 0.01994 = 0.01842 -0.00713 -0.00149 -0.00888 N1 3 0.429110 0.498934 0.204328 11.00000 0.01627 0.01554 = 0.01300 -0.00350 -0.00012 -0.00440 N2 3 0.536871 0.562962 0.071567 11.00000 0.02001 0.01858 = 0.01361 -0.00709 0.00162 -0.00794 H2 2 0.556198 0.573822 0.013566 11.00000 0.03055 C1 1 0.553064 0.639125 0.112288 11.00000 0.01713 0.01436 = 0.01262 -0.00495 -0.00066 -0.00427 C2 1 0.477329 0.589096 0.203641 11.00000 0.01408 0.01559 = 0.01335 -0.00404 -0.00165 -0.00199 C3 1 0.458198 0.486359 0.123060 11.00000 0.01352 0.01560 = 0.01468 -0.00497 -0.00249 -0.00146 C4 1 0.344790 0.430393 0.277410 11.00000 0.01581 0.01821 = 0.01472 -0.00224 0.00050 -0.00571 H4A 2 0.275989 0.403808 0.252107 11.00000 0.02334 H4B 2 0.272936 0.480988 0.307320 11.00000 0.01722 C5 1 0.447223 0.334153 0.342595 11.00000 0.01958 0.01464 = 0.01138 -0.00413 0.00008 -0.00247 C6 1 0.597056 0.335564 0.355767 11.00000 0.02273 0.01950 = 0.02192 -0.00390 -0.00454 -0.00578 H6 2 0.643929 0.399507 0.317850 11.00000 0.02877 C7 1 0.682505 0.247534 0.420719 11.00000 0.02463 0.02682 = 0.02704 -0.00668 -0.01089 -0.00110 H7 2 0.786529 0.249382 0.429620 11.00000 0.04872 C8 1 0.618489 0.158079 0.472859 11.00000 0.03493 0.02192 = 0.01774 -0.00364 -0.00835 0.00322 H8 2 0.681162 0.094871 0.517097 11.00000 0.03670 C9 1 0.469249 0.156687 0.460115 11.00000 0.03397 0.01685 = 0.01807 -0.00111 0.00255 -0.00438 H9 2 0.425153 0.092579 0.498189 11.00000 0.03629 C10 1 0.384032 0.243855 0.395236 11.00000 0.02165 0.01747 = 0.01817 -0.00585 0.00171 -0.00473 H10 2 0.283584 0.238958 0.386254 11.00000 0.03075 C11 1 0.724497 0.632211 0.122305 11.00000 0.01677 0.01744 = 0.01206 -0.00114 -0.00143 -0.00581 C12 1 0.844492 0.546369 0.110225 11.00000 0.02043 0.02030 = 0.02690 -0.00654 -0.00286 -0.00339 H12 2 0.822309 0.490072 0.091822 11.00000 0.03012 C13 1 0.998617 0.540482 0.122972 11.00000 0.01918 0.02484 = 0.03493 -0.00397 -0.00290 -0.00129 H13 2 1.085033 0.480613 0.112548 11.00000 0.03366 C14 1 1.031482 0.619565 0.148057 11.00000 0.02019 0.03123 = 0.02537 0.00338 -0.00831 -0.01058 H14 2 1.140557 0.613671 0.155035 11.00000 0.03168 C15 1 0.911744 0.705239 0.161083 11.00000 0.02940 0.02523 = 0.01834 0.00062 -0.00669 -0.01421 H15 2 0.934758 0.761491 0.178804 11.00000 0.03082 C16 1 0.758730 0.711707 0.147731 11.00000 0.02313 0.02014 = 0.01422 -0.00368 -0.00098 -0.00777 H16 2 0.671247 0.774207 0.155400 11.00000 0.02522 C17 1 0.463497 0.757733 0.063437 11.00000 0.01787 0.01557 = 0.01501 -0.00417 -0.00295 -0.00435 C18 1 0.527220 0.817244 -0.016672 11.00000 0.02439 0.02556 = 0.01693 -0.00199 -0.00049 -0.00477 H18 2 0.632022 0.782235 -0.039358 11.00000 0.02896 C19 1 0.445132 0.921540 -0.066181 11.00000 0.03424 0.02816 = 0.01984 0.00413 -0.00345 -0.00836 H19 2 0.491164 0.962055 -0.122775 11.00000 0.03978 C20 1 0.297010 0.966911 -0.036760 11.00000 0.03496 0.01930 = 0.03036 0.00044 -0.01027 -0.00103 H20 2 0.236050 1.042093 -0.073609 11.00000 0.04828 C21 1 0.233298 0.908815 0.042816 11.00000 0.02375 0.02054 = 0.03136 -0.00816 -0.00346 0.00007 H21 2 0.128291 0.939699 0.064530 11.00000 0.03209 C22 1 0.316505 0.804611 0.093340 11.00000 0.02021 0.01870 = 0.01958 -0.00605 -0.00009 -0.00501 H22 2 0.268159 0.766595 0.149153 11.00000 0.01830 O3 4 0.938936 0.157561 0.747555 11.00000 0.02540 0.02318 = 0.01772 -0.01104 0.00119 -0.00898 O4 4 1.080493 0.120555 0.482979 11.00000 0.02093 0.02013 = 0.01371 -0.00589 0.00221 -0.00818 N3 3 1.024283 0.162905 0.608871 11.00000 0.01705 0.01445 = 0.01405 -0.00533 0.00012 -0.00549 N4 3 0.971670 0.008941 0.609165 11.00000 0.01875 0.01562 = 0.01216 -0.00545 0.00116 -0.00634 H4 2 0.949635 -0.038513 0.586924 11.00000 0.02845 C23 1 0.909758 0.014220 0.694604 11.00000 0.01601 0.01450 = 0.01196 -0.00509 0.00045 -0.00351 C24 1 0.956663 0.119812 0.690162 11.00000 0.01414 0.01621 = 0.01478 -0.00526 -0.00121 -0.00315 C25 1 1.029591 0.097683 0.558739 11.00000 0.01218 0.01563 = 0.01456 -0.00510 -0.00176 -0.00251 C26 1 1.073618 0.269005 0.574909 11.00000 0.01708 0.01530 = 0.01995 -0.00570 -0.00014 -0.00715 H26A 2 1.092731 0.280433 0.627926 11.00000 0.01305 H26B 2 1.174398 0.257019 0.540696 11.00000 0.02307 C27 1 0.948449 0.363465 0.523732 11.00000 0.01888 0.01441 = 0.01852 -0.00607 -0.00136 -0.00717 C28 1 0.811061 0.403740 0.566477 11.00000 0.02197 0.02069 = 0.01939 -0.00847 -0.00051 -0.00575 H28 2 0.796721 0.373245 0.629972 11.00000 0.02188 C29 1 0.693806 0.489239 0.520085 11.00000 0.02180 0.02240 = 0.03187 -0.01234 -0.00285 -0.00243 H29 2 0.596737 0.515442 0.552403 11.00000 0.03486 C30 1 0.712364 0.534798 0.430501 11.00000 0.02845 0.01713 = 0.03250 -0.00361 -0.01018 -0.00656 H30 2 0.632420 0.593225 0.398304 11.00000 0.03383 C31 1 0.847807 0.495670 0.387342 11.00000 0.03437 0.02122 = 0.02040 0.00029 -0.00375 -0.01158 H31 2 0.864006 0.527726 0.324103 11.00000 0.03218 C32 1 0.965642 0.410080 0.434087 11.00000 0.02471 0.01942 = 0.02081 -0.00518 0.00288 -0.00956 H32 2 1.062138 0.382861 0.405297 11.00000 0.02242 C34 1 0.627807 0.130016 0.699942 11.00000 0.02087 0.01762 = 0.01734 -0.00538 -0.00041 -0.00417 C33 1 0.731292 0.029771 0.702130 11.00000 0.01549 0.01755 = 0.01227 -0.00459 -0.00079 -0.00334 H34 2 0.669002 0.193012 0.697955 11.00000 0.02638 C35 1 0.466924 0.140797 0.701256 11.00000 0.01952 0.02350 = 0.01894 -0.00525 -0.00162 0.00112 H35 2 0.394652 0.212690 0.699592 11.00000 0.02885 C36 1 0.409727 0.052392 0.704885 11.00000 0.01654 0.03302 = 0.02263 -0.00994 -0.00198 -0.00520 H36 2 0.296882 0.057770 0.705378 11.00000 0.02930 C37 1 0.512469 -0.048027 0.707415 11.00000 0.02111 0.03115 = 0.03284 -0.01690 0.00211 -0.01105 H37 2 0.474250 -0.110611 0.711112 11.00000 0.03282 C38 1 0.672665 -0.059152 0.706051 11.00000 0.01953 0.02170 = 0.02643 -0.01166 0.00056 -0.00553 H38 2 0.744046 -0.133112 0.707600 11.00000 0.02160 C39 1 0.991714 -0.084709 0.768978 11.00000 0.01704 0.01574 = 0.01445 -0.00366 -0.00173 -0.00596 C40 1 0.920493 -0.110202 0.852205 11.00000 0.02246 0.02667 = 0.01703 -0.00554 0.00080 -0.00184 H40 2 0.813814 -0.066638 0.861940 11.00000 0.03833 C41 1 0.999476 -0.194645 0.921515 11.00000 0.03295 0.03311 = 0.01483 -0.00223 -0.00138 -0.00362 H41 2 0.946417 -0.208916 0.977307 11.00000 0.04222 C42 1 1.150238 -0.252947 0.908134 11.00000 0.03212 0.02294 = 0.02273 -0.00047 -0.01003 -0.00210 H42 2 1.205876 -0.309925 0.957628 11.00000 0.03438 C43 1 1.220972 -0.228353 0.825582 11.00000 0.02306 0.02381 = 0.02946 -0.00270 -0.00358 0.00125 H43 2 1.327583 -0.269053 0.814439 11.00000 0.04337 C44 1 1.142115 -0.144528 0.755845 11.00000 0.01931 0.02151 = 0.02129 -0.00477 0.00158 -0.00252 H44 2 1.194915 -0.130870 0.697470 11.00000 0.03664 HKLF 4 REM JTM875_0m_a.res in P-1 REM R1 = 0.0469 for 7122 Fo > 4sig(Fo) and 0.0613 for all 9388 data REM 613 parameters refined using 0 restraints END WGHT 0.0832 0.0000 REM Highest difference peak 0.426, deepest hole -0.204, 1-sigma level 0.061 Q1 1 0.6405 0.6346 0.1175 11.00000 0.05 0.43 Q2 1 1.0618 -0.1174 0.7604 11.00000 0.05 0.39 Q3 1 0.4050 0.7942 0.0816 11.00000 0.05 0.39 Q4 1 1.0024 0.3170 0.5460 11.00000 0.05 0.39 Q5 1 0.6729 0.0676 0.7157 11.00000 0.05 0.38 ; _shelx_res_checksum 84540 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.46307(9) 0.62158(7) 0.26376(5) 0.02014(18) Uani d 1 O O2 0.41552(9) 0.41700(7) 0.10586(5) 0.01982(18) Uani d 1 N N1 0.42911(10) 0.49893(7) 0.20433(6) 0.01533(19) Uani d 1 N N2 0.53687(11) 0.56296(8) 0.07157(6) 0.0166(2) Uani d 1 H H2 0.5562(16) 0.5738(12) 0.0136(10) 0.031(4) Uiso d 1 C C1 0.55306(12) 0.63913(9) 0.11229(7) 0.0145(2) Uani d 1 C C2 0.47733(12) 0.58910(9) 0.20364(7) 0.0149(2) Uani d 1 C C3 0.45820(12) 0.48636(9) 0.12306(7) 0.0149(2) Uani d 1 C C4 0.34479(13) 0.43039(9) 0.27741(7) 0.0171(2) Uani d 1 H H4A 0.2760(16) 0.4038(11) 0.2521(9) 0.023(3) Uiso d 1 H H4B 0.2729(14) 0.4810(11) 0.3073(8) 0.017(3) Uiso d 1 C C5 0.44722(13) 0.33415(9) 0.34260(7) 0.0158(2) Uani d 1 C C6 0.59706(14) 0.33556(10) 0.35577(8) 0.0218(2) Uani d 1 H H6 0.6439(17) 0.3995(12) 0.3179(10) 0.029(4) Uiso d 1 C C7 0.68251(15) 0.24753(11) 0.42072(9) 0.0269(3) Uani d 1 H H7 0.787(2) 0.2494(14) 0.4296(11) 0.049(5) Uiso d 1 C C8 0.61849(16) 0.15808(11) 0.47286(8) 0.0271(3) Uani d 1 H H8 0.6812(17) 0.0949(13) 0.5171(10) 0.037(4) Uiso d 1 C C9 0.46925(15) 0.15669(10) 0.46011(8) 0.0253(3) Uani d 1 H H9 0.4252(17) 0.0926(13) 0.4982(10) 0.036(4) Uiso d 1 C C10 0.38403(14) 0.24386(9) 0.39524(8) 0.0195(2) Uani d 1 H H10 0.2836(18) 0.2390(12) 0.3863(10) 0.031(4) Uiso d 1 C C11 0.72450(12) 0.63221(9) 0.12231(7) 0.0162(2) Uani d 1 C C12 0.84449(14) 0.54637(10) 0.11023(8) 0.0232(3) Uani d 1 H H12 0.8223(16) 0.4901(12) 0.0918(10) 0.030(4) Uiso d 1 C C13 0.99862(15) 0.54048(11) 0.12297(9) 0.0289(3) Uani d 1 H H13 1.0850(17) 0.4806(13) 0.1125(10) 0.034(4) Uiso d 1 C C14 1.03148(15) 0.61956(11) 0.14806(9) 0.0278(3) Uani d 1 H H14 1.1406(17) 0.6137(12) 0.1550(10) 0.032(4) Uiso d 1 C C15 0.91174(15) 0.70524(11) 0.16108(8) 0.0246(3) Uani d 1 H H15 0.9348(17) 0.7615(12) 0.1788(10) 0.031(4) Uiso d 1 C C16 0.75873(14) 0.71171(10) 0.14773(7) 0.0193(2) Uani d 1 H H16 0.6712(16) 0.7742(12) 0.1554(9) 0.025(4) Uiso d 1 C C17 0.46350(12) 0.75773(9) 0.06344(7) 0.0162(2) Uani d 1 C C18 0.52722(14) 0.81724(11) -0.01667(8) 0.0242(3) Uani d 1 H H18 0.6320(17) 0.7822(12) -0.0394(9) 0.029(4) Uiso d 1 C C19 0.44513(16) 0.92154(11) -0.06618(9) 0.0307(3) Uani d 1 H H19 0.4912(18) 0.9621(13) -0.1228(11) 0.040(4) Uiso d 1 C C20 0.29701(17) 0.96691(11) -0.03676(9) 0.0311(3) Uani d 1 H H20 0.2361(19) 1.0421(15) -0.0736(11) 0.048(5) Uiso d 1 C C21 0.23330(15) 0.90881(10) 0.04282(9) 0.0264(3) Uani d 1 H H21 0.1283(17) 0.9397(12) 0.0645(10) 0.032(4) Uiso d 1 C C22 0.31651(13) 0.80461(10) 0.09334(8) 0.0197(2) Uani d 1 H H22 0.2682(15) 0.7666(11) 0.1492(9) 0.018(3) Uiso d 1 O O3 0.93894(9) 0.15756(7) 0.74756(5) 0.02053(18) Uani d 1 O O4 1.08049(9) 0.12056(7) 0.48298(5) 0.01794(17) Uani d 1 N N3 1.02428(10) 0.16291(7) 0.60887(6) 0.01483(19) Uani d 1 N N4 0.97167(11) 0.00894(8) 0.60916(6) 0.01509(19) Uani d 1 H H4 0.9496(16) -0.0385(12) 0.5869(10) 0.028(4) Uiso d 1 C C23 0.90976(12) 0.01422(9) 0.69460(7) 0.0142(2) Uani d 1 C C24 0.95666(12) 0.11981(9) 0.69016(7) 0.0151(2) Uani d 1 C C25 1.02959(12) 0.09768(9) 0.55874(7) 0.0142(2) Uani d 1 C C26 1.07362(13) 0.26901(9) 0.57491(8) 0.0170(2) Uani d 1 H H26A 1.0927(14) 0.2804(10) 0.6279(8) 0.013(3) Uiso d 1 H H26B 1.1744(16) 0.2570(11) 0.5407(9) 0.023(3) Uiso d 1 C C27 0.94845(13) 0.36346(9) 0.52373(7) 0.0165(2) Uani d 1 C C28 0.81106(13) 0.40374(10) 0.56648(8) 0.0202(2) Uani d 1 H H28 0.7967(15) 0.3732(11) 0.6300(9) 0.022(3) Uiso d 1 C C29 0.69381(14) 0.48924(10) 0.52008(9) 0.0249(3) Uani d 1 H H29 0.5967(18) 0.5154(13) 0.5524(10) 0.035(4) Uiso d 1 C C30 0.71236(15) 0.53480(10) 0.43050(9) 0.0263(3) Uani d 1 H H30 0.6324(17) 0.5932(13) 0.3983(10) 0.034(4) Uiso d 1 C C31 0.84781(15) 0.49567(10) 0.38734(9) 0.0263(3) Uani d 1 H H31 0.8640(17) 0.5277(12) 0.3241(10) 0.032(4) Uiso d 1 C C32 0.96564(14) 0.41008(10) 0.43409(8) 0.0218(2) Uani d 1 H H32 1.0621(16) 0.3829(11) 0.4053(9) 0.022(3) Uiso d 1 C C34 0.62781(13) 0.13002(10) 0.69994(8) 0.0190(2) Uani d 1 C C33 0.73129(12) 0.02977(9) 0.70213(7) 0.0154(2) Uani d 1 H H34 0.6690(16) 0.1930(12) 0.6980(9) 0.026(4) Uiso d 1 C C35 0.46692(13) 0.14080(10) 0.70126(8) 0.0225(3) Uani d 1 H H35 0.3947(16) 0.2127(12) 0.6996(9) 0.029(4) Uiso d 1 C C36 0.40973(14) 0.05239(11) 0.70489(8) 0.0240(3) Uani d 1 H H36 0.2969(17) 0.0578(12) 0.7054(9) 0.029(4) Uiso d 1 C C37 0.51247(14) -0.04803(11) 0.70741(9) 0.0261(3) Uani d 1 H H37 0.4742(17) -0.1106(13) 0.7111(10) 0.033(4) Uiso d 1 C C38 0.67266(13) -0.05915(10) 0.70605(8) 0.0217(2) Uani d 1 H H38 0.7440(15) -0.1331(11) 0.7076(9) 0.022(3) Uiso d 1 C C39 0.99171(12) -0.08471(9) 0.76898(7) 0.0157(2) Uani d 1 C C40 0.92049(14) -0.11020(11) 0.85220(8) 0.0237(3) Uani d 1 H H40 0.8138(18) -0.0666(13) 0.8619(10) 0.038(4) Uiso d 1 C C41 0.99948(16) -0.19464(12) 0.92151(9) 0.0297(3) Uani d 1 H H41 0.9464(19) -0.2089(14) 0.9773(11) 0.042(4) Uiso d 1 C C42 1.15024(16) -0.25295(11) 0.90813(9) 0.0281(3) Uani d 1 H H42 1.2059(17) -0.3099(13) 0.9576(10) 0.034(4) Uiso d 1 C C43 1.22097(15) -0.22835(11) 0.82558(9) 0.0286(3) Uani d 1 H H43 1.3276(19) -0.2691(14) 0.8144(11) 0.043(4) Uiso d 1 C C44 1.14211(13) -0.14453(10) 0.75585(8) 0.0223(3) Uani d 1 H H44 1.1949(17) -0.1309(13) 0.6975(10) 0.037(4) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0268(4) 0.0196(4) 0.0143(4) -0.0054(3) 0.0002(3) -0.0068(3) O2 0.0239(4) 0.0199(4) 0.0184(4) -0.0089(3) -0.0015(3) -0.0071(3) N1 0.0163(4) 0.0155(4) 0.0130(5) -0.0044(3) -0.0001(3) -0.0035(4) N2 0.0200(5) 0.0186(5) 0.0136(5) -0.0079(4) 0.0016(4) -0.0071(4) C1 0.0171(5) 0.0144(5) 0.0126(5) -0.0043(4) -0.0007(4) -0.0049(4) C2 0.0141(5) 0.0156(5) 0.0133(5) -0.0020(4) -0.0017(4) -0.0040(4) C3 0.0135(5) 0.0156(5) 0.0147(5) -0.0015(4) -0.0025(4) -0.0050(4) C4 0.0158(5) 0.0182(5) 0.0147(5) -0.0057(4) 0.0005(4) -0.0022(4) C5 0.0196(5) 0.0146(5) 0.0114(5) -0.0025(4) 0.0001(4) -0.0041(4) C6 0.0227(6) 0.0195(5) 0.0219(6) -0.0058(5) -0.0045(5) -0.0039(5) C7 0.0246(6) 0.0268(6) 0.0270(7) -0.0011(5) -0.0109(5) -0.0067(5) C8 0.0349(7) 0.0219(6) 0.0177(6) 0.0032(5) -0.0083(5) -0.0036(5) C9 0.0340(7) 0.0169(5) 0.0181(6) -0.0044(5) 0.0025(5) -0.0011(5) C10 0.0216(5) 0.0175(5) 0.0182(6) -0.0047(4) 0.0017(4) -0.0058(5) C11 0.0168(5) 0.0174(5) 0.0121(5) -0.0058(4) -0.0014(4) -0.0011(4) C12 0.0204(6) 0.0203(6) 0.0269(7) -0.0034(5) -0.0029(5) -0.0065(5) C13 0.0192(6) 0.0248(6) 0.0349(8) -0.0013(5) -0.0029(5) -0.0040(6) C14 0.0202(6) 0.0312(7) 0.0254(7) -0.0106(5) -0.0083(5) 0.0034(5) C15 0.0294(6) 0.0252(6) 0.0183(6) -0.0142(5) -0.0067(5) 0.0006(5) C16 0.0231(5) 0.0201(5) 0.0142(5) -0.0078(5) -0.0010(4) -0.0037(5) C17 0.0179(5) 0.0156(5) 0.0150(5) -0.0044(4) -0.0030(4) -0.0042(4) C18 0.0244(6) 0.0256(6) 0.0169(6) -0.0048(5) -0.0005(5) -0.0020(5) C19 0.0342(7) 0.0282(7) 0.0198(7) -0.0084(6) -0.0034(5) 0.0041(5) C20 0.0350(7) 0.0193(6) 0.0304(7) -0.0010(5) -0.0103(6) 0.0004(5) C21 0.0238(6) 0.0205(6) 0.0314(7) 0.0001(5) -0.0035(5) -0.0082(5) C22 0.0202(5) 0.0187(5) 0.0196(6) -0.0050(4) -0.0001(4) -0.0061(5) O3 0.0254(4) 0.0232(4) 0.0177(4) -0.0090(3) 0.0012(3) -0.0110(4) O4 0.0209(4) 0.0201(4) 0.0137(4) -0.0082(3) 0.0022(3) -0.0059(3) N3 0.0171(4) 0.0144(4) 0.0141(5) -0.0055(3) 0.0001(3) -0.0053(4) N4 0.0188(4) 0.0156(4) 0.0122(5) -0.0063(4) 0.0012(3) -0.0055(4) C23 0.0160(5) 0.0145(5) 0.0120(5) -0.0035(4) 0.0004(4) -0.0051(4) C24 0.0141(5) 0.0162(5) 0.0148(5) -0.0032(4) -0.0012(4) -0.0053(4) C25 0.0122(4) 0.0156(5) 0.0146(5) -0.0025(4) -0.0018(4) -0.0051(4) C26 0.0171(5) 0.0153(5) 0.0200(6) -0.0071(4) -0.0001(4) -0.0057(4) C27 0.0189(5) 0.0144(5) 0.0185(6) -0.0072(4) -0.0014(4) -0.0061(4) C28 0.0220(6) 0.0207(6) 0.0194(6) -0.0058(5) -0.0005(5) -0.0085(5) C29 0.0218(6) 0.0224(6) 0.0319(7) -0.0024(5) -0.0029(5) -0.0123(5) C30 0.0285(6) 0.0171(5) 0.0325(7) -0.0066(5) -0.0102(5) -0.0036(5) C31 0.0344(7) 0.0212(6) 0.0204(6) -0.0116(5) -0.0037(5) 0.0003(5) C32 0.0247(6) 0.0194(5) 0.0208(6) -0.0096(5) 0.0029(5) -0.0052(5) C34 0.0209(5) 0.0176(5) 0.0173(6) -0.0042(4) -0.0004(4) -0.0054(5) C33 0.0155(5) 0.0175(5) 0.0123(5) -0.0033(4) -0.0008(4) -0.0046(4) C35 0.0195(5) 0.0235(6) 0.0189(6) 0.0011(5) -0.0016(4) -0.0053(5) C36 0.0165(5) 0.0330(7) 0.0226(6) -0.0052(5) -0.0020(4) -0.0099(5) C37 0.0211(6) 0.0312(7) 0.0328(7) -0.0110(5) 0.0021(5) -0.0169(6) C38 0.0195(5) 0.0217(6) 0.0264(6) -0.0055(5) 0.0006(5) -0.0117(5) C39 0.0170(5) 0.0157(5) 0.0145(5) -0.0060(4) -0.0017(4) -0.0037(4) C40 0.0225(6) 0.0267(6) 0.0170(6) -0.0018(5) 0.0008(5) -0.0055(5) C41 0.0329(7) 0.0331(7) 0.0148(6) -0.0036(6) -0.0014(5) -0.0022(5) C42 0.0321(7) 0.0229(6) 0.0227(7) -0.0021(5) -0.0100(5) -0.0005(5) C43 0.0231(6) 0.0238(6) 0.0295(7) 0.0012(5) -0.0036(5) -0.0027(5) C44 0.0193(5) 0.0215(6) 0.0213(6) -0.0025(5) 0.0016(5) -0.0048(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 N1 C3 111.64(9) C2 N1 C4 124.66(9) C3 N1 C4 123.46(9) C3 N2 C1 113.00(9) C3 N2 H2 120.6(10) C1 N2 H2 125.0(10) N2 C1 C17 109.90(9) N2 C1 C11 112.56(8) C17 C1 C11 112.87(9) N2 C1 C2 100.97(9) C17 C1 C2 112.28(8) C11 C1 C2 107.66(8) O1 C2 N1 126.04(10) O1 C2 C1 127.35(10) N1 C2 C1 106.60(9) O2 C3 N2 128.73(11) O2 C3 N1 123.75(10) N2 C3 N1 107.51(9) N1 C4 C5 114.99(9) N1 C4 H4A 106.2(8) C5 C4 H4A 111.3(8) N1 C4 H4B 107.8(8) C5 C4 H4B 109.6(7) H4A C4 H4B 106.5(11) C6 C5 C10 119.12(10) C6 C5 C4 122.60(10) C10 C5 C4 118.14(10) C5 C6 C7 120.13(12) C5 C6 H6 119.7(8) C7 C6 H6 120.1(8) C8 C7 C6 120.31(12) C8 C7 H7 120.1(10) C6 C7 H7 119.6(10) C9 C8 C7 119.67(11) C9 C8 H8 120.5(9) C7 C8 H8 119.8(9) C8 C9 C10 120.23(12) C8 C9 H9 118.6(9) C10 C9 H9 121.2(9) C9 C10 C5 120.53(11) C9 C10 H10 118.3(9) C5 C10 H10 121.1(9) C12 C11 C16 119.64(11) C12 C11 C1 121.58(10) C16 C11 C1 118.72(9) C11 C12 C13 120.00(12) C11 C12 H12 120.6(8) C13 C12 H12 119.4(8) C14 C13 C12 119.98(12) C14 C13 H13 119.8(9) C12 C13 H13 120.2(9) C13 C14 C15 120.38(11) C13 C14 H14 117.6(9) C15 C14 H14 122.0(9) C16 C15 C14 119.69(12) C16 C15 H15 119.8(8) C14 C15 H15 120.5(8) C15 C16 C11 120.30(11) C15 C16 H16 120.7(8) C11 C16 H16 119.0(8) C22 C17 C18 119.23(10) C22 C17 C1 122.18(10) C18 C17 C1 118.43(9) C19 C18 C17 120.52(11) C19 C18 H18 120.1(8) C17 C18 H18 119.3(8) C18 C19 C20 119.97(12) C18 C19 H19 119.5(9) C20 C19 H19 120.5(9) C21 C20 C19 119.90(12) C21 C20 H20 120.2(10) C19 C20 H20 119.9(10) C20 C21 C22 120.26(12) C20 C21 H21 120.9(9) C22 C21 H21 118.8(9) C17 C22 C21 120.10(12) C17 C22 H22 122.1(7) C21 C22 H22 117.8(7) C24 N3 C25 111.59(9) C24 N3 C26 124.84(9) C25 N3 C26 123.38(9) C25 N4 C23 112.94(9) C25 N4 H4 121.9(9) C23 N4 H4 123.2(9) N4 C23 C39 112.81(8) N4 C23 C33 109.64(8) C39 C23 C33 113.22(9) N4 C23 C24 100.50(8) C39 C23 C24 108.32(9) C33 C23 C24 111.65(8) O3 C24 N3 126.04(10) O3 C24 C23 126.87(10) N3 C24 C23 107.09(9) O4 C25 N4 128.38(10) O4 C25 N3 124.03(10) N4 C25 N3 107.59(9) N3 C26 C27 111.43(9) N3 C26 H26A 103.9(7) C27 C26 H26A 111.4(7) N3 C26 H26B 107.1(8) C27 C26 H26B 113.4(8) H26A C26 H26B 109.1(11) C32 C27 C28 118.94(11) C32 C27 C26 121.17(10) C28 C27 C26 119.88(10) C29 C28 C27 120.50(12) C29 C28 H28 118.9(7) C27 C28 H28 120.6(7) C30 C29 C28 119.94(11) C30 C29 H29 121.5(9) C28 C29 H29 118.5(9) C31 C30 C29 120.16(12) C31 C30 H30 119.4(9) C29 C30 H30 120.4(9) C30 C31 C32 119.80(12) C30 C31 H31 121.4(8) C32 C31 H31 118.8(8) C27 C32 C31 120.66(11) C27 C32 H32 118.3(8) C31 C32 H32 121.1(8) C33 C34 C35 119.93(11) C33 C34 H34 119.6(8) C35 C34 H34 120.5(8) C34 C33 C38 119.35(10) C34 C33 C23 122.86(10) C38 C33 C23 117.67(9) C36 C35 C34 120.38(11) C36 C35 H35 120.6(8) C34 C35 H35 119.0(8) C35 C36 C37 119.94(11) C35 C36 H36 122.2(8) C37 C36 H36 117.9(8) C36 C37 C38 119.91(12) C36 C37 H37 120.8(8) C38 C37 H37 119.3(8) C37 C38 C33 120.49(11) C37 C38 H38 117.8(8) C33 C38 H38 121.7(8) C44 C39 C40 119.25(10) C44 C39 C23 120.75(10) C40 C39 C23 119.82(9) C39 C40 C41 120.20(11) C39 C40 H40 119.4(9) C41 C40 H40 120.4(9) C42 C41 C40 120.24(12) C42 C41 H41 122.5(10) C40 C41 H41 117.3(10) C43 C42 C41 119.73(12) C43 C42 H42 120.8(9) C41 C42 H42 119.4(9) C42 C43 C44 120.30(11) C42 C43 H43 121.2(10) C44 C43 H43 118.5(10) C39 C44 C43 120.26(11) C39 C44 H44 121.6(9) C43 C44 H44 118.1(9) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C2 1.2106(13) O2 C3 1.2242(13) N1 C2 1.3734(14) N1 C3 1.4041(14) N1 C4 1.4586(14) N2 C3 1.3431(14) N2 C1 1.4609(14) N2 H2 0.918(16) C1 C17 1.5296(14) C1 C11 1.5333(15) C1 C2 1.5423(15) C4 C5 1.5099(15) C4 H4A 0.993(14) C4 H4B 1.015(13) C5 C6 1.3895(16) C5 C10 1.3948(16) C6 C7 1.3936(17) C6 H6 1.001(16) C7 C8 1.3885(19) C7 H7 0.967(18) C8 C9 1.3820(19) C8 H8 0.985(15) C9 C10 1.3875(17) C9 H9 0.990(16) C10 H10 0.951(15) C11 C12 1.3883(15) C11 C16 1.3931(16) C12 C13 1.3961(17) C12 H12 0.982(15) C13 C14 1.3787(19) C13 H13 0.993(15) C14 C15 1.3910(19) C14 H14 0.973(15) C15 C16 1.3871(17) C15 H15 0.978(15) C16 H16 1.005(13) C17 C22 1.3908(15) C17 C18 1.3943(16) C18 C19 1.3839(17) C18 H18 1.008(14) C19 C20 1.389(2) C19 H19 0.983(17) C20 C21 1.3823(19) C20 H20 1.009(17) C21 C22 1.3919(16) C21 H21 0.985(15) C22 H22 0.973(13) O3 C24 1.2105(13) O4 C25 1.2256(13) N3 C24 1.3700(14) N3 C25 1.4017(14) N3 C26 1.4691(14) N4 C25 1.3458(14) N4 C23 1.4663(13) N4 H4 0.916(15) C23 C39 1.5282(15) C23 C33 1.5347(15) C23 C24 1.5420(15) C26 C27 1.5089(15) C26 H26A 0.998(13) C26 H26B 0.993(14) C27 C32 1.3883(17) C27 C28 1.3959(16) C28 C29 1.3877(16) C28 H28 0.983(14) C29 C30 1.3872(19) C29 H29 0.995(15) C30 C31 1.3824(19) C30 H30 0.950(15) C31 C32 1.3935(17) C31 H31 0.981(16) C32 H32 0.965(14) C34 C33 1.3904(15) C34 C35 1.3957(16) C34 H34 0.989(15) C33 C38 1.3919(16) C35 C36 1.3795(18) C35 H35 0.990(14) C36 C37 1.3882(17) C36 H36 0.985(14) C37 C38 1.3888(16) C37 H37 0.959(16) C38 H38 1.009(13) C39 C44 1.3899(15) C39 C40 1.3900(16) C40 C41 1.3929(17) C40 H40 0.993(15) C41 C42 1.3860(18) C41 H41 0.951(17) C42 C43 1.3791(19) C42 H42 0.977(15) C43 C44 1.3939(17) C43 H43 0.984(16) C44 H44 0.986(16) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N2 H2 O2 2_665 0.918(16) 1.930(16) 2.8446(13) 173.3(14) N4 H4 O4 2_756 0.916(15) 1.958(15) 2.8613(12) 168.3(14) C8 H8 Cg7 . 0.985(16) 2.987(16) 3.5734(14) 119.3(11) C15 H15 O3 2_766 0.978(15) 2.451(16) 3.3830(17) 159.2(13) C19 H19 Cg7 1_564 0.983(17) 2.732(17) 3.6805(15) 162.4(14) C22 H22 O3 2_666 0.973(13) 2.586(14) 3.3111(15) 131.4(11) C31 H31 Cg3 . 0.981(16) 2.917(15) 3.8944(15) 174.2(12) C41 H41 Cg3 1_546 0.951(17) 2.830(17) 3.6570(15) 146.0(15) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C3 N2 C1 C17 -114.96(10) C3 N2 C1 C11 118.31(10) C3 N2 C1 C2 3.78(11) C3 N1 C2 O1 177.87(10) C4 N1 C2 O1 3.27(16) C3 N1 C2 C1 -2.49(11) C4 N1 C2 C1 -177.09(9) N2 C1 C2 O1 178.98(10) C17 C1 C2 O1 -64.02(14) C11 C1 C2 O1 60.83(13) N2 C1 C2 N1 -0.65(10) C17 C1 C2 N1 116.35(9) C11 C1 C2 N1 -118.81(9) C1 N2 C3 O2 174.03(10) C1 N2 C3 N1 -5.44(12) C2 N1 C3 O2 -174.58(10) C4 N1 C3 O2 0.09(16) C2 N1 C3 N2 4.92(12) C4 N1 C3 N2 179.59(9) C2 N1 C4 C5 -87.88(12) C3 N1 C4 C5 98.14(12) N1 C4 C5 C6 26.89(15) N1 C4 C5 C10 -157.39(10) C10 C5 C6 C7 0.13(17) C4 C5 C6 C7 175.80(11) C5 C6 C7 C8 -0.21(19) C6 C7 C8 C9 -0.05(19) C7 C8 C9 C10 0.38(19) C8 C9 C10 C5 -0.47(18) C6 C5 C10 C9 0.21(17) C4 C5 C10 C9 -175.66(10) N2 C1 C11 C12 -12.47(15) C17 C1 C11 C12 -137.58(11) C2 C1 C11 C12 97.93(12) N2 C1 C11 C16 170.28(10) C17 C1 C11 C16 45.17(13) C2 C1 C11 C16 -79.32(12) C16 C11 C12 C13 -0.44(18) C1 C11 C12 C13 -177.67(11) C11 C12 C13 C14 0.4(2) C12 C13 C14 C15 0.2(2) C13 C14 C15 C16 -0.76(19) C14 C15 C16 C11 0.70(18) C12 C11 C16 C15 -0.10(17) C1 C11 C16 C15 177.20(10) N2 C1 C17 C22 100.75(12) C11 C1 C17 C22 -132.70(11) C2 C1 C17 C22 -10.78(15) N2 C1 C17 C18 -74.61(13) C11 C1 C17 C18 51.94(14) C2 C1 C17 C18 173.85(10) C22 C17 C18 C19 -0.30(19) C1 C17 C18 C19 175.21(12) C17 C18 C19 C20 -1.0(2) C18 C19 C20 C21 1.4(2) C19 C20 C21 C22 -0.5(2) C18 C17 C22 C21 1.23(18) C1 C17 C22 C21 -174.10(11) C20 C21 C22 C17 -0.9(2) C25 N4 C23 C39 -120.60(10) C25 N4 C23 C33 112.22(10) C25 N4 C23 C24 -5.46(11) C25 N3 C24 O3 178.72(10) C26 N3 C24 O3 -6.11(17) C25 N3 C24 C23 -0.65(11) C26 N3 C24 C23 174.52(9) N4 C23 C24 O3 -175.88(10) C39 C23 C24 O3 -57.40(14) C33 C23 C24 O3 67.93(14) N4 C23 C24 N3 3.48(10) C39 C23 C24 N3 121.96(9) C33 C23 C24 N3 -112.71(9) C23 N4 C25 O4 -175.29(10) C23 N4 C25 N3 5.39(12) C24 N3 C25 O4 177.82(9) C26 N3 C25 O4 2.57(16) C24 N3 C25 N4 -2.82(12) C26 N3 C25 N4 -178.07(9) C24 N3 C26 C27 -95.07(12) C25 N3 C26 C27 79.55(12) N3 C26 C27 C32 -107.67(12) N3 C26 C27 C28 70.96(13) C32 C27 C28 C29 -0.20(17) C26 C27 C28 C29 -178.86(11) C27 C28 C29 C30 0.40(18) C28 C29 C30 C31 -0.37(19) C29 C30 C31 C32 0.14(19) C28 C27 C32 C31 -0.04(18) C26 C27 C32 C31 178.61(11) C30 C31 C32 C27 0.06(19) C35 C34 C33 C38 -0.31(17) C35 C34 C33 C23 175.69(10) N4 C23 C33 C34 -107.02(12) C39 C23 C33 C34 126.03(11) C24 C23 C33 C34 3.45(15) N4 C23 C33 C38 69.04(13) C39 C23 C33 C38 -57.91(13) C24 C23 C33 C38 179.52(10) C33 C34 C35 C36 0.12(18) C34 C35 C36 C37 0.12(19) C35 C36 C37 C38 -0.2(2) C36 C37 C38 C33 -0.02(19) C34 C33 C38 C37 0.26(18) C23 C33 C38 C37 -175.94(11) N4 C23 C39 C44 23.53(15) C33 C23 C39 C44 148.79(11) C24 C23 C39 C44 -86.81(12) N4 C23 C39 C40 -161.42(10) C33 C23 C39 C40 -36.16(14) C24 C23 C39 C40 88.24(12) C44 C39 C40 C41 0.13(19) C23 C39 C40 C41 -174.99(12) C39 C40 C41 C42 0.7(2) C40 C41 C42 C43 -1.1(2) C41 C42 C43 C44 0.6(2) C40 C39 C44 C43 -0.63(19) C23 C39 C44 C43 174.45(11) C42 C43 C44 C39 0.3(2) _cod_database_fobs_code 1548674